Drug Analysis Test No. 19-502 Summary Report

Drug Analysis Test No. 19-502 Summary Report

Collaborative Testing Services, IncFORENSIC TESTING PROGRAM

P.O. Box 650820 Sterling, VA 20165-0820

e-mail: [email protected]: +1-571-434-1925

Website: www.cts-forensics.com

Each sample pack consisted of two questioned samples containing powder substances, which participants were requested to analyze. Data were returned from 527 participants and are compiled into the following tables:

PageReport Contents:

Manufacturer ' s Information 2

Summary Comments 3

Table 1 a : Drug Analysis ( Item 1 ) 4

Table 1 b : Examination Methods ( Item 1 ) 15

Table 2 a : Drug Analysis ( Item 2 ) 30

Table 2 b : Examination Methods ( Item 2 ) 40

Table 3 : Additional Comments 55

Appendix : Data Sheet

This report contains the data received from the participants in this test. Since these participants are located in many countries around the world, and it is their option how the samples are to be used (e.g., training exercise, known or blind proficiency testing, research and development of new techniques, etc.), the results compiled in the Summary Report are not intended to be an overview of the quality of work performed in the profession and cannot be interpreted as such. The Summary Comments are included for the benefit of participants to assist with maintaining or enhancing the quality of their results. These comments are not intended to reflect the general state of the art within the profession.

Participant results are reported using a randomly assigned "WebCode". This code maintains participant's anonymity, provides linking of the various report sections, and will change with every report.

Drug Analysis Test 19-502

Manufacturer's InformationEach sample pack consisted of two items. Item 1 contained 300 mg of powder consisting of acetaminophen. Item 2

contained 295 mg of powder consisting of approximately 2% Methylphenidate Hydrochloride and 98% lactose.

Methylphenidate is a Schedule II controlled substance in the United States.

SAMPLE PREPARATION-

The acetaminophen in Item 1 was a pure powder. The methylphenidate hydrochloride in Item 2 was a pure powder

that was combined with lactose. The two powders were mixed thoroughly to ensure homogeneity.

ITEM 1 (PREPARATION): Approximately 300 mg of the powder was weighed out and deposited into a glassine bag

which was folded and secured with a label. The folded glassine bag was placed into a small zip top bag, which was

heat sealed and then placed into a pre-labeled envelope.

ITEM 2 (PREPARATION): Approximately 295 mg of the powder containing methylphenidate hydrochloride was

weighed out and deposited into a glassine bag which was folded and secured with a label. The folded glassine bag

was placed into a small zip top bag, which was heat sealed and then placed into a pre-labeled envelope.

SAMPLE PACK ASSEMBLY: One of each of the Item 1 and Item 2 envelopes was placed into a larger pre-labeled

sample pack envelope.

VERIFICATION: The above substances were identified by predistribution laboratories, who used the following

combined list of techniques: color tests, FTIR, GC, and GC/MS.

( 2 )Printed: December 12, 2019 Copyright ©2019 CTS, Inc


Summary Comments

This test was designed to allow participants to assess their proficiency in the qualitative analysis of questioned

samples that may contain controlled substances. Item 1 contained a powder consisting of acetaminophen, also

known as paracetamol. Item 2 contained a powder consisting of lactose and approximately 2% methylphenidate

hydrochloride. In the United States, methylphenidate is a Schedule II controlled substance (See Manufacturer's

Information for preparation details).

All 527 participants reported that no controlled substance was identified in Item 1. Many participants reported in

their results and/or additional comments that acetaminophen was found in Item 1. For Item 2, 522 of 527

participants (99.1%) reported methylphenidate. One participant reported a presumptive identification of

threo-propylphenidate. The remaining four participants reported "No controlled substance detected/identified",

however two of these participants mention methylphenidate in their additional comments.

The most common examination methods utilized for both items include GC/MS, color tests, and FTIR.



Drug Analysis (Item 1)

TABLE 1a - Item 1 Results

Controlled Substance Detected Controlled Substance DetectedWebCode WebCode

No controlled substance detected/identified22NWVG

No controlled substance detected/identified23FFXX

No controlled substance detected/identified2CHQW8

No controlled substance detected/identified2D92NZ

No controlled substance detected/identified2EAA7R

No controlled substance detected/identified2EATV9

No controlled substance detected/identified2F8K7Z

No controlled substance detected/identified2HRTGG

No controlled substance detected/identified2J6YUQ

No controlled substance detected/identified2J8NZ9

No controlled substance detected/identified2LPXY8

No controlled substance detected/identified2M37TM

No controlled substance detected/identified; Acetaminophen

2NC3C7

No controlled substance detected/identified2NDFUD

No controlled substance detected/identified2NJZYP

No controlled substance detected/identified2PZNUV

No controlled substance detected/identified2U9YKC

No controlled substance detected/identified2Y4RUY

No controlled substance detected/identified32V2R8

No controlled substance detected/identified34PG4A

No controlled substance detected/identified379ZYK

No controlled substance detected/identified38DG8X

No controlled substance detected/identified38QPM7

No controlled substance detected/identified38TZGA

No controlled substance detected/identified39DMF6

No controlled substance detected/identified3AFCHZ

No controlled substance detected/identified3AJ3LX

Acetaminophen3CTXU9

Paracetamol3EFPDQ

No controlled substance detected/identified3EHGJD

No controlled substance detected/identified3MF3V8

No controlled substance detected/identified3PNQC3

No controlled substance detected/identified3T8AEF

No controlled substance detected/identified3W7KAF

No controlled substance detected/identified3WM8Y3

No controlled substance detected/identified3X2DRY

No controlled substance detected/identified3YJBEW


42QWUA

No controlled substance detected/identified42RZDD

No controlled substance detected/identified4439N4

No controlled substance detected/identified48M7CU

No controlled substance detected/identified48NVJC

No controlled substance detected/identified4A3BEQ

No controlled substance detected/identified; Contains Acetaminophen

4A6EBT

No controlled substance detected/identified4C6BEN

No controlled substance detected/identified4CGZCF

No controlled substance detected/identified4CM8XB

No controlled substance detected/identified4EJJU4

No controlled substance detected/identified4G3TT3

No controlled substance detected/identified4GAJET

No controlled substance detected/identified4H6HUX





No controlled substance detected/identified4HLUAH

No controlled substance detected/identified4HY7DA

No controlled substance detected/identified; acetaminophen (paracetamol)

4J6P6Q

No controlled substance detected/identified4P6XHK

No controlled substance detected/identified4PTB8B

No controlled substance detected/identified4WZA62

No controlled substance detected/identified4X9YYR

No controlled substance detected/identified4XKLCM

No controlled substance detected/identified4XV8L4

No controlled substance detected/identified638VW6

No controlled substance detected/identified; Acetaminophen indicated

63CAA6

No controlled substance detected/identified6A2LZL

No controlled substance detected/identified6BF7QB

No controlled substance detected/identified6BK2ET

No controlled substance detected/identified6BWUZV

No controlled substance detected/identified6D78VY

No controlled substance detected/identified6FW7CH

No controlled substance detected/identified6KD63P

No controlled substance detected/identified6LD2RC

No controlled substance detected/identified6MT7M4

No controlled substance detected/identified6UPYLX

No controlled substance detected/identified6WDT3Y

No controlled substance detected/identified6XTW7Q

No controlled substance detected/identified6ZYKZ2

No controlled substance detected/identified73AUWX

No controlled substance detected/identified74YDCB

No controlled substance detected/identified78AZQV

No controlled substance detected/identified798ARZ

No controlled substance detected/identified7C6YZK

No controlled substance detected/identified7DF93B


7F7B8Y

No controlled substance detected/identified7H9UR8

No controlled substance detected/identified7JQRCJ

No controlled substance detected/identified7KFNPW

No controlled substance detected/identified7L92D4

No controlled substance detected/identified7LCE68

No controlled substance detected/identified7MELNX

No controlled substance detected/identified7PDMAG

No controlled substance detected/identified; acetaminophen

7PRZND

No controlled substance detected/identified7QU6FE


7X2KRA

No controlled substance detected/identified7ZQXAR

No controlled substance detected/identified82Z2WG

No controlled substance detected/identified84PDFU

No controlled substance detected/identified89N2T3

No controlled substance detected/identified8AV9BF

No controlled substance detected/identified8BC2QR

No controlled substance detected/identified8BJJAV

No controlled substance detected/identified8DZBJB

No controlled substance detected/identified8ER66U

No controlled substance detected/identified8EVW7B

No controlled substance detected/identified8G24P3





No controlled substance detected/identified8GJ7L4

No controlled substance detected/identified8L8CWE

No controlled substance detected/identified8N47ZV

No controlled substance detected/identified8NFYLW

No controlled substance detected/identified8PTGT9

No controlled substance detected/identified8QN3F9

No controlled substance detected/identified8RG9HK

No controlled substance detected/identified8TDM9J

No controlled substance detected/identified8U7W3F

No controlled substance detected/identified8UL3H6

No controlled substance detected/identified8XL498

No controlled substance detected/identified8Y7JD3

No controlled substance detected/identified8YX4NA


92VZG9

No controlled substance detected/identified93WFZ7


96UGNB

No controlled substance detected/identified96Z3P4

No controlled substance detected/identified9BH9QX

No controlled substance detected/identified9DCCYH

No controlled substance detected/identified9GPP9Y

No controlled substance detected/identified9GVH7R

No controlled substance detected/identified9L72F2


9Q2BMZ

No controlled substance detected/identified9QVGR2

No controlled substance detected/identified9T2VN8

No controlled substance detected/identified; Acetaminophen Confirmed

9VBHWQ

No controlled substance detected/identified9VV2CJ

No controlled substance detected/identified; Contains acetaminophen

9WP244

No controlled substance detected/identified; Analysis indicates presence of acetaminophen.

9ZFW8P

No controlled substance detected/identifiedA2GH2E

No controlled substance detected/identifiedA2Z298

No controlled substance detected/identifiedA3EQAY

No controlled substance detected/identifiedA46PQH

No controlled substance detected/identifiedA6ZD68

No controlled substance detected/identifiedA7FLEL

No controlled substance detected/identifiedA9GZGR

No controlled substance detected/identifiedAAPJFH

No controlled substance detected/identifiedAB3L8T

No controlled substance detected/identifiedACVYUZ


AD7U78


AT9QWQ

No controlled substance detected/identifiedAUBBGY

No controlled substance detected/identifiedAVBKWG

No controlled substance detected/identifiedAZE79L


B28CAX

No controlled substance detected/identifiedB4XM2Q

No controlled substance detected/identifiedBAY2HL

No controlled substance detected/identifiedBBJXPY


BCEHCX


BCVWF2





No controlled substance detected/identifiedBEQ4QR

No controlled substance detected/identifiedBFWXNB

No controlled substance detected/identifiedBHVR83

No controlled substance detected/identifiedBJD9VM

No controlled substance detected/identifiedBJUGL4

No controlled substance detected/identifiedBMVGUM


BNKCBJ

No controlled substance detected/identifiedBWEH6A

No controlled substance detected/identifiedBZEUYP

No controlled substance detected/identifiedC29CK4

No controlled substance detected/identifiedC6UZDG

No controlled substance detected/identifiedC7VKPN

No controlled substance detected/identifiedC9FQRR

No controlled substance detected/identifiedCAFJAY

No controlled substance detected/identifiedCC37GR

No controlled substance detected/identifiedCDGFRD

No controlled substance detected/identifiedCE3CTY

No controlled substance detected/identifiedCF9URU

No controlled substance detected/identifiedCFPXEU

No controlled substance detected/identifiedCGXUKE

No controlled substance detected/identifiedCJRH4A

No controlled substance detected/identifiedCMUC7K

No controlled substance detected/identifiedCQ2VVD

No controlled substance detected/identifiedCRMW9L

No controlled substance detected/identifiedCUTCLJ

No controlled substance detected/identifiedCVJKM9

No controlled substance detected/identifiedCY3TV9

No controlled substance detected/identifiedCYTFTY

No controlled substance detected/identifiedCZRPX2

No controlled substance detected/identifiedD4LYAM

No controlled substance detected/identifiedD63ZNB

No controlled substance detected/identified; Paracetamol

D763UD

No controlled substance detected/identifiedD7GZQH

No controlled substance detected/identifiedDALLLV


DARLB4

No controlled substance detected/identifiedDERDFZ

No controlled substance detected/identifiedDF2QDP

No controlled substance detected/identifiedDK2JK8

No controlled substance detected/identifiedDLTXVX

No controlled substance detected/identifiedDNWCGM

No controlled substance detected/identifiedDQ6ECU

No controlled substance detected/identifiedDRV8Z6

No controlled substance detected/identifiedDUXY3Q

No controlled substance detected/identifiedDVKRAZ

No controlled substance detected/identifiedDW9UUA

No controlled substance detected/identifiedDY6N7R

No controlled substance detected/identifiedDZPCU7

No controlled substance detected/identifiedDZU9HP

No controlled substance detected/identifiedDZWPV2

No controlled substance detected/identifiedE7RLZY

No controlled substance detected/identifiedE8KJ96

No controlled substance detected/identifiedE9KV8Z

No controlled substance detected/identifiedEB2VYU





No controlled substance detected/identifiedEDNEZR

No controlled substance detected/identifiedEE2436

No controlled substance detected/identifiedEHK6E4

No controlled substance detected/identifiedEMXT99

No controlled substance detected/identifiedEUY667

No controlled substance detected/identifiedEXDP6Z


EZ4ZWT

No controlled substance detected/identifiedF2ZD9H

No controlled substance detected/identifiedF3NBG4


F4HXWT

AcetaminophenF7RQMR

No controlled substance detected/identifiedF9TJTJ

No controlled substance detected/identifiedFAA6E2

No controlled substance detected/identifiedFAMTMF

No controlled substance detected/identifiedFEZULR


FF2QNU

No controlled substance detected/identifiedFGX9ZG

No controlled substance detected/identifiedFN98ZF

No controlled substance detected/identifiedFNLU32

No controlled substance detected/identifiedFPHCD4

No controlled substance detected/identifiedFQ3EGC


FR6UFW

No controlled substance detected/identifiedFRNCEG

No controlled substance detected/identifiedFVAG78

No controlled substance detected/identifiedFW97QA

No controlled substance detected/identifiedFZYEZH

No controlled substance detected/identifiedG29BVT

No controlled substance detected/identifiedG3BFPF

No controlled substance detected/identifiedG3P274

No controlled substance detected/identifiedG4462V

No controlled substance detected/identifiedG72CZT

No controlled substance detected/identifiedG84ZKD

No controlled substance detected/identifiedG93M8N

No controlled substance detected/identifiedGD849Q

No controlled substance detected/identifiedGEZG8G

No controlled substance detected/identifiedGFWR8Q

No controlled substance detected/identifiedGJ4W8K

No controlled substance detected/identifiedGKU7UF

No controlled substance detected/identifiedGLKGMU

No controlled substance detected/identifiedGN2ACW


GRJTWR

ParacetamolGT79AF


GTJHQN

No controlled substance detected/identifiedGTZ49J

No controlled substance detected/identifiedGWR42E

No controlled substance detected/identifiedGX4YM7

No controlled substance detected/identifiedH33BGB


H4JX7X

No controlled substance detected/identifiedH6G8N9

No controlled substance detected/identified; Acetaminophen was detected but this is not controlled

H82CRB

No controlled substance detected/identifiedH98RVH






HAB7WC

No controlled substance detected/identifiedHC4Y99


HE9PZV

No controlled substance detected/identifiedHF9332

No controlled substance detected/identifiedHFCPGU

No controlled substance detected/identifiedHGJRJR

No controlled substance detected/identifiedHJNYPK

No controlled substance detected/identifiedHJPD9D


HM9JGM

No controlled substance detected/identifiedHPDXCT


HQ6HZ8

No controlled substance detected/identifiedHQQMF7

No controlled substance detected/identifiedHUMQY8

No controlled substance detected/identifiedHV4U3Y

No controlled substance detected/identifiedHYEZ96


HZTHAP

No controlled substance detected/identifiedJ64TZY

No controlled substance detected/identifiedJ73MP2

No controlled substance detected/identifiedJ9MXMZ

No controlled substance detected/identifiedJAJU9U

No controlled substance detected/identifiedJARGEG

No controlled substance detected/identifiedJBP7YJ


JEA3UN

No controlled substance detected/identifiedJF3Z2V

No controlled substance detected/identifiedJJEM6T

No controlled substance detected/identifiedJKGK3P

No controlled substance detected/identifiedJNGVXP

No controlled substance detected/identifiedJPK8EK

No controlled substance detected/identified; Acetaminophen, OTC.

JW7638

No controlled substance detected/identifiedJYBYTP

No controlled substance detected/identifiedJZNBRU

No controlled substance detected/identifiedK382YC

No controlled substance detected/identifiedK3CWNV

No controlled substance detected/identifiedK4TWZX

No controlled substance detected/identifiedK6QZBL

No controlled substance detected/identifiedK8678N

No controlled substance detected/identifiedKDWRH3

No controlled substance detected/identifiedKFT83E

No controlled substance detected/identified; Acetaminophen detected

KGAA4L


KGP6MD

No controlled substance detected/identifiedKK4B3E

No controlled substance detected/identified; Only paracetamol detected.

KLDBAG

No controlled substance detected/identifiedKN87X4

No controlled substance detected/identifiedKPTU2Y

No controlled substance detected/identifiedKQ4VNX

No controlled substance detected/identifiedKRH8JG


KT3THR

No controlled substance detected/identified; Acetaminophen (non-controlled) identified

KT7Y9R

No controlled substance detected/identifiedKUB2NQ

No controlled substance detected/identifiedKWMR4L





No controlled substance detected/identifiedKWRK4Z

No controlled substance detected/identifiedKZLBFD

No controlled substance detected/identifiedL6T6AV

No controlled substance detected/identifiedL9L79N

No controlled substance detected/identifiedLAWY3D

No controlled substance detected/identifiedLB28QH

No controlled substance detected/identifiedLC9PAL

No controlled substance detected/identifiedLD63AL

No controlled substance detected/identifiedLDUGZ6

No controlled substance detected/identifiedLEHGXU

No controlled substance detected/identifiedLEYM68

No controlled substance detected/identifiedLFYE3K

No controlled substance detected/identifiedLJUH3Y

No controlled substance detected/identifiedLME8MC

No controlled substance detected/identifiedLNTUYY

No controlled substance detected/identifiedLQT4U9

No controlled substance detected/identifiedLRAKHT


LUF68E

No controlled substance detected/identifiedLXFCQQ

No controlled substance detected/identifiedLZ7DWE

No controlled substance detected/identified; Detected acetaminophen in the sample by GCMS.

M8NA88


MA3KGX

No controlled substance detected/identifiedMBRV8Q

No controlled substance detected/identifiedMDPHJ2

No controlled substance detected/identifiedMECYZH

No controlled substance detected/identifiedMEK372

No controlled substance detected/identifiedMFGD7A

No controlled substance detected/identifiedMG7PYN

No controlled substance detected/identifiedMGMXXQ

No controlled substance detected/identifiedMGRHFR

No controlled substance detected/identifiedMJU348

No controlled substance detected/identified; No controlled substances were detected in the powder, which contained paracetamol (also known as acetaminophen)

ML9PA8

No controlled substance detected/identifiedMQEJV3

No controlled substance detected/identifiedMTXP3C

No controlled substance detected/identifiedMTYR4W

No controlled substance detected/identifiedMURPC4

No controlled substance detected/identifiedMWWZYC

No controlled substance detected/identifiedMX922T

No controlled substance detected/identifiedMXUNMW


N2NXFU

No controlled substance detected/identifiedN3ETMG

No controlled substance detected/identifiedN3GVN2

No controlled substance detected/identifiedN62WCW

No controlled substance detected/identifiedN6PK6X

No controlled substance detected/identifiedN7X6PL

No controlled substance detected/identifiedN8F6Y4

No controlled substance detected/identifiedN9KQFN

No controlled substance detected/identifiedNBB2H3

No controlled substance detected/identifiedNBEFU4

No controlled substance detected/identifiedND7VKJ

No controlled substance detected/identifiedNEC6AP





No controlled substance detected/identifiedNGEW9P

No controlled substance detected/identifiedNJHM6J

No controlled substance detected/identifiedNL8XB4

No controlled substance detected/identifiedNNEF9Y

No controlled substance detected/identifiedNWFVPD

No controlled substance detected/identifiedNZYAVY

No controlled substance detected/identifiedP2RFVQ

No controlled substance detected/identifiedP2YU4R

No controlled substance detected/identifiedP4YKNE

No controlled substance detected/identifiedP9M493

No controlled substance detected/identifiedPAD4DZ

No controlled substance detected/identifiedPAFDF4

No controlled substance detected/identifiedPCXZXK


PDQYZP

No controlled substance detected/identifiedPHWMAR

No controlled substance detected/identifiedPJYA4D

No controlled substance detected/identifiedPMYGPA

No controlled substance detected/identifiedPNAHB9

No controlled substance detected/identifiedPPYWGK

No controlled substance detected/identifiedPTTEER

No controlled substance detected/identifiedPVVPFE

No controlled substance detected/identifiedPWCQRG

No controlled substance detected/identifiedPWHZNM


PYHAGC

No controlled substance detected/identifiedQ22MUC

No controlled substance detected/identifiedQ3UYFY

No controlled substance detected/identifiedQB2BC9

No controlled substance detected/identifiedQCL4FR

No controlled substance detected/identifiedQF4BNR

No controlled substance detected/identifiedQH7MKL

No controlled substance detected/identifiedQHBFGF

No controlled substance detected/identifiedQKDZ7U


QLKA4T

No controlled substance detected/identifiedQNBGKA

No controlled substance detected/identifiedQPT7KL

No controlled substance detected/identifiedQQFR8H

No controlled substance detected/identifiedQQR4EF

No controlled substance detected/identifiedQWJ8P8

No controlled substance detected/identifiedR4MVCC

No controlled substance detected/identifiedR7NHQV

No controlled substance detected/identifiedR9UX4T

No controlled substance detected/identifiedRAUG6F

No controlled substance detected/identifiedRCF4YN

No controlled substance detected/identifiedRCKFKY

No controlled substance detected/identifiedRCTDGH

No controlled substance detected/identifiedRCX7EB

No controlled substance detected/identifiedRGDM49


RGG3TF

No controlled substance detected/identifiedRJ7G9G

No controlled substance detected/identifiedRJWJMR

No controlled substance detected/identifiedRLH6WN

No controlled substance detected/identifiedRPFRBJ





No controlled substance detected/identifiedRWQRRN

No controlled substance detected/identified; Acetaminophen, an over-the counter medication was identified.

T2BVWQ

No controlled substance detected/identifiedT4LH7V

No controlled substance detected/identifiedT7LQB7

No controlled substance detected/identifiedTBEC69

No controlled substance detected/identifiedTFXNJJ

No controlled substance detected/identifiedTGWLDD

No controlled substance detected/identifiedTMHNXB

No controlled substance detected/identifiedTMRAAC

No controlled substance detected/identifiedTXRZTY

No controlled substance detected/identifiedU2HY68

No controlled substance detected/identifiedU4XGYJ

No controlled substance detected/identifiedU8GMGE

No controlled substance detected/identifiedUAU2EE

No controlled substance detected/identifiedUAZCER

It contains paracetamol.UDC6BX


UF487E

No controlled substance detected/identifiedUL7GD8

No controlled substance detected/identifiedUNJRNH

No controlled substance detected/identifiedUNXEZ7

No controlled substance detected/identifiedUQ82Z6

No controlled substance detected/identifiedUR43VF

No controlled substance detected/identifiedUT7U4A

No controlled substance detected/identifiedUY3M44

No controlled substance detected/identifiedUZD9DJ

No controlled substance detected/identifiedV2PJA9

No controlled substance detected/identified; Acetaminofen

V9JB24

No controlled substance detected/identifiedVAJ72M

No controlled substance detected/identifiedVBAGTF

No controlled substance detected/identifiedVBDCGY

No controlled substance detected/identifiedVG6K2T

No controlled substance detected/identifiedVGFLL7

No controlled substance detected/identifiedVKMUC4


VMN8DA

No controlled substance detected/identifiedVMV6BT

No controlled substance detected/identified; Acetaminophen/paracetamol

VN49RX

No controlled substance detected/identifiedVQ37RJ

No controlled substance detected/identifiedVQ863Z

No controlled substance detected/identifiedVQHQCF

No controlled substance detected/identifiedVRKRHT

No controlled substance detected/identifiedVRU6ZP

Paracetamol (acetaminophen) - Not confirmed

VUVFA7

No controlled substance detected/identifiedVXYZRC

No controlled substance detected/identifiedW4L64D

ParacetamolW4YYF8

No controlled substance detected/identifiedW6TKBJ

No controlled substance detected/identifiedW7Y7CC


W8JV2C

No controlled substance detected/identifiedWA3YL3

No controlled substance detected/identifiedWANCJF

No controlled substance detected/identifiedWB7PEB





No controlled substance detected/identifiedWB9YCW

No controlled substance detected/identifiedWC3MUR

No controlled substance detected/identifiedWDHHDJ

No controlled substance detected/identifiedWEK2XR

ParacetamolWLGVXL

No controlled substance detected/identifiedWLLQL6

No controlled substance detected/identifiedWNUFWM

No controlled substance detected/identifiedWPDQEZ

No controlled substance detected/identifiedWPZUBF

No controlled substance detected/identifiedWRWQ9V

No controlled substance detected/identifiedWTXBNA

No controlled substance detected/identifiedWU2HZA


WV6XW9

No controlled substance detected/identifiedWWN6QB

No controlled substance detected/identifiedWWPC6J

No controlled substance detected/identifiedX26HGQ

No controlled substance detected/identifiedX324EF

No controlled substance detected/identifiedX3A8HE

No controlled substance detected/identifiedX6DTMK

No controlled substance detected/identifiedX9F44Y

No controlled substance detected/identifiedXA7PHD

No controlled substance detected/identifiedXAGNE8

No controlled substance detected/identifiedXB344B

No controlled substance detected/identifiedXDTLKG

No controlled substance detected/identifiedXHG7UJ

No controlled substance detected/identifiedXK4RV8

No controlled substance detected/identifiedXKP6JK

No controlled substance detected/identifiedXLH3RQ

No controlled substance detected/identifiedXLJTXA

No controlled substance detected/identifiedXN73YF

No controlled substance detected/identified; No controlled or related substances were identified in Exhibit 1. Acetaminophen was identified in Exhibit 1.

XUF3ND

No controlled substance detected/identifiedXVNXUW

AcetaminophenXVZTYB

No controlled substance detected/identifiedXW2DKQ

No controlled substance detected/identifiedXW4NB9

No controlled substance detected/identified; Item 1 contains Paracetamol

XX8V82

No controlled substance detected/identifiedXXV4NK

No controlled substance detected/identifiedXYAKMJ

No controlled substance detected/identifiedY34KD6

No controlled substance detected/identified; Acetaminophen (non-controlled) was identified in the analysis.

YAMNL8

No controlled substance detected/identifiedYF6TPM

AcetaminophenYGH8DW

No controlled substance detected/identifiedYHYWUL


YLG4A9


YLTH46

No controlled substance detected/identified; acetaminophen indicated, No controlled or related substances identified

YMHRXE


YTEKW8

No controlled substance detected/identifiedYU3WXU

No controlled substance detected/identifiedYU9YB8

No controlled substance detected/identifiedYV2WHD





No controlled substance detected/identifiedYZZ7TF

No controlled substance detected/identifiedZ2BT4K

No controlled substance detected/identifiedZ98ZPU

No controlled substance detected/identifiedZEPU6X

No controlled substance detected/identifiedZG83ZQ

No controlled substance detected/identifiedZLNFVC

No controlled substance detected/identifiedZLQ3CQ

No controlled substance detected/identifiedZLY7YW

No controlled substance detected/identifiedZMZTZ9

No controlled substance detected/identified; Laboratory Analysis determined the presence of Acetaminophen.

ZNA3NZ

No controlled substance detected/identified; Acetaminophen (NCC)

ZPNMFA

No controlled substance detected/identifiedZQT3NM

No controlled substance detected/identifiedZRBBRA

No controlled substance detected/identifiedZYLYAJ

No controlled substance detected/identifiedZYXVD4

No controlled substance detected/identifiedZZKK3V

Response Summary - Item 1Participants: 527

Other: 0

527No Controlled substance(s) detected/identified:



Examination Methods (Item 1)TABLE 1b

Color Crystal UVFTIR GC/MSGC OtherLC MicroTLCWebCode

22NWVG

23FFXX

2CHQW8

2D92NZ

2EAA7R

2EATV9

2F8K7Z

2HRTGG

2J6YUQ

2J8NZ9

2LPXY8

weight2M37TM

2NC3C7

2NDFUD

2NJZYP

NMR, handheld Raman2PZNUV

2U9YKC

2Y4RUY

32V2R8

34PG4A

weight determination379ZYK

TruNarc38DG8X

38QPM7

38TZGA

39DMF6

3AFCHZ

3AJ3LX

QTOF LCMS3CTXU9

LC/MS3EFPDQ

3EHGJD

3MF3V8

Handheld Thermo Scientific TruNarc Raman Spectroscopy

3PNQC3

3T8AEF

3W7KAF

3WM8Y3



TABLE 1b


3X2DRY

3YJBEW

42QWUA

42RZDD

4439N4

48M7CU

48NVJC

4A3BEQ

4A6EBT

4C6BEN

4CGZCF

4CM8XB

4EJJU4

Screening4G3TT3

FTIR-ATR4GAJET

4H6HUX

4HLUAH

4HY7DA

4J6P6Q

4P6XHK

4PTB8B

4WZA62

4X9YYR

GC/IR4XKLCM

4XV8L4

638VW6

LC-TOF63CAA6

6A2LZL

6BF7QB

6BK2ET

6BWUZV

6D78VY

6FW7CH

6KD63P

6LD2RC

6MT7M4

6UPYLX



TABLE 1b


LC/MS/MS6WDT3Y

6XTW7Q

6ZYKZ2

73AUWX

74YDCB

78AZQV

798ARZ

7C6YZK

7DF93B

7F7B8Y

7H9UR8

7JQRCJ

7KFNPW

Raman spectroscopy7L92D4

7LCE68

7MELNX

7PDMAG

7PRZND

7QU6FE

7X2KRA

7ZQXAR

82Z2WG

84PDFU

89N2T3

Weight determination8AV9BF

FTIR with ATR accessory8BC2QR

8BJJAV

CHCl3/0.45N NaOH extraction prior to GC/MS run 1; direct in CHCl3 for run 2

8DZBJB

8ER66U

8EVW7B

8G24P3

8GJ7L4

8L8CWE

8N47ZV

8NFYLW

8PTGT9



TABLE 1b


8QN3F9

8RG9HK

8TDM9J

8U7W3F

8UL3H6

DART-TOF8XL498

8Y7JD3

8YX4NA

92VZG9

93WFZ7

96UGNB

96Z3P4

9BH9QX

9DCCYH

9GPP9Y

9GVH7R

9L72F2

9Q2BMZ

9QVGR2

9T2VN8

9VBHWQ

9VV2CJ

9WP244

TruNarc9ZFW8P

A2GH2E

A2Z298

A3EQAY

A46PQH

A6ZD68

A7FLEL

A9GZGR

DART-MSAAPJFH

AB3L8T

ACVYUZ

AD7U78

AT9QWQ

ATRAUBBGY



TABLE 1b


AVBKWG

AZE79L

B28CAX

B4XM2Q

NMR, LCMSBAY2HL

BBJXPY

BCEHCX

BCVWF2

BEQ4QR

BFWXNB

BHVR83

MarquisBJD9VM

BJUGL4

BMVGUM

FT-Raman, LC-MSBNKCBJ

BWEH6A

BZEUYP

C29CK4

C6UZDG

C7VKPN

C9FQRR

CAFJAY

CC37GR

RamanCDGFRD

Electronic BalanceCE3CTY

CF9URU

CFPXEU

RamanCGXUKE

CJRH4A

CMUC7K

CQ2VVD

CRMW9L

CUTCLJ

Portable Raman SpectroscopyCVJKM9

CY3TV9

CYTFTY

CZRPX2



TABLE 1b


D4LYAM

D63ZNB

D763UD

D7GZQH

DALLLV

DARLB4

DERDFZ

DF2QDP

DK2JK8

DLTXVX

DNWCGM

DQ6ECU

DRV8Z6

Two separate samplings in two GC/MS instruments used.

DUXY3Q

DVKRAZ

DW9UUA

DY6N7R

DZPCU7

DZU9HP

DZWPV2

E7RLZY

E8KJ96

E9KV8Z

EB2VYU

EDNEZR

EE2436

EHK6E4

EMXT99

EUY667

EXDP6Z

EZ4ZWT

F2ZD9H

F3NBG4

F4HXWT

GC-FIDF7RQMR

F9TJTJ

FAA6E2



TABLE 1b


FAMTMF

FEZULR

FF2QNU

FGX9ZG

GC/IRDFN98ZF

FNLU32

FPHCD4

FQ3EGC

FR6UFW

FRNCEG

FVAG78

FW97QA

FZYEZH

G29BVT

G3BFPF

G3P274

G4462V

G72CZT

G84ZKD

G93M8N

GD849Q

GEZG8G

GFWR8Q

GJ4W8K

GKU7UF

GLKGMU

Raman spectroscopyGN2ACW

GRJTWR

GT79AF

GTJHQN

GTZ49J

GWR42E

GX4YM7

H33BGB

H4JX7X

H6G8N9

H82CRB



TABLE 1b


H98RVH

LC=LC-QTOF-MSHAB7WC

HC4Y99

HE9PZV

HF9332

LCMSHFCPGU

HGJRJR

HJNYPK

HJPD9D

HM9JGM

HPDXCT

RamanHQ6HZ8

HQQMF7

HUMQY8

HV4U3Y

HYEZ96

HZTHAP

J64TZY

J73MP2

J9MXMZ

JAJU9U

LCMSJARGEG

JBP7YJ

JEA3UN

JF3Z2V

JJEM6T

JKGK3P

JNGVXP

JPK8EK

JW7638

JYBYTP

JZNBRU

K382YC

DART-TOFK3CWNV

K4TWZX

K6QZBL

K8678N



TABLE 1b


KDWRH3

TruNarc Handheld Raman Spectrometer

KFT83E

RamanKGAA4L

KGP6MD

KK4B3E

KLDBAG

Weight DeterminationKN87X4

KPTU2Y

KQ4VNX

KRH8JG

KT3THR

KT7Y9R

KUB2NQ

KWMR4L

KWRK4Z

KZLBFD

L6T6AV

L9L79N

LAWY3D

LB28QH

LC9PAL

LD63AL

LDUGZ6

FTIR-ATRLEHGXU

LEYM68

LFYE3K

LJUH3Y

FTIR with ATRLME8MC

LNTUYY

Accurate Mass - Orbitrap Mass Spectrometry

LQT4U9

LRAKHT

LUF68E

LXFCQQ

Weight determinationLZ7DWE

M8NA88

MA3KGX



TABLE 1b


MBRV8Q

MDPHJ2

MECYZH

MEK372

MFGD7A

MG7PYN

MGMXXQ

MGRHFR

UHPLC-DADMJU348

ML9PA8

MQEJV3

MTXP3C

MTYR4W

MURPC4

MWWZYC

MX922T

MXUNMW

N2NXFU

N3ETMG

Weight DeterminationN3GVN2

N62WCW

N6PK6X

N7X6PL

Handheld Raman SpectroscopyN8F6Y4

N9KQFN

NBB2H3

Handheld Raman SpectroscopyNBEFU4

ExtractionND7VKJ

NEC6AP

NGEW9P

NJHM6J

NL8XB4

NNEF9Y

NWFVPD

NZYAVY

P2RFVQ

P2YU4R



TABLE 1b


P4YKNE

P9M493

PAD4DZ

PAFDF4

PCXZXK

PDQYZP

PHWMAR

GC retention time matchPJYA4D

PMYGPA

PNAHB9

PPYWGK

PTTEER

PVVPFE

PWCQRG

PWHZNM

UPLCPYHAGC

Q22MUC

Q3UYFY

QB2BC9

QCL4FR

QF4BNR

QH7MKL

QHBFGF

QKDZ7U

QLKA4T

QNBGKA

QPT7KL

QQFR8H

QQR4EF

QWJ8P8

R4MVCC

Weight DeterminationR7NHQV

R9UX4T

RAUG6F

RCF4YN

RCKFKY

RCTDGH



TABLE 1b


RCX7EB

RGDM49

RGG3TF

RJ7G9G

Portable Raman SpectroscopyRJWJMR

RLH6WN

RPFRBJ

RWQRRN

T2BVWQ

T4LH7V

T7LQB7

TBEC69

LC/MSTFXNJJ

TGWLDD

TMHNXB

TMRAAC

TXRZTY

U2HY68

U4XGYJ

U8GMGE

UAU2EE

UAZCER

UDC6BX

UF487E

UL7GD8

UNJRNH

UNXEZ7

UQ82Z6

UR43VF

UT7U4A

UY3M44

UZD9DJ

V2PJA9

V9JB24

VAJ72M

VBAGTF

VBDCGY



TABLE 1b


VG6K2T

VGFLL7

VKMUC4

Did a base extractionVMN8DA

VMV6BT

VN49RX

VQ37RJ

VQ863Z

VQHQCF

VRKRHT

VRU6ZP

VUVFA7

VXYZRC

DART-QTOFW4L64D

UPLC-QTOFMSW4YYF8

W6TKBJ

W7Y7CC

W8JV2C

WA3YL3

WANCJF

WB7PEB

WB9YCW

WC3MUR

WDHHDJ

WEK2XR

Raman Spectroscopy & LC-MS / QTOF & GCMS/MS

WLGVXL

WLLQL6

WNUFWM

WPDQEZ

WPZUBF

WRWQ9V

WTXBNA

Handheld Raman Spectometer (TruNarc)

WU2HZA

WV6XW9

WWN6QB

WWPC6J



TABLE 1b


X26HGQ

X324EF

X3A8HE

X6DTMK

X9F44Y

XA7PHD

XAGNE8

XB344B

XDTLKG

XHG7UJ

XK4RV8

XKP6JK

Raman SpectroscopyXLH3RQ

XLJTXA

XN73YF

XUF3ND

XVNXUW

QTOF LCMSXVZTYB

Raman spectroscopy (TruNarc)XW2DKQ

XW4NB9

XX8V82

XXV4NK

Raman was used as a screening test

XYAKMJ

Y34KD6

YAMNL8

YF6TPM

YGH8DW

YHYWUL

YLG4A9

YLTH46

LC/MSYMHRXE

YTEKW8

YU3WXU

YU9YB8

YV2WHD

YZZ7TF

portable Raman spectroscopyZ2BT4K



TABLE 1b


Z98ZPU

ZEPU6X

LC-MS/MSZG83ZQ

DART/TOF-MS, weight determination

ZLNFVC

ZLQ3CQ

ZLY7YW

ZMZTZ9

ZNA3NZ

ZPNMFA

ZQT3NM

DART/TOFMSZRBBRA

ZYLYAJ

ZYXVD4

ZZKK3V

368 3258 36 5222457

527

Percent

Participants

GC/MSGCFTIR UV TLCCrystalColor

Response Summary

70% 1%49% 7% 99%5%11%1%

4

LC

2

Micro

0.4%

Total Participants:



Drug Analysis (Item 2)



Methylphenidate22NWVG

Methylphenidate23FFXX

Methylphenidate2CHQW8

Methylphenidate2D92NZ

Methylphenidate2EAA7R

Methylphenidate2EATV9

methylphenidate2F8K7Z

Methylphenidate2HRTGG

methylphenidate2J6YUQ

Methylphenidate (CII)2J8NZ9

Methylphenidate2LPXY8

methylphenidate2M37TM

Methylphenidate2NC3C7

Methylphenidate2NDFUD

Methylphenidate2NJZYP

Methylphenidate2PZNUV

Methylphenidate2U9YKC

Methylphenidate2Y4RUY

Methylphenidate32V2R8

METHYLPHENIDATE34PG4A

Methylphenidate379ZYK

Methylphenidate38DG8X

Methylphenidate38QPM7

methylphenidate38TZGA

Methylphenidate39DMF6

Methylphenidate - Schedule II3AFCHZ

Methylphenidate3AJ3LX

Methylphenidate3CTXU9

Methylphenidate3EFPDQ

methylphenidate3EHGJD

Methylphenidate3MF3V8

Methylphenidate3PNQC3

Methylphenidate3T8AEF

Methylphenidate3W7KAF

Methylphenidate3WM8Y3

Methylphenidate3X2DRY

methylphenidate3YJBEW

Methylphenidate42QWUA

Methylphenidate42RZDD

Methylphenidate4439N4

Methylphenidate48M7CU

Methylphenidate48NVJC

ritalin4A3BEQ

Contains Methylphenidate4A6EBT

Methylphenidate4C6BEN

Methylphenidate4CGZCF

Contains methylphenidate4CM8XB

Methylphenidate4EJJU4

The controlled substance detected preliminarily was Methylphenidate.

4G3TT3

Methylphenidate4GAJET

methylphenidate4H6HUX

Methylphenidate4HLUAH

Methylphenidate4HY7DA

methylphenidate4J6P6Q

Methylphenidate4P6XHK

Methylphenidate4PTB8B





Methylphenidate4WZA62

Methylphenidate.4X9YYR

Methylphenidate4XKLCM

Methylphenidate4XV8L4

methylphenidate638VW6

Methylphenidate63CAA6

Methylphenidate6A2LZL

Methylphenidate6BF7QB

Methylphenidate6BK2ET

Methylphenidate6BWUZV

Methylphenidate6D78VY

Methylphenidate6FW7CH

Methylphenidate6KD63P

methylphenidate6LD2RC

Methylphenidate6MT7M4

Methylphenidate6UPYLX

methylphenidate6WDT3Y

Methylphenidate6XTW7Q

Methylphenidate6ZYKZ2

No controlled substance detected/identified73AUWX

Methylphenidate74YDCB

Methylphenidate78AZQV

The controlled substance detected was Methylphenidate

798ARZ

Methylphenidate7C6YZK

Methylphenidate7DF93B

Methylphenidate7F7B8Y

Methylphenidate / Schedule II7H9UR8

Methylphenidate7JQRCJ

Methylphenidate7KFNPW

Methylphenidate7L92D4

Methylphenidate7LCE68

methylphenidate7MELNX

Methylphenidate7PDMAG

methylphenidate + lactose7PRZND

Methylphenidate7QU6FE

Methylphenidate7X2KRA

Methylphenidate7ZQXAR

Methylphenidate82Z2WG

Methylphenidate84PDFU

Methylphenidate89N2T3

Methylphenidate8AV9BF

Methylphenidate8BC2QR

Methylphenidate8BJJAV

Methylphenidate8DZBJB

Methylphenidate8ER66U

Methylphenidate8EVW7B

methylphenidate8G24P3

Methylphenidate (CII)8GJ7L4

Methylphenidate8L8CWE

methlyphenidate8N47ZV

Methylphenidate8NFYLW

Methylphenidate8PTGT9

Methylphenidate8QN3F9

Methylphenidate8RG9HK

Methylphenidate8TDM9J

Methylphenidate8U7W3F

Methylphenidate, Schedule II.8UL3H6

Methylphenidate8XL498





Methylphenidate8Y7JD3

Methylphenidate8YX4NA

Methylphenidate92VZG9

Methylphenidate93WFZ7

Methylphenidate96UGNB

methylphenidate96Z3P4

Methylphenidate9BH9QX

Methylphenidate9DCCYH

Methylphenidate. Preliminary Result. The substance cannot be confirmed due to lack of reference material.

9GPP9Y

methylphenidate9GVH7R

Methylphenidate HCl9L72F2

methylphenidate9Q2BMZ

Methylphenidate9QVGR2

methylphenidate9T2VN8

Methylphenidate9VBHWQ

methylphenidate9VV2CJ

Contains methylphenidate9WP244

methylphenidate9ZFW8P

MethylphenidateA2GH2E

MethylphenidateA2Z298

MethylphenidateA3EQAY

methylphenidateA46PQH

METHYLPHENIDATEA6ZD68

MethylphenidateA7FLEL

methylphenidateA9GZGR

MethylphenidateAAPJFH

MethylphenidateAB3L8T

MethylphenidateACVYUZ

MethylphenidateAD7U78

methylphenidateAT9QWQ

MethylphenidateAUBBGY

MethylphenidateAVBKWG

methylphenidateAZE79L

MethylphenidateB28CAX

methylphenidateB4XM2Q

MethylphenidateBAY2HL

methylphenidate (CII)BBJXPY

methylphenidateBCEHCX

Methylphenidate (II)BCVWF2

methylphenidateBEQ4QR

MethylphenidateBFWXNB

MethylphenidateBHVR83

MethylphenidateBJD9VM

MethylphenidateBJUGL4

MethylphenidateBMVGUM

Methylphenidate (and lactose)BNKCBJ

MethylphenidateBWEH6A

methylphenidateBZEUYP

MethylphenidateC29CK4

MethylphenidateC6UZDG

METHYLPHENIDATEC7VKPN

methylphenidateC9FQRR

MethylphenidateCAFJAY

METHYLPHENIDATECC37GR

MethylphenidateCDGFRD

MethylphenidateCE3CTY

MethylphenidateCF9URU





methylphenidateCFPXEU

MethylphenidateCGXUKE

No controlled substance detected/identifiedCJRH4A

Methylphenidate - CDS IICMUC7K

MethylphenidateCQ2VVD

methylphenidateCRMW9L

MethylphenidateCUTCLJ

MethylphenidateCVJKM9

MethylphenidateCY3TV9

MethylphenidateCYTFTY

Methylphenidate, schedule II controlled substance

CZRPX2

MethylphenidateD4LYAM

MethylphenidateD63ZNB

MethylphenidateD763UD

MethylphenidateD7GZQH

MethylphenidateDALLLV

MethylphenidateDARLB4

MethylphenidateDERDFZ

MethylphenidateDF2QDP

MethylphenidateDK2JK8

MethylphenidateDLTXVX

Methylphenidate IIDNWCGM

MethylphenidateDQ6ECU

methylphenidateDRV8Z6

MethylphenidateDUXY3Q

MethylphenidateDVKRAZ

MethylphenidateDW9UUA

methylphenidateDY6N7R

MethylphenidateDZPCU7

MethylphenidateDZU9HP

MethylphenidateDZWPV2

MethylphenidateE7RLZY

MethylphenidateE8KJ96

methylphenidateE9KV8Z

MethylphenidateEB2VYU

MethylphenidateEDNEZR

MethylphenidateEE2436

METHYLPHENIDATEEHK6E4

MethylphenidateEMXT99

MethylphenidateEUY667

MethylphenidateEXDP6Z

Methylphenidate is listed in [Legislation].EZ4ZWT

MethylphenidateF2ZD9H

MethylphenidateF3NBG4

Methylphenidate, LactoseF4HXWT

MethylphenidateF7RQMR

MethylphenidateF9TJTJ

MethylphenidateFAA6E2

Methylphenidate HydrochlorideFAMTMF

Methylphenidate (Preliminary result). The substance cannot be confirmed due to lack of reference material.

FEZULR

methylphenidate and lactoseFF2QNU

MethylphenidateFGX9ZG

MethylphenidateFN98ZF

methylphenidateFNLU32

MethylphenidateFPHCD4

Methylphenidate (C-II)FQ3EGC

MethylphenidateFR6UFW





MethylphenidateFRNCEG

MethylphenidateFVAG78

MethylphenidateFW97QA

MethylphenidateFZYEZH

MethylphenidateG29BVT

MethylphenidateG3BFPF

MethylphenidateG3P274

MethylphenidateG4462V

MethylphenidateG72CZT

MethylphenidateG84ZKD

MethylphenidateG93M8N

Item #01.002 contains Methylphenidate, a schedule II controlled non-narcotic substance.

GD849Q

MethylphenidateGEZG8G

MethylphenidateGFWR8Q

Methylphenidate- confirmed as Class B controlled drug under [Legislation].

GJ4W8K

MethylphenidateGKU7UF

Methylphenidate CDS IIGLKGMU

Methylphenidate hydrochlorideGN2ACW

MethylphenidateGRJTWR

MethylphenidateGT79AF

MethylphenidateGTJHQN

MethylphenidateGTZ49J

MethylphenidateGWR42E

MethylphenidateGX4YM7

MethylphenidateH33BGB

MethylphenidateH4JX7X

Methylphenidate, CIIH6G8N9

Methylphenidate and N-Isopropylbenzylamine(not controlled)

H82CRB

MethylphenidateH98RVH

MethylphenidateHAB7WC

MethylphenidateHC4Y99

methylphenidateHE9PZV

MethylphenidateHF9332

methylphenidateHFCPGU

methylphenidateHGJRJR

MethylphenidateHJNYPK

MethylphenidateHJPD9D

Contains MethylphenidateHM9JGM

methylphenidate, a schedule II CDSHPDXCT

Methylphenidate and lactoseHQ6HZ8

methylphenidateHQQMF7

MethylphenidateHUMQY8

methylphenidateHV4U3Y

MethylphenidateHYEZ96

MethylphenidateHZTHAP

Methylphenidate foundJ64TZY

methylphenidateJ73MP2

MethylphenidateJ9MXMZ

MethylphenidateJAJU9U

methylphenidateJARGEG

MethylphenidateJBP7YJ

MethylphenidateJEA3UN

MethylphenidateJF3Z2V

MethylphenidateJJEM6T

MethylphenidateJKGK3P

MethylphenidateJNGVXP





MethylphenidateJPK8EK

Methylphenidate,CII.JW7638

MethylphenidateJYBYTP

methylphenidateJZNBRU

MethylphenidateK382YC

Methylphenidate (Schedule II)K3CWNV

MethylphenidateK4TWZX

methylphenidateK6QZBL

MethylphenidateK8678N

MethylphenidateKDWRH3

MethylphenidateKFT83E

No controlled substance detected/identified; Lactose

KGAA4L

Contains MethylphenidateKGP6MD

methylphenidateKK4B3E

MethylphenidateKLDBAG

MethylphenidateKN87X4

MethylphenidateKPTU2Y

MethylphenidateKQ4VNX

MethylphenidateKRH8JG

MethylphenidateKT3THR

Methylphenidate identifiedKT7Y9R

Methylphenidate / Schedule IIKUB2NQ

MethylphenidateKWMR4L

methylphenidateKWRK4Z

MethylphenidateKZLBFD

No controlled substance detected/identifiedL6T6AV

MethylphenidateL9L79N

MethylphenidateLAWY3D

Methylphenidate hydrochlorideLB28QH

MethylphenidateLC9PAL

MethylphenidateLD63AL

MethylphenidateLDUGZ6

MethylphenidateLEHGXU

MethylphenidateLEYM68

MethylphenidateLFYE3K

Methylphenidate (isomer form not determined)

LJUH3Y

MethylphenidateLME8MC

Methylphenidate (isomer form not determined)

LNTUYY

MethylphenidateLQT4U9

MethylphenidateLRAKHT

methylphenidateLUF68E

Methylphenidate (Schedule II)LXFCQQ

Methylphenidate was detected.LZ7DWE

MethylphenidateM8NA88

MethylphenidateMA3KGX

MethylphenidateMBRV8Q

MethylphenidateMDPHJ2

The controlled substance detected was Methylphenidate

MECYZH

methylphenidateMEK372

MethylphenidateMFGD7A

MethylphenidateMG7PYN

methylphenidateMGMXXQ

methylphenidateMGRHFR

MethylphenidateMJU348

The powder contained methylphenidateML9PA8

MethylphenidateMQEJV3

MethylphenidateMTXP3C





MethylphenidateMTYR4W

methylphenidateMURPC4

MethylphenidateMWWZYC

MethylphenidateMX922T

methylphenidateMXUNMW

MethylphenidateN2NXFU

MethylphenidateN3ETMG

MethylphenidateN3GVN2

Methylphenidate, Schedule II.N62WCW

methylphenidateN6PK6X

MethylphenidateN7X6PL

Methylphenidate HydrochlorideN8F6Y4

MethylphenidateN9KQFN

MethylphenidateNBB2H3

Methylphenidate HydrochlorideNBEFU4

MethylphenidateND7VKJ

MethylphenidateNEC6AP

Methylphenidate / Schedule IINGEW9P

Methylphenidate identifiedNJHM6J

MethylphenidateNL8XB4

MethylphenidateNNEF9Y

MethylphenidateNWFVPD

methylphenidateNZYAVY

MethylphenidateP2RFVQ

MethylphenidateP2YU4R

MethylphenidateP4YKNE

Threo-Propylphenidate (presumptively identified)

P9M493

MethylphenidatePAD4DZ

MethylphenidatePAFDF4

MethylphenidatePCXZXK

MethylphenidatePDQYZP

MethylphenidatePHWMAR

MethylphenidatePJYA4D

MethylphenidatePMYGPA

MethylphenidatePNAHB9

MethylphenidatePPYWGK

MethylphenidatePTTEER

MethylphenidatePVVPFE

MethylphenidatePWCQRG

Methylphenidate.PWHZNM

Contains MethylphenidatePYHAGC

MethylphenidateQ22MUC

MethylphenidateQ3UYFY

MethylphenidateQB2BC9

MethylphenidateQCL4FR

MethylphenidateQF4BNR

MethylphenidateQH7MKL

MethylphenidateQHBFGF

METHYLPHENIDATEQKDZ7U

methylphenidate, LactoseQLKA4T

methylphenidateQNBGKA

MethylphenidateQPT7KL

methylphenidateQQFR8H

MethylphenidateQQR4EF

MethylphenidateQWJ8P8

MethylphenidateR4MVCC

MethylphenidateR7NHQV

MethylphenidateR9UX4T





MethylphenidateRAUG6F

MethylphenidateRCF4YN

MethylphenidateRCKFKY

MethylphenidateRCTDGH

MethylphenidateRCX7EB

MethylphenidateRGDM49

MethylphenidateRGG3TF

Methylphenidate (C-II) foundRJ7G9G

MethylphenidateRJWJMR

MethylphenidateRLH6WN

MethylphenidateRPFRBJ

MethylphenidateRWQRRN

methylphenidate, a controlled substance(schedule II) was identified.

T2BVWQ

methylphenidateT4LH7V

methylphenidateT7LQB7

MethylphenidateTBEC69

MethylphenidateTFXNJJ

METHYLPHENIDATETGWLDD

Methylphenidate II CDSTMHNXB

Item 2 contains methylphenidate.TMRAAC

MethylphenidateTXRZTY

MethylphenidateU2HY68

MethylphenidateU4XGYJ

MethylphenidateU8GMGE

MethylphenidateUAU2EE

MethylphenidateUAZCER

It contains methylphenidate.UDC6BX

MethylphenidateUF487E

methylphenidateUL7GD8

MethylphenidateUNJRNH

methylphenidateUNXEZ7

methylphenidate, salt form not determinedUQ82Z6

MethylphenidateUR43VF

methylphenidateUT7U4A

MethylphenidateUY3M44

MethylphenidateUZD9DJ

methylphenidateV2PJA9

MethylphenidateV9JB24

MethylphenidateVAJ72M

MethylphenidateVBAGTF

MethylphenidateVBDCGY

methylphenidateVG6K2T

MethylphenidateVGFLL7

MethylphenidateVKMUC4

MethylphenidateVMN8DA

MethylphenidateVMV6BT

MethylphenidateVN49RX

MethylphenidateVQ37RJ

MethylphenidateVQ863Z

MethylphenidateVQHQCF

MethylphenidateVRKRHT

MethylphenidateVRU6ZP

MethylphenidateVUVFA7

MethylphenidateVXYZRC

Methylphenidate HClW4L64D

MethylphenidateW4YYF8

MethylphenidateW6TKBJ

MethylphenidateW7Y7CC





MethylphenidateW8JV2C

methylphenidateWA3YL3

MethylphenidateWANCJF

methylphenidateWB7PEB

Methylphenidate/DexmethylphenidateWB9YCW

MethylphenidateWC3MUR

MethylphenidateWDHHDJ

MethylphenidateWEK2XR

MethylphenidateWLGVXL

MethylphenidateWLLQL6

MethylphenidateWNUFWM

methyl (alpha)-phenyl-2-piperidine acetate OR METHYLPHENIDATE

WPDQEZ

MethylphenidateWPZUBF

MethylphenidateWRWQ9V

Methylphenidate (Listed in [Legislation])WTXBNA

methylphenidateWU2HZA

MethylphenidateWV6XW9

methylphenidateWWN6QB

MethylphenidateWWPC6J

MethylphenidateX26HGQ

methylphenidateX324EF

MethylphenidateX3A8HE

methylphenidateX6DTMK

methylphenidateX9F44Y

MethylphenidateXA7PHD

MethylpenidateXAGNE8

methylphenidateXB344B

MethylphenidateXDTLKG

MethylphenidateXHG7UJ

MethylphenidateXK4RV8

methylphenidateXKP6JK

MethylphenidateXLH3RQ

MethylphenidateXLJTXA

methylphenidateXN73YF

Methylphenidate (Schedule II) was identified in Exhibit 2. Scheduling information reported is based on the US Code of Federal Regulations, Title 21, Section 1308.

XUF3ND

MethylphenidateXVNXUW

MethylphenidateXVZTYB

methylphenidateXW2DKQ

MethylphenidateXW4NB9

item 2 contains Methylphenidate(Schedule II) and lactose

XX8V82

MethylphenidateXXV4NK

methylphenidateXYAKMJ

MethylphenidateY34KD6

MethylphenidateYAMNL8

MethylphenidateYF6TPM

Methylphenidate (Ritalin)YGH8DW

MethylphenidateYHYWUL

methylphenidateYLG4A9

MethylphenidateYLTH46

MethylphenidateYMHRXE

MethylphenidateYTEKW8

MethylphenidateYU3WXU

MethylphenidateYU9YB8

MethylphenidateYV2WHD

METHYLPHENIDATEYZZ7TF

MethylphenidateZ2BT4K





methylphenidateZ98ZPU

MethylphenidateZEPU6X

MethylphenidateZG83ZQ

Methylphenidate; salt form not determined.ZLNFVC

methylphenidateZLQ3CQ

MethylphenidateZLY7YW

MethylphenidateZMZTZ9

Laboratory analysis determined the presence of Methylphenidate, which is a Schedule II controlled substance under US CFR Title 21, Part 1308.

ZNA3NZ

Methylphenidate (CII)ZPNMFA

MethylphenidateZQT3NM

MethylphenidateZRBBRA

MethylphenidateZYLYAJ

methylphenidateZYXVD4

MethylphenidateZZKK3V

Participants: 527

Response Summary - Item 2

Methylphenidate:

No Controlled substance(s) detected/identified: 4

522

Other: 1



Examination Methods (Item 2)TABLE 2b

Color UVFTIR GC/MSGC OtherLC MicroCrystal TLCWebCode

22NWVG

23FFXX

2CHQW8

2D92NZ

2EAA7R

2EATV9

2F8K7Z

2HRTGG

2J6YUQ

2J8NZ9

2LPXY8

weight2M37TM

GCIR2NC3C7

2NDFUD

2NJZYP

NMR, Handheld Raman2PZNUV

2U9YKC

2Y4RUY

GC/IR32V2R8

34PG4A

weight determination379ZYK

TruNarc38DG8X

38QPM7

38TZGA

39DMF6

3AFCHZ

3AJ3LX

QTOF LCMS3CTXU9

LC/MS3EFPDQ

3EHGJD

3MF3V8

Handheld Thermo Scientific TruNarc Raman Spectroscopy

3PNQC3

3T8AEF

3W7KAF

3WM8Y3



TABLE 2b


Retention time confirmation3X2DRY

3YJBEW

42QWUA

42RZDD

GC retention time confirmation4439N4

48M7CU

48NVJC

4A3BEQ

4A6EBT

4C6BEN

4CGZCF

4CM8XB

4EJJU4

Screening4G3TT3

FTIR-ATR4GAJET

4H6HUX

4HLUAH

4HY7DA

4J6P6Q

4P6XHK

4PTB8B

4WZA62

4X9YYR

GC/IR4XKLCM

4XV8L4

638VW6

LC-TOF63CAA6

6A2LZL

6BF7QB

6BK2ET

6BWUZV

6D78VY

6FW7CH

6KD63P

6LD2RC

6MT7M4

LC/MS6UPYLX



TABLE 2b


LC/MS/MS6WDT3Y

6XTW7Q

6ZYKZ2

73AUWX

74YDCB

78AZQV

798ARZ

7C6YZK

DART-TOF7DF93B

7F7B8Y

7H9UR8

7JQRCJ

7KFNPW

Raman spectroscopy7L92D4

7LCE68

7MELNX

7PDMAG

7PRZND

7QU6FE

7X2KRA

7ZQXAR

82Z2WG

84PDFU

89N2T3

Weight determination8AV9BF

FTIR with ATR accessory8BC2QR

8BJJAV

8DZBJB

8ER66U

8EVW7B

8G24P3

8GJ7L4

8L8CWE

8N47ZV

8NFYLW

8PTGT9

8QN3F9



TABLE 2b


GC-IR8RG9HK

8TDM9J

8U7W3F

8UL3H6

DART-TOF8XL498

8Y7JD3

8YX4NA

GCIR92VZG9

93WFZ7

96UGNB

96Z3P4

9BH9QX

9DCCYH

9GPP9Y

9GVH7R

9L72F2

9Q2BMZ

9QVGR2

9T2VN8

9VBHWQ

9VV2CJ

9WP244

TruNarc9ZFW8P

GC/IRA2GH2E

A2Z298

Retention TimeA3EQAY

A46PQH

A6ZD68

A7FLEL

A9GZGR

DART-MSAAPJFH

AB3L8T

ACVYUZ

AD7U78

AT9QWQ

AUBBGY

AVBKWG



TABLE 2b


LC-MS/MSAZE79L

GCIRB28CAX

LCMS mass accuracy and MS2B4XM2Q

NMR, LCMSBAY2HL

BBJXPY

BCEHCX

BCVWF2

BEQ4QR

BFWXNB

BHVR83

MarquisBJD9VM

BJUGL4

BMVGUM

FT-Raman, LC-MSBNKCBJ

BWEH6A

BZEUYP

C29CK4

C6UZDG

C7VKPN

C9FQRR

CAFJAY

CC37GR

RamanCDGFRD

Electronic BalanceCE3CTY

CF9URU

CFPXEU

RamanCGXUKE

CJRH4A

CMUC7K

CQ2VVD

CRMW9L

CUTCLJ

Portable Raman SpectroscopyCVJKM9

CY3TV9

CYTFTY

CZRPX2

D4LYAM



TABLE 2b


D63ZNB

D763UD

GC/IRD7GZQH

DALLLV

DARLB4

DERDFZ

DF2QDP

DK2JK8

DLTXVX

DNWCGM

DQ6ECU

DRV8Z6

Two separate samplings in two GC/MS instruments used.

DUXY3Q

DVKRAZ

DW9UUA

DY6N7R

DZPCU7

DZU9HP

DZWPV2

E7RLZY

E8KJ96

E9KV8Z

EB2VYU

EDNEZR

EE2436

EHK6E4

EMXT99

EUY667

EXDP6Z

EZ4ZWT

F2ZD9H

F3NBG4

F4HXWT

GC-FIDF7RQMR

F9TJTJ

FAA6E2



TABLE 2b


FAMTMF

FEZULR

FF2QNU

FGX9ZG

GC/IRDFN98ZF

FNLU32

GC-IRFPHCD4

FQ3EGC

FR6UFW

FRNCEG

FVAG78

FW97QA

Retention time comparisonFZYEZH

G29BVT

G3BFPF

G3P274

G4462V

G72CZT

G84ZKD

G93M8N

GD849Q

GEZG8G

Retention TimeGFWR8Q

GJ4W8K

GKU7UF

GLKGMU

Raman spectroscopy, Ion chromatography

GN2ACW

GCIRGRJTWR

GT79AF

GTJHQN

GTZ49J

GWR42E

GX4YM7

H33BGB

H4JX7X

H6G8N9



TABLE 2b


H82CRB

H98RVH

LC=LC-QTOF-MSHAB7WC

HC4Y99

HE9PZV

HF9332

LCMSHFCPGU

HGJRJR

HJNYPK

GC/IRHJPD9D

HM9JGM

HPDXCT

RamanHQ6HZ8

HQQMF7

HUMQY8

HV4U3Y

HYEZ96

GCIRHZTHAP

J64TZY

J73MP2

J9MXMZ

JAJU9U

LCMSJARGEG

JBP7YJ

JEA3UN

JF3Z2V

JJEM6T

JKGK3P

JNGVXP

JPK8EK

JW7638

JYBYTP

JZNBRU

K382YC

DART-TOFK3CWNV

K4TWZX

K6QZBL



TABLE 2b


K8678N

KDWRH3

TruNarc Handheld Raman Spectrometer

KFT83E

RamanKGAA4L

KGP6MD

KK4B3E

GC-IRDKLDBAG

Weight DeterminationKN87X4

KPTU2Y

KQ4VNX

KRH8JG

KT3THR

KT7Y9R

KUB2NQ

KWMR4L

KWRK4Z

KZLBFD

L6T6AV

L9L79N

LAWY3D

LB28QH

LC9PAL

LD63AL

LDUGZ6

FTIR-ATRLEHGXU

LEYM68

LFYE3K

GC/FTIRLJUH3Y

FTIR with ATRLME8MC

GC/IRLNTUYY

Accurate Mass - Orbitrap Mass Spectrometry

LQT4U9

LRAKHT

LUF68E

LCMSLXFCQQ

Weight determinationLZ7DWE

M8NA88



TABLE 2b


LactoseMA3KGX

MBRV8Q

MDPHJ2

MECYZH

MEK372

MFGD7A

MG7PYN

MGMXXQ

MGRHFR

UHPLC-DADMJU348

ML9PA8

MQEJV3

MTXP3C

MTYR4W

MURPC4

MWWZYC

MX922T

MXUNMW

N2NXFU

N3ETMG

Weight DeterminationN3GVN2

N62WCW

N6PK6X

N7X6PL

Handheld Raman SpectroscopyN8F6Y4

N9KQFN

NBB2H3

Handheld Raman SpectroscopyNBEFU4

GC Retention TimeND7VKJ

NEC6AP

NGEW9P

NJHM6J

NL8XB4

NNEF9Y

NWFVPD

NZYAVY

P2RFVQ



TABLE 2b


P2YU4R

P4YKNE

P9M493

PAD4DZ

PAFDF4

PCXZXK

PDQYZP

PHWMAR

GC retention time matchPJYA4D

PMYGPA

PNAHB9

PPYWGK

PTTEER

PVVPFE

PWCQRG

PWHZNM

UPLCPYHAGC

Q22MUC

Q3UYFY

QB2BC9

QCL4FR

QF4BNR

QH7MKL

QHBFGF

QKDZ7U

QLKA4T

QNBGKA

QPT7KL

QQFR8H

QQR4EF

QWJ8P8

R4MVCC

Weight DeterminationR7NHQV

R9UX4T

GC Retention Time confirmation with Methylphenidate standard

RAUG6F

RCF4YN



TABLE 2b


RCKFKY

RCTDGH

RCX7EB

Confirmation with retention time using reference standard.

RGDM49

RGG3TF

RJ7G9G

Portable Raman SpectroscopyRJWJMR

RLH6WN

RPFRBJ

RWQRRN

T2BVWQ

T4LH7V

T7LQB7

TBEC69

LC/MSTFXNJJ

TGWLDD

TMHNXB

TMRAAC

TXRZTY

U2HY68

U4XGYJ

U8GMGE

UAU2EE

UAZCER

UDC6BX

UF487E

LC/MS (Orbitrap)UL7GD8

UNJRNH

UNXEZ7

UQ82Z6

UR43VF

UT7U4A

UY3M44

UZD9DJ

V2PJA9

V9JB24



TABLE 2b


VAJ72M

VBAGTF

VBDCGY

VG6K2T

VGFLL7

VKMUC4

VMN8DA

VMV6BT

VN49RX

VQ37RJ

VQ863Z

VQHQCF

VRKRHT

VRU6ZP

VUVFA7

VXYZRC

DART-QTOFW4L64D

UPLC-QTOFMSW4YYF8

W6TKBJ

W7Y7CC

W8JV2C

WA3YL3

WANCJF

WB7PEB

WB9YCW

WC3MUR

WDHHDJ

WEK2XR

Raman Spectroscopy & LC-MS / QTOF & GC-MS/MS

WLGVXL

Retention TimeWLLQL6

WNUFWM

WPDQEZ

WPZUBF

WRWQ9V

FTIR RamanWTXBNA

Handheld Raman Spectrometer (TruNarc)

WU2HZA



TABLE 2b


WV6XW9

WWN6QB

WWPC6J

X26HGQ

X324EF

X3A8HE

X6DTMK

X9F44Y

XA7PHD

XAGNE8

XB344B

XDTLKG

XHG7UJ

XK4RV8

XKP6JK

Raman SpecroscopyXLH3RQ

XLJTXA

XN73YF

XUF3ND

XVNXUW

QTOF LCMSXVZTYB

Raman spectroscopy (TruNarc)XW2DKQ

XW4NB9

XX8V82

XXV4NK

Raman was used as a screening testXYAKMJ

Y34KD6

YAMNL8

YF6TPM

YGH8DW

YHYWUL

YLG4A9

YLTH46

LC/MSYMHRXE

YTEKW8

YU3WXU

YU9YB8



TABLE 2b


YV2WHD

YZZ7TF

portable Raman spectroscopyZ2BT4K

Z98ZPU

ZEPU6X

ZG83ZQ

DART/TOF-MS, weight determination

ZLNFVC

ZLQ3CQ

GC-IRZLY7YW

ZMZTZ9

RamanZNA3NZ

ZPNMFA

ZQT3NM

DART/TOFMSZRBBRA

ZYLYAJ

ZYXVD4

ZZKK3V

368 4242 74 5232575

527

Percent

GC/MSGCFTIR UV TLCCrystalColor

Response Summary

70% 1%46% 14% 99%5%14%1%

7

LC Micro

2

0.4%

Total Participants:

Participants



Additional CommentsTABLE 3

Additional CommentsWebCode

First item found to contain Acetaminophen.2NDFUD

Acetaminophen was detected in Item 1. Methylphenidate and Lactose were detected in Item 2.2PZNUV

Item 1 contains acetaminophen; Item 2 also contains possible lactose.2U9YKC

ITEM 1 POWDER CONTAINED ACETAMINOPHEN.34PG4A

The presence of acetaminophen was indicated in Item 1.38QPM7

Item 1 found to contain Acetaminophen.39DMF6

1 a ) Acetaminophen was detected in itme 1.3EHGJD

Acetaminophen was identified in Item 1. Lactose was identified in Item 2.3MF3V8

Acetaminophen identified in Item 1.3WM8Y3

Acetaminophen was confirmed in Item 1.4CGZCF

Item 1 contains acetaminophen4CM8XB

For the Item 2, the substance was reported as preliminary, because there is no reference material available to report a confirmed result of the substance mentioned above.

4G3TT3

Analysis of item 1 indicated the presence of Acetaminophen. Analysis of item 2 also indicated the presence of Lactose.

4P6XHK

Item 1 contains Acetaminophen. Item 2 also contains Lactose.4PTB8B

Item 1 : Acetaminophen.4X9YYR

Acetaminophen identified in Item #1.638VW6

Item 1 is Acetaminophen6BWUZV

Item 1 contained acetaminophen. Item 2 contained acetaminophen.6D78VY

Acetaminophen identified in Item #16FW7CH

Item 1 is contain Acetaminophen. Item 2 is contain Methylphenidate which listed on [Legislation].6KD63P

1.1) Acetaminophen present.6LD2RC

Acetaminophen was indicated in the powder from item 1.6MT7M4

Acetaminophen was detected in Item 1 using GC-MS confirmation6ZYKZ2

Item 1 found to contain Acetaminophen. Item 2 found to contain Lactose and Methylphenidate73AUWX

Item-1: The No controlled substance detected was Acetaminophen (paracetamol). Item -2: Methylphenidate is not a drug included in the general scrutiny developed in the Analytical Chemistry Section.

798ARZ

Lab does not test for salts or diluents7JQRCJ

Acetaminophen found in item 17KFNPW

Acetaminophen was confirmed in item 1.7L92D4

In item 1 was detected Acetaminophen. In item 2 was detected Lactose.7LCE68

Lab does not test for salts or diluents.7PDMAG

Item 1 was found to contain Acetaminophen.7QU6FE

Paracetamol detected in test item 1.7ZQXAR

Acetaminophen for Item 18NFYLW



TABLE 3Additional CommentsWebCode

Item 1 was identified as acetaminophen-not a controlled substance.8QN3F9

Identified Acetaminophen in Item #1 (not a controlled susbtance). Presence of Lactose indicated in Item #2 (not a controlled substance).

8TDM9J

Acetaminophen was detected in item 1.8UL3H6

Item 1 contains acetaminophen.8Y7JD3

Sample No. 1 contains acetaminophen. Analysis sample No. 2 contains methylphenidate and lactose.96UGNB

Acetaminophen identified in item 196Z3P4

Item 1 contains Acetaminophen.9GVH7R

Examinations of the white powder from item 1 indicated the presence of Acetaminophen.9L72F2

Acetaminophen was confirmed in Item #1.9QVGR2

Item1- Acetaminophen9T2VN8

Item one contains acetaminophen which is not a controlled substance. Item two contains methylphenidate which is a controlled substance.

9WP244

Analysis of Item 1 found to contain Acetaminophen. Analysis of Item 2 also indicated the presence of Lactose.

AB3L8T

While not controlled Item #1 was identified as acetaminophen.BAY2HL

Item 1 contains Acetaminophen / No ID CDSBCVWF2

Upon analysis, i found Item 1 to be Acetominophen while Item 2 to be Methylphenidate which was listed in First Schedule, [Legislation].

BHVR83

Item 1 was identified as AcetaminophenBMVGUM

Item 1 contains Acetaminophen which is not controlled. Item 2 Methylphenidate. It also has an unknown peak; not identified nor further pursued. This was only present in the base to chloroform extract and not in the methanol extract.

BWEH6A

Item 1 contained acetaminophen.BZEUYP

IN THE ITEM #2 COMPARED WITH LIBRARY OF THE INSTRUMENTS (GC/MS) RESULT METHYLPHENIDATE BUT CAN NOT BE CONFIRMED BECAUSE DO NOT HAVE A REFERENCE MATERIAL AVAILABLE.

CC37GR

Item #1 Acetaminophen was indicated.CDGFRD

Item 1 was identified as containing AcetaminophenCVJKM9

Item 1 was found to contain Acetaminophen, a non-controlled substance.CY3TV9

Acetaminophen was confirmed in Item 1.CYTFTY

Item 1 contained acetaminophen. Item 2 also contained lactose.DF2QDP

Acetaminophen was confirmed for Item 1.DK2JK8

Examinations of Item 1 identified Acetaminophen.DLTXVX

Item 1: Screening tests indicate the presence of AcetaminophenDUXY3Q

Acetaminophen was detected in Item 1.DVKRAZ

Item 1: acetaminophen was indicated but not confirmedE9KV8Z

The item 1 contains Acetaminophen, which is not a controlled substance. The item 2 contains Methylphenidate, which is controlled by US legislation.

EE2436




Item 1 was determined to be acetaminophen. Item 2 was found to be a mixture of methylphenidate and sugar (e.g. lactose). A base extraction was performed on Item 2 for FT-IR analysis, therefor no salt form was determined.

EMXT99

Item 1 was identified as Acetaminophen.F9TJTJ

Item 1 : AcetaminophenFAMTMF

Acetaminophen was detected in item 1.FN98ZF

Item 1 determined to contain acetaminophen.FNLU32

Item 1 contains paracetamol. Item 2 also contains lactose.FPHCD4

Acetaminophen was detected in Item #1.FRNCEG

Acetaminophen was indicated in item 1FW97QA

Item 1: Acetaminophen detectedFZYEZH

Item 1: Identified Acetaminophen. Item 2: I addition to identifying Methylphenidate I also identified Lactose.

G29BVT

Acetaminophen identified in item 1.G4462V

Item 1- Paracetamol was detected which is not controlled under the provisions of [Legislation]. Item 2- Also contained Lactose, which is not controlled under the provisions of [Legislation].

GJ4W8K

Item 1: acetaminophen. Item 2: lactose.GN2ACW

Item 1 was identified as Acetaminophen.GTZ49J

Acetaminophen is detected in Item 1(one)GWR42E

Acetaminophen was observed in Item 1.H98RVH

Item 1 was found to contain Acetaminophen, a non-controlled substance. Item 2 was found to contain Methylphenidate, a controlled substance, and indicated the presence of Lactose, a non-controlled substance.

HF9332

Item 1 was found to contain acetaminophen. Item 2 also contains lactose.HJNYPK

Acetaminophen identified in Item 1.JF3Z2V

Item 1 contained Acetaminophen. Item 2 also contained Lactose.JPK8EK

item 1 indicated presence of acetaminophen, wasn't confirmed due to lack of known standardK6QZBL

Item 1 Acetaminophen detected. Item 2 Lactose detectedKGAA4L

Item 1: Did a base/chloroform extraction after running initial sample.KRH8JG

Acetaminophen was identified in Item 1. Lactose was detected in Item 2 via FTIR.KZLBFD

From GCMS results in Item 2, methylphenidate was indicated. However in the absence of a certified reference material we are unable to confirm. This compound is not controlled under [Association], but would be controlled under [Legislation] as a prescription only medication.

L6T6AV

Item 1 was found to contain acetaminophen. Item 2 was also found to contain a substance consistent with lactose.

LB28QH

No controlled or related substances identified. Acetaminophen (non-controlled) was identified in Exhibit 1. Methylphenidate (Schedule II) was identified in Exhibit 2.

LXFCQQ

Item 1 was found to contain Acetaminophen, which is not a controlled substance.MDPHJ2

Item-1: The No controlled substance detected was Acetaminophen (paracetamol). Item -2: Methylphenidate is not a drug included in the general scrutiny developed in the Analytical Chemistry Section.

MECYZH




item 1 - acetaminophenMGMXXQ

Item 1 contained paracetamol (acetaminophen). Item 2 contained 1.8% of methylphenidate and lactose.MJU348

The substance identified in Item 1 was Acetaminophen. This set of examinations should also go toward credit for General Chemical Testing.

MTXP3C

Item 1 was identified to contain acetaminophenMWWZYC

Item 1 contains Acetaminophen.N3ETMG

Item 1 was found to contain paracetamol. Item 2 was found to contain methylphenidate. Paracetamol is not a Controlled Drug listed in the [Legislation]. Methylphenidate is a Class B Controlled Drug listed in the [Legislation].

N8F6Y4

Acetaminophen was also confirmed in Item 1.N9KQFN

Item # 1) acetaminophen shown with FTIR, no STD run on GC/MS therefore could not say detected. Item # 2) lactose may also be present in this item.

NBB2H3

Item 1 was found to contain paracetamol. Item 2 was found to contain methylphenidate. Paracetamol is not a Controlled Drug listed in the [Legislation]. Methylphenidate is a Class B Controlled Drug listed in the [Legislation].

NBEFU4

ITEM 1: Acetaminophen was identified in the representative sample of the apparent fine white powder found inside the folded wax paper bag labeled "Test No. 19-502; Item 1".

P9M493

Item 1 - No control substance detected and from analysis it was found to be Acetaminophen. Item 2- Methylphenidate is controlled under [Legislation] and lactose was detected as diluent.

PAD4DZ

Acetaminophen was also confirmed in Item 1.PCXZXK

Item 2: Methylphenidate is a controlled substance under [Legislation]PMYGPA

Acetaminophen was identified in item 1PVVPFE

I confirmed that item 1 contained acetaminophen.QB2BC9

Contains: Item 1: AcetaminophenQH7MKL

Item #1: Identified in the analysis was acetaminophen (noncontrolled).QHBFGF

Item 1: Acetaminophen detected by GCMSQPT7KL

Sample 1 was determined to be a non-controlled substance, confirmed to be Acetaminophen.QQR4EF

Currently no functioning IR to perform another confirmatory test. For item 1, acetaminophen indicated. Also did base CHCl3 extraction after MeOH extraction. Did not run base CHCl3 GC vial on GC due to instrument not functioning at time of analysis.

R4MVCC

Acetaminophen was identified in item 1. Lactose was also indicated in item 2.RCKFKY

Item 1 contains AcetaminophenRCX7EB

Item 1 confirmed to contain acetaminophen.RJWJMR

Item 1 contains acetaminophen.RPFRBJ

Ex. 1 was found to contain Acetaminophen, an over-the-counter medication.T2BVWQ

Item 1 contains acetaminophen.TMRAAC

Item 1 was identified as Acetaminophen.TXRZTY

Item 1 was found to be AcetaminophenU4XGYJ

Acetaminophen was detected in Item 1.UAU2EE

In item 1 was detected Acetaminophen.UAZCER




Item 1: Acetaminophen is no controlled substance under [Legislation]. Item 2: Methylphenidate is a controlled substance under [Legislation].

UF487E

Item 1 contained acetaminophen.UNXEZ7

Item 1 contained acetaminophen.UQ82Z6

Item 1 was reported as indications of Paracetamol (acetaminophen).UZD9DJ

Acetaminophen (APAP) was detected / identified in item 1.VAJ72M

Paracetamol was detected in Item 1.VQ37RJ

Item #1a Indicates acetaminophen.VQHQCF

Item 1 was found to contain Acetaminophen. Item 2 also indicated the presence of Lactose.VRKRHT

Based on analysis, I have found:- 1) Item 1 to contain Acetaminophen. 2) Item 2 to contain Methylphenidate which was listed in [Legislation].

VXYZRC

Methylphenidate HCl is a controlled substance in United States Controlled substances Act in section 1308 title 21 Schedule 2, d-4 ACSCN:1724.

W4L64D

Our data are accredited by General requirement for the competence of testingW4YYF8

Item 1 was found to contain acetaminophenW7Y7CC

Acetaminophen was identified in Item 1WB7PEB

Item 1 - Acetaminophen indicated, but not confirmed.WDHHDJ

Acetaminophen was identified in Item 1. Lactose was indicated in Item 2 by FTIR. No confirmatory test available.

WLLQL6

Item 1 was acetaminiphen. item 2 contained lactose too.WPDQEZ

Item 1 identified as acetaminophen.WPZUBF

Acetaminophen was detected in Item 1.WTXBNA

Acetaminophen (a non-controlled substance) was identified in item 1.WWPC6J

item 1-acetaminophenX324EF

Acetaminophen identified in item 1.X3A8HE

1) Item 1 was found to contain Acetaminophen. 2) Item 2 was found to contain Methylpenidate which is listed under [Legislation].

XAGNE8

Acetaminophen identified in item 1.XDTLKG

Item 1 was found to contain acetaminophen.XK4RV8

Item 1 was identified as acetaminophen.XLH3RQ

Item 1 contained acetaminophen.XN73YF

Item 1 0.226 gram, acetaminophen. Item 2 0.283 gram, methylphenidate, schedule II.XVNXUW

Item 1 contains acetaminophen.XW2DKQ

Item 1: was identified as Paracetamol. Item 2: In addition to methylphenidate, lactose was identied too.XYAKMJ

1a.) Acetaminophen (noncontrolled) was identified in the analysis.Y34KD6

Benzeneacetic acid, methyl ester was also detected in item 2.YGH8DW

Analytical data suggested the presence of acetaminophen listed as “indicated” above [Table 1a: Item 1 Results]; but due to insufficient analysis of this non-controlled substance it was not conclusively identified

YMHRXE

Paracetamol was present in item 1YU3WXU




In item 1 was detected Acetaminophen. In item 2 also detected lactose.YV2WHD

Item 1 (19-502-1) contained the non-controlled substance acetaminophen.YZZ7TF

Item 1: acetaminophen identified. Item 2: lactose identified in addition to methylphenidate.Z2BT4K

Paracetamol was indicated in Item 1.ZG83ZQ

Item 1: Acetaminophen detectedZLY7YW

1. Upon analysis, I found Item 1 to be Acetaminophen. 2. Upon analysis, I found Item 2 to be Methylphenidate which is listed under [Legislation].

ZMZTZ9

Item 1 contained acetaminophen.ZYXVD4

-End of Report-(Appendix may follow)


Collaborative Testing Services ~ Forensic Testing Program

Test No. 19-502: Drug Analysis

DATA MUST BE SUBMITTED BY Oct. 21, 2019, 11:59 p.m. TO BE INCLUDED IN THE REPORT

Participant Code: U1234A WebCode: QDHHY4

The Accreditation Release section can be accessed by using the "Continue to Final Submission" button above. Thisinformation can be entered at any time prior to submitting to CTS.

Scenario:An investigator has submitted two questioned powdered substances for analysis. Please examine the samples and determineif any controlled substances are present.

Please note: The controlled status of substances is based on the list in section 1308 of Title 21 Code of Federal Regulations under the UnitedStates Controlled Substances Act.

Items Submitted (Sample Pack DA2):Item 1: First powdered substanceItem 2: Second powdered substance

1a.) Were any controlled substances present in Item 1? If yes, list each substance.

1b.) What methods were used to examine Item 1?(If color and/or crystal tests are used, please simply check the appropriate method below. Specificcolor and crystal tests will not be listed in the summary report.)

Color Tests FTIR LC Crystal Tests GC UV

TLC GC/MS Microscopic

Other (specify):

No controlled substance detected/identifiedControlled Substance(s) detected/identified(please list below). Indicate salt form if determined.

Test No. 19-502 Data Sheet, continued Participant Code: U1234AWebCode: QDHHY4

2a.) Were any controlled substances present in Item 2? If yes, list each substance.

2b.) What methods were used to examine Item 2?(If color and/or crystal tests are used, please simply check the appropriate method below. Specificcolor and crystal tests will not be listed in the summary report.)

Color Tests FTIR LC Crystal Tests GC UV

TLC GC/MS Microscopic

Other (specify):

3.) Additional CommentsPlease note: Any additional formatting applied in the free form space below will not transfer to the Summary Report and may cause your information tobe illegible. This includes additional spacing and returns that present your responses in lists and tabular formats.

No controlled substance detected/identifiedControlled Substance(s) detected/identified(please list below). Indicate salt form if determined.

Test No. 19-502 Data Sheet, continued Participant Code: U1234AWebCode: QDHHY4

RELEASE OF DATA TO ACCREDITATION BODIES

The Accreditation Release is accessed by pressing the "Continue to Final Submission" button online and can becompleted at any time prior to submission to CTS.

CTS submits external proficiency test data directly to ASCLD/LAB, ANAB, and/or A2LA. Please select one of thefollowing statements to ensure your data is handled appropriately.

This participant's data is intended for submission to ASCLD/LAB, ANAB, and/or A2LA. (Accreditation Release section below must becompleted.)

This participant's data is not intended for submission to ASCLD/LAB, ANAB, and/or A2LA.

Have the laboratory's designated individual complete the following stepsonly if your laboratory is accredited in this testing/calibration discipline

by one or more of the following Accreditation Bodies.

Step 1: Provide the applicable Accreditation Certificate Number(s) for your laboratory

ANAB Certificate No.(Include ASCLD/LAB Certificate here)

A2LA Certificate No.

Step 2: Complete the Laboratory Identifying Information in its entirety

Authorized Contact Person and Title

Laboratory Name

Location (City/State)

Drug Analysis Test No. 19-502 Summary Report

Documents

Transcript of Drug Analysis Test No. 19-502 Summary Report