3-D photonic bandgap structures in the microwave regime by fused deposition of multimaterials
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Transcript of 3-D photonic bandgap structures in the microwave regime by fused deposition of multimaterials
3-D photonic bandgapstructures in themicrowave regime byfused deposition ofmultimaterials
Mauricio E Pilleux
Mehdi AllahverdiYouren Chen
Yicheng Lu Mohsen A Jafari and
Ahmad Safari
The authors
Author information may be found at the end of the article
Keywords
Design Layered manufacturing Alumina Ceramics
Abstract
Three-dimensional photonic bandgap (PBG) structuresusing alumina (Al2O3) as the high permittivity materialwere modeled and then the structures were fabricated byFused Deposition of Multi-materials (FDMM) technologyA nite element method and a real-time electromagneticwave propagation software were used to simulate anddesign the layered PBG structures for applications in themicrowave frequency range The modeling predicted a 3-Dphotonic bandgap in the 165ndash235 GHz range FDMMprovides a computer-controlled process to generate 3-Dstructures allowing high fabrication exibility andefciency Electromagnetic measurements displayed thepresence of a bandgap between 171ndash233 GHz showinga good agreement with the predicted values These PBGstructures are potential candidates for applications inadvanced communication systems
Electronic access
The research register for this journal is available at
httpwwwemeraldinsightcomresearch_registers
The current issue and full text archive of this journal is
available at
httpwwwemeraldinsightcom1355-2546htm
1 Introduction
Photonic bandgap (PBG) crystals are periodic
dielectric structures that alternate high and
low permittivity materials in order to obtain
an electromagnetic stop-band in a desired
direction depending upon the periodicity of
the structure PBG crystals were proposed in
the late 1980rsquos and since then there have been
extensive theoretical and experimental works
devoted to this new reg eld in order to
understand and exploit the properties of these
structures (Berger 1999 Dowling et al
2000) The dielectric or metallic periodic
structure gives rise to a forbidden band of
frequencies or photonic bandgap which
essentially changes the electromagnetic wave
propagation properties through the structure
These structures have received increasing
interest in recent years because of their
capability to conreg ne electromagnetic (EM)
waves in all three spatial dimensions
(Yablobovitch 1993 1997) A variety of
potential applications such as thresholdless
lasers high quality-single mode LEDs
microwave antennas light diodes an all kinds
of optical circuits have been suggested and
some have already been demonstrated
(Joannopoulos et al 1995)
For the microwavemillimeter wave region
in which our interest is focused applications
involve control of signal propagation quiet
oscillators frequency selective surfaces
narrow band reg lters and antenna substrates
For the latter case if a conventional substrate
is used then a large portion of the antenna
radiation is emitted into the substrate (since it
has a higher dielectric constant than air) and a
great part of this radiation is trapped inside
the substrate because of total internal
remacr ections In consequence not only more
than 50 percent of the radiated energy is lost
but also heat dissipation and temperature
effects arise in the substrate Instead if an
appropriate PBG substrate is selected then
the energy can be directed towards the
radiating direction (total remacr ection by the
PBG structure) thus improving the antenna
directivity and eliminating the substrate heat
Rapid Prototyping JournalVolume 8 middot Number 1 middot 2002 middot pp 46ndash52q MCB UP Limited middot ISSN 1355-2546DOI 10110813552540210413301
This project was supported by the New Jersey
Commission on Science and Technology under the
Research Excellence Program We wish to
acknowledge the helpful assistance provided by
Mr Ferdus Safari and by Mr Kian Seyed We also
appreciate the assistance of Dr Edip Niver with the
microwave characterization
46
dissipation There have been many reports for
the application of PBG structures as antenna
substrates such as (Brown and McMahon
1996 Sievenpiper et al 1999) Our research
will focus on the design and fabrication of 3-D
PBG structures with applications in the
millimeter-wave band Such structures are
made by a rapid prototyping technique
discussed below
Many groups have performed research in
photonic structures using alumina as the high
permittivity dielectric material (Masuda et al
1999 Jessensky et al 1998 Shingubara et al
1997 Feiertag et al 1997) The use of anodic
porous alumina formed by the anodization of
aluminum in an appropriate acid solution
has attracted attention as a starting material
for 2-D PBG structures with typical
dimensions in the nano- or micrometers since
this process is a typical example of a naturally
occurring ordered structure (Masuda et al
1999 Jessensky et al 1998 Shingubara et al
1997) Also Feiertag et al developed a
microfabrication technique for building 3-D
PBG structures using x-ray lithography with
bandgaps in the infrared region (Feiertag et al
1997) These structures have a lattice
constant of 85 mm and are made with 22 mm
diameter rods
Jin et al made microwave measurements on
a 2-D octagonal quasiperiodic photonic
crystal composed of an array of 23 pound 23 rows of
alumina cylinders (Jin et al 1999) The
diameter of the alumina cylinders was
612 mm so the reg lling fraction was 49
percent The authors found a bandgap
between 89 and 105 GHz that the position
and width of the bandgap did not depend on
the incidence direction and that it can appear
even if the arrayrsquos dimensions are lowered to
11 rows of cylinders Because of these
characteristics this photonic quasicrystal
seems to be more suitable for waveguide
applications than as a periodic photonic
crystal For this purpose waveguides were
fabricated by removing 3 rows of cylinders
leaving a 157-mm wide empty path from one
side of the array to the opposite one which
was approximately half of a wavelength at the
gap center The results show a high efreg ciency
of straight and bending guides
For the fabrication of PBG structures in the
mm-range there are few rapid prototyping
processes available Fused Deposition of
Ceramics (FDC) or its modireg ed version for
multimaterials presents several advantages
for the fabrication of the PBG periodic
structures for use in the microwave region
since the minimum part shapes are in the
order 05 mm (Danforth et al 1998 Safari
et al 1998a Safari et al 1998b Jafari et al
2000) The main advantage of this technique
is the rapid prototyping of the complex design
which means that the geometry and the
dimensions of a sample can be easily modireg ed
by the use of a CAD software FDMM makes
it possible to build PBG structures up to
frequencies close to 100 GHz
In this paper we present the application of
a novel fabrication technique fused
deposition of multimaterials (FDMM) to the
manufacturing of PBG structures in order
demonstrate the feasibility of the technique
for this purpose The advantage of FDMM is
the rapid fabrication of complex designs using
a computer-controlled system with no need
for mold or any hard tooling Conventional
fabrication processes require initial making of
bulk pieces of dielectric materials followed by
machining andor etching to form the desired
structures with alternating high and low
dielectric constant materials On the other
hand FDMM deposits the desired materials
only where required by the design and
therefore is capable of making complex PBG
structures
2 Experimental procedure
The modeling was based on a reg nite element
shareware Fortran program written by the
Photonics Research Team of Imperial College
(London UK) and was adapted to this
research in order to incorporate the specireg c
structures that were modeled (Pendry et al
1992 Pendry 1996) Frequency-domain
modeling was also performed using the High
Frequency Structure Simulator (HFSS)
commercial software from Ansoft
Corporation (Pittsburgh PA) This is a
powerful program that can perform real-time
simulation of the wave propagation though
2-D or 3-D dielectric or metallic periodic
structures of any complex geometry The
electromagnetic measurements were carried
out in a Network Analyzer (Hewlett Packard
model HP8510C) with open-ended
waveguides
The geometry of the structure that was
built by FDMM in this work is shown in
Figure 1 The size of the unit cell and in
consequence the spacing between bars and
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
47
the geometry of the cross-section of each bar
of the structure was chosen so that the
bandgap would lie in the 15 plusmn 95 GHz
frequency range Alumina was used as the
high permittivity dielectric material (relative
permittivity 1r = 96) and air as the low
permittivity one
The fabrication of the PBG structures was
performed using the multimaterial deposition
equipment designed and fabricated at Rutgers
University and is described elsewhere (Jafari
et al 2000) The feedstock materials for the
FDMM process were reg laments of alumina
and ICW-06 wax (Stratasys Inc Eden
Prairie MN) The alumina reg lament was
fabricated using A152-SG alumina powder
(Alcoa New Milford CT) which was coated
with a surfactant by mixing 150 g of alumina
in a 30 gL solution of stearic acid in toluene
and then mixing the slurry for 4 h The
mixture was then reg ltered and then air dried in
order to remove the solvent The loss on
ignition test at 550 8 C for 1 h indicated that the
stearic acid adsorption was 19 wt percent
Once the coated alumina powder was dried it
was mixed with ECG-9 thermoplastic binder
(developed at Rutgers University) (McNulty
et al 1998a b) in a Haake System 9000 high-
shear mixer (Haake-Fisons Paramus NJ)
with a twin-roller blade mixing bowl operating
at 100 rpm The alumina powder volume
fractions successfully used were 60 and 62 vol
percent solids loading The compounded
alumina-binder system was then extruded at
90 8 C into continuous reg laments several meters
long through a 178-mm diameter nozzle
using the same system but with a single screw
extruding attachment
Using the input from the PBG modeling a
CAD reg le was made in order to fabricate the
structure using the FDMM equipment The
geometry of the PBG structure required the
use of a supporting material below the
alumina rods during fused deposition and
ICW-06 wax was utilized for this purpose
The part was fabricated by the successive
deposition of the wax and the alumina-loaded
reg lament in a layer-by-layer manner The
alumina reg lament was loaded into a liquereg er
heated to 130 8 C having a 500 mm diameter
nozzle The wax reg lament was deposited using
a similar liquereg er and nozzle at a working
temperature of 72 8 C The CADCAM system
gave instructions to the FDMM equipment so
that the liquereg er would move and deposit
material in a predereg ned tool pathTo avoid bending of the alumina bars while
performing the binder burnout (BBO)
process it was necessary to initially remove
the wax from the fabricated structure so that it
could be replaced by a temperature resistant
support material during the BBO process
The wax removal was carried out in an oven
by placing the as-fabricated part for 10 min at
a temperature of 110 8 C This time-
temperature combination allowed the removal
of the wax without deforming the alumina-
polymer structure The dewaxed structure
was subsequently reg lled with zirconia powder
in order provide a refractory mechanical
support to avoid bending of the alumina bars
when subjected to the BBO cycle The BBO
was carried out by heating the structure to
550 8 C for 1 h immediately followed by a
partial sintering at 1050 8 C for 1 h The
heating from 100 to 350 8 C was carried out at
10 8 Ch in order to avoid any excessive
degassing of the sample from the calcination
of the organic components that might deform
the structure Finally sintering was carried
out at 1600 8 C for 1 h in a different furnace
3 Results and discussion
31 Design and simulation
The objective of the theoretical simulation of
the PBG structures was to solve Maxwellrsquos
equations inside the desired PBG geometry
As previously indicated our simulation used
two different computational methods to
investigate the PBG structure The reg rst one
the Fortran-code software was used to
reformulate Maxwellrsquos equations on a lattice
by dividing the space into a set of small cells
with a coupling between neighboring ones
(OEgrave zbay et al 1994) Then it calculated the
Figure 1 CAD drawing of the unit cell of the PBG structurefabricated by FDMM Each bar is 28 mm long with a2 pound 2 mm2 square cross-section and a pitch separation of8 mm The lling ratio of the structure is 38 percent
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
48
propagation of the EM reg elds through a
periodic dielectric structure in layer-by-layer
manner by means of a transfer matrix (Pendry
et al 1992) The transfer matrix can then be
used to evaluate the bulk dispersion and
transmission through a reg nite thickness slab of
the material since its eigenvectors are the
solutions for the electric and magnetic reg eld at
each point for a given frequency v Then the
band structure k = k(v) can be calculated
from these eigenvalues Since the transfer
matrix dereg nes how the waves cross a slab of
the material the transmission coefreg cients can
also be calculated The input to the program is
the geometry of the periodic structure as well
as the frequency v (or energy) of interest
The Transfer Matrix method was applied
to calculate the energy bandgap of the
alumina structure with rectangular rods as
shown in Table I and Figure 2 We
demonstrated that the reg lling ratio (ie the
ratio between the volume of material in the
unit cell and the total volume of the unit cell)
and the dielectric constant ratios are the major
factors that affect the bandgap existence and
the width of the bandgap frequency The
lattice constants of the structure determine
the starting frequency and the width of the
bandgap The shape of the dielectric rod is not
important since the results with square and
cylindrical rods were similar and the rods can
be either of a high permittivity material
surrounded by air or they can be made of air
embedded in a dielectric material The
frequency of the bandgap scales linearly with
the unit cell length which is dereg ned by thesize and the space between the rods This is
due to the linearity of Maxwellrsquos equations
Our second approach was to solveMaxwellrsquos equations in the frequency-domain
and for this purpose the High Frequency
Structure Simulator (HFSS) software wasused The wave-guide simulator method was
used to calculate the EM wave distribution in
the propagation direction (z-direction) The
inputs for the program were the geometry of
the structure which is dereg ned in terms of its
unit cell the monochromatic source and the
boundary conditions at the surface edges The
structure used was made of rectangular
alumina rods of 2 pound 2 mm2 cross section with
a pitch separation of 8 mm between rods The
structure exhibits a bandgap starting around
147 GHz with a bandgap width of 8 GHz
The modeling indicated that the structure
behaved like a Bragg remacr ector ie all the
incident energy was remacr ected The
transmission coefreg cient calculated by the
HFSS program has the same bandgap range
as that shown in Figure 2 using the T-matrix
approach
4 FDMM fabrication
The FDMM process was used to fabricate the
PBG structure shown in Figure 1 ie each
2 pound 2 mm2 square cross-section alumina bar
was 28 mm long with a pitch separation of
8 mm The bars were deposited parallel to
each other in each layer and perpendicular to
the direction of the immediate upper and
lower neighboring layers For every second
layer there was a shift in the position of the
rods by a half lattice constant (every reg fth layer
is identical so that a unit cell was constituted
of 4 rows of bars)
The FDMM fabrication of the PBG
structures was made with the multimaterial
deposition equipment using alumina-loaded
and wax reg laments as feedstock materials The
fabrication was made by the successive
deposition of the reg laments in a layer-by-layer
manner reg nishing each layer before
proceeding to the next one The main
problem encountered was the lack of adhesion
of the alumina layers to the underlying wax
layer The deposition parameters (deposition
speeds and mass macr ow rate) were adjusted to
overcome this problem thus improving the
adhesion of the two materials so that the
Table I Comparison between the results of the simulationand the electromagnetic measurements of the PBGstructure with square alumina rods The cross section ofthe rods is 2 mm and the pitch is 8 mm
Bandgap (GHz) Dvgapvmidgap
165plusmn235 35171plusmn233 31
Figure 2 Transmission loss of the alumina structure with square cross-sectionrods (2 pound 2 mm2)
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
49
successive layers could be deposited
appropriately Figure 3shows an as-fabricated
PBG structure with the support wax
surrounding itThe BBO cycle procedure used was the
same one as for the fabrication of other
electroceramic materials made with this
method (McNulty et al 1998a b) The wax
removal was optimized so that the alumina
rods would not bend due to their own weight
while the wax was macr owing around it for
removal The optimum temperature for the
wax removal was 110 8 C and at this
temperature it only required 10 min for the
wax to macr ow away from alumina bars In the
BBOpresintering cycle the parts were
embedded in zirconia powder in order to
provide support for the overhanging alumina
bars This procedure proved effective for
supporting the bars while not reacting with
the structure The removal of the zirconia was
simple and done using a macr ow of pressurized
air Following this the sintering cycle
densireg ed the structure leaving the typical
reg nished structure shown in Figure 4
Electromagnetic measurements were
carried out on a stack of 4 ordf unit cellsordm of the
sintered PBG structures Each unit cell
consisted of 4 stacks of bars so the
measurement involved 16 layers of bars with
the incident radiation perpendicular to the
ordf topordm side of the unit cell shown in Figure 4 A
stop band was detected between 171 and
233 GHz These results are in good
agreement with the simulation results for this
structure shown in Table I The
rearrangement of the stacks of ordf unit cellsordm
among each other gave identical results
In summary the feasibility of FDMM as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region has been
demonstrated It appears that the complex
ceramic structure fabricated in this research
cannot be made by traditional molding
methods (Knitter et al 2001) A practical
fabrication procedure for example would
involve the fabrication of individual bars and
stacking them using templates In contrast
rapid prototyping seems to be a unique way to
make such complex structures To our
knowledge another rapid prototyping
technique called Robocasting was used to
fabricate similar PBG structures (Cesarano
et al 2001)
5 Conclusions
A photonic bandgap (PBG) structure was
designed and modeled so that it would have
a bandgap in the microwave frequency
Figure 3 The photograph shows the deposition of alumina(bright) and ICW-06 wax (dark) The wax had to beremoved before BBO and sintering of the part
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
50
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
dissipation There have been many reports for
the application of PBG structures as antenna
substrates such as (Brown and McMahon
1996 Sievenpiper et al 1999) Our research
will focus on the design and fabrication of 3-D
PBG structures with applications in the
millimeter-wave band Such structures are
made by a rapid prototyping technique
discussed below
Many groups have performed research in
photonic structures using alumina as the high
permittivity dielectric material (Masuda et al
1999 Jessensky et al 1998 Shingubara et al
1997 Feiertag et al 1997) The use of anodic
porous alumina formed by the anodization of
aluminum in an appropriate acid solution
has attracted attention as a starting material
for 2-D PBG structures with typical
dimensions in the nano- or micrometers since
this process is a typical example of a naturally
occurring ordered structure (Masuda et al
1999 Jessensky et al 1998 Shingubara et al
1997) Also Feiertag et al developed a
microfabrication technique for building 3-D
PBG structures using x-ray lithography with
bandgaps in the infrared region (Feiertag et al
1997) These structures have a lattice
constant of 85 mm and are made with 22 mm
diameter rods
Jin et al made microwave measurements on
a 2-D octagonal quasiperiodic photonic
crystal composed of an array of 23 pound 23 rows of
alumina cylinders (Jin et al 1999) The
diameter of the alumina cylinders was
612 mm so the reg lling fraction was 49
percent The authors found a bandgap
between 89 and 105 GHz that the position
and width of the bandgap did not depend on
the incidence direction and that it can appear
even if the arrayrsquos dimensions are lowered to
11 rows of cylinders Because of these
characteristics this photonic quasicrystal
seems to be more suitable for waveguide
applications than as a periodic photonic
crystal For this purpose waveguides were
fabricated by removing 3 rows of cylinders
leaving a 157-mm wide empty path from one
side of the array to the opposite one which
was approximately half of a wavelength at the
gap center The results show a high efreg ciency
of straight and bending guides
For the fabrication of PBG structures in the
mm-range there are few rapid prototyping
processes available Fused Deposition of
Ceramics (FDC) or its modireg ed version for
multimaterials presents several advantages
for the fabrication of the PBG periodic
structures for use in the microwave region
since the minimum part shapes are in the
order 05 mm (Danforth et al 1998 Safari
et al 1998a Safari et al 1998b Jafari et al
2000) The main advantage of this technique
is the rapid prototyping of the complex design
which means that the geometry and the
dimensions of a sample can be easily modireg ed
by the use of a CAD software FDMM makes
it possible to build PBG structures up to
frequencies close to 100 GHz
In this paper we present the application of
a novel fabrication technique fused
deposition of multimaterials (FDMM) to the
manufacturing of PBG structures in order
demonstrate the feasibility of the technique
for this purpose The advantage of FDMM is
the rapid fabrication of complex designs using
a computer-controlled system with no need
for mold or any hard tooling Conventional
fabrication processes require initial making of
bulk pieces of dielectric materials followed by
machining andor etching to form the desired
structures with alternating high and low
dielectric constant materials On the other
hand FDMM deposits the desired materials
only where required by the design and
therefore is capable of making complex PBG
structures
2 Experimental procedure
The modeling was based on a reg nite element
shareware Fortran program written by the
Photonics Research Team of Imperial College
(London UK) and was adapted to this
research in order to incorporate the specireg c
structures that were modeled (Pendry et al
1992 Pendry 1996) Frequency-domain
modeling was also performed using the High
Frequency Structure Simulator (HFSS)
commercial software from Ansoft
Corporation (Pittsburgh PA) This is a
powerful program that can perform real-time
simulation of the wave propagation though
2-D or 3-D dielectric or metallic periodic
structures of any complex geometry The
electromagnetic measurements were carried
out in a Network Analyzer (Hewlett Packard
model HP8510C) with open-ended
waveguides
The geometry of the structure that was
built by FDMM in this work is shown in
Figure 1 The size of the unit cell and in
consequence the spacing between bars and
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
47
the geometry of the cross-section of each bar
of the structure was chosen so that the
bandgap would lie in the 15 plusmn 95 GHz
frequency range Alumina was used as the
high permittivity dielectric material (relative
permittivity 1r = 96) and air as the low
permittivity one
The fabrication of the PBG structures was
performed using the multimaterial deposition
equipment designed and fabricated at Rutgers
University and is described elsewhere (Jafari
et al 2000) The feedstock materials for the
FDMM process were reg laments of alumina
and ICW-06 wax (Stratasys Inc Eden
Prairie MN) The alumina reg lament was
fabricated using A152-SG alumina powder
(Alcoa New Milford CT) which was coated
with a surfactant by mixing 150 g of alumina
in a 30 gL solution of stearic acid in toluene
and then mixing the slurry for 4 h The
mixture was then reg ltered and then air dried in
order to remove the solvent The loss on
ignition test at 550 8 C for 1 h indicated that the
stearic acid adsorption was 19 wt percent
Once the coated alumina powder was dried it
was mixed with ECG-9 thermoplastic binder
(developed at Rutgers University) (McNulty
et al 1998a b) in a Haake System 9000 high-
shear mixer (Haake-Fisons Paramus NJ)
with a twin-roller blade mixing bowl operating
at 100 rpm The alumina powder volume
fractions successfully used were 60 and 62 vol
percent solids loading The compounded
alumina-binder system was then extruded at
90 8 C into continuous reg laments several meters
long through a 178-mm diameter nozzle
using the same system but with a single screw
extruding attachment
Using the input from the PBG modeling a
CAD reg le was made in order to fabricate the
structure using the FDMM equipment The
geometry of the PBG structure required the
use of a supporting material below the
alumina rods during fused deposition and
ICW-06 wax was utilized for this purpose
The part was fabricated by the successive
deposition of the wax and the alumina-loaded
reg lament in a layer-by-layer manner The
alumina reg lament was loaded into a liquereg er
heated to 130 8 C having a 500 mm diameter
nozzle The wax reg lament was deposited using
a similar liquereg er and nozzle at a working
temperature of 72 8 C The CADCAM system
gave instructions to the FDMM equipment so
that the liquereg er would move and deposit
material in a predereg ned tool pathTo avoid bending of the alumina bars while
performing the binder burnout (BBO)
process it was necessary to initially remove
the wax from the fabricated structure so that it
could be replaced by a temperature resistant
support material during the BBO process
The wax removal was carried out in an oven
by placing the as-fabricated part for 10 min at
a temperature of 110 8 C This time-
temperature combination allowed the removal
of the wax without deforming the alumina-
polymer structure The dewaxed structure
was subsequently reg lled with zirconia powder
in order provide a refractory mechanical
support to avoid bending of the alumina bars
when subjected to the BBO cycle The BBO
was carried out by heating the structure to
550 8 C for 1 h immediately followed by a
partial sintering at 1050 8 C for 1 h The
heating from 100 to 350 8 C was carried out at
10 8 Ch in order to avoid any excessive
degassing of the sample from the calcination
of the organic components that might deform
the structure Finally sintering was carried
out at 1600 8 C for 1 h in a different furnace
3 Results and discussion
31 Design and simulation
The objective of the theoretical simulation of
the PBG structures was to solve Maxwellrsquos
equations inside the desired PBG geometry
As previously indicated our simulation used
two different computational methods to
investigate the PBG structure The reg rst one
the Fortran-code software was used to
reformulate Maxwellrsquos equations on a lattice
by dividing the space into a set of small cells
with a coupling between neighboring ones
(OEgrave zbay et al 1994) Then it calculated the
Figure 1 CAD drawing of the unit cell of the PBG structurefabricated by FDMM Each bar is 28 mm long with a2 pound 2 mm2 square cross-section and a pitch separation of8 mm The lling ratio of the structure is 38 percent
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
48
propagation of the EM reg elds through a
periodic dielectric structure in layer-by-layer
manner by means of a transfer matrix (Pendry
et al 1992) The transfer matrix can then be
used to evaluate the bulk dispersion and
transmission through a reg nite thickness slab of
the material since its eigenvectors are the
solutions for the electric and magnetic reg eld at
each point for a given frequency v Then the
band structure k = k(v) can be calculated
from these eigenvalues Since the transfer
matrix dereg nes how the waves cross a slab of
the material the transmission coefreg cients can
also be calculated The input to the program is
the geometry of the periodic structure as well
as the frequency v (or energy) of interest
The Transfer Matrix method was applied
to calculate the energy bandgap of the
alumina structure with rectangular rods as
shown in Table I and Figure 2 We
demonstrated that the reg lling ratio (ie the
ratio between the volume of material in the
unit cell and the total volume of the unit cell)
and the dielectric constant ratios are the major
factors that affect the bandgap existence and
the width of the bandgap frequency The
lattice constants of the structure determine
the starting frequency and the width of the
bandgap The shape of the dielectric rod is not
important since the results with square and
cylindrical rods were similar and the rods can
be either of a high permittivity material
surrounded by air or they can be made of air
embedded in a dielectric material The
frequency of the bandgap scales linearly with
the unit cell length which is dereg ned by thesize and the space between the rods This is
due to the linearity of Maxwellrsquos equations
Our second approach was to solveMaxwellrsquos equations in the frequency-domain
and for this purpose the High Frequency
Structure Simulator (HFSS) software wasused The wave-guide simulator method was
used to calculate the EM wave distribution in
the propagation direction (z-direction) The
inputs for the program were the geometry of
the structure which is dereg ned in terms of its
unit cell the monochromatic source and the
boundary conditions at the surface edges The
structure used was made of rectangular
alumina rods of 2 pound 2 mm2 cross section with
a pitch separation of 8 mm between rods The
structure exhibits a bandgap starting around
147 GHz with a bandgap width of 8 GHz
The modeling indicated that the structure
behaved like a Bragg remacr ector ie all the
incident energy was remacr ected The
transmission coefreg cient calculated by the
HFSS program has the same bandgap range
as that shown in Figure 2 using the T-matrix
approach
4 FDMM fabrication
The FDMM process was used to fabricate the
PBG structure shown in Figure 1 ie each
2 pound 2 mm2 square cross-section alumina bar
was 28 mm long with a pitch separation of
8 mm The bars were deposited parallel to
each other in each layer and perpendicular to
the direction of the immediate upper and
lower neighboring layers For every second
layer there was a shift in the position of the
rods by a half lattice constant (every reg fth layer
is identical so that a unit cell was constituted
of 4 rows of bars)
The FDMM fabrication of the PBG
structures was made with the multimaterial
deposition equipment using alumina-loaded
and wax reg laments as feedstock materials The
fabrication was made by the successive
deposition of the reg laments in a layer-by-layer
manner reg nishing each layer before
proceeding to the next one The main
problem encountered was the lack of adhesion
of the alumina layers to the underlying wax
layer The deposition parameters (deposition
speeds and mass macr ow rate) were adjusted to
overcome this problem thus improving the
adhesion of the two materials so that the
Table I Comparison between the results of the simulationand the electromagnetic measurements of the PBGstructure with square alumina rods The cross section ofthe rods is 2 mm and the pitch is 8 mm
Bandgap (GHz) Dvgapvmidgap
165plusmn235 35171plusmn233 31
Figure 2 Transmission loss of the alumina structure with square cross-sectionrods (2 pound 2 mm2)
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
49
successive layers could be deposited
appropriately Figure 3shows an as-fabricated
PBG structure with the support wax
surrounding itThe BBO cycle procedure used was the
same one as for the fabrication of other
electroceramic materials made with this
method (McNulty et al 1998a b) The wax
removal was optimized so that the alumina
rods would not bend due to their own weight
while the wax was macr owing around it for
removal The optimum temperature for the
wax removal was 110 8 C and at this
temperature it only required 10 min for the
wax to macr ow away from alumina bars In the
BBOpresintering cycle the parts were
embedded in zirconia powder in order to
provide support for the overhanging alumina
bars This procedure proved effective for
supporting the bars while not reacting with
the structure The removal of the zirconia was
simple and done using a macr ow of pressurized
air Following this the sintering cycle
densireg ed the structure leaving the typical
reg nished structure shown in Figure 4
Electromagnetic measurements were
carried out on a stack of 4 ordf unit cellsordm of the
sintered PBG structures Each unit cell
consisted of 4 stacks of bars so the
measurement involved 16 layers of bars with
the incident radiation perpendicular to the
ordf topordm side of the unit cell shown in Figure 4 A
stop band was detected between 171 and
233 GHz These results are in good
agreement with the simulation results for this
structure shown in Table I The
rearrangement of the stacks of ordf unit cellsordm
among each other gave identical results
In summary the feasibility of FDMM as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region has been
demonstrated It appears that the complex
ceramic structure fabricated in this research
cannot be made by traditional molding
methods (Knitter et al 2001) A practical
fabrication procedure for example would
involve the fabrication of individual bars and
stacking them using templates In contrast
rapid prototyping seems to be a unique way to
make such complex structures To our
knowledge another rapid prototyping
technique called Robocasting was used to
fabricate similar PBG structures (Cesarano
et al 2001)
5 Conclusions
A photonic bandgap (PBG) structure was
designed and modeled so that it would have
a bandgap in the microwave frequency
Figure 3 The photograph shows the deposition of alumina(bright) and ICW-06 wax (dark) The wax had to beremoved before BBO and sintering of the part
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
50
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
the geometry of the cross-section of each bar
of the structure was chosen so that the
bandgap would lie in the 15 plusmn 95 GHz
frequency range Alumina was used as the
high permittivity dielectric material (relative
permittivity 1r = 96) and air as the low
permittivity one
The fabrication of the PBG structures was
performed using the multimaterial deposition
equipment designed and fabricated at Rutgers
University and is described elsewhere (Jafari
et al 2000) The feedstock materials for the
FDMM process were reg laments of alumina
and ICW-06 wax (Stratasys Inc Eden
Prairie MN) The alumina reg lament was
fabricated using A152-SG alumina powder
(Alcoa New Milford CT) which was coated
with a surfactant by mixing 150 g of alumina
in a 30 gL solution of stearic acid in toluene
and then mixing the slurry for 4 h The
mixture was then reg ltered and then air dried in
order to remove the solvent The loss on
ignition test at 550 8 C for 1 h indicated that the
stearic acid adsorption was 19 wt percent
Once the coated alumina powder was dried it
was mixed with ECG-9 thermoplastic binder
(developed at Rutgers University) (McNulty
et al 1998a b) in a Haake System 9000 high-
shear mixer (Haake-Fisons Paramus NJ)
with a twin-roller blade mixing bowl operating
at 100 rpm The alumina powder volume
fractions successfully used were 60 and 62 vol
percent solids loading The compounded
alumina-binder system was then extruded at
90 8 C into continuous reg laments several meters
long through a 178-mm diameter nozzle
using the same system but with a single screw
extruding attachment
Using the input from the PBG modeling a
CAD reg le was made in order to fabricate the
structure using the FDMM equipment The
geometry of the PBG structure required the
use of a supporting material below the
alumina rods during fused deposition and
ICW-06 wax was utilized for this purpose
The part was fabricated by the successive
deposition of the wax and the alumina-loaded
reg lament in a layer-by-layer manner The
alumina reg lament was loaded into a liquereg er
heated to 130 8 C having a 500 mm diameter
nozzle The wax reg lament was deposited using
a similar liquereg er and nozzle at a working
temperature of 72 8 C The CADCAM system
gave instructions to the FDMM equipment so
that the liquereg er would move and deposit
material in a predereg ned tool pathTo avoid bending of the alumina bars while
performing the binder burnout (BBO)
process it was necessary to initially remove
the wax from the fabricated structure so that it
could be replaced by a temperature resistant
support material during the BBO process
The wax removal was carried out in an oven
by placing the as-fabricated part for 10 min at
a temperature of 110 8 C This time-
temperature combination allowed the removal
of the wax without deforming the alumina-
polymer structure The dewaxed structure
was subsequently reg lled with zirconia powder
in order provide a refractory mechanical
support to avoid bending of the alumina bars
when subjected to the BBO cycle The BBO
was carried out by heating the structure to
550 8 C for 1 h immediately followed by a
partial sintering at 1050 8 C for 1 h The
heating from 100 to 350 8 C was carried out at
10 8 Ch in order to avoid any excessive
degassing of the sample from the calcination
of the organic components that might deform
the structure Finally sintering was carried
out at 1600 8 C for 1 h in a different furnace
3 Results and discussion
31 Design and simulation
The objective of the theoretical simulation of
the PBG structures was to solve Maxwellrsquos
equations inside the desired PBG geometry
As previously indicated our simulation used
two different computational methods to
investigate the PBG structure The reg rst one
the Fortran-code software was used to
reformulate Maxwellrsquos equations on a lattice
by dividing the space into a set of small cells
with a coupling between neighboring ones
(OEgrave zbay et al 1994) Then it calculated the
Figure 1 CAD drawing of the unit cell of the PBG structurefabricated by FDMM Each bar is 28 mm long with a2 pound 2 mm2 square cross-section and a pitch separation of8 mm The lling ratio of the structure is 38 percent
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
48
propagation of the EM reg elds through a
periodic dielectric structure in layer-by-layer
manner by means of a transfer matrix (Pendry
et al 1992) The transfer matrix can then be
used to evaluate the bulk dispersion and
transmission through a reg nite thickness slab of
the material since its eigenvectors are the
solutions for the electric and magnetic reg eld at
each point for a given frequency v Then the
band structure k = k(v) can be calculated
from these eigenvalues Since the transfer
matrix dereg nes how the waves cross a slab of
the material the transmission coefreg cients can
also be calculated The input to the program is
the geometry of the periodic structure as well
as the frequency v (or energy) of interest
The Transfer Matrix method was applied
to calculate the energy bandgap of the
alumina structure with rectangular rods as
shown in Table I and Figure 2 We
demonstrated that the reg lling ratio (ie the
ratio between the volume of material in the
unit cell and the total volume of the unit cell)
and the dielectric constant ratios are the major
factors that affect the bandgap existence and
the width of the bandgap frequency The
lattice constants of the structure determine
the starting frequency and the width of the
bandgap The shape of the dielectric rod is not
important since the results with square and
cylindrical rods were similar and the rods can
be either of a high permittivity material
surrounded by air or they can be made of air
embedded in a dielectric material The
frequency of the bandgap scales linearly with
the unit cell length which is dereg ned by thesize and the space between the rods This is
due to the linearity of Maxwellrsquos equations
Our second approach was to solveMaxwellrsquos equations in the frequency-domain
and for this purpose the High Frequency
Structure Simulator (HFSS) software wasused The wave-guide simulator method was
used to calculate the EM wave distribution in
the propagation direction (z-direction) The
inputs for the program were the geometry of
the structure which is dereg ned in terms of its
unit cell the monochromatic source and the
boundary conditions at the surface edges The
structure used was made of rectangular
alumina rods of 2 pound 2 mm2 cross section with
a pitch separation of 8 mm between rods The
structure exhibits a bandgap starting around
147 GHz with a bandgap width of 8 GHz
The modeling indicated that the structure
behaved like a Bragg remacr ector ie all the
incident energy was remacr ected The
transmission coefreg cient calculated by the
HFSS program has the same bandgap range
as that shown in Figure 2 using the T-matrix
approach
4 FDMM fabrication
The FDMM process was used to fabricate the
PBG structure shown in Figure 1 ie each
2 pound 2 mm2 square cross-section alumina bar
was 28 mm long with a pitch separation of
8 mm The bars were deposited parallel to
each other in each layer and perpendicular to
the direction of the immediate upper and
lower neighboring layers For every second
layer there was a shift in the position of the
rods by a half lattice constant (every reg fth layer
is identical so that a unit cell was constituted
of 4 rows of bars)
The FDMM fabrication of the PBG
structures was made with the multimaterial
deposition equipment using alumina-loaded
and wax reg laments as feedstock materials The
fabrication was made by the successive
deposition of the reg laments in a layer-by-layer
manner reg nishing each layer before
proceeding to the next one The main
problem encountered was the lack of adhesion
of the alumina layers to the underlying wax
layer The deposition parameters (deposition
speeds and mass macr ow rate) were adjusted to
overcome this problem thus improving the
adhesion of the two materials so that the
Table I Comparison between the results of the simulationand the electromagnetic measurements of the PBGstructure with square alumina rods The cross section ofthe rods is 2 mm and the pitch is 8 mm
Bandgap (GHz) Dvgapvmidgap
165plusmn235 35171plusmn233 31
Figure 2 Transmission loss of the alumina structure with square cross-sectionrods (2 pound 2 mm2)
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
49
successive layers could be deposited
appropriately Figure 3shows an as-fabricated
PBG structure with the support wax
surrounding itThe BBO cycle procedure used was the
same one as for the fabrication of other
electroceramic materials made with this
method (McNulty et al 1998a b) The wax
removal was optimized so that the alumina
rods would not bend due to their own weight
while the wax was macr owing around it for
removal The optimum temperature for the
wax removal was 110 8 C and at this
temperature it only required 10 min for the
wax to macr ow away from alumina bars In the
BBOpresintering cycle the parts were
embedded in zirconia powder in order to
provide support for the overhanging alumina
bars This procedure proved effective for
supporting the bars while not reacting with
the structure The removal of the zirconia was
simple and done using a macr ow of pressurized
air Following this the sintering cycle
densireg ed the structure leaving the typical
reg nished structure shown in Figure 4
Electromagnetic measurements were
carried out on a stack of 4 ordf unit cellsordm of the
sintered PBG structures Each unit cell
consisted of 4 stacks of bars so the
measurement involved 16 layers of bars with
the incident radiation perpendicular to the
ordf topordm side of the unit cell shown in Figure 4 A
stop band was detected between 171 and
233 GHz These results are in good
agreement with the simulation results for this
structure shown in Table I The
rearrangement of the stacks of ordf unit cellsordm
among each other gave identical results
In summary the feasibility of FDMM as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region has been
demonstrated It appears that the complex
ceramic structure fabricated in this research
cannot be made by traditional molding
methods (Knitter et al 2001) A practical
fabrication procedure for example would
involve the fabrication of individual bars and
stacking them using templates In contrast
rapid prototyping seems to be a unique way to
make such complex structures To our
knowledge another rapid prototyping
technique called Robocasting was used to
fabricate similar PBG structures (Cesarano
et al 2001)
5 Conclusions
A photonic bandgap (PBG) structure was
designed and modeled so that it would have
a bandgap in the microwave frequency
Figure 3 The photograph shows the deposition of alumina(bright) and ICW-06 wax (dark) The wax had to beremoved before BBO and sintering of the part
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
50
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
propagation of the EM reg elds through a
periodic dielectric structure in layer-by-layer
manner by means of a transfer matrix (Pendry
et al 1992) The transfer matrix can then be
used to evaluate the bulk dispersion and
transmission through a reg nite thickness slab of
the material since its eigenvectors are the
solutions for the electric and magnetic reg eld at
each point for a given frequency v Then the
band structure k = k(v) can be calculated
from these eigenvalues Since the transfer
matrix dereg nes how the waves cross a slab of
the material the transmission coefreg cients can
also be calculated The input to the program is
the geometry of the periodic structure as well
as the frequency v (or energy) of interest
The Transfer Matrix method was applied
to calculate the energy bandgap of the
alumina structure with rectangular rods as
shown in Table I and Figure 2 We
demonstrated that the reg lling ratio (ie the
ratio between the volume of material in the
unit cell and the total volume of the unit cell)
and the dielectric constant ratios are the major
factors that affect the bandgap existence and
the width of the bandgap frequency The
lattice constants of the structure determine
the starting frequency and the width of the
bandgap The shape of the dielectric rod is not
important since the results with square and
cylindrical rods were similar and the rods can
be either of a high permittivity material
surrounded by air or they can be made of air
embedded in a dielectric material The
frequency of the bandgap scales linearly with
the unit cell length which is dereg ned by thesize and the space between the rods This is
due to the linearity of Maxwellrsquos equations
Our second approach was to solveMaxwellrsquos equations in the frequency-domain
and for this purpose the High Frequency
Structure Simulator (HFSS) software wasused The wave-guide simulator method was
used to calculate the EM wave distribution in
the propagation direction (z-direction) The
inputs for the program were the geometry of
the structure which is dereg ned in terms of its
unit cell the monochromatic source and the
boundary conditions at the surface edges The
structure used was made of rectangular
alumina rods of 2 pound 2 mm2 cross section with
a pitch separation of 8 mm between rods The
structure exhibits a bandgap starting around
147 GHz with a bandgap width of 8 GHz
The modeling indicated that the structure
behaved like a Bragg remacr ector ie all the
incident energy was remacr ected The
transmission coefreg cient calculated by the
HFSS program has the same bandgap range
as that shown in Figure 2 using the T-matrix
approach
4 FDMM fabrication
The FDMM process was used to fabricate the
PBG structure shown in Figure 1 ie each
2 pound 2 mm2 square cross-section alumina bar
was 28 mm long with a pitch separation of
8 mm The bars were deposited parallel to
each other in each layer and perpendicular to
the direction of the immediate upper and
lower neighboring layers For every second
layer there was a shift in the position of the
rods by a half lattice constant (every reg fth layer
is identical so that a unit cell was constituted
of 4 rows of bars)
The FDMM fabrication of the PBG
structures was made with the multimaterial
deposition equipment using alumina-loaded
and wax reg laments as feedstock materials The
fabrication was made by the successive
deposition of the reg laments in a layer-by-layer
manner reg nishing each layer before
proceeding to the next one The main
problem encountered was the lack of adhesion
of the alumina layers to the underlying wax
layer The deposition parameters (deposition
speeds and mass macr ow rate) were adjusted to
overcome this problem thus improving the
adhesion of the two materials so that the
Table I Comparison between the results of the simulationand the electromagnetic measurements of the PBGstructure with square alumina rods The cross section ofthe rods is 2 mm and the pitch is 8 mm
Bandgap (GHz) Dvgapvmidgap
165plusmn235 35171plusmn233 31
Figure 2 Transmission loss of the alumina structure with square cross-sectionrods (2 pound 2 mm2)
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
49
successive layers could be deposited
appropriately Figure 3shows an as-fabricated
PBG structure with the support wax
surrounding itThe BBO cycle procedure used was the
same one as for the fabrication of other
electroceramic materials made with this
method (McNulty et al 1998a b) The wax
removal was optimized so that the alumina
rods would not bend due to their own weight
while the wax was macr owing around it for
removal The optimum temperature for the
wax removal was 110 8 C and at this
temperature it only required 10 min for the
wax to macr ow away from alumina bars In the
BBOpresintering cycle the parts were
embedded in zirconia powder in order to
provide support for the overhanging alumina
bars This procedure proved effective for
supporting the bars while not reacting with
the structure The removal of the zirconia was
simple and done using a macr ow of pressurized
air Following this the sintering cycle
densireg ed the structure leaving the typical
reg nished structure shown in Figure 4
Electromagnetic measurements were
carried out on a stack of 4 ordf unit cellsordm of the
sintered PBG structures Each unit cell
consisted of 4 stacks of bars so the
measurement involved 16 layers of bars with
the incident radiation perpendicular to the
ordf topordm side of the unit cell shown in Figure 4 A
stop band was detected between 171 and
233 GHz These results are in good
agreement with the simulation results for this
structure shown in Table I The
rearrangement of the stacks of ordf unit cellsordm
among each other gave identical results
In summary the feasibility of FDMM as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region has been
demonstrated It appears that the complex
ceramic structure fabricated in this research
cannot be made by traditional molding
methods (Knitter et al 2001) A practical
fabrication procedure for example would
involve the fabrication of individual bars and
stacking them using templates In contrast
rapid prototyping seems to be a unique way to
make such complex structures To our
knowledge another rapid prototyping
technique called Robocasting was used to
fabricate similar PBG structures (Cesarano
et al 2001)
5 Conclusions
A photonic bandgap (PBG) structure was
designed and modeled so that it would have
a bandgap in the microwave frequency
Figure 3 The photograph shows the deposition of alumina(bright) and ICW-06 wax (dark) The wax had to beremoved before BBO and sintering of the part
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
50
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
successive layers could be deposited
appropriately Figure 3shows an as-fabricated
PBG structure with the support wax
surrounding itThe BBO cycle procedure used was the
same one as for the fabrication of other
electroceramic materials made with this
method (McNulty et al 1998a b) The wax
removal was optimized so that the alumina
rods would not bend due to their own weight
while the wax was macr owing around it for
removal The optimum temperature for the
wax removal was 110 8 C and at this
temperature it only required 10 min for the
wax to macr ow away from alumina bars In the
BBOpresintering cycle the parts were
embedded in zirconia powder in order to
provide support for the overhanging alumina
bars This procedure proved effective for
supporting the bars while not reacting with
the structure The removal of the zirconia was
simple and done using a macr ow of pressurized
air Following this the sintering cycle
densireg ed the structure leaving the typical
reg nished structure shown in Figure 4
Electromagnetic measurements were
carried out on a stack of 4 ordf unit cellsordm of the
sintered PBG structures Each unit cell
consisted of 4 stacks of bars so the
measurement involved 16 layers of bars with
the incident radiation perpendicular to the
ordf topordm side of the unit cell shown in Figure 4 A
stop band was detected between 171 and
233 GHz These results are in good
agreement with the simulation results for this
structure shown in Table I The
rearrangement of the stacks of ordf unit cellsordm
among each other gave identical results
In summary the feasibility of FDMM as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region has been
demonstrated It appears that the complex
ceramic structure fabricated in this research
cannot be made by traditional molding
methods (Knitter et al 2001) A practical
fabrication procedure for example would
involve the fabrication of individual bars and
stacking them using templates In contrast
rapid prototyping seems to be a unique way to
make such complex structures To our
knowledge another rapid prototyping
technique called Robocasting was used to
fabricate similar PBG structures (Cesarano
et al 2001)
5 Conclusions
A photonic bandgap (PBG) structure was
designed and modeled so that it would have
a bandgap in the microwave frequency
Figure 3 The photograph shows the deposition of alumina(bright) and ICW-06 wax (dark) The wax had to beremoved before BBO and sintering of the part
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
50
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
region Computer simulation was performed
using T-Matrix and frequency-domain
approaches The results with both methods
showed a bandgap in the required frequency
region Further electromagnetic
measurements conreg rmed the existence of the
bandgap in the predicted region The
modeling demonstrated that the photonic
bandgap can be predicted in a structure of a
given geometry and material thus allowing
the engineering of PBG structures for specireg c
applications The experimental values
recorded for the bandgap are in good
agreement with those predicted by the
models indicating the effectiveness of the
simulation in predicting the real behavior of
the structure
FDMM has demonstrated its feasibility as a
manufacturing tool to fabricate complex 3-D
PBG structures that can be applied in the
microwave frequency region PBG structures
were prototyped using alumina and wax the
latter was used as a supporting material
during deposition of alumina rods The
successful removal of the wax and the use of a
structural supporting agent during the BBO-
presintering cycle allowed successful
sintering of the structure In short FDMM is
found to be a promising tool for the
fabrication of PBG crystals in the microwave
frequency range
(Mauricio E Pilleux Mehdi Allahverdi and
Ahmad Safari are at the Ceramic amp Materials
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Youren Chen and
Yicheng Lu are at the Electrical amp Computer
Engineering Department Rutgers The State
University of New Jersey Piscataway New
Jersey 08854 USA Mohsen A Jafari is at the
Industrial Engineering Department Rutgers
The State University of New Jersey
Piscataway New Jersey 08854 USA)
References
Berger B (1999) ldquoPhotonic crystals and photonicstructuresrdquo Current Opinion in Solid State andMaterials Science 4 pp 209-16
Brown ER and McMahon OB (1996) ldquoHigh zenithaldirectivity from a dipole antenna on a photoniccrystalrdquo Applied Physics Letters 68 No 9pp 1300-2
Cesarano J Smay JE Lin SY Stuecker JN and LewisJA (2001) ldquoSolid freeform fabrication of photonicband gap structures in the 100 GHz regimerdquo 103rdAnnual Meeting of the American Ceramic SocietyA3B-12-2001-P p 40
Contopanagos H Zhang L and Alexopoulos N (1998)ldquoThin frequency-selective lattices integrated in novelcompact MIC MMIC and PCA architecturesrdquo IEEETransactions on Microwave Theory and Techniques46 pp 1936-48
Danforth SC Agarwala M Bandyopadhyay ALangrana N Jamalabad VR Safari A and vanWeeren R (1998) ldquoSolid freeform fabricationmethodsrdquo United States Patent No 5738817
Dowling JP Everitt H and Yablonovitch E (2000)ldquoPhotonic amp Sonic Band-Gap Bibliographyrdquohttphomeearthlinknet jpdowlingpbgbibhtmlThis site is continuously updated and has acomprehensive list of bibliographic references on thesubject
Feiertag G Ehrfeld W Freimuth H Kolle H Lehr HSchmidt M Sigalas MM Soukoulis CMKiriakidis G Pedersen T Kuhl J and Koenig W(1997) ldquoFabrication of photonic crystals by deepx-ray lithographyrdquo Applied Physics Letters 71No 11 pp 1441-3
Jafari MA Han W Mohammadi F Safari A DanforthSC and Langrana N (2000) ldquoA novel system forfused deposition of advanced multiple ceramicsrdquoRapid Prototyping Journal 6 No 3 pp 161-74
Jessensky O Muller F and Gosele U (1998) ldquoSelf-organized formation of hexagonal pore arrays inanodic aluminardquo Applied Physics Letters 72 No 10pp 1173-5
Jin C Cheng B Man B Li Z Zhang D Ban S andSun B (1999) ldquoBand gap and wave guiding effectin a quasiperiodic photonic crystalrdquo Applied PhysicsLetters 75 No 13 pp 1848-50
Joannopoulos J Meade RD and Winn JN (1995)Photonic Crystals Princeton University PressPrinceton NJ
Knitter R Bauer W Gohring D and Hauszligelt J (2001)ldquoManufacturing of ceramic microcomponents by arapid prototyping process chainrdquo AdvancedEngineering Materials 3 No 1ndash2 pp 49-54
Masuda H Ohya M Asoh H Nakao M Nohtomi Mand Tamamura T (1999) ldquoPhotonic crystal usinganodic porous aluminardquo Japanese Journal ofApplied Physics Part 2 38 No 12A pp L1403-5
McNulty TF Mohammadi F Bandyopadhyay AShaneeld DJ Danforth SC and Safari A
Figure 4 PBG ldquounit cellrdquo structure fabricated by FDMMafter sintering at 1600 8 C for 1 h
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
51
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52
(1998a) ldquoDevelopment of a binder formulation forfused deposition of ceramicsrdquo Rapid PrototypingJournal 4 No 4 pp 144-50
McNulty TF Shaneeld DJ Danforth SC and Safari A(1998b) ldquoDispersion of lead zirconate titanate forfused deposition of ceramicsrdquo Journal of theAmerican Ceramic Society 82 No 7 pp 1757-60
Ozbay E Michel E Tuttle G Biswas R Sigalas M andHo K-M (1994) ldquoMicromachined millimeter-wavephotonic band-gap crystalsrdquo Applied PhysicsLetters 64 No 16 pp 2059-61
Pendry JB (1996) ldquoCalculating photonic bandgapstructuresrdquo Journal of Physics Condensed Matter 8pp 1085-108
Pendry JB and MacKinnon A (1992) ldquoCalculation ofphoton dispersion relationsrdquo Physical ReviewLetters 69 No 19 pp 2772-5
Safari A Danforth SC Bandyopadhyay A Janas VFand Panda RK (1998a) ldquoOriented piezo electricceramics and ceramicpolymer compositesrdquo UnitedStates Patent No 5796207
Safari A Janas VF Bandyopadhyay A Panda RKAgarwala M and Danforth SC (1998b) ldquoCeramicComposites and methods for producing samerdquoUnited States Patent No 5818149
Shingubara S Okino O Sayama Y Sakaue H andTakahagi T (1997) ldquoOrdered two-dimensionalnanowire array formation using self-organizednanoholes of anodically oxidized aluminumrdquoJapanese Journal of Applied Physics Part 1 36No 12B pp 7791-5
Sievenpiper D Zhang L Broas RFJ Alexopolous NGand Yablonovitch E (1999) ldquoHigh-ImpedanceElectromagnetic Surface with a Forbidden BandrdquoIEEE Transactions on Microwave Theory andTechniques 47 No 11 pp 2059-74
Yablonovitch E (1993) ldquoPhotonic band-gap structuresrdquoJournal of the Optical Society of America 10 No 2pp 283-95
Yablobovitch E (1997) ldquoInhibited spontaneous emissionin solid state physics and electronicsrdquo PhysicalReview Letters 58 No 20 pp 2059-62
3-D photonic bandgap structures in the microwave regime
Mauricio E Pilleux et al
Rapid Prototyping Journal
Volume 8 middot Number 1 middot 2002 middot 46ndash52
52