Calibration of Thermocouples.
33
LSN Reviews From: Sent: To: Attachments: Alka Jain [[email protected]] Thursday, August 03, 2006 10:30 AM Don Bannon lab notebook.doc; TCALREGRESSIONAPRI3-26, 2006.xls; T_CALREGRESSIONAPR15-16, 2004.xls Please save the attachments. Alka
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Transcript of Calibration of Thermocouples.
LSN Reviews
From:Sent:To:Attachments:
Alka Jain [[email protected]]Thursday, August 03, 2006 10:30 AMDon Bannonlab notebook.doc; TCALREGRESSIONAPRI3-26, 2006.xls;T_CALREGRESSIONAPR15-16, 2004.xls
Please save the attachments.
Alka
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AJ, Mayl5, 2006
Calibration of Thermocouples
Equipment and Supplies:1. Calibrated glass-mercury thermometer (range: 0-500C, graduations: 0.1 0C, S/N 1709,AN 007617, calibration date: July 14, 2005; calibration due: July 14, 2006)2. 39 Type T self adhesive thermocouples (Omega Engineering Inc., model SAl-T-72)3. 60 type non adhesive thermocouples (Omega Engineering Inc., model 5SC-TT-T-30-72)4. 20 5K-ohm thermistors (Omega Engineering Inc., model ON-901-44007)5. Thermocouple connectors (Omega Engineering Inc., model SMP-T-F and model SMP-T-MF)6. Coming stirrer hot plate7. Magnetic stirrer8. HP 34970A Data Acquisition/Switch Unit including three channel data logger cards(S/N MY44010920, AN 012033, calibration date: Jan. 27, 2006; cal. due: Jan. 26, 2007)9. HP Bench Link Data Logger Software, version 1.1, 199710. Thermocouple wire (Omega Engineering Inc., model TT-T-24SLE, lot #'s ICP12629PTCC012827P, ICP12794P IHCO13000P)11. One 3.5L glass beaker12. DI Water
Procedure:99 Type T thermocouples (39 adhesive and 60 non adhesive) and 20 5K-ohm thermistorsare placed in 3.5L glass beaker more than half filled with DI water. The beaker is placedon hot plate and water is continuously stirred using magnetic stirrer to maintain uniformtemperature. Various temperature settingswere obtained by adding cold and hot water.The beaker was insulated with layers of bubble wrap and paper towel. The hot plate iskept warm for higher temperature settings in order to maintain constant temperaturesduring measurements. Several temperature measurements were taken between 200C and500C.Allow water bath to stabilize and collect 17 temperature measurements per thermocoupleand per thermistor in rapid fashion, within 10 seconds using automated data logger. Raisethe water temperature to next temperature setting, allow temperature to stabilize, collect17 temperature measurements per thermocouple and per thermistor, and so on until theentire range is represented. Increments of temperature at each step are approximately 40C.Average temperature is calculated for each thermocouple and thermistor at alltemperature settings and recorded. These data points are plotted against standardtemperature settings to generate regression curve. The computed slopes and intercepts(offset) are utilized for temperature correction (see attached data Table 1).
TABLE1: Channel Number, CorrespondingThermocouple/Thermistor and Corresponding Slopeand Intercept Configuration in HP Data Logger
TABLEI: Channel Number, CorrespondingThermocouple/Thermistor and Corresponding Slopeand Intercept Configuration in HP Data Logger
TABLEI: Channel Number, CorrespondingThermocouple/Thermistor and Corresponding Slopeand Intercept Configuration in HP Data Logger
TABLEI: Channel Number, CorrespondingThermocouple/Thermistor and Corresponding Slopeand Intercept Configuration in HP Data Logger
TABLE1: Channel Number, CorrespondingThermocouple/Thermistor and Corresponding Slopeand Intercept Configuration in HP Data Logger
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1 2 3 4 5 6 7 0 9 10 11 12 13 14 15 16 17 Is 19 20 21 22 22 24 25 20 27 28 20 30
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