Iluka Resources Limited Mineral Sands By-Product Disposal

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Iluka Resources Limited Mineral Sands By-Product Disposal Planning Permit 15-105 Crown Allotments 91, 94, 95, 96 Parish of Telangatuk Environmental Management Plan and Rehabilitation Performance Report – H1 2020 Iluka Ref: UDOCS 0090-426461582-1177 Contact: Ian Williams Environment Superintendent, Murray Basin [email protected]

Transcript of Iluka Resources Limited Mineral Sands By-Product Disposal

Iluka Resources Limited Mineral Sands By-Product Disposal

Planning Permit 15-105

Crown Allotments 91, 94, 95, 96

Parish of Telangatuk

Environmental Management Plan and Rehabilitation Performance Report – H1 2020

Iluka Ref: UDOCS 0090-426461582-1177

Contact: Ian Williams

Environment Superintendent, Murray Basin [email protected]

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

i

Document control

Revision Details of review or changes Prepared by Date created

A Draft S. Alexander 25-03-2020

0 Final S. Alexander 18-09-2020

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

ii

Table of contents 1 EXECUTIVE SUMMARY ....................................................................................................... 5 2 INTRODUCTION ................................................................................................................... 6

2.1 PLANNING PERMIT 15-105 ......................................................................................................... 6 2.2 COMMENCEMENT OF THE PERMIT .......................................................................................... 6 2.3 ENDORSED PLANS ...................................................................................................................... 9 2.4 PERFORMANCE REPORTING .................................................................................................... 9 2.5 REHABILITATION AND VEGETATION MANAGEMENT PLAN ................................................. 10

3 DELIVERY AND DISPOSAL OF MATERIALS INTO PIT 23 ............................................... 10 4 MONITORING RESULTS .................................................................................................... 10

4.1 GROUNDWATER ........................................................................................................................ 10 4.2 SURFACE WATER QUALITY ..................................................................................................... 31 4.3 NOISE .......................................................................................................................................... 35 4.4 PM10 CONCENTRATIONS IN AIR .............................................................................................. 35 4.5 RADIATION MONITORING – OTHER ........................................................................................ 37

5 MANAGEMENT ACTIONS .................................................................................................. 41 5.1 MONITORING BORE AUDITS .................................................................................................... 41 5.2 GROUNDWATER FLOW PATHS FROM PIT 23 ........................................................................ 41 5.3 GROUNDWATER MODEL REVIEW AND RECALIBRATION .................................................... 43 5.4 MAXIMUM SURFACE LEVEL OF DISPOSED MATERIALS IN PIT 23 ..................................... 43 5.5 NON-COMPLIANCES ................................................................................................................. 43 5.6 COMMENTS AND COMPLAINTS RECEIVED ........................................................................... 43 5.7 H1 2020 COMPLETED ACTIONS ............................................................................................... 43 5.8 H2 2020 PROPOSED ACTIONS ................................................................................................. 43 5.9 OTHER MATTERS ...................................................................................................................... 44

6 REFERENCES .................................................................................................................... 45 7 APPENDICES ...................................................................................................................... 46

APPENDIX A: MONITORING DATA (LAB) – RADIATION – SURFACE WATER ................................ 46 APPENDIX B: MONITORING DATA (LAB) – GROUNDWATER .......................................................... 47 APPENDIX C: MONITORING DATA (FIELD) – GROUNDWATER ...................................................... 79 APPENDIX D: MONITORING DATA (LAB) – SURFACE WATER ....................................................... 98 APPENDIX E: MONITORING DATA (FIELD) – SURFACE WATER .................................................. 104

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

iii

List of tables Table 1: Pit 23 bore status (as at 30/06/2020) ................................................................................................. 10

Table 2: Monitoring bores - standing water Levels (mAHD) ............................................................................ 13

Table 3: Groundwater monitoring locations – ionic ratio balance results ......................................................... 16

Table 4: Groundwater radionuclide concentrations vs. ionic balance ratios, H1 2020 .................................... 20

Table 5: Groundwater quality exceedances vs ionic balance ratios, H1 2020 ................................................. 30

Table 6:Selenium groundwater trigger levels for GW01, H1 2020 ................................................................... 30

Table 7: Surface water monitoring - ionic ratio balance results ........................................................................ 32

Table 8: Monitoring program – radionuclide concentrations in surface water .................................................. 34

Table 9: Radon concentrations within Pit 23 for H1 2020 ................................................................................ 38

Table 10: Thoron concentrations within Pit 23 for H1 2020 ............................................................................. 38

Table 11: Gross Alpha radiation in PM10 dust .................................................................................................. 40

List of figures Figure 1: Douglas Mine and Pit 23 regional location .......................................................................................... 7

Figure 2: Pit 23 location ...................................................................................................................................... 8

Figure 3: Pit 23 updated groundwater monitoring network (as at 31/12/2019) ................................................ 12

Figure 4: Groundwater elevation (mAHD) – bores in predicted flow path ........................................................ 14

Figure 5: Groundwater elevation (mAHD) – bores up-gradient of Pit 23 ......................................................... 14

Figure 6: Groundwater elevation (mAHD) – cross-gradient and background bores ........................................ 15

Figure 7: U-238 and ionic balance trends – up-gradient bores (1 of 2) ............................................................ 26

Figure 8: U-238 and ionic balance trends – up-gradient bores (2 of 2) ............................................................ 26

Figure 9: Ra-228 and ionic balance trends – up-gradient bores (1 of 2) .......................................................... 26

Figure 10: Ra-228 and ionic balance trends – up-gradient bores (2 of 2) ........................................................ 26

Figure 11: U-238 and ionic balance trends – down-gradient bores (1 of 2) ..................................................... 27

Figure 12: U-238 and ionic balance trends – down-gradient bores (2 of 2) ..................................................... 27

Figure 13: Ra-228 and ionic balance trends – down-gradient bores (1 of 2) ................................................... 27

Figure 14: Ra-228 and ionic balance trends – down-gradient bores (2 of 2) ................................................... 27

Figure 15: U-238 and ionic balance trends – cross-gradient bores (1 of 2) ..................................................... 28

Figure 16: U-238 and ionic balance trends – cross-gradient bores (2 of 2) ..................................................... 28

Figure 17: Ra-228 and ionic balance trends – cross-gradient bores (1 of 2) ................................................... 28

Figure 18: Ra-228 and ionic balance trends – cross-gradient bores (2 of 2) ................................................... 28

Figure 19: U-238 and ionic balance trends – bores representing background (1 of 2) .................................... 29

Figure 20: U-238 and ionic balance trends – bores representing background (2 of 2) .................................... 29

Figure 21: Ra-228 and ionic balance trends – bores representing background (1 of 2) .................................. 29

Figure 22: Ra-228 and ionic balance trends – bores representing background (2 of 2) .................................. 29

Figure 23: GW01 - Selenium as compared against ionic balance trends ........................................................ 31

Figure 24: Ra-226 and Ra-228 in surface water .............................................................................................. 34

Figure 25: Uranium and U-238 in surface water .............................................................................................. 35

Figure 26: PM10 dust concentrations at neighbouring residences vs. daily rainfall .......................................... 36

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

iv

Figure 27: Pit 23 air quality (PM10) monitoring locations .................................................................................. 36 Figure 28: Radon and thoron detectors ........................................................................................................... 37

Figure 29: Radon concentration in air, H1 2020 .............................................................................................. 39

Figure 30: Thoron concentration in air, H1 2020 ............................................................................................. 39

Figure 31: Gross Alpha Radiation in PM10 Dust – H1 2020............................................................................ 40

Figure 32: 2019 vs 2020 interpreted groundwater contours (EMM 2019; EMM 2020) .................................... 42

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

5

1 Executive Summary Iluka Resources Limited (Iluka) operates the Pit 23 by-products disposal facility located at the Douglas Mine in the Kanagulk area and within the municipality of the Horsham Rural City. Pursuant to Planning Permit 15-105 issued by Horsham Rural City Council (HRCC), and the subsidiary Pit 23 Incoming Waste Monitoring Plan (IWMP), the Pit 23 facility is approved for the disposal of mineral separation by-products and used dust filter bags from the Iluka Hamilton Mineral Separation (MSP) which contain or are contaminated with Naturally Occurring Radioactive Material (NORM), and concrete and steel which contains or is contaminated with NORM associated with plant and infrastructure from nominated Iluka sites within Victoria.

Complementing the IWMP are the endorsed Pit 23 Environmental Management Plan (EMP) which addresses the identification, management and monitoring of environmental risks associated with the approved development and use; and the endorsed Rehabilitation and Vegetation Management Plan (R&VMP) which addresses the future rehabilitation of the Pit 23 facility including infrastructure decommissioning, landform reinstatement and end land use. This report is submitted in accordance with Section 12.2 of the endorsed Iluka Pit 23 EMP and outlines the results of monitoring and management actions undertaken during the period 1st January 2020 to 30th June 2020. Key commentary on environmental monitoring outcomes and performance against compliance objectives in the Pit EMP for the H1 2020 reporting period:

• There were no exceedances of applicable limits for radionuclides or any other analytes in groundwater in bores down-gradient of Pit 23 attributable to disposal activities;

• There were no surface water discharges from the Pit 23 disturbance area;

• There were no exceedances of applicable limits for radionuclides or any other analytes in groundwater-fed surface water sites down-gradient of Pit 23 attributable to disposal activities;

• No noise complaints were received;

• There were no exceedances of the PM10 limit attributable to Pit 23 operations; • There were no exceedances of the air concentration limits for radon or thoron;

• Measured concentrations of gross alpha radiation in airborne dust were within the range of historical values; and

• Updated groundwater level contours and flow-paths show no material change from the hydrogeological model contours developed in 2015 by CDM Smith.

Detailed assessment of compliance, key results and management actions are provided in Section 4 and 5 of the enclosed report.

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

6

2 Introduction Iluka Resources Limited (Iluka) operates the Pit 23 by-products disposal facility located at the Douglas Mine in the Kanagulk area and within the municipality of the Horsham Rural City (Figure 1 and Figure 2).

Pursuant to Planning Permit 15-105 issued by Horsham Rural City Council (HRCC), and the subsidiary Pit 23 Incoming Waste Monitoring Plan (IWMP), the Pit 23 facility is approved for the disposal of mineral separation by-products and used dust filter bags from the Iluka Hamilton Mineral Separation (MSP) which contain or are contaminated with Naturally Occurring Radioactive Material (NORM), and concrete and steel which contains or is contaminated with NORM associated with plant and infrastructure from nominated Iluka sites within Victoria.

2.1 Planning Permit 15-105

Under the Horsham Planning Scheme the subject land is in the Farming Zone and under the provisions of that zone a permit is required for use and development for Industry (Refuse Disposal). On 25th February 2017 Planning Permit 15-105, (the Permit) was issued by the Horsham Rural City Council as the Responsible Authority to allow:

Use and development of the land for the disposal of waste by-products associated with or sourced through mineral sands processing undertaken at the Hamilton Mineral Separation Plant (MSP), including waste by-products and contaminated materials resulting from the processing and transport operations as follows:

o By-products from the processing of heavy mineral concentrate at the Hamilton MSP;

o used dust filter bags from the Hamilton MSP; and

o Other chemically inert material contaminated with naturally occurring radioactive material.

in accordance with the endorsed plans.

2.2 Commencement of the Permit

Condition 1 of the Permit states: This permit does not come into operation until:

a. Iluka has applied to the Department of Economic Development, Jobs, Transport and Resources to vary the 2003 Work Plan to identify a new endues utilisation of Pit 23 and to vary the rehabilitation plan; and

b. Iluka has applied to the Minister to surrender part of MIN 5367 (Pit 23); and

c. The Department of Economic Development, Jobs, Transport and Resources has approved the Work Plan Variation; and

d. The Minister has registered the partial surrender of MIN 5367.

The permit comes into operation on the same day the Work Plan Variation is approved, and the partial surrender of MIN 5367 is registered.

The Variation to the 2003 Douglas Mine Work Plan was approved on the 13th April 2017, and the partial surrender of MIN5367 was registered on 11th May 2017, this being the date of commencement of the Permit.

QUANTONG NATIMUK

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5900000 5900000

HRCC-PP-15-105 MIN5367

TELANGATUK EAST

HARROW

N

Black Range State Park

0 2.5 5 km 5880000

Map Projection: MGA Zone 54

Legend

Douglas mine

Pit 23

HRCC-PP-15-105

MIN5367 tenement

DOUGLAS LOCATION PLAN

ORIG:

N.Travers

DRAWN: D.G.S.

SCALE: 1:250,000

(A4)

DATE: May 2018

DWG No:

247670 ver.00 FIGURE: 1

NATIMUK FRANCES ROAD

580000

560000

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00

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D A O R S E I N H C

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Pit 10

Pit 23 Pit 9

Pit 22

Pit 5

Pit 21

Pit 12

N Pit 11

Pit 19

Pit 2 Pit 3

Pit 1

Legend

Pit 23 haul road 0 Mine Access Road Truck wash circuit Pit 23 crest Pit Crests

Roads

250

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community

Meters

500 1,000 1,500 2,000

LOCATION OF PIT 23

L:\Maps\2018\Unregistered\Douglas\mxd\Pit 23 Annual Report 2017

DRAWN: N. Travers

DATE:26/06/2018 FIGURE: 2

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

9

2.3 Endorsed Plans

Conditions 2, 3, 9, 14, 16 and 34 of the Permit relate to various management plans that once approved by the Responsible Authority will be endorsed to form part of the Permit, which includes:

• Incoming Waste Monitoring Plan (IWMP);

• Environmental Management Plan (EMP), incorporating; o Groundwater Monitoring and Management Plan (GWMMP); o Surface Water Monitoring and Management Plan (SWMMP); o Air Quality/Dust Control Plan (AQMP); and

• Rehabilitation and Vegetation Management Plan (R&VMP) The plans were endorsed by Horsham Rural City Council on 17th July 2017.

2.4 Performance reporting

Section 12.2 of the endorsed EMP (Rev 4, July 2017) outlines the routine reporting requirements for the mineral sands by-product disposal operations which are:

A review of the performance will be completed and an EMP and Rehabilitation Performance report prepared annually, or less frequently as may be agreed with the Responsible Authority.

Each EMP and Rehabilitation Performance Report will include, at least:

• for the period from the previous EMP and Rehabilitation Performance Report:

o the total tonnage of materials disposed of;

o the average and maximum number of deliveries of materials disposed of per day; and

o the results of all measurements of:

noise levels made in response to a complaint regarding noise;

PM10 concentrations in air at sensitive receptors;

environmental radiation monitoring results in accordance with the approved Radiation Management Plan, which will generally include:

- radon concentration in air;

- gross alpha activity concentration of airborne dust; and

- radionuclide concentrations in groundwater and surface water;

discussion of any implications of the results of groundwater level monitoring on groundwater flow paths from Pit 23; and

descriptions of any model review and recalibration completed and the results of subsequent model re-runs;

• the maximum elevation of the upper surface of materials disposed of at the end of the reporting period;

• a detailed discussion of all non-compliant events including progress toward resolution;

• a summary of comments and complaints received and resulting actions;

• plans for the next year; and

• discussion on other matters considered relevant by the Responsible Authority or Iluka.

Deficiencies identified in an EMP and Rehabilitation Performance Report that can be addressed without amendment of this plan will be addressed as soon as practicable.

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

10

Per Section 13.2 of the EMP, the EMP and Rehabilitation Performance Reports will be subject to review by an independent auditor prior to submission to the Responsible Authority.

2.5 Rehabilitation and Vegetation Management Plan

Due to continued operations within Pit 23 no actions relevant to rehabilitation and vegetation management were undertaken in the H1 2020 reporting period.

3 Delivery and Disposal of Materials into Pit 23 No wastes were disposed into Pit 23 during the H1 2020 reporting period.

4 Monitoring Results 4.1 Groundwater

4.1.1 Bore network status The Pit 23 bore network includes several new monitoring bores installed in 2018 per the recommendations in the independent desktop review of proposed by-product disposal (EES, 2016). The augmented bore network therefore satisfies Condition 28(c) of the Permit. The status of Pit 23 monitoring bore network is given in Table 1. The blocked monitoring bore (BW36) has been decommissioned and replaced with a new monitoring bore (BW36A) which was installed in October 2019. Consistent with Section 7.6.3 the replacement bore (“BW36A”) was installed by a licensed driller pursuant to a ‘Licence to Construct Works’ (Works Licence WLE074849) issued by GWM Water. As per Condition 28(d) of the Permit, bore installation was supervised by qualified hydrogeologist. Bore locations are provided in Figure 3.

Table 1: Pit 23 bore status (as at 30/06/2020)

Well ID Comment Status / Condition

BORES UP-GRADIENT OF PIT 23 WRK301 OK WRK302 OK WRK303 OK WRK304 OK GW08 Installed 18/10/18 OK GW06 Installed 23/5/18 OK GW05 Installed 17/10/18 OK BORES DOWN-GRADIENT OF PIT 23 (IN PREDICTED FLOW PATH) BW36 Decommissioned in October 2019 Blocked BW36A Installed 15/10/19 To replace BW36 WRK300 OK GW01 Installed 23/5/18 OK GW02 Installed 17/10/18 OK GW03 Installed 17/10/18 OK BW5 In predicted flow path OK BORES CROSS-GRADIENT TO PIT 23 FLOW PATH GW04* Installed 18/10/18 OK

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

11

Well ID Comment Status / Condition

GW07 Installed 23/5/18 OK BW28A * OK BW45B Installed 18/10/18 – replaced BW45 OK BORES REPRESENTATIVE OF BACKGROUND IWB2 Representative of background OK IWB6 Representative of background OK BW53 (“Puls”) Representative of background OK * BW28A and GW04 are incorrectly referenced in the current endorsed EMP (Rev 4, July 2017) as being down-gradient of Pit 23. Groundwater modelling per CDM Smith (2014) and EMM (2019) indicate that BW28A and GW04 are cross-gradient to the predicted flow path from Pit 23.

Legend Pit 23

Pit 23 Particle Tracks

Bore Position/Purpose

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Background

Cross-gradient

Down-gradient

Up-gradient

Proposed bore

White Lake

BW5

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Bitter Swamp

McGlashin Swamp

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Ti Tree Swamp

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GW03

BW53 (Puls)

GW02

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GW01

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BW36

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WRK300 (!

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GW04 !(

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GW07

BW45B GW05 WRK301

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IWB6

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WRK303

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WRK304

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WRK302 !(

GW06

!(

IWB2

N Site photo: 5 Oct. 2018

DOUGLAS MINE

GW08

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0 500 1,000 m

PIT 23 MONITORING BORE NETWORK & GROUNDWATER FLOW PATH

ORIG:

S.Alexander

DRAWN: D.G.S.

SCALE: 1:25,000

(A3)

DATE: June 2020

DWG No: 257184 ver.01 FIGURE: 3

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

4.1.2 Standing water levels In accordance with Section 7.9.1 of the current endorsed EMP (Rev 4, July 2017) groundwater levels are measured on a monthly basis at bores WRK300 – WRK304 inclusive, GW01 to GW08 inclusive and BW36A and BW45B. All other bores (BW5, BW28A, BW53, IWB2 and IWB6) are measured on a biannual basis. Groundwater level hydrographs for these bores expressed in groundwater elevation (metres above Australian Height Datum, mAHD) are given in Table 2 and Figure 4 – Figure 6. Data includes that obtained during scheduled events and ad-hoc measurements. All bores along the predicted flow path (Figure 4) exhibit stable standing water levels in the preceding 24-month period and in comparison to long-term trends; bores up-gradient of Pit 23 (Figure 5) exhibit relatively stable water levels with minor fluctuation.

Table 2: Monitoring bores - standing water Levels (mAHD)

Bore ID Jan-20 Feb-20 Mar-20 Apr-20 May-20 Jun-20

BORES UP-GRADIENT OF PIT 23

GW05 179 178.94 178.98 178.84 178.9 178.96

GW06 176.22 176.13 176.22 176.24 176.20 176.26

GW08 177.66 177.5 177.63 177.37 177.49 177.6

WRK301 178.18 178.16 178.2 178.29 178.16 178.15

WRK302 176.59 176.67 176.62 176.68 176.7 176.67

WRK303 179.52 179.8 179.83 179.85 179.83 179.79

WRK304 180.36 180.29 180.35 180.25 180.5 180.36

BORES DOWN-GRADIENT OF PIT 23 (IN PREDICTED FLOW PLATH)

BW05 147.30 147.46 * * * *

WRK300 175.04 175 175.05 175.01 175.11 175.06

BW36A 174.53 174.51 174.54 174.23 174.34 174.41

GW01 173.44 173.41 173.43 173.60 173.53 173.50

GW02 170.81 170.79 170.76 170.65 170.81 170.71

GW03 162.07 162.14 162.12 161.89 161.99 161.97

BORES CROSS GRADIENT TO PIT 23 FLOW PATH

BW28A 152.68 152.46 * * * *

BW45B 177.38 177.31 177.35 177.37 177.36 177.34

GW04 178.39 178.38 178.43 178.12 178.24 178.2

GW07 172.43 172.47 172.46 172.44 172.47 172.43

BORES REPRESENTATIVE OF BACKGROUND

IWB2 179.70 179.67 * * * *

IWB6 176.74 176.82 * * * *

BW53 ("Puls") 175.83 175.84 * * * * Notes

• bores are listed according to their position relative to the Pit 23 groundwater flow path • bores down-gradient (on predicted flow path) are listed in order of their position along the path of flow • dates marked with an asterisk (*) indicates no scheduled sampling required

13

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

14

Figure 4: Groundwater elevation (mAHD) – bores in predicted flow path

Figure 5: Groundwater elevation (mAHD) – bores up-gradient of Pit 23

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

15

Figure 6: Groundwater elevation (mAHD) – cross-gradient and background bores

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

16

4.1.3 Groundwater quality

4.1.3.1 Ionic balance ratios Per Section 7.9.2 of the current endorsed EMP (Revision 4, July 2017) chloride:sulfate (CL:SO4) and sodium:calcium (Na:Ca) ratios in groundwater are assessed from results obtained during scheduled and/or follow-up groundwater sampling events. Per the EMP, a consecutive reduction in either ratio of >10% applies as a potential indicator of seepage from Pit 23 having arrived in a bore and is a trigger for further investigation. Per the EMP, further investigation would include:

• comparing the timing of the consecutive >10% reduction in ionic ratios with the hydrogeological model predictions;

• comparing the timing of the ionic balance trigger with other analytes (e.g. radionuclides, heavy metals) to identify any corresponding exceedances in those analytes in the same rounds of sampling;

• where such a correlation exists completing a detailed investigation of cause and impact, including possible reviews of hydrogeological or solute transport models.

Calculated Cl:SO4 and Na:Ca for the reporting period are given in Table 3. As above, this includes ratios as determined from the results of scheduled and follow-up sampling. Reductions of >10% in one or both ratios in consecutive and/or follow-up sampling events occurred on one (1) occasion in the reporting period in a bore (GW01) down-gradient to Pit 23: As detailed further in Section 4.1.3.3, the ionic balance trigger corresponded with an elevated Selenium result, however, this result is below the precautionary limit based on background values which have naturally elevated concentrations at GW01 and are above the standard SEPP WoV objectives. These observations are not considered to be associated with Pit 23.

Table 3: Groundwater monitoring locations – ionic ratio balance results

Bore ID

Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (Ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (Ratio)

% Red.

Repeated ratio

exceedance? BORES UP-GRADIENT OF PIT 23 GW05 28/11/2018 3100 560 5.5 I.D. 1800 170 10.6 I.D.

15/01/2019 3800 790 4.8 13% 2200 200 11.0 -4%

19/02/2019 3700 740 5.0 10% 2000 180 11.1 -5%

8/07/2019 3100 660 4.7 2% 1900 140 13.6 -23%

15/01/2020 2600 640 4.0 14% 1700 81 20.9 -55% 20/02/2020 2800 620 4.5 4% 1900 87 21.8 -61%

GW06 12/06/2018 6600 1500 4.4 I.D. 3400 660 5.2 I.D.

14/01/2019 6700 1700 3.9 10% 3400 630 5.4 -5%

21/03/2019 6800 1600 4.3 3% 3400 620 5.5 -6%

17/04/2019 7000 1500 4.7 -18% 3500 640 5.5 -1%

22/05/2019 6800 1400 4.9 -23% 3400 670 5.1 6%

18/06/2019 6800 1500 4.5 -15% 3400 580 5.9 -9%

4/07/2019 6800 1500 4.5 -15% 3500 610 5.7 -6%

22/01/2020 6000 1600 3.8 17% 3400 610 5.6 3% 24/02/2020 6700 1500 4.5 1% 3400 600 5.7 1%

GW08 29/11/2018 5300 1100 4.8 I.D. 2800 390 7.2 I.D.

14/01/2019 6600 1300 5.1 -5% 3200 540 5.9 17%

18/02/2019 6700 1400 4.8 1% 3300 540 6.1 15% Yes (Na:Ca) 10/07/2019 6700 1200 5.6 -10% 3600 550 6.5 -10%

20/01/2020 6500 1300 5 10% 3400 520 6.5 0% 25/02/2020 6700 1300 5.2 8% 3600 540 6.7 -2% 5/05/2020 6800 1300 5.2 6% 3800 400 9.5 -45%

26/07/2017 3100 640 4.8 I.D. 1600 240 6.7 I.D.

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

17

Bore ID

Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (Ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (Ratio)

% Red.

Repeated ratio

exceedance?

WRK301

11/01/2018 3100 650 4.8 2% 1700 250 6.8 -2%

10/07/2018 3100 480 6.5 -35% 1700 260 6.5 4%

21/01/2019 3400 670 5.1 21% 1700 290 5.9 10%

18/02/2019 3400 690 4.9 24% 1700 260 6.5 0% Yes (CL:SO4) 15/07/2019 3200 570 5.6 -11% 1700 230 7.4 -26%

22/01/2020 3100 600 5.2 8% 1700 260 6.5 12%

25/02/2020 3200 600 5.3 5% 1800 270 6.7 10%

WRK302 10/07/2018 6500 1300 5.0 -15% 3500 520 6.7 8%

14/01/2019 6500 1500 4.3 13% 3500 490 7.1 -6%

18/02/2019 6700 1400 4.8 4% 3300 540 6.1 9%

21/03/2019 6600 1500 4.4 12% 3500 490 7.1 -6%

17/04/2019 6600 1300 5.1 -2% 3400 530 6.4 5%

22/05/2019 6700 1300 5.2 -3% 3500 510 6.9 -2%

4/07/2019 6400 1400 4.6 -5% 3600 460 7.8 -10%

1/08/2019 6500 1400 4.6 -7% 3400 480 7.1 1%

20/01/2020 6200 1500 4.1 10% 3500 460 7.6 3% WRK303 25/07/2017 2100 570 3.7 I.D. 1200 93 12.9 I.D.

11/01/2018 2100 550 3.8 -4% 1300 97 13.4 -4%

10/07/2018 2400 570 4.2 -10% 1400 110 12.7 5%

14/01/2019 2500 620 4.0 4% 1500 130 11.5 9%

15/07/2019 2700 570 4.7 -17% 1600 120 13.3 -16%

23/01/2020 2700 560 4.8 -2% 1800 140 12.9 4% WRK304 10/07/2018 2200 640 3.4 0% 1400 93 15.1 -3%

14/01/2019 2200 680 3.2 6% 1400 87 16.1 -7%

15/07/2019 2400 640 3.8 -16% 1500 94 16.0 1%

22/01/2020 2500 700 3.6 5% 1700 100 17.0 -7%

5/03/2020 2500 640 3.9 -4% 1600 110 14.5 9%

BORES DOWN-GRADIENT OF PIT 23 BW05 18/10/2018 8800 800 11.0 -23% 4900 260 18.8 -11%

17/01/2019 8300 960 8.6 17% 4500 290 15.5 35%

20/03/2019 8400 890 9.4 10% 4700 260 18.1 24% Yes (Na:Ca) 3/07/2019 8300 860 9.7 -12% 4600 240 19.2 -24%

13/01/2020 7800 870 9.0 7% 4700 240 19.6 -2%

BW36 12/07/2017 2200 420 5.2 I.D. 1300 74 17.6 I.D.

10/01/2018 2000 360 5.6 -6% 1200 82 14.6 17%

6/03/2018 1900 360 5.3 -1% 1100 61 18.0 -3%

Bore blocked - replaced with BW36A in Oct 2019 11/12/19 1200 160 7.5 I.D. 760 76 10.0 I.D.

16/01/20 1200 90 13.33 -78% 770 69 11.2 -12%

GW01 7/06/2018 930 110 8.5 I.D. 490 82 6.0 I.D.

15/01/2019 3400 400 8.5 -1% 1800 65 27.7 -363%

20/03/2019 3500 420 8.3 2% 2000 68 29.4 -6%

15/04/2019 3700 370 10.0 -18% 1900 75 25.3 9%

14/05/2019 3400 360 9.4 -11% 2100 64 32.8 -18%

18/06/2019 3400 420 8.1 5% 1800 56 32.1 -16%

8/07/2019 3400 400 8.5 0% 1900 58 32.8 -18%

15/01/2020 3500 470 7.4 12% 1900 92 20.7 37%

20/02/2020 3400 450 7.6 11% 1900 73 26.0 21% Yes (Both) GW02 28/11/2018 2100 410 5.1 I.D. 1300 38 34.2 I.D.

15/01/2019 2000 330 6.1 -18% 1200 26 46.2 -35%

10/07/2019 2300 330 7.0 -15% 1300 21 61.9 -34%

14/01/2020 2100 340 6.2 11% 1200 19 63.2 -2%

3/03/2020 2000 290 6.9 1% 1200 17 70.6 -14%

GW03 28/11/2018 2900 510 5.7 I.D. 1800 190 9.5 I.D.

15/01/2019 3100 590 5.3 8% 1900 270 7.0 26%

19/02/2019 3500 630 5.6 2% 1800 180 10.0 -6%

10/07/2019 3400 540 6.3 -20% 1900 170 11.2 -59%

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

18

Bore ID

Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (Ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (Ratio)

% Red.

Repeated ratio

exceedance? 14/01/2020 3300 550 6 5% 1800 160 11.3 -1%

WRK300 10/01/2018 1700 320 5.3 6% 1000 150 6.7 13%

6/03/2018 1700 330 5.2 8% 920 130 7.1 8%

17/07/2018 1600 290 5.5 -4% 880 140 6.3 6%

18/10/2018 1700 310 5.5 -3% 910 130 7.0 -5%

21/01/2019 1800 300 6.0 -9% 910 150 6.1 3%

18/02/2019 1700 330 5.2 7% 910 130 7.0 -11%

21/03/2019 1800 310 5.8 -5% 1000 180 5.6 12%

17/04/2019 1800 290 6.2 -13% 970 150 6.5 -3%

16/07/2019 1700 300 5.7 6% 990 130 7.6 -26%

16/01/2020 1700 310 5.5 3% 1100 150 7.3 4%

BORES CROSS-GRADIENT OF PIT 23 BW28A * 20/08/2018 7200 870 8.3 -14% 3600 510 7.1 7%

17/01/2019 7100 1000 7.1 9% 3500 540 6.5 2%

18/02/2019 7200 1100 6.5 16% 3400 490 6.9 -5%

3/07/2019 7100 920 7.7 -9% 3600 500 7.2 -11%

13/01/2020 6900 960 7.2 7% 3400 460 7.4 -3%

26/02/2020 7000 850 8.2 -7% 3600 490 7.3 -2%

BW45B 29/11/2018 4800 840 5.7 I.D. 2500 290 8.6 I.D.

17/01/2019 5100 960 5.3 7% 2500 320 7.8 9%

6/03/2019 5100 910 5.6 2% 2500 310 8.1 6%

20/03/2019 5300 960 5.5 3% 2700 320 8.4 2%

15/04/2019 5400 810 6.7 -17% 2600 300 8.7 -1%

14/05/2019 5100 870 5.9 -3% 2900 320 9.1 -5%

18/06/2019 5300 860 6.2 -8% 2700 290 9.3 -8%

8/07/2019 5000 860 5.8 -9% 2800 310 9.0 -16%

14/08/2019 4900 860 5.7 -7% 2600 320 8.1 -4%

15/01/2020 4900 920 5.3 8% 2800 320 8.8 3%

26/02/2020 5100 810 6.3 -8% 2700 300 9.0 0%

GW04 * 28/11/2018 2700 690 3.9 I.D. 1700 120 14.2 I.D.

15/01/2019 2800 720 3.9 1% 1900 110 17.3 -22%

8/07/2019 2800 640 4.4 -13% 1700 120 14.2 18%

1/08/2019 3000 570 5.3 -35% 1600 140 11.4 34% Yes (Na:Ca)

12/09/2019 2900 680 4.3 -10% 1700 130 13.1 24% Yes (Na:Ca)

15/01/2020 2900 520 5.6 -27% 1600 140 11.4 19%

20/02/2020 2800 540 5.2 -19% 1700 130 13.1 8%

GW07 7/06/2018 5500 890 6.18 I.D. 3000 460 6.522 I.D.

17/01/2019 5700 1100 5.18 16% 2900 560 5.179 21%

19/02/2019 5700 1000 5.70 8% 2800 410 6.829 -5%

21/03/2019 5900 990 5.96 4% 3100 440 7.045 -8%

3/07/2019 5800 880 6.59 -27% 3100 390 7.949 -53%

9/01/2020 5700 1000 5.7 14% 3100 400 7.8 3%

26/02/2020 5600 890 6.3 5% 3100 390 7.9 0%

BORES REPRESENTATIVE OF BACKGROUND IWB2 18/10/2018 1200 160 7.5 6% 670 11 60.9 -7%

10/01/2019 1200 160 7.5 0% 660 11 60.0 7%

11/07/2019 1200 170 7.1 6% 650 9.2 70.7 -18%

14/01/2020 1200 160 7.5 -6% 670 9.7 69.1 2%

IWB6 3/07/2018 350 200 1.8 3% 300 6.7 44.8 -5%

10/01/2019 360 220 1.6 6% 290 6.3 46.0 -3%

11/07/2019 350 190 1.8 -13% 300 6 50.0 -9%

14/01/2020 330 250 1.3 28% 340 7.2 47.2 6%

20/02/2020 340 190 1.8 3% 310 6.3 49.2 2%

BW53 (Puls)

3/07/2018 790 270 2.9 -22% 530 34 15.6 -173%

10/01/2019 570 230 2.5 15% 350 37 9.5 39%

19/02/2019 860 330 2.6 11% 520 43 12.1 22% Yes (Both) 10/07/2019 840 310 2.7 -9% 530 29 18.3 -93%

13/01/2020 750 310 2.4 11% 500 29 17.2 6% 26/02/2020 770 310 2.5 8% 520 31 16.8 8%

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

19

Bore ID

Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (Ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (Ratio)

% Red.

Repeated ratio

exceedance? NOTES

• Calculated ratios in green represent values that increase following an initial “>10%” reduction (i.e. no consecutive >10% reduction)

• Calculated ratios in red represent values above the “>10%” reduction threshold (initial identified exceedance). • Calculated ratios in red highlight represent a confirmed “>10%” reduction in consecutive or follow-up samples • I.D. = insufficient data to allow calculation of ionic ratio (only one data-point available) • GW04 has previously been incorrectly referenced as being down gradient of Pit 23. Groundwater modelling and particle

tracking per EMM (2019) indicate that GW04 is cross-gradient to the predicted groundwater flow path from Pit 23. • BW28A is incorrectly referenced in the EMP (Revision 4) as being down-gradient of Pit 23. Groundwater modelling and

particle tracking per CDM Smith (2014) and EMM (2019) indicate that BW28A is cross-gradient to the predicted groundwater flow path from Pit 23.

4.1.3.2 Radionuclide concentrations In accordance with Section 7.6.7 of the EMP, biannual groundwater samples obtained from the monitoring locations are subjected to in-field and laboratory analysis for a suite of target parameters, which includes target radionuclides (Thorium, Uranium, Radium-226, Radium-228 and Uranium- 238). Radionuclide concentrations determined during both scheduled and follow-up sampling are presented in Table 4. Ionic balance ratios are also shown to identify any potential correlation with seepage from Pit 23. In summary:

• several exceedances of the Uranium-238 (U-238) and Radium-228 (Ra-228) upper trigger levels were observed in the reporting period in several bores up-gradient and cross-gradient to Pit 23 (i.e. in bores not on the predicted flow path or which represent local background conditions);

• ionic balance ratios showed frequent fluctuation spatially and temporally, and between samples obtained over relatively short time periods, with no correlation to radionuclide concentrations. This suggests that the measured radionuclide concentrations and ‘exceedances’ are the product of natural variation, consistent with the findings of previous groundwater studies for the greater Douglas site (Jacobs 2014; CDM Smith 2014; EMM 2018).

The long-term trends in Ra-228 and U-238 concentrations verses ionic balance ratios are shown in Figure 7 – Figure 22. Consistent with the above summary, there is no evident correlation between elevated radionuclide concentrations and fluctuation or declining trends in Cl:SO4 or Na:Ca ratios. It is recognised that this ionic balance ratio ‘percentage-reduction’ approach to trigger the completion of a groundwater investigation in the current endorsed EMP (Rev 4, July 2017) was based on limited available baseline data at the time of EMP development. This method is thus conservative and overly sensitive to natural variation and is likely to result in ‘false flag’ exceedances, as demonstrated in the McGlashin Swamp Seepage Exceedances Assessment completed by EMM in the 2018 reporting period (EMM, 2018). That is, the current approach does not consider trend-based change in groundwater chemistry that accounts for seasonality or other influences on groundwater chemistry over a sufficient period of time. Revised site-specific trigger levels for groundwater quality, developed using the now expanded monitoring dataset and applying a trend-based trigger approach across all target analytes per the ANZECC/ARCMANZ (2000) guidelines, will therefore be implemented in the next revision of the EMP (Revision 5).

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

20

Table 4: Groundwater radionuclide concentrations vs. ionic balance ratios, H1 2020

Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time

(Years) *

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red. Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a

Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a BORES UP-GRADIENT OF PIT 23

GW05

15/11/2018 <0.002 <0.002 <0.025 0.05 0.12 5.5 I.D. 10.6 I.D.

N/A –

bores are up- gradient of Pit

23

Cl:SO4 and Na:Ca ratios

shown to demonstrate

natural variation only

15/01/2019 <0.002 <0.002 <0.025 <0.05 0.09 4.8 13% 11 -4% 19/02/2019 <0.002 <0.002 <0.025 <0.05 <0.08 5 -10% 11.1 -5%

8/07/2019 <0.002 0.001 <0.025 0.02 <0.08 4.7 2% 13.6 -23% 15/01/2020 <0.002 <0.001 <0.025 0.03 0.13 4.1 14% 21.0 -55% 20/02/2020 <0.002 <0.001 <0.025 0.04 0.1 4.5 4% 21.8 -61%

GW06

12/06/2018 <0.002 0.072 0.037 0.11 0.14 4.4 I.D. 5.1 I.D. 14/01/2019 <0.002 0.105 1.3 0.05 0.22 3.9 10% 5.4 -5% 21/03/2019 <0.002 0.071 0.877 <0.05 0.09 4.2 3% 5.5 -6% 17/04/2019 <0.002 0.089 1.1 0.06 0.19 4.7 -18% 5.5 -1% 22/05/2019 <0.002 0.079 0.975 0.04 0.14 4.9 -23% 5.1 6% 18/06/2019 <0.002 0.003 <0.025 0.04 0.2 4.5 -15% 5.9 -9%

4/07/2019 <0.002 0.072 0.889 0.06 0.17 4.5 -15% 5.7 -6% 22/01/2020 <0.002 0.003 0.025 0.04 0.21 3.8 17% 5.6 3% 24/02/2020 <0.002 0.003 1.33 0.16 0.08 4.5 1% 5.7 1%

GW08

29/11/2018 <0.002 0.002 0.025 0.09 0.24 4.8 I.D. 7.2 I.D. 14/01/2019 <0.002 0.064 0.79 <0.05 <0.08 5.1 -5% 5.9 17% 18/02/2019 <0.002 0.009 0.111 0.09 0.12 4.8 1% 6.1 15% 10/07/2019 <0.002 0.024 <0.025 0.04 0.08 5.9 -10% 6.5 -10% 20/01/2020 <0.003 0.001 2.86 0.07 <0.08 5.0 10% 6.5 0% 25/02/2020 <0.004 0.001 1.31 0.07 0.09 5.2 8% 6.7 -2%

5/05/2020 <0.002 <0.001 0.148 0.06 <0.08 5.2 6% 9.5 -45%

WRK301

10/07/2018 <0.002 0.008 0.049 0.14 0.17 6.5 -35% 6.5 4% 21/01/2019 <0.002 0.017 0.21 0.07 0.09 5 21% 5.9 10% 18/02/2019 <0.002 0.005 0.062 0.05 <0.08 4.9 24% 6.5 0%

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

21

Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time

(Years) *

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red. Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a

Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a 15/07/2019 <0.002 0.008 0.037 0.04 0.11 5.6 -11% 7.4 -26%

22/01/2020 0.0024 0.005 0.037 0.06 <0.08 5.2 8% 6.5 12% 25/02/2020 <0.002 0.005 0.395 0.01 <0.08 5.3 5% 6.7 10%

WRK302

10/07/2018 <0.002 0.059 0.148 0.19 0.76 5 -15% 6.7 8% 14/01/2019 <0.002 0.048 0.593 0.16 1.01 4.3 13% 7.1 -6% 18/02/2019 <0.002 0.046 0.568 0.31 1.14 4.8 4% 6.1 9% 21/03/2019 <0.002 0.116 1.43 0.27 0.94 4.4 12% 7.1 -6% 17/04/2019 <0.002 0.018 0.222 0.21 1.08 5.1 -2% 6.4 5% 22/05/2019 <0.002 <0.002 <0.025 0.12 0.84 5.1 -3% 6.9 -2%

4/07/2019 <0.002 0.001 0.086 0.24 0.91 4.6 -5% 7.8 -10% 1/08/2019 <0.002 <0.001 0.728 0.22 0.92 4.6 -7% 7.1 1%

20/01/2020 <0.002 <0.001 0.296 0.34 1.02 4.1 10% 7.6 3%

WRK303

10/07/2018 <0.002 <0.002 <0.025 <0.06 <0.09 4.2 -10% 12.7 5% 14/01/2019 <0.002 <0.002 <0.025 <0.05 <0.08 4 4% 11.5 9% 15/07/2019 <0.002 <0.001 <0.025 0.04 <0.08 4.7 -17% 13.3 -16% 23/01/2020 <0.002 <0.001 <0.025 0.03 <0.08 4.8 -2% 12.9 4%

WRK304

10/07/2018 <0.002 <0.002 <0.025 <0.05 <0.08 3.4 0% 15.1 -3% 14/01/2019 <0.002 <0.002 <0.025 <0.05 <0.08 3.2 6% 16.1 -7% 15/07/2019 <0.002 <0.001 <0.025 0.02 <0.08 3.8 -16% 16 1% 22/01/2020 <0.002 <0.001 2.7 <0.01 <0.08 3.6 5% 17 -7%

5/03/2020 <0.002 <0.001 <0.025 <0.01 <0.08 3.9 -4% 14.5 9% BORES DOWN-GRADIENT OF PIT 23 (IN PREDICTED FLOW PATH)

BW36A 11/12/2019 <0.002 0.002 <0.025 0.07 0.17 7.5 I.D. 10 I.D.

16/01/2020 <0.002 <0.001 <0.025 <0.01 <0.08 13.3 -78% 11.2 -12%

WRK300

18/10/2018 <0.002 <0.001 N.S. N.S. N.S. 5.5 -3% 7 -5%

36 years 21/01/2019 <0.002 <0.002 <0.025 <0.05 <0.08 6 -9% 6.1 3% 18/02/2019 <0.002 <0.002 <0.025 <0.05 <0.08 5.2 7% 7 -11% 21/03/2019 <0.002 0.002 <0.025 <0.05 <0.08 5.8 -5% 5.6 12%

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

22

Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time

(Years) *

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red. Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a

Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a 17/04/2019 <0.002 <0.002 <0.025 0.03 0.09 6.2 -13% 6.5 -3%

16/07/2019 <0.002 <0.002 <0.025 0.03 <0.08 5.7 6% 7.6 -26% 16/01/2020 <0.002 0.001 <0.025 0.02 0.08 5.5 3% 7.3 4%

GW01

7/06/2018 <0.002 <0.001 <0.025 <0.05 <0.08 8.4 I.D. 6 I.D.

88 years

15/01/2019 <0.002 <0.001 <0.025 0.48 1.36 8.5 -1% 27.7 -363% 20/03/2019 <0.002 0.001 <0.025 0.48 0.72 8.3 2% 29.4 -6% 15/04/2019 <0.002 <0.001 <0.025 0.4 1.2 10 -18% 25.3 9% 14/05/2019 0.0095 0.009 <0.025 0.47 1.36 9.4 -11% 32.8 -18% 18/06/2019 <0.002 <0.002 <0.025 0.46 1.29 8 5% 32.1 -16%

8/07/2019 <0.002 0.002 <0.025 0.28 0.77 8.5 0% 32.7 -18% 15/01/2020 <0.002 <0.001 <0.025 0.32 0.81 7.4 12% 20.7 37% 20/02/2020 <0.002 <0.001 <0.025 0.32 0.9 7.6 11% 26.0 21%

GW02

28/11/2018 <0.002 <0.001 <0.025 0.05 0.11 5.1 I.D. 34.2 I.D.

144 years 15/01/2019 <0.002 <0.001 <0.025 0.05 0.15 6 -18% 46.1 -35% 10/07/2019 <0.002 <0.001 0.296 0.1 0.32 7 -15% 61.9 -34% 14/01/2020 <0.002 <0.001 <0.025 0.05 0.14 6.2 11% 63.2 -2%

3/03/2020 0.004 <0.001 <0.025 0.08 0.27 6.9 1% 70.6 -14%

GW03

28/11/2018 <0.002 <0.002 0.025 0.07 0.16 5.7 I.D. 9.5 I.D.

176 years 15/01/2019 <0.002 <0.002 <0.025 <0.05 <0.08 5.3 8% 7 26% 19/02/2019 <0.002 <0.002 <0.025 <0.05 <0.08 5.6 2% 10 -6% 10/07/2019 <0.002 <0.001 <0.025 0.01 <0.08 6.3 -20% 11.2 -59% 14/01/2020 <0.002 <0.001 <0.025 0.01 <0.08 6 5% 11.3 -1%

BW05

18/10/2018 <0.002 0.03 <0.025 <0.05 <0.08 11 -23% 18.8 -11%

500+ years 17/01/2019 <0.002 0.004 0.037 <0.05 <0.08 8.6 17% 15.5 35% 20/03/2019 <0.002 0.003 0.049 <0.05 <0.08 9.4 10% 18.1 24%

3/07/2019 <0.002 0.003 <0.025 0.03 <0.08 9.6 -12% 19.2 -24% 13/01/2020 0.002 <0.025 <0.01 <0.08 9.0 7% 19.6 -2%

BORES CROSS-GRADIENT OF PIT 23

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

23

Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time

(Years) *

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red. Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a

Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a

BW28A *

20/08/2018 <0.002 0.005 0.074 0.09 <0.08 8.3 -14% 7 7%

N/A -

Bores not on flow path from

Pit 23

Cl:SO4 and Na:Ca ratios

shown to demonstrate

natural variation only

17/01/2019 <0.002 0.005 1.48 0.13 <0.08 7.1 9% 6.5 2% 18/02/2019 <0.002 0.005 0.173 0.17 <0.08 6.5 16% 6.9 -5% 3/07/2019 <0.002 0.006 0.679 0.13 <0.08 7.7 -9% 7.2 -11%

13/01/2020 <0.002 0.006 2.16 0.1 <0.08 7.2 7% 7.4 -3%

26/02/2020 <0.002 0.007 0.234 0.12 <0.08 8.2 -7% 7.3 -2%

BW45B

29/11/2018 <0.002 <0.001 <0.025 0.22 0.86 5.6 I.D. 8.6 I.D.

17/01/2019 <0.002 0.001 <0.025 0.42 2.4 5.3 7% 7.8 9% 6/03/2019 <0.002 0.001 <0.025 0.45 2.6 5.6 2% 8 6%

20/03/2019 <0.002 0.012 0.037 0.83 2.77 5.5 3% 8.4 2% 15/04/2019 <0.002 0.005 0.667 0.53 3.08 6.7 -17% 8.7 -1% 14/05/2019 <0.002 0.015 0.099 0.63 2.94 5.9 -3% 9 -5% 18/06/2019 <0.002 0.012 0.222 0.69 3.4 6.2 -8% 9.3 -8% 8/07/2019 <0.002 0.014 0.148 0.72 3.18 5.8 -9% 9 -16%

14/08/2019 <0.002 0.002 0.025 0.52 2.2 5.7 -7% 8.1 -4% 15/01/2020 <0.002 0.006 0.099 0.51 2.81 5.3 8% 8.75 3% 26/02/2020 <0.002 <0.001 0.086 0.52 2.9 6.3 -8% 9 0%

GW04

28/11/2018 <0.002 <0.002 <0.025 0.07 0.15 3.9 I.D. 14.2 I.D. 15/01/2019 <0.002 <0.002 <0.025 0.09 0.19 3.9 1% 17.3 -22% 8/07/2019 <0.002 <0.001 <0.002 0.1 0.2 4.4 -13% 14.2 18% 1/08/2019 <0.002 <0.001 <0.025 0.13 0.24 5.3 -35% 11.4 34%

12/09/2019 <0.002 <0.001 <0.025 0.12 0.24 4.3 -10% 13.1 24% 15/01/2020 <0.002 <0.001 <0.025 0.1 0.25 5.6 -27% 11.4 19% 20/02/2020 <0.002 <0.001 <0.025 0.14 0.26 5.2 -19% 13.1 8%

GW07

7/06/2018 <0.002 0.001 <0.025 <0.05 <0.08 6.2 I.D. 6.5 I.D. 17/01/2019 <0.002 <0.001 0.296 0.06 0.32 5.2 16% 5.2 21% 19/02/2019 <0.002 <0.001 0.556 <0.05 0.28 5.7 8% 6.8 -5%

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Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time

(Years) *

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red. Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a

Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a 21/03/2019 <0.002 <0.001 <0.025 <0.05 0.12 6 4% 7 -8%

3/07/2019 <0.002 <0.001 0.259 0.06 0.2 6.6 -27% 7.9 -53% 9/01/2020 <0.002 <0.001 2.04 0.08 0.19 5.7 14% 7.8 3%

26/02/2020 <0.002 <0.001 0.037 0.07 0.24 6.3 5% 7.9 0% BORES REPRESENTATIVE OF BACKGROUND

IWB2

18/10/2018 <0.002 <0.001 <0.025 0.03 <0.08 7.5 6% 60.9 -7%

N/A - Bores not on flow path from Pit 23

10/01/2019 <0.002 <0.001 <0.025 <0.05 0.08 7.5 0% 60 7% 11/07/2019 <0.002 <0.001 <0.025 0.03 <0.08 7 6% 70.6 -18% 14/01/2020 <0.002 <0.001 <0.025 0.06 0.12 7.5 -6% 69.1 2%

IWB6

3/07/2018 <0.002 <0.001 0.037 <0.05 <0.08 1.7 3% 44.8 -5% 10/01/2019 <0.002 <0.001 <0.025 <0.05 <0.08 1.7 6% 46 -3% 11/07/2019 <0.002 <0.001 <0.025 0.02 <0.08 1.8 -13% 50 -9% 14/01/2020 <0.002 <0.001 <0.025 0.03 <0.08 1.3 28% 47.2 6% 20/02/2020 <0.002 <0.001 <0.025 0.02 <0.08 1.8 3% 49.2 2%

BW53 (“Puls”)

3/07/2018 <0.002 <0.001 <0.025 <0.05 0.11 2.9 -22% 15.6 -173% 10/01/2019 <0.002 <0.001 <0.025 <0.05 0.19 2.5 15% 9.6 39% 19/02/2019 <0.002 <0.001 <0.025 <0.05 0.16 2.6 11% 12.1 22% 10/07/2019 <0.002 <0.001 <0.025 0.04 0.11 2.7 -9% 18.3 -93% 13/01/2020 <0.002 <0.002 <0.025 0.04 0.12 2.4 11% 17.2 6% 26/02/2020 <0.002 <0.002 <0.025 0.03 0.17 2.5 8% 16.8 8%

NOTES • < = results below the laboratory limit of detection. These are treated as a negative (-) concentrations in figures presented in this report to allow graphical representation. • Results highlighted in orange indicate an exceedance of the precautionary trigger • Results highlighted in pink indicate an exceedance of the upper trigger • Calculated ratios in green represent values that increase following an initial “>10%” reduction (i.e. no consecutive >10% reduction) • Calculated ratios in red represent values above the “>10%” reduction threshold (initial identified exceedance). • Calculated ratios in red highlighted represent a confirmed “>10%” reduction in consecutive or follow-up samples • N.S. = not sampled / analysed

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Bore ID

Date

Thorium Uranium U-238 Ra226 Ra228 CL:SO4 Na:Ca Groundwater Travel Time (mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L) Ratio % Red. Ratio % Red.

Precautionary trigger n/a 0.17 0.17 4.3 1.7 n/a n/a n/a n/a (Years) * Upper trigger n/a 0.2 0.2 5 2 n/a n/a n/a n/a

• I.D. = insufficient data to allow calculation of ionic ratio (only one data-point available) • Groundwater arrival year is based on groundwater model predictions (particle tracking) per CDM Smith (2015) and EMM (2019), and assumes that groundwater flow originates from Pit 23 immediately on commencement of the first by-product disposal to into Pit 23 (December 2011).

• GW04 is incorrectly referenced in the EMP (Revision 4) as being down gradient of Pit 23. Groundwater modelling and particle tracking per EMM (2019) indicate that GW04 is cross-gradient to the predicted groundwater flow path from Pit 23.

• BW28A is incorrectly referenced in the EMP (Revision 4) as being down-gradient of Pit 23. Groundwater modelling and particle tracking per CDM Smith (2014) and EMM (2019) indicate that BW28A is cross-gradient to the predicted groundwater flow path from Pit 23.

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Figure 7: U-238 and ionic balance trends – up-gradient bores (1 of 2) Figure 8: U-238 and ionic balance trends – up-gradient bores (2 of 2)

Figure 9: Ra-228 and ionic balance trends – up-gradient bores (1 of 2)s

Figure 10: Ra-228 and ionic balance trends – up-gradient bores (2 of 2)

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Figure 11: U-238 and ionic balance trends – down-gradient bores (1 of 2) Figure 12: U-238 and ionic balance trends – down-gradient bores (2 of 2)

Figure 13: Ra-228 and ionic balance trends – down-gradient bores (1 of 2)

Figure 14: Ra-228 and ionic balance trends – down-gradient bores (2 of 2)

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Figure 15: U-238 and ionic balance trends – cross-gradient bores (1 of 2) Figure 16: U-238 and ionic balance trends – cross-gradient bores (2 of 2)

Figure 17: Ra-228 and ionic balance trends – cross-gradient bores (1 of 2)

Figure 18: Ra-228 and ionic balance trends – cross-gradient bores (2 of 2)

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Figure 19: U-238 and ionic balance trends – bores representing background (1 of 2) Figure 20: U-238 and ionic balance trends – bores representing background (2 of 2)

Figure 21: Ra-228 and ionic balance trends – bores representing background (1 of 2)

Figure 22: Ra-228 and ionic balance trends – bores representing background (2 of 2)

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4.1.3.3 Other analytes In accordance with Section 7.6.7 of the EMP, biannual groundwater samples obtained from the monitoring locations are subjected to in-field and laboratory analysis for a suite of target parameters. Analyte concentrations above trigger limits that coincided with ionic balance ratio triggers are presented in Table 5 & Table 6 and Figure 23. In summary:

• sampling detected an elevated selenium result at GW01 during February as part of the follow up sampling required due to an ionic balance trigger that occurred during January’s scheduled sampling;

• sufficient data is available to determine background concentrations for GW01, which is determined as the 75th percentile value based on the mean and standard deviation of the available data. For GW01, the 75th percentile (background) value is higher than the standard SEPP WoV objectives and therefore applies as the upper trigger (background value); and

• all results are consistent with historical values and do not indicate seepage from Pit 23.

Table 5: Groundwater quality exceedances vs ionic balance ratios, H1 2020

Bore ID

Date Se CL:SO4 Na:Ca

(mg/L) Ratio % Red. Ratio % Red. Precautionary trigger 0.017 n/a n/a n/a n/a

Upper trigger 0.02 n/a n/a n/a n/a GW01 15/01/2020 0.018 7.4 12% 20.7 37%

Down 20/02/2020 0.025 7.6 11% 26.0 21% Gradient 2 sample av 0.022

Table 6:Selenium groundwater trigger levels for GW01, H1 2020

GW01

Se (mg/L)

AVG

Std Dev

Background

(av+2SD)

Prec Trigger

(85% of b/g)

Upper

Trigger

Ion. Bal. Rep. Exceedance?

2- sample

AVG

Comment

7/06/2018 0.002 No min 5 results reqd for statistical analysis 15/01/2019 0.052 0.027 0.035 0.098 No 0.027 min 5 results reqd for statistical analysis 20/03/2019 0.054 0.036 0.029 0.095 No 0.053 min 5 results reqd for statistical analysis 15/04/2019 0.050 0.040 0.025 0.090 No 0.052 min 5 results reqd for statistical analysis 14/05/2019 0.070 0.046 0.026 0.097 0.082 0.097 No 0.060

18/06/2019

0.039

0.045

0.023

0.091

0.077

0.091

Yes (Cl:SO4)

0.055

Cl:SO4 ratio triggered, SE below Precautionary trigger

8/07/2019 0.063 0.047 0.022 0.092 0.078 0.092 No 0.051

15/01/2020

0.018

0.044

0.023

0.089

0.076

0.089 Yes (Both

ratio's)

0.041 Both ratio's triggered, Se below Precautionary trigger

20/02/2020

0.025

0.046

0.018

0.082

0.070

0.082

Yes (Both ratio's)

0.022

Both ratio's triggered, Se below Precautionary trigger

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Figure 23: GW01 - Selenium as compared against ionic balance trends

All groundwater quality monitoring data (laboratory and field data) for the reporting period for all parameters monitored is provided in Appendix B and Appendix C of this report, respectively.

4.2 Surface water quality

4.2.1 Runoff-fed surface water sites In accordance with Section 8.7.1 of the EMP, surface water samples must be obtained from nominated runoff-fed surface water monitoring points if a discharge of run-off from the disturbed area of Pit 23 and surrounds occurs. No discharges occurred during the reporting period and subsequently no follow-up monitoring was required.

4.2.2 Groundwater-fed surface water sites In accordance with Section 8.7.2 of the EMP, quarterly surface water samples obtained from the nominated groundwater-fed surface water monitoring points down-gradient of Pit 23 (i.e. surface water features receiving groundwater base-flow) are analysed for a suite of target parameters to identify the potential expression of Pit 23 groundwater seepage.

Results obtained for specific parameters are summarised in sections 4.2.2.1 - 4.2.2.3 below. All surface water quality monitoring data for the reporting period and for all parameters monitored (laboratory and field results) is provided in Appendix D and Appendix E of this report.

4.2.2.1 Ionic balance ratios Assessment of potential Pit 23 seepage and expression into surface waters is based on an analysis of Cl:SO4 and Na:Ca ratios obtained from quarterly monitoring, with a consecutive reduction in either ratio of >10% applied as potential indicator of Pit 23 seepage and expression at surface.

Ionic ratio results for nominated surface water monitoring locations in the H1 2020 reporting period are given in Table 7. The data presented includes results preceding and following the H1 2020 reporting period to show longer-term trends and to demonstrate the influence of seasonality in both the availability of data (ability to obtain samples) and the influence that this natural variability has on surface water chemistry and hence the calculated ratios. The reliability of ratios calculated from data obtained after a long elapsed period of time (i.e. due to a lack of recent samples), and which suggest

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a consecutive >10% ratio exceedance, thus need to be interpreted with caution as they are more likely to reflect natural variation than any influence of Pit 23 seepage. With reference to Table 7, no reductions of >10% exceedances in either one or both ratio’s occurred during the reporting period.

Table 7: Surface water monitoring - ionic ratio balance results

Sample Point

Sample Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (ratio)

% Red. Repeated ratio

exceedance?

GROUNDWATER-FED SITES ALONG FLOW PATH FROM PIT 23

DUSW20 (NW drainage line)

26/06/2017 DRY DRY DRY DRY DRY DRY DRY DRY N/A

12/09/2017 360 61 5.90 I.D. 230 27 8.52 I.D.

11/10/2017 1100 150 7.33 -24% 630 71 8.87 -4%

15/01/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

19/06/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

17/07/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

8/08/2018 1100 200 5.50 25% 660 52 12.69 -43%

12/09/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

17/10/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

8/01/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

9/04/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

14/08/2019 82 36 2.28 59% 100 9.3 10.75 15%

16/09/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

24/10/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

1/04/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

15/06/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

DUSW24 (McGlashin Swamp)

26/06/2017 530 8 66.3 I.D. 430 87 4.94 I.D.

12/09/2017 500 38 13.2 80% 330 62 5.32 -8%

11/10/2017 530 46 11.5 83% 360 69 5.22 2%

15/01/2018 970 68 14.3 -24% 690 42 16.43 -215%

19/06/2018 2100 57 36.8 -158% 1200 66 18.18 -11%

17/07/2018 2100 69 30.4 17% 1300 65 20.00 -10%

14/08/2018 1900 72 26.4 13% 1100 63 17.46 13% Yes (CL:SO4) 12/09/2018 2000 89 22.5 15% 1300 71 18.31 -5% Yes (CL:SO4) 17/10/2018 2700 130 20.8 8% 1500 92 16.30 11%

1/11/2018 3100 130 23.8 -15% 1800 100 18.00 -10%

8/01/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

9/04/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

14/08/2019 3300 820 4.02 81% 1900 270 7.04 57%

16/09/2019 4700 960 4.9 76% 2600 330 7.88 52% Yes (Both) 24/10/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

1/04/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

15/06/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

DUSW5B (White Lake)

26/06/2017 100000 8300 12.0 I.D. 53000 1700 31.176 I.D.

11/09/2017 3200 390 8.2 32% 1800 130 13.846 56%

11/10/2017 44000 5200 8.5 30% 23000 1400 16.429 47% Yes (Both) 15/01/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

19/06/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

17/07/2018 100000 7000 14.3 -69% 59000 1600 36.88 -124%

17/10/2018 120000 9700 12.4 13% 65000 2000 32.50 12%

1/11/2018 170000 9400 18.1 -27% 100000 1200 83.33 -126%

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Sample Point

Sample Date CL-

(mg/L) SO4

(mg/L) CL:SO4 (ratio)

% Red. Na

(mg/L) Ca

(mg/L) Na:Ca (ratio)

% Red. Repeated ratio

exceedance?

8/01/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

9/04/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

14/08/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

16/09/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

24/10/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

1/04/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

15/06/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

GROUNDWATER-FED ANALOGUE / REFERENCE SITES (NOT ON PIT 23 FLOW PATH)

DUSW22 (Shaw's Gully)

26/06/2017 DNS DNS DNS DNS DNS DNS DNS DNS N/A

23/08/2017 190 35 5.4 I.D. 110 14 7.86 I.D.

11/10/2017 1700 180 9.4 -74% 840 91 9.23 -17%

15/01/2018 470 17 27.6 -193% 240 27 8.89 4%

19/06/2018 3600 410 8.8 68% 1800 160 11.25 -27%

17/07/2018 3200 330 9.7 -10% 1700 140 12.14 -8%

17/10/2018 2800 280 10.0 -3% 1400 120 11.67 4%

8/01/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

9/04/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

2/07/2019 2100 340 6.18 38% 1400 120 11.67 0%

1/08/2019 970 160 6.06 39% 550 44 12.5 -&% Yes (Cl:SO4) 24/10/2019 740 140 5.29 14% 410 34 12.06 -3% Yes (Cl:SO4) 7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

1/04/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

15/06/2020 3200 360 8.9 -68% 1700 150 11.3 6%

DUSW14 (Costello's Creek)

26/06/2017 DRY DRY DRY DRY DRY DRY DRY DRY N/A

13/09/2017 190 34 5.59 I.D. 130 13 10.00 I.D.

11/10/2017 1400 260 5.38 4% 850 49 17.35 -73%

15/01/2018 DRY DRY DRY DRY DRY DRY DRY DRY N/A

19/06/2018 1800 310 5.81 -8% 1100 67 16.42 5%

17/07/2018 1800 330 5.45 6% 1200 58 20.69 -26%

17/10/2018 1600 280 5.71 -5% 1000 50 20.00 3%

8/01/2019 2400 350 6.86 -20% 1400 50 28.00 -40%

9/04/2019 2200 240 9.17 -34% 1300 49 26.53 5%

2/07/2019 2200 360 6.11 33% 1300 74 17.57 34%

1/08/2019 1900 340 5.59 39% 1200 44 27.27 -3% Yes (Cl:SO4) 24/10/2019 1800 290 6.21 -2% 1200 46 26.09 -48%

7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

1/04/2020 2200 240 9.2 -0.5% 1300 45 28.9 -0.1%

DUSW45 (Brooksby's Swamp)

8/01/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

9/04/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

14/08/2019 5900 2100 2.81 I.D. 3400 730 4.66 I.D.

24/10/2019 DRY DRY DRY DRY DRY DRY DRY DRY N/A

7/01/2020 DRY DRY DRY DRY DRY DRY DRY DRY N/A

NOTES • Calculated ratios in green represent values that increase following an initial “>10%” reduction (i.e. no consecutive >10% reduction) • Calculated ratios in red represent values above the “>10%” reduction threshold (initial identified exceedance). • Calculated ratios in red highlight represent a confirmed “>10%” reduction in consecutive or follow-up samples • I.D. = insufficient data to allow calculation of ionic ratio (only one data-point available) • DUSW45 (Brooksby’s Swamp) is not required to be monitored under the EMP however samples are collected at this location to aid in

understanding of seasonal fluctuations in water quality across the region.

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4.2.2.2 Radionuclide concentrations Section 7.9.1 of the EMP prescribes the locations for surface water monitoring and the monitoring frequency, as summarised in Table 8. These locations are subject to sampling and laboratory analysis for radionuclides (Thorium, Uranium, Radium-226, Radium-228 and Uranium-238). Radionuclide monitoring results for the reporting period are presented in Figure 24 and Figure 25. The corresponding monitoring data for radionuclides in surface water is provided in Appendix A. Note that for concentrations reported as below the laboratory limit of reporting / limit of detection (as indicated by “<”) the numerical value is treated as a negative concentration to enable graphical representation in order to demonstrate that sampling for that analyte was undertaken in compliance with the EMP. The monitoring results for radionuclides in surface water obtained during the reporting period confirm nil exceedances of any precautionary or upper trigger. Further, no off-site discharges from the confines of Pit 23 or immediate area occurred. Note that long-term data for these surface water points is available and the data presented in Figure 24 and Figure 25 represents all current data for these points.

Table 8: Monitoring program – radionuclide concentrations in surface water

Surface water monitoring locations Frequency

DUSW14 – Costello’s Creek DUSW5B – White Lake DUSW24 – McGlashin Swamp DUSW20 – North-west drainage line DUSW22 – Southern Drainage Line

• Quarterly; or • During or following an off-site discharge event (creek and drainage

lines only)

Figure 24: Ra-226 and Ra-228 in surface water

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Figure 25: Uranium and U-238 in surface water

4.2.2.3 Other analytes In accordance with Section 8.7.2 of the EMP, quarterly samples (if available) obtained from the monitoring locations are subjected to in-field and laboratory analysis for a suite of target parameters.

As discussed in Sections 4.2.1 and 4.2.2.1 there have been no runoff or discharges from site throughout the reporting period and no instances where ionic balance ratios were triggered at surface water monitoring locations that may be influenced from groundwater discharge.

4.3 Noise

In accordance with Section 10.1.4 of the endorsed EMP, noise level measurements will be undertaken in the unlikely event that noise complaints are received. No noise related complaints were received during the reporting period, and hence no noise levels measurements were undertaken.

4.4 PM10 concentrations in air In accordance with Sections 9.6 and 10.1.4 of the endorsed EMP, the concentration of PM10 dust in air at the Lyon’s and Chadwick’s residences is measured using high volume (‘hi-vol’) air samplers on a one-in-six day monitoring cycle. The location of these hi-vol air samplers relative to Pit 23 are shown in Figure 27. 12-month rolling results for PM10 compared to daily rainfall are shown in Figure 26. Results adhere to the expected year-on-year pattern of lower airborne PM10 concentrations in winter months.

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Figure 26: PM10 dust concentrations at neighbouring residences vs. daily rainfall

No results above the PM10 concentration limit (0.06 mg/m3) were recorded at either the Lyons or Chadwicks residences during the H1 2020 reporting period.

N

Pit 10

Pit 23

Chadwicks ?!

Pit 9

Pit 22 Lyons ?

Pit 5

Pit 21

Pit 12

Pit 19 Pit 2

Pit 3

Pit 11 Pit 1

The Rises ?!

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community

0 500

Meters 1,000 2,000 3,000 4,000

AIR QUALITY MONITORING LOCATIONS (PM10 - Hi Vols)

L:\Maps\2018\Unregistered\Douglas\mxd\Pit 23 Annual Report 2017

DRAWN: N. Travers

DATE:26/06/2018 FIGURE: 27

Legend

!? PM10 monitoring Pit 23 crest

Pit Crests

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4.5 Radiation monitoring – other

It is a requirement of the Iluka Radiation Management Licence 300042022 that works relating to the minerals sands by-product disposal into Pit 23 are conducted in accordance with a Radiation Management Plan (RMP) and a Radioactive Waste Management Plan (RWMP), including the monitoring programs under those plans, to ensure that radiation doses are below the prescribed limit. Radiation monitoring relevant to this performance report includes:

• Radon concentrations in air;

• Gross alpha activity concentration of airborne dust; and

• Radionuclide concentrations in groundwater and surface water. Results for radon concentrations in air and gross alpha activity concentration of airborne dust are detailed below. Results for radionuclides in groundwater and surface water are detailed in Sections 4.1.3.2 and 4.2.2.2, respectively.

4.5.1 Radon concentrations in air Monitoring of radon concentrations in air is undertaken at four locations within and immediately adjacent to Pit 23 and at two residences east of Pit 23 (Chadwick’s) and south of Pit 23 (Rises). Radon monitoring is undertaken using Landauer “Radtrak2” radon/thoron track etch detectors and the newer Rapidos High Sensitivity (“Rapidos HS”) radon detectors (Figure 30). The Rapidos HS detectors were implemented in Q4 2018 for side-by-side comparison with the existing Radtrak2 detectors, with initial results from the Rapidos HS detectors indicating that airborne radon levels are significantly lower than those indicated by the less sensitive Radtrak2 detectors, and therefore provide a more accurate measure of actual airborne radon levels in the vicinity of Pit 23 and at local residences. This side-by-side comparison will continue through 2020 to allow for meaningful statistical comparison of radon data between units over time. No high-sensitivity thoron detectors are available and thoron monitoring will continue using the Radtrack2 detectors. Radon and Thoron monitoring results for the reporting period are presented in Table 9 and Table 10, and also in Figure 29 and Figure 30. All measured radon and thoron levels in the H1 2020 reporting period were well below the reportable levels irrespective of the detectors used.

Figure 28: Radon and thoron detectors

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EMP and Rehabilitation Performance Report – H1 2020

Table 9: Radon concentrations within Pit 23 for H1 2020

Location

Radon concentration in air (Bq/m3)

Rapidos High Sensitivity (Bq/m³)

Reportable level

Jul 19 - Sep 19

Oct 19 - Dec 19

Jan 20 - Mar 20

Apr 20 - Jun 20

Jul 19 - Sep 19

Oct 19 - Dec 19

Jan 20 - Mar 20

Apr 20 - Jun 20

Pit 23 East 100 <15 <15 16 ± 16 <15 <7 11 ± 7 <4 <3

Pit 23 North 100 <15 <15 <15 <15 <7 <8 4 ± 3 <3

Pit 23 West 100 <15 <20 <15 <15 <7 <8 <4 <3

Pit 23 South 100 <15 <15 <20 <15 <7 <7 <3 <3

Chadwick’s 100 <15 <15 <15 <15 <7 8 ± 7 6 ± 3 <3

Rises 100 <15 <15 <15 <15 <7 <7 <4 <3

Table 10: Thoron concentrations within Pit 23 for H1 2020

Location

Thoron concentration in air (Bq/m3)

Radtrak2 Detectors

Reportable level

Jun18 To

Sep18

Oct18 To

Jan19

Jan19 To

Apr19

Apr19 To

Jul19

Jul19 To

Sep19

Oct19 To

Dec19

Jan20 To

Mar20

Apr20 To

Jun20 Pit 23 East 1000 77 +/- 32 40 +/- 20 67 ± 32 34 ± 20 58 ± 26 100 ± 36 <20 <20

Pit 23 North 1000 <40 <20 42 ± 28 <30 <30 <40 23 ± 12 <20

Pit 23 West 1000 <40 132 +/- 32 119 ± 32 68 ± 22 66 ± 26 83 ± 40 58 ± 16 <20

Pit 23 South 1000 92 +/- 34 162 +/- 28 - 138 ± 30 115 ± 30 133 ± 38 81 ± 18 <20

Chadwick’s 1000 <40 21 +/- 16 <30 <30 <30 <40 <20 <20

Rises 1000 <40 <20 36 ± 28 <30 <30 <40 <20 <20

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Figure 29: Radon concentration in air, H1 2020

Figure 30: Thoron concentration in air, H1 2020

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4.5.2 Gross alpha concentrations in airborne dust As noted in Section 4.4, sampling for airborne particulates in PM10 dust is conducted using high volume (hi-vol) air samplers located at the Chadwick’s, Lyons and Rises residences (see Figure 27). On a quarterly basis hi-vol units are run for a continuous 96 hour period for purposes of monitoring gross alpha concentration in air, which represents a total air sample volume of approximately 6,000 m3. The filters are weighed to determine the total dust loading in mg/m3 and then analysed for gross alpha activity expressed as millibequerels/m3 (mBq/m3). The results for the monitoring period are in line with historical values and are shown in Table 11 and Figure 31.

Table 11: Gross Alpha radiation in PM10 dust

Location Run Date Sample / Filter No. Air Volume (m3) Activity Conc (mBq/m3)

Chadwick’s 22/02/2020 031219GF25 5892 0.120 Lyon’s 22/02/2020 031219GF26 5929 0.161 Rises 22/02/2020 031219GF27 5913 0.173 Chadwick’s 21/06/2020 031219GF90 6012 0.048 Lyon’s 21/06/2020 031219GF91 6165 <0.063 Rises 21/06/2020 031219GF88 6059 0.038

Figure 31: Gross Alpha Radiation in PM10 Dust – H1 2020

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5 Management Actions 5.1 Monitoring bore audits

In accordance with Section 7.6.2 of the EMP, audits of the monitoring bore network are undertaken on monthly or bi-annually and outcomes reported annually within this EMP and Rehabilitation Performance Report. Bore integrity (e.g. physical condition, blocked/dry or poor yield) is assessed as part of the groundwater monitoring program. As per Section 4.1.1 of this report, all bores are in serviceable condition with the exception of BW36 which is blocked and was replaced with BW36A in October 2019.

5.2 Groundwater flow paths from Pit 23

In accordance with Section 7.9.1 of the EMP, groundwater levels measured at bores WRK300 – WRK304 inclusive, GW1 to GW7 inclusive, GW9, BW36A and BW45B are used to construct groundwater contours in the area of Pit 23 and surrounds and infer groundwater flow paths from Pit 23, with these levels and flow paths compared with the groundwater levels and flow paths predicted by the hydrogeological model. Groundwater level contours are provided in Figure 32 (EMM 2019; EMM 2020). This compares the 2019 modelled contours per EMM (2019), and interpreted groundwater contours as at June 2020 including standing water level data for new monitoring bores installed in 2018 and 2019. From these June 2020 contours it is confirmed that:

• groundwater contours and flow-paths are consistent with the 2019 modelled contours and prior year contours; and

• groundwater flow from Pit 23 is still to the north and north-west.

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Figure 32: 2019 vs 2020 interpreted groundwater contours (EMM 2019; EMM 2020)

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5.3 Groundwater model review and recalibration

Sections 7.10 and 8.7.2 of the endorsed EMP outlines the circumstances that will trigger a review and recalibration of the hydrogeological model.

An update of the Douglas Mine (inclusive Pit 23) hydrogeological model was commissioned through EMM Consulting in December 2018 in response to the potential groundwater seepage impacts identified during surface water monitoring at McGlashin’s Swamp in the 2017 reporting period. This also satisfied the commitment for a review of the model within two (2) years of the Planning Permit being granted.

Whilst complimentary seepage impact investigation (EMM, 2018) determined that the observed exceedances were associated with natural phenomena and un-related to Pit 23, a review and update of the groundwater model was required in accordance with the Pit 23 EMP.

Preliminary findings of the 2019 groundwater model update were presented to the Responsible Authority and Pit 23 Technical Reference Group (TRG) by Iluka and EMM Consulting personnel at a meeting held at the HRCC Council Chambers on 23rd May 2019. The final modelling report was completed and provided to the Responsible Authority in Q3 2019.

This modelling will be used to validate existing model predictions on the groundwater flow path and groundwater flow rates from the Pit 23 facility, and to inform updates to groundwater-related content with the next iteration of the Pit 23 Environmental Management Plan (EMP, Rev 5).

5.4 Maximum surface level of disposed materials in Pit 23

In accordance with Section 7.9.1 of the EMP, the maximum elevation of the upper surface of materials disposed of at the end of the reporting period must be reported. The Pit 23 void consists of an upper and lower disposal area; no wastes were disposed into Pit 23 during the H1 2020 reporting period. Accordingly, the survey undertaken on the 8th of December 2017 confirming the upper surface of materials deposited in Pit 23 (i.e. the elevation of capped material in the upper disposal area) remains unchanged at 193 mAHD.

5.5 Non-compliances

There were no non-compliances for the H1 2020 reporting period. 5.6 Comments and complaints received

No complaints or comments were received during the H1 2020 reporting period. 5.7 H1 2020 Completed Actions

There were no actions required to be completed during the reporting period. 5.8 H2 2020 Proposed Actions

The following actions are planned for H2 2020:

• submission of the updated Pit 23 Incoming Waste Monitoring Plan (IWMP) and Environmental Management Plan (EMP) as required by the default two-year review periods stipulated within these plans. The updated EMP will include outcomes of the updated groundwater modelling completed by EMM in 2019;

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• annual review of the Pit 23 Risk Analysis and Response Plan (RARP) risk register as per Section 6 of the EMP; and

• Installation of groundwater monitoring bore GW04A to be located between GW04 and BW36A as previously agreed with Auditor.

5.9 Other matters

5.9.1 Annual geotechnical audit In accordance with Section 10.5.2 and 10.5.3 of the EMP, geotechnical audits are completed on an annual basis with the last audit completed in December 2019 (AMC Consultants, 2019). The next audit is scheduled for November 2020.

5.9.2 Pit 23 Risk Register annual review Per Section 6 of the EMP, the Pit 23 Risk Analysis and Response Plan (RARP) was developed by AECOM Australia Pty Ltd who recommended that the Pit 23 Risk Register (contained as Appendix A of the RARP) be reviewed annually at the time when EMP and Rehabilitation Performance Reports are developed. Reviews of the Pit 23 RARP risk register were conducted in December 2018 and presented in the prior 2018 EMP and Rehabilitation Performance Report submitted to the Responsible Authority on 3rd June 2019. A review of the Pit 23 RARP risk register was undertaken in April 2019 as part of the review and update of the Environmental Management Plan (EMP) and is scheduled to be reviewed in H2 2020.

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6 References ANZECC/ARMCANZ (2000) National Water Quality Management Strategy: Australian and New Zealand Guidelines for Fresh and Marine Water Quality. Australian and New Zealand Environment and Conservation Council and Agricultural and Resource Management Council of Australia and New Zealand, Canberra, Australian Capital Territory, October 2000.

CDM Smith (2014) Douglas Mine Site Hydrogeological Modelling. Completed on behalf of Iluka Resources, November 2014

CDM Smith (2015) Douglas Mine – Particle Tracking of Seepage Water. Completed on behalf of Iluka Resources, February 2015

EMM (2018) Pit 23 Groundwater – Assessment of Seepage Indicator Exceedances, November 2018 (Report S180265, Rev 2 Final), issued for Iluka Resources Ltd

EMM (2019) Groundwater Model Update and Predictive Scenario Modelling – Douglas Mine. Prepared by EMM Consulting for Iluka Resources Ltd, September 2019.

EES (2016) Independent Desktop Review For The Continuation Of Mineral By-Products Disposal Into Pit 23 At Iluka’s Douglas Mine Site, Northwest Victoria No. 215071v2 dated April 2016. Prepared by Environmental Earth Sciences, Melbourne, Victoria. (TRIM T18729).

AMC Consultants (2019) Douglas Mine Pit 23 Geotechnical Audit & Risk Assessment, 10th December 2019.

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7 Appendices Appendix A: Monitoring Data (Lab) – Radiation – Surface Water

Surface water ID

Date

Thorium Uranium U238 Ra226 Ra228

(mg/L) (mg/L) (Bq/L) (Bq/L) (Bq/L)

Precautionary trigger n/a 0.17 0.17 4.3 1.7 Upper trigger n/a 0.2 0.2 5 2

Q1 2020 DUSW05B 7/01/2020 DRY DRY DRY DRY DRY DUSW14 7/01/2020 DRY DRY DRY DRY DRY DUSW20 7/01/2020 DRY DRY DRY DRY DRY DUSW22 7/01/2020 DRY DRY DRY DRY DRY DUSW24 7/01/2020 DRY DRY DRY DRY DRY DUSW45 7/01/2020 DRY DRY DRY DRY DRY

Q2 2020 DUSW05B 1/04/2020 DRY DRY DRY DRY DRY DUSW05B 15/06/2020 DRY DRY DRY DRY DRY DUSW14 1/04/2020 0.0045 <0.001 <0.025 <0.01 <0.08 DUSW20 1/04/2020 DRY DRY DRY DRY DRY DUSW20 15/06/2020 DRY DRY DRY DRY DRY DUSW22 1/04/2020 DRY DRY DRY DRY DRY DUSW22 15/06/2020 <0.002 <0.001 <0.025 <0.01 <0.08 DUSW24 1/04/2020 DRY DRY DRY DRY DRY DUSW24 15/06/2020 DRY DRY DRY DRY DRY DUSW45 1/04/2020 DRY DRY DRY DRY DRY DUSW45 15/06/2020 DRY DRY DRY DRY DRY

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Appendix B: Monitoring Data (Lab) – Groundwater

Variable Unit Sample Point Date Result Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW07 9/01/2020 62 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW05 13/01/2020 480 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW28A 13/01/2020 400 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 84 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW03 14/01/2020 160 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW02 14/01/2020 31 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_IWB2 14/01/2020 31 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_IWB6 14/01/2020 17 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW01 15/01/2020 26 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW45B 15/01/2020 8 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW05 15/01/2020 44 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW04 15/01/2020 32 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW36A 16/01/2020 310 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK300 16/01/2020 260 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 20/01/2020 170 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK302 20/01/2020 95 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK304 22/01/2020 42 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW06 22/01/2020 200 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK301 22/01/2020 360 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK303 23/01/2020 40 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_IWB6 20/02/2020 18 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW04 20/02/2020 27 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW05 20/02/2020 43 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW01 20/02/2020 25 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW06 24/02/2020 180 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 25/02/2020 170 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK301 25/02/2020 370 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW07 26/02/2020 91 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW45B 26/02/2020 8 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW28A 26/02/2020 410 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 58 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW02 3/03/2020 51 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_WRK304 5/03/2020 45 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 5/05/2020 150 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW07 9/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW05 13/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW28A 13/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW03 14/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW02 14/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_IWB2 14/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_IWB6 14/01/2020 0

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Variable Unit Sample Point Date Result Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW01 15/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW45B 15/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW05 15/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW04 15/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW36A 16/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK300 16/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 20/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK302 20/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK304 22/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW06 22/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK301 22/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK303 23/01/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_IWB6 20/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW04 20/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW05 20/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW01 20/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW06 24/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 25/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK301 25/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW07 26/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW45B 26/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW28A 26/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW02 3/03/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_WRK304 5/03/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_PZ_GW08 5/05/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW07 9/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW05 13/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW28A 13/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW03 14/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW02 14/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_IWB2 14/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_IWB6 14/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW01 15/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW45B 15/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW05 15/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW04 15/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW36A 16/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK300 16/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW08 20/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK302 20/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK304 22/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW06 22/01/2020 0

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Variable Unit Sample Point Date Result Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK301 22/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK303 23/01/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_IWB6 20/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW04 20/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW05 20/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW01 20/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW06 24/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW08 25/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK301 25/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW07 26/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW45B 26/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW28A 26/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW02 3/03/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_WRK304 5/03/2020 0 Alkalinity (Hydroxide) as CaCO3 mg/L DG_A_I_PZ_GW08 5/05/2020 0 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW07 9/01/2020 62 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW05 13/01/2020 480 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW28A 13/01/2020 400 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 84 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW03 14/01/2020 160 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW02 14/01/2020 31 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_IWB2 14/01/2020 31 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_IWB6 14/01/2020 17 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW01 15/01/2020 26 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW45B 15/01/2020 8 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW05 15/01/2020 44 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW04 15/01/2020 32 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW36A 16/01/2020 310 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK300 16/01/2020 260 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW08 20/01/2020 170 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK302 20/01/2020 95 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK304 22/01/2020 42 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW06 22/01/2020 200 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK301 22/01/2020 360 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK303 23/01/2020 40 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_IWB6 20/02/2020 18 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW04 20/02/2020 27 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW05 20/02/2020 43 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW01 20/02/2020 25 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW06 24/02/2020 180 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW08 25/02/2020 170 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK301 25/02/2020 370 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW07 26/02/2020 91

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

50

Variable Unit Sample Point Date Result Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW45B 26/02/2020 8 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW28A 26/02/2020 410 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 58 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW02 3/03/2020 51 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_WRK304 5/03/2020 45 Alkalinity (Total) as CaCO3 mg/L DG_A_I_PZ_GW08 5/05/2020 150 Aluminium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.07 Aluminium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.22 Aluminium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.02 Aluminium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.1 Aluminium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.02 Aluminium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.11 Aluminium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.14 Aluminium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.29 Aluminium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.57 Aluminium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 4.7 Aluminium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.02 Aluminium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.05 Aluminium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.06 Aluminium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.19 Aluminium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.01 Aluminium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.24 Aluminium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.05 Aluminium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.07 Aluminium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.58 Aluminium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.04 Aluminium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.1 Aluminium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.03 Aluminium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.02 Aluminium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.93 Aluminium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.1 Aluminium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.01 Aluminium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.21 Aluminium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.09 Aluminium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 4.8 Aluminium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.01 Aluminium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.08 Aluminium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.03 Aluminium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.05 Aluminium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.01 Ammonia Nitrogen mg/L DG_A_I_PZ_GW07 9/01/2020 0.074 Ammonia Nitrogen mg/L DG_A_I_PZ_BW05 13/01/2020 0.12 Ammonia Nitrogen mg/L DG_A_I_PZ_BW28A 13/01/2020 0.19 Ammonia Nitrogen mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 3.4

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

51

Variable Unit Sample Point Date Result Ammonia Nitrogen mg/L DG_A_I_PZ_GW03 14/01/2020 0.022 Ammonia Nitrogen mg/L DG_A_I_PZ_GW02 14/01/2020 0.06 Ammonia Nitrogen mg/L DG_A_I_PZ_IWB2 14/01/2020 0.013 Ammonia Nitrogen mg/L DG_A_I_PZ_IWB6 14/01/2020 0.011 Ammonia Nitrogen mg/L DG_A_I_PZ_GW01 15/01/2020 0.007 Ammonia Nitrogen mg/L DG_A_I_PZ_BW45B 15/01/2020 0.054 Ammonia Nitrogen mg/L DG_A_I_PZ_GW05 15/01/2020 0.029 Ammonia Nitrogen mg/L DG_A_I_PZ_GW04 15/01/2020 0.009 Ammonia Nitrogen mg/L DG_A_I_PZ_BW36A 16/01/2020 0.016 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK300 16/01/2020 0.006 Ammonia Nitrogen mg/L DG_A_I_PZ_GW08 20/01/2020 0.12 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK302 20/01/2020 0.12 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK304 22/01/2020 0.1 Ammonia Nitrogen mg/L DG_A_I_PZ_GW06 22/01/2020 0.12 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK301 22/01/2020 0.07 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK303 23/01/2020 0.14 Ammonia Nitrogen mg/L DG_A_I_PZ_IWB6 20/02/2020 0.052 Ammonia Nitrogen mg/L DG_A_I_PZ_GW04 20/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_GW05 20/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_GW01 20/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_GW06 24/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_GW08 25/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK301 25/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_GW07 26/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_BW45B 26/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_BW28A 26/02/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 3.1 Ammonia Nitrogen mg/L DG_A_I_PZ_GW02 3/03/2020 0.02 Ammonia Nitrogen mg/L DG_A_I_PZ_WRK304 5/03/2020 0.01 Ammonia Nitrogen mg/L DG_A_I_PZ_GW08 5/05/2020 0.02 Anions (Total) meq/L DG_A_I_PZ_GW07 9/01/2020 180 Anions (Total) meq/L DG_A_I_PZ_BW05 13/01/2020 250 Anions (Total) meq/L DG_A_I_PZ_BW28A 13/01/2020 220 Anions (Total) meq/L DG_A_I_PZ_BW53/Puls 13/01/2020 30 Anions (Total) meq/L DG_A_I_PZ_GW03 14/01/2020 110 Anions (Total) meq/L DG_A_I_PZ_GW02 14/01/2020 68 Anions (Total) meq/L DG_A_I_PZ_IWB2 14/01/2020 37 Anions (Total) meq/L DG_A_I_PZ_IWB6 14/01/2020 16 Anions (Total) meq/L DG_A_I_PZ_GW01 15/01/2020 110 Anions (Total) meq/L DG_A_I_PZ_BW45B 15/01/2020 160 Anions (Total) meq/L DG_A_I_PZ_GW05 15/01/2020 88 Anions (Total) meq/L DG_A_I_PZ_GW04 15/01/2020 92 Anions (Total) meq/L DG_A_I_PZ_BW36A 16/01/2020 43 Anions (Total) meq/L DG_A_I_PZ_WRK300 16/01/2020 59

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

52

Variable Unit Sample Point Date Result Anions (Total) meq/L DG_A_I_PZ_GW08 20/01/2020 210 Anions (Total) meq/L DG_A_I_PZ_WRK302 20/01/2020 210 Anions (Total) meq/L DG_A_I_PZ_WRK304 22/01/2020 86 Anions (Total) meq/L DG_A_I_PZ_GW06 22/01/2020 210 Anions (Total) meq/L DG_A_I_PZ_WRK301 22/01/2020 110 Anions (Total) meq/L DG_A_I_PZ_WRK303 23/01/2020 89 Anions (Total) meq/L DG_A_I_PZ_IWB6 20/02/2020 15 Anions (Total) meq/L DG_A_I_PZ_GW04 20/02/2020 92 Anions (Total) meq/L DG_A_I_PZ_GW05 20/02/2020 93 Anions (Total) meq/L DG_A_I_PZ_GW01 20/02/2020 110 Anions (Total) meq/L DG_A_I_PZ_GW06 24/02/2020 220 Anions (Total) meq/L DG_A_I_PZ_GW08 25/02/2020 220 Anions (Total) meq/L DG_A_I_PZ_WRK301 25/02/2020 110 Anions (Total) meq/L DG_A_I_PZ_GW07 26/02/2020 180 Anions (Total) meq/L DG_A_I_PZ_BW45B 26/02/2020 160 Anions (Total) meq/L DG_A_I_PZ_BW28A 26/02/2020 220 Anions (Total) meq/L DG_A_I_PZ_BW53/Puls 26/02/2020 30 Anions (Total) meq/L DG_A_I_PZ_GW02 3/03/2020 66 Anions (Total) meq/L DG_A_I_PZ_WRK304 5/03/2020 85 Anions (Total) meq/L DG_A_I_PZ_GW08 5/05/2020 220 Arsenic (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.002 Arsenic (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.007 Arsenic (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.53 Arsenic (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.006 Arsenic (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.045 Arsenic (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001 Arsenic (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Arsenic (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.084 Arsenic (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.002 Arsenic (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Arsenic (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.002 Arsenic (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.009 Arsenic (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.003 Arsenic (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.005 Arsenic (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.006

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

53

Variable Unit Sample Point Date Result Arsenic (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.002 Arsenic (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.003 Arsenic (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.002 Arsenic (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.004 Arsenic (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.5 Arsenic (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.007 Arsenic (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.001 Arsenic (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.01 Arsenic (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Barium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.025 Barium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.029 Barium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.074 Barium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.046 Barium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.033 Barium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.039 Barium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.003 Barium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.023 Barium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.053 Barium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.032 Barium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.019 Barium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.026 Barium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.27 Barium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.032 Barium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.006 Barium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.022 Barium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.028 Barium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.021 Barium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.01 Barium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.04 Barium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.022 Barium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.022 Barium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.016 Barium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.044 Barium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.024 Barium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.006 Barium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.013 Barium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.025 Barium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.03 Barium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.07 Barium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.043 Barium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.035 Barium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.03 Barium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.005

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

54

Variable Unit Sample Point Date Result Boron (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 1.9 Boron (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 1.4 Boron (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.89 Boron (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.19 Boron (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.3 Boron (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.14 Boron (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.07 Boron (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.04 Boron (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.13 Boron (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.9 Boron (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 1 Boron (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.46 Boron (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.06 Boron (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.24 Boron (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 1.1 Boron (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 1.3 Boron (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.62 Boron (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 1.8 Boron (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.58 Boron (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.48 Boron (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.07 Boron (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.58 Boron (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 1.1 Boron (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.14 Boron (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 1.6 Boron (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 1.3 Boron (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.57 Boron (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 1.5 Boron (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.84 Boron (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.8 Boron (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.15 Boron (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.11 Boron (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.6 Boron (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 1.3 Cadmium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.0002

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

55

Variable Unit Sample Point Date Result Cadmium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.0002 Cadmium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.0002 Calcium mg/L DG_A_I_PZ_GW07 9/01/2020 400 Calcium mg/L DG_A_I_PZ_BW05 13/01/2020 240 Calcium mg/L DG_A_I_PZ_BW28A 13/01/2020 460 Calcium mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 29 Calcium mg/L DG_A_I_PZ_GW03 14/01/2020 160 Calcium mg/L DG_A_I_PZ_GW02 14/01/2020 19 Calcium mg/L DG_A_I_PZ_IWB2 14/01/2020 9.7 Calcium mg/L DG_A_I_PZ_IWB6 14/01/2020 7.2 Calcium mg/L DG_A_I_PZ_GW01 15/01/2020 92 Calcium mg/L DG_A_I_PZ_BW45B 15/01/2020 320 Calcium mg/L DG_A_I_PZ_GW05 15/01/2020 81 Calcium mg/L DG_A_I_PZ_GW04 15/01/2020 140 Calcium mg/L DG_A_I_PZ_BW36A 16/01/2020 69 Calcium mg/L DG_A_I_PZ_WRK300 16/01/2020 150 Calcium mg/L DG_A_I_PZ_GW08 20/01/2020 520 Calcium mg/L DG_A_I_PZ_WRK302 20/01/2020 460 Calcium mg/L DG_A_I_PZ_WRK304 22/01/2020 100 Calcium mg/L DG_A_I_PZ_GW06 22/01/2020 610 Calcium mg/L DG_A_I_PZ_WRK301 22/01/2020 260 Calcium mg/L DG_A_I_PZ_WRK303 23/01/2020 140

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

56

Variable Unit Sample Point Date Result Calcium mg/L DG_A_I_PZ_IWB6 20/02/2020 6.3 Calcium mg/L DG_A_I_PZ_GW04 20/02/2020 130 Calcium mg/L DG_A_I_PZ_GW05 20/02/2020 87 Calcium mg/L DG_A_I_PZ_GW01 20/02/2020 73 Calcium mg/L DG_A_I_PZ_GW06 24/02/2020 600 Calcium mg/L DG_A_I_PZ_GW08 25/02/2020 540 Calcium mg/L DG_A_I_PZ_WRK301 25/02/2020 270 Calcium mg/L DG_A_I_PZ_GW07 26/02/2020 390 Calcium mg/L DG_A_I_PZ_BW45B 26/02/2020 300 Calcium mg/L DG_A_I_PZ_BW28A 26/02/2020 490 Calcium mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 31 Calcium mg/L DG_A_I_PZ_GW02 3/03/2020 17 Calcium mg/L DG_A_I_PZ_WRK304 5/03/2020 110 Calcium mg/L DG_A_I_PZ_GW08 5/05/2020 400 Cations (Total) meq/L DG_A_I_PZ_GW07 9/01/2020 180 Cations (Total) meq/L DG_A_I_PZ_BW05 13/01/2020 260 Cations (Total) meq/L DG_A_I_PZ_BW28A 13/01/2020 220 Cations (Total) meq/L DG_A_I_PZ_BW53/Puls 13/01/2020 29 Cations (Total) meq/L DG_A_I_PZ_GW03 14/01/2020 100 Cations (Total) meq/L DG_A_I_PZ_GW02 14/01/2020 67 Cations (Total) meq/L DG_A_I_PZ_IWB2 14/01/2020 37 Cations (Total) meq/L DG_A_I_PZ_IWB6 14/01/2020 17 Cations (Total) meq/L DG_A_I_PZ_GW01 15/01/2020 110 Cations (Total) meq/L DG_A_I_PZ_BW45B 15/01/2020 160 Cations (Total) meq/L DG_A_I_PZ_GW05 15/01/2020 88 Cations (Total) meq/L DG_A_I_PZ_GW04 15/01/2020 91 Cations (Total) meq/L DG_A_I_PZ_BW36A 16/01/2020 44 Cations (Total) meq/L DG_A_I_PZ_WRK300 16/01/2020 65 Cations (Total) meq/L DG_A_I_PZ_GW08 20/01/2020 220 Cations (Total) meq/L DG_A_I_PZ_WRK302 20/01/2020 210 Cations (Total) meq/L DG_A_I_PZ_WRK304 22/01/2020 88 Cations (Total) meq/L DG_A_I_PZ_GW06 22/01/2020 220 Cations (Total) meq/L DG_A_I_PZ_WRK301 22/01/2020 110 Cations (Total) meq/L DG_A_I_PZ_WRK303 23/01/2020 98 Cations (Total) meq/L DG_A_I_PZ_IWB6 20/02/2020 16 Cations (Total) meq/L DG_A_I_PZ_GW04 20/02/2020 95 Cations (Total) meq/L DG_A_I_PZ_GW05 20/02/2020 93 Cations (Total) meq/L DG_A_I_PZ_GW01 20/02/2020 110 Cations (Total) meq/L DG_A_I_PZ_GW06 24/02/2020 220 Cations (Total) meq/L DG_A_I_PZ_GW08 25/02/2020 230 Cations (Total) meq/L DG_A_I_PZ_WRK301 25/02/2020 110 Cations (Total) meq/L DG_A_I_PZ_GW07 26/02/2020 180 Cations (Total) meq/L DG_A_I_PZ_BW45B 26/02/2020 160 Cations (Total) meq/L DG_A_I_PZ_BW28A 26/02/2020 220

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

57

Variable Unit Sample Point Date Result Cations (Total) meq/L DG_A_I_PZ_BW53/Puls 26/02/2020 30 Cations (Total) meq/L DG_A_I_PZ_GW02 3/03/2020 65 Cations (Total) meq/L DG_A_I_PZ_WRK304 5/03/2020 85 Cations (Total) meq/L DG_A_I_PZ_GW08 5/05/2020 230 Chloride mg/L DG_A_I_PZ_GW07 9/01/2020 5700 Chloride mg/L DG_A_I_PZ_BW05 13/01/2020 7800 Chloride mg/L DG_A_I_PZ_BW28A 13/01/2020 6900 Chloride mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 750 Chloride mg/L DG_A_I_PZ_GW03 14/01/2020 3300 Chloride mg/L DG_A_I_PZ_GW02 14/01/2020 2100 Chloride mg/L DG_A_I_PZ_IWB2 14/01/2020 1200 Chloride mg/L DG_A_I_PZ_IWB6 14/01/2020 330 Chloride mg/L DG_A_I_PZ_GW01 15/01/2020 3500 Chloride mg/L DG_A_I_PZ_BW45B 15/01/2020 4900 Chloride mg/L DG_A_I_PZ_GW05 15/01/2020 2600 Chloride mg/L DG_A_I_PZ_GW04 15/01/2020 2900 Chloride mg/L DG_A_I_PZ_BW36A 16/01/2020 1200 Chloride mg/L DG_A_I_PZ_WRK300 16/01/2020 1700 Chloride mg/L DG_A_I_PZ_GW08 20/01/2020 6500 Chloride mg/L DG_A_I_PZ_WRK302 20/01/2020 6200 Chloride mg/L DG_A_I_PZ_WRK304 22/01/2020 2500 Chloride mg/L DG_A_I_PZ_GW06 22/01/2020 6000 Chloride mg/L DG_A_I_PZ_WRK301 22/01/2020 3100 Chloride mg/L DG_A_I_PZ_WRK303 23/01/2020 2700 Chloride mg/L DG_A_I_PZ_IWB6 20/02/2020 340 Chloride mg/L DG_A_I_PZ_GW04 20/02/2020 2800 Chloride mg/L DG_A_I_PZ_GW05 20/02/2020 2800 Chloride mg/L DG_A_I_PZ_GW01 20/02/2020 3400 Chloride mg/L DG_A_I_PZ_GW06 24/02/2020 6700 Chloride mg/L DG_A_I_PZ_GW08 25/02/2020 6700 Chloride mg/L DG_A_I_PZ_WRK301 25/02/2020 3200 Chloride mg/L DG_A_I_PZ_GW07 26/02/2020 5600 Chloride mg/L DG_A_I_PZ_BW45B 26/02/2020 5100 Chloride mg/L DG_A_I_PZ_BW28A 26/02/2020 7000 Chloride mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 770 Chloride mg/L DG_A_I_PZ_GW02 3/03/2020 2000 Chloride mg/L DG_A_I_PZ_WRK304 5/03/2020 2500 Chloride mg/L DG_A_I_PZ_GW08 5/05/2020 6800 Chromium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.01 Chromium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

58

Variable Unit Sample Point Date Result Chromium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.003 Chromium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.005 Chromium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.025 Chromium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.01 Chromium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.003 Chromium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.002 Chromium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.005 Chromium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.002 Chromium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.008 Chromium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Chromium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.002 Chromium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.033 Chromium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.031 Cobalt (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.026 Cobalt (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.014 Cobalt (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.018 Cobalt (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.002 Cobalt (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.002 Cobalt (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.035 Cobalt (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.03 Cobalt (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.009 Cobalt (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.007 Cobalt (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.009 Cobalt (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.027

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

59

Variable Unit Sample Point Date Result Cobalt (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.002 Cobalt (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.012 Cobalt (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.007 Cobalt (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.051 Cobalt (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.003 Cobalt (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.025 Cobalt (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.032 Cobalt (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.027 Cobalt (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.016 Cobalt (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Cobalt (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Copper (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.011 Copper (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.029 Copper (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.01 Copper (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.007 Copper (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.005 Copper (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.004 Copper (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.005 Copper (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.004 Copper (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.007 Copper (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.011 Copper (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.004 Copper (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.003

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

60

Variable Unit Sample Point Date Result Copper (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.019 Copper (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.004 Copper (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.002 Copper (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.003 Copper (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.002 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 9/01/2020 18000 Electrical Conductivity µS/cm DG_A_I_PZ_BW05 13/01/2020 23000 Electrical Conductivity µS/cm DG_A_I_PZ_BW28A 13/01/2020 21000 Electrical Conductivity µS/cm DG_A_I_PZ_BW53/Puls 13/01/2020 3100 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 14/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 14/01/2020 7200 Electrical Conductivity µS/cm DG_A_I_PZ_IWB2 14/01/2020 4100 Electrical Conductivity µS/cm DG_A_I_PZ_IWB6 14/01/2020 1700 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 15/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 15/01/2020 16000 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 15/01/2020 9100 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 15/01/2020 9500 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 16/01/2020 4800 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 16/01/2020 6200 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 20/01/2020 20000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 20/01/2020 19000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 22/01/2020 9000 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 22/01/2020 21000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 22/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 23/01/2020 9100 Electrical Conductivity µS/cm DG_A_I_PZ_IWB6 20/02/2020 1600 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 20/02/2020 9200 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 20/02/2020 8800 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 20/02/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 24/02/2020 20000 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 25/02/2020 19000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 25/02/2020 10000 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 26/02/2020 17000 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 26/02/2020 15000 Electrical Conductivity µS/cm DG_A_I_PZ_BW28A 26/02/2020 21000 Electrical Conductivity µS/cm DG_A_I_PZ_BW53/Puls 26/02/2020 3100 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 3/03/2020 6800 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 5/03/2020 8800 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 5/05/2020 20000 Fluoride mg/L DG_A_I_PZ_GW07 9/01/2020 0.28 Fluoride mg/L DG_A_I_PZ_BW05 13/01/2020 0.55

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

61

Variable Unit Sample Point Date Result Fluoride mg/L DG_A_I_PZ_BW28A 13/01/2020 0.51 Fluoride mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.12 Fluoride mg/L DG_A_I_PZ_GW03 14/01/2020 0.27 Fluoride mg/L DG_A_I_PZ_GW02 14/01/2020 0.1 Fluoride mg/L DG_A_I_PZ_IWB2 14/01/2020 0.17 Fluoride mg/L DG_A_I_PZ_IWB6 14/01/2020 0.1 Fluoride mg/L DG_A_I_PZ_GW01 15/01/2020 0.64 Fluoride mg/L DG_A_I_PZ_BW45B 15/01/2020 1.3 Fluoride mg/L DG_A_I_PZ_GW05 15/01/2020 0.11 Fluoride mg/L DG_A_I_PZ_GW04 15/01/2020 0.18 Fluoride mg/L DG_A_I_PZ_BW36A 16/01/2020 0.68 Fluoride mg/L DG_A_I_PZ_WRK300 16/01/2020 0.36 Fluoride mg/L DG_A_I_PZ_GW08 20/01/2020 0.21 Fluoride mg/L DG_A_I_PZ_WRK302 20/01/2020 0.62 Fluoride mg/L DG_A_I_PZ_WRK304 22/01/2020 0.32 Fluoride mg/L DG_A_I_PZ_GW06 22/01/2020 0.28 Fluoride mg/L DG_A_I_PZ_WRK301 22/01/2020 0.6 Fluoride mg/L DG_A_I_PZ_WRK303 23/01/2020 0.26 Fluoride mg/L DG_A_I_PZ_IWB6 20/02/2020 0.1 Fluoride mg/L DG_A_I_PZ_GW04 20/02/2020 0.15 Fluoride mg/L DG_A_I_PZ_GW05 20/02/2020 0.11 Fluoride mg/L DG_A_I_PZ_GW01 20/02/2020 0.68 Fluoride mg/L DG_A_I_PZ_GW06 24/02/2020 0.29 Fluoride mg/L DG_A_I_PZ_GW08 25/02/2020 0.2 Fluoride mg/L DG_A_I_PZ_WRK301 25/02/2020 0.53 Fluoride mg/L DG_A_I_PZ_GW07 26/02/2020 0.29 Fluoride mg/L DG_A_I_PZ_BW45B 26/02/2020 1.1 Fluoride mg/L DG_A_I_PZ_BW28A 26/02/2020 0.36 Fluoride mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.11 Fluoride mg/L DG_A_I_PZ_GW02 3/03/2020 0.1 Fluoride mg/L DG_A_I_PZ_WRK304 5/03/2020 0.36 Fluoride mg/L DG_A_I_PZ_GW08 5/05/2020 0.22 Iron (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.06 Iron (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.42 Iron (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 6 Iron (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.27 Iron (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 4.8 Iron (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.05 Iron (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.07 Iron (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.27 Iron (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.03 Iron (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.13 Iron (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.02 Iron (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.02

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

62

Variable Unit Sample Point Date Result Iron (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 8.8 Iron (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.05 Iron (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.02 Iron (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.01 Iron (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.02 Iron (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.03 Iron (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.52 Iron (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.06 Iron (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.09 Iron (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.01 Iron (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.04 Iron (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.04 Iron (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.04 Iron (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.02 Iron (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.03 Iron (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.04 Iron (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.18 Iron (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 6.8 Iron (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.34 Iron (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.04 Iron (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.02 Iron (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.02 Lead (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.007 Lead (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.002 Lead (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.006 Lead (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.006 Lead (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

63

Variable Unit Sample Point Date Result Lead (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.01 Lead (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Lead (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Magnesium mg/L DG_A_I_PZ_GW07 9/01/2020 300 Magnesium mg/L DG_A_I_PZ_BW05 13/01/2020 450 Magnesium mg/L DG_A_I_PZ_BW28A 13/01/2020 520 Magnesium mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 61 Magnesium mg/L DG_A_I_PZ_GW03 14/01/2020 200 Magnesium mg/L DG_A_I_PZ_GW02 14/01/2020 140 Magnesium mg/L DG_A_I_PZ_IWB2 14/01/2020 94 Magnesium mg/L DG_A_I_PZ_IWB6 14/01/2020 20 Magnesium mg/L DG_A_I_PZ_GW01 15/01/2020 230 Magnesium mg/L DG_A_I_PZ_BW45B 15/01/2020 310 Magnesium mg/L DG_A_I_PZ_GW05 15/01/2020 100 Magnesium mg/L DG_A_I_PZ_GW04 15/01/2020 180 Magnesium mg/L DG_A_I_PZ_BW36A 16/01/2020 76 Magnesium mg/L DG_A_I_PZ_WRK300 16/01/2020 120 Magnesium mg/L DG_A_I_PZ_GW08 20/01/2020 480 Magnesium mg/L DG_A_I_PZ_WRK302 20/01/2020 410 Magnesium mg/L DG_A_I_PZ_WRK304 22/01/2020 120 Magnesium mg/L DG_A_I_PZ_GW06 22/01/2020 510 Magnesium mg/L DG_A_I_PZ_WRK301 22/01/2020 260 Magnesium mg/L DG_A_I_PZ_WRK303 23/01/2020 150 Magnesium mg/L DG_A_I_PZ_IWB6 20/02/2020 19 Magnesium mg/L DG_A_I_PZ_GW04 20/02/2020 160 Magnesium mg/L DG_A_I_PZ_GW05 20/02/2020 100 Magnesium mg/L DG_A_I_PZ_GW01 20/02/2020 220 Magnesium mg/L DG_A_I_PZ_GW06 24/02/2020 490 Magnesium mg/L DG_A_I_PZ_GW08 25/02/2020 500 Magnesium mg/L DG_A_I_PZ_WRK301 25/02/2020 260 Magnesium mg/L DG_A_I_PZ_GW07 26/02/2020 300 Magnesium mg/L DG_A_I_PZ_BW45B 26/02/2020 300 Magnesium mg/L DG_A_I_PZ_BW28A 26/02/2020 530 Magnesium mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 62 Magnesium mg/L DG_A_I_PZ_GW02 3/03/2020 140

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

64

Variable Unit Sample Point Date Result Magnesium mg/L DG_A_I_PZ_WRK304 5/03/2020 110 Magnesium mg/L DG_A_I_PZ_GW08 5/05/2020 500 Manganese (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.009 Manganese (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.13 Manganese (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 1.4 Manganese (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.036 Manganese (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 2 Manganese (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.55 Manganese (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.009 Manganese (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.009 Manganese (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.031 Manganese (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.077 Manganese (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.039 Manganese (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.055 Manganese (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 3.1 Manganese (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.13 Manganese (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.014 Manganese (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.018 Manganese (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.01 Manganese (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.022 Manganese (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.046 Manganese (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.007 Manganese (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.008 Manganese (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.045 Manganese (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.029 Manganese (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.006 Manganese (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.029 Manganese (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.01 Manganese (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.019 Manganese (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.008 Manganese (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.051 Manganese (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 1.4 Manganese (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.028 Manganese (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.52 Manganese (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.009 Manganese (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.007 Mercury (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.0001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

65

Variable Unit Sample Point Date Result Mercury (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.0002 Mercury (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.0001 Mercury (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.0002 Mercury (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.0001 Molybdenum (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.002 Molybdenum (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.002 Molybdenum (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.002 Molybdenum (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.002 Molybdenum (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

66

Variable Unit Sample Point Date Result Molybdenum (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.002 Molybdenum (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Molybdenum (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Nickel (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.03 Nickel (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Nickel (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.013 Nickel (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Nickel (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.008 Nickel (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.006 Nickel (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.003 Nickel (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.002 Nickel (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.022 Nickel (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.045 Nickel (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.005 Nickel (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.007 Nickel (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.012 Nickel (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.005 Nickel (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.009 Nickel (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.021 Nickel (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.003 Nickel (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.013 Nickel (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.003 Nickel (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.004 Nickel (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.002 Nickel (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.009 Nickel (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.005 Nickel (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.028 Nickel (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.016 Nickel (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.009 Nickel (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.002 Nickel (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.024

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

67

Variable Unit Sample Point Date Result Nickel (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.048 Nickel (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.013 Nickel (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Nickel (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.005 Nickel (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.003 Nickel (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.008 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW07 9/01/2020 0.56 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW05 13/01/2020 1.1 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW28A 13/01/2020 0.22 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 5 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW03 14/01/2020 1.4 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW02 14/01/2020 8.4 Nitrate-Nitrogen mg/L DG_A_I_PZ_IWB2 14/01/2020 4.4 Nitrate-Nitrogen mg/L DG_A_I_PZ_IWB6 14/01/2020 8.9 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW01 15/01/2020 1.2 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW45B 15/01/2020 0.03 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW05 15/01/2020 4.2 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW04 15/01/2020 3 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW36A 16/01/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK300 16/01/2020 0.66 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW08 20/01/2020 0.29 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK302 20/01/2020 0.34 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK304 22/01/2020 2.2 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW06 22/01/2020 0.13 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK301 22/01/2020 0.22 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK303 23/01/2020 2.8 Nitrate-Nitrogen mg/L DG_A_I_PZ_IWB6 20/02/2020 9.6 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW04 20/02/2020 3.4 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW05 20/02/2020 4.3 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW01 20/02/2020 1.5 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW06 24/02/2020 0.14 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW08 25/02/2020 0.31 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK301 25/02/2020 0.1 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW07 26/02/2020 0.58 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW45B 26/02/2020 0.064 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW28A 26/02/2020 0.15 Nitrate-Nitrogen mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 4 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW02 3/03/2020 14 Nitrate-Nitrogen mg/L DG_A_I_PZ_WRK304 5/03/2020 2.2 Nitrate-Nitrogen mg/L DG_A_I_PZ_GW08 5/05/2020 0.33 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW28A 13/01/2020 0.016 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.042

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

68

Variable Unit Sample Point Date Result Nitrite-Nitrogen mg/L DG_A_I_PZ_GW03 14/01/2020 0.02 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW02 14/01/2020 0.018 Nitrite-Nitrogen mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_IWB6 14/01/2020 0.004 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW01 15/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW45B 15/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW05 15/01/2020 0.16 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW04 15/01/2020 0.018 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW36A 16/01/2020 0.014 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK300 16/01/2020 0.12 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK302 20/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW06 22/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK301 22/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_IWB6 20/02/2020 0.007 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW04 20/02/2020 0.015 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW05 20/02/2020 0.1 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW01 20/02/2020 0.004 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW06 24/02/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW07 26/02/2020 0.009 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW45B 26/02/2020 0.01 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW28A 26/02/2020 0.006 Nitrite-Nitrogen mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.012 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW02 3/03/2020 0.024 Nitrite-Nitrogen mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 pH pH units DG_A_I_PZ_GW07 9/01/2020 6.5 pH pH units DG_A_I_PZ_BW05 13/01/2020 7.1 pH pH units DG_A_I_PZ_BW28A 13/01/2020 6.6 pH pH units DG_A_I_PZ_BW53/Puls 13/01/2020 6.9 pH pH units DG_A_I_PZ_GW03 14/01/2020 6.5 pH pH units DG_A_I_PZ_GW02 14/01/2020 5.7 pH pH units DG_A_I_PZ_IWB2 14/01/2020 5.7 pH pH units DG_A_I_PZ_IWB6 14/01/2020 5.6 pH pH units DG_A_I_PZ_GW01 15/01/2020 5.6 pH pH units DG_A_I_PZ_BW45B 15/01/2020 4.8 pH pH units DG_A_I_PZ_GW05 15/01/2020 6 pH pH units DG_A_I_PZ_GW04 15/01/2020 5.9 pH pH units DG_A_I_PZ_BW36A 16/01/2020 6.9 pH pH units DG_A_I_PZ_WRK300 16/01/2020 6.8

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

69

Variable Unit Sample Point Date Result pH pH units DG_A_I_PZ_GW08 20/01/2020 6.4 pH pH units DG_A_I_PZ_WRK302 20/01/2020 6 pH pH units DG_A_I_PZ_WRK304 22/01/2020 6.5 pH pH units DG_A_I_PZ_GW06 22/01/2020 6.6 pH pH units DG_A_I_PZ_WRK301 22/01/2020 7.2 pH pH units DG_A_I_PZ_WRK303 23/01/2020 6.1 pH pH units DG_A_I_PZ_IWB6 20/02/2020 5.6 pH pH units DG_A_I_PZ_GW04 20/02/2020 5.7 pH pH units DG_A_I_PZ_GW05 20/02/2020 5.9 pH pH units DG_A_I_PZ_GW01 20/02/2020 5.4 pH pH units DG_A_I_PZ_GW06 24/02/2020 6.6 pH pH units DG_A_I_PZ_GW08 25/02/2020 6.3 pH pH units DG_A_I_PZ_WRK301 25/02/2020 7.3 pH pH units DG_A_I_PZ_GW07 26/02/2020 6.5 pH pH units DG_A_I_PZ_BW45B 26/02/2020 4.9 pH pH units DG_A_I_PZ_BW28A 26/02/2020 6.6 pH pH units DG_A_I_PZ_BW53/Puls 26/02/2020 6.7 pH pH units DG_A_I_PZ_GW02 3/03/2020 5.6 pH pH units DG_A_I_PZ_WRK304 5/03/2020 6.3 pH pH units DG_A_I_PZ_GW08 5/05/2020 6.3 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW07 9/01/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW05 13/01/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.045 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.58 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW03 14/01/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW02 14/01/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.011 Phosphorus (Ortho) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW01 15/01/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW05 15/01/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW04 15/01/2020 0.006 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.034 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW08 20/01/2020 0.009 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.008 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.15 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW06 22/01/2020 0.017 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.01 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.01 Phosphorus (Ortho) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.008 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW04 20/02/2020 0.009 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW05 20/02/2020 0.006 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW01 20/02/2020 0.004

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

70

Variable Unit Sample Point Date Result Phosphorus (Ortho) mg/L DG_A_I_PZ_GW06 24/02/2020 0.011 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW08 25/02/2020 0.005 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.007 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW07 26/02/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.04 Phosphorus (Ortho) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.54 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW02 3/03/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.008 Phosphorus (Ortho) mg/L DG_A_I_PZ_GW08 5/05/2020 0.007 Radium 226 Bq/L DG_A_I_PZ_GW07 9/01/2020 0.08 Radium 226 Bq/L DG_A_I_PZ_BW05 13/01/2020 0.01 Radium 226 Bq/L DG_A_I_PZ_BW28A 13/01/2020 0.1 Radium 226 Bq/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.04 Radium 226 Bq/L DG_A_I_PZ_GW03 14/01/2020 0.01 Radium 226 Bq/L DG_A_I_PZ_GW02 14/01/2020 0.05 Radium 226 Bq/L DG_A_I_PZ_IWB2 14/01/2020 0.06 Radium 226 Bq/L DG_A_I_PZ_IWB6 14/01/2020 0.03 Radium 226 Bq/L DG_A_I_PZ_GW01 15/01/2020 0.32 Radium 226 Bq/L DG_A_I_PZ_BW45B 15/01/2020 0.51 Radium 226 Bq/L DG_A_I_PZ_BW45B 15/01/2020 0.51 Radium 226 Bq/L DG_A_I_PZ_GW05 15/01/2020 0.03 Radium 226 Bq/L DG_A_I_PZ_GW04 15/01/2020 0.1 Radium 226 Bq/L DG_A_I_PZ_BW36A 16/01/2020 0.01 Radium 226 Bq/L DG_A_I_PZ_WRK300 16/01/2020 0.02 Radium 226 Bq/L DG_A_I_PZ_GW08 20/01/2020 0.07 Radium 226 Bq/L DG_A_I_PZ_WRK302 20/01/2020 0.34 Radium 226 Bq/L DG_A_I_PZ_WRK304 22/01/2020 0.01 Radium 226 Bq/L DG_A_I_PZ_GW06 22/01/2020 0.04 Radium 226 Bq/L DG_A_I_PZ_WRK301 22/01/2020 0.06 Radium 226 Bq/L DG_A_I_PZ_WRK303 23/01/2020 0.03 Radium 226 Bq/L DG_A_I_PZ_IWB6 20/02/2020 0.02 Radium 226 Bq/L DG_A_I_PZ_GW04 20/02/2020 0.14 Radium 226 Bq/L DG_A_I_PZ_GW05 20/02/2020 0.04 Radium 226 Bq/L DG_A_I_PZ_GW01 20/02/2020 0.32 Radium 226 Bq/L DG_A_I_PZ_GW06 24/02/2020 0.08 Radium 226 Bq/L DG_A_I_PZ_GW08 25/02/2020 0.07 Radium 226 Bq/L DG_A_I_PZ_WRK301 25/02/2020 0.01 Radium 226 Bq/L DG_A_I_PZ_GW07 26/02/2020 0.07 Radium 226 Bq/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.03 Radium 226 Bq/L DG_A_I_PZ_BW45B 26/02/2020 0.52 Radium 226 Bq/L DG_A_I_PZ_BW28A 26/02/2020 0.12 Radium 226 Bq/L DG_A_I_PZ_GW02 3/03/2020 0.08 Radium 226 Bq/L DG_A_I_PZ_WRK304 5/03/2020 0.01

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

71

Variable Unit Sample Point Date Result Radium 226 Bq/L DG_A_I_PZ_GW08 5/05/2020 0.06 Radium 228 Bq/L DG_A_I_PZ_GW07 9/01/2020 0.19 Radium 228 Bq/L DG_A_I_PZ_BW05 13/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_BW28A 13/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.12 Radium 228 Bq/L DG_A_I_PZ_GW03 14/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW02 14/01/2020 0.14 Radium 228 Bq/L DG_A_I_PZ_IWB2 14/01/2020 0.12 Radium 228 Bq/L DG_A_I_PZ_IWB6 14/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW01 15/01/2020 0.81 Radium 228 Bq/L DG_A_I_PZ_BW45B 15/01/2020 2.81 Radium 228 Bq/L DG_A_I_PZ_BW45B 15/01/2020 2.81 Radium 228 Bq/L DG_A_I_PZ_GW05 15/01/2020 0.13 Radium 228 Bq/L DG_A_I_PZ_GW04 15/01/2020 0.25 Radium 228 Bq/L DG_A_I_PZ_BW36A 16/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_WRK300 16/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW08 20/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_WRK302 20/01/2020 1.02 Radium 228 Bq/L DG_A_I_PZ_WRK304 22/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW06 22/01/2020 0.21 Radium 228 Bq/L DG_A_I_PZ_WRK301 22/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_WRK303 23/01/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_IWB6 20/02/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW04 20/02/2020 0.26 Radium 228 Bq/L DG_A_I_PZ_GW05 20/02/2020 0.1 Radium 228 Bq/L DG_A_I_PZ_GW01 20/02/2020 0.9 Radium 228 Bq/L DG_A_I_PZ_GW06 24/02/2020 0.16 Radium 228 Bq/L DG_A_I_PZ_GW08 25/02/2020 0.09 Radium 228 Bq/L DG_A_I_PZ_WRK301 25/02/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW07 26/02/2020 0.24 Radium 228 Bq/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.17 Radium 228 Bq/L DG_A_I_PZ_BW45B 26/02/2020 2.9 Radium 228 Bq/L DG_A_I_PZ_BW28A 26/02/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW02 3/03/2020 0.27 Radium 228 Bq/L DG_A_I_PZ_WRK304 5/03/2020 0.08 Radium 228 Bq/L DG_A_I_PZ_GW08 5/05/2020 0.08 Selenium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.01 Selenium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.011 Selenium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.009 Selenium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.002 Selenium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Selenium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.003 Selenium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Selenium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.002

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

72

Variable Unit Sample Point Date Result Selenium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.018 Selenium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.019 Selenium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.031 Selenium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.022 Selenium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.003 Selenium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.003 Selenium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.016 Selenium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.011 Selenium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.013 Selenium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.008 Selenium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.008 Selenium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.025 Selenium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.001 Selenium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.022 Selenium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.025 Selenium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.025 Selenium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.01 Selenium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.016 Selenium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.006 Selenium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.009 Selenium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.018 Selenium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.008 Selenium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Selenium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.002 Selenium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.012 Selenium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.017 Silver (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

73

Variable Unit Sample Point Date Result Silver (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.002 Silver (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Silver (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Sodium mg/L DG_A_I_PZ_GW07 9/01/2020 3100 Sodium mg/L DG_A_I_PZ_BW05 13/01/2020 4700 Sodium mg/L DG_A_I_PZ_BW28A 13/01/2020 3400 Sodium mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 500 Sodium mg/L DG_A_I_PZ_GW03 14/01/2020 1800 Sodium mg/L DG_A_I_PZ_GW02 14/01/2020 1200 Sodium mg/L DG_A_I_PZ_IWB2 14/01/2020 670 Sodium mg/L DG_A_I_PZ_IWB6 14/01/2020 340 Sodium mg/L DG_A_I_PZ_GW01 15/01/2020 1900 Sodium mg/L DG_A_I_PZ_BW45B 15/01/2020 2800 Sodium mg/L DG_A_I_PZ_GW05 15/01/2020 1700 Sodium mg/L DG_A_I_PZ_GW04 15/01/2020 1600 Sodium mg/L DG_A_I_PZ_BW36A 16/01/2020 770 Sodium mg/L DG_A_I_PZ_WRK300 16/01/2020 1100 Sodium mg/L DG_A_I_PZ_GW08 20/01/2020 3400 Sodium mg/L DG_A_I_PZ_WRK302 20/01/2020 3500 Sodium mg/L DG_A_I_PZ_WRK304 22/01/2020 1700 Sodium mg/L DG_A_I_PZ_GW06 22/01/2020 3400 Sodium mg/L DG_A_I_PZ_WRK301 22/01/2020 1700 Sodium mg/L DG_A_I_PZ_WRK303 23/01/2020 1800 Sodium mg/L DG_A_I_PZ_IWB6 20/02/2020 310 Sodium mg/L DG_A_I_PZ_GW04 20/02/2020 1700 Sodium mg/L DG_A_I_PZ_GW05 20/02/2020 1900 Sodium mg/L DG_A_I_PZ_GW01 20/02/2020 1900 Sodium mg/L DG_A_I_PZ_GW06 24/02/2020 3400 Sodium mg/L DG_A_I_PZ_GW08 25/02/2020 3600 Sodium mg/L DG_A_I_PZ_WRK301 25/02/2020 1800 Sodium mg/L DG_A_I_PZ_GW07 26/02/2020 3100

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

74

Variable Unit Sample Point Date Result Sodium mg/L DG_A_I_PZ_BW45B 26/02/2020 2700 Sodium mg/L DG_A_I_PZ_BW28A 26/02/2020 3600 Sodium mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 520 Sodium mg/L DG_A_I_PZ_GW02 3/03/2020 1200 Sodium mg/L DG_A_I_PZ_WRK304 5/03/2020 1600 Sodium mg/L DG_A_I_PZ_GW08 5/05/2020 3800 Sulfate mg/L DG_A_I_PZ_GW07 9/01/2020 1000 Sulfate mg/L DG_A_I_PZ_BW05 13/01/2020 870 Sulfate mg/L DG_A_I_PZ_BW28A 13/01/2020 960 Sulfate mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 310 Sulfate mg/L DG_A_I_PZ_GW03 14/01/2020 550 Sulfate mg/L DG_A_I_PZ_GW02 14/01/2020 340 Sulfate mg/L DG_A_I_PZ_IWB2 14/01/2020 160 Sulfate mg/L DG_A_I_PZ_IWB6 14/01/2020 250 Sulfate mg/L DG_A_I_PZ_GW01 15/01/2020 470 Sulfate mg/L DG_A_I_PZ_BW45B 15/01/2020 920 Sulfate mg/L DG_A_I_PZ_GW05 15/01/2020 640 Sulfate mg/L DG_A_I_PZ_GW04 15/01/2020 520 Sulfate mg/L DG_A_I_PZ_BW36A 16/01/2020 90 Sulfate mg/L DG_A_I_PZ_WRK300 16/01/2020 310 Sulfate mg/L DG_A_I_PZ_GW08 20/01/2020 1300 Sulfate mg/L DG_A_I_PZ_WRK302 20/01/2020 1500 Sulfate mg/L DG_A_I_PZ_WRK304 22/01/2020 700 Sulfate mg/L DG_A_I_PZ_GW06 22/01/2020 1600 Sulfate mg/L DG_A_I_PZ_WRK301 22/01/2020 600 Sulfate mg/L DG_A_I_PZ_WRK303 23/01/2020 560 Sulfate mg/L DG_A_I_PZ_IWB6 20/02/2020 190 Sulfate mg/L DG_A_I_PZ_GW04 20/02/2020 540 Sulfate mg/L DG_A_I_PZ_GW05 20/02/2020 620 Sulfate mg/L DG_A_I_PZ_GW01 20/02/2020 450 Sulfate mg/L DG_A_I_PZ_GW06 24/02/2020 1500 Sulfate mg/L DG_A_I_PZ_GW08 25/02/2020 1300 Sulfate mg/L DG_A_I_PZ_WRK301 25/02/2020 600 Sulfate mg/L DG_A_I_PZ_GW07 26/02/2020 890 Sulfate mg/L DG_A_I_PZ_BW45B 26/02/2020 810 Sulfate mg/L DG_A_I_PZ_BW28A 26/02/2020 850 Sulfate mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 310 Sulfate mg/L DG_A_I_PZ_GW02 3/03/2020 290 Sulfate mg/L DG_A_I_PZ_WRK304 5/03/2020 640 Sulfate mg/L DG_A_I_PZ_GW08 5/05/2020 1300 Thorium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.002

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

75

Variable Unit Sample Point Date Result Thorium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.0024 Thorium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.002 Thorium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.002 Total Dissolved Solids mg/L DG_A_I_PZ_GW07 9/01/2020 11000 Total Dissolved Solids mg/L DG_A_I_PZ_BW05 13/01/2020 15000 Total Dissolved Solids mg/L DG_A_I_PZ_BW28A 13/01/2020 14000 Total Dissolved Solids mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 1800 Total Dissolved Solids mg/L DG_A_I_PZ_GW03 14/01/2020 6700 Total Dissolved Solids mg/L DG_A_I_PZ_GW02 14/01/2020 4200 Total Dissolved Solids mg/L DG_A_I_PZ_IWB2 14/01/2020 2300 Total Dissolved Solids mg/L DG_A_I_PZ_IWB6 14/01/2020 1100 Total Dissolved Solids mg/L DG_A_I_PZ_GW01 15/01/2020 7400 Total Dissolved Solids mg/L DG_A_I_PZ_BW45B 15/01/2020 10000 Total Dissolved Solids mg/L DG_A_I_PZ_GW05 15/01/2020 5400 Total Dissolved Solids mg/L DG_A_I_PZ_GW04 15/01/2020 5600 Total Dissolved Solids mg/L DG_A_I_PZ_BW36A 16/01/2020 2900 Total Dissolved Solids mg/L DG_A_I_PZ_WRK300 16/01/2020 3600

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

76

Variable Unit Sample Point Date Result Total Dissolved Solids mg/L DG_A_I_PZ_GW08 20/01/2020 14000 Total Dissolved Solids mg/L DG_A_I_PZ_WRK302 20/01/2020 13000 Total Dissolved Solids mg/L DG_A_I_PZ_WRK304 22/01/2020 5600 Total Dissolved Solids mg/L DG_A_I_PZ_GW06 22/01/2020 15000 Total Dissolved Solids mg/L DG_A_I_PZ_WRK301 22/01/2020 6800 Total Dissolved Solids mg/L DG_A_I_PZ_WRK303 23/01/2020 5600 Total Dissolved Solids mg/L DG_A_I_PZ_IWB6 20/02/2020 1300 Total Dissolved Solids mg/L DG_A_I_PZ_GW04 20/02/2020 6100 Total Dissolved Solids mg/L DG_A_I_PZ_GW05 20/02/2020 5600 Total Dissolved Solids mg/L DG_A_I_PZ_GW01 20/02/2020 7000 Total Dissolved Solids mg/L DG_A_I_PZ_GW06 24/02/2020 14000 Total Dissolved Solids mg/L DG_A_I_PZ_GW08 25/02/2020 15000 Total Dissolved Solids mg/L DG_A_I_PZ_WRK301 25/02/2020 7100 Total Dissolved Solids mg/L DG_A_I_PZ_GW07 26/02/2020 11000 Total Dissolved Solids mg/L DG_A_I_PZ_BW45B 26/02/2020 11000 Total Dissolved Solids mg/L DG_A_I_PZ_BW28A 26/02/2020 15000 Total Dissolved Solids mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 1900 Total Dissolved Solids mg/L DG_A_I_PZ_GW02 3/03/2020 4000 Total Dissolved Solids mg/L DG_A_I_PZ_WRK304 5/03/2020 5000 Total Dissolved Solids mg/L DG_A_I_PZ_GW08 5/05/2020 14000 Uranium (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.004 Uranium (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.006 Uranium (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.006 Uranium (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.003 Uranium (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.005 Uranium (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

77

Variable Unit Sample Point Date Result Uranium (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.003 Uranium (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.005 Uranium (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.007 Uranium (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.007 Uranium (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.001 Uranium (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.001 Uranium 238 Bq/L DG_A_I_PZ_GW07 9/01/2020 2.04 Uranium 238 Bq/L DG_A_I_PZ_BW05 13/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_BW28A 13/01/2020 2.16 Uranium 238 Bq/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW03 14/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW02 14/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_IWB2 14/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_IWB6 14/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW01 15/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_BW45B 15/01/2020 0.099 Uranium 238 Bq/L DG_A_I_PZ_BW45B 15/01/2020 0.099 Uranium 238 Bq/L DG_A_I_PZ_GW05 15/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW04 15/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_BW36A 16/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_WRK300 16/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW08 20/01/2020 2.86 Uranium 238 Bq/L DG_A_I_PZ_WRK302 20/01/2020 0.296 Uranium 238 Bq/L DG_A_I_PZ_WRK304 22/01/2020 2.7 Uranium 238 Bq/L DG_A_I_PZ_GW06 22/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_WRK301 22/01/2020 0.037 Uranium 238 Bq/L DG_A_I_PZ_WRK303 23/01/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_IWB6 20/02/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW04 20/02/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW05 20/02/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW01 20/02/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_GW06 24/02/2020 1.33 Uranium 238 Bq/L DG_A_I_PZ_GW08 25/02/2020 1.31 Uranium 238 Bq/L DG_A_I_PZ_WRK301 25/02/2020 0.395 Uranium 238 Bq/L DG_A_I_PZ_GW07 26/02/2020 0.037 Uranium 238 Bq/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_BW45B 26/02/2020 0.086 Uranium 238 Bq/L DG_A_I_PZ_BW28A 26/02/2020 0.234 Uranium 238 Bq/L DG_A_I_PZ_GW02 3/03/2020 0.025 Uranium 238 Bq/L DG_A_I_PZ_WRK304 5/03/2020 0.025

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

78

Variable Unit Sample Point Date Result Uranium 238 Bq/L DG_A_I_PZ_GW08 5/05/2020 0.148 Zinc (Total) mg/L DG_A_I_PZ_GW07 9/01/2020 0.011 Zinc (Total) mg/L DG_A_I_PZ_BW05 13/01/2020 0.002 Zinc (Total) mg/L DG_A_I_PZ_BW28A 13/01/2020 0.006 Zinc (Total) mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0.007 Zinc (Total) mg/L DG_A_I_PZ_GW03 14/01/2020 0.049 Zinc (Total) mg/L DG_A_I_PZ_GW02 14/01/2020 0.015 Zinc (Total) mg/L DG_A_I_PZ_IWB2 14/01/2020 0.006 Zinc (Total) mg/L DG_A_I_PZ_IWB6 14/01/2020 0.004 Zinc (Total) mg/L DG_A_I_PZ_GW01 15/01/2020 0.037 Zinc (Total) mg/L DG_A_I_PZ_BW45B 15/01/2020 0.044 Zinc (Total) mg/L DG_A_I_PZ_GW05 15/01/2020 0.02 Zinc (Total) mg/L DG_A_I_PZ_GW04 15/01/2020 0.014 Zinc (Total) mg/L DG_A_I_PZ_BW36A 16/01/2020 0.019 Zinc (Total) mg/L DG_A_I_PZ_WRK300 16/01/2020 0.012 Zinc (Total) mg/L DG_A_I_PZ_GW08 20/01/2020 0.027 Zinc (Total) mg/L DG_A_I_PZ_WRK302 20/01/2020 0.012 Zinc (Total) mg/L DG_A_I_PZ_WRK304 22/01/2020 0.017 Zinc (Total) mg/L DG_A_I_PZ_GW06 22/01/2020 0.005 Zinc (Total) mg/L DG_A_I_PZ_WRK301 22/01/2020 0.018 Zinc (Total) mg/L DG_A_I_PZ_WRK303 23/01/2020 0.016 Zinc (Total) mg/L DG_A_I_PZ_IWB6 20/02/2020 0.006 Zinc (Total) mg/L DG_A_I_PZ_GW04 20/02/2020 0.014 Zinc (Total) mg/L DG_A_I_PZ_GW05 20/02/2020 0.023 Zinc (Total) mg/L DG_A_I_PZ_GW01 20/02/2020 0.016 Zinc (Total) mg/L DG_A_I_PZ_GW06 24/02/2020 0.004 Zinc (Total) mg/L DG_A_I_PZ_GW08 25/02/2020 0.026 Zinc (Total) mg/L DG_A_I_PZ_WRK301 25/02/2020 0.01 Zinc (Total) mg/L DG_A_I_PZ_GW07 26/02/2020 0.009 Zinc (Total) mg/L DG_A_I_PZ_BW45B 26/02/2020 0.035 Zinc (Total) mg/L DG_A_I_PZ_BW28A 26/02/2020 0.007 Zinc (Total) mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0.012 Zinc (Total) mg/L DG_A_I_PZ_GW02 3/03/2020 0.03 Zinc (Total) mg/L DG_A_I_PZ_WRK304 5/03/2020 0.012 Zinc (Total) mg/L DG_A_I_PZ_GW08 5/05/2020 0.024 Results that are italicised are equal to less than values i.e. 0.001 = <0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

79

Appendix C: Monitoring Data (Field) – Groundwater

Variable Unit Sample Point Date Result Dissolved Oxygen mg/L DG_A_I_PZ_GW07 9/01/2020 8.1 Dissolved Oxygen mg/L DG_A_I_PZ_BW05 13/01/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_BW28A 13/01/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_BW53/Puls 13/01/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_GW02 14/01/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 14/01/2020 0.5 Dissolved Oxygen mg/L DG_A_I_PZ_IWB2 14/01/2020 0.1 Dissolved Oxygen mg/L DG_A_I_PZ_IWB6 14/01/2020 4.1 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 15/01/2020 5.3 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 15/01/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 15/01/2020 0.2 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 15/01/2020 3.9 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 16/01/2020 0.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 16/01/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 20/01/2020 4.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 20/01/2020 7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 22/01/2020 10.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 22/01/2020 7.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 22/01/2020 1.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 23/01/2020 9.8 Dissolved Oxygen mg/L DG_A_I_PZ_IWB6 20/02/2020 3.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 20/02/2020 5 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 20/02/2020 0.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 20/02/2020 5 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 24/02/2020 8.2 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 24/02/2020 7.1 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 24/02/2020 8.7 Dissolved Oxygen mg/L DG_A_I_PZ_BW05 24/02/2020 0.1 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 25/02/2020 4 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 25/02/2020 1.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW07 26/02/2020 7.1 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 26/02/2020 0.4 Dissolved Oxygen mg/L DG_A_I_PZ_BW28A 26/02/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_BW53/Puls 26/02/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 27/02/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 27/02/2020 1 Dissolved Oxygen mg/L DG_A_I_PZ_IWB2 27/02/2020 0.1 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 28/02/2020 0.5 Dissolved Oxygen mg/L DG_A_I_PZ_GW02 3/03/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 5/03/2020 9.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW07 18/03/2020 9.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 19/03/2020 0.5

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

80

Variable Unit Sample Point Date Result Dissolved Oxygen mg/L DG_A_I_PZ_GW02 19/03/2020 2.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 19/03/2020 0.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 20/03/2020 5 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 20/03/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 20/03/2020 4.5 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 23/03/2020 0.1 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 23/03/2020 0.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 23/03/2020 9.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 23/03/2020 6.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 23/03/2020 5.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 24/03/2020 10.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 24/03/2020 9.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 24/03/2020 1 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 6/04/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW02 6/04/2020 2 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 6/04/2020 2.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 6/04/2020 5.5 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 7/04/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW07 7/04/2020 10.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 7/04/2020 0.8 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 7/04/2020 0.1 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 7/04/2020 4.2 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 14/04/2020 4.5 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 14/04/2020 9.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 14/04/2020 6.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 14/04/2020 9.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 14/04/2020 9.2 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 14/04/2020 1.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW07 1/05/2020 8.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 1/05/2020 0.6 Dissolved Oxygen mg/L DG_A_I_PZ_GW02 1/05/2020 1.7 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 5/05/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 5/05/2020 5.6 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 5/05/2020 6.8 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 5/05/2020 8.5 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 5/05/2020 4.3 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 6/05/2020 0.6 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 6/05/2020 4.6 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 6/05/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 6/05/2020 0.5 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 8/05/2020 10.3 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 8/05/2020 9.2 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 8/05/2020 1 Dissolved Oxygen mg/L DG_A_I_PZ_GW03 11/06/2020 1.4

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

81

Variable Unit Sample Point Date Result Dissolved Oxygen mg/L DG_A_I_PZ_GW02 11/06/2020 2.2 Dissolved Oxygen mg/L DG_A_I_PZ_BW45B 11/06/2020 0.3 Dissolved Oxygen mg/L DG_A_I_PZ_GW05 11/06/2020 0.6 Dissolved Oxygen mg/L DG_A_I_PZ_WRK303 16/06/2020 9.2 Dissolved Oxygen mg/L DG_A_I_PZ_WRK301 16/06/2020 0.8 Dissolved Oxygen mg/L DG_A_I_PZ_WRK302 16/06/2020 6.7 Dissolved Oxygen mg/L DG_A_I_PZ_WRK304 16/06/2020 9.5 Dissolved Oxygen mg/L DG_A_I_PZ_GW08 16/06/2020 7.9 Dissolved Oxygen mg/L DG_A_I_PZ_GW06 16/06/2020 8 Dissolved Oxygen mg/L DG_A_I_PZ_GW07 17/06/2020 9.4 Dissolved Oxygen mg/L DG_A_I_PZ_GW04 17/06/2020 6.2 Dissolved Oxygen mg/L DG_A_I_PZ_BW36A 17/06/2020 0 Dissolved Oxygen mg/L DG_A_I_PZ_GW01 17/06/2020 4.4 Dissolved Oxygen mg/L DG_A_I_PZ_WRK300 17/06/2020 0.6 Dissolved Oxygen Field % DG_A_I_PZ_GW07 9/01/2020 96 Dissolved Oxygen Field % DG_A_I_PZ_BW05 13/01/2020 4 Dissolved Oxygen Field % DG_A_I_PZ_BW28A 13/01/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_BW53/Puls 13/01/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_GW02 14/01/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_GW03 14/01/2020 11 Dissolved Oxygen Field % DG_A_I_PZ_IWB2 14/01/2020 1 Dissolved Oxygen Field % DG_A_I_PZ_IWB6 14/01/2020 44 Dissolved Oxygen Field % DG_A_I_PZ_GW01 15/01/2020 65 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 15/01/2020 3 Dissolved Oxygen Field % DG_A_I_PZ_GW05 15/01/2020 5 Dissolved Oxygen Field % DG_A_I_PZ_GW04 15/01/2020 45 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 16/01/2020 2 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 16/01/2020 4 Dissolved Oxygen Field % DG_A_I_PZ_GW08 20/01/2020 51 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 20/01/2020 80 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 22/01/2020 123 Dissolved Oxygen Field % DG_A_I_PZ_GW06 22/01/2020 94 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 22/01/2020 21 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 23/01/2020 98 Dissolved Oxygen Field % DG_A_I_PZ_IWB6 20/02/2020 37 Dissolved Oxygen Field % DG_A_I_PZ_GW04 20/02/2020 62 Dissolved Oxygen Field % DG_A_I_PZ_GW05 20/02/2020 8 Dissolved Oxygen Field % DG_A_I_PZ_GW01 20/02/2020 62 Dissolved Oxygen Field % DG_A_I_PZ_GW06 24/02/2020 83 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 24/02/2020 82 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 24/02/2020 108 Dissolved Oxygen Field % DG_A_I_PZ_BW05 24/02/2020 1 Dissolved Oxygen Field % DG_A_I_PZ_GW08 25/02/2020 46 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 25/02/2020 15

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

82

Variable Unit Sample Point Date Result Dissolved Oxygen Field % DG_A_I_PZ_GW07 26/02/2020 91 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 26/02/2020 4 Dissolved Oxygen Field % DG_A_I_PZ_BW28A 26/02/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_BW53/Puls 26/02/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 27/02/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_GW03 27/02/2020 23 Dissolved Oxygen Field % DG_A_I_PZ_IWB2 27/02/2020 1 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 28/02/2020 7 Dissolved Oxygen Field % DG_A_I_PZ_GW02 3/03/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 5/03/2020 110 Dissolved Oxygen Field % DG_A_I_PZ_GW07 18/03/2020 115 Dissolved Oxygen Field % DG_A_I_PZ_GW03 19/03/2020 7 Dissolved Oxygen Field % DG_A_I_PZ_GW02 19/03/2020 26 Dissolved Oxygen Field % DG_A_I_PZ_GW05 19/03/2020 8 Dissolved Oxygen Field % DG_A_I_PZ_GW04 20/03/2020 55 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 20/03/2020 2 Dissolved Oxygen Field % DG_A_I_PZ_GW01 20/03/2020 50 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 23/03/2020 5 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 23/03/2020 17 Dissolved Oxygen Field % DG_A_I_PZ_GW06 23/03/2020 112 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 23/03/2020 78 Dissolved Oxygen Field % DG_A_I_PZ_GW08 23/03/2020 58 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 24/03/2020 117 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 24/03/2020 107 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 24/03/2020 12 Dissolved Oxygen Field % DG_A_I_PZ_GW03 6/04/2020 2 Dissolved Oxygen Field % DG_A_I_PZ_GW02 6/04/2020 28 Dissolved Oxygen Field % DG_A_I_PZ_GW05 6/04/2020 26 Dissolved Oxygen Field % DG_A_I_PZ_GW04 6/04/2020 61 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 7/04/2020 5 Dissolved Oxygen Field % DG_A_I_PZ_GW07 7/04/2020 124 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 7/04/2020 14 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 7/04/2020 4 Dissolved Oxygen Field % DG_A_I_PZ_GW01 7/04/2020 46 Dissolved Oxygen Field % DG_A_I_PZ_GW08 14/04/2020 42 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 14/04/2020 110 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 14/04/2020 79 Dissolved Oxygen Field % DG_A_I_PZ_GW06 14/04/2020 112 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 14/04/2020 106 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 14/04/2020 16 Dissolved Oxygen Field % DG_A_I_PZ_GW07 1/05/2020 102 Dissolved Oxygen Field % DG_A_I_PZ_GW03 1/05/2020 10 Dissolved Oxygen Field % DG_A_I_PZ_GW02 1/05/2020 29 Dissolved Oxygen Field % DG_A_I_PZ_GW05 5/05/2020 7

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

83

Variable Unit Sample Point Date Result Dissolved Oxygen Field % DG_A_I_PZ_GW04 5/05/2020 59 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 5/05/2020 76 Dissolved Oxygen Field % DG_A_I_PZ_GW06 5/05/2020 98 Dissolved Oxygen Field % DG_A_I_PZ_GW08 5/05/2020 45 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 6/05/2020 10 Dissolved Oxygen Field % DG_A_I_PZ_GW01 6/05/2020 48 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 6/05/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 6/05/2020 11 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 8/05/2020 110 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 8/05/2020 101 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 8/05/2020 10 Dissolved Oxygen Field % DG_A_I_PZ_GW03 11/06/2020 11 Dissolved Oxygen Field % DG_A_I_PZ_GW02 11/06/2020 25 Dissolved Oxygen Field % DG_A_I_PZ_BW45B 11/06/2020 5 Dissolved Oxygen Field % DG_A_I_PZ_GW05 11/06/2020 12 Dissolved Oxygen Field % DG_A_I_PZ_WRK303 16/06/2020 99 Dissolved Oxygen Field % DG_A_I_PZ_WRK301 16/06/2020 9 Dissolved Oxygen Field % DG_A_I_PZ_WRK302 16/06/2020 76 Dissolved Oxygen Field % DG_A_I_PZ_WRK304 16/06/2020 101 Dissolved Oxygen Field % DG_A_I_PZ_GW08 16/06/2020 90 Dissolved Oxygen Field % DG_A_I_PZ_GW06 16/06/2020 89 Dissolved Oxygen Field % DG_A_I_PZ_GW07 17/06/2020 106 Dissolved Oxygen Field % DG_A_I_PZ_GW04 17/06/2020 66 Dissolved Oxygen Field % DG_A_I_PZ_BW36A 17/06/2020 0 Dissolved Oxygen Field % DG_A_I_PZ_GW01 17/06/2020 46 Dissolved Oxygen Field % DG_A_I_PZ_WRK300 17/06/2020 18 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 9/01/2020 18000 Electrical Conductivity µS/cm DG_A_I_PZ_BW05 13/01/2020 23000 Electrical Conductivity µS/cm DG_A_I_PZ_BW28A 13/01/2020 21000 Electrical Conductivity µS/cm DG_A_I_PZ_BW53/Puls 13/01/2020 3100 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 14/01/2020 7200 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 14/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_IWB2 14/01/2020 4100 Electrical Conductivity µS/cm DG_A_I_PZ_IWB6 14/01/2020 1700 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 15/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 15/01/2020 16000 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 15/01/2020 9100 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 15/01/2020 9500 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 16/01/2020 4800 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 16/01/2020 6200 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 20/01/2020 20000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 20/01/2020 19000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 22/01/2020 9000 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 22/01/2020 21000

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

84

Variable Unit Sample Point Date Result Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 22/01/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 23/01/2020 9100 Electrical Conductivity µS/cm DG_A_I_PZ_IWB6 20/02/2020 1600 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 20/02/2020 9200 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 20/02/2020 8800 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 20/02/2020 11000 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 24/02/2020 20000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 24/02/2020 21418 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 24/02/2020 11028 Electrical Conductivity µS/cm DG_A_I_PZ_BW05 24/02/2020 26137 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 25/02/2020 19000 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 25/02/2020 10000 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 26/02/2020 17000 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 26/02/2020 15000 Electrical Conductivity µS/cm DG_A_I_PZ_BW28A 26/02/2020 21000 Electrical Conductivity µS/cm DG_A_I_PZ_BW53/Puls 26/02/2020 3100 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 27/02/2020 6264 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 27/02/2020 11744 Electrical Conductivity µS/cm DG_A_I_PZ_IWB2 27/02/2020 4391 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 28/02/2020 6702 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 3/03/2020 6800 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 5/03/2020 8800 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 18/03/2020 18659 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 19/03/2020 11466 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 19/03/2020 7661 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 19/03/2020 9930 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 20/03/2020 10246 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 20/03/2020 17176 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 20/03/2020 11894 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 23/03/2020 6579 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 23/03/2020 6524 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 23/03/2020 21654 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 23/03/2020 21205 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 23/03/2020 21994 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 24/03/2020 8880 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 24/03/2020 10494 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 24/03/2020 11729 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 6/04/2020 10786 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 6/04/2020 6985 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 6/04/2020 8969 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 6/04/2020 9537 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 7/04/2020 16100 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 7/04/2020 17634 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 7/04/2020 6109

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

85

Variable Unit Sample Point Date Result Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 7/04/2020 6147 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 7/04/2020 10768 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 14/04/2020 20165 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 14/04/2020 9188 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 14/04/2020 19537 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 14/04/2020 20786 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 14/04/2020 10163 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 14/04/2020 10855 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 1/05/2020 18549 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 1/05/2020 11556 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 1/05/2020 7680 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 5/05/2020 9644 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 5/05/2020 10199 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 5/05/2020 21063 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 5/05/2020 21656 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 5/05/2020 20000 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 6/05/2020 17490 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 6/05/2020 11635 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 6/05/2020 6792 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 6/05/2020 6527 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 8/05/2020 9028 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 8/05/2020 10206 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 8/05/2020 11777 Electrical Conductivity µS/cm DG_A_I_PZ_GW03 11/06/2020 11544 Electrical Conductivity µS/cm DG_A_I_PZ_GW02 11/06/2020 7351 Electrical Conductivity µS/cm DG_A_I_PZ_BW45B 11/06/2020 17545 Electrical Conductivity µS/cm DG_A_I_PZ_GW05 11/06/2020 9582 Electrical Conductivity µS/cm DG_A_I_PZ_WRK303 16/06/2020 11423 Electrical Conductivity µS/cm DG_A_I_PZ_WRK301 16/06/2020 11866 Electrical Conductivity µS/cm DG_A_I_PZ_WRK302 16/06/2020 21094 Electrical Conductivity µS/cm DG_A_I_PZ_WRK304 16/06/2020 9211 Electrical Conductivity µS/cm DG_A_I_PZ_GW08 16/06/2020 21647 Electrical Conductivity µS/cm DG_A_I_PZ_GW06 16/06/2020 21615 Electrical Conductivity µS/cm DG_A_I_PZ_GW07 17/06/2020 18941 Electrical Conductivity µS/cm DG_A_I_PZ_GW04 17/06/2020 10215 Electrical Conductivity µS/cm DG_A_I_PZ_BW36A 17/06/2020 7029 Electrical Conductivity µS/cm DG_A_I_PZ_GW01 17/06/2020 11626 Electrical Conductivity µS/cm DG_A_I_PZ_WRK300 17/06/2020 6543 pH pH units DG_A_I_PZ_GW07 9/01/2020 6.22 pH pH units DG_A_I_PZ_BW05 13/01/2020 6.98 pH pH units DG_A_I_PZ_BW28A 13/01/2020 6.45 pH pH units DG_A_I_PZ_BW53/Puls 13/01/2020 6.8 pH pH units DG_A_I_PZ_GW02 14/01/2020 5.4 pH pH units DG_A_I_PZ_GW03 14/01/2020 6.13

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

86

Variable Unit Sample Point Date Result pH pH units DG_A_I_PZ_IWB2 14/01/2020 5.43 pH pH units DG_A_I_PZ_IWB6 14/01/2020 5.35 pH pH units DG_A_I_PZ_GW01 15/01/2020 5.36 pH pH units DG_A_I_PZ_BW45B 15/01/2020 4.72 pH pH units DG_A_I_PZ_GW05 15/01/2020 5.85 pH pH units DG_A_I_PZ_GW04 15/01/2020 5.63 pH pH units DG_A_I_PZ_BW36A 16/01/2020 6.83 pH pH units DG_A_I_PZ_WRK300 16/01/2020 6.69 pH pH units DG_A_I_PZ_GW08 20/01/2020 6.2 pH pH units DG_A_I_PZ_WRK302 20/01/2020 5.93 pH pH units DG_A_I_PZ_WRK304 22/01/2020 6.07 pH pH units DG_A_I_PZ_GW06 22/01/2020 6.49 pH pH units DG_A_I_PZ_WRK301 22/01/2020 6.96 pH pH units DG_A_I_PZ_WRK303 23/01/2020 5.83 pH pH units DG_A_I_PZ_IWB6 20/02/2020 5.18 pH pH units DG_A_I_PZ_GW04 20/02/2020 5.41 pH pH units DG_A_I_PZ_GW05 20/02/2020 5.72 pH pH units DG_A_I_PZ_GW01 20/02/2020 5.13 pH pH units DG_A_I_PZ_GW06 24/02/2020 6.28 pH pH units DG_A_I_PZ_WRK302 24/02/2020 5.74 pH pH units DG_A_I_PZ_WRK303 24/02/2020 5.63 pH pH units DG_A_I_PZ_BW05 24/02/2020 6.84 pH pH units DG_A_I_PZ_GW08 25/02/2020 6.06 pH pH units DG_A_I_PZ_WRK301 25/02/2020 6.79 pH pH units DG_A_I_PZ_GW07 26/02/2020 6.2 pH pH units DG_A_I_PZ_BW45B 26/02/2020 4.7 pH pH units DG_A_I_PZ_BW28A 26/02/2020 6.32 pH pH units DG_A_I_PZ_BW53/Puls 26/02/2020 6.41 pH pH units DG_A_I_PZ_BW36A 27/02/2020 6.56 pH pH units DG_A_I_PZ_GW03 27/02/2020 5.95 pH pH units DG_A_I_PZ_IWB2 27/02/2020 5.33 pH pH units DG_A_I_PZ_WRK300 28/02/2020 6.55 pH pH units DG_A_I_PZ_GW02 3/03/2020 5.26 pH pH units DG_A_I_PZ_WRK304 5/03/2020 5.9 pH pH units DG_A_I_PZ_GW07 18/03/2020 6.42 pH pH units DG_A_I_PZ_GW03 19/03/2020 6.26 pH pH units DG_A_I_PZ_GW02 19/03/2020 5.51 pH pH units DG_A_I_PZ_GW05 19/03/2020 5.91 pH pH units DG_A_I_PZ_GW04 20/03/2020 5.63 pH pH units DG_A_I_PZ_BW45B 20/03/2020 4.59 pH pH units DG_A_I_PZ_GW01 20/03/2020 5.33 pH pH units DG_A_I_PZ_BW36A 23/03/2020 6.68 pH pH units DG_A_I_PZ_WRK300 23/03/2020 6.57 pH pH units DG_A_I_PZ_GW06 23/03/2020 6.45

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

87

Variable Unit Sample Point Date Result pH pH units DG_A_I_PZ_WRK302 23/03/2020 5.93 pH pH units DG_A_I_PZ_GW08 23/03/2020 6.18 pH pH units DG_A_I_PZ_WRK304 24/03/2020 6.04 pH pH units DG_A_I_PZ_WRK303 24/03/2020 5.8 pH pH units DG_A_I_PZ_WRK301 24/03/2020 6.96 pH pH units DG_A_I_PZ_GW03 6/04/2020 6.13 pH pH units DG_A_I_PZ_GW02 6/04/2020 5.42 pH pH units DG_A_I_PZ_GW05 6/04/2020 5.91 pH pH units DG_A_I_PZ_GW04 6/04/2020 5.59 pH pH units DG_A_I_PZ_BW45B 7/04/2020 4.52 pH pH units DG_A_I_PZ_GW07 7/04/2020 6.27 pH pH units DG_A_I_PZ_WRK300 7/04/2020 6.59 pH pH units DG_A_I_PZ_BW36A 7/04/2020 6.71 pH pH units DG_A_I_PZ_GW01 7/04/2020 5.25 pH pH units DG_A_I_PZ_GW08 14/04/2020 6.24 pH pH units DG_A_I_PZ_WRK304 14/04/2020 6.07 pH pH units DG_A_I_PZ_WRK302 14/04/2020 5.97 pH pH units DG_A_I_PZ_GW06 14/04/2020 6.5 pH pH units DG_A_I_PZ_WRK303 14/04/2020 5.86 pH pH units DG_A_I_PZ_WRK301 14/04/2020 6.95 pH pH units DG_A_I_PZ_GW07 1/05/2020 6.36 pH pH units DG_A_I_PZ_GW03 1/05/2020 6.09 pH pH units DG_A_I_PZ_GW02 1/05/2020 5.36 pH pH units DG_A_I_PZ_GW05 5/05/2020 5.85 pH pH units DG_A_I_PZ_GW04 5/05/2020 5.54 pH pH units DG_A_I_PZ_WRK302 5/05/2020 5.93 pH pH units DG_A_I_PZ_GW06 5/05/2020 6.47 pH pH units DG_A_I_PZ_GW08 5/05/2020 6.21 pH pH units DG_A_I_PZ_BW45B 6/05/2020 4.34 pH pH units DG_A_I_PZ_GW01 6/05/2020 5.27 pH pH units DG_A_I_PZ_BW36A 6/05/2020 6.67 pH pH units DG_A_I_PZ_WRK300 6/05/2020 6.57 pH pH units DG_A_I_PZ_WRK304 8/05/2020 6.03 pH pH units DG_A_I_PZ_WRK303 8/05/2020 5.83 pH pH units DG_A_I_PZ_WRK301 8/05/2020 6.94 pH pH units DG_A_I_PZ_GW03 11/06/2020 6.23 pH pH units DG_A_I_PZ_GW02 11/06/2020 5.5 pH pH units DG_A_I_PZ_BW45B 11/06/2020 4.48 pH pH units DG_A_I_PZ_GW05 11/06/2020 5.95 pH pH units DG_A_I_PZ_WRK303 16/06/2020 5.92 pH pH units DG_A_I_PZ_WRK301 16/06/2020 7.04 pH pH units DG_A_I_PZ_WRK302 16/06/2020 6.02 pH pH units DG_A_I_PZ_WRK304 16/06/2020 6.15 pH pH units DG_A_I_PZ_GW08 16/06/2020 6.3

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

88

Variable Unit Sample Point Date Result pH pH units DG_A_I_PZ_GW06 16/06/2020 6.6 pH pH units DG_A_I_PZ_GW07 17/06/2020 6.38 pH pH units DG_A_I_PZ_GW04 17/06/2020 5.72 pH pH units DG_A_I_PZ_BW36A 17/06/2020 6.78 pH pH units DG_A_I_PZ_GW01 17/06/2020 5.45 pH pH units DG_A_I_PZ_WRK300 17/06/2020 6.66 Redox Potential (Eh) mV DG_A_I_PZ_GW07 9/01/2020 568 Redox Potential (Eh) mV DG_A_I_PZ_BW05 13/01/2020 50 Redox Potential (Eh) mV DG_A_I_PZ_BW28A 13/01/2020 196 Redox Potential (Eh) mV DG_A_I_PZ_BW53/Puls 13/01/2020 -191 Redox Potential (Eh) mV DG_A_I_PZ_GW02 14/01/2020 304 Redox Potential (Eh) mV DG_A_I_PZ_GW03 14/01/2020 119 Redox Potential (Eh) mV DG_A_I_PZ_IWB2 14/01/2020 440 Redox Potential (Eh) mV DG_A_I_PZ_IWB6 14/01/2020 485 Redox Potential (Eh) mV DG_A_I_PZ_GW01 15/01/2020 217 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 15/01/2020 281 Redox Potential (Eh) mV DG_A_I_PZ_GW05 15/01/2020 187 Redox Potential (Eh) mV DG_A_I_PZ_GW04 15/01/2020 197 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 16/01/2020 -34 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 16/01/2020 239 Redox Potential (Eh) mV DG_A_I_PZ_GW08 20/01/2020 192 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 20/01/2020 243 Redox Potential (Eh) mV DG_A_I_PZ_WRK304 22/01/2020 217 Redox Potential (Eh) mV DG_A_I_PZ_GW06 22/01/2020 493 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 22/01/2020 486 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 23/01/2020 170 Redox Potential (Eh) mV DG_A_I_PZ_IWB6 20/02/2020 236 Redox Potential (Eh) mV DG_A_I_PZ_GW04 20/02/2020 240 Redox Potential (Eh) mV DG_A_I_PZ_GW05 20/02/2020 210 Redox Potential (Eh) mV DG_A_I_PZ_GW01 20/02/2020 250 Redox Potential (Eh) mV DG_A_I_PZ_GW06 24/02/2020 227 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 24/02/2020 370 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 24/02/2020 415 Redox Potential (Eh) mV DG_A_I_PZ_BW05 24/02/2020 49 Redox Potential (Eh) mV DG_A_I_PZ_GW08 25/02/2020 182 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 25/02/2020 374 Redox Potential (Eh) mV DG_A_I_PZ_GW07 26/02/2020 162 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 26/02/2020 242 Redox Potential (Eh) mV DG_A_I_PZ_BW28A 26/02/2020 -8 Redox Potential (Eh) mV DG_A_I_PZ_BW53/Puls 26/02/2020 -35 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 27/02/2020 -56 Redox Potential (Eh) mV DG_A_I_PZ_GW03 27/02/2020 65 Redox Potential (Eh) mV DG_A_I_PZ_IWB2 27/02/2020 192 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 28/02/2020 135

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

89

Variable Unit Sample Point Date Result Redox Potential (Eh) mV DG_A_I_PZ_GW02 3/03/2020 276 Redox Potential (Eh) mV DG_A_I_PZ_WRK304 5/03/2020 237 Redox Potential (Eh) mV DG_A_I_PZ_GW07 18/03/2020 366 Redox Potential (Eh) mV DG_A_I_PZ_GW03 19/03/2020 55 Redox Potential (Eh) mV DG_A_I_PZ_GW02 19/03/2020 270 Redox Potential (Eh) mV DG_A_I_PZ_GW05 19/03/2020 256 Redox Potential (Eh) mV DG_A_I_PZ_GW04 20/03/2020 198 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 20/03/2020 350 Redox Potential (Eh) mV DG_A_I_PZ_GW01 20/03/2020 276 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 23/03/2020 -42 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 23/03/2020 112 Redox Potential (Eh) mV DG_A_I_PZ_GW06 23/03/2020 161 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 23/03/2020 207 Redox Potential (Eh) mV DG_A_I_PZ_GW08 23/03/2020 184 Redox Potential (Eh) mV DG_A_I_PZ_WRK304 24/03/2020 164 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 24/03/2020 186 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 24/03/2020 112 Redox Potential (Eh) mV DG_A_I_PZ_GW03 6/04/2020 76 Redox Potential (Eh) mV DG_A_I_PZ_GW02 6/04/2020 207 Redox Potential (Eh) mV DG_A_I_PZ_GW05 6/04/2020 237 Redox Potential (Eh) mV DG_A_I_PZ_GW04 6/04/2020 300 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 7/04/2020 306 Redox Potential (Eh) mV DG_A_I_PZ_GW07 7/04/2020 176 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 7/04/2020 184 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 7/04/2020 -11 Redox Potential (Eh) mV DG_A_I_PZ_GW01 7/04/2020 274 Redox Potential (Eh) mV DG_A_I_PZ_GW08 14/04/2020 209 Redox Potential (Eh) mV DG_A_I_PZ_WRK304 14/04/2020 363 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 14/04/2020 399 Redox Potential (Eh) mV DG_A_I_PZ_GW06 14/04/2020 470 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 14/04/2020 360 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 14/04/2020 190 Redox Potential (Eh) mV DG_A_I_PZ_GW07 1/05/2020 129 Redox Potential (Eh) mV DG_A_I_PZ_GW03 1/05/2020 -10 Redox Potential (Eh) mV DG_A_I_PZ_GW02 1/05/2020 173 Redox Potential (Eh) mV DG_A_I_PZ_GW05 5/05/2020 356 Redox Potential (Eh) mV DG_A_I_PZ_GW04 5/05/2020 590 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 5/05/2020 268 Redox Potential (Eh) mV DG_A_I_PZ_GW06 5/05/2020 208 Redox Potential (Eh) mV DG_A_I_PZ_GW08 5/05/2020 168 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 6/05/2020 343 Redox Potential (Eh) mV DG_A_I_PZ_GW01 6/05/2020 283 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 6/05/2020 -26 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 6/05/2020 185

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

90

Variable Unit Sample Point Date Result Redox Potential (Eh) mV DG_A_I_PZ_WRK304 8/05/2020 209 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 8/05/2020 245 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 8/05/2020 180 Redox Potential (Eh) mV DG_A_I_PZ_GW03 11/06/2020 43 Redox Potential (Eh) mV DG_A_I_PZ_GW02 11/06/2020 220 Redox Potential (Eh) mV DG_A_I_PZ_BW45B 11/06/2020 279 Redox Potential (Eh) mV DG_A_I_PZ_GW05 11/06/2020 308 Redox Potential (Eh) mV DG_A_I_PZ_WRK303 16/06/2020 222 Redox Potential (Eh) mV DG_A_I_PZ_WRK301 16/06/2020 117 Redox Potential (Eh) mV DG_A_I_PZ_WRK302 16/06/2020 217 Redox Potential (Eh) mV DG_A_I_PZ_WRK304 16/06/2020 191 Redox Potential (Eh) mV DG_A_I_PZ_GW08 16/06/2020 177 Redox Potential (Eh) mV DG_A_I_PZ_GW06 16/06/2020 211 Redox Potential (Eh) mV DG_A_I_PZ_GW07 17/06/2020 180 Redox Potential (Eh) mV DG_A_I_PZ_GW04 17/06/2020 202 Redox Potential (Eh) mV DG_A_I_PZ_BW36A 17/06/2020 -28 Redox Potential (Eh) mV DG_A_I_PZ_GW01 17/06/2020 240 Redox Potential (Eh) mV DG_A_I_PZ_WRK300 17/06/2020 200 Standing Water Level mAHD DG_A_I_PZ_GW07 9/01/2020 172.436 Standing Water Level mAHD DG_A_I_PZ_BW05 13/01/2020 147.299 Standing Water Level mAHD DG_A_I_PZ_BW28A 13/01/2020 177.055 Standing Water Level mAHD DG_A_I_PZ_BW53/Puls 13/01/2020 175.83 Standing Water Level mAHD DG_A_I_PZ_GW02 14/01/2020 170.81 Standing Water Level mAHD DG_A_I_PZ_GW03 14/01/2020 162.07 Standing Water Level mAHD DG_A_I_PZ_IWB2 14/01/2020 179.706 Standing Water Level mAHD DG_A_I_PZ_IWB6 14/01/2020 176.74 Standing Water Level mAHD DG_A_I_PZ_GW01 15/01/2020 173.435 Standing Water Level mAHD DG_A_I_PZ_BW45B 15/01/2020 177.38 Standing Water Level mAHD DG_A_I_PZ_GW05 15/01/2020 179 Standing Water Level mAHD DG_A_I_PZ_GW04 15/01/2020 178.39 Standing Water Level mAHD DG_A_I_PZ_BW36A 16/01/2020 174.525 Standing Water Level mAHD DG_A_I_PZ_GW08 20/01/2020 177.66 Standing Water Level mAHD DG_A_I_PZ_WRK302 20/01/2020 176.59 Standing Water Level mAHD DG_A_I_PZ_WRK304 22/01/2020 180.36 Standing Water Level mAHD DG_A_I_PZ_GW06 22/01/2020 176.224 Standing Water Level mAHD DG_A_I_PZ_WRK301 22/01/2020 178.18 Standing Water Level mAHD DG_A_I_PZ_WRK303 23/01/2020 179.52 Standing Water Level mAHD DG_A_I_PZ_IWB6 20/02/2020 176.82 Standing Water Level mAHD DG_A_I_PZ_GW04 20/02/2020 178.38 Standing Water Level mAHD DG_A_I_PZ_GW05 20/02/2020 178.94 Standing Water Level mAHD DG_A_I_PZ_GW01 20/02/2020 173.405 Standing Water Level mAHD DG_A_I_PZ_GW06 24/02/2020 176.134 Standing Water Level mAHD DG_A_I_PZ_WRK302 24/02/2020 176.67 Standing Water Level mAHD DG_A_I_PZ_WRK303 24/02/2020 179.8

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

91

Variable Unit Sample Point Date Result Standing Water Level mAHD DG_A_I_PZ_BW05 24/02/2020 147.459 Standing Water Level mAHD DG_A_I_PZ_GW08 25/02/2020 177.5 Standing Water Level mAHD DG_A_I_PZ_WRK301 25/02/2020 178.16 Standing Water Level mAHD DG_A_I_PZ_GW07 26/02/2020 172.476 Standing Water Level mAHD DG_A_I_PZ_BW45B 26/02/2020 177.31 Standing Water Level mAHD DG_A_I_PZ_BW28A 26/02/2020 176.835 Standing Water Level mAHD DG_A_I_PZ_BW53/Puls 26/02/2020 175.84 Standing Water Level mAHD DG_A_I_PZ_BW36A 27/02/2020 174.505 Standing Water Level mAHD DG_A_I_PZ_GW03 27/02/2020 162.14 Standing Water Level mAHD DG_A_I_PZ_IWB2 27/02/2020 179.676 Standing Water Level mAHD DG_A_I_PZ_GW02 3/03/2020 170.79 Standing Water Level mAHD DG_A_I_PZ_WRK304 5/03/2020 180.29 Standing Water Level mAHD DG_A_I_PZ_GW07 18/03/2020 172.466 Standing Water Level mAHD DG_A_I_PZ_GW03 19/03/2020 162.12 Standing Water Level mAHD DG_A_I_PZ_GW02 19/03/2020 170.76 Standing Water Level mAHD DG_A_I_PZ_GW05 19/03/2020 178.98 Standing Water Level mAHD DG_A_I_PZ_GW04 20/03/2020 178.43 Standing Water Level mAHD DG_A_I_PZ_BW45B 20/03/2020 177.35 Standing Water Level mAHD DG_A_I_PZ_GW01 20/03/2020 173.425 Standing Water Level mAHD DG_A_I_PZ_BW36A 23/03/2020 174.535 Standing Water Level mAHD DG_A_I_PZ_GW06 23/03/2020 176.224 Standing Water Level mAHD DG_A_I_PZ_WRK302 23/03/2020 176.62 Standing Water Level mAHD DG_A_I_PZ_GW08 23/03/2020 177.63 Standing Water Level mAHD DG_A_I_PZ_WRK304 24/03/2020 180.35 Standing Water Level mAHD DG_A_I_PZ_WRK303 24/03/2020 179.83 Standing Water Level mAHD DG_A_I_PZ_WRK301 24/03/2020 178.2 Standing Water Level mAHD DG_A_I_PZ_GW03 6/04/2020 161.89 Standing Water Level mAHD DG_A_I_PZ_GW02 6/04/2020 170.65 Standing Water Level mAHD DG_A_I_PZ_GW05 6/04/2020 178.84 Standing Water Level mAHD DG_A_I_PZ_GW04 6/04/2020 178.12 Standing Water Level mAHD DG_A_I_PZ_BW45B 7/04/2020 177.37 Standing Water Level mAHD DG_A_I_PZ_GW07 7/04/2020 172.446 Standing Water Level mAHD DG_A_I_PZ_BW36A 7/04/2020 174.225 Standing Water Level mAHD DG_A_I_PZ_GW01 7/04/2020 173.595 Standing Water Level mAHD DG_A_I_PZ_GW08 14/04/2020 177.37 Standing Water Level mAHD DG_A_I_PZ_WRK304 14/04/2020 180.25 Standing Water Level mAHD DG_A_I_PZ_WRK302 14/04/2020 176.68 Standing Water Level mAHD DG_A_I_PZ_GW06 14/04/2020 176.244 Standing Water Level mAHD DG_A_I_PZ_WRK303 14/04/2020 179.85 Standing Water Level mAHD DG_A_I_PZ_WRK301 14/04/2020 178.29 Standing Water Level mAHD DG_A_I_PZ_GW07 1/05/2020 172.476 Standing Water Level mAHD DG_A_I_PZ_GW02 1/05/2020 170.81 Standing Water Level mAHD DG_A_I_PZ_GW05 5/05/2020 178.9 Standing Water Level mAHD DG_A_I_PZ_GW04 5/05/2020 178.24

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

92

Variable Unit Sample Point Date Result Standing Water Level mAHD DG_A_I_PZ_WRK302 5/05/2020 176.7 Standing Water Level mAHD DG_A_I_PZ_GW06 5/05/2020 176.204 Standing Water Level mAHD DG_A_I_PZ_GW08 5/05/2020 177.49 Standing Water Level mAHD DG_A_I_PZ_BW45B 6/05/2020 177.36 Standing Water Level mAHD DG_A_I_PZ_GW01 6/05/2020 173.525 Standing Water Level mAHD DG_A_I_PZ_BW36A 6/05/2020 174.335 Standing Water Level mAHD DG_A_I_PZ_WRK304 8/05/2020 180.5 Standing Water Level mAHD DG_A_I_PZ_WRK303 8/05/2020 179.83 Standing Water Level mAHD DG_A_I_PZ_WRK301 8/05/2020 178.16 Standing Water Level mAHD DG_A_I_PZ_GW02 11/06/2020 170.71 Standing Water Level mAHD DG_A_I_PZ_BW45B 11/06/2020 177.34 Standing Water Level mAHD DG_A_I_PZ_GW05 11/06/2020 178.96 Standing Water Level mAHD DG_A_I_PZ_WRK303 16/06/2020 179.79 Standing Water Level mAHD DG_A_I_PZ_WRK301 16/06/2020 178.15 Standing Water Level mAHD DG_A_I_PZ_WRK302 16/06/2020 176.67 Standing Water Level mAHD DG_A_I_PZ_WRK304 16/06/2020 180.36 Standing Water Level mAHD DG_A_I_PZ_GW08 16/06/2020 177.6 Standing Water Level mAHD DG_A_I_PZ_GW06 16/06/2020 176.264 Standing Water Level mAHD DG_A_I_PZ_GW07 17/06/2020 172.436 Standing Water Level mAHD DG_A_I_PZ_GW04 17/06/2020 178.2 Standing Water Level mAHD DG_A_I_PZ_BW36A 17/06/2020 174.405 Standing Water Level mAHD DG_A_I_PZ_GW01 17/06/2020 173.495 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 9/01/2020 16.41 Standing Water Level (mBTOC) m DG_A_I_PZ_BW05 13/01/2020 5.47 Standing Water Level (mBTOC) m DG_A_I_PZ_BW28A 13/01/2020 4.01 Standing Water Level (mBTOC) m DG_A_I_PZ_BW53/Puls 13/01/2020 10.3 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 14/01/2020 15.57 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 14/01/2020 10.35 Standing Water Level (mBTOC) m DG_A_I_PZ_IWB2 14/01/2020 12.21 Standing Water Level (mBTOC) m DG_A_I_PZ_IWB6 14/01/2020 1.96 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 15/01/2020 19.08 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 15/01/2020 19.87 Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 15/01/2020 21.3 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 15/01/2020 23.85 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 16/01/2020 26.21 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 16/01/2020 24.58 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 20/01/2020 13.31 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 20/01/2020 13.69 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 22/01/2020 18.71 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 22/01/2020 13.29 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 22/01/2020 18.6 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 23/01/2020 20.88 Standing Water Level (mBTOC) m DG_A_I_PZ_IWB6 20/02/2020 1.88 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 20/02/2020 23.86

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

93

Variable Unit Sample Point Date Result Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 20/02/2020 21.36 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 20/02/2020 19.11 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 24/02/2020 13.38 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 24/02/2020 13.61 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 24/02/2020 20.6 Standing Water Level (mBTOC) m DG_A_I_PZ_BW05 24/02/2020 5.31 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 25/02/2020 13.47 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 25/02/2020 18.62 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 26/02/2020 16.37 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 26/02/2020 19.94 Standing Water Level (mBTOC) m DG_A_I_PZ_BW28A 26/02/2020 4.23 Standing Water Level (mBTOC) m DG_A_I_PZ_BW53/Puls 26/02/2020 10.29 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 27/02/2020 26.23 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 27/02/2020 10.28 Standing Water Level (mBTOC) m DG_A_I_PZ_IWB2 27/02/2020 12.24 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 28/02/2020 24.62 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 3/03/2020 15.59 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 5/03/2020 18.78 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 18/03/2020 16.38 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 19/03/2020 10.3 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 19/03/2020 15.62 Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 19/03/2020 21.32 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 20/03/2020 23.81 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 20/03/2020 19.9 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 20/03/2020 19.09 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 23/03/2020 26.2 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 23/03/2020 24.57 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 23/03/2020 13.29 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 23/03/2020 13.66 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 23/03/2020 13.34 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 24/03/2020 18.72 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 24/03/2020 20.57 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 24/03/2020 18.58 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 6/04/2020 10.53 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 6/04/2020 15.73 Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 6/04/2020 21.46 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 6/04/2020 24.12 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 7/04/2020 19.88 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 7/04/2020 16.4 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 7/04/2020 24.61 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 7/04/2020 26.51 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 7/04/2020 18.92 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 14/04/2020 13.6 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 14/04/2020 18.82

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 14/04/2020 13.6 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 14/04/2020 13.27 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 14/04/2020 20.55 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 14/04/2020 18.49 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 1/05/2020 16.37 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 1/05/2020 10.43 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 1/05/2020 15.57 Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 5/05/2020 21.4 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 5/05/2020 24 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 5/05/2020 13.58 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 5/05/2020 13.31 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 5/05/2020 13.48 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 6/05/2020 19.89 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 6/05/2020 18.99 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 6/05/2020 26.4 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 6/05/2020 24.51 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 8/05/2020 18.57 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 8/05/2020 20.57 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 8/05/2020 18.62 Standing Water Level (mBTOC) m DG_A_I_PZ_GW03 11/06/2020 10.45 Standing Water Level (mBTOC) m DG_A_I_PZ_GW02 11/06/2020 15.67 Standing Water Level (mBTOC) m DG_A_I_PZ_BW45B 11/06/2020 19.91 Standing Water Level (mBTOC) m DG_A_I_PZ_GW05 11/06/2020 21.34 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK303 16/06/2020 20.61 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK301 16/06/2020 18.63 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK302 16/06/2020 13.61 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK304 16/06/2020 18.71 Standing Water Level (mBTOC) m DG_A_I_PZ_GW08 16/06/2020 13.37 Standing Water Level (mBTOC) m DG_A_I_PZ_GW06 16/06/2020 13.25 Standing Water Level (mBTOC) m DG_A_I_PZ_GW07 17/06/2020 16.41 Standing Water Level (mBTOC) m DG_A_I_PZ_GW04 17/06/2020 24.04 Standing Water Level (mBTOC) m DG_A_I_PZ_BW36A 17/06/2020 26.33 Standing Water Level (mBTOC) m DG_A_I_PZ_GW01 17/06/2020 19.02 Standing Water Level (mBTOC) m DG_A_I_PZ_WRK300 17/06/2020 24.56 Temperature °C DG_A_I_PZ_GW07 9/01/2020 18.7 Temperature °C DG_A_I_PZ_BW05 13/01/2020 16.9 Temperature °C DG_A_I_PZ_BW28A 13/01/2020 17.7 Temperature °C DG_A_I_PZ_BW53/Puls 13/01/2020 19.3 Temperature °C DG_A_I_PZ_GW02 14/01/2020 18.1 Temperature °C DG_A_I_PZ_GW03 14/01/2020 20.6 Temperature °C DG_A_I_PZ_IWB2 14/01/2020 18.2 Temperature °C DG_A_I_PZ_IWB6 14/01/2020 18 Temperature °C DG_A_I_PZ_GW01 15/01/2020 19.8 Temperature °C DG_A_I_PZ_BW45B 15/01/2020 21

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

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Variable Unit Sample Point Date Result Temperature °C DG_A_I_PZ_GW05 15/01/2020 22.5 Temperature °C DG_A_I_PZ_GW04 15/01/2020 23.1 Temperature °C DG_A_I_PZ_BW36A 16/01/2020 20 Temperature °C DG_A_I_PZ_WRK300 16/01/2020 21.3 Temperature °C DG_A_I_PZ_GW08 20/01/2020 17.7 Temperature °C DG_A_I_PZ_WRK302 20/01/2020 17.3 Temperature °C DG_A_I_PZ_WRK304 22/01/2020 20.3 Temperature °C DG_A_I_PZ_GW06 22/01/2020 17.9 Temperature °C DG_A_I_PZ_WRK301 22/01/2020 23.2 Temperature °C DG_A_I_PZ_WRK303 23/01/2020 16.1 Temperature °C DG_A_I_PZ_IWB6 20/02/2020 17.6 Temperature °C DG_A_I_PZ_GW04 20/02/2020 17 Temperature °C DG_A_I_PZ_GW05 20/02/2020 17.2 Temperature °C DG_A_I_PZ_GW01 20/02/2020 18.1 Temperature °C DG_A_I_PZ_GW06 24/02/2020 18 Temperature °C DG_A_I_PZ_WRK302 24/02/2020 17.5 Temperature °C DG_A_I_PZ_WRK303 24/02/2020 23 Temperature °C DG_A_I_PZ_BW05 24/02/2020 17.1 Temperature °C DG_A_I_PZ_GW08 25/02/2020 18 Temperature °C DG_A_I_PZ_WRK301 25/02/2020 24.6 Temperature °C DG_A_I_PZ_GW07 26/02/2020 18.3 Temperature °C DG_A_I_PZ_BW45B 26/02/2020 16.7 Temperature °C DG_A_I_PZ_BW28A 26/02/2020 17.6 Temperature °C DG_A_I_PZ_BW53/Puls 26/02/2020 18.1 Temperature °C DG_A_I_PZ_BW36A 27/02/2020 17.7 Temperature °C DG_A_I_PZ_GW03 27/02/2020 20 Temperature °C DG_A_I_PZ_IWB2 27/02/2020 18 Temperature °C DG_A_I_PZ_WRK300 28/02/2020 16.9 Temperature °C DG_A_I_PZ_GW02 3/03/2020 18.5 Temperature °C DG_A_I_PZ_WRK304 5/03/2020 19.4 Temperature °C DG_A_I_PZ_GW07 18/03/2020 18.5 Temperature °C DG_A_I_PZ_GW03 19/03/2020 20 Temperature °C DG_A_I_PZ_GW02 19/03/2020 18.2 Temperature °C DG_A_I_PZ_GW05 19/03/2020 23.3 Temperature °C DG_A_I_PZ_GW04 20/03/2020 17 Temperature °C DG_A_I_PZ_BW45B 20/03/2020 17.8 Temperature °C DG_A_I_PZ_GW01 20/03/2020 17.3 Temperature °C DG_A_I_PZ_BW36A 23/03/2020 16.3 Temperature °C DG_A_I_PZ_WRK300 23/03/2020 16.9 Temperature °C DG_A_I_PZ_GW06 23/03/2020 17.7 Temperature °C DG_A_I_PZ_WRK302 23/03/2020 17.3 Temperature °C DG_A_I_PZ_GW08 23/03/2020 18.4 Temperature °C DG_A_I_PZ_WRK304 24/03/2020 17.5 Temperature °C DG_A_I_PZ_WRK303 24/03/2020 17.7

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Temperature °C DG_A_I_PZ_WRK301 24/03/2020 18 Temperature °C DG_A_I_PZ_GW03 6/04/2020 18 Temperature °C DG_A_I_PZ_GW02 6/04/2020 17.8 Temperature °C DG_A_I_PZ_GW05 6/04/2020 17.3 Temperature °C DG_A_I_PZ_GW04 6/04/2020 17.1 Temperature °C DG_A_I_PZ_BW45B 7/04/2020 16.8 Temperature °C DG_A_I_PZ_GW07 7/04/2020 18.2 Temperature °C DG_A_I_PZ_WRK300 7/04/2020 16.3 Temperature °C DG_A_I_PZ_BW36A 7/04/2020 16.9 Temperature °C DG_A_I_PZ_GW01 7/04/2020 17.4 Temperature °C DG_A_I_PZ_GW08 14/04/2020 18.3 Temperature °C DG_A_I_PZ_WRK304 14/04/2020 19.2 Temperature °C DG_A_I_PZ_WRK302 14/04/2020 17.3 Temperature °C DG_A_I_PZ_GW06 14/04/2020 17.8 Temperature °C DG_A_I_PZ_WRK303 14/04/2020 19.7 Temperature °C DG_A_I_PZ_WRK301 14/04/2020 21 Temperature °C DG_A_I_PZ_GW07 1/05/2020 18 Temperature °C DG_A_I_PZ_GW03 1/05/2020 17.4 Temperature °C DG_A_I_PZ_GW02 1/05/2020 17.6 Temperature °C DG_A_I_PZ_GW05 5/05/2020 16.1 Temperature °C DG_A_I_PZ_GW04 5/05/2020 15.2 Temperature °C DG_A_I_PZ_WRK302 5/05/2020 17.2 Temperature °C DG_A_I_PZ_GW06 5/05/2020 17.6 Temperature °C DG_A_I_PZ_GW08 5/05/2020 18.1 Temperature °C DG_A_I_PZ_BW45B 6/05/2020 16.3 Temperature °C DG_A_I_PZ_GW01 6/05/2020 16 Temperature °C DG_A_I_PZ_BW36A 6/05/2020 16.5 Temperature °C DG_A_I_PZ_WRK300 6/05/2020 17.7 Temperature °C DG_A_I_PZ_WRK304 8/05/2020 15.9 Temperature °C DG_A_I_PZ_WRK303 8/05/2020 16.9 Temperature °C DG_A_I_PZ_WRK301 8/05/2020 16.4 Temperature °C DG_A_I_PZ_GW03 11/06/2020 17.5 Temperature °C DG_A_I_PZ_GW02 11/06/2020 17.9 Temperature °C DG_A_I_PZ_BW45B 11/06/2020 16.9 Temperature °C DG_A_I_PZ_GW05 11/06/2020 17 Temperature °C DG_A_I_PZ_WRK303 16/06/2020 16.3 Temperature °C DG_A_I_PZ_WRK301 16/06/2020 16 Temperature °C DG_A_I_PZ_WRK302 16/06/2020 17.2 Temperature °C DG_A_I_PZ_WRK304 16/06/2020 15.5 Temperature °C DG_A_I_PZ_GW08 16/06/2020 17.7 Temperature °C DG_A_I_PZ_GW06 16/06/2020 17.5 Temperature °C DG_A_I_PZ_GW07 17/06/2020 18 Temperature °C DG_A_I_PZ_GW04 17/06/2020 16 Temperature °C DG_A_I_PZ_BW36A 17/06/2020 15.1

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

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Variable Unit Sample Point Date Result Temperature °C DG_A_I_PZ_GW01 17/06/2020 16 Temperature °C DG_A_I_PZ_WRK300 17/06/2020 16.6

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

98

Appendix D: Monitoring Data (Lab) – Surface water

Variable Unit Sample Point Date Result Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_SW_DUSW14 1/04/2020 320 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_SW_DUSW19 1/04/2020 87 Alkalinity (Bicarbonate) as CaCO3 mg/L DG_A_I_SW_DUSW22 15/06/2020 110 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_SW_DUSW14 1/04/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_SW_DUSW19 1/04/2020 0 Alkalinity (Carbonate) as CaCO3 mg/L DG_A_I_SW_DUSW22 15/06/2020 0 Alkalinity (Hydroxide) as OH mg/L DG_A_I_SW_DUSW14 1/04/2020 0 Alkalinity (Hydroxide) as OH mg/L DG_A_I_SW_DUSW19 1/04/2020 0 Alkalinity (Hydroxide) as OH mg/L DG_A_I_SW_DUSW22 15/06/2020 0 Alkalinity (Total) as CaCO3 mg/L DG_A_I_SW_DUSW19 1/04/2020 87 Aluminium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.19 Aluminium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 4.3 Aluminium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.09 Ammonia Nitrogen mg/L DG_A_I_SW_DUSW14 1/04/2020 0.012 Ammonia Nitrogen mg/L DG_A_I_SW_DUSW19 1/04/2020 0.13 Ammonia Nitrogen mg/L DG_A_I_SW_DUSW22 15/06/2020 0.01 Anions (Total) meq/L DG_A_I_SW_DUSW14 1/04/2020 72 Anions (Total) meq/L DG_A_I_SW_DUSW19 1/04/2020 9.6 Anions (Total) meq/L DG_A_I_SW_DUSW22 15/06/2020 100 Antimony (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Antimony (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Antimony (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Arsenic (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.003 Arsenic (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.002 Arsenic (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Barium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.12 Barium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.076 Barium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.088 Beryllium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Beryllium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Beryllium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Boron (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.3 Boron (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.67 Boron (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.12 Cadmium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.0002 Cadmium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.0002 Cadmium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.0002 Calcium mg/L DG_A_I_SW_DUSW14 1/04/2020 45 Calcium mg/L DG_A_I_SW_DUSW19 1/04/2020 17 Calcium mg/L DG_A_I_SW_DUSW22 15/06/2020 150 Cations (Total) meq/L DG_A_I_SW_DUSW14 1/04/2020 68 Cations (Total) meq/L DG_A_I_SW_DUSW19 1/04/2020 9.4

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

EMP and Rehabilitation Performance Report – H1 2020

99

Variable Unit Sample Point Date Result Cations (Total) meq/L DG_A_I_SW_DUSW22 15/06/2020 100 Chloride mg/L DG_A_I_SW_DUSW14 1/04/2020 2200 Chloride mg/L DG_A_I_SW_DUSW19 1/04/2020 190 Chloride mg/L DG_A_I_SW_DUSW22 15/06/2020 3200 Chromium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Chromium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Chromium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Cobalt (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Cobalt (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.003 Cobalt (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Copper (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Copper (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.003 Copper (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Cyanide (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.063 Electrical Conductivity µS/cm DG_A_I_SW_DUSW14 1/04/2020 7400 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 7/01/2020 1100 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 17/06/2020 290 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 7/01/2020 870 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 1/04/2020 1000 Electrical Conductivity µS/cm DG_A_I_SW_DUSW22 15/06/2020 10000 Electrical Conductivity µS/cm DG_A_I_SW_DUSW23 15/06/2020 620 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 7/01/2020 1100 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 15/06/2020 250 Electrical Conductivity µS/cm DG_A_I_SW_DUSW27 15/06/2020 200 Fluoride mg/L DG_A_I_SW_DUSW14 1/04/2020 0.27 Fluoride mg/L DG_A_I_SW_DUSW19 1/04/2020 0.54 Fluoride mg/L DG_A_I_SW_DUSW22 15/06/2020 0.35 Iron (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 2.9 Iron (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 2.6 Iron (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.51 Lead (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Lead (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.005 Lead (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Magnesium mg/L DG_A_I_SW_DUSW14 1/04/2020 90 Magnesium mg/L DG_A_I_SW_DUSW19 1/04/2020 13 Magnesium mg/L DG_A_I_SW_DUSW22 15/06/2020 250 Manganese (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.23 Manganese (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.031 Manganese (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.046 Mercury (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.0001 Mercury (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.0001 Mercury (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.0001 Molybdenum (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Molybdenum (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Molybdenum (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Nickel (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Nickel (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.005 Nickel (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW14 1/04/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW17 7/01/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW17 17/06/2020 0.24 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW19 7/01/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW19 1/04/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW22 15/06/2020 0.005 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW23 15/06/2020 1.9 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW26 7/01/2020 0.71 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW26 15/06/2020 1 Nitrate-Nitrogen mg/L DG_A_I_SW_DUSW27 15/06/2020 0.082 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW17 7/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW17 17/06/2020 0.01 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW19 7/01/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW23 15/06/2020 0.009 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW26 7/01/2020 0.009 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW26 15/06/2020 0.019 Nitrite-Nitrogen mg/L DG_A_I_SW_DUSW27 15/06/2020 0.005 Nitrogen (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.71 Nitrogen (Total) mg/L DG_A_I_SW_DUSW17 7/01/2020 1.2 Nitrogen (Total) mg/L DG_A_I_SW_DUSW17 17/06/2020 1.6 Nitrogen (Total) mg/L DG_A_I_SW_DUSW19 7/01/2020 0.51 Nitrogen (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.6 Nitrogen (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.54 Nitrogen (Total) mg/L DG_A_I_SW_DUSW23 15/06/2020 2.5 Nitrogen (Total) mg/L DG_A_I_SW_DUSW26 7/01/2020 2.5 Nitrogen (Total) mg/L DG_A_I_SW_DUSW26 15/06/2020 2.5 Nitrogen (Total) mg/L DG_A_I_SW_DUSW27 15/06/2020 1.8 pH pH units DG_A_I_SW_DUSW14 1/04/2020 7.5 pH pH units DG_A_I_SW_DUSW17 7/01/2020 9.3 pH pH units DG_A_I_SW_DUSW17 17/06/2020 7.4 pH pH units DG_A_I_SW_DUSW19 7/01/2020 8.3 pH pH units DG_A_I_SW_DUSW19 1/04/2020 8.3 pH pH units DG_A_I_SW_DUSW22 15/06/2020 7.6 pH pH units DG_A_I_SW_DUSW23 15/06/2020 7.4 pH pH units DG_A_I_SW_DUSW26 7/01/2020 8.6 pH pH units DG_A_I_SW_DUSW26 15/06/2020 7.6 pH pH units DG_A_I_SW_DUSW27 15/06/2020 7.3

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Phosphorus (Ortho) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.004 Phosphorus (Ortho) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.004 Phosphorus (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.049 Phosphorus (Total) mg/L DG_A_I_SW_DUSW17 7/01/2020 0.07 Phosphorus (Total) mg/L DG_A_I_SW_DUSW17 17/06/2020 0.057 Phosphorus (Total) mg/L DG_A_I_SW_DUSW19 7/01/2020 0.028 Phosphorus (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.08 Phosphorus (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.004 Phosphorus (Total) mg/L DG_A_I_SW_DUSW23 15/06/2020 0.004 Phosphorus (Total) mg/L DG_A_I_SW_DUSW26 7/01/2020 0.11 Phosphorus (Total) mg/L DG_A_I_SW_DUSW26 15/06/2020 0.052 Phosphorus (Total) mg/L DG_A_I_SW_DUSW27 15/06/2020 0.11 Potassium mg/L DG_A_I_SW_DUSW14 1/04/2020 13 Potassium mg/L DG_A_I_SW_DUSW19 1/04/2020 6.2 Potassium mg/L DG_A_I_SW_DUSW22 15/06/2020 16 Radium 226 Bq/L DG_A_I_SW_DUSW14 1/04/2020 0.01 Radium 226 Bq/L DG_A_I_SW_DUSW22 15/06/2020 0.01 Radium 228 Bq/L DG_A_I_SW_DUSW14 1/04/2020 0.08 Radium 228 Bq/L DG_A_I_SW_DUSW22 15/06/2020 0.08 Selenium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Selenium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Selenium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Silver (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Silver (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.003 Silver (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Sodium mg/L DG_A_I_SW_DUSW14 1/04/2020 1300 Sodium mg/L DG_A_I_SW_DUSW19 1/04/2020 170 Sodium mg/L DG_A_I_SW_DUSW22 15/06/2020 1700 Strontium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.72 Strontium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.2 Strontium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 1.9 Sulfate mg/L DG_A_I_SW_DUSW14 1/04/2020 240 Sulfate mg/L DG_A_I_SW_DUSW19 1/04/2020 120 Sulfate mg/L DG_A_I_SW_DUSW22 15/06/2020 360 Thallium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.003 Thallium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Thallium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Thorium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.0045 Thorium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.0057 Thorium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.002 Tin (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001 Tin (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Tin (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Titanium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.007 Titanium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.15 Titanium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.003 Total Dissolved Solids mg/L DG_A_I_SW_DUSW14 1/04/2020 4400 Total Dissolved Solids mg/L DG_A_I_SW_DUSW17 7/01/2020 650 Total Dissolved Solids mg/L DG_A_I_SW_DUSW17 17/06/2020 1400 Total Dissolved Solids mg/L DG_A_I_SW_DUSW19 7/01/2020 560 Total Dissolved Solids mg/L DG_A_I_SW_DUSW19 1/04/2020 640 Total Dissolved Solids mg/L DG_A_I_SW_DUSW22 15/06/2020 7200 Total Dissolved Solids mg/L DG_A_I_SW_DUSW23 15/06/2020 630 Total Dissolved Solids mg/L DG_A_I_SW_DUSW26 7/01/2020 800 Total Dissolved Solids mg/L DG_A_I_SW_DUSW26 15/06/2020 3000 Total Dissolved Solids mg/L DG_A_I_SW_DUSW27 15/06/2020 320 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW14 1/04/2020 0.71 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW17 7/01/2020 1.2 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW17 17/06/2020 1.4 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW19 7/01/2020 0.51 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW19 1/04/2020 0.6 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW22 15/06/2020 0.54 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW23 15/06/2020 0.53 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW26 7/01/2020 1.8 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW26 15/06/2020 1.4 Total Kjeldahl Nitrogen mg/L DG_A_I_SW_DUSW27 15/06/2020 1.7 Total Oxidised Nitrogen as N mg/L DG_A_I_SW_DUSW14 1/04/2020 0.006 Total Oxidised Nitrogen as N mg/L DG_A_I_SW_DUSW19 1/04/2020 0.006 Total Oxidised Nitrogen as N mg/L DG_A_I_SW_DUSW22 15/06/2020 0.006 Total Suspended Solids mg/L DG_A_I_SW_DUSW14 1/04/2020 27 Total Suspended Solids mg/L DG_A_I_SW_DUSW17 7/01/2020 93 Total Suspended Solids mg/L DG_A_I_SW_DUSW17 17/06/2020 92 Total Suspended Solids mg/L DG_A_I_SW_DUSW19 7/01/2020 1 Total Suspended Solids mg/L DG_A_I_SW_DUSW19 1/04/2020 40 Total Suspended Solids mg/L DG_A_I_SW_DUSW22 15/06/2020 6 Total Suspended Solids mg/L DG_A_I_SW_DUSW23 15/06/2020 14 Total Suspended Solids mg/L DG_A_I_SW_DUSW26 7/01/2020 34 Total Suspended Solids mg/L DG_A_I_SW_DUSW26 15/06/2020 98 Total Suspended Solids mg/L DG_A_I_SW_DUSW27 15/06/2020 33 Turbidity NTU DG_A_I_SW_DUSW17 7/01/2020 41 Turbidity NTU DG_A_I_SW_DUSW17 17/06/2020 1100 Turbidity NTU DG_A_I_SW_DUSW19 7/01/2020 32 Turbidity NTU DG_A_I_SW_DUSW19 1/04/2020 40 Turbidity NTU DG_A_I_SW_DUSW23 15/06/2020 310 Turbidity NTU DG_A_I_SW_DUSW26 7/01/2020 170 Turbidity NTU DG_A_I_SW_DUSW26 15/06/2020 2700 Uranium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Uranium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.001 Uranium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Uranium 238 Bq/L DG_A_I_SW_DUSW14 1/04/2020 0.025 Uranium 238 Bq/L DG_A_I_SW_DUSW22 15/06/2020 0.025 Vanadium (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.004 Vanadium (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.006 Vanadium (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.001 Zinc (Total) mg/L DG_A_I_SW_DUSW14 1/04/2020 0.01 Zinc (Total) mg/L DG_A_I_SW_DUSW19 1/04/2020 0.008 Zinc (Total) mg/L DG_A_I_SW_DUSW22 15/06/2020 0.007 Results that are italicised are equal to less than values i.e. 0.001 = <0.001

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Appendix E: Monitoring Data (Field) – Surface water

Variable Unit Sample Point Date Result Dissolved Oxygen mg/L DG_A_I_SW_DUSW14 1/04/2020 4.3 Dissolved Oxygen % DG_A_I_SW_DUSW14 1/04/2020 47 Dissolved Oxygen mg/L DG_A_I_SW_DUSW17 7/01/2020 9.9 Dissolved Oxygen % DG_A_I_SW_DUSW17 7/01/2020 100 Dissolved Oxygen mg/L DG_A_I_SW_DUSW17 17/06/2020 10.4 Dissolved Oxygen % DG_A_I_SW_DUSW17 17/06/2020 102 Dissolved Oxygen mg/L DG_A_I_SW_DUSW19 7/01/2020 9.7 Dissolved Oxygen % DG_A_I_SW_DUSW19 7/01/2020 111 Dissolved Oxygen mg/L DG_A_I_SW_DUSW19 1/04/2020 10.2 Dissolved Oxygen % DG_A_I_SW_DUSW19 1/04/2020 110 Dissolved Oxygen mg/L DG_A_I_SW_DUSW22 15/06/2020 10.2 Dissolved Oxygen % DG_A_I_SW_DUSW22 15/06/2020 99 Dissolved Oxygen mg/L DG_A_I_SW_DUSW23 15/06/2020 10.8 Dissolved Oxygen % DG_A_I_SW_DUSW23 15/06/2020 104 Dissolved Oxygen mg/L DG_A_I_SW_DUSW26 7/01/2020 10 Dissolved Oxygen % DG_A_I_SW_DUSW26 7/01/2020 106 Dissolved Oxygen mg/L DG_A_I_SW_DUSW26 15/06/2020 10.7 Dissolved Oxygen % DG_A_I_SW_DUSW26 15/06/2020 101 Dissolved Oxygen mg/L DG_A_I_SW_DUSW27 15/06/2020 10.5 Dissolved Oxygen % DG_A_I_SW_DUSW27 15/06/2020 102 Electrical Conductivity µS/cm DG_A_I_SW_DUSW14 1/04/2020 7400 Electrical Conductivity µS/cm DG_A_I_SW_DUSW14 1/04/2020 7879 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 7/01/2020 1100 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 7/01/2020 1109 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 17/06/2020 290 Electrical Conductivity µS/cm DG_A_I_SW_DUSW17 17/06/2020 318 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 7/01/2020 870 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 7/01/2020 891 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 1/04/2020 1000 Electrical Conductivity µS/cm DG_A_I_SW_DUSW19 1/04/2020 1126 Electrical Conductivity µS/cm DG_A_I_SW_DUSW22 15/06/2020 10000 Electrical Conductivity µS/cm DG_A_I_SW_DUSW22 15/06/2020 10999 Electrical Conductivity µS/cm DG_A_I_SW_DUSW23 15/06/2020 620 Electrical Conductivity µS/cm DG_A_I_SW_DUSW23 15/06/2020 658 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 7/01/2020 1100 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 7/01/2020 1115 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 15/06/2020 250 Electrical Conductivity µS/cm DG_A_I_SW_DUSW26 15/06/2020 269 Electrical Conductivity µS/cm DG_A_I_SW_DUSW27 15/06/2020 200 Electrical Conductivity µS/cm DG_A_I_SW_DUSW27 15/06/2020 218 pH pH units DG_A_I_SW_DUSW14 1/04/2020 7.5 pH pH units DG_A_I_SW_DUSW14 1/04/2020 7.48

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result pH pH units DG_A_I_SW_DUSW17 7/01/2020 9.3 pH pH units DG_A_I_SW_DUSW17 7/01/2020 9.3 pH pH units DG_A_I_SW_DUSW17 17/06/2020 7.4 pH pH units DG_A_I_SW_DUSW17 17/06/2020 7.69 pH pH units DG_A_I_SW_DUSW19 7/01/2020 8.3 pH pH units DG_A_I_SW_DUSW19 7/01/2020 8.18 pH pH units DG_A_I_SW_DUSW19 1/04/2020 8.3 pH pH units DG_A_I_SW_DUSW19 1/04/2020 7.68 pH pH units DG_A_I_SW_DUSW22 15/06/2020 7.6 pH pH units DG_A_I_SW_DUSW22 15/06/2020 6.76 pH pH units DG_A_I_SW_DUSW23 15/06/2020 7.4 pH pH units DG_A_I_SW_DUSW23 15/06/2020 7.45 pH pH units DG_A_I_SW_DUSW26 7/01/2020 8.6 pH pH units DG_A_I_SW_DUSW26 7/01/2020 8.74 pH pH units DG_A_I_SW_DUSW26 15/06/2020 7.6 pH pH units DG_A_I_SW_DUSW26 15/06/2020 7.82 pH pH units DG_A_I_SW_DUSW27 15/06/2020 7.3 pH pH units DG_A_I_SW_DUSW27 15/06/2020 7.62 Redox Potential (Eh) mV DG_A_I_SW_DUSW14 1/04/2020 193 Redox Potential (Eh) mV DG_A_I_SW_DUSW17 7/01/2020 160 Redox Potential (Eh) mV DG_A_I_SW_DUSW17 17/06/2020 215 Redox Potential (Eh) mV DG_A_I_SW_DUSW19 7/01/2020 210 Redox Potential (Eh) mV DG_A_I_SW_DUSW19 1/04/2020 184 Redox Potential (Eh) mV DG_A_I_SW_DUSW22 15/06/2020 203 Redox Potential (Eh) mV DG_A_I_SW_DUSW23 15/06/2020 319 Redox Potential (Eh) mV DG_A_I_SW_DUSW26 7/01/2020 181 Redox Potential (Eh) mV DG_A_I_SW_DUSW26 15/06/2020 288 Redox Potential (Eh) mV DG_A_I_SW_DUSW27 15/06/2020 249 Temperature (Water) °C DG_A_I_SW_DUSW14 1/04/2020 17.1 Temperature (Water) °C DG_A_I_SW_DUSW17 7/01/2020 17.1 Temperature (Water) °C DG_A_I_SW_DUSW17 17/06/2020 14.3 Temperature (Water) °C DG_A_I_SW_DUSW19 7/01/2020 20.6 Temperature (Water) °C DG_A_I_SW_DUSW19 1/04/2020 18.2 Temperature (Water) °C DG_A_I_SW_DUSW22 15/06/2020 11.9 Temperature (Water) °C DG_A_I_SW_DUSW23 15/06/2020 12.7 Temperature (Water) °C DG_A_I_SW_DUSW26 7/01/2020 16.7 Temperature (Water) °C DG_A_I_SW_DUSW26 15/06/2020 12.1 Temperature (Water) °C DG_A_I_SW_DUSW27 15/06/2020 13.2 Turbidity NTU DG_A_I_SW_DUSW14 1/04/2020 42.3 Turbidity NTU DG_A_I_SW_DUSW17 7/01/2020 41 Turbidity NTU DG_A_I_SW_DUSW17 7/01/2020 77.2 Turbidity NTU DG_A_I_SW_DUSW17 17/06/2020 1100 Turbidity NTU DG_A_I_SW_DUSW17 17/06/2020

Turbidity NTU DG_A_I_SW_DUSW19 7/01/2020 32

Iluka Resources Ltd Planning Permit 15-105: Mineral Sands By-Product Disposal (Pit 23)

Iluka Ref: UDOCS 0090-426461582-1177 FINAL (Rev 0)

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Variable Unit Sample Point Date Result Turbidity NTU DG_A_I_SW_DUSW19 7/01/2020 33.4 Turbidity NTU DG_A_I_SW_DUSW19 1/04/2020 40 Turbidity NTU DG_A_I_SW_DUSW19 1/04/2020 45.4 Turbidity NTU DG_A_I_SW_DUSW22 15/06/2020 6.74 Turbidity NTU DG_A_I_SW_DUSW23 15/06/2020 310 Turbidity NTU DG_A_I_SW_DUSW26 7/01/2020 170 Turbidity NTU DG_A_I_SW_DUSW26 7/01/2020 164 Turbidity NTU DG_A_I_SW_DUSW26 15/06/2020 2700 Turbidity NTU DG_A_I_SW_DUSW27 15/06/2020 139