OPERABLE UNIT 5 NEW PROPERTY PHASE I FIELD REPORT

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Environmental Restoration Program

OPERABLE UNIT 5 NEW PROPERTY PHASE I FIELD REPORT

MOUND PLANT MIAMISBURG, OHIO

VOLUME II -APPENDICES A-G

July 1995

Final (Revision 1)

U.S. Department of Energy Ohio Field Office

EG&G Mound Applied Technologies

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DATA QUALIFIERS

The primary data qualifiers to be applied, as described in the CLP Functional Guidelines and in Section

4.0 and 5.0 of Appendix H, of the QAPjP (DOE 1993c).

u

]

R

N

NJ

UJ

The material was analyzed, but was not detected. The associated numerical value is the sample quantitation limit.

The associated numerical value is an estimated quantity.

The data are unusable (compound may or may not be present). Resampling and reanalysis is necessary for verification.

Presumptive evidence of presence of material.

Presumptive evidence of the presence of the material at an estimated quantity.

The material was analyzed for, but was not detected. The sample quantitation limit is an estimated quantity.

Subqualifiers are used to assist in data aisessnient by mdicating the source of the primaCy qualifier. These

subqualifiers are attached to the pruDary- qualifier, separated. by a hyphen. The following is a list of

allowable subqualifiers.

SUBQUAL~RS-ORGAlflCS

B c H K s I p (+) (-)

Qualified due to method blank or a field blank Qualified due to calibration Holding time exceeded Qualified due to surrogate recovery Qualified due to matrix spike recovery Qualified due to internal recovery Pesticide/PCB results have >25% difference on two different columns Potential positive bias (added after subqualifier with a parentheses) Potential negative bias (added after subqualifier with a parentheses)

SUBQUAL~RS - INORGAlflCS

B c H s I D

Qualified due to method blank of field blank Qualified due to calibration Holding time exceeded Qualified due to matrix spike recovery Interference (ICP serial dilution, ICS, or GFAA spike recovery) Duplicate (replicate limits exceeded)

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L (+) (-)

Qualified due to LCS Potential positive bias (added after subqualifier with a parentheses) Potential negative bias (added after subqu~fier with a parentheses)

Examples of fmal qualification might be J-C, UJ-S(+), UJ-BC(-}, etc .

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APPENDIX A

BORING LOGS FOR OU9 MONITORING WELLS IN THE NEW PROPERTY

•

ss u

•• s

10

15

• DEPTK

_a. so

WeU Materials

1A BACKFILl..; QrouL

ISO:ta::N: Jir sloe, 4A PVC. 1.25•.

GRClnlDWA TEll HOUR DATE

09126/SJ

Pr'Ojecc Manaver ~AGE:

1 of _L_

TopsoiL

Brown sandy silt. very stif!', damp, trace clay.

Browa &Ad gmy IUdy lilt. moderately stiff. damp, tnc:e rock

Cnpc~~ts. ma: day.

Total Depm • 10.0 (eeL

GEOLOGIC LOG ••

Well Materials

ss u lA Bentcnite.

ss u 5

. 3A

4A

10

SS U SA

15

• GROUMDVATER

Project 11anager i'AGE:

1 of 1

Lilhclogic Description

TopsaiL

8tOWD sill and day, vuy stiff. mcist. same sand. trace grawL

BlUM~ md P'IY eta~ silt. hard. mcist. tna: sand. uace nxi: l'lapat:1la.

Oray shale. moderately weachemt. limey.

Tow Oepdl • 15.5 Ceet.

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•

Sample Ocptn r---r------1

T A ID

0

ss u

ss u 2A

SS U 4A

10

1.S

Well Mau:riail

:.. .. .-., .;

ss u SA ISCREleN: .or slat. us-.

DATE

~ r--+---1---J J.._ _ _.__-'----l

Pr'oject Manager

Pill • brurm sandy silt. moist. trace gravel. trace clay tile.

Brurm sandy gravelly silt. hard. moist. tnee clay.

Brawn sud ud pllftl. medium duse. moist. some silt. uace cabbies.

ToW Dcpdl • 20.0 tees.

•

Sample WeU Materials

T A JD

ss u 1A • Bcuuomce. BtCIWII sandy, cl.ayey silt, very sill'f, moW. trace g:r"~WL

• lA

10 ss u 4A

SA

~~IU:.Ic:.t'l: .ar stet. PVc. us·.

• ss u 6A

DEPTKIKCIIII OAT!

Sample Oeprh t--,---.----1

T A 10

0

Well Materials

BACKFILl.; Cement beniollite gzout.

• s ss u 0001

10 ss u 0002

ss u 0003

• CROUHD\IAT£R

DEPTH KC1Jil DATE

22.21 08:38 09/20/90

MOUND PLANT ~rojec:t Manager

John S. Pl'ic:e

Uthologic: Description

~AGE:

1 ot "

Dark yeLlowish brawn (lOYR 3/4) silty clay, still', low plwic:ity,

moist. tncc of sand.

Dark yelloMsh brawn (lOYR 3/4) sandy day, very srifl', low plaltil:ity, moist. trace rme to cousc ~i.

BIOMI (lOYR 3/4) sandy, paveUy clay, very swr. low plastil:icy,

moe.

Brawn (lOYR. 3/4) clayey, pavelly sand, poorly pdcd. modcntely dasc.moi&

BlGMI (lOYR. 5/3) silty sand. -u pdcd. very dense.

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GEOLOGIC LOG

ID 20 ss u 0004

2S ss u 00115

30 ss u 0006

ss u (XDI

Well Maccri.ala

:..·,_ ..:

Well Q:)Q

MOUND PLANT Project Mane9er

John B. Price

Lit.hologic Dcscnpcion

OU~ brawn (2.5Y 5/4) clayey, gravelly sand. dC11SC, ._L

PAG£;

_2_ of f.

OIM: blOWil (lSY S/4) clayey, ~lly sud, paorty padcd, dense.

wee.

Dam pay (JY 4/1) sudy, ~Y clay, medium stiit low pluliciey. moil&.

I..iPC yaiowish biOWII (2.SY 5/4) eta~. gnrwllysaAd. very dcuse, ,.,.,

GEOLOGIC LOG

·• Sample . Dcplll t-~....:.,-----i T A I'D

50

ss ss u 0011

• 60 ss u oou

6S ss u 0013

ss u 0014

70 ss u oou

•

WeU Maccrial5

:..".,.;.. ..;

Well CoG

Project Menao;er

Ligbt oliw bi'OW'Il (l.SY S/4) silty, gravelly sand. deASC. wee.

Dart p8yil!l bi!OWII (l.SY 4/2) gravelly saud. poody ro -u graded. m.odclaleiy deuc. ..c.

GEOLOGIC LOG

• Sample Well M.accrials

ss u 0016

7S

80 ss u 0017

• 8S ss u 0018

90 ss u 0019

ss u 0020

9S

•

Well CaA

Project Manaver PAG£: MOUND PLANT

4 of I.

Ugl:lc olive bl'OWII (2.5Y 5/4) eta~. sandy grawt, very c1c11se. weL

Ugl:lc yetlawisb bl'OWII (UY 6/4) to oiM: brawn (2.5Y 4/4) eta~. gmeiJy saDd, wetl pdcd. clcac. -L

Ugl:lc ye!lowiiJl brawn (2.SY 6/4) to olive browft (2.SY 4/4) ClaJ'=Y, pvdy sud. w.:ll p-aded. clcue., -L

Olive btaWD (2.5Y 4/4) ~. pwlly Ulld. -u padcd. wrr dale.w.t.

TOUl Dcpda • 9.5.0 Cect.

WcUMaccrW&

ss u 0001

• 5

ss u 0002

10

ss u 0003

lS

ss u 0004

•

MOUND PLANT PAG£:

Usbologic Description

Out yeUowish browa (lOYR. 4/4) silty clay, leu. stia, low pluticicy, sligbdy moil&. same saDCL

Dart yeilolriiJl browa (lOYR. 4/G) sudy, siicy clay, sUa to very aia., medilllll plu&icicy, maisL

of _s_

Dart yetigwisb brown (lOYR. 4/4 to 4/6) ~sand. soft to medilllll sua. medium plaaicicy, very moist, trace ruse to medilllll pveL

Ydlowilll brown (lOYR.S/1) clayey sud. -u paded. verrdaue.

mail&.

Ugbt yellowWI bJOWD (10Yll6/4) ~. silty sud. medium dcase. asoiiL

GEOLOGIC LOG

• Well Maccriala ID

ss u ooas · BczuoDice

ss u 0006

30

• lS ss u 0008

·~-

ss u 0009

4S

•

WeU Con

Project Manager

John B. Prfce PAGE:

......L at _L

L.i.glu o!M: browa (UYR S/4) gnm:Uy, sandy, silty ctay, nifr. low plaslicUy, moisL

a. Orayilil browa (UY S /2) sandy clay, very swr. low plalliciry,

moilc.

om: pay (SY 4/1) sanc~y c~ay, vcrr ma to lwd.lolr piaaicicy, mail&.

SW Browa (lOYR.S/3) sand, weU graded. dense:. wet, tncc of silL

L.i.gllC o!M browa (UYRS/4) sud. inccrta,.:rai poorty IDd wet1 padcd. cfeDSC. wet. tncc of rme co medium pawl.

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GEOLOGIC LOG

Sample Deptll 1'-~-----:

T A 10

ss ti 0010

so

ss u 0011

s.s

ss u 0017,

60

ss u 0013

ss u 0014

70

ss u oou

Well Materials

GltClJND\IATER DEPTM HOUR DATE 25.55 08:42 08/19/89 25.26 08:4_2_ 09/20/90

Well Coil

MOUND PLANT Project Manager

John 8. Price

PAGE:

_3_ of _'i_

Uth

... ·

Uthologic Ocsaipcicn

Olive brown (2Sl 4/4) sand with silt and clay, interta~rcd, well and poorly graded. medium dense, wet.

Dark cnayis1l brown (2.SYR 4/2) silty, pawlly sand. poorty graded. dease.WU.

. Dam pyisla biawa (2.SY 4/2) gnwJJy Wid., well graded.

moclcnt.dy dcasc, wee. cncc of lilt.

SP Omyish brawn ('Z.SY .5/2) S&Dd. poorly graded. c:oane grmed. modaaccly dcmc. wet. tna: fine pawL

SP Orayisla btoW'Il (l.SY .5/2) S&Dd. poorty graded. c:oazse ~ modcftccly deDsc. wet, tnaa: fine pawL

GEOLOGIC LOG

WeU Materials

iS

ss u 0016

80

u 0017

• as

ss u 0018

.. 90

ss u 0019

95

ss u 0020

• GRCUMO\IAT R DEPTH HOUR OATE 25.55 08:42 08/19/89

_25_L26 08•42 09/20/90

MOUND PLANT Projec~ Manager

John B. Pf'ice PAGE:

4 of _s_

... · SP Dark gnyish brown (UY 4/2) sand. poorly gnded, modcracdy dea.sc. -L

·.:··.·

SM Dart grayish brown (UY 5/2) silty sud. -u graded.lllodcmcly c1cuc. -c. tn= t1Ac co medium graftl.

SW. Dark payilll bZUWD (l.SY S/2) sud. -u graded. ccaae paiDcd, lllodcnldy dcu:. wa. uacc ruu: lO medium graiAect paftt.

SP Dam grayisb bZUWD (l.SY 4/2) sud, poorty pdcd, t1Ac paiacd. lllodcnldy deue. w.:L

Dart pyiiD bZUWD (l.SY 4/2) prldly sud. wetl graded. IIIQdcnSeJy dczlsc. w.:L

Dart &nyisll broM~ (l.5Y 4/2) silty saad. poorty padcd. modaarcly clcuc.WU.

GEOLOGIC LOG

• Oeptll r---:Samr--..,PI_e_. ---1

T A lD

100

ss u 0021

lQS

ss u 002l

110

• ss u 0023

115

120

•

WcU Materials

.-. . ... .._,__

WcU CaA

Projec' Mana;er

John 8. Price

U&hologie DCSC'riptioa

PAGE:

_s_ of _s_

SM OIM: b!OWII (l.SY 4/4) siltysaad. intcriayl:rcd., w.:U aad poorly

graded. madcmtcly dcDse, wa.

OIM: b10W11 (l.SY 4/4) ~. siltysaad. intcdayercd.. well aDd poorly padcd. deDic to very dcDse, W.:L

OIM btOWil ('2.SY 4/4) lilly sud. poorty padcd. modcmdy dcDse. ...

To&aJ Deptll • 117.0 (CCL

•

s

• u CXIOl

10

lS

ss u ems

•

Well Materials Well Coli

MOUND PLANT

SP 81DWII to lipc bn:I'Ml pave.Uy Alld. coarse paiAcct. dry, IIODSZDcificd. DO ccmcat. appn:llimaccly 4090 pavct up co 1 iadl in diameter. 111Droundcd. HNU•O

a. Bn:I'Mllilly. alldy day', dalE blVWDIDOCdiq. Wm. bip pl.lllidcy. ~ moisc, DO C~:~~~at. aocaradflcd. app~CllDmaee1y S'ii pii'V'IIIilup to 1/4 iadl ill dia.lllca:l'. HNU•O.

SM- upc blVWD to blVWillilly, ~Y AAd. acmantiracd.DO ccmcac. SP llliCiillc. poody pldcd. appn:llimaccly ~ pvd up to 1 iadl in ~. S'llbftnmdcd. HNU•O.

SP lJpc blVWD to pay pPCUy Alld, coarse pained. poorly padcd. 'ft&k1y CII:IIICIItCd. wa:.appraximaldy .309& pwi up to 1/'Z IN:tl in diamcta". ~ HNU•O.

GEOLOGIC LOG

WeU Materials ID

SS LI 0004

2S · Bcntanit~

ss u ooas

• ss u 0006

3S

40

•

WeU Con

MOUND PLANT Pr"oject Manager"

Uthalogic Descriptiaa

PAGE:

...1.... of _L

SP Light brgwn silty, grawUy sand. caazse grained. poorly graded. wak1y cemcn~d. M:t. ncmsuatified. 409& gra¥el up ta 1 inch ill cliame~r. subrovncled. HNU • 0.

Ught brgwn ta gray gravelly sand. ccazsc grained. poorly graded. saNmtcd. nansuarified. no ccmcnr. approxima~ly 4090 grawi up to 1 il1dl ill cliameter. subrowuled. HNU •0 •

Lipt brown silty, gmetly sand. caanc: grained. poarty graded. sacumcd. aOilltratified. watly c:cmcnted. apprazimatcly 3QIN pawl up co 1 il1dl in diameter. S1IDrowldcd. HNU•O.

Total Dcpdl • 39.2 teet.

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• APPENDIX B

FIELD LOGBOOKS

B.l SITE MANAGER LOGBOOK B.2 SOIL GAS LOGBOOK B.3 FIDLER LOGBOOK B.4 SEEP LOGBOOK

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B.l SITE MANAGER LOGBOOK

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LOG eo-oK

PROJECT TITLE: EG&G MOUND OUS NEW PROPERTY PHASE I RI/FS FIELD INVESTIGA TJONS

WORK SITE: MOUND PLANT Miamisburv. Qh;o

OU5 New Pronerty

ACTIVITY: Mound OU5 New Praoerty Phase 1 RllfS

field Investigations

CONTRACT#: -----------------------------TASKORDER: ~:.~~~96~------------------------

PROJECTMANAGER: ~Th~o~mwa~s~n~a~n~k-----------------------COMPANY NAME I ADDRESS: Science A/2p/icatjons lntemationst Coepocat;on

.. 4031 Colonel Glenn HwY .Davton. Ohio 45431

TELEPNC-NE NUMBERS: ~(5:..&..:1311411:..;:4::=2 ... 9-;a2al.l691Ui9'------------

SUPERVISORS: OU5 Manager: Alan S.Qesard (513.1865-3859 SAIC Pcqj. Manager: Thomas Tank (51~1429-2699

EMeRGENCY RESPONCE: Police /Ambulance I Eire fi11 or 865-404Q

PROCEDURES: sop 1.1. sop 1.3. SOP 1.4. soP 1.5. sop t.6. SOP 1.8. SOP 1. 15. SOP 2.2. SOP 2.9.

SOp 6. 7. SOP for petrex t=nviranmental Survsys.

START DATE: ___ :r~--..'11/f/J:~y-ai_~___.;;./~.:...:;'f_:_. ----

END DATE:------------------------------

Date (mmldd/yy): t,/Z4/14 Of : OtJA PAGE _L OF 1

Task Team Members:

Narrative (include time and location):

• /1'30 • ( Z(5' t.vAJtf{

, ~it. 4J 1' s<i

Daily Weather Conditions: A.M. ---Jtr.:..· ..:.J~~~~'Hv~si"'--:!1:.6H{~U_,.1----JI:...::::5':....:..F ________ _

• P.M. Slmct I ftntlz ft C4ft:t!/

Record~ By __ ~;..;;;.~:_·..;;:: .. =·-._, _l..t.-.:.{Z;;;...4--.f~ff......__ OA :hecked B~ ~¥ h

Date (mmtdd/yy}: _ _;_I;...:./2~~'-1.;_94..;,.._ __ TIME : 0 %' 00 PAGE l__ OF 'L-

Task Team Members:

.Jct!N D.htlt~


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Pb. z.. ~ f;vr~<

Vuti d/lit.ocr. I

og 10- {/16. CutfzNy /tN£S. )u,tV(J't?~J 4fq frtNf tllkl

lllO-tZ1tJ. LPNCJI

/2.1() -lj20 Ct.Jttiltll~ OAf @1/N-I

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4.l l~ool r. teJr l.ttt. le!b fit' Ht!41 f/rl~t" Al/;cact 11 ·No! A IJ. I.

ftAtUL tHa/fi : 01- OS'I$ .. t:JI- 1194- rZ1. {BMt).

Daily Weather Conditions: A.M; . at/fiCA!_ t, rfolZI( ld/ fj!IN I 3,-r'f:

P.M. 5/bVU..

Recorded By __ \2..¥.M;~&J-.~___;;;;:?e!:..-=.;;;;::=:---OA Checked By . ~i"\ -. ~j

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Daily Weather Conditions: A.M •

P.M.·

NA

Recorded By ____ v: __ ~_¢...;;.a__.ii_.;;;;:~..._=====- QA Checked

Date {mmlddlyy): --:..j.I(-=U-=1/:......~:9...~..4__::W::::..:E.~::::D::;...__TlME: O'l' ::..3.:.0 __ · PAGE _j__ OF l

Task Team Members: PG,4 .j ()HN 1>1"1'\1 IJ

Narrative (inc!ude time and location):

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. LZO~ .. lfOtJ l.uA)trl .

Daily Weather Conditions: A.M.

P.M. .f

~ ~{}~'-·~l Recorded By ----J.o~fl'.'li~-/--· .:::J::::=:=--- OA Checked a: · 1 ~4

-

• Date (mmtdd/yy): If 2... 1- 114- 1Ht.JgS

Task Team Members:

TIME: 0 ~ OQ PAGE_·_( OF____....._

P& 5 To~\ UmJIS

?111.-'t ?M r1/Jff


OAJ I i/c. -<) (Jft(J

• Daily Weather Cond~ions: A.M., dni?zlt mit!- At/It':" ,th/N, 4tJul' ,

. P.M. ____ ..;._loo»J,.~.;....._--------------

~J >.~- YJ:>tl>~ Recorded By __ ....;\ ;....r:f.~'f.l __ v;...-_ ........ · -='·-;!::-~-a:=::::::=- OA Checked By ~(\

Date (mm/dd/yy): ( {31 / ?4 ~t7Al TIME: Q~tJQ __ _ PAGE __!___ OF --

Task Team Members: 'Pb (c ·.

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t2Do - .1!) t¥Jsi1E .

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Daily Weather Conditions: AM. ~Cia.?J'-!ltd~, Jol:a~rtl:.e)f~(ltf~l-.... , ~~~--=Z=O:.....;"F;.__ _______ .....,

P.M.

• Date (mm'ddlyy): _z'-'j'1-/'+t(...s.;1tf-::;:;;;, ;,..._ ___ TIME:

Task Team Members: PG i-0 AZD PAGE _l_ OF ___,, _____

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'

Record~ By __ :;i~~~e:!::::6:z;::.:~~r-----OA Checked By 2~

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Date (mmldd/yy): 1, / Z... ( Cft/-Task Team Members:

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PAGE _j_ OF. 2-

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Daily Weather Conditions: A.M. ...!:. t,:::::~,:.::::IJ.:.:.-·~/2r.:;.· ~~~-Tt ---.C""'·le.:;;;o./;..._ _________ _

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Recorded By ~ • OACheckedBy \i~

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Date (mnv'dd/yy): z..j :z../qf • ·,TIME : /I!Jr· --- PAGE _1::-oF 2-

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Date (mm/ddlyy}: . Z. ( ~ ( Cfl

Task Team Members:

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TIME: 01-4{) __ PAGE _.1_ OF 1. PG· to

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• Date (mm/dd/yy): _-z..._,_/...;;;~-+~-q"-y~--TIME: dtt

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Task Team Members:

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P.M. 2~ "E: {1.,_,., t:: lcJ,

Recoro~ By y~ ~ OA Checked By -~~__.;~~~~--

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Date (mmldd/yy): z.j-, ( q<.{. TlME: 014? -- PAGE _j_ OF 2.:» Task Team Members: PG-12-XllM.\ J=Oax v: \ s'a · ~?


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-· Date (mm/dd/yy}: 2...(7(<14 Task Team Members: w J=l,...,,.\o

TIME: dl+-: __ PAGE ...2::::: OF L

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P.M". Nft .

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' • DATE COlLECTED (MMIDDIYY): ____ _ TIME: (HH:MM) ------

MOUND SAMPLE NUtdBIS6: -1200

SAMPLING -

LOCATION CODE: -UU..J.N..I.ll&.-..;::.....,..------ DESCRIPTION: MOUND OUS NEW PROPERTY SEEPS

POINT CODE: ---'_......._ ___ .::a.....,....---- DESCRIPTION: SEeP NUMQE;B 1

SAMPLE-

MEDIA CODE: _.5CK5 ___ D,ESCRIPTION: -....lll:qoWI~.Mioii~IUIUii.L.-------- DEPTH ____ TO ___ _

• WEA

. FIELD OBSERVATIONS: ------------......_~_...iiili~Cr~-----------------

SAMPLE TYPE:

GRAB § SPATIAL COMPOSITE TIME COMPOSITE QC TRIP BLANK QC RINSATE QC FIELD BLANK

UNITS READING

OTHER (SPECIFY)

SAMPLE COLLECTED: YES NO

SAP SAMPLING PROCEDURE WAS FOlLOWED? YES NO . ,fiELD CHANGE ORDER REFERENCE NO: ____ ___;:....,...-__

IF SAP WAS NOT FOLLOWED. SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:----------__;:,..,~-

.. .• : .. RECORDED By: __ ___;, _________ _

(SIGNATURE) OA CHECKED BY:--------------

ISIGNATURE)

\t.i·;i•'l ~

, ~,..

~··· I

METHOD NAME AND NUMBER PRESERVATIVES C~O·C II AIR BILL II LABORATORY

ANALYSIS lTYPENOL)

"' .. Volatile Organics HCL pH< 2, 4°C IT

2- 1 LlTER Semi-Volatile Organics COOL 4°C IT

2 -.1 LITER COOL IT

1 - 1 LITER Plastic HN03 pH,2, 4°C IT

1 - 1 LITER Plastic NaOH pH>12,4°C IT

2- 1 LITER Amber Glass COOL 4°C IT

1 - 1 LITER Plastic Chloride COOL4°C IT

1 - 1 LITER Plastic fluoride COOL 4°C IT

1 - 1 LITER Plastic Sulfate IT

1 - 1 LITER Plastic Nitrate I Nitrite IT

1 - 1 LITER Amber Glass Total Organic Carbon CTOCl IT

1 - 1 LITER Plastic Total Dissolved Solids ITDS) IT

1 - 1 LITER Plastic Total Suspended Solids (TSS) COOL 4°C IT

1 - 1 LITER Plastic Total Nitrogen (TKN) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Alkalinity COOL4°C IT

1 - 1 LITER Plastic Ammonia H2S04 pH<2,4°C IT

1- 40ML Plastic Rad Screen COOL 4°C IT

1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,4°C PACE

1- 260ML Glass Tritium COOL4°C PACE

SAMPLE ID'S lliNSATE: TRIP BLANK: FIELD BLANK: •·

RECORDED BY: OA CHECI<ED BY: (SIGNATURE) (SIGNATURE)

t-: ;-

...... , ··----- ~~ ' --- ~* ~---- .. .. ·-·-·.- .. -···~-· . ... . . .. : =·-·---~-· ·__;.;..;..:::: .

• -·

I

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/ SMPLE PARAMETER ~

SURFACE WAlE QUAUTr' SAMFUNG RECORD

005 NP PAGC: _OF'_

LOTZONTROL 0 NA

SAI.IFt.:: I E _K':.:.....· ----

ACC.:..7 C~ COCE _A __ _

LOCATION ro

SAllPU:IO

. LOG OATE

).HAL'r'TICJ.L LAS COCE ----------~ CCCE SlUe

s:AMPUNC PS!OO: SiAR'i ------/:~:L::t~ -------s:AMPUNG MEiriOO __;GRAB:::;;:;;,;:;;;_ _______ ;~ OATE Sali -------

COMMENTS ----------+-~----------·/

PNW.Ien:R MEJ.SURSIEMI'S:

Fon:::N'TTAJ... OF' litOROG' pH

SPEClFIC CONOUC!ANCE. E:c .. Eh

1\CP

. ALK

00

S.WPl! itPES':

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! WEATHER; fo99V. ov ( /l.C/tj +-, ;f. dt~rzu, tE6F, 11 bJUu. fx.l ~ . ~ I ,.

·~

~ REQUIRED PPE: Jt;M pufFd. r-yffEM ·. V~tf, c~!JRf.· ·sk£/ it:JtJ/s, tA# ?ltfrU'.S

'ng i dividuals attended the daily "tailgate" safety meeting: (Signatures) . {(., .

Site Health & Safety Officer

OATE:. __ ,~(u;;;.._,.,j,(-=-14...:..._ ___ TIME: Of: 30 1 ..

4

~ ij !'

WEATHER: __ ~~=o~/~d~,--·~~~v~~~~=~~~,~~-~--~~&U~z~~~.---~-4~0~~--~+~~W~I~N~J~c~~~i~lf ________ ~~

WPICr 'f diUUS51tJAJ:

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OY/ g individuals attended the daily "tailgate" safety meeting: (Signatures}

oATE:~<r-=-/3-..:..r{/~9~4 _____ TIME: (.) ?' c1.;;;..() _

!

r:-··· --~___,;,.__-REQUI~ED.PPE: UEwt

1QfltJIEdrMi, f'llftzly lfiMg.S, Val-, c~r,. sla/tf:tc..

~(}d/;, 'lai,I(J .

·ng individuals attended the daily "tailgate" safety r:neetinQ: (Signatures)

••

DATE: __ 2--~-o/...;;.2....:../__;4;....;.r./ ___ TIME; /) /!; : I D

wEATHER: Celt:l. · 1 s:*r Cua~

- ~ . ~~~ -l ~!_ ..

The following individuals attended the daily "tailgate" safety meeting: (Signatures) .. ·"

•

oATE: 2-/-r / qc.f TIME: DB : 20

WEATHER: t~ ZZ •..;:'"

REQUIRED ·PPE; t\o.vd \.1g..\=s 1

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~uaJs attended the daily "tailgate• safety meeting: (Signatures)

Site~afety Officer

:.; ..

• DATE:. __ z.._,_/_'1;...&../....:.q'f-'------ TIME: 0 ~ : 3 5 ·.

-

WORKING CONDITIONS:---------------------

The following individuals attended the daily "tailgate": safety meeting: (Signatures)

2- ( I 0 I 94= TIME: __

weATHER: 'l ° F t v~ ~t&. 4 I~. ~on~ Cle~

= ~:

·------------~--------

The following individuaJs attended the daily "tailgate" safety meeting: (Signatures)

! .

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i .! ,.

:!· ,, j (

TIME: D 8 ; 5 S"

-:? . C' r--WEATHER: ~(p ·r

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The following individuals attended the daily "tailgate" safety meeting: (Signatures)

':~· Si;;;th7satety Officer

OA TE: . .--;;2~/_.2.....,.1:~/:__9.J...lf""'---- Tl ME: V J : 50

WEATHER:~~~2~~-f~~(4:·~~~S~k~i~~~~~--------------------------~---

REQUIRED PPE; ~,...C~ C;\a.c;~s ,. 'S-tu\-t&!d. "!kts 1 ~to~

attended the daily "tailgate" safety meeting: (Signatures)

~atety Officer

L . !

: I ' I .i I

: .• i

DATE: __ z .... /.;:;;;.z...;..~'-/1;;...:4-~--TIME: Or: "f':i""

The following individuals attended the daily "tailgate" safety meeting: (Signatures}

DATE: __ Z+/t=l-::..;.)""-1 4-..:_ ___ TIME: 0 "T"' _tJ _

WEATHER : ____ .;::C.O:::.:l:..::d:...._...;,l.;:;...-=~::;;..;a;...."...:.F._.,.._....,;It:.;;..A;._z-.~-'1 ... , .....:C .. tf;..:.:h:.:.:Hf;.c.._ ________ _

]o/t's d!,scuJstd:

- ltv tqk:b

REQUIRED PPE: __ .:;.;m:.::~=1....::..:;DI2x:..c;d;"""':1~9h~~"""~=....;,=--. ------------~ .. ~

The following individuaJs attended the daily "tailgate" safety meeting: (Signatures}

~dq . .. ...

.. Site Heaith & Safety Officer

' -, ' li

DATE:. __ -"3.-r-0.:.r-~/,..f...~-4 ____ TIME: tJ 2o.o~-

REQUIREDPPE; ______________________________ ~---------------l-ook, • !ttug.s.

t I

The following individuals attended the daily "tailgate" safety meeting: (Signatures)

v~ Site HeaJth

•

•

•

•

B.2 SOIL GAS LOGBOOK

•

•

LOG BOOK

PROJECTTITLE: EG&G MOUND OUSNEW PROPERTY PHASE I RVFS FIELD INVESTIGATIONS

~ · .. WORK SITE: MOUND PLANT

Miamisburg. Ohio

· OU5 New Property

ACTIVITY: ·Mound OU5 New Property .Phase 1 Rl/FS

Field liwestigations

CONTRACT#: --------------------------------TASKORDER: ~-3~4~8~96~------~--~---------------

PROJECT MANAGER: ·-.,.!..IThwo'"'m!..!.!ia:!.l::s~T.!..5:awn~k-· -------~ .. -. _..__~ COMPANY NAME I ADDRESS: Science Applications International Corporation

4031 Colonel Glenn Hwy .Dayton. Ohio 45431

TELEPHONENUMBERS: ~&~1~~1~4~2~9-=26~9~9~---------------------

SUPERVISORS: OU5 Manager: Alan Spesard (51~)865-3859

SAIC Proj. Manager.· Thomas Tank (513)429-2699

EMERGENCY RESPONCE: Police /Ambulance I Fire 911 or 865-4040

PROCEDURES: SOP 1.1. SOP 1.3 I SOP 1.4. SOP 1.5. SOP 1.6.

SOP 1.8. SOP 1.15. SOP 2.2. SOP 2.9.

SOP 6. 7. SOP for Petrex Environmental Survevs.

STARTDATE: --------------~~---------------ENDDATE: ----------------------------------

,--------• 1 111 .I .. II iJ,f .ill fQW I, , . . _:; QM7 , .... N

True North

Location Map

LEGEND

c=J Structures

-·-·- Plant Boundary

==== Paved/Unpaved Roadway

_ .. _ .. _ 5Ephemeral

I ream

• Fidler and Soli Gas Sample

0 Fidler Sample

Jlll_E:

PHASE 1 ADLER AND SOIL GAS S~VEY

AQUAE:

2

I

~=)Aift===== ~L'-- ~ -- _j r ." ~J .::::::::_ ..... ' i~--- \

~. -r

AT ALL ADLER SURVEY POINTS, A st.R=ACE RADIOLOGICAL SOL SAMPLE WU. BE COli.EClED FOR ANALYSIS AT

. 1HE ~D PLANT SOL SCREENNQ FACUTY

- --- --~

;u

~ a

'\

8 38

9 39

10 40

11 41 .

12 42

13 43

44

15 45

16 46

17 47

18 48

19 49

20 50

21 51 ~·, \ (:,AS

22 52 so.\ GAs

23 53 So,\ ~!a

24 54'$o .• \ C,e..~

25 55 "5o~\ C:,o.s 26 56Sc;.\ ~~

27 57<;o.\ C,e.-s

58 -so·,\ ~~ ~~(pS

29 59

30 60 .L&~ a-s

... ,. , ..... -------..

PAGE FIELD LOG PAGE FIELD LOG

91

62 I' I' · 92

93

94

95

96

97

96

99

100

101

106

n 107

78 108

79 -sc,, t &o.-c )NCEA I 109

80 \\ 110

81 ,, 111

82 112

83 113

84 114

85 115

86 116

87 117

88 118

89 119

90 120

-

• (mmlddlyy): __ 2.-+/-"t..;...,f ''-C}..:...f..:....-__ TIME: Ot30

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• Date (mmldd/yy): __ 1...;..,/.:;;..2dz...,.1/q~y'---__ TIME: II : 30 PAGE~ OF ._3

Task Team Members:

.:J1) CSAtC) Jtt {SAIC.)


//'~(). tZOo /.ttri fm.t r,P/Il. # 5 gt 450. {Atdf "'<' MC!IItM)

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1~"10- t'/53 0~ € 10517- -~ 4A.UL

Daily Weather Conditions: A.M. ____.Q!J.u.la-..J....------------r----· ---P.M. &/i., ~ 10' F, k)i,J, frm \J (i) ¥

OA Checked By _-:?_V_· ..;...;;..;.~---------=---

.mmlddlyy): z.j Z//11./ TIME : __f!:/.:-: 55 . PAGE ~ OF .3

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JD ()~'£.) m (NEtrr) ·

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FIDLER

LOG BOOK

PROJECT TITLE: EG&G MOUND OUS NEW PROPERTY PHASE I RI/FS FIELD INVESTIGATIONS

WORK SITE: MOUND PLANT

Miamisburg. Ohio

OU5 New Property

ACTIVITY: Mound OU5 New Property Phase 1 RilES

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CONTRACT#: --~~~~--~----------~------TASKORDER: _34~·~8~9~6 __________________________ __

PROJECTMANAGER: ~Th~o=m~a~s~~Tc~a~n~k _______________ __

COMPANY NAME I ADDRESS: Science Applications International Corporation 4031 Colonel Glenn Hwy ~Davtonl Ohio 454:31 ·

TELEPHONENUMBERS: ~(~5~13~)~4~2~~~26~9~9~--------------------

SUPERVISORS: OU5 Manager: Alan Spesard (51 :i)865-3859

SAIC Projl Manager: Thomas Tank (513)429-2699

EMERGENCY RESPONCE: Police /Ambulance I Eire 911 or 865-4040

PROCEDURES: sop 1 I 1 I soP 617

START DATE: ---=3':..1-fz~/CJ.:..,_'f~.--________ _

ENDDATE: ---------------------------------

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1/14/93

NOT& AT A1J_ ADLER SURVEY POINJB, A SLfiFACE RADIOLOGICAL SOL SAMPLE WLL BE COI.l..EClED FOR ANALYSIS AT TiiE MOlttD PLANT SOL SCREENING FACUTY

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ALJ<AUNITY

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SAMPLE TYPE:

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QC RINSATE QC FIELD BLANK

FIELD MEASUREMENTS READING UNITS .. AIA .. ..::a. .,

OTHER (SPECIFY)

SAMPLE COLLECTED: @> . NO • SAP SAMPLING PROCEDURE WAS FOLLOWED? @ NO FIELD CHANGE ORDER REFERENCE NO: -------- ~

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~~--~----~------------~------~----~~~~----~~--~ lX 3- 40ML Glass Volatile Organics HCL pH<2, 4°C IT

LABORATORY

1 - 1 LITER Plastic CLP Metals HN03 pH,2, 4°C IT.

1 - 1 LITER Plastic Cyanide NaOH pH> 12,4°C IT

2 - 1 LITER Amber Glass Explosives IT

1 - 1 LITER Plastic Chloride IT

1 - 1 LITER Plastic Fluoride IT


1 - 1 LITER Plastic Nitrate I Nitrite H2S04 pH< 2,4°C IT

1 - 1 LITER Amber Glass Total Organic Carbon ITOCI H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Dissolved Solids ITDSI IT

1 - 1 LITER Plastic Total Suspended Solids ITSSI IT

1 - 1 LITER Plastic Total Nitrogen ITKNI H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus ITPI H2S04 pH:< 2,4°C IT

1 - 1 LITER Plastic Alkalinity IT

1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C IT

1 - 40ML Plastic Rad Screen IT

GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH <2,4°C PACE

Glass Tritium PACE

Ns¢39$1

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I WEATHE"------------------------~~~---------------------------------

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SAMPLE TYPE:

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READING UNITS

OTHER (SPECIFY)


SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO . ,fiELD CHANGE ORDER REFERENCE NO: ------;::..,----

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(SIGNATURE) (SIGNATURE)

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C~O-C II METHOD NAME AND NUMBER PRESERVATIVES

ANALYSIS (TYPENOl) AIR BILL II LABORATORY

.. .. Volatile Organics HCl pH< 2, 4°C IT

2- 1 LITER Semi-Volatile Organics IT

2 -.1 LITER COOL IT

1 - 1 LITER Plastic IT

1 - 1 LITER Plastic NaOH pH> 12,4°C IT

2 - 1 LITER Amber Glass COOL 4°C IT




1 - 1 LIT_J:R Plastic Nitrate I Nitrite IT

1 - 1 LITER Amber Glass Total Organic Carbon (TOC) IT

1 - 1 LITER Plastic Total Dissolved Solids (TDS) IT

1 - 1 LITER Plastic Total Suspended Solids (TSS) IT

1 - 1 LITER Plastic Total Nitrogen (TKN) H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Alkalinity COOL 4°C IT


1 - 40ML Plastic Rad Screen COOL 4°C IT

1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,4°C PACE

1 - 250ML Glass Tritium PACE

SAMPLE ID'S RINSATE: ______ TRIP BLANK:------ FIElD BLANK: _____ _

RECORDED BY: OA CHECI<ED BY:--------------~-----: (SIGNATURE)

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SURFACE WATF:R QUALJTY SAMFUNG RECORD

FAO~CODE--~~~~~----. L-ocATION 10 ---!:NEW=-..!.PR~:t<OP:::.!.---LOG o.ATE _ ____::3A;...;;.;.J...:,ff.~/'i,_,..y __

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AU<AUNiiY

pH (mg/1 Cc C03 )

l st 2nd Jrd 8.90 AJA- NL a. so a . .:so 8.05 7.80 I

7.50 0 "-.J:A'\ 0 (6.S'Z.) 6.50 - -5.70 z.4S" 200

5.10 1'2.907<-.of 7:'7~ ( c_,.4)

<4-.80 2.16 lz84f4.73 I .-..so. Z89 r~r4s'i I 4.25 zqo{.of./R) -z.Set '11.'7.1.

4.00 za., 1-:r 67\ .l.C\~ (:J.4-i

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SAMPLE ID NUMBER: _N_S2_0_0_1 ---- DATE COLLECTED. (MMIDDIYY): _3~0...:..::~~!1,,__/ct...:...q...__ TIME: (HH:MM) --&../5=-/5~---MOUND SAMPLE NUMBER: MND16- ocro3 -0200

SAMPLING -

LOCATION CODE: MNQ16 DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

POINT CODE: SEEP2 DESCRIPTION: SEEP NUMBERkf' ~ ~/ilf SAMPLE - z_ .n/t:J ?/~o)iy

'MErnA .. ~ODE: 55 DESCRIPTION: Spring I Seep Water DEPTH Su£.4CL. TO ----=-M.;;,_~.a_ __

WEATHER: CiPt+ ' ovc.rco (b I @. a2. 0 E . . . ·FIELD OBSERVATIONS: :ltefk' 1'1kU~ ~ wdl ) tdg cflu., ; lou) e i' L,/MlA,.

SAMPLE TYPE:

GRAB § SPATIAL COMPOSITE TIME COMPOSITE QC TRIP BLANK QC RINSATE QC FIELD BLANK OTHER (SPECIFY)

FIELD MEASUREMENTS READING UNITS

IVk -7

'

~ 7 . SAMPLE COLLECTED: 8 NO

SAP SAMPLING PROCEDURE WAS FOLLOWED? @ NO FIELD CHANGE ORDER REFERENCE NO: --------- ~ IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:------------- ~

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CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES C-0-C #

VOLUME TYPE ANALYSIS fTYPE/VOl) lABORATORY

3- 40ML Glass Volatile Organics HCL pH<2, 4°C ::c /(p-1 IT I

2- 1 LITER Amber Glass Semi-Volatile Organics COOL 4°C IT '

2- 1 LITER Amber Glass Pesticides I PCBs COOL 4°C IT

1 - 1 LITER Plastic CLP Metals HN03 pH,2, 4°C IT


2- 1 LITER Amber Glass Explosives COOL 4°C IT

1 - 1 LITER Plastic Chloride COOL 4°C IT

1 - 1 LITER Plastic Fluoride COOL 4°C IT

1 - 1 LITER Plastic Sulfate COOL 4°C IT

1 - 1 LITER Plastic Nitrate I Nitrite H2S04 pH<2,4°C IT

1 - 1 LITER Amber Glass Total Organic Carbon (TOC) H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Dissolved Solids (TDS) COOL 4°C IT


1 - 1 LITER Plastic Total Nitrogen ITKN) H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus ITP) H2S04 pH< 2,4°C IT

'1 - 1 LITER Plastic Alkalinity COOL 4°C IT ~ 1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C IT "t>

1 - 40ML Plastic Rad Screen COOL 4°C ' IT ~ GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,4°C PACE ~

Glass Tritium COOL 4°C PACE

N5tt~t M5 Ql(/J ll SAMPLE ID'S RINSATE: f/S¢.l~l FIELD DUPLICATE:

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SURFACE WATER OUAL!i'Y SAMPUNG RECORD

-FAClUTY CODE 005 NP FAGC:: I OF' 1 --LOCATION ID

NEW PROP . ------~------ LOT CON'i'ROL NO __...NA-..._ __ _

5.JJJPL£ 10 NSZ.QOl - SAUPL.E i'Y?E--:;K:-· ----

. LOG DATE 3/Z.9/lJ4 ACCli.•tJ\.NC.E CODE _A __ _

ANAL.YTlCIL LAS CODE ___ ..;..!'1....;./t ____ _ LOGG8 CODE SAIC

I S.WPI.! itPES:

, - F1EI..O R - R!P'I.JC,ll't

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. SURFACE WATFR QUAUTY SAMP~NG RECORD .

pH I AI.KALlNITY GRAPH .. PACE _OF' -..

F'.J.OLm' COOE 005 NP

-l-ocATION 10 NE.W PROP ALJ<ALlNITf

lOG DATE: pH (mg/1 Co C03 )

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ERROR Ai +:50:1 Xt - X21 t st I 2nd Jr-c

8.90 17 X5 X 100=_%

8.so / 8..30 /

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1st = - 8.05 / ..

-- 7.80 v 2nd= - 7.50/

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pH CHECK AF'i'ER Tri'RATION - /5.10 I

7.00- <4-.80 I 4 • .50 I ..

4.00- - 4.25 II - -4.00 II ..

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SAMPLE ID NUMBER: NS2011 DATE COLLECTED (MMIDDNY): ~3+h-=zq.$-1--/q.&-..,tf __ _ ~,

MOUND SAMPLE NUMBER: MND16- 0103 - 1200

TIME: (HH:MM) ~JS~/_,5'-----

SAMPLING -

LOCATION CODE: _.Mu.~N..uP.._.1""'"6________ DESCRIPTION: _,M=O....,U....,N.....,D,._,O....,U.u5~N=EW....__._P......,R=O-&-JPE ..... R_._.TL-LY_....S,....E..,_E,_,PS..___ _____ _

POINT CODE: ___,S,...E...,E~P2..__________ DESCRIPTION: _....S...,E-EP._...._NU=M=B,..EoaJ..R.J4,t.._--t--.a__~~U--'ll~=...t-A~'f,___ _____ _

SAMPLE - Z- <lJtp jJ~oj-;'1

MEDIA CODE: 55 DESCRIPTION: ____,S...,p:.ud&,Qng,_.,/_..S"~~~'ee...,p._.W....,a....,te..,.r ________ DEPTH Ju.-fo.tt TO _l.J=.::A_....._ __ WEATHER: (Au. I {11UA tA¢/A J @, 3;? 'f FIELD OBSERVATIONS: tdlliu C/tllt. J,£1tJ.a. Sd!'(IJI/.N~. EIOicJ esl. 4> B. 0 LP~

SAMPLE TYPE:



NA ~ /

OTHER (SPECIFY) -------

SAMPLE COLLECTED: ® NO ~ l7

SAP SAMPLING PROCEDURE WAS FOLLOWED? ~ NO FIELD CHANGE ORDER REFERENCE NO: ---------

IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

RECORDED By: _n-=~A-..ao0~~h~4L-.;~..r....=~· ;..;:;_::::;....=:;__ __ _

~TIIRFl QA CHECKED BY: ___ - ..l£/~$1!!':!~~Z:;;~~::::;~--.:...__-

(SIGNATUREi -----.J

CONTAINER VOLUME

METHOD NAME AND NUMBER PRESERVATIVES ANALYSIS (TYPENOL)

.. 3 ~ 40ML Glass Volatile Organics HCL pH< 2, 4°C

2 - 1 LITER Amber Glass Semi-Volatile Organics

2 - 1 LITER Amber Glass Pesticides /.PCBs

1 - 1 LITER Plastic ClP Metals HN03 pH,2, 4°C

1 - 1 LITER Plastic Cyanide NaOH pH> 12,4°C

2 - 1 LITER Amber Glass Explosives

1 - 1 LITER Plastic Chloride

1 - 1 LITER Plastic Fluoride

1 - 1 LITER Plastic Sulfate

1 - 1· LITER Plastic Nitrate I Nitrite H2S04 pH< 2,4°C

1 - 1 LITER Amber Glass Total Organic Carbon (TOC) H2S04 pH<2,4°C

1 - 1 liTER Plastic Total Dissolved Solids (TOS) COOL 4°C

1 - 1 LITER Plastic Total Suspended Solids (TSS)

1 - 1 LITER Plastic Total Nitrogen (TKN) H2S04 pH<2,4°C

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH< 2,4°C

1 - 1 LITER Plastic Alkalinity

1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C

Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,4°C

Glass Tritium

SAMPLE tO'S RINSATE: NA TRIP BLANK: -£-li~~UifiC...&--

RECORDED BY: _ ___;~...14Jlld.o'iJ2QIU:Ia_.~~oc..-1)1«~-&-~:looll.M..vLr.w=:: . .=.::::::;....__ ____ _ (SIGNATURE)

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~rAClUil' CODE 005 NP PAGE I OF. --LOCATION 10· LOT CONi'ROL NO _NA ___ _

SAUPU: 10 N CS ZO If ~p~~E---K~·-------

.LOG DATE ACCE?TANCE CODE _A __ _

,.I.NAL."m~ L'S CODE ---.:~:.-fr _____ _ LO<NER CODE SAIC

SAMPUNG PSlOD: COMP~,~ --~'-'-'~0 ____ __ SAMPUNG MErriOO OATC: SENT __ 3..:../ t,;;..,;f:J.,.;.{'/;..:.4 __

COMM~ -----------------------------~~------------~-AMplf. tr dvplirA/E tel NS 'Z. ao I. f?umu.tc. .

P~ET'ER UEASUREJJENI'S:

POT'ENTW. OF HYDROGEN pH

SPECIFlC CONOUCT:ANCE Ec

REDOX POTENTlAL. Eh

TEMPERATURE Tl.(p

AU<AUNI'iY ( CaC~) . AU<

OlSSOLVED OXYGeN DO

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umho:s/cm Alit-" rnvoft.S AJ'A

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SURFACE WATF:R QU.AL!Tl' SAMPUNG RECORD • pH I AUW.INITY GRAPH

F~UTYCOOE--~~~~NP~-----L-ocATION 10 .....:.NEW.=...:PROP:.=:.---l.OG Cl.'.TE: __ _;3;;;...t/~3:;.:::tJ.,._/9.~..4..:..-.-..

ERROR AT <4-.So:f X1 X~ X2 )x 100=3.~ . <f1(P 1{~~'( 1st = :r.t'% 3. 3'-

Znd = llfr ":'

pH CHECX AF'iER TTTRA:noN

7.00 - t#'' 4.00 - __ 3_._?_,_

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pH

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pH (mg/1 Co CO:s)

1st 2nd 3rd 6.90 Nfl- ""' 6.so 1 6..30 8.05 I 7.60 I~ I

7.50 laf (¥..//,) ~ (7-.0f.) 6.50 !5"6 1214(,.4-'1 5.70 ZBo(S:.f.1 Z91 5.10 Z!l!:(~oz 3()$"( .£'(. v) <4-.80 AIR. -<4-.50 Z..'7'1 3()1 I <4-.25 3(}2. (4.Z~ ~/d (.f..tr. <4-.00 l?d~ (1.t;f 512 (~~ :) ' w~lvts ·li.s ( ) #£ pH 41/u~ · . m1t.f: JN.. UJJit AJti~ A&iel/bl .

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SAMPLE ID NUMBER: NSaOOl DATE COLLECTED (MMIDDNY): 3 ,/3o/'tlf= TIME: <HH:MM) O'loo MOUND SAMPLE NUMBER: MND16-03/l- 0200

SAMPLING -

LOCATION CODE: -IMIUJNI.DP£..11LX6 _______ _ DESCRIPTION: MOUNP OU5 NEW PROPERTY SEEPS

POINT CODE: --lS.t~:Ea.~=ELLP!o£..3 --------- DESCRIPTION: SEEP NUMBER 3

SAMPLE-

MEDIA CODE: 55 DESCRIPTION: Spring I Seep Water DEPTH $~ TO IJA WEATHER: ~ ~ 35 °£ FIELDO~SERVA~ INA/U 'SI. Mlllt'f IJ£[pa f/f?lt..R/111'. f!tJI.cJ ~sf . .o f,(J£P('f

SAMPLE TYPE:

GRAB § SPATIAL COMPOSITE TIME COMPOSITE QC TRIP BLANK



NA " --:7

OTHER (SPECIFY)

~ '7

---------~---------------------------------------~ ~

RECORDED By: ~ ~ (SIGNATURE)

QA CHECKED BY: __ :\4~;e/~z·~:i:~~==-~~~------(SIGNATUREl

\N oq_

CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES LABORATORY

VOLUME TYPE ANALYSIS . ITYPENOL) ·

3- 40ML Glass Volatile Organics HCL pH<2, 4°C IT

2- 1 LITER Amber Glass Semi-Volatile Organics COOL 4°C l~qafA I~B[P 32~ '12_ IT

2- 1 LITER Amber Glass Pesticides I PCBs COOL 4°C 3t5817l.. IT

1 - 1 LITER Plastic CLP Metals HN03 .pH,2, 4°C 31.1 'llsz. IT




1 - 1 LITER Plastic· Fluoride COOL 4°C IT

1 - 1 LITER Plastic Sulfate COOL 4°C IT


1 - 1 LITER Amber Glass Total Organic Carbon ITOC) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Total Dissolved Solids ITDS) COOL 4°C IT

1 - 1 LITER Plastic Total Suspended Solids ITSS) COOL 4°C IT

1 - 1 LITER Plastic Total Nitrogen ITKN) H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus ITP) H2S04 pH< 2,4°C IT


1 - 1 LITER Plastic Ammonia H2S04 pH<2 IT ~ 1 - 40ML Plastic Rad Screen COOL 4°C IT ~ -/tGAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,-tae- . PACE

1 - 250ML Glass Tritium COOL 4°C PACE ~

.. 1 I• t I

!JScft3¢2. 1:: {llf'NK: NSf}l{dl ... ~

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SAMPLE ID'S RINSATE: TRIP BLANK:

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S2U1PLE PARAHE'l'ER VAI.lJES

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. rACIUT'r' COOE

005 NP PAGE I OF j --LOCATION 10

NEW PROP LOT CON'l'ROL NO ta

S..WPL£ 10 1\JS :100 I ~PL£ Tt?E K·.

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AN.ALYT'IC\L I.).B COOE t:!." LOCGER COOE SAIC

SAMPUNG PER!OO: SiART o 9t:Jo COUPI.£iE: D~Af.

SAYPUNG METriOO GRAB DATE SENT 3/Ib/14

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SPEClFlC CONOUcr.111CE. Ee umhcsiem 1892..

REDOX FOTENT'IAl.. Eh mvclt:: Z4S:2.

TadPe:?.ATURE TMP •c '1.0

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OISSOLYEO OXYGEN 00 m9/l ft. :t

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. . -FAOLJT'r" cooe: 005 NP ... -L-ocATION 10 NEW' PROP .. ALKAUNfiY

,1..,00 DATE pH (mg/1 Ca COJ)

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pH CHECX Af'i"ER TTT'RA110N ..

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DATE COLL,ECTED (MMIDDIYY): ----- TIME: (HH:MM) _· ------

.. MOUND SAMPLE NUfVII:St::tr."-..'-..u.III.UoO'..uo<----__.11-M2auOO.._ __ _ .. '

SAMPLING -

LQCATION CODE: -UU..a-......_~------- DESCRIPTION: MOUND OUS NEW PROPERTY SEEPS

POINT CODE: ---liiiU:al=l~--~------ DESCRIPTION: SEEP NUMBER 3

SAMPLE -

MEDIA CODE: -¥111~--'"'"".., . ..,, ____ TO ___ _

WEATHER·.~-------------~~--~~-------------------------

'· FIELDOBSERVATIONS: __________ ~--------------------------

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SAMPLE TYPE:

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READING UNITS

OTHER (SPECIFY)

I I

SAMPLE COLLECTED: YES NO . .

• •· I

· SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ----------

IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:--------------

fl~~ .. ?RDED By: ---------· _. --:----(SIGNATURE)

QA CHECKED BY:--'--------------"-----(SIGNATURE)

I .I

·:· , CONT AlNER CONT AlNER METHOD NAME AND NUMBER PRESERVATIVES

VOLUME . TYPE ANAlYSIS (TYPENOl) AIR Bill# CONTAINER

·LABORATORY LOT II

C-0-C II

3 -· 40Ml Glass Volatile Organics IT

2 - 1 liTER Amber Gla IT

2- 1 liTER IT


1 - 1 LITER Plastic NaOH pH> 12,4°C IT

2 - 1 LITER Amber Glass Explosives IT


1 - 1 LITER Plastic Fluoride . I ~ IT

1 - 1 UTEA . Plastic s ; I IT


1 - 1 liTER Amber Glass Total Organic Carbon (TOC) IT

1 - 1 LITER Plastic Total Dissolved Solids (TOS) IT

1 - 1 liTER Plastic Total Suspended Solids (TSS) COOL4°C IT

1 - l.UTEA Plastic Total Nitrogen (TKN) H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH< 2,4°C IT



1 - 40Ml Plastic Rad Screen IT

1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH< 2,4°C PACE \

1 - 250ML Glass Tritium COOl4°C PACE

Ill 1.'1 SAMPLE 10' S RINSA TE: ----:-,:-. __ TRIP BLANK: -..,..------ FIELD BlANK: ------ FIELD DUPLICATE: ------..

~ECORDED BY: OA CHECKED BY:------------------(SIGNATURE) (SIGNATURE)

. •' tl . '·

. J.

. ·~

.J'

•

•

•

S»D?.LE PARAMETER vnm;s

SURFACE WATF:R OUAU1Y SAMPUNG RECORD

• CXlS NP F"AQUTY COOE. __ ,_;,_;;;.._ ______ _ FAG~ _OF_

LOC\TION 10 NEW PROP

LOT CON'i'ROL NO ....;,;;RA-._ __ _

s;..v.(Ft££0 SA.IJPL:: i'Y?E _ .... K~:-----

LOG OATE: ACa:?i'ANCE: COOE _A ___ _

ANALYnCAL L'B COOE ---------- l.OCGS CCOE

S)J.IFWNC P~!OO: Si)..Ri

GRAB

COMM~ ------------------------~---------------------

pH

Ec

e::n

T'MP

. AI..K

OISSOLYEO OXYGEN 00

SWPl£ TYPES:

1'- F1!J.D R-~

IC - IOIOWI'I J. - .w::ID SUI«

s.u. umhc:/cm

mvclt.:

•c

m9/f

m9/l

I r i I

s.wFUHC: J.IE'l'HOCS.:

C - CR.ta SP - SU8WtRSI8t.t PVW ptt - PO!:I$'CIUC PWP 0 - <mfER (SP!Cf t) · .

5£fp ,, 4~ · .

• . . SURF' ACE WATF:R QUALitY SAMPUNG RECORD

•

•

• pH I ALKALlNITY GRAPH

.. F~UTYCOQE--~OCS~NP~------L-ocATION 10 NEW PROP

LOG DATE 3{3tJ('f4

ERROR Ai +.SO!/

1st = Z.t..:~%

xs x 1 oo::Z.'; X1 - X21

· 2tlcr- lift %

pH CHECK A.F'i"ER Tl'i'RA}TON

7.oo· - -:o:-..... t:.-·--' ..... r-4.oo - _._1_. 1_1:_ .. _

SIMPLE m ---.:...::N..-.S~4.,:;...p..,::;;..~.;_l _

·,., 0 ..... u

.•'

g (J

.::::::. ell

E -~ z ~ ~

2

I I I I I

I I I I

I I I I I I

I

I I I I I

I I I I

3

I

'

' I I I I I I I

I

I I I I

I I I I I I

-4- 5

~ ICI.DCZI om. fat DCna' IICn:l ..... ~-~ .

:·.

' I I I I I

I

I I I I I

6

I I I

I I I I I

7

pH

PACE _L_ OF _j_

AU<AUNITY pH· (mg/1 Ca COl)

1st 2nd .3rc 8.90 loll All 8.60 8..30 8.05 7.80 7.50 0 (','If 07'?-.03 6.50 IJ'2IJ 7t:.. '3 n /dt'J/'·" :S) . 5.70 '2./I'J ~<:t. :) Z.OS' ( s:. ~,.) 5.10 Z3'Df4.9' r) AI~

-+.80 .z~z.· zu.l4. ~) l 4.50 Z3t/-- Z2"lf.tf..« Z) 4.2.5 Zs'-f-1~ lr4) ztot~

·'' J 4.00 Z!t f;f.tJ It) Z3L 7 .9.J> VALUi1 IIJ ( ) AU. pH iF . . fttt ~ft plf- kiM NtJt /t'U.D!'iJ/JSI:

I 1 r 1 ·TT I I If I I I I

' I I I 1 r I I I I II

I II T I I I I I : I· I

I I I I I I I I I

I I -I I I I f 11 I I I I I ., I i I I I t l

. I I I 11'

I I i I I I I I I I I I

I I I I I I I I I I I I I I I I I t· I I J I I I I I I I I

a 9 10 11 12

I I ~. I

i!

--•--...-..~ ..... 1!11111111!111--·-~ ~~-···. -----~:7:·· ·::. __ ·;;:;.; __ -;.;.:..·.·....;::;,...;....:.:.._;_;_;;:::;' == . =· • J::.,:.;:..: :! .... '.'!. ··.:.:.: :.. 7 I

r

SAMPLE ID NUMBER: NS4001 DATE COLLECTED (MMJDDNY): 3/JO/f4 J I

TIME: (HH:MM) .....:/~0~. _·o...;:o:;._ __ _

MOUND SAMPLE NUMBER: MND16- d4d8. 0200

SAMPLING-

LOCATION CODE: _.M.DJN:.uDc..~l:.x6________ DESCRIPTION: MOUND OUS NEW PROPERTY SEEPS

POINT CODE: SEEP4 DESCRIPTION: SEEP NUMBER 4

SAMPLE-

MEDIA CODE: 55 DESCRIPTION: Spring J'Seep Water DEPTH 5Uilt= TO --=-N~/1:...__ __

WEATHER: 5vNN'I ~I 1/JWLNitffNf clouds, 4o-F~ st. batzE FIELD OBSERVATIONS: AJtt/g VEtz.y McJity /,t(iJa ~1/N,. ~lew t. )/. 110 I. 0 lPM

SAMPLE TYPE: .


FIELD MEASUREMENTS BEADING UNITS

/'JA

OTHER (SPECIFY)

SAMPLE COLLECTED: <f§) NO ' .

SAP SAMPLING PROCEDURE WAS FOLLOWED? @ NO FIELD CHANGE ORDER REFERENCE NO: --------


RECORDED By: --"""'~'(hti~Q~:=§~?.t;::;._~:._. .. ---(SIGNATURE)

OA CHECKED BY: ~~ (S·u3NATURE}

. I

:&.;.·!~ ~:C!i ·.· .•

~ I I I 'l I I

, • •I' I I

CONTAINER CONTAINER METHOD NAME' AND NUMBER PRESERVATIVES C-0-C II

VOLUME TYPE ANALYSIS (TYPENOL)

3- 40ML Glass Volatile Organics HCL pH<2, 4°C II(,- 2., 2- 1 LITER Amber Glass Semi-Volatile Organics COOL 4°C

2- 1 LITER Amber Glass Pesticides I PCBs ·COOL 4°C

1 - 1 LITER Plastic CLP Metals :HN03 pH,2, 4°C

1 - 1''LITER Plastic· Cyanide . NaOH pH> 12,4°C

2- 1 LITER Amber Glass Explosives ,COOL 4°C

1 - 1 LITER Plastic Chloride COOL 4°C

1 - 1 L.ITER Plastic Fluoride COOL 4°C

1 - 1 LITER Plastic Sulfate COOL 4°C

1 - 1 LITER Plastic Nitrate I Nitrite H2S04 pH <.2,4°C

1 - 1 LITER Amber Glass Total Organic Carbon ITOC) H2S04 pH< 2,4°C

1 - 1 LITER Plastic Total Dissolved Soljds (TDS) COOL 4°C

1 - 1 LITER Plastic Total Suspended Solids ITSS) COOL 4°C

1 - 1 LITER Plastic Total Nitrogen ITKN) H2S04 pH< 2,4°C

1 - 1 LITER Plastic Total Phosphorus ITP) H2S04 pH< 2,4°C

1 - 1 LITER Plastic Alkalinity COOL 4°C

1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C ·

1- 40ML Plastic Rad Screen COOL 4°C

GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH<2.~

1 - 260ML Glass COOL 4°C

RINSATE: 9 NA . TRIP BLANK: ~~ f.)~~ I¢/ SAMPLE ID'S N.S,..31111.. ·~ANK: QA~EC ED BY: RECORDEDBY: ~~

(SIGNATURE)

LABORATORY

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

PACE

+ PACE

~ PARAMETER VM.l'J!S SURFACE WATER OUALli'Y SAMPUNG RECORD

005 NP PAGE ___!_ OF' _

LOC\TION 10 LOT CON'i'ROL NO _!&......._ __ _

SA.MPLE 10 SA.MPU: iYPE: _ ... K,_· ----

. LOG OATE: ACCE.-•J\.NCE: COOE _A __ _

J.NAL.'r11CA.L LAB cooe: ___ I.I;.;.A _____ _ LOGGER COOE SAIC

SA.MPUNG PS!OO: Si'ARi too4 COMPt..::'i"E _..;..;/ O;;;...'S...:'3:::;._· ~-

SAMPUNG MErtiOO GRAB OATE: SOO '3/3() /74

COMMENTS 1DH J'bwtl 7:.0 ,lit• f.Dij pH t9t¢ t/..tJ lH= 4.0'5j

stope = '~- 1=

PN't'J.(E!ER M£ASURalENT'S: .

POTE:NTTAL OF' HYDROGEN pH s.u. ~.91

SPECIFIC CONDUCTANCE. Ec · vmhc:s/cm t, l&fl

REDOX PO'T'ENTlAl Eh mvcit: St=!--1

TE:.(PERATURE NP ·c 8-.4

AIJ<ALlNCTY (CGC0:s) . . AU< mg/1 Z"$4-

OlSSOLYEO OXYGEN 00 mg/f 1~./

.&e::ZP'I'N«.:":t c:::::a:s: ~ It~~ H-f«7r~

s.wPU: 1"t'PES:

r - Fl!l.D R - ltEf'UC:ATt IC - ICHCWH A - ,&CD St.N«

SP-~~

o - ana (SP!CF'I

.. (· ,.·~ . . ·-.:..'71 s

. suRFACE WArrR auAL.Itl' SAMPUNG RECORD :: .... ' .

pH I AUW.INITY GRAPH ~.· t

.. : --~ .. ' ...

·. . . .• . . ~· ..

F'..aUTY CODE aJ5 NP

-.. LOCATION 10 NEW PROP

LOG DATE: pH

X1 E:!ROR AT ~.50:1 - X21 X5 X 100=___%

8.90 8.60

.,.

·::(-! H·;·

r•···:: "'' .,: .

>t> . . .

·mr. ~-.. · •.;-' ,,wz .$;.

I

•

.

.

.....

1st = ... .....

2nd= .,. ,. .

pH CHECK AFn:R TITRATION

7.00-..

o4..00-

SAMPLE m

. .. I

-,., 0 I I I I ... u c I I u I ,_ II Ct II E -- II

~ II

I %

~ il

II' ...J v I <

I I

2. .3 + s

·Z:~;;.. . ·• ~ ......_ OIZL PC1t Dmft' IICftl "'liiiS ~ Qllll)· . . - ..

8 • .30 8.05 7.80 7.50 6.50 5.70 5. to .o4-.80

. .... so .. o4..2S

o4..0o /I

j{P•/ I II I

Ill v

I I I I I I

I I I I

J/ I

I I I I

I I I

6 7 8

pH

PAGE _oF"_

ALKAUNiiY (mg/1 Co ~O:s)

1st 2nd 3t"d

/ v .

. . I

/ /

. / ./

/ I / I

/ /

.. . .. I

.. . -· -. .

I I • I I I 11

I I

... . ... I I

I I I I l I I

I I

I Ill ..

'

.

I ,. I

I I I I I I

9 10 11 12 . .

...

\~-, . r. ~ ... f •••••

~ .· ·: --~ '·l

SAMPLE 10 NUMBER: _N_S4_0_1_1 ---- DATE COLLECTED (~~DIYY): ------ TIME: (HH:MM) ------

MOU~D SAMPLE NUMBER: MND16- - 1200

SAMPLING-

_.M_N ..... D ..... luo6.__________ DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

-=::lliil;Ji~--------- DESCRIPTION: SEEP NUMBER 4

SAMPLE -

MEDIA CODE: ...~5"""5~-----' Spring I Seep Water DEPTH ____ TO ___ _

WEATHER=-----------~~-~-----------------------------. . .

SAMPLE TYPE:

..

GRAB TIME COMPOSITE QC RINSATE OTHER (SPECIFY)

SAMPLE COLLECTED:

§ SPATIAL COMPOSITE QC TRIP BLANK QC FIELD BLANK

YES. NO

READING UNITS

. SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------


R~CORD~D By: ----. _-. __ .-. -. _-, -._-_,--------:--l~lnM 1\ TIIQJ:\

QA CHECKED BY:-------------------

METHOD NAME AND NUMBER PRESERVATIVES C-0-C # AIR BILL/I

CONTAINER LABORATORY

ANALYSIS . (TYPENOl) LOT II

3- 40ML Volatile Organics HCL pH<2, 4°C IT

2- 1 LITER COOL 4°C IT

2- 1 LITER COOL 4°C IT

1 - 1 LITER Plastic HN03 pH,2, 4°C IT

1 - 1 LITER Plastic N~OH' pH> 12,4°C IT

2- 1 LITER Amber Glass Explosives IT

1 - 1 LITER· Plastic Chloride IT


1 - 1 LITER Plastic Sulfat~ IT


1 - 1 LITER Amber Glass Total Organic Carbon (TOC) IT

1 - 1 LITER Plastic Total Dissolved Solids HDS) IT

1 - 1 LITER Plastic Total Suspended Solids (TSSJ COOL 4°C IT

1 - 1 liTER Plastic Total Nitrogen (TKN) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Total Phosphorus (TPI H2S04 pH< 2,4°C IT


1 - 1 LITER Plastic Ammonia H2S04 pH<2,4°C IT

1.- 40ML Plastic Rad Screen COOL 4°C IT lJ -1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH<2,4°C PACE I

1 - 260ML Glass Tritium COOl4°C PACE

II II I ''01

. SAMPLE ID'S fUNSATE: TRIP BLANK: FIELD BLANK: FIELD DUPLICATE: • .! • ·' •.•\:

RECORDED BY: QA CHECKED BY:

I I" I (SIGNATURE) (SIGNATURE)

II I' I

.. ,., .. l . .-; ......

- ... .,..._. I ·-s..··. ~~~:,,

•. · :~:;~~:j'

·.· I !

.I ,.--

Pt I l .;

' . ·' . I I

I ;

I ..

i

----------------. --.

SAMPLE PABAMETER VAlDES

SURFACE WATF:.?. OUAUi'Y SAMPUNG RECORD

~rACtt..m' cooe:

LOCATION 10

SA.UPU: 10

. LOG DATI:

005 NP

NEW PROP

FlACC: _OF'

LOT CONTROL NO _HI.;;,;;;;;:. __

SAUFLE iYFE-..:.K:::..·---

ACa:FiANCE COOE _A __

~'r11CAL. L!B COOE ---------- t.OGGS ecce: _..;;;SJ.;;;;'y;;;;c;;.__

SAMPUNG PE:R!OO: COMPt£,~ --------

SAMPUNG MEi'nOO DATE SEN'i ---------

COMM~ ---------------r'-------------------7 I

I

FlOTEN'l"W. OF' HYDROGEN pH s.u. Ec umho:s/c:m

Eh mvoft:l

NF •c

. AU< mq/1

DO mq/!

s.aJ.rPt.£ irPES: SAUPUNC llEn-fOOS:

r-raa R-~ C - CRM SJII - StJIJLitRSZ8l

IC - ICHOWH J. - .W::O 8UIOC ~ - p~ 11tNP 0 -<rna (SPEC .

.. · ~ .

SURFACE WATF:?.. QUALITY SAMPUNG RECORD • pH I ALKALINITY GRAPH ·

005 NP . FACttJ'TY cooe: _.;;.;;..;.. ___ _ .. L-ocATION 10 ~NEW=:.....;.PR=KOP=---LOG OATE: ___ 3:.....;/3;.,..0.,._/lf..._i-_._

ERROR Ai •• 50:1 Xl X~ X21x 100..9~

-·1st = 6.51%

2nd= Nit ~ .

pH CHECX AFTER TTT'RA:tiON

.. 7 .. oo· - =1-.. tJY 4.00- .. 4,~,3

. S».~PLE m N S 5 {!~ ,·

-- ....

-1"'1

0 . ~ u cr u

~ E -·

I

I

2.

I •

I - . I I I

3 5

-

I

I

6

I I

7

pH

pH

8.90 8.60 8 . .30 8.05 7.80. 7.50 6.50 5.70 5.10

·4.80 4.50 4..25 4.00

I

I I

a

PACC:: __.I_ OF' __j_

AL.KAUNI"iY · --(mg/1 Co C03)

1st 2nd .:Srd

"""" -""""""- 1JA

. ' O(:i_M) OLl.,,) too (~.zA) flo{ t,.4:M ~) t5tJ rs:~ ') /,2 /rtJ(S.M Nit I

it '.1-4{4.1-I:. 1~(4.?1 1'1s-14.UJ /1/,(4-.IJ'' ) 1=1':1- Rt~Z'f -/flf

.. IIIIJ ( 4-.D+

' I ' 1 I u I I

I I I I I I I I I I I I : I·•

I I I I I I

I I ! . r.

I

I I j_

9 10 11 12.

·-··· ' \ • ·-.~·.·;~ ... ··-""""······-···· ... "1

SAMPLE ID NUMBER: _N_Ss_o_o1 ___ _ DATE COLLECTED {MMIDDNY): TIME: (HH:MM) ___,/.._Q_4_b __ MOUND SAMPLE NUMBER: MND16- 0" I I - 0200

SAMPLING •

LOCATION CODE: _.Mw.~N:..uDC-A1'Jol.6 _______ _ DESCRIPTION: MOUND OUS NEW PROPERTY SEEPS '

POINT CODE: ___,S...,.E ..... E .... Px..S ________ _ DESCRIPTION: SEEP NUMBER 5

SAMPLE • !

MEDIA CODE: ...Jo5w.5 ___ ,DESCRIPTION: Spring I Seep Water DEPTH 5t1P:. WEATHER: SV/!N. W/ tN/fiMiffiiAII Clg;ds 4ot'F

FIELD OBSERVATIONS: (N{tfu.. S'/. MtJLtv /JefrJu. Sttlff/I'Nt PIMJ Esf. cu t. S" l.Pt'f

SAMPLE TYPE:

GRAB § SPATIAL COMPOSITE TIME COMPOSITE QC TRIP BLANK


FIELD MEASUREMENTS BEADING

NR -"" ....

, OTHER (SPECIFY) -------

:

'

UNITS

SAMPLE COLLECTED: ... @.. . ~0 SAP SAMPLING PRO:CE~URE WAS FOLLOWED? @:) NO FIELD CHANGE ORDER REFERENCE NO: -------- ~


-----------------------------~~------------------------------------------------------------~ .I

OA CHECKED. BY: __ W-fl-iiUGdh:;::ac:;.;;;...~ ............ =tt.=·=-==-------

v, I -ll., I

-p!siGNATURE)

r '_.,_iffillrrr ~c ~~~-;; ... , ........ ~., ,~Mt ntt-luiR · · . rrn::;: . · . . . ,. r .. .,;~ 0::'!f'-i'>"':(;~··;;; "''Co<';~J.~'0;,·,,.-<1. J'f..if;~;,,,;n

CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES C-0-C II AIR BILL/I CONTAINER

LABORATORY VOLUME TYPE ANAlYSIS ITYPENOl) LOT II .

3- 40Ml Glass Volatile Organics HCl pH< 2, 4°C :T/{p-2 !qi~P9 ~fi/CIB" '3'J..I,rl¢q 3 IT

2- 1 LITER Amber Glass Semi-Volatile Organics COOl4°C 3 It¢(.) 1 ;I,. IT

2- 1 LITER Amber Glass Pesticides I PCBs COOl4°C 3fg~~e;L IT I:

1 - 1 LITER Plastic ClP Metals HN03 pH,2, 4°C .3 a-1 Ll(65~ IT

I : 1 - 1 LITER Plastic Cyanide NaOH pH>12,4°C .• .3 ;z_ I'· I¢ 5'a__ IT

2- 1 LITER Amber Glass Explosives ' ..,..

3 3 ;1. I (»J;t COOl4°C IT

1 - 1 LrTER Plastic Chloride COOL4°C Lf0PJ ~q;L IT

1 - 1 LITER Plastic Fluoride C00l4°C /..frj I tf¢q~ IT

1 - 1 LITER Plastic Sulfate COOl4°C HrJJ40~~ IT

1 - 1 LITER Plastic Nitrate I Nitrite · H2S04 pH<2,4°C 3l) ~·¢5;z_ IT

1 - 1 LITER Amber Glass Total Organic Catbon (TOC) H2S04 pH< 2,4°C 33;21¢01~ IT

1 - 1 LITER Plastic Total Dissolved Solids (TDS) COOl4°C 3 ;l_JlJ¢5~ IT

1 - 1 LITER Plastic Total Suspended Solids (TSS) COOl4°C l.l~ I il ~'} ·?-,. IT

1 - 1 LITER Plastic Total Nitrogen (TKN) H2S04 pH< 2,4°C ... '-1 ¢ I '-1 (6q ;L IT

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH< 2,4°C .:: . 3 J.-J4t/'-5=L IT

1 - 1 LITER Plastic Alkalinity C00l4°C .. .3 ;Ljl-f (J~ .;L IT

1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C . 't(JI Y(41:L IT t 1- 40Ml Plastic Rad Screen COOl4°C "' ~ ~ .. 3att70'/3 IT t

~~·-~GAl Plastic Pu, Th,U,Ac,Ra,Sr ,Am,Gamma HN03 pH< 2,4A& 1'/lo--2.. 'llfoq~JtJ'IZ NA PACE ~

1 - 260Ml Glass Tritium COOl4°C 4 { 1\JA PACE ~

' SAMPLEIP'S RINSATE: NA TRIPPLANK: t!Sp!- fiELPPI!ANK: NS¢1¢1 =-=~:~::NA ~ECORD~DBY: ~~~·~~-~-~~-ft~~~~~~~·~~~~~~~~ OACHECKEDBY:~~~~~-~~~~~~~~~~~~~~~

~r (SIGNATURE)_. (SIGNATURE) ·--

-·. - ~"";· . . ' . :~

.- : i ~

·r1~ 1 ~·~, . ! ~

SAMPLE PARAMETER VALDES

SURFACE WATER OUAUi"Y SAMPUNG RECORD

OC5 NP FACC: _j_ OF ....:._

LOCATION 10 NEH PROP

LOT CONTROL NO _..NA=----

S..WP~ !D ~p~~E--~K_..· ______ _

-LOG DATE ACCE.=TANCS: CODE _A __ _

ANAL.YnCAL. LAB CODE -----:.N.;.;.P. ______ _ LOGGER CODE SAIC

SAMPUNG PERIOD:

SAMPUNG MEiriOD

SiARi

GRAB

/04S COMPL.::.i"E: II 1 4 . DATe: Sc:Ni 3/3atf~

COMMENTS p#- ~ll?Nd·?-.o ,H= ;r.oz..j fH ,Jmt¢. 4.o 1pll= 5. 'f'f..

5/opl. = 1~? •

P~e:rER M~RE).{EHTS:

POl'EN'l'lAL OF HYDROGEN pH s.u. fl. =l-3 S?EClflC CONDUCTANCE. Ec umhe:s/c:m 583

REOOXPOTEN'llAL. Eh mvelt:s .35"3 .. :r TE:MPERATURE TUP •c Cf.4

Al..KAUNrrt' (CeC~) . AU< m9/l 115'

DISSOLVED OXYGEN DO m9/l /1. I

.IC:E:l"'''NCE c:a:s: ~ R~~H-H:n'~

SAJ,IPl£ rtP~ S.WPUNG METHODS:

,. - FIELD It - R£PUC(l'E c- eR.A8 .

IC - ICNCWH A - .u:::D SUI« pp - P'DtiSI').UC I'UUP .

. ...

51-·-

• . SURFACE WATF:R QUALm' SAMPUNG RECORD . pH I AI.lW.lNI'1'Y GRAPH .. .. .. · . PAGE _or:-_ -. . . ..

FJ\OUT"'" CODE 005 NP. . LOCATION 10 NEW PROP AU<AUNITY

LOG OATE pH (mg/1 Ca CO:s)

X1 - X21

I st 2nd Yd ERROR AT .o!-.50:

X5 X 100=_;t 8.90 / a. so /

8.30 " .

/

1st = 8.05 / ..

% 7.80 /

2nd= ·- 7.50 / .... . / 6.50 ..

5.70 / pH CHECK AFTER 11TRATION 5.10 / I 7.oo· • "".ao

- 4.SQI' j

4.00- - -4-..tS . . A.oo I' . .

• SAMPLE m o/ . . . . . I I • i 1 -

I I I I 1 I I I

I I I I _ ..... -.., I ~ I I I .

0 I I I I II I I I I I I I ! I· I .. u I I I I I I I I I 0

u I I I I I

' v ' Ol

E -~ I .. %

~ :«! I

I I I I I I I I I I I I I I I

2 3 + 5 s 7 a 9 10 11 12

pH

•

!:it,;;,-.~~·;~ .. ,. " ·. .. ' ,;;.;;-; .: ~-;:;;_~>;:;,•:!::~:"-3-:E:§. ., '":'..'::..-':-~.., l ; I

SAMPLE 10 NUMBER: _N_Ss_0_1_1 ---- DATE COLLECTED (MMIDDIYY): ____ _ TIME: (HH:MM) ------

MOUND SAMPLE NUMBER: UJ· Mw.;N~~:~~D:..&J.16.._-_· --·--1u.2.x:OO"-----

SAMPLING-

1 LOCATION CODE:. _.MmN..uP.u1.x.6________ DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

POINT CODE: SEEPS ' llESCRIPTION: ~Su.E.a..E~-.P .uNJ.LUMIXUllBEiai.R.L.I5~t...-___________ _

SAMPLE -t : I" 1,'

MEDIA CODE: 55 DESCRIPTION: Spring I Seep Water DEPTH ____ TO...:....· ___ _

WEAl~ ·

FIELDOBSERV~--. . ~ '-----------~ I •

----------SAt:!fLE TYPE: . . FIELD MEASlJAEMEf:ITS READING UNITS GRAB · § SPATIALCOMPDSITE .. ----- TIME COMPOSITE QC TRIP. BLANK ----- QC RINSATE QC FIELD BLANK ·~ ~ OTHER (SPECIFY) - ..

SAMPLE COLLECTED: YES NO !.1

SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------... IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

RECORDED By: ---------------:--- QA CHECKED BY:----------------·. (SIGNATURE) (SIGNATURE)

.... _.;.···

CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES C-0-C # AIR BILL#


VOLUME' .

TYPE ANALYSIS ITYPENOL) LOT#

3- 40ML Glass Volatile Organics · HCL pH<2, 4°C IT

2- 1 LITER Amber Glass Semi-Volatile Organics COOL4°C IT

2 ·- 1 LITER Amber Glas·s COOL 4°C IT

1 - 1 LITE;R Plastic HN03 pH,2, 4°C IT

1,- 1 LITER Plastic IT

2- 1 LITE~ Amber Glass Explosives IT



1 - 1 LITER . Plastic Sulfate COOL4°C IT


1 - 1 LITER Amber Glass Total Organic Carbon (TOC) H2S04 pH<2,4°C IT

1 - 1 LITER Plastic Total Dissolved Solids (TDS) COOL4°C IT

1 - 1 Plastic Total Suspended Solids (TSS) COOL4°C IT


1 - 1 LITER Plastic Total Phosphorus ITP) H2S04 pH<2,4°C IT



1 - 40ML Plastic Rad Screen COOL 4°C IT v

1 - 2 GAL Plastic Pu,Th,U Ac,Ra,Sr,Am,Gamma · HN03 pH< 2,4°C PACE -1':

1 - 250ML Glass Tritium COOL4°C PACE

'' RINSATE: TRIP BLANK: FIELD BLANK: FIELD DUPLICATE:

1'

SAMPLE ID'S

RECORDED BY: OA CHECKED BY: (SIGNATURE) (SIGNATURE) ; I

a -qr !'" . f · ~'~---t .. ,;; .. ~_ ............... w~ ...... --.·:· -·-·-·~•.,......._ .. .

lf-=. TIT·

~ ~· " ~ .. .. r ·,· .. '

SIMPLE PARAME'l'ER V7U.DES

SURFACE WATER auALirY SAMPUNG RECORD

CXJS NP PACC: _oF_

LOC\TIOH 10 LOT CON'T'ROL NO· _NA---. __ _

$.1l~Pt.£ 10 ~F~~E---K-·------

. LOG OAi'E ACCEO.-t;l.NCE: COO£ _A __ _

,.i.J'W..YnCAL LAB cooe: ---------------- r.ks cooe: SArc /

$.1l~PUHG PE?.!OO: Si»rr -------- / COMPL£::. ---------

s..v-lFUHG METriOO .....;GRAB~;;;...--------'-~ OATC: SOO -------/

COMM~ ---------------------~~-----------------------/

P.&.P.AUErcR J.(E'StJREJ.lEMl'S:

POTEN'l'TAL. OF HYDROGEN

S?E~C CONDUCTANCE

REDOX Porc:mtAL..

'TSIPE!tl.nJRE

AU<AUNrrt: (C4C0,)

SWPt.£ T'I1'ES:

r-~UD R-~

IC - ICHOWH A - M::D SUI«

""-'P . AU(

I

I I

s.u. umhc:s/c:m

mq/1

00 : mq/1

S.WPUNC J.lEli-fOCS: c -<:R.Ia §'-~p

, - P£R~St~UC I'UVJ' o - ana (SP!CFT'

•

• ~

>

. .

...

..

..

' .. I

. SURFACE WATER QUALJi'Y SAMPUNG RECORD . pa I .Al:.RALINri'Y GRAm

. . .. .. - - · . ·. PACE: _L OF"_!__ . . ·- ..

FACLiiY cooe: 005 NP - -' AU<AUNiiY L-ocATION 10 Naf PROP

LOG OA.TE 3t50('14 pH (mg/1 Co C03 )

- 1st 2nd Jrd I X1 - X21 8.90 NA ....... AlA ER!lOR Ai +.SO: . xs X 100=Jjf_,:

8.60 I 8 • .:30 -

8.05 f ..

. 1st.= t.11 %: - 7.80 ' -2nd= IJ- .. 7.50 l~(;t.z.o ! " (?. 'J?:'

"" . 5.S6 1Jijj({,-4&t fi,O •· .

ZDS(5;~ ~) 2.()0 (! ~'%.) - S.70 ~H CHECK AFTER Tl'l"RA:rtON S.10 Nil.. ~~~ . -

ZJ/14·"11 2/)ft, ( +· ~J 7.00- 1fo+ +.80 I + Z/3 7(), _(_ "~-· 'S [3_ I 4.50

... 4.00- 4 .. o+ - +.25 'Z/'5{ -1-ZI. J 211 {t(-.4 ~)

...... 4.00 'ZI?-r ~IJ1. ) 2./~ I

• SIMPLE m N s· (,.(I f1J I VAUlt~ /Aj L") AU. pH 4JU~· . . ftrl.ttl pi ··wJfllfltJt JldiliVttl . .

. I I • I

I .. I -·· -···. - t ..,

0 I I I I l _l I ... u l c .. · u I I I I ..

' I ' C't I I E I ··-~ I

z

~-~

I I I I I I I I t· I I I I I I I I I I

2. 3 + s 5 ·7 a 9 10 11 12.

. pH

-

.m '""'"··· .. • . . .· ·. -.·.· __ -.-.,.·- .. ·. .·.·.:·_!".! ....... ;""'•~ :..:.·.:::;,.~, .. ::,.-.. ~_-_._:-"·' __ ·_ ., ' . . • .• --=r::.-~3 ~--·· .. ·~T~_--:- . .f!~""'!~~~~:~-~:.t'::~:~-~0-~~-~-~~~~-~-~-~-~-~~-~~-~-~,";.~~··-~ ~::;__~ !.:.; • • • • • •• • •••. -··-· I -:····- _,.,. •• • -··----·-. J":-'

. ; I :

SAMPLE ID NUMBER: NSS001 DATE COLLECTED (MMJDDNY): J ~~() /94 TIME: (HH:MM) // Z" MOUND SAMPLE NUMBER: MND16· I/ I 3 · 0200

SAMPLING •

LOCATION CODE: _.MUJNcuD'-J1...,.6 _______ _ DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

POINT CODE: __..!SIII..LE....,E..._P6~-------- DESCRIPTION: SEEP NUMBER 6

SAMPtE •

· MEDIA CODE: 55 DESCRIPTION: Spring I Seep Water DEPTH S tJitF TO __,Mf....;;..:.;..._~

WEATHER: 40"E !~ "::· ~~c-:1 . FIELD OBSERVATIONS: · ;:~ c:;= t ;;;;4/.1~ FIIJid t'Sf 6.J Z. 0 LPII1

SAMPLE TYPE:

GRAB § SPATIAL COMPOSITE FIELD MEASUREMENTS READING UNITS

TIME COMPOSITE QC TRIP BLANK ~ ::::» Nlr -

QC RINSATE QC FIELD BLANK OTHER (SPECIFY) I

SAMPLE COLLECTED: § NO v SAP SAMPLING PROCEDURE WAS FOLLOWED? @ NO FIELD CHANGE ORDER RE¢ERENCE NO: --------


. RECORDED By: __ V.:!_.9.4#~u7=?::s;...=s:;.,._._ _____ _ (SIGNATURE) 9./J..u~ OA CHECKED BY: --.Y:..P."IriBUII!I<Ioa.c..::I-=~-~--=-;..;;..;_;==~----

(SIGNA TURE)

I

LABORATORY CONTAINER METHOD NAME AND NUMBER PRESERVATIVES

TYPE ANALYSIS (TYPENOL)

Glass Volatile Organics HCL pH< 2, 4°C IT

Amber Glass Semi-Volatile Organics COOL 4°C IT I

1 LITER Amber Glass Pesticides I PCBs

Plastic CLP Metals

- 1 LITER Plastic Cyanide

- 1 LITER Amber Glass Explosives

Plastic Chloride

- 1 LITER Plastic Fluoride


1 - 1 LITER Plastic Nitrate I Nitrite

1 - 1 LITER Amber Glass Total Organic Carbon (TOC)

1 - 1 LITER Plastic Total Dissolved Solids (lOS)


1 - 1 LITER Plastic Total Nitrogen (TKN)

1 - 1 LITER Plastic Total Phosphorus (TP)

'1 - 1 LITER Plastic Alkalinity

1 - 1 LITER Plastic H2S04 pH< 2,4°C IT Ml Ammonia ~---4-----+------------+-------+-+---~~--~~~~----~~

1 - 40ML Plastic Rad Screen COOL 4°C IT "

SAMPLE ID'S RINSATE: NA TRIP BLANK: NSai3.· 17(2_ FIELD BLANK: NS~I¢1 FJELD DUPLICATE: NA ~ECORDEDBY: ~~-~~~~~~~~~~~~·~~·~~~~-~~ QACHECKEDBY:~~~~~-~~~L~~~~~~=========~ I (SIGNATURE) (SIGNATU~

. t:.. .. -~ .....

I ; . . ..

SAMPLE PARAMETER v:u.trEs

SURFACE WATER QUALify SAMPUNG RECORD

-F'ACli..IT'r' CODE 005 NP

LOCATION ID . NEH" PROP

SAI.IPL:: !D NS ~(J~I

·.LOG DATE: ~/34/94 I

.4J'W..YT1CAL LlJ3 CODE ~~~

· SAMPUNG PERIOD: START

SAMPUNG MEitiOD GRAB

1/Zt.

UITCO~OLNO-B~-----

SAMPL:: T't'PE-..::.::K-.· ----

ACCE..-t~CS: CODE_A ___ _

LOGGE:t CODE _.;;;;;SU!;.;;;;;;;.;;;C;.._ __

COMPL£: c. __ I Z.._6_L_· --

COMMENTS {ffl f.IJwd jZ. 0 pi= ;.. 00 ,: /1/1 SfAftlt:/ .f.tJ ,eH= 4. 13) r!tpl ~ 9?-.. t,

PARAUEI'ER t.CE'SURalEHTS:

POTENTW.. OF HYDROGEN pH s.u. 'lot SPEClflC CONOUcrANCS: Ec umho:s/c:m 5=12...

REDOX PO'T!N'TlAL Eh mvoft:s Z:'f/. 5"

TE:MPERATURE TMP •c =/- .• 4 .

Al.KAUNrrt' (CaCO:,) . AL..K mg/1 213

DISSOLVED OXYGEN 00 mg/f 14.t

JoC::::E:PrNC:E c::::ca: ~ R....RftJ l ... cs::s:.ucE ~ H-+C1r CE:I'EiUNED

SAUPl£ itPES:

t:-Fut:l R-~ X: - IOIOWH A - ..CO SUNIC

S.WPUHC UETHOOS:

c;- c:RM

PP - PERISDUC l'tJIDI .

-(,:> ·-

• . SURFACE WATER QUA!Ji'Y SAMPUNG RECORD .

pH I AI..'lW.INITY GRAPH ' ' - .

?AGE · . _or_ . . ·--· FAOUlY CODE 005 NP

' L-oc...\TION 10 NEW PROP AU<AUNiiY

LOG OATE 3/3fJ/94- -pH -(mg/1 Ca C03 )

EllROR Ai +.SO:r X 1

- X2

1

t st 2nd .31"'d 8.90

X5 X 100=___% 8.60 7 8...30 /

. ..

tst = % 8.05 /

7.80 ,.

2.nd =. .. 7.50 Aa .

6.50 .. 5.70 /

pH CHECX )..fiER 1TTRATION 5.10 / I

7.00 -

~"J\"ff'r 4.80 / 4..50 / I

4.00- 4.25/ . . .. ·4.efO . .. . ~m 'ld~~6SI-

//~.: - --- -. . • I I , ,I ! I T

II I I I I I I I I I I

_ ..... -, v .I I I I I I 0 I I I I I I I I I : '' .. u . CJ I I I I I

c.J I I I I I f

' I

eft I I E - I I I

~ I

z .I

~ I I I

:i! I I I I I

I I I I I I I I I I

I I I I I l I

2. 3 + 5 s 7 a 9 10 11 12.. '

pH

•

; I

l i .

• . ,. r j l

l

I I .

SAMPLE ID NUMBER: _N_S_60_.1~1----- DATE COLLECTED (MMIODNY): ----- TIME: (HH:MM) ------

MOUND SAMPLE NUMBER: ..&lMtu.NucD'""lB._-__ ."'""'lu.2JIPQO.:...-__ _

SAMPLING • ·•

LOCATION CODE: _.M-NL.DD"'-'1~.~~6 _______ _ DESCRIPTION: MOUN(l OU5 NEW PROPERTY SEEPS ' - OINT CODE: SfEPu DESCRIPTION: SEEP tJUM6EB § '

·sAMPLE-..

• . tdEDIA CODE: 55- DESCRIPTION: Spdog l Saap Wll&t DEPTH TO

~. • . WEATHER: . ',

·~~ FIELD OBSERVATIONS: I .

~-• . .~

SAt:!fLE TYPE: FIELD Mt:ASUREME~TS READING UNITS

GRAB § SPATIALCOMPOSITE --~ ~ TIME COMPOSITE QC TRIP BLANK

,::::,., 1- QC RINSATE • QC FIELD BLANK

~ 1- OTHER (SPECIFY) : ....._

SAMPLE COllECTED: YES NO ~

,. . . SAP SAMPLIN~ PROCEDURE. WAS FOllOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------

If SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:--------------

--------------------------------------------------------------------- ~ "' --------------~----------------------------------------------------------

RECORDED By: --------------QA CHECKED BY: __ ...,.._.. _____________ _

(SIGNATURE) I SIGNA TUREJ

CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES C-0-C # AIR BILL#


VOLUME. TYPE ANALYSIS (TYPENOL) LOT#

3- 40ML Glass Volatile Organics H pH<2, 4°C IT

2- 1 LITER Amber Glas COOL 4°C IT

2- 1 LITER IT


1 - 1 LITER Plastic Cyanide IT

2- 1 LITER Amber Glass Explosives IT

1 - 1 LITER Plastic Chloride IT . 1 - 1 LITER Plastic Fluoride IT



1 - 1 LITER Amber Glass Total Organic Carbon (TOC) ~2S04 pH<2,4°C. IT



1 - 1 LITE~. Plastic Total Nitrogen (TKN) ,H2S04 pH< 2,4°C IT

1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH< 2,4°C ' IT "


1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C ·I IT

1 -.40ML Plastic Rad Screen COOL 4°C IT

1 - 2 GAL Plastic Pu, Th,U,Ac,Ra,Sr ,Am, Gamma HN03 pH< 2,4°C PACE " 1 - 250ML Glass Tritium COOL4°C .. 'PACE ~

I •

:;I

SAMPLE ID'S RINSATE: TRIP BLANK: FIELD BLANK: FIELD DUPLICATE:

RECORDED BY: QA CHECKED BY: (SIGNATURE) (SIGNATURE)

; . : ~ I ... I

~ •.1' 1 I .

.J

. .•• ~. ~ '

~ PARAMETER VM.m.S

SURFACE WAre::P.. auA!Jry S..WPUNG RECORD

005 NP

LOCATION 10 NDf PROP

5'AJJPLE 10

. LOG OATE:

AI'W.'mCAL. us ecce: -------7....-SAUPUNG i=e:.:t!OO: = 1_

SAUPUNG MErnOO .

PAGE _OF'_

LOT CONTROL NO _JD.iiiooiiOOO. __ _

SAMPLE Tl'FE-...::K.:..'----

ACa:Fi'ANCE COOE _A __ _

LOGGER COOE S&IC

COMFL.Et~

CAli: SEkT -------

~ CCMM~ ----------------~~--------------------------/·

I

I'· FAR.4.ME1"ER J.CE.&StJREllEN'TS:

POTC:NT'IAL OF' HYOROGEN pH

Sf'EQF'IC CONOUCT).NCE. Ec

REDOX FOmi11AL. e:n

'TSCPE?.ATURE TMP

.ALKAL.JNITY (C4C~) . AI..K

00

s:.wPt.! i'I'P!S:

F' - l1!lJ.J R - ltf:Pt.lCA1'E X - IOCMH J. - M:iZJ 8UHK

s.u. ·umhos/c:m

mvotts

•c

mg/1

mg/1

I r i I

SAI.lPUHC UET'HOOS:

c; - ~ '!!il' - SU8U!R!ZSLt pU

,. - ~~~ .PWP 0 - <mCIR (SHelf)

• -~

..

•

•

. SURF"ACE WATF:R QUALitY SAMPUNG RECORD . pH/~GRAFH _j_ OF" _j_ .. ~ ~- ·. PAGE .. ..

f"AaUlY COOE 005 NP

- ALKAUNIIY L-OCATION 10 Nai' PROP

3/30/94 -pH

. (mg/1 Co C03 ) LOG OA'TE

t st 2nd .3rc I XI - X21 8.90 rAJA "" NA _ERROR AT + . .50: _. XS =!' 1 OO=Z.Z~ a. so -8.30 ...

1st = Z.1~ 8.05 7.80

~-

.. . -

~ (r.(Js' a f?./o) 2nd= tJit .. ""1.50 -t:,:~ It,.+' !Sl>/,.l !) • .

6.50 . "

5.70 Z.ID fS:' ') 'ZZI pH CHECX AF'i!R TITRA:nON 5.10 NL N~ I •. -

ZZ:J(4.? r) 11/l.. . 7.00 - 1-,0{, +.80 . ZZS(tf..~ Z.10{f.• ~J .:fr 4-.SO

4.00- f.()~. - <4-..25 zzr Z'JZ- f ~-l.~l'l 4.00 · z:ztr -t-J:JJ 2!-l- I -.

SAMPLE m NS-=!-DOI . \11\L.ulf.~ IIJ ( ') ldt... plf "i4JRIN--. -- flrt:"!Jf- !11 . ""' . IJIJ/-. ·Jte!titvtt. ~ ·-

--I I •J I ..Ll

I I I -··· -- I I I I I I I I .., ..

0 I I I I I I I I I I : 1-• ... u I I I c .-. u ! .,. '

Cl I E - I ?: ..

z I ~ I I I I

I I I I I I ' ~

<

' I I I t

2 3 -4o 5 6 7 8 9 10 11 . 12

pH

, . :1

•j i/ I; . '

...-~ .. ·--- .... ~~ .....

SAMPLE ID NUMBER: NSZ001 DATE COLLECTED (MM/DDIYY): _3L-/'J:.....:()._,_f...:.'f....!..f_. _

MOUND SAMPLE NUMBER: MND16-I308 - 0200

SAMPLING -

TIME: (HH:MM) -.L/_.4 ...... 3-=5~-__ , LOCATION CODE: ....~M.!..I.IN!..!..!D~11..!o!6'---------- DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

POINT CODE: ____,S....,E=-"E:.L.P..J..7 _________ _ DESCRIPTION: SEEP NUMBER 7

SAMPLE -

MEDIA CODE: 55 DESCRIPTION: ----.!S.a,owrilllng:i-J/..J,S~e~epOL..WLUllat~erL--______ _

WEATHER: OlltloHI1 f"/. h,uu /Pf S". 1 45"r FIELD OBSERVATIONS: Wtffu 11· Nr/~J.y ·J~f,;/tL ~//; • floi(J ~Sf 4J , • J

NO/fE: fAIAfrL ,~HIAIJ NVW,t.. dut.IA!J S"IWp/.IN' '

SAMPLE TYPE:

GRAB

TIME COMPOSITE

QC RINSATE

OTHER (SPECIFY)

§ SPATIAL ~OMPOSITE QC TRIP BLANK

QC FIELD BLANK

SAMPLE COLLECTED: B NO

FIELD MEASUREMENTS

Nlr 0

! I: . .

•• ...

DEPTH 1Utf TO _ _..}J-=-If'----

/.olP~

BEADING UNITS

.!>



RECORDED By: -----:-~-~~L·.,..;~-~,_= -;;;;;;;;;;==--;:__, __ (SIGNATURE)

•••••

OA CHECKED BY: --~-=11-9-(...,.S~m.qG~~-fll..c..U.#-lR~.Ao~w;~:::~~~t..o~~-----

• •

LABORATORY CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES

VOlUME TYP.E ANAlYSIS '(TYPENOl)

3 - 40ML Glass Volatile Organics HCL pH< 2, 4°C IT

2 - 1 LITER Amber Glass Semi-Volatile Organics COOL 4°C IT

2 - 1 LITER Amber Glass Pesticides I PCBs COOL 4°C IT

1 - 1 LITER Plastic ClP Metals HN03 pH,2, 4°C IT




1 - 1 LITER Plastic Fluoride CO.OL 4°C IT

1 - 1 LITER Plastic Sulfate COPL 4°C IT


1 - 1 LITER Amber Glass Total Organic Carbon (TOC) H2S04: pH< 2,4°C IT




1 - 1 LITER Plastic Total Phosphorus (TP) H2S04 pH< 2,4°C IT

IT V\ ~ IT "'l

1 - 1 LITER Plastic Alkalinity COOL 4°C

1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C

IT ~

PACE (;'\i-

1 - 40ML Plastic Rad Screen CO.OL 4°C

GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma HN03 pH<2AAG-

Glass Tritium COOL 4°C PACE jJ ~

' ,.

FIElD DUPLICATE: IJA \Ices

(SIGNATURtF'""=-

SAMPLE ID'S RINSATE~: ~ TRIP BLANK: NS$13911. FIELD BLANK: NSt./~1 RECORDED BY: _ ... Th.'1lttdAJU!_ QA CHECKED BY: -------=-=~=~~::.:::s;;::---------

(SIGNATURE)

~~-,-..... -.::. -:-·- ~:-~; .......... :. --······. -~ ;·t.:...~. - .. -~-=-=$

~ •··.

~ i.~i i Mtl

I ~·;; ;~.

'I ; J :. 1

• ... i

. ,

,·;: ., ·l .

I

, t

I. !_ i

SAMPLE PARAMET.ER VAU:JF.s SURFACE WATER QUALITY SAMPUNG RECORD

-F"ACll.J1Y CODE 005 NP PACE: _!_OF' _j__

LOC\TION ID N!.W PROP LOT CON'i'ROL NO _NA;;.;;;,;.. __ _

S..WPLE 10 NS :tool S..WPLE: iYPE-..;oK-..· ----

LOG DATE 3/30/94 ACCS..-t:A.NCE CODE _A ___ _

J.I'W..'mCAL. L4B CODE __ ....:N...;:;_.A _____ _ LOGGER CODE _.....,SU=C __ _

SAMPUNG PERIOD: COMPW::.:1:. __ f_Si_"-'"-· ---SAMPUNG MEiHOD GRAB DATE SENT __ '3.;...f.;...~O....:j_7...;.4 __

COMMENTs ftl tfmrd. z.O pt=- f, Of/ pH <;UW<J 4.o ,eN-: g_ 1/ !/()(}(. = 101. (,

j

P~ETER WDSURalENTS.:

PO'T'EN1"1AL OF' HYOROGEN pH s.u. ~.=/-5

SFEClAC CONOUcrANCE. Ec. umho:s/cm ~40.

RECOX FOT'ENTTAL Eh mvolt: ZBI. 2...

1't:MPERATURE TMP •c S.'1-°C

AU<AUNITY (CcC~) . ALK m9/l zz~

DISSOLVED OX'YGEN 00 mg/l 4.8 ...

I s-uPLE 'I"'''PES:

,_ F1I!1D It-~

lC - ICNCWH A - .W:::C 8UHJ(

I j I

S.WPUHC J.tETMOCS:

c:- QWJ

pp - PERJ:ST,ILJC .

13 ..

• . SURFACE WATF:F. QUAJ.Jt( SAMPUNG RECORD . pH I AUW.lNITY GRAPH . .

. . .. PAGE _OF'_ · . -· ..

F'AOLm' eccE: 005 NP

-1.-0CATION 10 NEW PROP AU<AUN

1r'J6,

LOG ~TE: pH (mg/1 Co 3 )

ER.~OR AT +.50:1 X1 - X2 1st 2nd/ 31"d .

8.90 I X 10Q=_J xs 8.60 I 8 . .30 /

-..

l.st = 8.05 -.. 7.80 I /

2nd= % 7.50 , I . 6.50 I ,

5.70 /

pH CHECX AFTER ~TION 5.10 I

. 7.00 -4.80/ 4.50

""'.oo·- - 4:25 lZ""'-00 -

. SAMPLE m

~I ....

.. . - --

f I I I I Ill I I I I I

• I/ I 1 I I - ..

\ -"' I I I I I 0 / I I I I ! I·•

..

.. c.J Cl I I I I I ! ..

(J I . II I I I I I . ·: ._.., , I I I

.. =- II I -~ I I

~ 1/ I

z II ..

~ I

lj

...J I I

< I

I

• I I I I I ' I I

' -2 3 + 5 6 1 8 9 10 , 1 12"'

pH

-"'U::'. IClUim IWa. Pal ocna" ICra ,_ WQ ~ Q/1&) . • .

.. - -.. • \ .. -,,

. . .. I

. ~-- .•• •• '':': : •. "'!.:::":

. ;

r==;.· •..... .:... ' .. -.-·-·· .. ' ' ' .. ~·~r•: ';·• .i. . .

'

SA~PLE ID NUMBER: _N_S7_0_1l ___ _ DATE COLLECTED (MwDDiYY): ------ TIME: (1-iH:MM) -----'---

MOUND SAMPLE NUMBER: ..~.~M.II.lNwDUJ1611L-----~ll.k2QlaOL..----~ .

SAMP,LING • . · I

LOCATION CODE: ...:~M"-UN:.uD.:..~l .... B________ DESCRIPTI9N: MOUNP OU5 NEW.PROPERTY SEEPS l ! .

POINT CODE: SE(:PZ DESCRIPTION: St:EP NUM6tR 7

SAMP.LE • . . . . . MEDIA CODE: DESCRIPTION: Spliog l SDDIJ WaiU[ DEPTH TO

. ' ~ I

WEATHER: -~

FIELD OBSERVATIONS: . ~ V'fLI

~ .. . . .. ~· I

SA~LETYPE: . FIELD MEASUfteM~NTS READING UNITS .

1- GRAB § SPATIALCOMPOSITE ~ TIME COMPOSITE QC TRIP BLANK ........

- QC RINSATE QC FIELD BLANK ~ OTHER {SPECIFY) '-- ...

SAMPLE COLLECTED: YES . NO • .. : .

SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------

IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------. . ~ ' '

RECORDED By: --------~-----;, • . . ·· (SIGNATURE) · ·

OA CHECKED BY:--------------(SIGNA TUREl

. -;

I '

METHOD NAM.E AND NUMBER ANALYSIS

3- 40ML Volatile Organics

2 7 1 LITER

2- 1 LITER

1 - 1 LITER Plastic

1 - 1 LITER Plastic

2- 1 LITER Amber Glass Explosives

1 - 1 LI"J:ER Plastic Chloride·

1 - 1 LITER Plastic Fluoride '·I•.




1 - 1 LITER Plastic Total Dissolved Solids (TDS)


1 - 1 LITER Plastic Total Nitrogen (TKN)

1 - 1 LITER Plastic Total Phosphorus (TP)

1 - 1 LITER Plastic Alkalinity

1 - 1 LITER Plastic Ammonia

1 - 40ML Plastic Rad Screen

1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma

1 - 250ML Glass Tritium - · ·• -· I •!I I :

SAMPLE ID'S RINSAH:: TRIP BLANK:

RECORDED BY: t' !• I 'P;' I · (SIGNATURE) . "'. '

PRESERVATIVES C-0-C #

(TYPENOL) .

HCL pH<2, 4°C

COOL 4°C

COOL 4°C I : .

HN03 pH,2, 4°C

COOL 4°C. · .. COOL 4°C> .•.

H2S04 pH<2

COOL 4°C .... ..

COOL 4°C

H2S04 pH<2,4°C

H2S04 pH< 2,4°C

GOOL 4°C

H2S04 pH< 2,4?C

COOL 4°C

HN03 pH<2,4°C

COOL 4°C

FIELD BLANK:

OA CHECKED BY: ., ..

AIR BILL# CONTAINER

lOT#

'

FIELD DUPLICATE:

(SIGNATURE)

lABORATORY

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

IT

PACE

PACE

··t~ .. ·:

-\J lJ)

;; . •• ~JI

'·' · lr · ..

, ... l ; ~ 'li'l'' ... -iit : i ~; .. !'. 'lr

·I: . l ; . I !r

~~~· ~='

ji'

f. ... j!: .. . ,. ':t'

. '

.. ,

. ' .i I

j) ~ ..

SNoiPLE PARAME:l'ER VALUES .

SURFACE WATFR OUAUrY SAMPUNG RECORD

-F'AClUTI" COOE CXJ5 NP PAGE _OF_

LOC\TION 10

S..WPl£ !0

NEil PROP I t..ar ~O~OL NO __...NI.~---

sJJjPtE:. il'?E K·

Adc:£.-t:a..NC~ COOE _·_A ___ _

I -.LOG DATE

).NAL.:m~ LAB COOE ---------- ,t.OGGE:t COOE I

sue

S..WPUNG PS!OO: SiARi' I --------------! COMPt£:~ -------------

SAMPUNG ME'i'riOO ......;GRAB==-----------------1

DAn: SENT -----------

COMM~ ----------------------~----------------------/

FAA.IJ.IEI'ER MEASURalENt'S:

P0'1'E:N11.A.L OF H'rUROGEN

SPEClflC CONOUcrANCE

REDOX POTENTtAL..

T'EMPE?.AnJRE

AU<AUNITY (CaC~)

DISSOLVED OXYGEN

,. - F1!l.D R - ICZJ"!~(L

·.· I ~;

I

i /

I I

pH S.U •

I

/ I

I

umho:r/e:n

rnvoft::

mg/f

mg/f

SAUFUNC UETHOOS:

C - QU.8 SP-~ P'U'l

IC - ICHO'A'H A - .W:::O SUIOC PP - P!RSDLJC PUUP 0 - <mUR (:sn:t:l t1 . .

•

•

•

..

SURFACE WATFF. OUAUi'Y SAMPUNG RECORD • pH I 1WO\LINITY GRAPH

FA01.!TY COOE _oo....;;..;.S.-NP..;;_ __ ~

LOCATION 10 ---=.NEH~..:.PR::.::RO::.:.P __ _

LOG D.A.TE __ _.:3::;..t.{_~_O.~-f '1.;...4:..._

ERROR AI 4.-0: xs X 1 00=~ - c; I X, - X21 0 3~

· 1st - ,1.3s;

2nd= IJ~ ":

pH CHECK Af'i'ER Tl'T'RA:rtON

. 7.oo· - _ .... 1~..-~tJ!"""":f_

4.00 - . 4.(){'

-"' 0 .. u c u

' at E -~

%

~ ...I <

I I

I I I I I I

I I

2

I

s

I I I

I

6

I I t

I I

7

pH

PACE _j_ Or _j_

ALKAUNii'Y

pH (mg/1 Co COJ)

1st 2nc :Src 8.90 IJI"t 11lft

"""" 8.60 8.JO . 8.05 J I 7.80

,. ~

7.50 tl(,.9/,) ~(,,f/,J 6.50 Z?JlJ (&,4 ~- ZOO(' '14J 5.70 ZfO (~~ ) Z1tJ_{_, ~,7) 5.10 AI~ z.'JS(S: C'f) 4.80 ·2Sf. Z.S8 ( 4 lH) -~-50 2B!IL4-~ fr_l z.'lo 1(..4/) 4.25 Z.~l (#/.. ~cz> Zfl « ~3Dl 4.00 2.,3 71. ~7) 2,3 1'4-lJ1

\IAlU£4) i"i (_ ) lfU: ptf· · Wl!fil+l. fitxjtl-pH WIH ··NtJf :

I I I

I .l I I I

I . .l I I

I I I I .J

I I I I I I

I I I I I

I I I

I I I I L I I I I I I

8 9 10 11 12

~

.

: :

I I

. ! ; I

' I I I I I.

I ! I-I'

- ..... _... _ _,.......,. ...... ~::-- • .,~ .,II _,"\1""! •• ·~::"',•,

,!;.::.r:t.:oa,t.:..,.:..:;-:;-~~- -~....==.~·· .. oM~-·

'·:-: • ~ l'{

•t r.' . ; :'

SAMPLE ID NUMBER: _N_s_ao_o_1 ___ _ DATE COLLECTED (MMIDDNY): 3/Jo /21 TIME: (HH:MM) 15 3 S

MOUND SAMPLE NUMBER: MND16- 03'03- 0200

SAMPLING -

LOCATION CODE: _.MJWNwD"'-J1a.w6:__________ DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

POINT CODE: ---lSoaEa~oEo.LP..w.B ________ ___,_ DESCRIPTION: SEEP NUMBER 8

SAMPLE -

MEDIA CODE: 55 DESCRIPTION: Spring I Seep Water DEPTH 'S111.F TO _Nfr~--

WEATHER: Ou«CMI, Sl. hafzE, 40°F FIELD OBSERVATIONS: WNd. Ck'M. /,efou., . SltHI{J!IAIJ· . C/IJicJ 61. cU 4. 0 fl>llt

SAMPLE TYPE:

GRAB

TIME COMPOSITE

QC RINSATE

OTHER (SPECIFY)

.I

§ SPATIAL COMPOSITE

QC TRIP BLANK

QC FIELD BLANK

SAMPLE COLLECTED: ~ NO

· FIELD MEASUREMENTS READING

AJA ~ -

I

~

UNITS

SAP SAMPLING PROCEDURE WAS FOLLOWED? ~ NO FIELD CHANGE ORDER REFERENCE NO: --------


REGORDED By: ____ Yn~~=~:=:::::~o:::::--____:..· __ (SIGNATURE) -=::::::::

QA CHECKED BY: ___ GJ-I+....ou.~trfj;u.u.'-';~~L...=....:;.:...=' ~~-----Vt=TUAE)

~~··.

", , •'I I

CONTAINER VOLUME

3 • 40ML

2- 1 LITER

2- 1 LITER

1 - 1 LITER

1 - 1 LITER

2- 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

1 - 1 LITER

CONTAINER TYPE

Glass

Amber Glass

Amber Glass

Plastic

Plastic

Amber Glass

Plastic

Plastic

Plastic

Plastic

Amber Glass

Plastic

Plastic

Plastic

Plastic

METHOD NAME AND NUMBER ANALYSIS

Volatile Organics

Semi-Volatile Organics

Pesticides I PCBs

CLP Metals

Cyanide

Explosives

Chloride

Fluoride

PRESERVATIVES (TYPENOL) lABORATORY

~1_-_1_L~IT_E_R __ r-P_Ia_s_tic ____ -+_A_Ik~a_ll_ni_tv ________________ r-c_o_o_L_4_o_c ______ r---+-----+---+-----~~~~~~~-----IT ____ -4~ 1 - 1 LITER Plastic Ammonia H2S04 pH< 2,4°C IT ~ 1 • 40ML Plastic Rad Screen

GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma

SAMPLE ID'S RINSATE:

RECORDED BY:

~ ., :; . . i

..;. '

)

.. ' !~ ~

J ! i !

SAMPLE PARAMETER VALtJES ·

SURFACE WATF:?.. OUA!irY SAMPUNG RECORD

CXJ5 NP PAGE I OF' \ --LOCATION 10

NEW PROP LOT CON'l"ROL NO ....,n ........ __ _

SAMPLE 10 SAUPL.E "i'Y?E-~K~· ----

~c~~ ______ 3~Z~3D~/?~i~-------- ACC£..-ti\NCE CODE _A ___ _

JJ-W..'I'TICl.l.. LAB cooe: --...:..AI.:..:Ir~----- LOGGER cooe: _SI.l'=;.;;;;.c __ _

S..WPUNG PS!OO:

SAMPUNG MErtiOO

PARJJ.CE!'ER l.lfASUREMe::HT.S:

F~ OF H"r''ROGEN pH

SPE~ CONDUCTANCE Ec

REDOX ParamAl. Eh

TEMPERATURE TMP

ALJ<AUNIT'I' ( C4C~) . AU<

DISSOLVED OX't'GEN 00 ..

s.u. umhc::s/cm

mvclt.s

•c

mg/1

mg/1

COMPL£1:. _ __,~1...;:/o~O....,O..._.....__ OA~ SEN'i __ '3.:...;/ 3-.b,_if:/:...:4;___

'·8.fa 183:0 ?5~. t:t .. .

B. I

Z89 s:o

.AC::EPT'JIC:t c::::cE:S: ~ It~~ l+-foet'~

S.WPl£ nPES:

, - F1E1.D It -~ IC - IC:NOWH J. - JQD 8UHI(

I I

i I

SAJ.IPUNG ue:n;oos: c - QUa S1' - SUBWERSI8t£ P\J1I.I

PP - P£:RrSl').UC .PtAIP 0 - Cl'tH£lit (SP!t:f"t) .

••

•

•

• SURFACE WATF:R. QUALITY SAMPUNG RECORD

~I ·-r--------~-_::.:_-

• pH I AUAI..INITY GRAPH

F'ACll!TY CODE -~OO;;.;;S;.....;.;,;NP:__ __ ' L-ocATION 10 ......;NEH~:-PRO~:::!.P __ _

LOG DATE--------

XS X 100=_% ERROR AT .... 50: X

1 - X

2 1

1st=·--%

2nd =·------%

.. pH CHECX AFT'ER T'ITRATION

. 7.00 - -----

pH

t st 8.90 8.60

PAGE / _OF'_

AU<ALJNITY (mg/1 Co ~03 )

2nd·

/ /

8.:50 8.05 ' t-;;-~-t----;o-:+------4----.l ..

'

7.80 I

7.50 '

6.50 I

5.70 / 5.1 (j ..... 80

;4.50 4.25 4.00

4.00 - ----- - ' ~~~-r------~-----~---~ S»H.E m - . ~/,/

-.., 0 ... u c u

' "' E -~ ·- z ~ ~

<

-----=:.../; . NO M6~f.

I I I I I i I f I I

Mlrtiii"ttttttt! /fttrttt+H-H-f-HH-1-+f-t+++~~~W1..W!..W.f.L.l1 ·-· ..

I I f I I I I I I I I I I I I I I I I I 1 : J. I

I I I I I I I I I I

I I I I I I I I I

I I

v

I I I .. "

"- ... ·. v:.>4iiiJfi ~i(9i'5.·@ ~hl<;ll . .f. .

· -·--·--·--... -... :=-::: ...•• ~~- l!f:.4\2J"i.iUC':US -:.-oi· . .:.;-:.-··. -: -··- .. - - • ·.-· :· . --:.-·~!'t;a.

SAMPLE ID NUMBER: _N_Sa_o_11 ___ _ DATE COLLECTED (MMIDDIYY): ____ _ TIME: (HH:MM) -------

MOUND MPLENUMBER: ~M~N~Du1~6·-----·~1~20~0~-----

SAMPLING -

LOCATIONC DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS . . . POINT CODE: ---l.ado~--------

~AMPLE -

DESCRIPTION: SEEP NUMBER 8

.... MEDIA CODE: _,5ouo5..__ ___ . . , :r~: Spdog I Seep Water DEPTH ____ TO ___ _

· WEAT~E8: ______________ ~---------"~~----------------------------------------------------FIELDOBSERVATIONS: _______ ·_·_s_..;:,· .....,~-··-. -fe,~~~>~r-------------------

.. . ' . ,,·'~

SA~LETYPE: FIELD MEASURE~ENTS READING UNITS

~ GRAB § SPATIALCOMPOSITE ..

~~ TIME COMPOSITE QC TRIP BLANK - QC RINSATE QC FIELD BLANK ......

I~ - OTHER (SPECIFY) .. - ~


SAP SAMPLING PROCEDURE WAS FOLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: -----------

IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:------------------------

REQORDE~ By: ------------------ OA CHECKED BY: -------------------------------(SIGNATURE) (SIGNATURE)

. .

METHOD NAME AND NUMBER PRESERVATIVES I C-0-C # ,. AIR BILL# ., CONTAINER

I LA BORA TORY ANALYSIS (TYPENOL) LOT#

Volatile Organics .. HCL pH<2, 4°C I I I I IT

2- 1 LITER Amber~l~ Semi-Volatile Organics COOL4°C I I I I IT

2- 1 pTER Amber Glass ~~cides I PCB~ . COOL4°C I .. I I I IT

1 - 1 LITER Plastic CLP M~ls.._ HN03' pH,2, 4°C I I I I IT

1 - 1 LITER I Plastic I Cyanide ~ I NaOH pH> 12,4°C I .I I I IT

2 - 1 LITER I Amber Glass I Explosives """ I I I IT COOL4°C I

1 - 1 LITER I Plastic Chloride ""'-1 COOL 4°C I I I I IT

1 - 1 LITER Plastic Fluoride I C01>L4°C .. I I I I IT

1 - 1 LITER Plastic Sulfate I COOL4°C"-.. I I I I IT

1 - 1 LITER Plastic Nitrate I Nitrite I H2S04 oH < 2.4CI'C-I L4-. I I I IT

1 - 1 LITER Amber Glass Total Organic Carbon (TOC) H2S04 pH< 2.4°C I ......... I I I IT ......

1 - 1 LITER Plastic Total Dissolved Solids (TDS) COOL4°C I "'-... I I I IT

1 - 1 LITER Plastic Total Suspended Solids (TSS) COOL4°C I ...-.... 1""'-'C/ - I I IT

1 - 1 LITER I Plastic I Total Nitrogen '(TKN) H2S04 pH< 2,4°C I .. ~ """-~~1 I IT

1 - 1 LITER I Plastic I Total Phosphorus (TP) H2S04 pH< 2,4°C I I \,J .......... ~ I IT

1 - 1 LITER I Plastic . I Alkalinity COOL4°C I I ""- I IT

1 - 1 LITER I Plastic I Ammonia H2S04 pH<2.4°C I I I I IT

1 - 40ML I Plastic I Rad Screen I COOL4°C I I I I IT . ~ 1 - 2 GAL I Plastic . I Pu,Th,U,Ac,Ra,Sr,Am,Gamma I HN03 pH< 2,4°C I I I I PACE .'.J

1 - 250ML I Glass , 1 Tritium .... 1 COOL4°_C I I I I PACE

SAMPLE ID'S RINSATE: · TRIP BLANK: FIELD BLANK: FIELD DUPLICATE: .. I

RECORPED BY: OA CHECKED BY: (SIGNATURE) ... (SIGNATURE)

l _.,.,;;;i~Ji!r!$, . .. --- --~===========-..... . .. . .. t===;

Sft'P 7~ LOl

- . ..... - STANDARD ALJ<AUNtrf rc:.ST RECORD .. •

' F'.&.CUTY COCE 005 NP

FIELO RE? ·~. SMihr LOCCATE 4/J/94

AI..KAUNrtY TEST KIT: Mol:)'f L.. ALl Dl

MANUF'Ac,ruR~ l±,.cJ; ALKAUNITY TESi KIT 10 ~r~r ~'1"

pH ME'l"C::R:

J.U.NUFACTURER 0~101'\ SE:RlAl. NO MOI2f£. ZSM I SbJ OOZ4CJS' .

LAS STANOARC . AI...KAUNtrr TEST' VALUES

KNOWN VALUE (at cH ..,ctDolnt - ~.:5)

.COCE SOUJT10N 10 (mg/1 CcC03) mg/1 CcC03

Nft cAr. 14Z;.a -10 . Z5tJ 2.41

• COMMENTS .IJSED -,uj,mp/E 'i,2.1"i..E 6f.lhlr1tf /i,lt. tJ:!.t:VItAeft. ~fg,t

f2f4. tfd'-!J. l:lf IJJ.d!ttlLftK..!J.MJ.e.t. IIJff:tl.tJ.'tz~ IJI.l!Nll.d.l· 1

/' /

./ /

'· .

..

-

l

IlL

. j

l j l . I I

• I

I I j

I

. I

{

.. ... ' ... ,_ .. •

I -. !

-

r 1-

- .SiANOARO AL.KAUNln' TEST RECORD

-F'Ac:Lm' c::OE aJS NP

~oRE?- .. LOCCATE

Al..'<AUNI'TY I~ I i<IT: /

.· .·

AU<AUNilY rc:sr i<ri ('-

I I

MANUF"ACTUR~ i . / I

I .'

pH UE1c..O::: /

I I.U.NUF'ACTUR~ SEW.. NO

I KN~ VALUE

AU<AUNI'TY TEST VALUES. LAB .. ST»lOARO (crt oH enctoolnt - ~~)

.CCOE SCUITtON 10 7g/l CcCOJ) .

mq/l c4COJ : - .. .. / • .. /

f7 . ./

. /

.~

COUUENTS / . .. .

.. / / /

/ /" / .. ./

.. /

-

u 103

.

• . ..... - STANDARD ALKAUNITY TEST RECORD .. ...

... 005 NP FA.Otm' COOE

.I F1ELD RE? . LOC OATE /

J.LJ<.WNiiY TEST KIT: / MANUF..I.CTURER 7m1c pH METER: . M.A.NUF..I.CTURER

~NO

i j'

v AL.KAUNrTY TEST VALUES LAB ST»tOARD . KNOWN VALUE. («t DH tndDalne • <l..5)

.COOE SOtunON ID (mg/1 .CcCOJ) mg/1 cCCOJ I

• I L

I . -: ·.

L ./

.. -. .

COUUENTS . . . .

. . L· ..

/ ./

/ .. . ·-

• . . ~

•. ~· ... ti' f. 4

"'

•

,. l· ... :--· ;;1 :i

..... ~-• '

. i

I I

JL

!:

..

.

- STANDARD AL..KALJNITY r::..ST RECORO

-F.l.Cllm' COOE CXJ5 NP

FiEL!J F.::? LOC:OJ.TE:

AL'<AUNtTY ~ i<IT:

MANUFAcnJP.ER 7=~10

pH ME1c..-;:

MANUFAcnJRER SE?.lAL. NO I

I AL..J<AUNrTY rc:sT V~£ us SI'~OARO /c KNOWN VAI..UE (czt oH endDai'lt • 4-!l)

.COOE sot.LmON 10 (mq/1 C4COJ) mq/1 c4COJ

I 1/

.. .I I

I

tffJ '

CO WENT'S l

I I /

; / ./

/

. . pH I ALRAI.JNITY VAUJES u . SURFACE WATER OUAL..11Y SAMPUNG RECORD

·-••• FACtL.J'T'r. CODE 005 NP PAGE l OF' I ... LOCATION 10

m.w·PROP LOG DATE: 1/}tf- 'J/Io/14 -,_

S..WPU:: rc.sr pH ALKAUNrTY (mg/1 CcC~ ) · UNC::..rc i~NTY 10 Krr 10 (S.U.) 'ffiUE VALUE FlELD VALUE (;;)

lt'lS IMJ 1/(J(,~ 4.~/) t<Jft Z93 tJfa NS ZIJOI ,, . .t/.SD ZB9 Jo!IS 300J •• 4.5D -z.cri' f'JS 4061 ,,

4.S7J Z3-# AIS SDOI ,, 4.,0 . 1?5' 1\l .5 t,t¥)) ,, /.~7J Z/3 NS =ltJtJJ ,, ./,5"/ zzs-JJS fttJJ. " 4-4~ . ' ZCJCf ~

~ &Jinc4 . . . .

.

• . - -.. -

·-

.. . . .

..

COUUEHrS Sfe: 5~d_lfd A{l4ft~i~ 7Qf /lJ.cp&i_ ,Z,L iJ!ve. YAiv£

Alld /JIIt~dd:z.4!J;. rJ.~Iv..r~, dl1 d./!~b..;i ¢:. ti.blllh~~

tJtlfl..tliill!l' ~.; . l!tJL 5Nt~ .,... ~

~-~~ lt-fiECI= .. ~ ~ ~~

•

t pH I ALKALINITY VALUFS. . . 1 0 lp ::!

~--------~----------------------------------------------~-~ -....;;, ~ SURFACE WATER QUALITY s.A.MPUNG RECORD "!

~ . .. . FACIUT'r. COOE CXlS NP

LOCATION 10 NEW PROP • PAGE

LOG DA1"E------------~·' -or ·I,

- --· SAY Pt.£ lUi pH

10 KIT 10 (S.U.) AL..KAUNI1Y (mg/1 C.:C~ )

7 ~UE VALUE FiELD VALU~

-..... UNC:..RrAlNTY . (;;)

/ -----/

,.

-/.

/. /

.~

• / /

v I

I I

I

COUUENT'S ----------------~------;.

------------------:-----:: -

•

•

STANDARD ELECTRICAL CONOUCTMTl' DATA

F'ACIUTY CODE oos NP LOG DATE J I z. 1 tri I

LOGGER CODE _SAI_c ______ _ ACCEPTANCE CODE __:A;:,_ ____ _

~u~cruR~/EcM~ID --~~5·(~3_0Q0~~7L~C~S~N~9~1b~O~Z~9=~~1Z~----------

Ec

AJr. Nt 11"-NL All

/0/Z . IOSZ..

1072 '-R:f =/-(Jr "TZ4 =t33 "Ts-B 71':11 +93 'XI+ 7"1.\-flSZ. i~/ ~'15

q()=/-

CfZ8 '14'1 t:tr,r Cf'fl 1010

aECTRICAL. CONOUCTMTY OF KNOWN SOUITlONS AT 25 ° C:

TEMPERATURE (°C) (LAS THERMOMET!R)

0 1 2 .3 4

s 6 7

8 9 10

11

12 1.3 1<4-15 16 17 18 19 20 21 22 2.3 2<4-2S

TEMPERATURE (°C) (Ec MET"E:R)

All CDUTtlN~~ I ~

Nl Ct , Nl. tl .. l:lt. •• " Nt. , •• ~ '-·3 ./lfDS/Z~ ,.,

S.-4--· . ~.S

+.t, ~3 /(J.3 ltJ. s-/2.1 /1.0 /1,CJ 1~·?' /S:9 f{,.Y /:}.~

J'J,'I !9. ~

ZO. ':1-zt.-+-zz." Z3.=f Z4.?

I

j'

I

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' I i

' .. i i

I~

'.f .. ,

•

•

•

;I .~~

10'0 ' ~----------------------------------------------------------- 3: srANOARO ELECTRICAL CONOUCTMTY DATA

FACIUTY CODE __ oos __ NP__________ LOG DATE ----r---------LOGGER CODE SAIC ACCEFTANCE CODE ,~Z ... ...:A;;..... _____ _

MANUF'ACTIJRER/Ec MET'ER 10 --------· --~~--------1

::LEC'T'RICAL CONOUCTM'TY OF' I KNOWN SOLUTIONS AT 25 ° C,r

KNOWN (mq/1 KCr) Ec ,(meter) _/

I I

I . TE:MPERATURE (°C)

Ec T!MPERATU~~: (LAS THERMO ) (Ec METER)

o I 11 ).

/3 I ...

I 5 - ·I 6

I 7

I 8

I 9

/i I 10 ;xv 11

"' I 12 ./ I 13

I 1<4-

I 15

I 16

I· 17

I 18

I 19

I 20

I 21

I 22 2J 2<4-25

COMM~ ----~---~------------~~-----------------=

-y' r. ~.·.; , .. ... ~ ~

I

'

r·. .. •• '. f ~.

•

•

•

. . . . . .. ··- . -...

SURFACE WATER Q(JALJTY SAMPUNG RECORD

~ I CALl:BRA'l'ION FACIUTY CODE 005 NP I I ----~~---------- · PAG~ 0~

- LOCATION 10 NEW PROP LOG OATE 3/Z'I/'14 - -

SAMPUNG INFORMATION

WffiiORAWAL METHOD

FILTER SIZ::~-NA---------i'HERMOME:i'ER 10

Ec MEi'E:R 10

pH UEJ'ER 10

'f st 3oao TLC M!n~; SAJ 9rboz.q 5/ z o~roN ZS'dll: ~ ODZ4-'J5

• PUMP 10 NA

ALi<AuNrTY KIT 10 ·HitCH ,_.~DEL AL-t>r 7£STICJT ~IT# 40"T . I . .

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CAUBRATION INFORMATION

DATE/ilME: OF u.sT E:c: CAUBRATJON- . (fACll>l'l) Hft~(o E£f!fJN/£ C/IK "'l{Zg/94 TIME OF Pti CAUBRATIO~ fa S"AttipiEj Dz 5dmpl£. 14t [Hilz' .f/idlb'/ .

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SHIPPING INFORMATION NA. . See appropriate sections ·in logDook · for sample sbipzent. infcn:ma.tion. ~· ·

L.AS(S) SHIPPED TO: · _ DATE(S) .SHIPPED: . . ~ METHOD OF SHIPMENT: . . . ~ -------

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SAMFUNG JNFORMAnON

wririORAWAL. MG'riOO ~~~~s~ ____ Hl ________________ _

i"Hs:?.MOMEt~~ 10 ----------

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pH Mc.1~=! 10 ----------PUMP tO _____________________ _

AU<AUNJTY'Ktr 10 --------

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CAic./Tl).lE OF VST Ec CAUSRAnON ·----------~----

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F'OR STANDARD SOLU110N pH 4, INSTRUMENT READING ---------

FOR STANDARD SOUmON .pH tO. SNSTRUMENT READING -· --------

Eh OF.CAUSRATION SOUinON ----------------

Eh R~ING IN C:.WSRATION SOUJliON AFT'C:.R INSiRUMEHT' MEASUREMENT ----

lc:MP. OF CAUSRATI9N SOUinON ( °C) --------------' .

S'rifPPrNG INFOR~TION NA. See appz:opriate sectiaos ·in ~ogboolc · · · far samp~e sbipaent. information. ·

LAS(S) S'rilPP TO:

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COMM

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· PAGC: OF --- LOCATION 10 _;..;;NEW;:;;.;.....::.:PRO:=.:.P------ LOC OATE ----------

SAMPUNG INFORMATION

wmfORAWAL MDHOO

FiLTER Sizs: __ NA ________ _

iHERMOM~ ID --------!cM~IO __________________ __

pH METER 10 ------------PUMP tO ____________________ __

ALKAUNfTY KlT' ID --------

Fta.o REP ----------INSTRUMENT(S) USED

CAUBRATION INFORMATION

oA'l"£..1'nl.cE. OF lAST Ec CAUBRATION --r------~-------

TIMEOFp~CWBRATIO~ ------~--~------------------------FOR STANOARO SOUJTlON pH 7. IN

FOR STANDARD SOLU'nON pH + NS'TRUMENT READING ---------

FOR STANDARD SOLU"nON p 1 O. INSTRU)dENT READING -· -----------.. Eh OF CAUSAATION SO

Eh READING IN CAUS ON SOLU"nON AfTER INSTRUt,tENT MEASUREMENT -----.

liiJP. OF CAUBAA N SOLUTION ( °C) ---------------

NA. . See appropriate sections ·in l.ogbook · -----+---- for sampl.e sbipaent. infm::matian. LAB(S) S ED TO: ·

.. OATE(S) • HIPPED: ..

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~ ~TION 10 ---NEH~~P.e~R0~P------------ l..CG DATE: ---------

SAMPUNG iNFORMAnON

wt'itiOAAWAL Me::inOO Fit.:I:..=t srz:: __ NA ________ _

iiiE? .. YOMEt:..-t 10---------

~MEt:..-tlO-------------------

pH Mc.t:..i 10 ---------

PUMPID--------------------

ALKAUNJTY KIT 10 --------

ReD~--------------------IN:STRUUOO(S) US£0 ____ __,__ ·~

~SRATION INFORMATION

DA~E OF lAST Ec CAUSRATION -r--------------nME OF .. p~ CUJSRAnO~ .;...· ---+--~------------

FOR STANDARD SOt.UnON pH 1, ! S'i'RUMENT R~ING ----------. .

FOR STANDARD SOt.tmON pH

FOR STANDARD SOt.UnON p 1 O. INSTRUMENT REIJJING -· ---------

Eh READING IN CAUSRA N SOI..IJnON A.FTER INS'i'RUJ.(ENT Me:ASUREMEN:r ----

. TncP. OF.CAUSRAnO SOt.tmON ( 0.C) -------------

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ll3 SURFACE WATF:R QUALm' SAMPUNG . RECORD ~ I CAI.lBRATictl

F"AClUT'Y COOE._....;OOS;.;;.;;.~NP~------ PAGE ... _or_ - LOCATION 10 _:.;:NE'if==-..:..:PROP=------ LOG DATE ---------

. SAMPUNG lNF'ORMATION

wtrriOAAWAL ~e:THOO T.RANSF.ER DEVICE .

Fii..'T'ER SIZ£ __ NA ________ _

i'HERMOM~ 10 --------~M~lo __________________ _

pH Mc:.u~.H 10 ---------- . . PUMPIO ____________________ __

AU<ALJNJTY l<lT 10 --------

REI.O REP ----------INSTRUMENT(S) USED

CAUSRAnON INFORMATION

OAT£/TlUE OF lAST 'Ec CAUSRATlON _.,.. ______________ _

TlME OF pfi CAUSRAnO~ ___ .,.__--:----------------

FOR ST.ANOARO SOI..UTION pH 7.

F'OR ST.ANOARO SOt..unON pH • INSTRUMENT READING -----------

FOR ST.ANOARO SOL.tmON 1 O. INSTRUMENT REA.OING .-· ----------

ON--------------------------------

Eh READING IN CAU nON SOUJnON AFTER INS'J"RUUENT MEJlSUREMEN:r -----ON SOt..unON ( °C) _....;.... ____________ _

MATION NA. . See appropriate sectiaos ·in l.ogbook ----.,t---- for sampl.e ship.aent. infODIB.tion. LAS(S} S PED TO: · OATE(S' • IPPED:

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SAMPUNG !NFORMAnON

WliriOP.AWAL ME'i'riOO TRANSFER DEVICE

ALI :.H S"LZ:: __ & ________ _

iHERMOME:l:.."'! 10 --------

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pH Me:.,:..=! 10------------1-

PUMPIO-----------------~-. AI..KAUNI'lY KJT 10 ______ ,___

FlEI..ORE?--------;-~,..-. INSTRUMENT(S) USED

· · . · · CAUSRATION INF'ORMATION

nME OF' pf1 CAUSRATIO~ -+-------------------pH 7. INS'l'RUMENT READING ---------

N pH "-• INSTRUMENT READING ----------

F'OR STANOARO SO ON pH 1 O. INS'l'RUMEHT READING -· ---------

SOUJnON--------------------------------

Eb READING IN RAnON SOutnON AFTC:.R INSTRUMENT Me:ASUREMetr ----

SRATIONSOLunON(0C)-------------------------

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ITEM o·ESCRIPTION

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LAST RECALL

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NEXT RECALL DATE

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COMMENTS

CATEGORY 1 M & TE CALl BRA TION LOG

........

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ITEM DESCRIPTION

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NAME DATE

- -···-- - ··-·. -- . ,

IDENTIFIER

CATEGORY 1

ITEM DESCRIPTION

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M & TE CAll BRA TION LOG

BACKGROUND CHECK

RESPONSE CHECK NAME DATE

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CATEGORY 1!

ITEM DESCRIPTION

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M & TE CALl BRA TION LOG

BACKGROUND CHECK

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ITEM DESCRIPTION


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NAME DATE

• \ • • SAMPLE ID NUMBER: NS0101 ------- DATE COLLECTED (MMIDDNY): . :¢9/tt"' TIME: (HH:MM) _,./-=-5..._/S~--MOUND SAMPLE NUMBER: MND16-QOOO- 3201

-SAMPLING -

DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

DESCRIPTION: AMBIENT BLANK #1

LOCATION CODE: -~M.u.~NL.11D~1u.6~-------

POINT CODE: __...~ACJB.u1'---------

SAMPLE -

MEDIA CODE: 72 DESCRIPTION: -'A;;uS.uT.uMwWwal41teKJr _________ _ NA To_NA~_ I

DEPTH

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TIME COMPOSITE

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CONTAINER I METHOD NAME AND NUMBER I PRESERVATIVES TYPE ANAlYSIS ITYPENOL)

Glass Volatile Organics J:ICL pH< 2, 4°C Ilfo-

CONTAINER LOT#

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LABORATORY

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sAMPLE ID's RINS~~~ BLANK: NSP.3gSl . •wrNK= ·v-rry, . . RECORDED BY: --~ OA ~Efi'/tiBY: ---~~~=--=~;t:!...._-==~~~~-------

ISIGNATURE) .

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SAMPLE ID NUMBER: NS0102 DATE COLLECTED (MMIDDIYY): _____ _ TIME: (HH:MM) _____ _

MOUND SAMPLE NUMBER: MND16- -3201

SAMPLING -

LOCATION CODE: _.M.u~N.u:D:~.~l.x.6 _______ _ DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS '

POINT CODE: ('82 DE'SCRIPTION: AMBIENT BLANK #2

SAMPLE -

MEDIA CODE: 72 DESCRIPTION: OW!!!' IIMIWI <

WEATHER: :z FIELD OBSERVATIONS: z

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SAMPLE TYPE: .

GRAB § SPATIALCOMPO TIME COMPOSITE QC TRIP K QC RINSATE QC D BLANK

BEADING UNITS

OTHER (SPECIFY) ~-------

YES NO

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IF SAP WAS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:--------------~ (/'\

RECORDED By: ------------- QA CHECKED BY:---------------· (SIGNATURE) (SIGNATURE)

CONTAINER I,CONTAINER I METHOD NAME AND NUMBER I PRESERVATIVES VOLUME TYPE ANAlYSIS . (TYPENOLJ

3- 40ML Glass Volatile Organics HCL pH<2, 4°C

..

C-0-C # AIR Bill# CONTAINER

LOT# LABORATORY

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SAMPl-E JD'S RINSATE: TRIP BLANK: · · FIELD BLANK: FIELD DUPLICATE: ., • II•

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MOUND SAMPLE NUMBER: MND16- DODO- 32oa

SAMPLING-

LOCATION CODE: _.MIUINwP~1.w.6 ___ _

POINT CODE: __,B....,B:u.1--------

SAMPLE-

DESCRIPTION: MOUND QU5 NEW PBOfEATY SEEES

DESCRIPTION: · Sample Bank Blank 111

ASTMWater DEPTH ~ TO -!""-~--

SAMPLE TYPE:

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CONTAINER I METHOD NAME AND NUMBER I PRESERVATIVES TYPE ANALYSIS : fTYPENOl) ·

LABORATORY

Glass I Volatile Organics I HCLIJH < 2, 4°C IT

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SAMPlE ID NUMBER: NS0202 DATE COllECTED (MMIDDIYY): ------ TIME: (HH:MM) _____ _

MOUND SAMPlE NUMBER: MND16- -3204

SAMPliNG -

lOCATION CODE: _.MI&LINI.DDc..~1~6--------=-- DESCRIPTION: MOUND OU5 NEW PROPERTY SEEPS

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VOLUME TYPE ANALYSIS ITYPENOL) lOT #

3 - 40ML Glass Volatile Organics HCL pH< 2, 4°C IT

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(SIGNATURE) ......... ~a~l~

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~r. TIME: (HH:MM) A.fA

MOUND SAMPLE NUMBER: MND16- oooo- 2201

SAMPLING -

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LOCATION C~ ~ESCRIPTION: MOUNP OUS NEW PROPERTY SEEPS

POINT CODE: ~ DESCRIPTION: __,T.&IIripiC-'BioUI.~~~~an..uk._.II~1---------------SAMPLE-

DEPTH NA TO ___ M~--

WEATHER: bU"' 1104' • «-- • I > < . • .., II

SAMPLE TYPE:

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READING UNITS

NA ---+<------1 ;>


SAMPLE COLLECTED: @ ~0 '-

SAP SAMPLING PROCEDURE WAS ~OUOWED? @ NO FIELD CHANGE ORDER REFERENCE NO: --------


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CONTAINER I METHOD NAME AND NUMBER I PRESERVATIVES TYPE ANALYSIS (TYPENOL) LABORATORY

Glass I Volatile Organics I HCL pH< 2, 4°C IT

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~--------~-----------+------------------------~--------------~~---------+------------~----------~~--------~,

SAMPLE ID'S RINSATE~ .=r~ANK: 7JS2_3¢/ FIELD BLANK: . AJS(I I~ I FIELD DUPLICATE: _IJ\ ___ _ f\ECORDED BY: . ~ 1 _ OA CHECKED BY: . 5~-:-- _ <.

(SIGNATURE)

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SAMPLING- • I . LOCATION CODE: MND16 · . . pESCRIPTION: MOUNO'QU5 NEW PRQPEBIY SEEPS

POINT CODE: Tf)2 • ··. DESCRIPTION:· _._I .... dA~.-~oBILUilat.UJok~I2--------------

SAMPLE- ·· ··· :

MEDIA CODE: Z2 · DESCRIPTION: ASIM Wat~r ! DEPTH 1\JA TO t.JA WEATHER: CJ.J...,@ 3a 0£ . FIELD OBSERVATIONS: ~ ~~~-~ ~ -~CAt&_-*>Jpiut~

SAMPLE TYPE: GRAB . . -~SPATIAL COMPOSITE TIME COMPOSITE QC TRIP BLANK QC RINSATE QC FIELD BLANK

FIELD MEASUREMENTS READING UNITS ..

NA- -7


SAMPLE COLLECTED: @ NO ~ ... ' -L

SAPSAMPLING PROCEDURE WAS ~OLLOWED? ·~ NO FIELOCHANGEORDERREFERENCENO: --------

IF SAP WAS NOT FOLLOWED. SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

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' CONTAINER CONTAINER METHOD NAME AND NUMBER PRESERVATIVES C-O-C # AIR BILL # CONTAINER LABORATORY

VOLUME TYPE ANALYSIS · (TYPENOL) LOT #

1..~- 40ML Glass Volatile Organics HC:L pH<2, 4°C :CJ(,- Z "tl~9a0u6B&, 31..ft,7l'13 IT

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. ··-· ·~----··-- ' !

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SAMPLE ID NUMBER: - NS0303 DATE COLLECTED (MMIDDNY): ------ TIME: (HH:MM) .-0 '

MOUND SAMPLE NUMBER: MND16- - 2203

SAMPLING -0

• ; .····

LOCATION CODE: _,Mia&JN~Do:L.l...,6.._ _______ _ I

DESCRIPTION: MOUND OU5 r-'EW PAOPEFJIY SEEPS

POINT CODE: TB3 ° • DESCRIPTION: Trip Blank H3 // -· SAMPLE -

, ·-/o/0 ...... -··

/ :RVATIONS: L

n~ ·/r I

SA~LETYPE: 0 ~ FIELD MEASUREMENTS READING UNITS I

GRAB § SPATIALCO~i?" 1- TIME COMPOSITE QC TRIP BLAN

;

1- QC RINSATE QC Fl~l NK 1- OTHER (SPECIFY)

0 0

0

SAM: COUECTED/NO

'

SAP SAMPLIN~OCEDUAE WAS FOJ_LOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------

AS NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

(SIGNATURE) QA CHECKED BY: (SIGNATURE) RECORDED ~y: ,....,.--------------

-

......._ w ~

METHOD NAME AND NUMBER I PRESERVATIVES ANALYSIS ITYPENOL)

C-0-C #

3- 40ML Volatile Organics HC~ pH]< 2, 4°C

AIR BILL#

'·, .. ·~~

CONTAINER LOT#

·, · ..

LABORATORY

IT

~---------------~---------------------r-----------------------------------~----------+--------------------------~---------------------r--------------------~-------------------------+-----------~~4 --.. ~ \N

<'

SAMPLE tO'S . RINSATE: TRIP BLANK: ·· ·· FIELD BLANK: FIELD DUPLICATE:------------------

RECORDED BY: .. ·. . ; OA CHECKED BY: . 1" i!

(SIGNATURE) (SIGNATURE)

I ill:'

" '

.., ~~i I •• • ·~>·· ~~ . -ac;:;.;.~-:-;l!lllt .. 1 • ~ ·.' :

SAMPLE JD NUMBER: NS0304 ------- DATE COLLECTED (MMIOD/YY): ----- TIME:· (HH:MM) --..,.-:;..-~ __ _

MOUND SAMPLE NUMBER: MN016- - 2204 _..•

SAMPLING -

LOCATION CODE: MND16 DESC~IPTION: MOUND OU5 NEW PROEEBTY SEEES .· POINT CODE: TB~ DESCRIPTION: __.T.I.Ijrlp~~-JBwlwan.wk-&Ru4 __ ~--·"_·· ----------

/ ; //

OESCRIPTIOti: ASIM Water ' ,/ DEPTH

SAMPLE -

MEDIA CODE: . 72 TO ·-t /' L

rJ\rt / qv\

·~L ,t/ \1 FIELD MEASUREMENTS READING UNITS 1-1-1-1--

SAP SAMPLING,.,PAOCEDUAE WAS F~LLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------'AS NOT FOllOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

.........

RECORDED By: ------------- QA CHECKED BY:--------------- ~ (SIGNATURE) (SIGNATURE)

..

I i

3- 4oML' Glass

PRESERVATIVES CTYPeivou·

HCL pH<2, 4"C

...

C-0-C # AIR BILL# CONTAINER

LOT# LABORATORY

lT

SAMPLE IO'S RJNSATE: TRIP 13LANK: .: .. FJELD BLANK: FIELD DUPLICATE: ____ ___,... ..... . . ' . .

flECOROED BY: OA CHECKED BY:------------------(SIGNATURE) (SIGNA TUREl

..... __ :- - ; --; =..::. .. , .. : -=~---~~ ~-----~---~ m-_, ....... , ---=-,

-\t ~

- '' ' • • ~.!..,.,!!.llk1!!!!1!. 4 j \ i ----- ---· -·~----.- . • -:.;,__. - .. - ....

SAMPLE ID NUMBER: I NS0401 DATE COLLI;CTED (MMJoD/YY): ------

MOUND SAMPLE NUMBER: MNDHf- - 4201 . I

SAMPLING -

LOCATION CODE: MND16 . DESCRIPTION: ooyunu yuiil m:YY r~P't:O! 1 ;;u:::J:rQ

POINT COpE: ----JAUllu..l ________ _ DESCRIPTION: 011\!Qt\ II: H I J /

SAMPLE- .. MEDIA CODE: 73 DESCRIPTION: QllliJP IIQIPI /

WEATHER: //?: FIELD OBSERVATIONS: _ \.,'All z

DEPTH ____ TO ___ _

SAMPLE TYPE:

GRAB . § SPATIAL TIME COMPOSITE QC TRIP QC RINSATE. QC nt:LJ+QLJ\!'j

FIELD MEASUREMENTS UNITS READING

OTHER (SPECIFY)

SAMPLE COLLECTED: NO

·nuucuunc WAS FO~LOWED? YES NO FIELD C~ANGE ORDER REFERENCE NO: ---------

NOT FOLLOWED, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

~ECORDED By: --------------T-- _OA CHECKED BY:----------------CSIGNATURE) CSIGNATUREJ

~-~

............ ~ ~

3 • 40ML Glass

2- 1 LITER Amber Glass

2 ~ 1 LITE.R Amber Glass

1 - 1 LITER Plastic CLP Metals -1 ~ 1 LITER I Plastic I·Cyanlde

-2- 1 LITER I Amber Glass I Explosives






1 - 1 LITER Plastic Total Dissolved Solids ITDS)

1 - 1 LITER Plastic Total Suspended Solids ITSS)

1 - 1 LITER I Plastic I Total Nitrogen CTKN) -

1 - 1 LITER I Plastic I Total Phosphorus ITP)

1 - 1 LITER I Plastic I Alkalinity -1 - 1 LITER Plastic Ammonia

1 - 40ML ·. Plastic Rad Screen ·. 1 - 2 GAL Plastic Pu,Th,U,Ac,Ra,Sr,Am,Gamma

. PRESERVATIVES ffYPENOL)

HCL pH<: 2, 4°C

COOL 4°C

COOL 4°C

COOL 4°C

COOL 4°C

H2S04 pH< 2,4°C

H2S04 pH<2,4°C

COOL 4°C

COOL 4°C

H2S04 pH<2,4°C

H2S04 pH< 2,4°C

COOL 4°C

H2S04 pH< 2,4~C

COOL 4°C

HN03 pH< 2,4°C

C-0-C # AIR BILL# CONTAINER I LA BORA TORY LOT#

IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT -IT

------~--~-----------+--------~-------+------~~------+-----~~-1 I. I I COOL 40C 0 :I . I I I ... PACE 'I t 1 - 250ML Glass ·Tritium

SAMPLE ID'S. RINSATE: - TRIP BLANK: FIELD BLANK: FIELD DUPLICATE:------i 'p .. . ..

0 •

flECOROED JJY: Q~ CHECI<ED BY:-----------------(SIGNATURE) (SIGNATURE)

I tl 01

. i

------------------~--------~-~~,~-=~-~~ ~ F= • ·- •. -... --·- .. ··-

• ! I • •• \. ' '· : I ~·~ --·· -~ ........ _ .. , . .. . . .. ·-·. ---------··--·~ •

• I

SAMPLE .ID NUMBER:· . NS0402 . .... PATE COUECTED (MMIOD/'(Y)': ------

MOUND SAMPLE NUMBER: MND16- - 4202 . .

SAMPLING -~ ... I . • . . •·

lOCATION CODE: . MND16 DESCRIPTION: MUUI'iU vuil m:vv rn~m:n 1 1 o;u:crt:J I

POINT CODE: _.A..IIJI2.._ _______ _ DESCRIPTION: I I!I'JWQ I h U& , • >

SAM~lE ·-• I

~EDIA qODE: 73 DESCRIPTION: Blose Water 7 /' DEPTH TO ____ _

WEATHER: . . ~

FIELD OBSERVATIONS: . · z '·~ I • / .. .,. .. .. :• .

SAMPLE TYPE: BEADING UNITS GRAB § SPATIALCOMPVOITE TIME COMPOSITE QC TRIP BLANK QC RINSATE QC FIELD BLI-N

OTHER (SPECIFY) / I I I I 7

SAMPLE COLLECTED: ~~ NO

SAP SAMPLING PAOc{o'UAE .WAS FQLLOWED? YES NO FIELD CHANGE ORDER REFERENCE NO: ---------

NOT FOLLOWt:D, SPECIFY WHAT DEVIATIONS WERE NECESSARY AND WHY:-------------

RECORDED By: ; : ·.: (;}A CHECKED BY:---------------(SIGNATURE)· . (SIGNATURE)

-

-... ~ --......

CONT ~INER ·I CONTAINER METHOD NAME AND NUMBER VOLUME . ·-... TYPE ANALYSIS

··-....

3- 40ML. I Glass · ................ Volatile Organics

2- 1 LITER Amber Glass Semt:_Volatlle Organics

2- 1 LITE~. Amber Glass PestlcldeS'-1. P,CBs

1 - 1 LITER Plastic CLP Metals '-.... "-......_

1 ·- 1 LITER I Plastic Cyanide -~

2- 1 LITER I Amber Glass I Explosives '....... --





1 - 1 LITER Amber Glass Total Organic Carbon ITO C)

1 - 1 LITER I Plastic I Total Dissolved Solids ITDS)

1 - 1 LITER I Plastic I Total Suspended Solids (TSS)

1 - 1 LITER I Plastic Total Nitrogen ITKN)

1 - 1.LITER I Plastic Total Phosphorus (TP)

1 - 1 LITER I Plastic Alkalinity

1 - 1 LITER I Plastic. I Ammonia

1 - 40ML, Plastic Rad Screen

1 - 2 GAL Plastic •.. Pu, Th,U,Ac,Ra,Sr ,Am,Gamma

1 - 260ML . 1 Glass . ·1 Tritium·

SAMPLE ID'S RINSATE: ... · · · TRIP BLANK:

RECORDED BY: (SIGNATURE)

...

PRESERVATIVES I . (TYPENOLI .. C-0-C #

HCL pH<2, 4°C I

COOL 4°C I

COOL 4°C I

HN03 pH,2, 4°C I

NaOH pH> 12,4°C I

. COOL 4°C I

I C06L 4°C I

I COOL 4°0..... ( I I

I COOL 4°C ~J

I H2S04 nH<2.4°C I ""'- ·'

I H2S04 nH<2.4°C I " COOL 4°C I

COOL 4°C I

H2S04 pH< 2,4°C I

H2S04 pH< 2.4°C I

COQL 4°C I

H2S04 pH<2.4°C I

COOL 4°C

HN03 pH< 2,4°C

I COOL4°C I FIELD BLANK: '.

OA CHECI<ED BY: ..

'

I . I· CONTAINER AIR BILL#

LOT#

I I

I I

I I

I I

I I

I I

I ..

' ' I

I I

I I

I I

"l I

I " I

I ' I

I 'k

I I --..... ..

I I '

FIELD DUPLICATE:

(SIGNA TUREI

'·-----------· ··-·- ··--.

I LABOR A TORY

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

I IT

~ ~

I 1 " 'I

I

tt••t,,

DATE EQUIPMENT RINSATE NO. ITEMS OECONEO BY

··--~----~--~--~--------r-~ .....

35: CITY: STATE;

IZATION:

55: CITY: STATE:

ZIP:

L/5

ZJP:

DATE CONT ACTED:(13-30-<=i"/ Ci3·31-~'/

Telecon:{ZJ Vis itO

DATE CONTACTE0:3-3o .,.~'/ 3·31-6/f'l

Telecon:f!:r. Visit{]

COMMENTS, ACTION, OATES .

•

•

•

•

•

•

APPENDIX C

ADDENDUM

NEW PROPERTY SOIL GAS SURVEY REPORT

•

. '

· NOV 30 '94 06:43PM . .

· November 30, 1994 ·

Mr. Thomas Tank Science Applications· lntemationat Corparation · 4031 Colonel Gl~ Jfiibway, sUite 300 Beavercreek, Ohio 4S43t-.i600

Dear Mr. Tank:

~.V:i

605 Parfet Street • SUite 100 . · LakewOOd., Colorado 802 fs

303-238.:0090. 800-845-5137. F~ 303-2~8-2522 .

Tel: . (513) 429-2699 ~ax: ·: (~13) 4~~-:-9557

I. ain. writing· to fOrmally repOt:t the reSults· of the Petrex soil gas sur.vey at the· New Pi-openy pf . the USDOE MouD.d Facility for Total Semivolatile .Hydrpcarbom· arid: Oil & .Grease .. Range · Hydrocarbons. ·

T~ date, resul~ for. Total Petroleum ·Hydrocarbons (divided·into the ~oups: aro~tics, anti . cycl<ialkaDes/alkenes) and Total Halogenated Hydrocar~on5. (as· responSe to PCE) have· been ·

·reported. Survey results for To1al Senlivolatile Hydrocarbons is presented iri Table 3 ·. {attached). To1al semivotatile. hydrocarbons are reported ~.the eombined response to naphthalene, Cl.t ~ · C15 ·alkyl naphtba.lene8; an4. Ct2· .ql4•· ~ Ct6 · polycyclic. · hydrocarbons. These coinpounds are. constituents of c!CQsote, ~ tar, and other heivy, high · · . belling poi:(lt fraction petroleum products. Naphthalene, and Cu a.Dd Cti 8.lkyl naphthalenes .. (e.g., methylnaphtbalene and ethyl- or dimethylnaphthalene) are alsp often found in medium to heavy weight fu~ and hf:ating oiis. ·. · · ·

' .

·OoJy low relative -levels .of Semivolatlle compoun(ls were detected ui·the soil g~ and only in a , small perCentage of the samples'. A . review. o( the mass. spectra of ·a11 ~amples. indicated that very few semivoiatile compoun4s are present in the soil . gas, and that . the majority of the responses ckrive from ~ presence of lighter. wei~ compounds particularly. nap4thalene .~ ·

. methylnapbtbalene-: ·The occurrence of these semivolatiles in Petrex soil. gas s~ples is ·.shovin in the mass gpecu:a of samples #13ifand #155 (a~hed).·. · ·

.. P~REX· ·~oil Gas :re~~~logy • Environmentiu ·&·Resource lp:yestigations . @ ~

•

•

•

NOV 30 '94 . 05:44PM

Mr.· Thomas Tank · November 30, 1994 Page.two· ·

. The highest level of SemivQlatile Hydrocarbons .(naph~ene and ·methylnap~ene) were detected in samples #67, and #91. Most samples containing semivolatile hydrocarbons wc;re· . collec~d pmicipally from the central and nrirtnem portions. of are site. ·,Three sampl~·. #136, ... #139, and #140, .Were collected from po~ .located On· the edge Of the accesS· road which defmes the northern margin of the property. Low level detections. in these samples. may derive · · from the use of petroleu.m in ~ area.· As· indieated ·by·. 'I.'ab~e 3, :overall .rCsponse ·to Semivolatile· Hydracarbons·in the soil~ as detected by thiS sm-Vey was so low as to not I#erit· .mapping. . . . .. . . .

A careful review of restiltS .for all soil gas samples ·indicated that no Oil:& Grease. Ra"nge HydrocarbonS (represen~ ·by · C13, Ct4 •. and · C1s ·. alkanes, cyc.lo~," .. alkelies·, cycloalkenes, dienes,· and.alkynes) w~re de~ in the' soil.gaS. Tlnis,. runable of resul~ and no map of areal distribution was gen~ied for these ~ytes. · . · . . . · · : · ·

Please attach this :Ie~r. ·Table 3, and the· mass. spectn of saniples ~138 and· #155 as· an.· addendUm to the final. report dated April ~3, .1.994. Also, please call me· if I ·can assist you ·further in·th~ evaluation of survey.fmdings~ ·

. . Since.-~ly,

ProjectMaDager

enel. ..

· .

••

. NOV 30 '94 ~: 44PM :

··Table 3: New Property Petrex SUrvey Results for Se~ivol.atiJe-Hydrocarbons . . .. -· . NERI Project: 2043-1E

Site: Operable Unit ·5, USQOE Mound Facility Analysis: Thennal DesOrption -·Mass Spectrometry . _Date of Analysis: 3110/94 . · Units: lon Counts

Sample_#

:1_

-Z 3 4 -5 e· 7 8

.9 10

·.11 .12.

·13 14 j5 16 17 18 19

. 20

Z1 . 22 23 24.

. 25. 26

: 2.7 28

"29

Total Semivolatile Hydrocarbons (a)

NO ~0 NO

·NO NO NO NO

"NO . 1,245

NO NO NO .. NO NO

·No -NO NO

8,163 . 1,224 .

NO NO

1".308 NO NO NO NO NO

1;029 ·No·.-

P.4/9 . . .

605 Parfet Street • SUite 100 Lakewood, ColoradQ 80215

~03-:238-:0090. 800-845-5137 · .Fax 303-238-25~2

' '' ..

•--------~~----~~-. PETRE.X Soil Gas Technology_ • .EQ:virom~erital & Resource Investigations _(i} ·

NOV.30 '94 ~:45PM P.S/9

• Table 3 (confd) ·

Total Semlvolatile Sample# . Hydro~s·. (a)

30 NO 31 NO 32. NO· . .

33- NO 34 875 35 NO 36 ·NO· 37 NO· .. 38 ND . -39. NO ..

40 NO. 41 NO 42· NO 43 NO 44 1,632 45 ~--46 NO 47 NO

• 48 Nl:> 49' NO 50 NO . . .. 51 ND 52 NO. 53 .No 54 NO 55- 1,080. 56 1,209 57 NO 58 · .. NO ..

59 NO 60 NO 61 NO 62 NO

·63 NO 64 No· 65 NO. 66- NO 67 10,454

'68 1'10 69 NO-

•• . .

· Page~of4 ·.

NOV 30 '94 05:45PM · · P.6/9

•• T~l~ 3 _(c:Ont'd) Total Semivotatae

. Sam~le# HydrOcarbons . (a) .

70 NO 71 NO 72 NO 73 3,249 74 NO· 75 NO

.. 76 NO ·7i NO

78 NO 79 4,758 80 NO 81 ·No· .... ·82 3,063 ..

. ..

83 NO 84 NO ..

85 NO 86 NO 87 ... NO Sa·

.. NO

• 89· . NO 90 NO 91 11,811 .

.92 NO "93 .NO 94 NO 95 .2.473 96 ND

. 97 NO .98 ND

99 NO 100 3.~ 101 NO .. f02 NO

.103 NO 104 NO 105· NO' 106 NO· 107 ·NO 108 Ne

•109 NO 110 NO ..

..

•• Page_3of4 ..

•

•

••• •

NOV 30 '94 06:45PM

. Table 3 (confd) "To~ Semivotatlle

Sample# Hydrocarbons (a)

11.1 .. NO

112· ·NO 113 N[} 114 NO 115 3.~ . 116. . NO."· 117 NO. 118" NO 119 NO 120 ND-121 "NO

. 122 ND-123 NO 124 NO ..

125 . 806 126 NO 127 NO 128 ·NO-·. 129 NO

·130 ·.NO 131 NO 132 5,069 133 NO 134 NO 135 NO 136 . 5.~86 137. NO 138 . 879. 139 6,713 140 . 4,899

141 ·NO 157. NO· 158 • NO 159 •· NO 160 * NO

Key: (a) in~nSftY of ~pcnse to icris of atomiC m8sses128, 142. 1_"53; . . 156, .178, -t84. 198, 202, a_nd 212. . . . .

NO Targeted compounds were ~ detected in this sample. • Travel Blank

Page.4cf4

' ..

P.?/9 .

...

.·

PlotData Page: 1 >·~ 0 4 3 . 1

~ Sample Nun~

0138: Scan Avg 1-20 (0.01 - 0.14 min) Q. 35000

5.5

30000

25000

~ 20000 Vl

z 0 fl-o tl) 15000 ~

~ I Ill

78 ~ 10000 i . Ill I I 9.1 > H

E-t <

E: ....:I 5000 Po ~

J ~ 11~1. I ~l~~l,l, Jl,, . . , 1~ ~a~tha~e~ ':t p::

~ ':t I I 0"1 ..

20 so 100 150 200 250 280 ~

2 ATOMIC M A:S S

• • •

PlotData 2 0 4 3 • i

Page: 1

~ 0155: Scan Avg 1-20 (0.01 - 0.14 min) a.

300000

·:

57 250000

200000

150000

69 91

100000 -

~ 50000

'!i

~Methylnaphthalene

1~

.. ~

~ 0 I I d II I I Ill •••

I I I I

'

~ 20 so 100 150 200 250 280

~ z

• • •

•

APPENDIXC

SOU.. GAS SURVEY REPORT

•

•

• FINAL REPORT ON THE FINDINGS

OF THE PETREX SOIL GAS SURVEY CONDUCTED FOR

SCIENCE APPLICATIONS INTERNATIONAL CORPORATION

AT THE MOUND PLANT LOCATED IN

MIAMISBURG, OHIO

PREPAREDBY: DATE:

• . On '"1'Yia±hv.vJ.,:4/} - -4'/3J?4 ~eney-Rood, Project~er -----------

APPROVED BY:

•

DATE:

NORTiiEAST RESEARCH INSTITIJTE 605 PARFET STREET, SUITE 100

LAKEWOOD, COLORADO 80215 (303) 238-0090

0494-2043£

Miamisburg, Ohio 04/13/94

TABLE OF.CONTENTS

• 1.0 EXECUTIVE SUMMARY 1

2.0 INTRODUCTION 2

3.0 OVERVIEW OF THE PETREX TECHNIQUE 2

4.0 OBJECTIVES 3

5.0 SCOPE OF WORK 3

6.0 FIELD ACTIVITIES 3

7.0 tv!ETHOD QA/QC 3 7.1 Lot Control 7.2 Travel Blanks

8.0 DISCUSSION 4 8.1 The Distribution of Aromatic Hydrocarbons 8.2 The Distribution of Cycloalkanes/ Alkenes

• 8.3 ID-GC/MS Results

9.0 CONCLUSIONS 6

10.0 RECONIMENDATIONS 6

11.0 LIMITATIONS 7

APPENDICES

A. PETREX Protocol B. Sample Mass Spectra C. Table 1 D. Plates 1-3 E. Histograms F. ID-GCIMS Results

• Northeast Research Institute LLC

•

•

•

:Miamisburg, Ohio 04/13/94

1.0 EXECUTIVE SUMMARY

Nonheast Research Institute (NERI) and Science Applications International Corporation (SAIC) recently completed a PETREX Soil Gas Survey at Operable Unit 5 (OU5), New Property Site, at the U.S. Department of Energy's Mound Plant located in Miamisburg, Ohio. Compounds of concern at this site included a variety of hydrocarbons and chlorinated compounds.

The purposes of the PETREX Soil Gas Survey were to identify the variety of hydrocarbons and chlorinateds in the soil gas, to identify potential source areas for these compounds, to determine preferential migration pathways and areal extents of these compounds, and to provide guidelines for the placement of follow-up soil borings and monitoring wells.

The C6-C11 aromatic hydrocarbons, predominantly benzene, toluene, ethylbenzene, and xylene(s) (BTEX), and the C4-Cs non-aromatic hydrocarbons were detected in the soil gas. The cycloalkanes/alkenes were selected to represent the C4 -Cg non-aromatic hydrocarbons due to their predominance on the spectra. The distributions of these compounds were mapped and potential source areas identified. In addition to hydrocarbons, elevated relative response levels for tetrachloroethene (PCE) were detected in the soil gas at two sampler locations.

Primary potential source areas for the aromatic hydrocarbons appeared to be located at the southwest and southeast comers of the site. Additional potential source areas for the aromatics, as indicated by slightly lower relative response levels, are located along the eastern and southern ;ite boundaries. Migration direction for the aromatics appeared to be in a general northeastsouthwest trend and may extend beyond the survey boundaries to the west, south, and east. The more significant potential souree areas for the non-aromatic hydrocarbons appeared to be located along the eastern site boundary and along the eastern boundary of Area 1 near sampler location 115. Additional potential source areas, as shown by slightly lower relative response levels, were located randomly throughout the southern half of the survey area_ Migration direction for the non-aromatics appeared to be in a general northeast-southwest direction and may extend beyond survey boundaries to the southwest and east. Elevated relative response values for PCE were identified in the soil gas at sampler locations 4 and 13. These incidences of elevated responses for PCE appeared random and discrete in nature •

Northeast Research Institute LLC 1

j

•

•

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04/13/94

2.0 INTRODUCTION

Northeast Research Institute (NERI) and Science Applications International Corporation (SAIC) recently completed a PETREX Soil Gas Survey at Operable Unit 5 (OUS), New Property Site, at the U.S. Department of Energy's (DOE) Mound Plant located in Miamisburg, Ohio. According to SAIC, the survey area was formerly a farm site and was subsequently acquired and maintained by the DOE as a vacant field. The Mound Plant proper exists to the north of the vacant field and survey area. Groundwater direction is believed to be in a northeast/southwest direction. The properties surrounding the survey area consist of light industry to the west and farms and houses to the south and east.

3.0 OVERVIEW OF TBE PETREX TECHNIQUE

Each PETREX soil gas sampler consists of two or three activated charcoal adsorption elements (collectors) housed in a resealable glass container in an inert atmosphere.

Soil gas sample collection is performed by unsealing the sampler and exposing the collector to the soil gas of the subsurface environment at the base of a shallow borehole. Sample collection proceeds via free vapor diffusion through the opening of the uncapped sampler container. Following a controlled period of time, the sampler is retrieved from the borehole, resealed, and submitted for analysis.

One collector from each soil gas sampler is analyzed by Thermal Desorption/Mass Spectrometry (TD-MS). Selected second collectors may be analyzed by Thermal Desorption-Gas Chromatography/Mass Spectrometry (TD-GCIMS) for compound confum.ation. At least ten percent of samplers used in any project are three collector samplers. The third collector is used for setting instrument sensitivity prior to analysis. Fourteen samplers were submitted for 1DGCIMS analysis, and results are discussed in Section 8.3 of this report.

Compounds are identified by comparison to standard reference spectra run on the same instrument. The mass spectral ion count of the appropriate indicator peak(s) for each compound or group of compounds is then plotted as relative response on a map and contoured using a variety of standard geostatistic:al analyses.

For a more detailed and tecbnic:al discussion of the method, please refer to Appendix A, PETREX Protocol.

Northeast Research IDstitute LLC 2

•

•

•


4.0 OBJECTIVES

The purposes of the PETREX Soil Gas Survey were to:

1. Identify the hydrocarbons and chlorinated compounds in the soil gas;

2. Identify potential source areas and determine preferential migration pathways of the identified compounds; and

3 · Provide guidelines for the placement of follow-up soil borings and monitoring wells.

5.0 SCOPE OF WORK

A total of 141 PETREX soil gas samplers were utilized for this. soil gas survey. The survey was designed by SAIC with sampler frequency approximately every 200 feet. The sampler locations are displayed on Plate 1, Appendix D.

6.0 FIELD ACI'IVITIES

Sampler installation was performed by a NERI Senior Geologist and personnel from SAIC who were simultaneously trained by the Geologist in the methods and protocols associated with performing a PETREX Soil Gas Survey. Sampler retrieval was performed by SAIC. According to field notes from SAIC, the samplers wete installed between February 21 and 24, 1994, and retrieved between March 7 and 8, 1994.

Sampler exposure time was determined by the use of time test samplers (time tests). !me test samplers were installed concurrently with the survey sampler installation and removed for analysis following varying exposure periods. The purpose of the time test samplers was to assess the loading rate of Volatile Organic Compounds (VOCs) and Semi-Volatile Organic Compounds (SVOCs) onto the PETREX collectors. Based upon the analyses of time test samplers, an exposure period of approximately 2 weeks was determined adequate to allow for an accurate interpretation of the data.

7.0 METHOD QA/QC

7.1 Lot Control

Quality assurance/quality control (QA/QC) collectors from each lot manufactured by NERI were analyzed by ID-MS to ensure that they were contaminant free before the lot of collectors used in the field was released from the PETREX laboratory. No compounds were detected above background on the QA/QC collectors .


•

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•


7.2 Travel Blanks

Four PETREX samplers were provided as travel blanks. These travel blanks remained sealed and traveled mth the survey samplers from the laboratory to the field and back to the laboratory to monitor for potential contamination of the survey samplers. The travel blanks were analyzed under the same instrument conditions as the survey collectors. Results of ID-MS analyses of the travel blanks for the targeted compounds are provided in Table 1, Appendix C.

A more detailed description of the PETREX QAJQC may be found in the PETREX Protocol located in Appendix A.

8.0RESULTS

The C6-Cll aromatic hydrocarbons, predominantly BTEX, and the C4-Cs non-aromatic hydrocarbons, represented by the cycloal.kanes/alkenes, were detected in the soil gas. The distributions of these compounds were mapped and are displayed on Plates 2 and 3, respectively, in Appendix D. Contouring intervals for Plates 2 and 3 were determined by breaks exhibited in the data and are displayed on the histograms included in Appendix E.

Plate 1: Sample Locations Plate 2: Relative Response of Aromatic Hydrocarbons Plate 3: Relative Response of Cycloalkanes/ Alkenes

-In addition to the presence of hydrocarbons, elevated response levels for PCE were detected in the vicinity of sampler locations 4 and 13. These occmrences appeared to be random and discrete and were not mapped. The ion counts for PCE (indicator mass peak 164) for the above listed samples were 660651 and 1838440, respectively.

The response values are reported in ion counts and are presented in tabular format in Table 1, Appendix C. Ion count values are the unit of measure assigned by the mass spectrometer to the relative intensities associated with each of the reported compounds. These intensity levels or response levels do not represent an actual concentration of the reported compounds; however, they are best utilized as a semiquantitative measurement. A difference in ion count values of an order of magnitude or more is considered significant wnen interpreting potential source areas and migration/dispersion pathways versus background areas.

Example mass spectra of the compounds identified are provided as Figures 1 and 2, Appendix B.

Table 2 lists the reported compounds and the· indicator mass peaks which were summed to represent the compound occum:nces reported on Plates 2 and 3 .

Northeast ReSearch Institute LLC 4-


TABLE2

• REPORTED COM:POUNDS AND THEIR INDICATOR MASS PEAKS

Compound

C6-C 11 Aromatic Hydrocarbons C4 -Cg Cycloalkanesl Alkenes

8.1 The Distribution of Aromatic Hydrocarbons

Indicator Mass PealcCs)

78,92,106,120,134,148 56,70,84,98,112

The distribution of the aromatic hydrocarbons in the soil gas was mapped and is displayed on Plate 2, AppendiX D. Primary potential source areas for the aromatic hydrocarbons appeared to be located at the southwest and southeast comers of the survey area. Additional potential source areas for the aromatics, as indicated by slightly lower relative response levels, were located along the eastern and southern site boundaries. Migration direction· appeared to be in a general northeast-southwest trend and may extend beyond the survey boundaries to the west, south, and east.

The relative response values reported at sampler locations 26, 36, and 67 were elevated due to interference associated with terpene compounds. Terpenes generally are naturally existing vegetative compounds whose molecular weights and fmgmentation patterns exist within the same molecular weight range as some of the aromatic hydrocarbons, thereby either masking the

• identification of the aromatics or elevating the reported values. Terpenes can, however, also be associated with a refined product such as turpentine. As a result, the samplers identified with terpenes were contoured on Plate 2, Appendix D, relative to surrounding, non-terpene interfered

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samplers. These samples were denoted by the letter "T".

8.2 The Distribution of Cycloalkanes/ Alkenes

The distribution of the C4-Cs cycloaikaneslalkenes in the soil gas was mapped as displayed on Plate 3, Appendix D. The more significant potential source areas for the non-aromatic hydrocarbons appeared to be located along the eastern site boundary and along the eastern boundary of Area 1 near sampler location 115. Additional potential somce areas, as shown by slightly lower relative response levels, were located randomly throughout the southern half of the survey area. Migration direction for the non-aromatics appeared to be in a general northeastsouthwest direction and may extend beyond SUIVey boundaries to the southwest and east.

8.3 TD-GC/MS Results

Fourteen samplers (4,13,15,16,18,23,30,31,32,36,38,49,51,57) were submitted for ID-GC/.MS analysis. One sampler, #57, was not able to be analy.zed, and as a result, only 13 samplers were reported. The purpose of the analyses was to confirm the presence of aromatic and nonaromatic hydrocarbons and PCE.


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04/13/94

The aromatic hydrocarbons, including BTEX, were confumed present on all 13 samplers

• analyzed. The cycloal.kanes/alkenes were only confumed present on samplers 31, 32, 36, 49, and 51. Since the cycloalkanes/alkenes were not detected on all samplers submitted for 'IDGC/MS analysis, minor modifications were made to the cycloalkanes/alkenes map (Plate 3, Appendix D). The non-aromatic hydrocarbons classified as alkanes were detected on samplers 49 and 51. PCE was confirmed present on samplers 4 and 13. PCE was also detected on sampler 23, which was not previously identified present, albeit at significandy lower amounts than 4 and 13. Trichloroethene (TCE) was detected on sampler 13, and terpenes were confirmed present on sampler 36.

9.0 CONCLUSIONS

The C6-C11 aromatic hydrocarbons and C4-Cs cycloalkaneslalkenes were detected in the soil gas. Based on the contouring of Plates 2 and 3, the potential source areas for the hydrocarbons did not appear to be associated with the Moimd Site proper. The potential source areas appeared predominandy along sun'ey boundaries in the southwest and eastern portions of the Sun'ey area. In addition to the hydrocarbons, elevated relative response values for PCE were detected in the soil gas at sampler locations 4 and 13. m-GC'M:S analyses confirmed the presence of a variety of hydrocarbons, PCE, TCE, and terpenes.

10.0 RECOMMENDATIONS

• ~:S~~on the findin~ of the PETREX Soil Gas ~urvey ~e-following recommendations can

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1. Extend the soil gas Sun'ey to the west, south, and east in areas where contaminant migration appeared to extend beyond current sun'ey boundaries. This additional sampling will provide data to help determine the areal limits of contaminant migration and define additional potential source areas.

2. Perform subsurface borings and piofiling of soils in areas of highest soil gas response to determine the vertical extent of chemical dispersion and aid in characterizing the environmental sigciiicance of the highest soil gas response levels. If the highest soil gas response levels are representative of environmentally significant subsurface contamination. then subsurface profiling should be performed in the intermediate or lower response levels until background conditions have been determined.


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11.0 Lll\fiTATIONS

.This report represents NERl's professional interpretation and judgment based on technical information gathered during investigative activities. Professional judgments expressed herein are restricted to facts available within the established limits of the scope of work, budget, and schedule. NERI assumes no responsibility for the existence or disclosure of conditions which did not come to its knowledge, or conditions not generally recognized as environmentally unacceptable, at the time this report was prepared.

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It is NERI's specific intent that all observations and conclusions presented will be used as a guide and not necessarily a firm course of action. unless explicitly stated as such. No warranties are expressed or implied and the information included in this report is not to be construed as legal advice .

F2043JR/04.13.94 • Northeast Research Institute LLC 7

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Northeast Research Institute LLC

APPENDIX A PETREX Protocol

04/13/94

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REVISED SEPTEMBER 1993

PETREX ENVIRONMENTAL SOIL GAS PROTOCOL

INTRODUCTION

The PETREX Technique provides a means by which trace quantities of gases from subsurface derived organic contaminants can be detected and collected at the earth's surface. The Technique is integrative, thereby eliminating the short-term variations associated with other gas/vapor detection methods. The PETREX Technique directly collects and records a broad range of organic compounds emanating from subsurface sources.

SOIL GAS COLLECTOR PREPARATION

Adsorption collector wires (after const:IUCtion) are cleaned by heating to 358° C in a high vacuum system. Wires are packed under an inert atmosphere in glass culture tubes. One collector out of every batch of thirty is checked for cleanUness by mass spectrometry. Another collector from the batch is checked for adsorptive capability. Based on the results, the batch of collectors is approved for release into the field .

SOIL GAS SAMPLER INSTALLATION

The sampler consists of two or three collectors, each a ferromagnetic wire coated with an activated charcoal adsorbent in a screw top glass culture tube. Each sampler is typically placed in a shallow hole, 14-18 inches deep. The hole is backfilled and the location is marked. The sampler is left in the ground from one to thirty days, then retrieved and sealed for transportation back to the laboratory for analysis. ·

The PETREX soil gas sampling technique is adaptable to various surface com:titions commonly encountered within survey areas. These surfaces typically include concrete, asphalt, grass, and gravel. Two installation methods are routinely utilized to adapt to these surface conditions.

The fli'St method utilizes a coring shovel for sampler installations in grass or otherwise loosely consolidated soil conditions. The shovel cores a 14 inch deep by 2 inch diameter hole in the surface soils.

PETREX soil gas samplers are placed (open end down) at the bottom of each core hole. The samplers are then backfilled with an aluminum foil plug and the original excavated soil. To complete installation, sample locations are marked with ribbon flagging and a numbered pin Jag, as well as entered into a field notebook and plotted on a field map.

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The second method of sampler installation utilizes an electric rotary hammer, equipped with an 18 inch by 1.5 inch diameter drill bit, for sampler installations under concrete, asphalt, or otherwise consolidated conditions. A hole is drilled through the surface to the dimensions of the drill bit equipped to the rotary hammer.

PETREX soil gas samplers are placed at the bottom of each drilled hole. For retrieval purposes, a cleaned galvanized steel wire is attached to each sampler. Aluminum foil is used to plug each hole to approximately two inches below grade. Then each hole is capped to grade with hydraulic cement. The hydraulic cement serves as protection from the external surface environment.

To complete sampler installation, sampler locations are marked with paint (where applicable), entered into a field notebook, and plotted on a field map.

SOIL GAS SAMPLER RETRIEVAL

PETREX soil gas samplers are retrieved following a time period that has allowed for the soil gas emanating from the subsurface environment of a survey area to equilibrate with the installed PETREX samplers. This time integration period is determined for each PETREX soil gas survey based on time calibration data or site conditions.

Retrieval operations are dependent on surface conditions and routinely consist of the following two methods.

The firSt method applies to grass covered or loosely consolidated soil conditions. A trowel is utilized to expose the backfilled samplers; then with a pair of tongs, the samplers are brought to the surface. At the surface, the samplers are sealed, cleaned; and labeled. Following retrieval, all debris are gathered and the core hole is backfilled with original material.

The second method applies to concrete, asphalt,· or other consolidated surface conditions. A hammer and chisel is utilized to remove the hydraulic cement plug and expose the sampler. By means of the pre-attached retrieval wire, the sampler is brought to the surface. At the surface, the retrieval wire is removed and the sampler is sealed, cleaned, and labeled. Following retrieval, each drill hole is backfilled and patched with cement or asphalt.

TIME CALmRATION SAMPLERS

Time calibration samplers are included in PETREX soil gas surveys, as appropriate. These samplers are included as a means of monitoring the loading rates of volatile and semivolatile organic compounds (VOCs and SVOCs) emanating from the soil gas at a survey area onto the PETREX collectors .

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During PETREX sampler installation. two sets of three to five time calibration samplers. are also installed at survey sample locations that best represent the range of soil gas response for the survey area. These representative locations are determined based on previous soils and/or groundwater smdies and other site specific conditions such as gradient and potential source areas.

The fll'St set of time calibration samplers are generally retrieved within a week or less following the initial installation and the second set one week later. Often., permanent on-site personnel are instructed to perform time calibration sampler retrieval.

Lengths of exposure periods of the survey samplers for each survey are determined baseci on the results of each respective set of time calibration samplers. Time calibration samplers are usually analyzed within 24 hours upon receipt at the laboratory. At the first indication of

. significant relative ion count intensities and significant total ion count values, the decision is made to retrieve the entire complement of survey samplers.

If there are no significant relative ion count intensities detected from the second set of time calibration samplers, then the survey samplers are allowed to equilibrate in the field for a maximum time period of up to 30 days. The average environmental PETREX soil gas survey requires a collector integration period of one day to two weeks.

METHOD OA/QC

Within _ey~ry $11n'eY .sampler,. the two or three collector wires should have adsorbed identical compounds. Like compounds on separate collectors relate an acceptable quality assurance (QA) during the survey's analysis. The first wire is analyzed by Thermal Desorption/Mass Spectrometry (TDIMS). The data from the first wire is reported on the relative response maps. The second wire is retained for analysis by Thermal Desorption-Gas Chromatography/Mass Spectrometry (TD-GC/MS), if warranted by the initial TDIMS analysis of the second wire.

Approximately ten percent of the total PETREX survey samplers contain tbree collector wires. The third collector wire, a QC collector wire, is used by the operator to test the mass spectrometer's operating conditions prior to survey analysis. Some of these quality control (QC) collectors are also used to check the mass spectrometer sensitivity during survey analysis. In addition., the QC collector may be used to compare the reproducibility of the • · · detected VOCs .

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TRAVEL BLANKS

• Two PETREX samplers, each containing a single collector wire, are included with each PETREX soil gas survey as travel blanks. These blanks are analyzed with the survey samplers to indicate whether there may have been contamination introduced to the survey samplers during installation or shipment. If compounds other than normal aanospherics (e.g., CO:z, H20, N2, and Ar) are detected on the blanks, these results are taken into consideration in the data presentation. This process, an initial step to data interpretation. involves the correction of ion count values of the detected blank contaminants from the entire survey's data set. The resulting ion count values are provided on the relative response maps.

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MASS SPECTROMETER TUNING

An Extranuclear Quadrupole C-50 Mass Spectrometer or similar instrument, equipped with a Curie-point pyrolysis/thermal desorption inlet, is used for collector analysis. Mass assignment and resolution are manually adjusted using a Perfluorotributylamine (PFTBA) standard or a built-in tuning program, depending on the insa:umem. A linear correction, based on the known spectrum of PFTBA, is calculated. This correction is applied to a second PFTBA spectrum. If correct mass (M/Z) values are obtaiiled, the operator proceeds to the next tuning step. If not, Step 1 is repeated until correct masses are obtained.

l?eak intensity ratios are set from the major peaks in the PFTBA spectrum using the following values:

Mass Spectrum !MlZl IDtCDsitics 69 - 100% 131 = 48% .±5% 219 = 50% .±5%

During tuning. the ion signal for mass (MIZ) 69 of PFTBA is measured at a preset sample pressure and detector voltage and compared to previous values at the same setting.

Electron energy is set to 70 electron volts. All other operating parameters, such as scans, scan range, and mass offset, are established in the computer program. These values may only be changed by the laboratory manager.

Tuning ·is performed at the beginning of a nm so that an individual survey is analyzed at the same set of instrumem conditions. The samplers are analyzed in random.order •

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LABORATORY ANALYSIS

• Periodic machine background and blank PETREX collector analyses are performed to assure that there is no carry-over between successive collectors. If there are peaks presem which are not related to atmospheric gases, the supervisor is notified and the mass spectrometer is shut down and cleaned as necessary.

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A written sample number record is kept during the analysis to prevem accidental cross numbering. The mass spectrometer control program contains appropriate "flag statements" that prompt the operator with a warning if an input sample number has already been analyzed. The operator then checks the current number, along with the disk storage location of the previously emered number to identify the true ~bering situation.

COMPOUND IDENTIFICATION

Compound identification is based on molecular weight, compound fragmentation, and isotope distribution, as applicable. Each VOC exhibits a unique mass spectral signature. NERl maintains a large library of spectra of individual compounds, accessible by computer. In addition, the company maintains a large library of mass spectra of commonly used chemical mixtures; e.g., gasolines, diesels, industrial oils and solvC?nts, coatings, plastics, etc. These spectra are used to assist in both compoWld and mixture identifications .

The ion coum response of an indicator peak(s); representative of the compound and away from interference by other compo'Wlds,_is _extracted for __ data presentatio_n and mapping.

INTERPRETATION OF SOIL GAS DATA

Soil gas data (including PETREX) reflect volatile and semivolatile organics collected at a point in the near surface. The sources of these volatile organics may be in the stratigraphic column and/or in groundwater below the collection point. Thus, the organics can be derived from surface spills, deposition, or migration into the deeper vadose zone, and groundwater. The soil gas survey reveals the mal extent of contamination and- is the optimum guide in identifying areas in order to develop a vertical profile, inCluding the drilling of soil borings· and monitoring wells.

Soil gas data are always semi-quantitative in that multiple sources in soil and/or groundwater cannot be differentiated. However, the higher ion responses are representative of higher concemrations in the subsurface, given that geologic conditions are relatively consistent.

Due to chemical differences between individual compounds, including their ability to both adsorb and desorb from the charcoal PETREX collector element, it is invalid to compare the

• ion count of a compound at oue sampling location to tbat of another compound.

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Patterns of compound distribution in the soil gas, as detected at the surface, can be strongly influenced by irregularities in the near surface and subsurface environment through which the soil gas diffuses. These irregularities include subsurface man-made structures, such as concrete foundations, drainage systems, and wells, and such naturally occurring structures as

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fractured and unfracmred bedrock, clay, and shale lenses.

Other factors influencing the soil gas signal include ground and surface water, the free carbon content of soils, microbiotic activity in the soil, and natural and synthetic ground cover.

All of these factors indicate that the most powerful use of soil gas data is in reconnaissance; identifying and mapping the relative abundance of the widest amy of chemical species and mixtures. Efforts to relate soil gas response directly to groundwater or soil contaminant concentrations is generally not regarded as productive owing to the assumptions that are required for heterogeneity and source distribution.

RELATIVE RESPONSE DETERMINATION AND MAPPING

The relative response values are reported as the ion counts of indicator peaks for any given compound or mixture. Sample locations on a base map are digitized as X-Y coordinates and ion coums for the reported compounds are plotted at respective locations •

~pping_ of the ion counts occurs after contour intervals for each compound or component class are deten:nined •. ··rn. orcter tO eStablish 'tlie coritour intervals, faCtors such as statistical analysis ·or ion count-distribution~· ·-physiochemical considerations, and component-source material relationships (if known) are taken into account for each compound or class, in each area, on an individual basis. Each map is then contoured by hand. The resultant contour zones for each compound or component class in each area are color coded on a relative basis depending on whether the data are interpreted to be of high, moderate to high, moderate, etc., intensity. . The response values found on each of the response maps are color coded and contoured on this basis •

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Miamisburg, Ohio


APPENDIXB Sample Mass Spectra

04/13/94

PlotData

• 6000000

5500000

- 5000000 ~ ;:::)

4500000 8 :z:

4000000 0 ...... z

3500000 ...... -t:rJ U'l 3000000 ~ fa 2500000 = t:rJ 2000000 > ...... H

~ 1500000

= 1.000000

500000

0

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•

2.0

2.043. i l::'a.ge: .1.

0161: Scan Avg 1-20 (0.01 - 0.14 min}

50

119

Ethylben ene/Xylene(s)

5

Toluen

1.00

1 3

10

l.SO

A'IOMIC MASS

Fi~e 1

c6-c11 Aromatic Hydrocarbons

2.00 250 2.80

.. ...

- PlotData

• ~ :z: ~ -

•

•

2.000000

1500000

1000000

500000

20

2043· 1

0050: Scan Avg 1-2.0 (0.01 - ·0.14 min) c4

6

so l.OO 150 200

ATOMIC MASS

Page: 1

Figure 2

C4-c8 Cycloalkanes/Alkenes

250 280


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APPENDIXC Table 1

Relative Ion Response Levels for Iden~ed Compounds

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TABLEl MOUND PLANT Miamisburg, Ohio

• Relative Response Levels (In Ion Counts)

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SAMPLE AROMATICS CYCLOS

1 28820 56257 2 158121 556829 3 64208 460380 4 84661 ND 5 7456 17092 6 72344 81012 7 45521 208179 8 53574 91910 9 4248 23497 10 42266 74391 11 173618 279814 12 41678 127612 13 34578 ND 14 119076 141719

• 15 446959 ND 16 235840 .. ND

·17 • , • * • • ~· .. 886273 .... 593894 18 2084379. ND 19 22143 51422 20 412872 139788 21 244155 73862 22 480249 639247 23 1766247 ND 24 231560 769866 2S 1436112 222147 26 T 114673 163205 27 555351 388464 28 29857 60132 29 45451 64610 30 1450015 ND 31 1404284 600379 32 1402078 458396 33 238314 38787 34 50554 75676

• 35 27320 75106

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TABLE! MOUND PLANT Miamisburg, Ohio

Relative Response Levels (In Ion Counts)

SAMPLE AROMATICS

36 T 11112 37 232762 38 1531622 39 36956 40- 27994 41 8041

42 l2502 43 16707 44 171483 45 41560 46 75378 47 27961 48 75128 49 1287539 50 733556

-51- .. 351215 .... S~ 41533

~ ... """' - . ~

53 77633 54 157112 55 317626 56 57374 57 388175 58 989759 59 50882 60 58010 61 35746 62 7935 63 60017 64 14459 65 35763 66 . 49570 67 T 204942 68 68124 69 141872 70 30910

Page2

CYCLOS

456949 44924

ND 63687 62662 7972

21334 75520

482506 173934 106348 74844

239799 6163327 3955851 1388404 159186 407866 551433 464066 106074

1104119 3360803

88608 127556 38210 10111

416555 24688

101433 55836

394667 229240 634879 B 44057

-- _____ __;,:;.._

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TABLEl MOUND PLANT Miamisburg, Ohio


SAMPLE AROMATICS

71 18906 72 123823 73 121634 74 78376 75 14073 76 52854 77 177893 78 25211 79 8727 80 45526 81 27195 82 164015 83 60032 84 78147 85 5034 86 15928 87 118717 88 39052" ....

89 24553 90 6338 91 12600 92 75084 93 26961 94 8415 95 47737 96 112534 97 7663 98 5091 99 57008 100 7574 101 5692 102 115370 103 9064 104 8949 lOS 118935

Page3

CYCLOS

112116 331751 184639 117493 37623

203957 387481

84198 11386 47273 62409

217241 203303 302429

16254 22504

341297 62916 54277 12751 30366

102738 74811 35136 98447

115212 16018 68551 92166 37287 10204

273792 33505 25183

253850

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TABLE I MOUND PLANT Miamisburg, Ohio



106 17798 53056 107 16322 43228 108 44480 90844 109 16586 36839 110 32339 52335 111 62579 228995 112 5234 12984 113 9807 31315 114 80253 140423 115 192494 1380517 116 33210 47313 117 15474 39597 118 101840 168517 119 23541 88283 120 1429 6650 1-21 345585 396604 122 74768 115919 123 211927 998754 124 1308 4242 125 29665 64494 126 58617 90720. 127 7005 17807 128 25869 44951 129 34829 69713 130 28349 47833 131 20960 50853 132 44733 78227 133 92563 291827 134 47949 66351 135 41005 88244 136 58252 114409 137 84567 95698 138 14822 27062 139 18521 75923 140 10855 23211

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TABLE! MOUND PLANT Miamisburg, Ohio



141 19636 44648 157 ND ND 158 ND ND 159 ND ND 160 ND 8089

TB TB TB TB

AROMATICS- C6-Cll Aromatic Hydrocarbons benzene, toluene, ethylbenzene, xylene(s} Indicator Mass Peak(s} 78,92,106,120,134,148

CYCLOS - C4-C8 Cycloalkanes/ Al.kenes Indicator Mass Peak(s) 56,70,84,98,112

TB - Travel Blank ND ·Not Detected B - Sampler Broken on Retrieval

;u #AMdMiMSMif!l*& i4

·· ·T- Terpene-Compounds Detected ·-· · ·2043-lA.TOl

2043-1A.XLS

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Miamisburg, Ohio


APPENDIXD Plates 1-3

04/13/94

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COMPOUNCSD~CTAB~

wm; PETREX SAMPLERS

The following compounds have be=n detected in soil gas with PEl'R.EX collectors and. identified by mass spe:uornetry. Ve:iSca.tion was obtained from duplicate PmE< cciled:ors using GC/MS or other qualitative analytical~

Most volatile c:cmpormds are detedable £rem grcmui water~ Semi-volatiles and the mast soluble oi volatiles tnay be d.etedable only from shallow grcmu:i water or vadcse.zr.me SOW'CI!S. The foDowing list is intended !or use as a guide to develapmg envitmi%%U!nia.l strategies. It shaald net be applied to specific: sites and situati.cm.s without advice from Northeast Research !Dstitute <NERD pe:scn:nel.

AROMAllC HYDROCARBONS ~

All a:cmcmc ~ frcm c, CBenzana) to Ca (e.g_ C. AlkVt Beran&)-~~ ldantt1\act:

Benzane Toluene • ~,

EltiVl mari'IYl benzsne

Al.JCANES ~

All C~~~ccn•nvcrcc::c:zr=ora tern c. (BI.Itane) to c. (Pentadac:cnas). c, ten=ne). dcc:.lna:I'Wift vancus Cllkyt gi'CI\.Q artcc:h8c1. anc: = C\'dCOIIccna 'WCift vaftOUI Cllkyt ;rcuc::s anccnac:t -lnc:ll..d'lQ .s;::Mtdl2=tf tda'UIIed:

Elhc:lne Eluh:lnal Penfanel ~ He;~tQn• ~ NC11"1Cn81 Oaccnas Unc:lac::n• oocec:cnas Tdcteccnas nc:tcdac:c:ln8l

. ~r:ltCCic::\8

~~·ntcnes ~ CVctcn8Qh:IMI

AUCENES COle4nd

CVcJo-«J=• Qr::=na ICl"a

~ 0crvt f:i~UI Mtlmyt~ Md'IYt r:x'CICitY c:vr:~CJ:~ncna Md'lyt hu'cna Tdmemyt haxc:'lnlt Md"'Yt CVCICh81Ci'18 Tdmaft'l\lt c:ydchexana ElhYl matnyt CVCIChazcne Elt1yt -mett'lyla1hyt cydchaxcna Md'IYt cda dac:c:ln8 Clmal'lyt haE21'C1'18 Clmatnyt cd'cna ElhYl masnvt adena Clmatnyt c.l'ldaccne

All alleenas tram Cs ~ana) to C,. CPentcdacena). ckanes wttn vaicn.:s Cik:yt and 01nar hydrcc:art:2cn O:ctJCI aftc:d'lad. and c. to c,. CVCICC*anas lrldudi'l; lnCSe wtm wmcu:s akyt gl'CUI:IS end omar nvcrocc:=cns cmac:ned - itCJding s=edftccuy tdanmlad:

Eltlylana Propyl ana Buranas Penranas Hazan• Ha=tan• Odanas Nonanas Oacanas

.. cydcbUtCWt

cv=:=·~ ,~·

CVclch&Ptana cv= Cldlln8 .

. C\'dcucnana . CVCodacana. 'Metnyt ,::Hmtane · Maft'IVS C\"c::Ch8Xena

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ADcVn• trc::m C. to c:,.

Dienes trcm C. to c,.

AlXYNES

DIENES

STYRENES s:yrane. M.rnyt sryr.,8 • end c; to c, JtYI'&nes

VOLAntE HALOGENATED COMPOUNDS

Vh¥t r:IYOIIde" C'l1orcma1hena Me~ cttetkJII' Olloretc:nn c:c:=on rua~adda ~ Qlc:nlcrll1nl:ln8l

TddiorcG1nan81 -Ta~OICd1Cin8l • ClctacgrcC)CMI ~ 'TifcNOI'CI81I'WW • Tetrad'llorcd'\ene Clc:::r=rcp~

SEMI· VOLAntE ORGANICS

H~ ~ ~ ~orcoenradane ~ Tabuct.tcxCiberal• ~ Hea:cd'mrCOibM•• Cltx'cmcd'llciC4Xc=ane PNnat Md'tt1~ c,. C. pt~e~as ~Mefnyt~rws

SULPHUR COMPOUNDS

HyarcQan SIJDd8 ~r:x=aa

OTHER DETeCTABLE COMPOUNDS

Elnancl Mathoa'yull"'CCI a Plcpcnct

• MIXTURES

SUfCinct Clmemyt Butcnd Hucnct Ncnanat MEK

·&

Tdd'llorcgrccane o=n=81"1Z11na ~ Clc:htcfadiiiUUicmatncne Tdd'llorct~ucrctnamcne ercmotam Qltrcm081h&::118 ~men. Clbrem~orcmetncDt Btcmodid*XCQI'Cpan8

• CcmQoU'1dr ~g a law alfldl'l fD ar::tlvr:ltlld c:c=cn

C,·C.N~ ~ Qdciicx~•

~· . actDUbaiWbl"' ntd8 ~ NIINbWar• ~:·

~· ~lift=-~ ~

BufCIIa• Me1hVt eutancn• Hexcncne Md'IVt HexaiiOIW Tdd&CCIIIOI• Ald&l'lyde BenzctdahVd• Acatctdahyde

'The PEiRCX Tad'TIIQue can detect end c::taacrartza trash and ~ad hydrcccrbon ~as InclUding:

<;cscan• OecdadluriaadlicO a..tllats • Jet fUatl (JPc11JPS) AWzllcn.;asciN ~·gc:sc8n8 HyCaulc :w2S

C.

l\'liamisburg, Ohio

•

•


APPENDIXE Histograms_

04/13/94

..

I

\

i /

j

i i. I

• 100

90

80

70

j 60

50

40

30

20

10

0 0 0 0 0 0

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ..... N C") "'t

• AROMATIC HYDROCARBONS HISTOGRAM

...------- ,-- -,- --.---- -' '----------. 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ao co ......, m m o ..-..- .....

0 0 0 0 0 N .....

t--t--1 0 0 0 0 0 0 0 0 0 0 C") "'t ..... .....

Relative Response (In Ion Counts)

Arrows indicate sample population breaks used to establish inteJVals on Plate 2.

I 0 0 0 0 0 0 0 0 0 0 II) co ..... .....

•

I I I I

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ...... co m 0 ..... ..... ..... ..... N N

2043AROM.HIS

...... -···- .. .. ... ·-·----· ·---······-- .. ·------· ---------------- .. --------~~----------~--:----------- --··------·

• • • CYCLOALKANES/ALKENES HISTOGRAM

80

70

60

il' 50

140 J.l.t 30

20 ·-1 10 -fl

0 -1•1 I ,1,1,.1.1-H-H-H•I I I I I I I I I I I I I I .I I I I I 1-1 I I I I 1-1 I I I I I I I I I I I I I I I I I I H-1-H 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N ..,. co c:o 0 N ..,. co c:o 0 ~ ~ CO:C:O .0 ~ ~ co c:o 0 N ; co co 0 N ~ co co 0 N -- - -- N N N C") C") C") ..,. ..,. ..,. ..,. U) U) U) U) co co

Relative Response (In Ion Counts)

Arrows indicate sample population breaks used to establish intervals on Plate 3.

2043CYCLHIS

______ ......... -----

Miamisburg, Ohio

•

•

• Northeast Research IDstitute LLC

APPENDIXF TD-GCJMS Results

04/13/94

I I;;

~

,. .

r r ~·

I·

. I , .

• esults of TD-GC/MS PETREX Sample Analysis

~ Project: 2043E Client: Science Applications International Corporation Site/Location: Miamisburg, Ohio Analysis: Thermal Desorption-Gas Chromatography/Mass Spectrometry Date of Analysis: 3/21/94-3/22/94 Units: Area Counts

Compound Toluene Tetrachloroethene

Compound Trichloroethene Toluene Tetrachloroethene

• Compound Benzene Toluene Ethylbenzene Styrene

Compound Benzene Toluene


•

Sample #4

Sample #13

Sample #15

Sample #16

Sample #18

Relative Area 19313

1237517

Relative Area 13765 40923

5110235

Relative Area 1027313

135186 . 41532 39121

Relative Area 16434 57626


62454

I i i I i:

'.

' I :

i.

I

i. I 1

i : , I

' I i : ! I

. I

; !

:j 'I

' . : I

~ Benzene Toluene Tetrachloroethene


Compound 1-Pentene Benzene Toluene

• mpound -Methyl-1-propene

Pentene (z)-1 ,3-pentadiene 1-Hexene

·Benzene Toluene

Compound Benzene Toluene Cyclopropylidencyclohexane 2-~-pinene•

•- Terpene

~ Jpound Wbc:nzene

Sample #23

Sample #30

Sample #31

Sample #32

Sample #36

Sample #38


39735 69178

Relative Area 3200242 : ·52475

Relative Area 13094

2726096 24963

Relative Area 70998 49267 69617 59921

4242294 77952


50904 237934 105303


.¥ ':1

I .. ! I

"

i , I

i j ! •

. t '!

. '

2

• Compound Pentane 3-~etllylpen~

Hexane Benzene 1 ,2-Dimetllyltranscyclopentane Heptane Metily lcyclohexane Toluene

Compound Pentane 2-~etllylpentane

3-~etlly !pentane Hexane Benzene Isopropycyclobutane

•

\ttetllylcyclohexane 1luene

GCMS2043

•

Sample #49

Sample #51

Relative Area 279900 153411 506985 206419 124750 438139 392250 411729

Relative Area 138879 118192 66045

309279 72490 13974 56767 77952

3

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LEGEND

99

Conlro c lors Entranc e

Features: S mple Location • Pefrex and Fidler o

0 Siruclures I 1 Bou ndary

p on d Roadway - - Poved/Unpove

- Ephemeral Stream 0 Fidler Sample

(/) 0

I I 141

60

123

101

100

-

('~--, 1--l ~

\\ "-~n lds',J' ~~ ~I 59 so "-

- 4SO

12so

14SO

~'- 16SO

- 1Bso

~ Plan t

"'~ ~

~~

Location Map

Sampl e Lo cati ons

Plate 1

I

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SAXONY ROAD

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November 1 0, 1994

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LEGEND

( I lon counts ) : Re lative Response Values n

[23 L 1 ,ooo,ooo

IS3 3DO, OOO - 999,999

nse Va lue T Relative Respo Elevated Due To Terpa nes.

Features:

d Fidler Sample Location e Petrex an 0 Struc tures

Plonl Boundary -- Paved/ Unpaved Roadway

----- Ephomoral Stream 0 Fidler Sa mple

C'\1 (/) 0

I I SOB~so

2SO

4SO

6SO

8SO

1oso

12SO

14SO

16SO

1Bso

Location Map

Relative Response

Aromatic Hydroca rbon s

Plate 2

_j

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~ 0.J (/) c.o

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BENNER ROAD

Relative e R s ponse Values(ln ion

l2a ~ 1,000,000

E;s 300,000 - 999,99~

ND None Detected

17 90

64

273

LEGEND

Features: S mple Location counts):

• Pelrex and Fid ler a D St ructu res

I 1 Boundary P on d Roadway Poved/Unpove

_=~- Ephemeral Stream

0 Fidler Sample

36U'Btr3- 2SO

709'2'- 4SO

6SO

8SO

10SO

12SO

14SO

16SO

18SO

Rela tive Respon se

/ Aik enes Cyc loa lkan es

Plate 3

• APPENDIXD

RADIOLOGICAL DATA (FIDLER & SOIL SCREENING FACILITY

•

•

::oa:: ~ 0

~- § ;·c. 1:1 .,

-~ r

~ ~ 1

0 s;

~ ~

._] c ::1 -<"'< _., -o:r ~~

:n 6:

i :1

~i ~§: O>C .!..O

• • APPENDIX D

Radiological Data (FIDLER survey and Mound Soil Screening Facility Data)

SMPID Contamination Criteria CHI FIDLER Readings Cl! I Contamination Criteria CH2 FIDLER Readings CH2 Plutonium-238

Units: CPM Units: CPM Units: CPM Units: CPM Units: pCilg

RESULTS RESULTS RESULTS RESULTS RESULTS NOTES

oooso 273.0 180.0 11112.0 11000.0 15.0 • OOOS2 273.0 190.0 11112.0 11000.0 17.0 a

OOOS4 273.0 200.0 11112.0 11000.0 8.0 a

OOOS6 273.0 200.0 11112.0 10000.0 14.0 a

OOOS8 273.0 190.0 11112.0 /2000.0 10.0 a

OOOS9 262.0 190.0 11112.0 10500.0 6.0 a

OOIS9 262.0 180.0 11112.0 11000.0 17.0 a

002SO 262.0 210.0 11112.0 10000.0 8.0 a

002S2 273.0 210.0 11112.0 11000.0 10.0 a

002S4 273.0 210.0 11112.0 10000.0 S.O a

002S6 273.0 230.0 11112.0 11000.0 13.0 a

002S8 273.0 230.0 11112.0 12000.0 12.0 a

004SO 273.0 170.0 11112.0 10000.0 12.0 a

004S2 273.0 220.0 11112.0 10000.0 7.0 a

004S4 273.0 180.0 11112.0 11000.0 4.0 a

004S6 273.0 220.0 11112.0 12000.0 19.0 a

004S8 273.0 210.0 11112.0 11000.0 10.0 a

006SO 262.0 160.0 11112.0 8000.0 11.0 a

006S2 262.0 190.0 11112.0 10000.0 12.0 a

006S4 262.0 150.0 11112.0 7500.0 9.0 a

006S6 262.0 200.0 11112.0 11000.0 4.0 a·

006S8 262.0 220.0 11112.0 11000.0 9.0 a

oo8so 262.0 240.0 11112.0 9500.0 16.0 a

OOSS2 262.0 210.0 11112.0 /2000.0 po.o • 008S4 262.0 210.0 11112.0 10000.0 8.0 a

008S6 262.0 200.0 11112.0 I /500.0 12.0 • 008S8 262.0 260.0 11112.0 11000.0 11.0 • OOSIO 262.0 220.0 11112.0 11000.0 11.0 • OOS11 262.0 200.0 11112.0 /1500.0 13.0 • OOSI2 262.0 220.0 11112.0 9000.0 15.0 a

OOSI3 262.0 180.0 11112.0 6500.0 17.0 a

OOSI4 262.0 170.0 11112.0 8500.0 5.0 • oosu 262.0 180.0 11112.0 10000.0 9.0 • OOSI6 262.0 210.0 11112.0 10000.0 13.0 • OOSI7 262.0 180.0 11112.0 10000.0 7.0 • OOSI8 262.0 180.0 11112.0 9500.0 13.0 • OOS20 262.0 180.0 11112.0 9500.0 14.0 a

OIOSO 273.0 150.0 11112.0 10000.0 11.0 a

OIOS2 273.0 200.0 11112.0 10000.0 14.0 • --·- ---

Highlighted areas represent detection above FIDLER contaminant criteria or above the Mound Soil Screening Facility detection limit.

• Thorium-232

Units: pCilg

RESULTS NOTES

0.9 a

0.9 • 1.3 a

1.4 a

1.2 a

1.4 a

0.9 a

0.7 a

0.9 • 0.7 a

1.1 a

0.7 a

1.0 a

0.7 a

0.7 a

0.9 a

0.9 a

0.8 a

1.1 a

1.1 a

0.1 • 1.2 • 1.0 a

1.3 • 0.8 a

1.2 • 0.1 • 1.6 • 1.8 • 0.8 • 1.2 • 1.0 • 1.4 • 0.9 • 0.9 a

1.2 • 0.9 a

1.3 • 1.2 •

:::ca:: 0 0 s. c: !!!. 5. 0 ::I '"0 -[

r

~ ~ ~

~

"* ~ ~

i:-g -<~ -'"0 \0:::1' -oeJ U.o

:n 6:

i ::t

> '"0'0

~~ 0 :;;· r!.lo

APPENDIX D Radiological Data (FIDLER survey and Mound Soil Screening Facility Data)

SMPID Conlamination Criteria Clll FIDLER Readings CHI Contamination Criteria CH2 FIDLER Readings CH2 Plutoniwn-238

Units: CPM Units: CPM Units: CPM Units: CPM Units: pCilg


OIOS4 273.0 240.0 11112.0 12000.0 11.0 a

OIOS6 273.0 230.0 11112.0 11000.0 8.0 a

OIOS8 273.0 220.0 11112.0 13000.0 14.0 a

012SO 262.0 190.0 11112.0 9000.0 6.0 a

012S2 262.0 160.0 11112.0 9000.0 6.0 a 012S4 262.0 250.0 11112.0 11000.0 17.0 a

012S6 262.0 240.0 11112.0 11000.0 7.0 a

012S8 262.0 245.0 11112.0 11500.0 11.0 a

014SO 273.0 150.0 11112.0 8000.0 1.0 a

014S2 273.0 160.0 11112.0 7000.0 10.0 a

014S4 273.0 260.0 11112.0 12000.0 20.0 a

014S6 273.0 230.0 11112.0 11000.0 11.0 a

014S8 273.0 230.0 11112.0 11000.0 19.0 • 016SO 262.0 110.0 11112.0 5000.0 12.0 a 016S2 262.0 170.0 11112.0 9000.0 10.0 a

016S4 262.0 210.0 11112.0 11000.0 20.0 a 016S6 262.0 220.0 11112.0 11000.0 16.0 a

016S8 262.0 220.0 11112.0 11500.0 ~.0 a

018SO 262.0 200.0 11112.0 10500.0 0.0 a 018S2 262.0 190.0 11112.0 10000.0 17.0 • 018S4 262.0 220.0 11112.0 I 1500.0 ~3.0 a

018S6 262.0 260.0 11112.0 11500.0 124.0 • 018S8 262.0 220.0 11112.0 10500.0 13.0 a

OISIO 262.0 170.0 11112.0 10000.0 23.0 • OISII 262.0 200.0 11112.0 15000.0 I'J.O a

OISI2 262.0 170.0 11112.0 10500.0 21.0 a

OISI3 262.0 160.0 11112.0 10000.0 10.0 • OISI4 262.0 180.0 11112.0 10000.0 25.0 ~ OISI5 262.0 190.0 11112.0 10000.0 17.0 a

OISI6 262.0 195.0 11112.0 10500.0 13.0 a

OISI7 262.0 150.0 11112.0 9000.0 15.0 a

OISI8 262.0 190.0 11112.0 10000.0 12.0 a

020SO 273.0 220.0 11112.0 11000.0 16.0 a

020S2 273.0 150.0 11112.0 7000.0 0.0 a

020S4 273.0 270.0 11112.0 11000.0 20.0 a

020S6 273.0 260.0 11112.0 uooo.o ~0 a

020S8 273.0 240.0 11112.0 11000.0 18.0 • 02SIO 273.0 190.0 11112.0 11000.0 8.0 a

-·----

• ighlighted areas represent detection above FIDLER contaminant criteria or above wnd Soil Screening Facility detection limit.

Thoriwn-232

Units: pCilg

RESULTS NOTES

0.9 a

1.7 a

1.7 a

1.2 • 1.0 • 0.9 a

1.4 a

1.4 a

0.2 • 0.6 a

1.0 • 1.2 a

1.1 • 0.3 a

0.8 a

1.8 a 0.7 a

1.3 a

0.1 a 1.2 • 1.4 • 1.1 a

1.3 a

1.1 a

1.7 • 0.9 • 1.6 a

1.3 a

1.5 a

0.8 a

1.3 • 0.8 • 1.1 a

0.3 • 1.5 • 0.8 • 1.3 • 0.5 a

•

::tl~ 0 0 ~- § o· c.

= "' -~ ~ ~ 1

0 c:: VI

~ ~

..... 11! ~q _.., ~[ v.o

:!1 !!. Q.

~ '8 ~

> "''0 ~~ o>< .:...o

• • APPENDIX D


SMPID Contamination Criteria CHI FIDLER Readings CHI Contamination Criteria CH2 FIDLER Readings CH2 Plutonium-238

Units: CPM Units: CPM Units: CPM Units: CPM Units: pCi/g


02SI2 273.0 220.0 11112.0 12000.0 11.0 a

02SI3 273.0 210.0 11112.0 12000.0 13.0 a

02SI4 273.0 200.0 11112.0 /2000.0 17.0 a

02SU 273.0 190.0 11112.0 11000.0 21.0 a

02SI6 273.0 210.0 11112.0 12000.0 IS.O a

02SI7 273.0 210.0 11112.0 12000.0 j22.0 a

02SIB 273.0 180.0 11112.0 11000.0 19.0 a

03SI4 273.0 200.0 11112.0 12000.0 13.0 a

03SIS 273.0 210.0 11112.0 12000.0 10.0 a

03SI6 273.0 190.0 11112.0 12000.0 ~.0 a

03SI7 273.0 220.0 11112.0 12000.0 19.0 a

04SIO 273.0 220.0 11112.0 12000.0 ~.0 a

04SI2 273.0 200.0 11112.0 12000.0 ~.0 a

04SI4 273.0 210.0 11112.0 12000.0 17.0 a

04SIS 273.0 200.0 11112.0 12000.0 11.0 a

04SI6 273.0 190.0 11112.0 11000.0 17.0 a

04SI7 273.0 190.0 11112.0 12000.0 18.0 a

04SI8 273.0 190.0 11112.0 13000.0 .0 a

0SS14 273.0 180.0 11112.0 12000.0 0.0 a

OSSIS 273.0 220.0 11112.0 13000.0 11.0 a

OSS16 273.0 200.0 11112.0 12000.0 16.0 a

OSSI7 273.0 190.0 11112.0 10000.0 24.0 a

06SIO 262.0 1SO.O 11112.0 10000.0 13.0 a

06SI2 262.0 200.0 11112.0 11500.0 p.o a

06SI4 262.0 200.0 11112.0 10000.0 7.0 a

06SIS 262.0 180.0 11112.0 11500.0 j20.0 • 06SI6 262.0 200.0 11112.0 1/SOO.O 14.0 a

06SI7 262.0 200.0 11112.0 IOSOO.O 16.0 • 06SI8 262.0 200.0 11112.0 12000.0 8.0 a

06S20 262.0 190.0 11112.0 10000.0 8.0 a 06S22 262.0 190.0 11112.0 8SOO.O 14.0 a 06S24 262.0 190.0 11112.0 11000.0 6.0 a

07S1S 262.0 190.0 11112.0 9SOO.O 8.0 a

07SI6 262.0 220.0 11112.0 11000.0 6.0 a

07SI7 262.0 18S.O 11112.0 10000.0 17.0 a

08SIO 262.0 190.0 11112.0 IOSOO.O 2.0 a

08SI2 262.0 2SO.O 11112.0 10000.0 16.0 a - L__ ---- -------

Highlighted areas represent detection above FIDLER contaminant criteria or above the Mound Soil Screening Facility detection limit.

• Thorium-232

Units: pCi/g

RESULTS NOTES

0.9 a

1.2 a

0.7 a

1.3 a '

1.1 a I

1.3 a

1.0 a

1.2 a

0.9 a

1.4 a

1.0 a

1.1 a

0.9 a

1.3 a

1.1 a

0.7 a

1.3 a

1.2 a

1.4 a

1.1 a

1.3 a

1.2 a

1.2 a

0.8 a

1.3 a

1.2 • 1.2 a

1.6 • 1.1 • 1.0 a

0.8 a

1.0 a

1.7 a

1.4 a

1.3 a

1.3 a

1.1 a

~== n o ~· 5 s· Q. ::s ., -[

r

~ ~

~

~ ~ ~

~ ..... "8 c :::1 .!<"'< _., :8[ Utn

::n n s:

l :::1

> '0 .,"8 ~~ o>< J:..o

APPENDIX D Radiological Data (FIDLER survey and Mound Soil Screening Facility Data)

SMPID Contamination Criteria CHI FIDLER Readings CHI Contamination Criteria CH2 FIDLER Readings CH2 Plutoniwn-238

Units:CPM Units: CPM Units: CPM Units: CPM Units: pCi/g


08SI4 262.0 230.0 11112.0 /1000.0 .0 a

08SI5 262.0 225.0 11112.0 I 1500.0 ~1.0 a

08SI6 262.0 240.0 11112.0 /1000.0 12.0 • 08SI7 262.0 245.0 11112.0 10500.0 11.0 a

08SI8 262.0 225.0 lllt2.0 11000.0 6.0 a

08S20 262.0 190.0 11112.0 9000.0 9.0 a

08S22 262.0 170.0 11112.0 11500.0 ~.0 a

08S24 262.0 240.0 11112.0 /1500.0 15.0 a

09SIS 262.0 210.0 11112.0 11000.0 16.0 a 09SI6 262.0 190.0 11112.0 11000.0 10.0 a 09SI7 262.0 230.0 11112.0 10500.0 9.0 a

OSII2 262.0 210.0 11112.0 UJOO.O INS

I OSlO 273.0 260.0 11112.0 /1000.0 10.0 a

IOSI2 273.0 210.0 11112.0 11000.0 7.0 a

IOSI4 273.0 220.0 11112.0 11000.0 11.0 a

lOS IS 273.0 220.0 11112.0 11000.0 13.0 a

IOSI6 273.0 250.0 11112.0 11000.0 p.o a

10517 273.0 220.0 11112.0 11000.0 f7.0 a

IOSI8 273.0 210.0 11112.0 11000.0 7.0 a

IOS20 273.0 230.0 11112.0 11000.0 p.o a

IOS22 273.0 220.0 11112.0 11000.0 17.0 a

IOS24 273.0 ISO.O 11112.0 7000.0 2.0 a

IISI5 273.0 220.0 11112.0 11000.0 ~.0 a

IISI6 273.0 230.0 11112.0 11000.0 6.0 a

IISI7 273.0 230.0 11112.0 11000.0 10.0 • 12SIO 262.0 230.0 11112.0 /1000.0 19.0 a

12SI2 262.0 170.0 11112.0 11000.0 8.0 a

12SI4 273.0 210.0 11112.0 11000.0 15.0 a

12SI6 273.0 270.0 11112.0 /1000.0 18.0 a

12SI8 273.0 230.0 11112.0 11000.0 12.0 a

12S20 273.0 220.0 11112.0 11000.0 9.0 a

12S22 273.0 180.0 11112.0 /1000.0 j9.0 a

12S24 273.0 250.0 11112.0 10000.0 13.0 a

14SIO 273.0 260.0 11112.0 11000.0 14.0 a

14SI2 273.0 190.0 11112.0 /1000.0 12.0 a

14SI4 273.0 190.0 11112.0 10000.0 0.0 a

14SI6 273.0 260.0 11112.0 10000.0 9.0 a ------------ ---- ----

.ighlighted areas represent detection above FIDLER contaminant criteria or above th.d Soil Screening Facility detection limit.

Thoriwn-232

Units: pCi/g

RESULTS NOTES

1.1 • 1.6 • 1.1 a

1.3 a

1.1 a

0.7 • 1.1 a .

1.4 a

I.S a

1.4 a

1.2 a

NS

0.9 • 1.3 a

I.S a

1.3 a

1.1 • I.S • 1.1 a

1.2 a

1.1 a

1.2 • 0.4 a

1.6 • 1.6 • 0.9 a

1.2 a

~.I INA

1.0 a

0.9 a

0.9 a

1.0 a

0.8 a

1.3 • 1.1 a

1.1 a

1.0 •

•

~3::: " 0 ~- § -· Q. g '"tl

-~ ~ ~

~

0 c:: Ul

~ ~

~ .... '8 ~q -'"0 -.o::r \Of}l Ul"

::!1 " c: :§ ~

~t ~~ u.o

• • APPENDIX D


SMPID Contamination Criteria CHI FIDLER Readings CHI Contamination Crireria CH2 FIDLER Readings CH2 Plulonium-238

Uniu: CPM Uniu:CPM Uniu: CPM Uniu: CPM Uniu: pCilg

RESULTS RESULTS RESULTS RESULTS -RESULTS NOTES . -14SI8 273.0 220.0 11112.0 12000.0 p.o • 14S20 273.0 190.0 11112.0 11000.0 7.0 a

14S22 273.0 280.0 11112.0 /2000.0 ~0 a

I4S24 273.0 200.0 11112.0 9000.0 9.0 a

16SIO 262.0 220.0 11112.0 11500.0 19.0 a

16SI2 262.0 230.0 11112.0 9500.0 16.0 a

16SI4 262.0 220.0 11112.0 10000.0 7.0 a

16SI6 262.0 210.0 11112.0 10000.0 0.0 • 16SI8 262.0 225.0 11112.0 10500.0 18.0 • 16S20 262.0 210.0 11112.0 10500.0 18.u a 16S22 262.0 230.0 11112.0 9500.0 11.11 a . 16S24 262.0 240.0 11112.0 12000.0 15.11 a

18SIO 262.0 200.0 11112.0 11000.0 120 a 18S12 262.0 250.0 11112.0 11000.0 15.0 a 18S14 262.0 230.0 11112.0 10000.0 8.0 • 18S16 262.0 210.0 11112.0 9500.0 130 a

18S18 262.0 220.0 11112.0 10000.0 8.0 a

18S20 262.0 140.0 11112.0 7500.0 14.0 • 18S22 262.0 200.0 11112.0 10000.0 23.0 a

18S24 262.0 250.0 11112.0 10000.0 16.0 a

20S10 273.0 220.0 11112.0 11000.0 17.h • 20S12 273.0 240.0 11112.0 11000.0 12 u a 20S14 273.0 210.0 11112.0 11000.0 0.0 a 20S16 273.0 260.0 11112.0 11000.0 8.0 a

20S18 273.0 200.0 11112.0 10000.0 18.0 a 20S20 273.0 230.0 11112.0 10000.0 10.0 a

20S22 273.0 290.0 11112.0 11000.0 23.•• • 20524 NA NA NA NA 12.U • 22S17 273.0 220.0 11112.0 11000.0 0.0 • 22S18 273.0 250.0 11112.0 11000.0 8.0 a

22S20 273.0 220.0 11112.0 11000.0 14.0 a

22S22 273.0 250.0 11112.0 11000.0 11.0 a

23S20 262.0 220.0 11112.0 9000.0 8.0 a

23S22 262.0 230.0 11112.0 9500.0 NS

24S22 273.0 220.0 11112.0 11000.0 18.0 a

2SII5 273.0 220.0 11112.0 uooo.o INA NA

~I_ __ 262.0 210.0 11112.0 13000.0 ~A NA -----

Highlighted areas represent detection above FlDLER contaminant criteria or above the Mound Soil Screening Facility detection limit.

• Thorium-232

Uniu: pCilg

RESULTS NOTES

0.9 • 0.9 a

1.4 a

0.7 • 0.8 a

0.8 • 1.1 a

1.1 • 1.2 • 1.0 • 0.8 • 1.1 • 1.1 a

1.0 • 1.2 • 1.3 a

1.3 • 1.2 • 0.9 a

1.1 • 1.3 • 1.3 • 1.4 a 1.7 • 1.1 a

1.4 • 1.4 • 1.3 • 1.2 • 0.8 a

0.7 a 1.4 • 1.2 a NS

1.6 a

NA NA

NA NA

•

APPENDIXE

1994 SEEP SAMPLING RESULTS

•

•

"3:: ~ 0 ~- § -· Q. g "'0 orr

.r

~ ~ 1

~ ~ ~

wl =~ !~ :0~ 'R-

::n 6: if 1

> "'0'0

~~ t;n>< l-..ll:'l1

• MOUND NEW PROPERTY

·--·--.---·. Mound Seep I

1-------- SompltiD EPA Somplt ID -·-----

------·-· Lab Somplt ID Date Collected ____ .,. ____

------··---···· -loorpnlcs

Aluminum --··· Antimony -Arsenic Barium BeryUium --Bismulh .. Cadmium -Calcium ... Chromium

-··· Cobalt -----Copper---·· Cyanide ~-----·

Lead ---·-· -------Uthlum Magnesium Manganese Merauy Molybdenum Nickel -Potassium -Selenium Silver Sodium· ... Thallium -Tin Vanadium Zinc

Seep616 NSIOOI

MND16-..0%06-0100 4790-001 REG

3129194 Rrso1t Val. Code

Ualts UOIL 47 J-0 UOIL 0.32 u UOIL 0.8 u UOIL 129 J UOIL O.S6 U-B UOIL SH U-B UOIL 0.4 u UOIL 217()()(] UOIL 4.9 J-B UOIL I U UOIL 3.4 J-0 UOIL 2.3 J-OB UOIL 624 J-0 UOIL 2.3 U-B UOIL 8.4

UOIL 64400 UOIL 26.8 J-0 UOIL 0.1 u UOIL I.SU UOIL 4.6U UOIL 14(1(] UOIL 0.~ u UOIL 3.7U UOIL 3810()( UOIL 1.5 UJ-1 UOIL 6.8U UOIL !17.6 UOIL 7.4 J-0

• APPENDIX£ • Seep Sampling Results (1994)

I I Seep610 Seep 610 (DUP) Seep617 Seep6l0 NSlOOI NSlOil NS3001 NS4001

MNDI6-090J.Gl00 MNDI6--0903-ll00 MND16--0317-0100 MNDl'-0408-0%00 4790-003 REG 4790-004 REG 4791-001 REG 4791-00% REG

3129194 03/'Z9194DUPE 3130194 3130194 Rrso1t VaL Code · Rrso1t Val. Code Rrso1t Val. Code Result VaL Code

-30.! J-0 84.9 J-0 727 J.o S49(l J-0

0.3..: u 0.32 u 0.32 u 0.32 u -0.8 u 0.81 0.8 u 0.8 u 43J 40.6J 42.6J 46.7 J

0.16 U-B 0.16 U·B 0.3~ U-B O.S2 U·B -38.9 U-B 3S.S U·B 60.~ U-B 46.7 U-B

0..4 u 0.4 u 0.4 u 0.4 u 128(K)(J 124()()(J 174()()(] 139000

u J-8 3 . ..: J-8 S.B J-B 8.9 J-B I U lU 1.1 3.4 -

1.4 J-0 2.7 J-0 3.4 J-0 . 7.6 l·D 0.25 UJ-08 1.1 UJ-DB 0.25 UJ-08 0.41 UJ-08 47~ J-0 161 J·D 1170 J-0 7830 J-0 2.2 U-B l..t U-8 1.2 U-8 1.8 U-8 5.9 SA 29.@ 16

23200 223()( 7SSOC: 35700 l . .t J-0 3.5 J-0 37.S J-0 129 J-0 0.1 u 0.1 u 0.1 u 0.1 u J.S U uu I.S U I.S U 4.6U 4.EU 4.E U 7.'1

·~011 101~ 315(1 252~ 0.~ UJ·I O.!l UJ·I 0.9 UJ-1 0.~ UJ-1

1 1.1 1.7 I 26200 24900 17200 5701X

uu 1.5 u 7.5U u UJ-1 6.8 u 6.8 u 6.8U uu

28.1 27.7 42.8 36.3 9.6 J-0 4.4 J-0 9.6 J-0 24.5 J-0

::OS: s. g ~- 8. g ., og

r

~

f

0 p; f

rJ [~ :0~ \0

""'-::!1 5: ::0

'8 ::l

> ~:s ~§: I.TI:OC wi.TI


Mound Sup I -------Sample tO --·

EPASamplt!ID lAbSamplt!ID Date Collected ---·--

------·~-

lnorpnk.s Units ---•w• Aluminum UG'L

' -~·..,_--

Antimony UG'L Arsenic UOIL ---· Barium UG'L .. Beryllium UG'L -Bismuth UOIL Cadmium ·-- UOIL ......,...,..._ ______ Calcium UOIL --Chromium UGIL -Cobalt UG'L Copper . -·· .. UG'L ~--- UGIL r:-=-------Iron UGIL ---Lead UGIL Uthlum ---- UG'L Magnesium UG'L Manganese UGIL Memuy UGIL Molybdenum UGIL Nickel UGIL ---Potassium UGIL

·--~

Selenium UGIL Silver UGIL Sodium UGIL ... Thallium UGIL Tin UGIL --Vanadium UGIL Zinc _!!GIL --

• APPENDIXE Seep Sampling Results (1994)

I I Seep6" Seep6ZI Seep614 NSSOOI NS6001 NS7001

MND16-06U.OZOO MND16-U13-0%00 MND16-1J08.0%00 4791.003 REG 4791-004 REG 4791-005 REG

Y.J0./94 !130194 Y.J0./94 Result VaLCGde Result VaL Code Result VaL Code

3041l J-D 254 J-D 391( J-D 0.32 u 0.~ u 0.3 u 0.8 u 0.~ 0.8 u

42.4 J 20.~ J 29.81 0.2 U-8 0.1~ U-8 0.32 U-8

35.1 U-8 37.~ U-8 41.5 U-8 0.4 u 0.4 u 0.4 u

80300 82300 1130()0 4.4 J-B f6 J-8 6J J-8 1.4 IU :u 5.7 J-D 3:2 J-D -~ 6.~ J-D

0.71 UJ-D8 0.~ UJ-DB 0.25 UJ-D8 J571l J-D 33~ J-D 618( J-D

2.1 U-8 o:~ u 2.~ U-8 3.4 1.7 u 18.1

1660c f69cjj 25300 II( J-D 9.J J-D 159 1-D 0.1 u 0.1 u 0.1 u 1.5 u 1.5 U 1.5 U 4.6 u uu 5 . ..c

l311l 766 2461l 0.9 UJ-1 0.9 UJ-1 0.9 UJ-1

0.92U 0.9ZU 1.4

IS400 13500 17500 7.'1U ..~ u uu 6.8U uu 6.8U 2 1a:~ 29.]

22.ti J-Q__ . ·- - - ~~fi ~. 25.4 J-D

• Seep62l

-- t-- --··-~-------- -----

NS8001 -MNDI6-0303-0ZOO -4791-006 REG

31'30.194 --Result VaL Code

-1--·--- ..

S46 J-D -~ ~-~·-··---·-·~ -- ..

0.3~ u 0.8 u

67.91 I 0.3~ U-8 -53.4 U-8 0.4 u -·

1420()0 ·---.. -·-- ------4.3 J-8 -·-----a.~ - '-·----· 2.8 J-D ----·--- ----·-~~

1.1 I-DB - ---··-786 J-D --2.3 U-8

-~

6.1 35100 -

17.3 J-D -0.1 u 1.5 u .. 4.6 u --- --

1500 -0.9 UJ-1 ...

0.92U 130000

u UJ-1 ·-6.8U 35.6 7.7 J-D

:::o:;:: ~ 0 !i. c::

5· 6.. ::3 '"0

0~

~ ~ ~

0 c: Y' z ~

0~ ~'&

~q ~d2 -el ~:

~ ~ '8 ~

~t ~~ trl>< ~tTl

• MOUND NEW PROPERTY ---

Mound Sup I ....... Sample/D

--·--EPA Sample ID --··- -Lab Sample ID .... Date Collected ..

---.

VolatUe Orpnlcs Acetone -. Acetonitrile Acrylonilrile Benzene Bromoclichloromethane Bromofonn Bromomethane

-2-Butanone

··-Carbon Disulfide Carbon Tetrachloride Chlorobenzene

-Chloroethane Chlorofonn ---Chloromethane Dibromochloromethane 1,1-Dichloroethane 1,2-Dichloroelhane 1,1-Dichloroethene 1,2-Dichloroetbene 1,2-Dichloropropane cis-1,3-Dichloropropcne trans-1,3-Dichloropropcne 1,2-Dielhylbenzcne Elhylbenzene .. 2-Hexanone 4-Melhyl-2-pentanone Methylene Odoride n-Hexane

--· S~ne

1,1,2,2-Tetrachloroethane Tecracllloroetbene

I ·-Seep 616 ·-NSI001

MND16-.0206-0100 4790-001 REG

3129194 Result VaL Code

Units UG/L 10 UJ-C-UG/L 100 u UG/L 100 u UG/L su UG/L su UOIL su UGIL UlU UGIL 10 u UGIL su UGIL su UOIL su UGIL IOU UG/L su UOIL IOU UOIL su UGIL. su UG/L su UOIL su UGIL su UOIL su UG/L su UOIL su UOIL su UGIL su UOIL I~ u UGIL I~ u UG/L su UOIL 10 u UOIL su UGIL su UOIL su

• APPENDIXE • Seep Sampling Results (1994)

r------· I I I I ---· -·----· See~ 610 Seep 610 (DUP) Seep617 ·--· Seep610 --

NS1001 NS1011 NS3001 NS4001 --MND16-41903.o100 MND16--0903-1100 MND16-.0317-0100 MND16--0408.0200

4790-003 REG 4790-004 REG 4791.001 REG 4791-002 REG ··-- ·-·-·--

3129194 03129194DUPE 3130194 3130194 Result v.a.Cocle Result VaL Code Result Val. Code Result VaL Code --

10 UJ-C- 10 UJ-C- 10 UJ-C- 10 UJ-C- ----100 u 100 u 100 u 100 u --100 u 100 u 100 u too u

su su su su su su su su

·---·----su su su su UlU UlU IOU 10 u 10 u IOU IOU to_u _______

-su su su su su su su su ·----su su su su

tou------1 IQ U 10 u 10 u su su su --~ u---·-----j

IOU IOU 10 u 10 u --su su su su su su su su su su su su --su su su su su su su su su su su su su su su su .5U su su -5 1]---su su su su su su su su

I~ u IOU !0 u IOU I~ u IOU 10 u 10 u su su su su

IOU IOU 10 u I~ u su su su su su su su su su su su .5U

"3:: n o :S. c: 5· [ ::s .,

0~

~ ~

1

g Y' z ~

0~

~~ ~d! ~~ ""'"-:!!

n 0:

" n "8 ~

;pf ~§: trJ>c V.trJ

• Toluene UGIL su

-1,1,1-Trichloroethane UGIL su 1,1,2-Trichloroelhanc UGIL su Trichloroethenc UGIL su 1,1,2-Trichlorotrifluoroe UGIL su Vinyl Acetare UGIL I~ u Vinyl Olloride UGIL 10 u Xylene, Total UGIL su Tentadvely Identified Compounds

• APPENDIX£ • Seep Sampling Results (1994)

su su su su ·------!------su su su s u .. --·-su su su su .5U su 8 .5U su su su s u

10 u 10 u 10 u ----10 u------

10 u 10 u 10 u IOU .5U .5U .5U ----·-s -:-:----- -· u

I

":!:: CD 0 ~. c !!!. a. 0 ::I .,

0~

~ ~ 1

~ f

wl !3~ !!~ ~~ .$>.-

::n !!. ~

~ '8 :::1

~ ;p'g ~§: tn>< O.m


Mound Sup I ~lt/0

EPA Sample 10 Lob Somplt 10 Oatt Colltcted

VolatUe Orpoles Ac::etone Acelonilrilc Acrylonitrile 8en1.ene Bromodiclll.oromcthane oromororm Bromo methane 2-Bulanonc .. C8lbon Disulfide C8lbon Tettaclll.oridc Chlorobc:nzme -· Chloroethanc ChloroCorm ChloroiiiCihanc · Dibi'OI'IIOclll.oromcthane 1,1-Dichloroechane 1.2-Dichlorocthanc 1,1-Dichlorocthenc 1,2-Dichlorocthene l.Z-Dichloropropane cis-1,3-DichJoropropenc rrans-1 ,3-Dichloroprop:nc 1,2-Diclhylbenzene Ethylbenzenc 2-HCIUUIOIIC 4-Melhyl-2-penlanonc !Methylene Chloride n-Hexane Sl)'rent

l,I,:Z,2-Tclrachloroclhanc Telmdllorocthenc

I Seep619 NSSOOt

MND16-.06U..ol00 4191-003 REG

3130/94 Result Val.. Code

Uolts UOIL 10 UJ..C UOIL IOC u tJO.IL ux u UOIL su UOIL su UOIL su UOIL 10 u UOIL to u UOIL su UOIL su UOIL su UOIL IOU UOIL su UOIL 1£ u UOIL u UOIL su UOIL su UOIL su UOIL su UOIL su UOIL su UOIL su UOIL su UOIL 5U UOIL ICU UOIL UJU UOIL su UOIL I(J U UOIL su UOIL su UOIL su


I I I Seep6U Seep6J4 Seep62J

~· NS700J NSIOOJ MNDl6-Ull-OlOO MND16-1308..ol00 MNDl6-.0303-0lOO

4791-804 REG 4791-005 REG 4791-006 REG YJ0/94 YJ0/94 YJ0/94

Result Val.. Code Result Val.. Code Result VIII. Code

I(J UJ-C· IIJ UJ-C· 10 UJ-C-100 UJ-S+ 100 u 100 u ---100 UJ·S+ 100 u tOO u i

su su su i su su su ! ---su su su

10 u 10 u IC U . IOU 10 u Ill U su su su su su 5U su su su

·--·---UIU UIU 10 u - ··~. su .'IU 50 10 u UJU !0 u ·--su su "'U su su su -su su su S UJ-S+ su su su su su su su su -su su su su 50 su

··-su su su su 3U ~ u

UJU Ill U l(U

I(J U Ill U uu su su su

10 u It U l(J u su su su su su su su su su

;;:a~ B 0 :s. c 5· 6.. ::s "'0

0~

~ ~

1

g .P' z ~

0~ s] a~ g''"CI ... :r -el ~::

::!1 6:

i

> "0 ;:v]

~~ .!.Jrn

• Toluene UGIL 1.1.1-Trichloroethane UOIL 1,1.2-Trichloroethane UGIL Trichloroethene UGIL 1,1 ,2-Trichlorotrinuoroe UOIL Vinyl Acetate UOIL .. Vinyl OIJoride UOIL Xylene, Total UOIL Tentatively Identified Compounds


su su su su ---su su 5 u su ····--~------su su su su - -su su su su

su su su su ·---

I~ u I~ u IC U IC U Ill U Ill U I~ u I~ u 1----"-1 su su su su --

I I I

::03: s. g 5· a 1:' ., OJ ~ ~ i

~ f

0~ §J [~ :0~ ':€.-

::!! IS:

i ::1

> .,-o ~l. m>c clom

• MOUND NEW PROPERTY ____ ... Mound Sttp I

·- SDmpltiD

EPA Samplt ID

. Lob Samplt ID Dott Colltcttd

-~-····

Semi-volatile OrpDics Acenaphthene -Acenapfnhyfene .... Anthracene Benzo(a)anthracenc Benzo(a)pymle

Benzo(b)Ouoranlhenc Benzo{J.h.i)perylene Benzo(t)Ouoranlhenc Benzoic Acid Benzyl Alcohol 2-Benzyl-4-d!Jorophenol bis(2-0lloroedJoxy)lncdJanc bis(l.Qioroelbyl)elher bls(2-f!lbylbellyl)phlhalate 4-Bromophenyl-pltcnylelher Butylbenzylphthalarc Carbazole 4-Qioro-3-melhylpbenol 4-ChloroaniUnc 2-Chloronaphlhalcnc i2.(]doropbenol !4.(]dorophcnyl-phenylelher !CJuysene

IDI-n-butylphlhalate ,DI-n-«tylphlhalate Dlbcnzo(a,h)anthracenc Dibenzofuran 1.2-Dic:hlorobenzenc I ,3-DichJorobe:nzenc 1,4-Dichlorobenzl::nc 3,3' -Dichlorobcnzidinc

---

I Seep616 -NS1001

MND16-..0l06-0l00 4790-001 REG

3119194 Result Vai.Cocle

. Units UG/L UJU UG/L J(J u UG/L Ill U UG/L 10 u UG/L ·~ u UG/L IC U UG/L IC U UGIL IC U UG/L S UJ-C UG/L UlU UGIL ICIU UG/L ·~ u UG/L 10 u UG/L HJU UG/L 10 u UG/L IC UJ-C UG/L 10 u UG/L 10 u UGIL u UJ-C UG/L IC U UG/L UIU UG/L 10 u UG/L Ill U UG/L HI U-8 UG/L Ill UJ-C UG/L. 10 u UG/L JtU UG/L IC U UG/L UIU UG/L I~ U UOII. ___ lilY -

• • APPENDIXE Seep Sampling Results (1994)

I J I . ~-·--

Seep610 Seep 610 (DUP) Seep617 Seep6:20 ·-·-NS%001 NSlOll NS3001 NS4001

MND16-090J.0200 P!IND16-0903-1ZOO MND16--0317-0l00 MND16--0408..0l00 4790-003 REG 4790-004 REG 4791..001 REG 4791-002 REG

*~··"-3119194 03119194DUPE 3130194 3130194

Resull VIII. Code Result VIII. Code Result Val. Code Result VaL Code -- - ·---

---· IIU ICJ U UlU UlU IIU UJU UlU 10 u

---~~--

IIU I~ u Ill U Ill U --IIU ·~ u Ill U Ill U IIU 10 u 10 u I~ u --IIU Ill u Ill U 10 u ---IIU Ill u l(U IOU

jo J( u 10 u ·----IIU u - -~-.. --. 53 UJ-C SO UI-C s~ UJ-e 52 UJ-C IIU IOU Ill U IOU ·---

- 10 IC U IIU u IOU IIU 10 u Ul u I(] ~lJ

·-· -I -------IIU IC U UIU 10 u ·-·-IIU IC U-B Ill U-B 10 u ----IIU UJU Ill U 10 u

II UJ-C 10 UJ-C 10 UJ-C 10 UJ-C IIU UJU 10 u 10 u IIU ICJ U 10 u 10 u II UJ-C Ul UJ-C 10 UJ-C Ul UJ-C --IIU 10 u to u IOU IIU 10 u It U IC U ---IIU 10 u J( u IC U --IIU 10 u ~~ u UJU -·-----II U-B 10 U-B Ul U-B l<l U·B II UJ-C IC UJ-C l(J UJ-C Ill UJ-C IIU lc u Ill U 10 u IIU UJU Ill U uu ---IIU 10 u IC U ICU IIU 10 u I( U Ill U ---IIU 10 u ·~ u UJU

'··········----II ,!! - ...

10 ,lJ_- ..... __ Ill u

-10 u

-

::03:: 0 0 ~- g o· c. ::s '"tl

0~

~

f

g .!-" z ~

0~ ~J ['"tl ... ::r -el i:.

!! !!. D.

::0

1

> '0

i] 0 D. c;n sc· \()[rl

• 2,4-Dicblorophcnol Diethylphthalate 2,4-Dimethylphenol Dimelhylphthalate 4,6-Dinltro-2-melhylphenol 2,4-Dinlttophenol 2,4-Dinlttotoluene 2,6-Dinltrotoluene Ftuoranlhene Fluorene Hellacblorobenzc:ne HeJiacblorobutadiene Hellacblorocyclopentadiene Hell&Cbloroelhane lndeno( 1,2,3-c,d)pyrene

lsophorone 2-Melhylnaphthalene 2-Melhylphenol 4-Melhylphenol N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Naphthalene --2-NittoanlUne l-NittoanlUne -4-NittoanlUne Nittobenzc:ne 2-Nitrophenol 4-Nitrophenol 2,2'-ollybis(I-Cbloropropane) Pentachlorophenol Phenan~ne

Phenol 'P)'n::ne 11.2,4-Tricblorobenzc:ne 2,4,S-Tricblorophenol 2,4,6-Tricblorophenol Tentatively ldenlified Com~

UGIL I U UG/L I U UG/L I U UOIL I U UOIL 2~ u UG/L 2~ u UOIL IC U UOIL IC U

UOIL I(JU

UGIL 10 u UOIL 10 u UG/L 10 u UOIL IC U UOIL IC U UOIL IC U UOIL I~ U UOIL IOU UOIL IOU UOIL I(JU

UOIL 10 u UOIL 10 u UOIL 10 u UOIL 26 u UOIL 26 UJ-C UOIL 26U UOIL 10 u UGIL uu UOIL 2~ u UGIL I~ u UOIL 26 u UOIL 10 u UGIL 10 u UOIL 10 u UOIL 10 u UGIL· 26 u U<M. I(J u

L_ -- - ..


JJU I( u I U I U --·----JJU HJU IOU IOU --JIU I(J u I U IC U

---~--

IIU I(JU I U IOU --2~ u 2SU 26U 26 u - -26U 2S U 26 u 26U -JIU IC U I(J u I(J u JJU I(JU I(J u IOU JJU I(J u IOU 10 U IIU IOU IOU 10 U ----JIU I(J u 10 u I(JU

-··-···--JJU I(JU 10 u I(J u

·-JIU IOU IOU I(JU -

10 u IOU I~ u JJU ----JJU IOU IOU IOU

·-·-JIU IC U IG U 10 u

-JJU I(J u I(JU 10 u __ , _____ JJU IC U 10 u IOU --·--IIU I(J u IOU 10 u ---·--JIU I(J u I(J u IOU

-·-·--· JJU I(J u I(JU IOU

·-··-·------JIU I(J u IOU IOU

·----·-·-· 26 u 2S U 26U 26 u -2~ UJ-C 2S UJ-C 26 UJ-C 26 UJ-C 26U 2SU 26U 26U JIU 10 u 10 u IOU JJU IOU IOU 10 u --2~ u 2SU 26U 26 u ---JIU IOU 10 u 10 u

-·-·-26U 2S U 26 u 26U

. ------JJU I(J u I(J u 10 u --JJU I(J u I(J u IOU JJU I(JU I(JU IC U --JJU 10 u 10 u I(J u

-·-26 u 2SU 26 u 26 u -JJU l~u I(J u IOU

2

~3::: ~ 8 c;;· ==' -· 0.. g "'0

0~

~ ;r 1

g ~

~ o;r ~J [d! -el ~~

""'-::!1 ~ c: ~ ~

"'0~ Jll'g ~ ::::1 rn9: ' >c ern


_ -------·--··- .. Mound Seep I SampleiD ------·

EPA Sample ID

---·-------·.Lab Sample ID Date Collected --

1---------

Seml-•olallle Orpnlcs

Acenaphthene --Acenaphlhylenc ---Anthracene Benzo(a)anthmcene Benzo(a)pyrene Benzo(b )Ouoranthene Benzo(g,h.i)pcrylene Benzo(lt)Ouoranthene Benzoic Acid

···-Benzyl Alcohol 2-Benzyl-okhlorophenol bls(2-Chloroelhoxy)melhane bis(2-Chloroelhyl)ether bis(2-Ethylhexyl)phlhaJate 4-Bromophenyl-phenylelher ButylbenzylphlhaJate Carbazole 4-Chloro-3-melhylphenol 4-ChloroaniUne 2-Chloronaphlhalene 2-Chlorophenol 4-Chlorophenyl-phenylelher Chrysene Di-n-butylphlhaJate Di-n-octylphlhaJate Dibenzo(a,h)anthracene Dibenzofuran .1.2-Dichlorobenzene I J-Dichlorobenzene 1,4-Dichlorobenzene 3,3'-Dichlorobenzidine

I Secp619 NSS001

MND16--0611-0l00 4791-003 REG

3130194 Raul I VaL Code

Unlls UGIL 10 v UGIL J( u UGIL IC U UGIL IOU UGIL I~ u UGIL I~ u UGIL I~ u UGIL ·~ u UGIL Sl UJ-C UGIL 10 u UGIL IOU UGIL 10 u UGIL 10 u UGIL 10 U-B UGIL 10 u UOIL 2 J-C-UGIL IC U UOIL IC U UGIL I~ UJ-C UGIL IO u UOIL I~ u UGIL 10 u UOIL 10 u UGIL 10 U-B UOIL 10 UJ-C UOIL IC U UGIL ·~ u UOIL ·~ u UOIL I~ u UOIL 10 u UOIL I~ u

• • APPENDIXE Seep SampUng Results (1994)

I I -Secp62l Seep614 ------ See~6l3 NS6001 NS7001 NS8001

MND16--ll13-0l00 MND16--1308-0200 MND16-0303-0200 4791-004 REG 4791-005 REG 4791-oo6 REG

.. 1--· ---- 1--3130194 3130194 3130194

Resull VaL Code Raul I VaL Code Raul I VaL Code

-I~ u 10 u 10 u --. ·~ u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u IOU IOU 10 u IOU IOU

I~ u I~ u 10 u 10 u I~ u IOU Sl UJ-C s~ UJ-C s~ UJ-C 10 u wu 10 u 1--

-IOU ou I~ u uu UJU 10 u - -- -· -IC U 10 u 10 u

·- -IC U 10 U-B 10 U-B I~ u 10 u 10 u I~ UJ-C 10 UJ-C

-I~ UJ-C

I~ u 10 u 10 u I~ u 10 u 10 u 10 UJ-C 10 UJ-C 10 UJ-C IOU IOU IOU I~ u IC U IOU 10 u I~ u I~ u 10 u I~ u 10 u 10 U-B I~ U-B I~ U-B IC UJ-C I~ UJ-C 10 UJ-C I~ u I~ u I~ u I~ u IOU IC U I~ u IC U I~ u IOU IC U ·~ u IOU I~ u 10 u 10 u I~ u 10 u

~:: " 0 :s. c::

~- 8. 0 :::1 '"l:l OJ

ro ~ ~

g :" z ~

0~ ~] g-'"l:l .. ::r -el ~:

::!! " c: ~ g

'"l:l~ &l'S " :::1 me: ' >c ::rn

• 2,4-Dicblorophcnol Diethylphlhalate --2,4-Dimethylphcnol Dimethyl phthalate 4,6-Dinitro-2-methylphcnol 2,4-Dinilrophenol 2,4-Dinilrotoluene 2,6-Dinilrotoluene Auoranthcne .. -Auorene Hexacblorobenzene Heuchlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lndeno( I ,2,3-e..d)pyn:ne lsophorone 2-Methylnaphthalene 2-Methylphenol

-· 4-Methylphenol N-NitroscHfl-n-propylamine N-Nitrosodiphenylamine Naphthalene 2-Nilroaniline .. 3-Nilroaniline 4-Nilroaniline Nilrobenzene 2-Nilrophcnol .. 4-Nilrophcnol 2,2'-oxybis( 1-Chloropropane) Pentacblorophcnol Phcnanthn:ne Phenol .. Pyn:ne I ,2,4-Trichlorobenune 2,4,S-Trichlorophcnol 2,4,6-Trichlorophcnol Tentatively Identified Compounds

UOIL Ill U UGIL Ill U UOIL Ill U UGIL Ill U UGIL 2E U UOIL 2E U UOIL IC U UGIL Ill U UOIL Ill U UOIL IIJU UOIL Ill U UOIL Ill U UOIL 10 u UOIL IOU UOIL 10 u UGIL Ill U UOIL Ill U UOIL Ill U UGIL lllU UOIL Ill U UOIL Ill U UOIL Ill U UGIL 2~ u UOIL 26 UJ-C UGIL 26U UOIL Ill U UOIL IOU UOIL 26 u UGIL 10 u UOIL 2E U UOIL Ill U UGIL Ill U UOIL Ill U UOIL Ill U UOIL 26U UOIL 10 u

7


I U Ill U Ill U ·- -· Ill U Ill U Ill U

·-·-10 u lllU Ill U IOU Ill U IOU 26U 2S U 26U .... 26U 2S U 26U Ill U IOU IC U Ill U Ill U lllU Ill U lllU lllU ---Ill U Ill U Ill U - . --~ 10 u lllU I<JU

·----· I~ u lllU lllU

·-·-Ill U 10 u 10 u I

_j

lllU 10 u IOU I

Ill U lllU lllU I I --·

Ill U IOU 10 u --·-Ill U -~ IC U u Ill U 1J• IC U

------IC

10 u lllU -· lllU ---· Ill U lllU lllU

···-·~u lllU lllU --·---· Ill U lllU lllU

-:l!iU su 6U 26 UJ-C 2S UJ-C 26 UJ-C 26U 2SU 26U

·-10 u 10 u 10 u 10 u lllU lllU

-26U 2S U 26 u IC U -Iii Ill U

... u --

2~ u 2SU 26 u Ill U IOU 10 u Ill U IC U IC U

-·· Ill U Ill U I~ u Ill U Ill U Ill U --2~ u 2S U 26U --Ill U 10 u IOU

I I

:0:03:: n o s. c: 5· a ::l .,

0~

~ ~ ~

g ;..n

f ~l 9~ !f., ., ::r -Ill ~:

::n f5: ~ l

.,~ ~i m9: ' )C

i::im


·~··-·····---

Mound Seep I Sample ID

-~--

EPA Sample ID -- lob Sample ID --------Date Collected -----··

-·------· Pcst~lda ud PCBt Aldrin aJpha-Btic ___ ..

alpha-Ollordanc Aroclor-1016 Aroclor -1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 - -----

·-· Aroclor-1260 ---·--.. beta-BHC ---4.4'-DDD 4,4'-DDB -------4,4'-DDT

--·· dclta·BHC Dieldrin Endosulfan I ---Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde_ Endrin Ketone gamma-BHC (Undanc) gamma-Ollordane Heptachlor Heptachlor Epoxidc [p.p'-Methoxychlor Toxapllene

--------Seep6Ui NS1001

MND16-0206-0200 4790-001 REG

3129/M Result VaL Code

UoltJ UOIL 0.052 u UOIL O.OS..! u UOIL 0.052 u UOIL IU UOIL 2.1 u UOIL 1U UOIL IU UOIL IU UOIL I U UOIL I U UOIL o.os" u UOIL 0.1 u UOIL 0.1 u UOIL 0.1 u UOIL o.os.~u

UOIL 0.1 u UOIL 0.052 u UOIL 0.1 u UOIL 0.1 u UOIL 0.1 u UOIL 0.1 u UOIL 0.1 u UOIL 0.05 u UOIL o.os~ u UOIL 0.05:.~U

UOIL 0.05..! u UOIL" 0.52 u UOIL 5.2U

• .• /PENDIXE • Seep Sampling Results (1994)

I .. ---~ Step6l0 Seep 610 (DUP) Seep617 Step610 .. NS2001 NS:ZOU NS3001 NS4001

MND16-fi03.0200 MND16--0903-1200 MNDI6--0317-0200 MNDI6-0408-0200 -4790-003 REG 4790-004 REG 4791-001 REG 4791-002 REG

3129/M 03129/MDUPE 3IJOJ94 3IJOJ94 Result VaL Code Result VaL Code Result Val. Code Result Val. Code

o.os .. u 0.05.1 u O.OSI u 0.051 u o.os~ u 0.052 u O.OSI u O.OSI u 0.05 u o.os~ u 0.051 u 0.051 u

IU IU IU IU l.l u 2.1 u ..!U 2U

IU 1U I U IU IU IU IU IU IU IU I U I U -- --------· --·-IU IU IU IU -IU IU IU IU

O.OS2 u 0.052 u 0.051 u 0.051 u -0.1 u 0.1 u 0.1 u 0.1 u -0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u

O.OS.; U 0.05.< u 0.051 u O.OSJ U 0.1 u 0.1 u 0.1 u 0.1 u

0.05.; u 0.05~ u 0.051 u 0.051 u - -0.1 u 0.1 u 0.1 u 0.1 u -0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u

0.05:.~U O.OS:.~U O.OSI U 0.051 u 0.0.52U 0.052 u 0.051 u 0.051 u 0.05 u 0.052 u 0.051 u 0.051 u o.os u 0.05 u 0.051 u 0.051 u o.s. u 0.5.; u O.SI U 0.51 u

5.:.1 u 5.:.1 u 5.1 u 5.1 u

6'~ ;S, c 5· a ::s '1:1

0~

~ ~ 1

g }II

z ~ ~

~] [~ -el ~:

::!'! !!.. 0.

i ::l

'1:1~ ~] n ::s me: ' >c wm

• MOUND NEW PROPERTY ·- ----

Mound Seep I ·---·----··-·-----· Sample/D

EPA Sample ID lAbSampkiD Date Collected ---

..

Pestk:ldes and PCBs Units Aldrin UGIL

····-alpha-BHC VGIL .. alpha-Chlordane UGIL Aroclor-1016 UGIL Aroclor-1221 UGIL Aroclor-1232 UGIL

-Aroclor-1242 UGIL Aroclor-1248 UGIL ..... Aroclor-12S4 UGIL --Aroclor-1260 UGIL bela-BHC UOIL 4,4'-DDD UGIL 4,4'-DDB UGIL .. 4,4'-DDT UGIL della-BHC UOIL Dieldrin UGIL Bndosulran 1 UOIL Bndosulran II UGIL Bndosulran Sulrare UGIL Endrin UOIL Bndrin Aldehyde UGIL Bndrin Ketone UGIL gamma-BHC (Lindane) UGIL gamma-OIIordane UGIL Heptachlor UGIL Heptachlor Epolide UOIL p.p'-Methoxychlor UOIL Toxaphene

--------,_ UGIL

. f-· I Seep619 NSSOOI

MND16-..0611-0200 4791..003 REG

Y30/94 Result Val. Code

O.OS..: u O.OS2 u o.os~ u

IU 2.1 u

I U IU I U I U IU

o.os u 0.1 u 0.1 u 0.1 u

O.OS2 U 0.1 u

O.OS2 U 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u

O.OSl U O.OS2 U O.OS2 U O.OS2 U

O.S2 U S.2U


Seep621 Seep614 Seep623 NS6001 NS7001 NS8001

MND16-1113-0200 MND16--13011-0200 MND16-..030J-0200 4791-004 REG 4791..005 REG 4791-006 REG

Y30/94 Y30194 Y30/94 Result VII. Code Result VII. Code Result Val. Code

I

o.os u O.OS2 u O.OS2 u ! ___ , O.OS2 v O.OS2 u O.OS2 u I o.os~ u O.OS..: u O.OS:l u

IU I U I U

2.1 u 2.1 u 2.1 u IU I U I U

IU I U I U I U I U I U --·--IV IU I U IU IU IU

O.OSl u O.OS:l U O.OS2 U

0.1 u 0.1 u 0.1 u ---0.1 v 0.1 u 0.1 u ----0.1 u 0.1 u 0.1 u

o.os~ u O.OS2 U O.OS2 U 0.1 u 0.1 u 0.1 u

o.os~ u O.OS2 U . O.OS.: U 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u ---0.1 u 0.1 u 0.1 u --0.1 u 0.1 u 0.1 u

O.OS2 U o.os u o.os u O.OS.: U o.os~ u o.os~ u O.OS2 U O.OS2 U o.os u o.os u O.OS2 U O.OS..: U o.s~ u O.S:.!U O.S:l U S.2U S.2 U S.2 U

-- ----

:;a~ ~ g §:a g ~ 0~

~ ~

1

0 c ~ z ~

0~

~l g'~ ... ::r -el ~:

::!1 n c:

i ~

;J>

l:S n = me: ' >< i=m


Mound Seep I -SampleiD

EPA Sample ID -----· Lab Sample ID Date Collected -

-·-·------··· -· -

Anions • Chloride Anions • Chloride -----·

Anions • tluortde Anions • Fluoride

Anions • Sulfate Anions -Sulfates -----·

Anions • NOiNOJ Anions • NOIN~

·-··---·--···--·-

MOUND NEW PROPERTY Mound Seep I ------·-

SampleiD EPA Sample ID ----Lab Sample ID Date Collected ·-

-·-------Anions • Chloride Anions - Chloride

Anions • tluortde Anions • Fluoride

Anions • Sulfate Anions -Sulfates

Anions- NOiN~ Anions - N()INO,

Seep616 NSIOOI

MNDI6-..0l06-0l00 AA5358REG

lfl9194 Result Val. Code

Units Man.. 1026

Units MOIL 0.14

Units Man.. 144 J-H,C·

Units Man.. 1.7

Seep619 NSSOOl

MND16--0611..0ZOO AA5384REG

Y.lOJ94 Result Val. Code

Units Man.. 46.3

Units MGn.. 0.14

Units Man.. 51.5 J-H,C-

Units Man.. 0.02U


I Seep610 Seep 610 (DVP) - Seep617 Seep6l0 NSlOOI NSlOII NSJOOI NS4001

MNDI6-0903-0ZOO MNDI6--0903-Il00 MNDI6-..0317..0ZOO MNDI6--0408..0ZOO AA5363REG AA5369REG AA5374REG AA5379REG

lfl9194 Olfl9194DVPE Y.lOJ94 3130194 Result VaL Code Result Val. Code Rrsult Val. Code Rrsull Val. Code

75.9 76.~ 357 191

0.17 0.15 0.15 0.18

74.5 J-H,C- 74.5 J-H,C- 84 J·H,C- 83 J-H,C-

-- -· 0.59 0.~ 0.3 0.02 u

-·-·-- -

Seep6ll Seep614 Seee 6D -NS6001 NS7001 NS8001

MND16--1113-0ZOO MND16--1308-0l00 MNDI6-..0303-0l00 AA5404REG AA5389REG AA53,_.REG

3i30J94 3130194 3130194 Result VII. Code Result VaL Code Result Val. Code

27.1 30.3 363

0.15 0.2i 0.18

'54 J-H,C- 46 J-H,C- 9.l J-H,C-

0.02U 0.02U 0.26

iti:S:: 0 0 s. c [!!. 6.. g ., 0~

~ ~ 1

g IJI

z ~

0~ g~ 3~ ~., .. ::r -e: :go ~-

:!1 !!. Q.

it!

~

.,~ &l~ 0 ::s rnS: I >c \:i;rn


Mound Sup I --------·· SampltiD ------

EPA Sample ID ·----·-···--· LabSampleiD --------.....

Date Collected ---·-·

-· ----···

AlkaUultJ Allcalinity --------···-··

MOUND NEW PROPERTY Mound Seep I -

SampleiD ---EPA Sample ID Lab Smnple ID ----·-Date Collected

---AlkaUullf ------Allcalinity -

Seep616 .. NSIOOI

MNDI6-..0206-0100 -·

REG ---· Yl9/94

Result VaL Code

Units MOIL 285

Seep619 NS5001

MNDI6--0611-0200 REG

3130194 Result VaL Code

Unlls MOIL 177


Seep610 Seep 610 (DUP) Seep617 Seep620 NSlOOI NSlOII NSJOOI NS4001

MNDI6--0903-0200 MNDI6--0903-Il00 MND16-..ol17..0200 MNDI6--0408-0200 REG REG REG REG

Yl9194 0Yl9194DUPE 3130194 3130194 Result v ... Code Result Val. Code Result VaL Code Result VaL Code

280 283 298 245

Seeo621 Seep614 Seep62l -NS6001 NS7001 NS8001 I

MNDI6-1113-0200 MNDI6-Il08-0200 MNDI6-..ol03-0200 REG REG REG

-···-·· 3130194 3130194 3130194

Result VaL Code Result VaL Code Result VaL Code

211 227 2811 -

S'~ :s. c 5· 6. ::::1 "0 og

!"'

~ ~

1

0 c !A

f il =~ [~ :0~ -g_

:n ~

i

> ;a''tl (JQ1il ~ ::::1 me: ' )(

O:m


------- Mound Step I SampkiD

-----EPA Sample ID

1--·----. Lab Sdmplt ID Date Collected

Ammonia Uolts Ammonia MOIL

-------MOUND NEW PROPERTY

------Mound Sup I SmnpltiD --------

EPA Sample ID ------·· - Lab Sample ID

Dare Collected -----· -·------

·-·--Ammoola Uults -Ammonia MOIL -·

-·· L-. ---

I Seep616 NSIOOI

MNDI6-0:zo6.0200 REG

3119194 Result Val. Code

O.OJU

Seep619 NS5001

MND16-0611.0200 REG


O.OlU

'

•• • APPENDIXE Seep Sampling Results (1994)

I I -·· Seep610 Seep 610 (DUP) Seep617 Seep620 NS2001 NS20U NS3001 NS4001

MND16-.o90J.0200 MNDI6-0903-1200 MNDI6-0317.o200 MNDI6-.e408-8200 REG REG REG REG --····-

3119194 03119194DUPE 3130194 3130.194 Result VII. Code Result Val. Code Result Val. Code Result Val. Code

----..

0.03 u 0.03U 0.03U 0.03 u --·h ____

--·

Seep621 Seep614 Seep6l3 - I NS6001 NS'JOOl NSIOOI MND16-1113-0200 MND16-IJ08.0200 MNDI6-0303-0200

REG REG REG ---~- ··-

3130194 3130194 3130194 Result VII. Code Result Val. Code Result Val. Code

-O.OJU O.OlU 0.03U

---

::o:;: ~ g ia: a 0 ::I ~

0~

~

f

g y. z n ~

0~

~~ jf~ ... :r -~ ~:

'11 [ 0.

::0 .g ~

~~ &l"R n ::I rne: ' >< :::itn


Mound Seep I ·---·------Samplt/D -----------·

EPA Sample ID -

LobSampkiD -· -. Datt Colltcttd ·-

----·-····

Total JQelclabl Nitrogen Total Kjeldahl Nitrogen

-------------------

MOUND NEW PROPERTY MoundSttpl

Sampk/D

EPASampkiD -LobSampkiD ------Datt Colltcttd ------

----··

Total JQelclabl Nitrogen Total Kjeldahl Nitrogen 1--

r---- --··· Seep 616 NSIOOI

MNDI6--0106-0100 AAS3SSREG

Yl9194 Result Val. Code

UDIII MOIL 0.23 J-C-

Seep619 NS5001

MNDI6-.o611.0100 AA5381 REG


Unlll MOIL o.~ J-C-


Seep610 Seep 610 (DUP) Seep617 Seep620 -NSlOOI NSlOU NS3001 NS4001

MNDI6-0903-0200 MNDI6--0903-UOO MNDI6-41317.0100 MNDI6--0408.o100 AAS360REG AAS366REG AAS371 REG AAS376REG

Yl9194 0Yl9194DUPE Y30J94 Y30J94 Result VII. Code Result VII. Code Result Val. Code Result VII. Code

-

0.31 J-C- 0.16 J-C- O.IS J-C- 0.3 J-C-

Seep611 Seep614 See1J613 NS6001 NS7001 NS8001

MNDI6--IIl3-0100 MND16--1308-0100 MNDI6-41303-0100 AA5401REG AA5386REG AA5391REG - .. -·-

3130194 3130194 3130194 Result VII. Code Result VII. Code Result VII. Code

··----

0.1 UJ-C O.lS J-C- 0.18 J-C-

--- -- ------

::a:: n o ~- § -- 0.. g ., OJ ~ ~ ~

0 c:: v.

z n ~

0~ fP~ 3~ [., ... ::r -~ ~:.

::n 6:

f ::1

.,,G'" Jcl'S n = me: ' >< com


MoumlSeepl -----------SampleiD

--· EPA Sample ID Lob Sample ID

·-· Date Collected

-·

Total Pbespborus Tolal Phosp~ _

------MOUND NEW PROPERTY

Mound Seep I .. SamplelD ---

------ EPA Sample ID LobSamplelD

-·-·-Date Collected

--

Total Pbespborus Tolal Phosphorus

----------

I Seep616 NS1001

MND16-..0106-0:ZOO REG


Units MOIL o.osu

Seep619 NSSOOI

MNDI6--06U..O:ZOO REG

]130/94 Result Val. Code

Units MOIL 0.1~


I Seep610 Seep 610 (DUP) Seep617 .. seee 6:ZO NS:ZOOI NS%011 NS3001 NS4001

MNDI6--0903-0100 MND16--0903-1100 MNDI6-..0317..0100 MND16--0408..0100 REG REG REG REG -----·

3119194 03119/94DUPE Y.J0/94 Y.J0/94 Result Val. Code Result Val. Code Result Val. Code Result Val. Code

---o.osu O.OSU 0.07U 0.4~ -------

-Seep611 Seep614 Seep613 NS6001 NS7001 NSBOOI

MNDI6-1113-0100 MND16--1308..0:ZOO MNDI6-..0303-0100 REG REG REG -------

]130/94 Y.J0/94 Y.J0/94 Result Val. Code Result Val. Code Result Val. Code

0.07U 0.37 o.osu ------- --

- ~. ----·-~ -- -··-- - -

:;~::~:,: ~ 0 ~. c ~. 6. g ., 0~

~ iif ~

0 c: }II

f oiif R-g 8~ [;q -Ill ~:

::!! ~

0:

~ g

.,~ Jg] ~ 1:1 me: I >c :Om


·-·· Mound Sup I SampleiD

EPA Sample ID lAb Sample ID Date Collected -

-

Total Dissolved Solids Totsl Dissolved Solids

MOUND NEW PROPERTY

Mound Seep I SampleiD

EPA Sample ID .... lAb Sample ID Date Collected

..

Total Dissolved Solids Totsl Dissolved ~olids

Seep616 NSIOOI

MND16-..0206-0200 REG

Yl9194 Result Val. Code

Units MOIL 23SO

Secp619 NSSOOI

MND16--0611..0ZOO REG

3f30J94 Result Val. Code

Uolts MOIL 320

• • APPENDIXE ~p Sampling Results (1994)

Secp610 Seep 610 (DUP) Seep617 Secp6ZO NS2001 NSZOII NS3001 NS4001

MND16-0903-0ZOO MNDJfi.-0903-1200 MND16--0317..0200 MNDI6--0408-0ZOO

REG REG REG REG

Yl9194 OY19194DUPE 3130194 3130194 Result VII. Code Result Val. Code Result Val. Code Result Val. Code -

529 S26 rm 684

Secp6Zl Seep614 Seep623 I

NS6001 NS7001 NS8001

MND16-1113-0ZOO MNDI6-1308-0200 MND16--0303-0ZOO I REG REG REG I

-3f30J94 3130194 3130194 I

Result VII. Code Result VII. Code Result Val. Code

---·--30.c 371 1060

- -- ---- -- --- -------

::oa::; 0 0 ;S, ~ !!!. [ g ., og

!"'

~ a' 1

g ~

z ~ .,

oa

~l If~ ~~ ~-

:!1 g. Q.

~ '8 ::1

.,~ ~g me: ' >< ~m



EPA Sample ID LobSampkiD -Date Collected

Total Orpnlc Carbon

Tolal Organic Carbon

MOUND NEW PROPERTY


EPA Sample ID LobSampkiD Date Colkcted

-·

Total Orpnlc Carbon

Tolal Organic Carbon

Seep616 NS1001

MNDI6--0l06-0ZOO 4790-001 REG

31Z9194 Result Val. Code

Units

MOIL 5.7 J

Seep619 NSS001

MND16--0611-0ZOO REG


Units

MOIL S.l J


--·- ----·--SeeD610 Seep 610 (DUP) Seep 617 Seep620 -----NSlOOI NSZ011 NS3001 NS4001

MNDJ6--0903-0lOO MNDI6--0903-UOO MNDI6--0317-0l00 MNDI6-0408-0ZOO REG REG REG REG ..

31Z9194 031Z9194DVPE 3130194 3130194 Result , Val. Code Result Val. Code Result Val. Code Result Val. Code

·-

---4.51 3J 4.61 2.2J _____ .. _

------

Seep6l1 Seep614 Seep6l3 ------NS6001 NS7001 NS8001

MND16--l113-0lOO MNDI6-·1308-0Z00 MND16--0303-0ZOO ··--·-·-

REG REG REG ...... ___ --3130194 3130194 3130194 --

Result Val. Code Result Val. Code Resnlt Val. Code

···-·--·---

------- ---1.8 J ).SJ 2.3 J

-------

~~ ~· § s· c. t:l "tt

0~

~ ~

~

g ~

f il 8~ [d! -el ~" ~-

:n ~

f

> '"tl"' !Ill'S " t:l me: 0 >c ~m


MowuiSeepl -----SampleiD

EPA Sample ID lAb Sample ID Date Collected

-

Total Suspeoded Solids Total Suspended Solids

MOUND NEW PROPERTY Mound Seep I

SampleiD EPA Sample ID lAb Sample ID Date Collected

Total Suspeoded Solids Total Suspendcd Solids

---~~-----

Seep616 NSIOOl

MNDI6-..0206-0100 4790-001 REG


Units MOIL 26

Seep619 NSSOOl

MND16-..o611~

REG l/J0/94

Result Val. Code

Units MOIL 139

:____ --- -- ~ --

• • APPENDIXE ~p Sampling Results (1994)

J Seep610 Seep 610 (DUP) Seep617 Seep620 NS2001 NS2011 NS3001 NS4001

MNDI6-0903-0200 MNDI6--0903-1200 MNDI6-..0317~ MNDI6--0408-0200 REG REG REG REG

3129194 03129194DUPE l/J0/94 Y.J0/94 Result Val. Code Result Val. Code Result Val. Code Result Val. Code

15 BU 25 317

'

Seep621 Seep614 SeepW NS6001 NS7001 NS8001

MND16-ll13-0200 MND16-IJ08..0200 MND16-0303-0200 REG REG REG

3130194 l/J0/94 l/J0/94 Result Val. Code Result Val. Code Result Val. Code

--BU 3](] 27

------

:::03::: 0 0 s. c 5· 8. :s ..,

0~

~ ~ ~

g ~

~ ~l 3~ ~~ -~ ~:

:!! 0 6: :::0 0

'8 ::l

..,~ ~'R 0 :s m9: • >< ~tn


Moutul Seep I

Sampi~ID

EPA Sampl~ ID

lAb Sample ID

Dot~ Collect~d

-

EXPLOSIVES 2-Amlno-4,6-Dinilrotolu 1.3-Dinilrobenzene 2.4-Dinilrotoluene 2,6-Dinilrotoluene HMX

-· Nilrobenzene Pentaerythritol Tetrani RDX ... Telryl 1,3,5-Trinilrobenzene 2,4,6-Trinllrotoluene

-MOUND NEW PROPERTY

Moutul~~pl

Sampl~ID

EPA Sample ID

lAb Sample ID

Dot~ Collect~d

EXPLOSJVF.S 2-Amino-4,6-DinilrOIOiu 1.3-Dinilrobenzene 2,4-Dinilrotoluene 2,6-Dinilrotoluene HMX Nilrobenzene Pentaerythritol Tetrani RDX Tetryl 1.3.5-Trinitrobem.ene 2.4.6-Trinitrotoluene

J Seep6U NSIOOI

MND16-0206-0100 REG

3119/94 Result Val. Code

Units UOIL 0.1 UJ-C UOIL 0.1 UJ-C UOIL 0.1 U1-C UOIL 0.1 U1-C UOIL 0.1 U1-C UOIL 0.1 UJ-C UOIL 3.4 1-C-UOIL 0.1 UJ-C UOIL 0.1 u UOIL 0.16 J-C-UOIL 0.1 UJ-C

Seep619 NS5001

MND16-0611~00

REG 3130194

Result Val. Code

Units UOIL 0.1 UJ-C UOIL 0.11 1-C-UOIL 0.34 UJ-C UGIL 0.1 UJ-C UOIL 0.1 UJ-C UOIL 0.1 UJ-C UOIL 111-C-UOIL 0.1 UJ-C UOIL 0.1 U-C UOIL 0.1 U-C UOIL _ _1M UJ-C

----

• APPENDIXE • Seep SampUng Results (1994)

I I Seep610 Seep 610 (DUP) Seep617 SeepQO NS2001 NS2011 NS3001 NS4001

MND16-0903-0200 MND16-0903-1200 MND16-~317~ MNDI~~

REG REG REG REG 3119194 03119/94DUPE 3130194 3130194

Result Val. Code Result Val. Code Result Val. Code Result Val. Code

0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 0.1 UJ-C 0.1 U1-C 0.1 U1-C

0.1 U1-C 0.1 U1-C 0.1 UJ-C 0.1 UJ-C 0.4 UJ-C 0.4 U1-C 0.44 1-C- 1.6 1-C-0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C -0.1 U-C 0.1 U-C 0.1 U-C 0.1 U-C 0.1 U-C 0.1 U-C 0.1 U-C 0.1 U-C OJ U1-C 0.1 UJ-C 0.1 UJ-C 0.1 U1-C

Seep621 Seep614 Seep623 NS6001 NS7001 NS8001

MND16-lll3-G200 MND16-1308-0200 MND16-41303-G200 REG REG REG

. 3130194 3130194 3130194 Result Val. Code Result Val. Code Result VaL Code

0.1 UJ-C 0.1 UJ-C 0.1 U1-C 0.1 UJ-C 2.9 1-C- 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 U1-C 0.1 U1-C 0.1 U1-C 0.4 UJ-C 2.7 1-C- 0.4 U1-C 0.1 UJ-C 0.1 UJ-C 0.1 UJ-C 0.1 u 0.1 u 0.1 u 0.1 u 1.8 0.1 u

L____ ··- Jl.! UJ-C 0.1 U1-C 0.1 U1-C ----- - ----- --- --- ----

::0~ (11 0 ;S. c:: l!l. 8. 0 :I ..,

O[ r

~ ~ 1

g ~

z ~

wl 9~ ~.., ... :r -el ~:.

!! 6: ::0

~

..,~ ~] me: ' >o t:!m


Mound Sup I SampkiD

EPA Sample ID LobSampklD Date Collected

Actlalum-217 Actinlum-227

Ameridum-241 Amcriclum-241

Gamma ScaD

8lsmulh-207 8ismulh-210 Ceslum-137 Cobalt-60

Isotopic: Plutonium Plutonlum-238 Plutonium-239n40

GammaSc:ao Potasslum-40

RADIUM-226 Radlum-226

Strontium 90 'Strondum-90

Isotopic Thorium Thorium-228 Thorium-230 Thorium-232

TrltlomJ Tridum

I

MDA

Ualts pCiJL 0.11

Units pC'IIL 0.03

Units pC'IIL <17 pCiiL <2.~

pCiiL <7.1 pCiiL <IS

Units pCiiL 0.~

pCi/L 0.21

Units pCi/L <100

Units pC'IIL 0.024

Units pC'IIL 1.9

Ualts pCiiL . 0.21 pCi/L· 0.18 pCiiL 0.14

Units pCiiL 330


I I I I I I I I Seep616 Seep610 Seep 610 (DVP) NS1001 NS2001 NS2011

MNDI'-.0206-0200 MND16-0903-0200 MNDI'--0903-1200 65-0110865.7 REG 65-000866.5 REG 65-0110867.3 REG

3129194 3129194 03129194DVPE Result UNC VaL Code MDA Result UNC Val. Code MDA Result UNC Val. Code

0.091}+/- 0.18 J-D 0.1~ O.lS+I- 0.2 J-D 0.11 0.063+1- 0.48 J-D

'

0.22+1- 0.24 J-D 0~ 0.009+1- 0.18 U-8 0.04 .0.081+1- 0.13 U-8

<17 N.A. u <I~ <14 N.A. u <13 <13 N.A .u <2. N.A. u <9.E <9.6 N.A. u <9.S <9.S N.A .U <7.1 N.A. u <I~ <10 N.A. u <14 <14 N.A .u <IS N.A u <18 <18 N.A. u <18 <18 N.A. u

-0.036+/- 0.14 \J-8 0.38 0.22+1- 0.35 0.28 0.000+/ 0.16 U-8 0.009+1- 0.13 U-8 0.24 -0.04S+I- 0.038 U-8 0.17 -O.CJ21+1- 0.02S U-8

<IOC N.A.U <-2S <-2S N.A.U <16 <16 N.A. u

0.39+1 o.~ U-8 0.013 0.31+1- 0.13 J-LS 0.03S 0.64+1- 0.29 J-LS

2.8+1- 1.3 J-L 2.S I.S+I- I.S U-8 2.3 1.8+1- I.S U-8

0.009+1- 0.1 UJ-S8 0.24 -0.036+/- 0.088 UJ-88 0.~ -0.054+1- 0.08~ UJ-58 0.027+1 0.071 UJ-8 0.21 0.04S+I- 0.1~ UJ-8 0.19 O.lS+I- 0.18 UJ-8

-0.009+1- 0.01~ UJ-85 O.IS -0.018+1- 0.017 UJ-85 0.14 -0.009+1- 0.01~ UJ-85

28+1- 170 U-8 33~ -81+1- 160 U-8 330 -110+1- 160 U-8

:;a3: n o ~- § o· c. ::I .,

og-r

~

f

g !-" z ~

rf [;}l ~~ ... -~ ~ g

:l> "tt"' ~'8 n ::s rnS: • >o ~1:11

• lsoloplc Uranium Units Uranium-234 pCiiL 0.18 0.96+1 Uranium-235 pCiiL 0.18 0.12+1-Uranium-238 pCiiL 0.1_11 0.34+1

.PPENDIXE • Seep Sampling Results (1994)

0.53 0.3~ 0.32+1 0.35 U-B 0.3~ 0.61+1- 0.48 U-B 0.1/ U-B 0.24 0.081+/ 0.2 U-B 0.24 0.29+1 0.2~ U-8 0.29 0.3 0.14+1 0.~ U-B 0.3 -0.027+1 0.15 U-B

::t'S: (11 0

~- § o· o. = 'tl 0~

~ ~

1

g u.

~ ~

0~ "] ~~ g-'tl ., ::r -t}l \0(11 \0

"""-:n ~

i

'tl~ <18] ~~ ' >C ~[rl


Mound Sup I

SamplelD EPA Sample ID LobSampklD Date Collected

A.c:tlulum-217 Actinium-227

A.merlclum-141 Americlum-241

Gamma Scan

Bismuth-207 Bismuth-210 Cesium-137 Cobalt-60

Isotopic Plutonium Plutonium-238 Plutonium-239n40

Gamma Scan Potassium-40

RADIUM-2l6 Radium-226

Strontium 90 Strontium-90

Isotopic Thorium Thorium-228 Thorium-230 Thorium-232

Trltlum3 Tritium

I

MDA

Uults pCiiL O.ll

Units pCiiL 0.01

Units pCiiL <8.3 pCiiL <9.6 pCiiL <II pCiiL <21l

Units pC"a/L 0.31 pC"a/L 0.19

Units pCiiL <-7.7

Units pC"a/L 0.018

Units pC"a/L 1.8

Units pC"a/L 0.24 pCiiL 0.21 pCiJL 0.16

Units pCiJL 331J


I I I I I I I Seep617 Seep620 Seep619 NS3001 NS4001 NS5001

MND16-0317-0l00 MND16--0408-0200 MNDlfi.-0611-0200 65-000902.5 REG 65-000903.3 REG 65-000904.1 REG

3130194 3130194 3130194 Result UNC VII. Code MDA Result UNC VII. Code MDA Result UNC Val. Code

0.099+1- 0.14 J-D 0.1 0.15+1- 0.17 J-D 0.14 0.43+1- 0.31 J-D

0.22+1- 0.21 1-D 0.04 0.045+1- 0.21 U-B 0.03 0.40+1· 0.35 J-D

<8.3 N.A. u <18 <18 N.A. u <0.14 <0.14 N.A. u <9.E N.A. u <18 <18 N.A. u <4.1l <4.(1 N.A. u <II N.A.U <6.~ <6.~ N.A.U <6.6 <6.6 N.A. u <21l N.A.U <18 <18 N.A.U <17 <17 N.A. u

---0.027+1- 0.24 U-B 0.3 0.021+1- 0.1~ U·B 0.39 0.13+1- 0.26

-0.021+1· 0.028 U-B 0.19 -0.018+1- 0.019 U-B 0.24 -0.054+1- 0.04~ U-B

<·7.7 N.A.U <98 <98 N.A.U <-15 <-15 N.A.U

'

0.13+1· 0.13 U-B 0.02 0.81+1- 0.24 J-LS 0.027 0.52+1- 0.25 U-B

0.51+1- 1.1 U-B 2.l 1.1+1- 1.4 U·B 1.9 0.64+1- 1.2 U-8

0.063+1- 0.12 UJ-SB 0.2 0.14+1- 0.16 J.S 0.28 0.50+1 0.~~ I·S 0.054+1- 0.12 UJ-B 0.17 0.090+1· 0.15 UJ-B 0.24 0.39+1 0.3 J-S

0.045+1· 0.08 J.s O.ll 0.090+1- 0.11 J.S 0.18 0.13+1- o.u J-S

220+1 171l J-LS 331l -62+1- 161l U-B 331l -120+1· 161l U-B

:;c~ n o :5. c: !!!. 6.. 0 ::s ., OJ ~

f

8 yo z ~

~~ ~] [~ -~ ~n ~-

!! 6: :;c

~

.,~ &'.:'"8 n ::s t;n~ ~tTl

• Isotopic Uranium Units Uranlum-234 pCi/L 0.3 Uranlum-235 pCiiL 0.23 Uranlum-238 pCi/L 0.28


0.40+1- 0.41 U-8 0.24 0.96+1- 0.4§ 0.3 0.80+1- 0.48 0.11+1- 0.19 U-8 0.18 0.21+1- 0.21 U-8 0.23 0.11+1- 0.19 U-8

0.045+1 0.14 U-8 0.22 0.21+1- 0.21 U-8 0.28 0.11+1- 0.19 U-8

::03: (11 0

~- § s· o. ::t ., og

r'

~

f

g Y' z ~

~~ 9~ B"~ -l}l ~(11

""'-~ Q.

i;' '8 ;l

.,~

~i r;n~ !:jm


Moutul s~~p I SompleiD

EPA Somple ID lDb Somple ID Dot~ Coll~cttd

AdlniDfll-227 Ac:tinlum-227

AmeridDfll-241 Americium-241

Gamma Sean Blsmuth-207 Blsmuth-210 Cesium-137 Cobalt-60

Isotopic Plutoolum Plutonlum-238 Plutonlum-2391240

Gamma Sean Potassium-40

RADIUM-226 Radium-226

Strontium 90 Slrontium-90

Isotopic Thorium Thorium-228 !Thorium-230 [Thorium-232

Trlllum3 ITridum

I

MDA

Units pCiiL O.lti

Units pC"IIL 0.04

Units pCiiL <9.4 pCiiL <2.~

pCiiL ~

pCiiL <18

Units pC"IIL 0.34 pCiiL 0.21

Uolts pCiiL <-74

Units pCiiL . 0.024

Uolts pCiiL 2.1

Units pCiiL 0.24 pCiiL. 0.21 pCiiL o.u

Units pCiiL 33£

• • APPENDIXE See_, SampUng Results (1994)

I I I I J I I I Seep621 Seep614 Seep623 NS6001 NS7001 NSBOOI

MND16-1113-0100 MNDI6-1308-0200 MND16-0J03.0200 65.ooo90S.O REG 65-G00906.8 REG 65.ooo907.6 REG

31301!14 31301!14 31301!14 Result VNC VaL Code MDA Result VNC VaL Code MDA Result VNC VaL Code

0.081+1- 0.16 1-D O.ll 0.22+1 0.2 J-D 0.1 0.054+1- 0.11 J-D

0.32+1- 0.31 1-D O.Oii -0.12+1· 0.~ U-B 0.01 0.29+1 0.24 J-D

•

<9.4 N.A .u <II <11 N.A. u <9.1 <9.1 N.A .u <2.S N.A. u <12 <l;l N.A. u <4.(] <4.CJ N.A .u I <22 N.A. .u <14 <14 N.A u <Ill <IV N.A .u .

<18 N.A u <16 <16 N.A. u <18 <18 N.A .u

0.090+1- 0.~ 0.31 0.21+1- 0.31 0.28 0.018+1 0.11 U-B -O.OS4+1- 0.04 U-B O.l!l -0.027+1 0.028 U-B 0.18 -0.009+1- 0.018 U-8

<-74 N.A.U <-2S <·2S N.A.U <31! <3Ci N.A. u

0.31+1· O.t!l J.LS 0.~ 0.69+1- 0.3 J-LS 0.02~ 0.4S+I- 0.21 U-B

0.81+1· 1.3 U-B u 1.4+1 I U·B u 0.48+1- 1.2 U-B

-O.OS4+1· 0.1~ UJ.SB 0.22 0.018+1 0.13 UJ.SB 0.23 -0.018+1 0.018 UJ-SB 0.16+1- 0.4 UJ-B 0.18 0.19+1· o.n UJ-8 o. .. 0.48+1 0.28 1-S

0.027+1 0.081 J-S 0.14 0.063+1 0.1 J.S o.u 0.000+1- 0 UJ-BS

-S9+1- l6CJ U-8 33CJ -ISO+/ 16Cl U-8 330 ·130+1 16Cl U-8

• •

= =

;:; ;:;

d E! '"'! 0

0

~ l ~ c:i ~ c:i~

~

0 c:i

== ;:;;:; c:~'~

0 a

~~ -:; ~

c:ic:i c:i

aft

" " 1---I

-~ c

i

~ ~ ~ ci d

~ ~ a

c:i 0

~~ ~ !~

j !a W

\ CIO

;:l;:l i:l e e: e li ..

::s

·a 1 ::')::')

Mound P

lant, ER

Program

Revision 0

OU

5, New

Property Phase I F

ield Report

Decem

ber 1994 A

ppendix E

Page E

·28

•

•

•

APPENDIXF

SURVEYOR'S REPORT

•

•

•

KUSMER & ASSOCIATES, INC.

ARCHITECTS • ENGINEERS • SURVEYORS

TO: Science Applications DATE: February 23, 1994 International Corporation ATTN: Mr. Thomas Tank 4031 Colonel Glenn Highway, Suite 300 Beavercreek, Ohio 45431-1600

ATTN: Mr. Tank

We are sending to you the following:

Project: Surveying Services/Subcontract # 51-940271-42 Subproject #01-0513-01-2340-300

Job No: 94400-Sl (083)

Three (3) copies of the site map dated 02/23/94. Three (3} copies of the cooroinate numbers. One (1) copy of the field notes. One (1) Diskette.

These are:

Submitted for.:your· approval _x_ For yqur use

For:·your review &".comments· ~ As you requested

To be returned Other

Comments:

!f you have any questions, please don't hesitate to call. Thank you.

Sincerely,

KUSMER & ASSOCIATES, INC.

W £o~ r\ Vi:sr~.av-w. R·::>bert Kusmer, P. S. President

WRK/blk

622 West State Street • Fremont, Ohio 43420 • 419-332-1027

• I········.

i

l

l

KUSMER & ASSOCIATES, INC. 622 West State Street

FREMONT. OHIO 43420 (419) 332-1027

: \' v • .. ..- / : ..... ~.

! I l~ J r ~· 1 n 7;~ \0!-1-'

i !

llltaler~ ...... - ... _,_,_ ... __ llcn.fo--1111.11&-

JOB Ljlll/f{~ 1/ SHEETNO. ________ OF _____ _

CALC1Jt.ATEOSY ~b ~ ~/,-'e<;, OATE /· Z4 4-? CHECKEOSY ________ OATE _____ _

SCALE

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.: .... --·····:..·-····-····:.··-······-.. -~ .................. :.. ···-- .. : ... ·-' : : : : j

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JOB----:--C, .'

SHEETNO._...;.._.~------ OF _____ _ KUSMER & ASSOCJA,£5, INC. ..

_.,,. I '• • CALCULATED ev·..._;_:........;... __ ..:,___.....:__ DATE . - :' .. .-· .... ··. --· 622 West State Street FREMONT, OHIO 43420

(419) 332·1027

~r--------------------------------------~:~:~E:~KE=D=BY~::::::::::::::~==D=AT=E::::::::::: . . ------·---......... ·-·-······-···· ................... .... . ............... ···-·· . -··· ... .

. . .

..... - , .. . ... ···-· ..... : ....... -i--... L .. . ___ i ______ !--------~-----------:--------------;. ............ : ------------I------~ ----··· ------ ---- -- . ... ·····-····-. -; ··------ ·····--··· ~ -·····.; ············--······-·-~·-····

...... ------·-··----.. ·-·····--· ··-· ·-·······--- ········':'-·--··-·······-·-··-:····--·············· . ~~ ; ··-·-··-···-- ...... ···-··-----. .

.... --·· -~----------------~---······---· .. ··········---· -~ ............ ; ... ·----: ..... L ....... -;.·-·····---~---··-·-··.:.. ·······-··-··-·-.. ········ : : : . .... ·····--·-·--·~---···':'·-··········:·... . ····---·······-· ........ _____ ............... ·--· ~ : :

-----:-·-·-··""·---.. -~--·· _ .. ,_ .... ; ; : : : : : i

....... ··-·--6-~---~----- ~---·---... : ......... ... ~ ............ :···-..... -~ .... -

•·-········-·····-········--··:-·····--'--·-·.;_··-················· .... ~. ·--~----1---' --'-·-···'-·--····'---·..:.._._,_;._ ... c ... - .... ,.

I ···-· ... ..... . ... ~. ··----·--·--·-···-··· -·· -·-···· ................ ···-·· __ _L __ tL t;q.~.LA3. .. ~-*_] _____ :_....... . .. . • . . . . .!;_ \ A,.q :.,,c:;-;c.o~ ~4 . . .

..•..• c···- -···"··---~--;_ ___ .:__ .•...... ·····- .:.. . ...... ~ ... --'-· ........ ;-~•--:..;..:._..:..~_..;.;;;;...__;,..-.• -,... •. --~······

, : T s , A. t .. ~:-'7 _., . : : . : ' ·- . :

: \c.l '2. un 2 . vz.. I : t-·····,--··~-·..:..·--'--··-'----- . .;.·------,-·-- T :

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.. . C?,UR~E-··1--------·--. ________ .. "!- .:-.--=-.1---·--·--·---·-------·-·-~--·, 1-101</Z ~ /.'f= 7._- z. I · ~ _ J_j_

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SAIC - f10L..JI\0 PLANT, MIAMISBURG, OHIO ---------

STATE PLAN COORDINATES PLANT COORDINATES COOR ~ SAIC :t 1\CRlH EAsT SOUTH WEST !;bEV . • ------ ------- -------1137 00~-19.6489 59~27~.78 1497~6..6.01 6108.33 3562 . .30 826.2 1107 ~-16 59~7.92 1~97~1.52 5792.22 3380.03 ~.0

1106 OD-OS-12 595036.00 1~97520.~~ 54.4.5. 70 3180.22 872.9 1105 ~-oa 5954.34..08 1497559.36 5099.18 2980.~2 88.3.6 11~ 00~~ 595832.15 1~97598.29 ~752.65 2780.61 88.3.0 1102 CXJ-OS-OJ 596230.23 1~97637.21 "D6.13 2580.81 895.7 1112 ~-os-a:J 596269.13 1~97239.13 ~206.33 2927.33 875.8 1111 ~-as~ 595871.05 1~97200.20 ~52.85 3127.1~ 811.6 1110 ~-ClS-08 5954.72.97 1497161.28 G..899.37 3326.9~ 820.6 1109 ~-ClS-12 595074.89 1497122.36 52~.89 .3526.75 836.3 1108 04.-ClS-16 59(.676.81 1497083.~ 5592.42 3726.55 813.1 1138 ~-ClS-19.6533 59~13.23 149~7.88 5908.90 3909.04. 793.9 1113 08-ClS-00 596308.03 1496841.~ 4.0J6.52 3273.85 870.3 111~ 08~ 595909.95 1496802.12 4.353. 04. 34.73.66 806.7 1115 08-QS-08 595511.87 1496763.20 6.699.57 3673.~6 776.3 1116 08-ClS-12 595113.79 149672~.28 506.6.09 3873.27 767.6 1117 08-ClS-16 594715.71 1496685 . .35 5392.61 4.073.07 760.0 1139 08-QS-19.6578 594.351.68 1496649.76 5709.49 4.255.79 754..5 1122 12-ClS-00 59636.6.92 14964.42.96 3806.72 3620.38 866.2 1121 12-QS-04 595948.84 1496404.04. 4153.24 3820.18 806.4 1120 12-os-08 595550.76 1496365.12 4499.76 4019.99 767.0 1119 12-QS-12 595152.69 1496326.20 ~.28 4.219.79 733.7 .1118 12-QS-16 594754..61 1496287.27 5192.81 4419.60 729.3 1140 12-QS-19.6623 594390.14 1496251. 64. 5510.07 4602.53 7~.8

• 1123 16-os-00 596385.82 1496044.88 3606.91 3966.90 828.5 112~ 16-QS-04 595987.74 1496005.96 3953.43 4166.70 760.2 1125 16-os-08 595589.66 1495967.04. 4299.96 4366.51 734.8

.1126 16-QS-12 595191.58 1495928.11 6.66.6. G..8 4.566.31 720.4 1127 16-os-16 594793.50 1495889.19 4993.00 4766.12 740.3

·1136 16-QS-20 594395.42 1495850.27 5339.52 4965.92 741.2 1129 20-os-12 595230.G..8 1495530.03 446.6.67 4912.84 713.7

.1128 20-os-16 594832.40 1495491.11 4793.20 5112.64. 722.6 ·1134. 20-QS-20 594434..32 1495452.19 5139.72 5312.~ 723.9 1132 24-QS-12 595269.37 1495131.96 426.6.87 5259.36 703.1

11133 24-QS-16 594871.29 1495093.04. ~93.39 5459.16 697.4 1130 20-CS-08 595628.56 1495568.96 4100.15 4713.03 725.4 1131 24-QS-08 595667.45 1495170.88 390J.35 5059.55 701.4

•

SAIC - MOUND PLANT, MIAMISBURG, OHIO ------------ ---------

STATE PLAN COORDINATES PLANT COORD INA TE:S COOR !! SAIC -~ I\ORTH EAST saJTH WEST f-LEV. • ----------------- ----11.37 ClO-OS-19.6489 59~27~.78 1~97~.01 6108.3.3 .3562 . .30 826.2 1107 OG-OS-16 59~6.37.92 1~97~1.52 5792.22 3380.0.3 ~-0 1106 OG-OS-12 595036.00 1~97520.~ ~.70 .3180.22 872.9 1105 oo-os-oa 59~.08 1~97559 . .36 5099.18 2980.~2 88.3.6 11~ CXJ-OS-Ql.. 5958.32.15 1~97598.29 ~752.65 2780.61 88.3.0 1102 ClO-OS-CXJ 5962.30.2.3 1~976.37.21 ~.1.3 2580.81 895.7 1112 ~-os-oo 596269.1.3 1~972.39.1.3 ~206 • .3.3 2927 . .3.3 875.8 1111 ~-as~ 595871.05 1~97200.20 4.552.85 .3127.1~ 811.6 1110 ~-05-08 595472.97 1~97161.28 ~99 . .37 3326.9~ 820.6 1109 ~-GS-12 59507~.89 1'-97122 . .36 52~.89 3526.75 8.36.3 1108 ~-QS-16 594.676.81 1'-97083.~ 5592.'-2 3726.55 81.3.1 11.38 ~-QS-19. 6533 594.313.23 1'-9~7.88 5908.90 .3909.~ 793.9 1113 DB~ 596308.03 1~96841.~ '-CXJ6.52 3273.85 870.3 111~ 08-QS~ 595909.95 1~96802.12 4.353.~ 34.73.66 806.7 1115 08-QS-08 595511.87 1'-9676.3. 20 ~99.57 .3673. ~ 776.3 1116 08-QS-12 595113.79 1~9672~.28 50'-6.09 .3873.27 767.6 1117 08-QS-16 5~715.71 1~96685.35 5392.61 ~73.07 760.0 1139 08-QS-19.6578 594.351.68 1~9664.9.76 5709.'-9 '-255.79 754.5 1122 12~ 596346.92 14~2.96 3806.72 .3620 . .38 866.2 1121 12~ 595948.84. 1~96404.-~ ~153.2~ 3820.18 806.~

1120 12-os-OB 595550.76 1~96365.12 4499.76 ~19.99 767.0 1119 12-QS-12 595152.69 1~96326.20 ~.28 4.219.79 733.7 1118 12-QS-16 5~754.61 1496287.27 5192.81 4419.60 729.3 11~ 12-QS-19.6623 594.390.1~ 1~96251.M 5510.07 4602.53 745.8

• 1123 16-0S-OJ 596385.82 1~96044.88 3606.91 3966.90 828.5 112~ 1~ 595987.7~ 1496005.96 3953.~ ~166.70 760.2 1125 16-os-OB 595589.66 1~95967.~ ~299.96 4.366.51 734..8

.1126 1~-12 595191.58 1~95928.11 ~-~ ~.31 720.~

1127 16-QS-16 5~793.50 1~95889.19 ~993.00 ~766.12 7~.3

1136 16-QS-20 594.395. 4.2 1~95850.27 5339.52 ~965.92 7'-1.2 1129 20-05-12 5952.30.~ 1~95530.0.3 ~.67 ~912.84. 713.7 1128 20-os-16 594832.40 1495491.11 ~793.20 5112.M 722.6

·1134. 20-os-20 594434.32 1495452.19 5139.72 5312.45 723.9 1132 24-QS-12 595269.37 1495131.96 42~.87 5259.36 703.1

·1133 24-QS-16 594871.29 1~95093.04. 4593.39 5459.16 697.4 1130 20-ClS-08 '595628.56 1~95568.96 4100.15 4.713.03 725.4. 1131 24-os-OB 595667.45 1495170.88 39(().35 5059.55 701.4

•••

SAIC - MOUND PLANT, MIAMI=:el.JRG. OHI,.."l

----------------------------------------STATE PLAN CCORDINATES PLANT COORDINATES .'. CqJR ~ SAIC !; I\ORTH EAST SOJTH LJEST !;b..EV.

------------- --------1137 CD-OS-19.66.89 59427~.78 1~97~~6.01 6108.33 3562.30 826.2 1107 00-05-16 59~6.37. 92 1~97~81.52 5792.22 3380.03 ~-0 1106 (J()....:.OS-12 595036.00 1~97520." 5445.70 3180.22 872.9 1105 oo-os-oa 59SQ...34..08 1~97559.36 5099.18 2980.~2 883.6 11~ OO-QS-Q4. 595832.15 1~97598.29 ~752.65 2780.61 883.0 1102 cx:HJS-co 596230.23 1~976.37.21 4.406.13 2580.81 895.7 1112 ~-os-oo 596269.1.3 1~972.39.1.3 ~206.33 2927 . .33 875.8 1111 ~-QS-Q4. 595871.05 1~97200.20 4.552.85 3127.1~ 811.6 1110 ~-os-oa 59~72.97 1~97161. 28 ~99.37 3326.9~ 820.6 1109 ~-QS-12 59507~.89 1~97122.36 52~.89 .3526.75 836.3 1108 ~-QS-16 594676.81 1~97083.~ 5592.42 3726.55 813.1 1138 ~-QS-19.6533 59~13.23 1~97047. 88 5908.90 .3909.04 793.9 1113 08-os-co 596308.03 14 96841. 04. ~.52 3273.85 870.3 111~ 08~ 595909.95 1496802.12 4353.~ 3473.66 806.7 1115 08-QS-QB 595511.87 1~96763.20 4699.57 3673.46 776.3 1116 08-QS-12 595113.79 1496724.28 5046.09 3873.27 767.6 1117 08-ClS-16 594715.71 1~96685.35 5392.61 ~3.07 760.0 1139 08-QS-19.6578 594351.68 1~96649.76 5709.~9 4255.79 7~.5

1122 12-os-co 596346.92 14964..42.96 3806.72 3620.38 866.2 1121 12-ClS-04. 595~.84 1496404.04. 4153.24 3820.18 806.4 1120 12-QS-08 595550.76 1496365.12 4499.76 W19.99 767.0 1119 12-ClS-12 595152.69 1496.326.20 ~.28 4219.79 733.7 1118 12-ClS-16 594754.61 1496287.27 5192.81 "19.60 729.3

• um 12-ClS-19.6623 5~90.14 1496251.64. 5510.07 4602.53 745.8 1123 16-0S-CXJ 596385.82 149604U..88 3606.91 3966.90 828.5 1124 16-ClS-04 595987.74 1496005.96 3953.~ 4166.70 760.2 1125 16-QS-08 595589.66 14 9596 7. 04. 4299.96 4366.51 . 734.8 1126 16-0S-12 595191.58 1495928.11 464.6.~ 4566.31 720.4 1127 16-ClS-16 594793.50 1495889.19 4993.00 4766.12 7W.3

·1136 16-ClS-20 5~95.42 1495850.27 5339.52 4965.92 741.2 1129 20-05-12 595230.48 1495530.03 ~.67 4912.84 713.7

•1128 20-CS-16 5~2.W 149~91.11 4793.20 5112.64. 722.6 .1134 20-CS-20 5~.32 1495452.19 5139.72 5312.45 723.9 1132 24.-ClS-12 595269.37 1495131.96 4246.87 5259 • .36 703.1

·1133 24.-ClS-16 594871.29 1495093.04. 4593.39 5459.16 697.4. 11.30 20-0S-08 595628.56 1495568.96 4100.15 4713.03 725.4 1131 24.-os-CJ8 595667.45 1495170.88 39ClJ.35 5059.55 701.4.

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200 400 600

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MOUND LABS MIAM ISB_URG ,_

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s 3600.0000

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----------------------~~--~'

( IN FJ!J!.1' ) 1 Inch ~ 100 tt.

POINT SOUTH WEST ELEVA 1lON DESCRIP1lON 1020 4653.3514 2716.4548 889.67 1021 4151. 7881 3033.5161 877.99 1022 4118.1317 3224.7091 857.53 1023 401 8.1589 3219.4 723 873.63 1024 3867.0687 3569.1371 864.02 1025 3739.4928 3742.7297 853.60 1026 -3664.5790-3893.1 582 -~ 838.40 1027 3489.8870 4154.2520 798.75 1028 3449.8759 4224.9256 783.56 1029 3434.1355 4207.9'196 786.84 1031 3671.0002 4850.2214 706 .08 1032 3789.9155 5040.8849 700.65 1033 3982.1 137 4854. 1326 707.21 1034 4103.3015 5010.0846 -703.99 1035 4391 .2207 5097.6014 704.19 1036 4289.1848 5234.2006 703.68 1037 4278.4474 5277.7330 700.02 1038 4211.3728 5420.6050 696.50 1039 4584.4576 4770.4702 714.67 1040 4532.1975 491 4.2975 707.25 1041 4700.7497 4731.2806 709.34 1042 4742.2923 4630.8521 714.50 104 3 4508.8136 4478.8668 733.36 1044 4985.1565 3607.3887 797.14 1045 4213.8143 371{0628 803.27 1046 3981.1068 4123.3460 771.50 1047 4806.0830 4285.4439 726.36 1048 4969.7404 4358.4081 720.18 1049 5049.3554 4345.1205 722.51 1050 4754.61 30 4140.7911 733.77 1051 4738.0978 3798.2787 751.69 1052 4613.6618 3708.5982 773.39 1053 4520.2463 3579.1534 789.55 1 OS4 4662.81 91 3360.7666 785.55 1055 4373.6346 3855.8835 790.36 1056 4417.8100 3661.8732 790.47 1057 4175.4641 4745.63 58 712.53 1058 4172.5642 4604.0739 716.98 1059 4237.4653 4532.6022 723.86 1060 4141.0655 4496.2768 722.39

w 399 8-404 SD 05 SD 04 8-398 SD 03 w 397 8-403 so 01 so 02 w 402 SD 26 w 400 SD 22 SD 19 8-401 so 20 SD 21 8-408 SD 18 SD 17 SD 16 8-406 8-409 SD 06 B- 405 SD 13 SD 14 SD 15 SD 12 SD 11 SD 10 SD 8 SD 9 8-407 SD 7 SD 23 SD 24 SD 25 SD 27

1 ~ We.\ Fl"'t Street • Dayton, Oh1o 45402

8/ 29/9-1-

T-Z9G

NEW PROPERTY MOUN D LABS

MIAMI SBURG, OHIO 0

0 0 0 0 0 0 D D 0 0 0 o . 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 D 0 0 0 0 0 d 0 0

d d 0 d d d d d d d 0 d d 0 0 0 0 0 0 0 0 0 {!) 0 0

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w w w 595600.0000 w w w w w N 596600.0000 w w

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0 1025 0

1024 0

1023 0

1022 0

1021 0

J .~~~--------------~----------~----l----------------+----------------~-------------~~--------------~--------------~---~-----------l----------------~---------------t----------------rN~59~60~? 00.0000 N 59620(l0000 .•

~-

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N 595800~.~00~0~0~----------~'-'--~-----------------~--~------------~-----------------~-----------------t----------------l------------------l---~~------y----t--~~s----------t----------------~----------------~----------------~-----------------~----------------~~~ 1032 0

N 595800.0000 1056 0 0 0 .,

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1033 c

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0

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-~~i---------------~----------------~-----------------t-----~1fut5[8~-----+----------------1-----------------r-~-------------t----------------t-----~~~-----t----------------~~--------------rN~59=o5600.0000 N !:.9560(l00 JO 1052 POINT NORTHING EASTlNG ELEVA TlON DESCRIPTION

1034 0

1057 0

10590 0

1051 0

N 595400~.QOO~O~O~-----------------~-----------------~----------------~--------~-------r-----------------t-----------------t----------------~~ - ____ __:_ ________ t-----------------j---------------+-----------------(N"---"5"'-"9 5400.0000

1038 1036

1043 0

105~0 0

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0 0 0 1035 N 595200.0000 · N 595200~.Qoo~o~o4---------~10~3~7~--~---------~~n-~---t----,-----------t----------------f----------------i-----------------r-~~~---------t----------------t-----~---------j·--------~------~------------~--~~

N 594800.0000 0 0 0 0 0 0 0 0

c:i d 0 0 0 N I{) ll)

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Ol m

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•

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594800.0000

100 0

r--•? GRAPHlC SCALE

"' 100 200 I

I I .,

1020 595949.8530 1497616 .6500 88\!.67 w 399 N01E: MP EL£V= 889.67',CASTlNG EL£V=888.84',G/S El£V=887.54'

1021 596275.6400 ' 1497120.7100 877.99 8-404 1022 596227.3080 1496932.69 00 857.53 SD 05 1023 596320.5150 1496896.1600 873.63 SD 04 1024 596313.6630 1496515.3100 864.02 8-398 1025 596358.1328 1496304.5199 853.60 SD 03 1026 596364.2132 1496136.5799 83tl.40 w 397

N01E: MP El£V=838.40',CASTl NG ELEV=8313.65',G/S ELEV= 836.65' 1027 596415.4439 1495826.6401 790.75 8-403 1028 596422.6858 1495745.7501 783.56 SD 01 1029 596444.0208 1495754.6801 786.84 SD 02 1031 595963.0000 1495267.6500 706.08 w 402

N01E: MP El£V=706.08',CASTlNG ELEV=70G.26',G/S ELEV=704.56' 1032 595775.9420 1495143.1400 700.65 SD 26 1033 595678.0580 1495392.6100 707.21 w 400

N01E: MP El£V=707.21',CASTlNG El£V=707.47',G/S ELEV=705.27' 1034 595503.2700 1495300.6500 703.99 SD 22 1035 595204.9130 1495339.8900 704.19 SD 19 1036 595241.4060 1495173.3400 703.68 B-401 1037 595233.2010 1495129.2600 700.02 SD 20 1038 595235.2640 1494971.4400 696.50 SD 21 1039 595164.0740 1495717.6300 714-.67 8-408 1040 595152.2510 1495565.0600 707.25 SD 18 1041 595074.3580 1495801.3600 709.34 SD 17 1042 595078.0130 1495909.9800 714.50 SD 16 1043 595353.4240 1495951.9400 733.36 B-406 1044 595279.6360 1496942.3600 797.14 B-409 1045 595938.0180 1496526.5700 803.27 SD 06 1046 595980.8650 1496057.7100 771 .50 B-405 1047 595162.6090 1496250.8900 726 .35 SD 13 1048 594983.4270 1496252.0500 720.18 SD 14 1049 594916.4120 1496297.0400 722.51 so 15 1050 595259.2384 1496351 .3605 733.77 so 12 1051 595425.7713 1496666.4588 751.69 SD 11 1052 595576.1405 1496696.7246 773.39 SD 10 1 053 595714.6866 1496 776.0178 789.55 so 8 1054 595675.0639 1497033.7965 785.55 so 9 1055 595733.8856 1496463.4383 790.36 B-407 1056 595773.8019 14-96658.3694 790.47 so 7 1057 595546.7971 1495571.2900 712.53 so 23 1058 595607.9177 1495699.0102 716.98 SD 24 1059 595578.3385 1495790.9092 723.86 so 25 1 060 595681 .1343 1495784.1672 722.39 so 27

~-~Weiss & n~ .. """ I

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Ol 0>

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" ..;-

" " ..;- " ~ ~ ( !N FEET ) ~ ~

j_DRAwr< l CHECKED .PH ~ ~ ~

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. - . - --~

' .-) r\ r

•

•

•

APPENDIXG

VERIFICATION SOD.. SAMPLING

•

•

•

DATA QUALIFIERS

The primary data qualifiers to be applied, as described in the CLP Functional Guidelines and in Section

4.0 and 5.0 of Appendix H, of the QAPjP (DOE 1993c).

u

J

R

N

NJ

UJ

The material was analyzed, but was not detected. The associated numerical value is the sample quantitation limit .

The associated numerical value is an estimated quantity.

The data are unusable (compound may or may not be present). Resampling and reanalysis is necessary for verification.

Presumptive evidence of presence of material.

Presumptive evidence of the presence of the material at an estimated quantity.

The material was analyzed for, but was not detected. The sample quantitation limit is an estimated quantity.

Subqualifiers are used to assist in data assessment by indicating the source of the primary qualifier. These

subqualifiers are attached to the primary qualifier, separated by a hyphen. The following is a list of

allowable subqualifiers.

SUBQUALIFIERS- ORGANICS

B c H K s I p (+} (-)

Qualified due to method blank or a field blank Qualified due to calibration Holding time exceeded Qualified due to surrogate recovery Qualified due to matrix spike recovery Qualified due to internal recovery Pesticide/PCB results have >25% difference on two different columns Potential positive bias (added after subqualifier with a parentheses) Potential negative bias (added after subqualifier with a parentheses)

SUBQUALIFIERS- INORGANICS

B c H s I D

Mound Plant, ER Program Revision 0

Qualified due to method blank of field blank Qualified due to calibration Holding time exceeded Qualified due to matrix spike recovery Interference (ICP serial dilution, ICS, or GFAA spike recovery) Duplicate (replicate limits exceeded)

OUS, New Property Phase 1 Field Report December 1994

Appendix G Page G-2

•

•

•

L (+) (-)

Qualified due to LCS Potential positive bias (added after subqualifier with a parentheses) Potential negative bias (added after subqualifier with a parentheses)

Examples of fmal qualification might be J-C, UJ-S(+), UJ-BC(-), etc .

Mound Plant, ER Program Revision 0

OU5, New Property Phase I Field Report December 1994

AppendixG Page G-3

w:: 5:[ 8 ., 0~

~

l

g ,!.II

~ E

ff !f ~-:n ~ w 1

d .aa.o


·-- ---------

SAIC Smnple ID NPSOOI -·······--

LDbSampkiD F4364REG Somplt Collection Date 515194 --

DV Result Qua IIIIer

-·-·~··.

Vola&Ue Orpulcs Vults 1.1.2· Trichloroethane liOIKO llll Trichloroelhene liOIKO llU 1,1.2· Triddonllriftuorocthane liOIKO !JR Vinyl Acetate UOIKO IIU VInyl Odoridc UOIKO IIU

-·~ .. Xylene, Total UOIKO IIU Tentatively Identified Compounds I

• APPENDIXG • Verification SoD Sampling Data

........ -NPS001 NPSOOl NPS004 NPS005 NPS006

D3286REG F4~REG D328'7REG D3288REG D3289REG 515194 515194 515194 515194 515194

DV DV DV DV DV Result QuaiUier Result Quallller Result QuaUDer Result Qualifier Raul& Qualifier 1

.. I

I ll 1 ll h liJ IIlii ll.VJ

·~ u 13U 12ll llll •• u

... u IIR I U llll •• u I

12 ll 11 u I• u IIU ·~ u I ·~ u 13 u •• u IIU •• u 12 u 2.1 J I U llU l<J u

B 3

:::03;

~- § -·c. g ., or

r

~

f

g ~

f

rf ~~ ~~ ~-

::!1 6:

{

if ~~ u.o

• MOUND NEW PROPERTY 1-·----· ----- --···-SAIC Sample ID ...... IAbSampk/D -Sample. Collecrion Dare

·---------· Semi-Yolallle Orpnlal

Ac:enaphlhene Ac:enaphthylene

. -Anthracene Benzo(a)anthrac:ene Benzo(a)pyrmc Benzo(b )Ouoranlhene Benzo(g.h.l)perylene Benz:o(k)Ouoranlhene Benzoic Acid ·--.-Benzyl Alcohol o-Benzyl-p-Chlorophenol bis(2-0tloroethoxy)methane bis(2-Chloroethyl)elher bis(2-Ethylhexyl)phthalate 4-Bromophenyl-phenylelher Butylbenzylphthalate Carbazole 4-Chloro-3·methylphenol 4-Chloroaniline 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenyl-phenylelher Chrysene 01-n-butylphthalate Di-n-octylphthalate Dibenzo(a,h)anthrac:ene Dibenzofuran 1.2-Dichlorobenzene I ,3-Dichlorobenzene I ,4-Dichlorobenzene 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Diethylphthalate 2.~Dillll:thylphenol

--- -··-

·=i NPSOOI

89961REG 515194

-DV

Result Qualifier

Units UOIKO 3!10 UJ UGIKO 3S(J UJ UOIKO 3Sil UJ UOIKO 3Sil UJ UOIKG 3Sil UJ UGIKO 3!1(] UJ UGIKO 3!1(] UJ UOIKO 3SC UJ UOIKO m UJ UGIKO 3S~ UJ UOIKO 3Sil UJ UOIKO 3SC UJ UOIKO 3Sil UJ UGIKO 3Sil UJ UOIKO 3Sil UJ UOIKO 3Sil UJ UOIKO 3Sil UJ UOIKO 3Sil UJ UGIKO 3Sil UJ UOIKO 3Sil UJ UOIKO 3Sil UJ UGIKO 3SO UJ UGIKG 3!10 UJ UG'KO 3SC UJ UOIKO 3SC UJ UGIKO 3Sil UJ UGIKO 3Sil UJ UOIKO 3!1(1 UJ UOIKO 3Sil UJ UGIKO 3Sil UJ UGIKO 3Sil UJ UGIKO JS(J UJ UOIKO 3Sil UJ

_l]OIKO 3Sil UJ -

• • APPENDIXG Verificadon SoU Sampling Data

I ·--

NPSOOJ NPSOOl NPS004 NPSOOS NPS006 B996JREG 89963REG 89964REG 8996SREG B9966REG

515/94 515194 515194 515194 515194

DV DV DV DV DV Result QuaiUier Result Qualifier Result Qualifier Result Qualmer Result Qualifier

41(] UJ 41~ u 400 u 36() u 411l UJ 41(] UJ 411l u <tOO u 36(] u 41<1 UJ 41(] UJ 41(] u 400 u 36< u 410 UJ 41(] UJ 411l u 400 u 36C u 41(] UJ 41[ UJ 41(] u 400 u 36C u 41(] UJ 41(] UJ 41(] u 400 u 361l u 410 UJ 41(] UJ 41(] u 400 u 361l u 410 UJ 41(] UJ 41(] u 400 u 36(] u 410 UJ 41(] UJ 42Q u 410 u 37Q u 410 UJ 41(] UJ 421l u 41(] u 370 u 410 UJ 41(] UJ 42(] u 41(] u 37(] u 41(] UJ 411l UJ 41C u 400 u 361l u 41(] UJ 41(] UJ 411l u 400 u 361J u 41(] UJ 41(] UJ 41C u 400 u 361l u 410 UJ 41(] UJ 41(] u 400 u 36(] u 41(] UJ 411l UJ 41~ u ~ u 3~ u 411l UJ 41(] UJ 41(] u 400 u 36() u 41(] UJ 41(] UJ 41(] u 400 u 360 u 411J UJ 41(] UJ 411JU 400U 361JU 41(1 UJ 41(] UJ 411JU 400U 360 u 411] UJ 41[ UJ 41(] u 400 u 36( u 41(] UJ 41(] UJ 41Q u ~u ~~ u 41(] UJ I

411l UJ 41(] u 400 u 36C u 41(] UJ

411l UJ 24(] J 18(] J 42(] 41(] UJ 41(] UJ 411l u ~u 36(] u 4!1l UJ

410 UJ 411JU 400U 361l u 41( UJ 41(] UJ 411JU 400U 361l u 41C UJ 41(] UJ 41(] u ~u ~u 41(] UJ 41(] UJ 411l u 400U 360 u 41(1 UJ -411l UJ 41Q u 400U 36C u 41(] UJ 41(] UJ 41(] UJ ~ UJ ~ UJ 411l UJ 41(] UJ 41(] u 400U 361J u 41(] UJ 41(] UJ 41(] u 400U 36(] u 410 UJ 411l UJ 41(] u 400U 361l u 4!0 UJ

:::o::: ~- § ... c. g oi

r

Iii

f

g ,!JI

f

fl .,;;p -~ f-

!ll 6:

I

> li n ~ G')loC

0.0


·- ·---·· ~AIC &unpleiD ... LabSampkiD

Samplt Collection Datt

·---··-u•~~· •·•

Seml·•olatlle Qramlcs Ualts Dimethyl phthalate UOIKO 4,6-Dinitro-2-mclhylphenol UOIKO 2,4-Dinittophr:nol UOIKO 2,4-Dinittotoluc:ne UOIKO -2,6-Dinittotoluene UOIKO fluoranlhene UOIKO ------fluomJC UOIKO Heddllorobenzene UOIKO Heuchlorobutadicne UOIKO ~uaclllorocyclop:ntadiene UOIKO HelUichloroclhane UOIKO lndeno( 1.2.~,d)p1~ne UOIKO lsopborone UOIKO 2-Melhylnaphlhalene UOIKO 2-Melhylphenol UOIKO

-· 4-Melhylphenol UOIKO N-Nitroso-di-n-propylamine UOIKO N-Nittosodiphenylamine UOIKO Naphthalene UOIKO

-· 2-Nilroaniline UOIKO .......... 3-Nilroaniline UOIKO 4-Nittoaniline UOIKO Nitrobenz.c:ne UOIKO 2-Nib'Ophenol UOIKO ·-4-Nib'Ophenol UOIKO 2,2' -oxybis(I-Chloropropane) UOIKO Pentachlorophenol UOIKO Phenan~ne UOIKO Phenol UOIKO Pyrene UOIKO 1,2,4-Trichlorobenz.c:ne UOIKO 2,4,5-Trichlorophr:nol UOIKO 2,4,6-Trichlorophenol UOIKO !enlallvely ldcfllified eomiJOUIIds

• APPENDIXG . Verification SoU Sampling Data

I I

NPSOOl NPSOOl NPS003 89961 REG B996lREG B9963REG

515/H 115114 SISIN

DV DV DV Result Qualifier Result Qualifier Result QuaDIIer

350 UJ 41[ UJ 41(] u 840 UJ 99(J UJ lOOC u 84C UJ 99IJ UJ lOOIJ u 350 UJ 410 UJ 41(1 u 3Sil UJ 410 UJ 41(1 u 3SO UJ 410 UJ 41(1 u 350 UJ 41( UJ 410 u 3SO UJ 4U UJ 410 u 350 UJ 410 UJ 410 u 350 UJ 4UI UJ 41~ u 350 UJ 4Ul UJ 41£ u 3SO UJ 41(1 UJ 41t u 350 UJ 410 UJ 410 u 35(] UJ 41~ UJ 410 UJ 35() UJ 410 UJ 4UI u 350 UJ 4111 UJ 41Cl u 350 UJ 4Ul UJ 410 u 3~ UJ 41~ UJ 4Ul U 350 UJ 410 UJ 410 u S40 UJ 99C UJ 1000 u 840 UJ ~ UJ II)O(J U 840 UJ 99C UJ 1000 u 350 UJ 41(1 UJ 41( u 350 UJ 410 Ul 41( u 840 UJ 99C UJ IOOC U 350 UJ 4UI UJ 41( u 840 UJ 99IJ UJ IOOIJ UJ 350 UJ 41Cl UJ 41~ u 350 UJ 41(] UJ 41C U 35(] UJ 4lfl UJ 410 u 3SO UJ 410 UJ 411l u 841l UJ 990 UJ 1000 u 350 UJ 410 UJ 410 u

5 II 7 ' . . -

• I I I I I I

NPSG04 NI'SIIOS NPS006 B9964REG B9965REG B9966REG

515194 515194 515194 -DV DV DV Result Qualifier Result Qwdlller Result Qualifier

- ·--400 364:

·---4iii u u UJ

980 u sse u 99(J UJ 9SO u sse u 99(J UJ ·-·- r-· -·--401] u 360 u 410 UJ -401] u 36(] u 41(1 UJ ~ u 36Cl u 4Ul UJ 400 u 36(] u 410 UJ 400 u 36Cl u 410 UJ

-·-·~·-· ----400 u 360 u ------uo UJ 400 u 36C u 4U UJ

.~ u 36( u f--~t !=-·---· UJ

400 u 36Cl u 4U UJ --r----- ------401] u ._36(] u m UJ

40C UJ 360 UJ 410 UJ 401] u 36() u 4lll UJ 40CJ u 36Cl u 4111 UJ -- . 400 u 360 u 410 UJ 401JU 36(] u 410 UJ 400U 360 u 410 UJ --980U sso u -~ UJ ----9Sil u sso u 990 UJ 980 u sso u 990 UJ 400U 360 u 410 UJ 4()()U 36Cl u 410 UJ 980U 88(; u 99(J UJ 401:U 36Cl u 410 UJ 98C UJ 880 UJ 990 UJ ·- --400U 36CJU 411l UJ 40CJU 36CJU 410

UJ ___

400U 36C U 41C UJ 4()(1U 36c:U 4U UJ !ni]U 88( u - 99C UJ 400U 36Cl u 4Hl UJ

'- 8, . Ill -- ·-

II ---- -- -- - -·········-

"'3: ~- § s· Q. t:l .,

0§" r

~

f

-~ ~

rf ~~ -~ ~-

::n 6:

{

d ~0


·--SA/C Samplt ID .. LabSampk/D

Samplt Cotltclion Dale

·----···-·

Pesticides and PCBs Aldrin alpha-BHC

-·-· alpha-Cblordanc Aroclor-1016

-· Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248

·-·· Aroclor-12S4

·-·-·· Aroclor-1260 ---bela-BHC 4,4'-DDD 4,4'-DDE -----···-4,4'-DDT della·BHC --·-Dieldrin Endosulfan I P.ndosulfan II Endosulfan Sulfate -Endrin Endrin Aldehyde Endrin Ketone gamma-BHC (Lindane)

gamma-Otlordanc -

Heptachlor Heptachlor Epollidc p,p'-Methoxyc:hlor Toxaphene

NPSOOI CF07471 REG

515194

DV Result Qualifier

-Units

UGIKO 1.8 UJ UGIKO 1.8 UJ UGIKO 1.8 UJ UGIKO 3S UJ UGIKO 70 UJ UGIKO 3S UJ UGIKO 3S UJ UGIKO 3~ UJ UGIKO 3S UJ UGIKO 3S UJ UGIKO 1.8 UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 1.8 UJ UGIKO 3.S UJ UGIKO 1.8 UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 3.S UJ UGIKO 1.8 UJ UGIKO 1.8 UJ UGIKO 1.8 UJ UGIKO 1.8 UJ UGIKO 18 UJ UG'KO 180 UJ

• APPENoi;,; G • Verlficadon SoU Sampling Data

I --

NPSI02 NPS003 NPS004 NPS005 NPS006 CF07467REG CF07468REG CF07469REG CF07470REG CF076Z8REG

515194 515194 515/94 515/94 515/94 --DV DV DV DV DV

Result Qualifier Result Qualifier Result Qualmer Result Qualifier Raalt Qualifier

2UJ 2.1 UJ 2 UJ 1.8 UJ ~ UJ

2 UJ 2.1 UJ :.: UJ 1.8 UJ 2 UJ

2 UJ 2.1 UJ 2 UJ 1.8 UJ 2 UJ :4( UJ 41 UJ 41 UJ 37 UJ 40 UJ

·8C UJ 82UJ 81 UJ 73 UJ 80 UJ

:4C UJ 41 UJ 41 UJ 37 UJ 40 UJ ;4o UJ 41 UJ 41 UJ 37 UJ 40 UJ

·-,4( UJ 41 UJ 41 UJ 37 UJ 40 UJ ,40 UJ 41 UJ 41 UJ 37 UJ 40UJ ·-

-· ~

40UJ --·40 UJ 41 UJ 41 UJ 37 UJ I 2 UJ 2.1 UJ ~ UJ 1.8 UJ 2UJ --

·4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4UJ-----

:4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ

·4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4UJ .. -

. 2 UJ 2.1 UJ 2 UJ 1.8 UJ 2UJ ___

·4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ

' 2 UJ 2.1 UJ 2 UJ 1.8 UJ 2 UJ 4UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ 4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ 4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ 4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ 4 UJ 4.1 UJ 4.1 UJ 3.7 UJ 4 UJ 2 UJ 2.1 UJ 2 UJ 1.8 UJ 2 UJ

2 UJ 2.1 UJ 2 UJ 1.8 UJ 2 UJ

2 UJ 2.1 UJ 2 UJ 1.8 UJ 2 UJ

2 UJ 2.1 UJ 2UJ 1.8 UJ UJ

20 UJ 21 UJ 20 UJ 18 UJ 2C UJ

200 UJ 210 UJ ~ UJ - I~ UJ 200 UJ

-- ----

~~ ~· § -·c. g ., Of

r

~

f

~ i

rl [~ -~ ~-:n

6: ~ 1

> .,,

~~ c!oo


-· - I SA/C Sample ID ·-- NPSOOI LDbSampkiD 3109318 REG ~le Collection Dale 515194

DV Result QualiDer ----------- "' ·--- -

ADIODS· Cblorlde UDits CHWRIDB - MOIKO s~ u

Anions • fluoride Uolts FLUORIDE MOIKO sou

··----------Anions • Sulfate Uolts -·-·-SULPATB MOIKO s~ u -------Anions • Nitrate/Nitrite Uolts NITRA TPJNITRITB MOIKO 10.1

• APPENDIXG Verificadon Soli Sampling Data

I I ----

NPS002 NPS003 -···

3209319REG 3209320REG 515194 515194

-··-· --DV DV

Result Qualtner Result QuaiiDer

~u ~u

611U 60U

60U 60U

-IS.6 7.73

I

NPS004 3209321 REG

515194

DV Result Quallner

_6C: u

611U

611U

IS.l

-· I - ·-------

··-·· NPS005 NPS006

·-·----· 3209311REG REG

515194 5/5194 ·----,--·--

DV DV Result QuaiiDer Result QualiOer ---

-----

611U 60U

--611U 60U ---

sou 60 u -·-

-- " ----·-------

20.4 IB.S

w~ ~- § c;· o. tl .,

0~

w

f

~ ~ ~

il ~~ ~f .,.._

:n 6:

f ~

d .co


SAIC Somple ID .. Lob Somple ID Sample Collutl011 Date

·-·

lnorgaula Units Aluminum MOIKO Antimony MGIKO -Arsenic MGIKO Barium MOIKO -----BeryUium MGIKG

-· Cadmium MGIKO

·-·-· Calcium MOIKO -Chromium MOIKO -------Cobalt MOIKO ------··-· Copper ··- --·-·. MGIKO Iron MGIKO Lead MGIKO Uthium MOIKO

··-· Magnesium MOIKO --· -· Manganese MOIKO Mercury MOIKO ---Molybdenum MOIKO Nickel MGIKO ----·-POI&SSium MGIKO Selenium MOIKO ---Silver MGIKO ------· Sodium MOIKO Thallium MGIKO Tin MGIKO TOTAL CY ANIDB MOIKO Vanadium MOIKO Zinc MOIKO

NPSOOl 3l09318REG

515194

DV Result Qualifier

3230 IU

1.7 I 4U 0.21 u 0.41 UJ

17500CI 5.7

2 3.SJ

7080 2.9 8.4

52400 241

0.08 UJ 0.88 u 4.7 IIIU

0.21 UJ 0.6 u 180

0.41 u 2.9U

0.25 u 0.6.1 u 14.3

• APPENDIXG Vertncadon SoD Sampling Data

NPSOOl NPS003 3l09319REG 3l093:ZO REG

515194 515194 DV DV

Result Qualifier Result Qualifier

lllOCI 13400 1.~ u I..! u s.s I I~ I

63.1 94.3 0.7 O.B:.t 0.5 Ul 0.47 UJ

77100 4670 13.1 16.4 9.5 10.4

IH I 21.81 20800 2S400

u.s U.3 U.9 ll

14800 4020 712 609

0.09 Ul 0.1 UJ 1.8 3.1

19.3 21.6 218 127U

0.29 J 0.41 0.74U 0.71 u 81.1 43.3 0.35 u 0.25U

3.5U 3.3 u 0.25U 0.25U

1.7 0.71 u 55.5 70

• I ----I I I

NPS004 NPS005 NPS006 3109311 REG 3l09311REG 3l093l3REG

515194 515194 515194 ---DV DV DV Result Qualifier Result Qualifier Result Qualifier

9340 3530 9870 I.IU I.IU I..! u 7.31 3.7 J 4.9 I --

73.4 20.5 100 O.S4 0.22 u 0.6 ---0.4E Ul 0.44 Ul 0.53 J --2420 81400 20200 --12.8 5.7 14 9.8 3.9 8.9 ---·-

13.3 I 12.5 J 23.6J ----·-17900 1050C 171()(]

9 S.l 23.6 --7 7.9 lUi -·---

201~ 40600 7430 ---695 219 551 0.08 UJ 0.07 UJ 0.42 ~----

2.3 2.5 1.9 --13.1 II IS.7 124 u 118U 134 u·--

--0.43 J 0.21 UJ 0.42 J 0.69U 0.66U 0.74 u ---35.7 12~ 57.9 0.3~ u 0.21 u 0.3 u 3.~ u 3.1 u 3.9

0.25 u 0.25 u 0.25 u u 1.9 1.8

- ~!-5 --39

--60.9

---

w::: ~· § c;· Q. ::I .,

Of r

~

f

g ~

l ~i ~~ {;;p :ge .... -::!!

6: w l

.,~ ~1 9S: c:;o

• • APPENbiXG

Verlncadoii Sod saiii~lliit bili

~:~~-~:~,~~~::__ =~ ----- 1----~J ----.--f----J~~=== . -~---=~-'=--~~---~:~~--!-. -_-----~---== !·~!£SG"'fi•IV ___ ·---- ___ ----- NPSOOI NPSOOJ ----- _______ N~-- ....... _ ·-----!46SttmpkiV --- ----~!~~!!. J209lltiiG ... JZ09U!_~ ........... _ .. ___ _

s=~-~~:~:~.:" == --Resall I :.c ~T-!Y Qtaalllkr Rnt I ~ -- -1-tw gu•llner Raull J- -:'J:~- ~ .. -----· !!Y gu.uner _

;:s:~~;;~2:- mE~----~~ -- 1§~-----~~t::i -~~~ijL;:~~-CS-~! ____ -------~--~ '!c'!! U!B-0!~- 0 ...... _ . UlB-01~ 2.628-01

T;hluml_____ --~·-Unlb-~- --~---

if.-J ________ .. _____ -pa;;j- - 2.698-01+/- --Uiii)~jj 1 ,_.,8-Q,.,J __ !:!!!!:!!r 1 •·iiiiill:l=!-!?_!!:~m.- _-- ---=-=:

~:~_-5~--~::~==--J~=~I- 6.S88t00t/J===-=-~~~-~~~- I U98tGitlj_ __ .!~~~--------1 __ , __ ,, ______ , ·--- .. . . - --·- .. ----·

~~:f __ 1.0l8!~ .: .-·_·--~-.~--=-

~~·--~=~~-::·:~~=ta~~in . :~~E- -~_jf=~i -_-}~[:_;-~-Pu-2l9

1'11-242

Ga~~~-~-~-==·~· u;;l.;-~=~==t------I 1------•·---·--

.~adlu~_-226 .... ___ PCm __ B.JOE·U!_ NA.1 1 -·-· w._ __ ,_~_J9e-on=~JiA lti ~-:~:----~~ ----~· .. _, ______ , ...... ,_,_, ____ _

Slronllum !HI I Unlll sR.iii ___ ... _ .. ____ ~ I'CIIO -1 z.09B-Oh/-l ... 948.o!l~ 1 J.69a.oatlj = --------··-----~---•----•-------• I 1-lsoloplc Tbortuan Unlll Tll·221 -;em- --USB-Oitl- 7.868-02 . •.

ib.ijjj_____ ~I'CKJ=I ·-!!e-o·~ _ ....... !li· .. ,____ I-PC!!!!_ 1.988-0I*l 7.428-02

---1 , ___ .................. -----·

Tll·2lZ

·---1 --·------- ........... ----·--·-lsolorkUnnlum'·----"~··-u-n-111-l-- ---I------I·

U-=ii4 ' - -Pero-~--4.ii9i-Oit1-l !-72B-Oli·====-=--=--=--=--I,I--9:-.-:-:II::B-O~It~lil •--~~=-:i~::::j ·::~ii~ ~- ~-~=--~~~-=-~ u:n;--·-·- .. ·---------,- rc110· u-:m---·-·---- --;cw-

1.908-0Zti -,1!!::!:! _________ I J.n8.oltt U48-01 • • ·- •

-·

~::::

~: [ g 'tl or

r

~

f

~ f

rl ~f .... -:n

6:

i ::l

'tl~ d'cl'i " ::I 9~ ::::o

-·' • APPENDJXG

VeaiOcaiJon Soli Sam1•llng Uaha

• ·:~~~:::::::. ~···~'! ~1

____ ~~ -~=~~~B..:--!·· - - c--;;-...., -I~ == -~:.~---~: -:~~~~~:-I_:~:::-::~-~ ~~~~!! !~'- -----_ ---· ___________ l109UI ~EG ----- lZ09JJ1 REG ll09J1J REG -··-····- ·-------·---·-··--·--··-·· ~!'.!!'1~~~!!!~!~~0.·!! _____ -----· ,------~519 .. _--,- ·--~-

······--··--·--- ---·· --!~-- ·- VNC ___ f -~!_QuaUOcr Rcsull J __ VNC _

51519-a Rcsull I IJNC .. !!! 9!!!!!!!!! . . ~! 9!!•UDcr _

Gamma Sun AM-W--

UuiiJ

~~~:~ ~~ =~-- tjrt~!i l=i~E ~~~~r ~JJ~~~-:~~ N.~~!!! •..... ------~- ==~--~~---·_-------·--1 I J-----·-··. __ .. __ .. ··-·····----- ____ 1. e '''

-------··----- ..... ··------·--- ··• ------···--

~I I 6.61E-Ol+/-l ).761!-0~J _____ J_!:!~~:~!~:I.--•·~1!-0IJ~---·-·-·--··-

-~-- -=~]- ~~]--::~:.~~E~~~:.- I 1---Gamn111 Scan ------· K-40 ·----I l.OSI!tGh/f--iiiiet~r===x- 1:81E!~!!!f= 1.7BE~ ~---~--~--- ~:.~--~

i~~~~r~~i;i?~;!~~--:== u-;u.~- === ----~----- --~------- . ~=-== =--=--=-==· ==-~------ -------- ----·. ·---PU-218 PCI/0 1.988-01t/- I.UE-0 U :UIE-411+/- NA UJ 8.988-0lt/- NA UJ Pu-.l:i9-- -- . -· PCI/0 . UlE-411t/- NA UJ 4.9lE-4ll+/- NA UJ . -i:nE-01;;: ·-· NA UJ -------·--·-- .. -------· --- ----- --·--- -~ --·-- ---·-- ---------· ------ ----·--···----I'U-242 PCI/0 4.46E·01t/· NA UJ 1.71E-411t/- NA UJ 1.11E-02t/· NA UJ - ·----- ·-----·- -·· ......... ---··-·-··-- ···--· -·-···--·

Gamma Spec iRadium-226

Strunlhuullll

SR-90

-... -.:=---=j• u~ii;·~~=-~==-~---~~~=-=j·· I -~==~- ----· ----···---- •--·····-- -··-. ····---. PCI/0 --~3~:~! .... -------i.&. U _1.68E-OI 1 ___ -..M_I_Q ______ , __ ~-~~~!~~ ; ______ tJA.

----···--····

-~=~ ··_ ·r-~;~~~~!~l=:~s.4oe.:ju--3--:~~=r-- ·----~·:8-0!1- -- -F -~-!~-~!!!·l.: ___ ~i:!~oH~:.·.·-~:·.::_-.~= hotut•l.: l"borhuu UuiU

~I[~- =-=-- ~~ -:::::: ~ y_;;;~ -~=--:::~:; I :~:::~ ___ ::!~::~!-· ----~= +~;;~z. ~~--- ~·~~~ F--·- -=~---_ TII-212 PCIIO 1.04Et00t/- 1.18E-OI J U7E-Git/· 9.441!-02 I.OIEtOO•I- 2.111!-01 J ~·······-· ···-·· ····-----·-·- ----- ------ ------- - -------- ----·----- -----

!~~~ !'~!!!~~~! ----U-114

UuiU ---·--·--·· ·•···------·· 1------t---

PCI/0 ·!==9.298-0t--;/: =~~]~E-01 -~ 9.188-Glt/- ---~=!86.E·ii!~,:=_!~IE.~!,.==~== ----I PCI/0 __ S.~!t _ 1.678-02 6.098-Glt/- 4.lOE-02t/- ___ 1.~ -----

PCI/0 9.44E-Oitl- l.SlE-01 1.76E-Gh/- . -U-llS ----·---U-118 !I.ZII!-Oit/· I.SSE-01

NA = Not Applicable

•

•

~n~EGc.G MOUND APPLIED TECHNOLOGIES P.O. BOX 3000 MIAMISBURG. OHIO 45343-3000• TEL (513) 865-4020

Mr. Arthur W. Kleinrath Project Engineer, Team Leader, MB U.S. Department of Energy Miamisburg Area Office P.O. Box66 Miamisburg, OH 45343

Dear Mr. Kleinrath:

Attached for your review are two copies of the . This document incorporated the resolution to the regulator comments on the Draft submittal. The comments with responses are also attached. With your concurrence, copies have been forwarded to Mr. Tim Fischer [U.S. EPA), Ms. Regina Bayer [Ch2M Hill), Mr. Brian Nickel [Ohio EPA), Ms. Jenifer Kwasniewski [Ohio EPA), Mr. John Sands [DOE/EM-40), Mr. George Rael [DOE/ AL) and Mr. Doug Draper [MMES/HAZWRAP).

If you require additional information, please contact me at [513) 865-3859 .

Approved: Charles S. Friedman Vice President ER&WM

cc w/ o enclosure: Charles S. Friedman [EG&GJ '0omaMnar=n~s~:'·~:_: :teG&Gl: · · ' Jim Zahora [EG&G)

cc w/ enclosure: Tim Fischer Brian Nickel Regina Bayer Jenifer Kwasniewski John Sands Gecirge Rael Doug Draper

[U.S. EPA)- 2 copies [Ohio EPA)- 3 copies [Ch2M Hill) [Ohio EPA) [DOE/EM-40) [DOE/AL) [MMES/HAZWRAP)

Sincerely,

/)I '· I If . \. { I ? ,.. i ' ' . ./, .. -et- -'-? .. Y· ~ . - . '· I . , ..

. ~ S. Alan Spes~rd

c '.

OU-5 Manager

State of Ohio Environmental Protection Agency

A ~,outhwest District Office ~South Main Street

, • · Dayton, Ohio 45402-2086 (513) 285-6357 FAX (513) 285-6404

January 3, 1995

Arthur Kleinrath US DOE Miamisburg Area Offic e 1 Mound Road P.O. Box 66 Miamisburg, Ohio 45343-0066

Dear Mr. Kleinrath:

~ - C'LA5

,J £_ t.-0 PtZO p

RE: US DOE MOUND MONTGOMERY COUNTY OU5 NEW PROPERTY PHASE I FIELD REPORT

George V. Voinovich Governor

The Ohio Environmental Protection Agency has received the responses to its comments on the

• draft The Ohio Environmental Protections Agency finds the responses to be adequate. It is the Agency's understanding that the document will be made available to the public with regulatory comment.

Should there be any questions concerning the above, please contact Kathy Lee Fox at (513) 285-6441 or me at (513) 285-6468.

Sincerely,

L //'2.-,/ Brian Nickel Mound Project Manager Office of Federal Facilities Oversight

cc: T. Fisher, USEPA Region V /. M. Williams, EG&G Mound J. Zahora, EG&G Mound A. Spesard, EG&G Mound K. Fox, OEPA/OFFO

@ Primed on recycled paper

OPERABLE UNIT 5 NEW PROPERTY PHASE I FIELD REPORT

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