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COMFUCHEM LABS/ INC.

12--22-'33 7s 15s00 * 8s03SAMDI.E: I'JL CCK309?83 l6itB202BCONDS.s EXTRACTED 12--'21/33 UNDILUTED

MID LIBRARY SEARCHDATA; GH8PI3683C29 f 531ENHANCED '10B 2N 0T>

CSI1375S.7 OH 20

BASE M/Z: 128RIC? 1593340,

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433 WA!DtB2P2B2»3> <31-20-3>

DATAj GH003683C20 #531 BASE M-'c; 123-- 128ENHANCED HQB 2N 0T> RIC: 1853580.-- 2170870,DATAj UNPNHANCED #531 COMPurnEM LABS- INC.

CSI137K.7 OH 20

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(•177/ 2-HETHYLHflPHTHfiLENE <Q2»13> <91-57~S>r 284169.

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MID LIBRARY SEARCHDATA: GH003683C20 ft 574 BASE M--Z: 123

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MID LIBRARY SEARCHDATA; GH609689C20 * 690 BASE H/2: 153EHHAHCED <106 2M 0T> RICs 1-19247.7 OH 2u

EXTRACTED 12/21/89 UNDILUTEDi

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?>\ ACENAPHTHENE <Q3#iP,> <33-32-3>

DATA: GH003683C20 #630 BASE M--Z: 153-- 161ENHANCED (108 2N 9T> RIC: 143247,-- 380331,DATA; UNENHANCED #630 COMPUCHEM LABS, INC,

CS*. 18756.7 ON 2?

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?.2--'22--83 7:15:00 4 10:41SAMPLE: I1."- CC#3?368? !D#B2?29CONCS,; EXTRoCTE:) 12-'2i-'33 UNDILUTED

CS#13756.7

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M--£ 100 150

MID LIBRARY SEARCHDATA; QH003583C20 # 705 BA^FENHANCED a0B 2" 0T> RIC:

OH ">P

163

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MID DUAL MASS SPECTRUM12--22--83 7:15:00 + 10:41SECOND SPECTRUMSAMPLE:, 1'JL CC#30?639 IDKB202B

[ 479 DIBENfiOFURAN ((33*13? <132-64-3>

DATA: GH003683C20 #705 BASE M--Zs 163-- 168ENHANCED U0B 2N 0T> RIC: 674315.-- 1361310,DATAj IJWENHANCED #705 COMPUCHPH LABS- INC.

CS#13756.7 OH 20

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COMPUCHEM LABS. INC. MID LIBRARY SEARCHDATA; GH009689C26 * 736 BASE M/2; 167

1*t» '^'"f ,'vvj 7*A* A*.* 53 r «

SAMPLE! 1UL1000

SAMPLE

15s 00 + ll!09 ENHANCED <10B 2M 0T>CC*303689 10*62026 CS*18756.7

C u t ' r ~ . 5 EXTRACTED 12/21/89 UNDILUTED

|lll 1 ,|l 1 III 1 hi., in | - | .11 , .,1. i .,,1 ll

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MID DUAL MASS SPECTRUM!.2--'22--83 7:15:09 + 11:03SECOND SPECTRUM

D \1UL CC#3P3689 1D&B202B432 FLUORENE (Q3#13? <86-73-7>

DATA: GH003683C20 #736 BASE M/Z: 167-- 167ENHANCED (108 2N 0T) RIC; 1062319,-' 1649440,DATA; UNENHANCED #736 COMP'JCHEM LABS- INC,

CS#13756.7 ON 20

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12/22/89 7:15:00 -t- 12:27SAMPLE: 1UL 00*363689 10*62626 CS*18756.7

MID LIBRARY SEARCHDATA; GH009689C26 * 822ENHANCED <10B 2M 0TJ

OH 26

BASE M.--Z: 178PIC: 756735,

in•£>in

1020

SAMPLE

C14.H1G

M WT 178g PK 178XftNK 1

PUR 782 •

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CONDS.i EXTRACTED 12/21/89 UNDILUTED

i .il l|li ,iill, i.. ..|. , .III. . ., |

444 PHEMAHTHREHE <Q4*7) <85-01-8> *

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MID DUAL MASS SPECTRUM12--22--83 7:15:09 + 12:27SECOND SPECTRUMSAMPLE: I1-"- CC&393639 IDKB202B

RENE i'Q4#7> <35-P!-8>

mil.p=»-i

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DATA: GH003633C29 #322 BASE M/Z: 173-- 178ENHANCED (106 2N 0T> RIC: 732575,•' 1570810.DATA; UNFNHANrED #322 COMPHCHCM LAB^- INC.

CS*. 13756,7 ON 20

UillLlllU Iml.llUl.lj.Ul-pJSSpHJSSpSf-Hp

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I | I | i [ i T ' I l Ir 189696.

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LIBRARY SEARCH12/22/89 7:15:00 + 12:31SAMPLE: ILL CC#303€89 ID*B202B

COMPUCHEM LABS

CS*18756.7

DATA: GH009683C20 # 826ENHANCED C10B 2N 8T)

ON 20

BASE M/E: 178RIC: 229375.

1266SAMPLE

C14.H1M MT]3 PKRANKIN?UR 464

| il|l l|l.i..ihl A, ., ,L. . .1493 ANTHRACENE (04*8) <120-12-7>

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DUAL MASS SPECTRUM12/22/83 7:15:09 + 12:31SAMPLE: HA CC#399689 ID

SECOND SPECTRUM DATA: Gf87.9 -i

COMPUCHEM LABS••£•

#826

43.9-

DATA: GH009689C20 #826 BASE M/E: 178/ 178RIC: 235423./ 355331.

7 ON 29<Q4#8) <120-12-7>

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12--22/33 7s-.5:00 + 13:15

MID LIBRARY SEARCHDATA; GH003683C20 # 375 BASE M/Z; 143

ir>

1012

SAMPLE

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I . j 1 i ! . |i 1 . 1 , |l. L . |

4 426 DI-N-BUTYL PHTHALATE ((34*3 > <84-74-2> *r

1 j II | ,1, 1 1) ll.

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MID DUAL MASS SPECTRUM DATA: GH003683C20 #875 BASE M/Z: 143/ 4112/22/33 7:15:00 -*• 1.3:15 ENHANCED <'10B 2N 0T> RIC; 100 63,/ 6 40'SECOND SPECTRUM DATA? MNENHANCED #875 COMPUCHEM LABS- JNC,SAMPLE: 1'JL CC&303689 IDJS202B CSH13756.7 nN 20

42?/)I-N-?ijTVi_ PHTHALATE (Q4#3> <94~74-2>

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COMFUCHEM LwBS. INC, MID LIBRARY SEARCHDATA; GH003683C20 # 323 BASE M/2: 202

12/22/83 7:15:00 * 14:04 ENHANCED '10B 2N 0Tj RIC: 1 46687,c«MO| p. < in rr.#-5«ocao tntRop^R r.<;*i»?w;.7 on tv

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i t . .ill III .ul; 1 ill. . l.i . il , .. i L. . j i. Hi .11,. . . . 1>., - i • • ' • ' • ' r ' • - i - 'i - i • - • - T| ' • r '• - • - - • — - r1 ,. . . , , . „

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431FLUORANTHENE (G4#!?j <206-44-0>

DATA: GH003633C20 #323 BASE M--Z: 202/ 202ENHANCED (10B 2N 0T> RIC; 15 46",-- 700415,DATA: IJNENHANCED #923 COMPHCHEM LABS- INC,

CSH18756.7 ON 20

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12/22/83 7:15s 00 +• 14:23

CONDST: EXTRACTED"J2/21/83 UNDILUTED

MID LIBRARY SEARCHDATA; GH00%R3C20 # 350 BASE M/Z; 4 3ENHANCED (106 2N 0T> RIC: 1302520.

C16.H10

M WT 202B PK 202SANK 1

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445 PYREHE (Q5#3> <123-00-0>*

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HID DUAL MASS SPECTRUM12/22/89 7;15500 t 14;23SECOND SPECTRUMSAMPLE? lUL CC*309689 10*62026

445 GYRENE (65*3) <129-00-0-

DATA: GH009689C20 *950 BASE M/2: 43/ 43ENHANCED (108 2N 0T> RIC: 1374208..•- 2109430,DATA: UHEHHAHCED *950 COHPUCHEM LA8S, INC.

CS*18756,7 OH 26

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400 450 500 550 600

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LIBRARY SEARCH12/22/89 7:15:00 + 16:01SAMPLE: 1UL CC#303683 ID#B232B

COMPIJCHEM LABSDATA: GH003689C20 #1057ENHANCED (10B 2H 0T)

CS#18756.7 ON 29

BASE M/E: 240RIC: 133631.

1000

SAMPLE

, LP18.H13 UTljw PK *

645

1000

-1000 ' • • l •M/E 58

.••i-.-;>. 'f <i|l l.nL485 BENZO(A)ANTHRACENE (Q5«6) <56-55-3>

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100 150 200 250 300 350 480

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DUAL MASS SPECTRUM DATA: GH909689C29 *1057 BASE M/E: 240/ 24612/22/89 7:15:90 + 16:91 . \ RIC: 143871. / 627711.

SECOND96.6-

48.0-

188.0-

58.0-

M/E96.8-

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188.0-

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SAMPLE: 1UL CC*399689 ID*B282B C5*18756.7 01SPECTRUM DATA: GH069689C20 *1057 405 BENZO(A)ANTHRACEHE <Q;

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LAB INSTRUCTIONS:

RECEIPT DATE 12/20/89 CASE* 18756 7 DUE DATE:

SEMI-VOLATILE JC ] RC ] DC ] C 1)GC/MS WORKSHEET COMPUCHEM* 309689

JEC D R 2 C ] DSC D C 1 :

Sample Prep Cede -~:7GC/MS; S-V; LL S/S; SOW 2/88 Instrument Coae 255

Compound List 497Surrogate Std 393Internal Std

SAMPLE ID#: B202B Dry Wt . i '^ '/. Moisture /^

GC/MS ANALYSISVolumes mixed: BN ul Acid_^ ulInternal Standard Volume Added - ulMixed Sample Volume Injected / ul ~Date of Sample Bottle Analyzed &2 / oil / 6JDFTPP F i 1 e n a m *E>Mf*f(£f-!&^ „ . Disk <-/69fS~1Standard Fi 1 en*Mrtfafy/J£/i&2£ Disk C i }Sample Fi \*r\**(*( 1 HOP1!£f¥*}£»}£> Disk { / )

i s

ANALYST(S): Injection Z /7 Work-up.

GC/MS R E V I E W| | Entry Codes OK,EA,JA, ES,AL,AH,PL,PH,FL,JS

CONDITION | | FH,NL,NH,YL,SL,SH,SM,YHCODE | I

| / I Non-Entry Codes IM,IL,IH,SU,CT,CS.PC,OT,DA| pi/ | ED, LF,LA,DI , CO,RN,DW,NS

I 1 ^Disposition: [ ] CompleteExtraneous Peak Search Results:

C ] Reinjection required.# of P e a k s Founds ( '^/~ \ v—-*^ v(\ \ C 3 R-eex t ract i on requi red

* Of H l t S : //"? j ^M y^

\^/ ^ [" J Dilute I—ZS 1—!)t of Surrogate Outliers: O

C ] Reinject NeatQu a l i t y Assurance Notict(s):

C 1 Send to QA* Notices Required fj)

, J- if / /GC/MS Review ^^ Date f1 / *" /^X Auditor Date===========================================================================REPORT INTEGRATION ^ _ Total t jjf Injections ,Final Reportable Package(s)

QA COMMENTS.

I n i t i a l s Date.

FINAL REVIEW I n i t i a l s DateA C 1 0 0 6 ( 0 ? / 8 T

18756 Q7 SfiMPLE DflTfl PPCKPGE

ASSIGNED TO:

EXTRACTION WORKSHEETSemi-Volaltlea/M.aceHaneoua

CompuChem Laboratories Inc. DATE ASSIGNED la- 1

PAGE OF

SAMPLENUMBER

SCHbflO

3/0/7^

PREPCODE

CASE1

CLIENT

J30IB

SBfiT

OC SAMPLE

TYPE

ss

m

B

onaNO.

SAMPLEWEIGHT (g)

VOLUME (Rri)

3,0.0

3O.O

•io.o

•30.0

30.0

30.0

30-O

lo.o

30.0

FINAL EXTRACT VOL (MLS)

01

ACK) PEST

AOJUSItDPH

B/NDATE

COMPT

a at

COMMENTS

FOR rtf..'

SURROGATE

SPIKE

NO

AMTLOT

NO

AMTLOT

S-Vol Actd B/N PMl OUtw Otor

393

05 ml.30 110

3012 20211.0ml. 10ml.

aofcis 308 oq

MANUAL COUNTER

FINAL VOLUME VARIFIED

SUPERVISOR REVIEWED

EXTRACTS RECEIVED BY

UJ(0ct^oaa.

•i£1

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COMPUCHEM * 009689 FILE: GH009689C20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE

CMP*

4946104116014214224744206204126224424364404604386066036254106024464394754346084774954356116264164784254024794016O5607476427428424

M/E

1529493128146146108146108451087011777136821391071229316218012812722510714216423619619616265163152138153184109168165165149

F

I

I

I

COMPOUND NAME SCAN

530

D4-1,4-DICHLOROBENZENE (IS* 420PHENOL (01*3)BIS(2-CHLOROETHYL)ETHER (012-CHLOROPHENOL (Ql«6>1,3-DICHLOROBENZENE <01tt7)1,4-DICHLOROBENZENE (01*8)BENZYL ALCOHOL <Qltt9>1,2-DICHLOROBEN2ENE <Q1«10>2-METHYLPHENOL (01*11)BIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOL (01*13)N-NITROSO-DI-N-PROPYLAMINEHEXACHLOROETHANE (01*15)NITROBENZENE (01*16)OS-NAPHTHALENE <IS*2>ISOPHORONE (02*2)2-NITROPHENOL (02*3)2.4-DIMETHYLPHENOL (Q2*4)BENZOIC ACID (02*5>BIS(2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENOL (02*7)1, 3,4-TRICHLOROBENZENE (Q2*NAPHTHALENE (02*9)4-CHLOROANILINE (Q2*10)HEXACHLOROBUTADIENE (Q2*ll>P-CHLORO-M-CRESOL (02*12)2-METHYLNAPHTHALENE (02*13)Dl0-ACENAPHTHENE (IS*3)HEXACHLOROCYCLOPENTADIENE (2,4,6-TRICHLOROPHENOL (03*32,4,5-TRICHLOROPHENOL (03*42-CHLORONAPHTHALENE (03*5)2-NITROANILINE (03*6)DIMETHYL PHTHALATE (03*7)ACENAPHTHYLENE <Q3*8)3-NITROANILINE (03*9)ACENAPHTHENE (03*10)2,4-DINITROPHENOL (03*11)4-NITROPHENOL (03*12)DIBENZOFURAN (03*13)2,4-DINITROTOLUENE (03*14)2,6-DINITROTOLUENE (03*15)DIETHYL PHTHALATE (03*16)

688

CORRECTED/REVIEWED BY

DATE

AREA

213000

*

754000

396000

:D BY

OUANTREPORTVALUE

40. 032. 3

61. 9

r 334. 0•1 T

o40. 0

J"l89. 04T/\ /\

9 — *r-

30. 6

T af. a46. 840. 0

t__ •~ &lOft"f? ACE. *t

3. 64 d

4. 5

1—9-15. 6

. 1

. 7

_^-

REPORTEDAMOUNT(UC/KC)

/ r • "' -i-1-00BDL LBDLBDLBDLBDLBDL

'V"''-glOOBDL

/> 4-teeojt * 1

BDLoOJ

BDLBDL

7>^ 63OOl&OOOBDLM l

BDLrz J OO

BDLBDLM » M I

/< 6eo

BDLBDLBDL

4OJ340J

/y, taojt IBrt /

/7 -t50JBDL

(Si /

1OOJ

BDL

DETECT.LIMIT(UG/K6)

< i '/ -, 330' 330

330330330330330330330330T (*330330

3303303301700 '33O

33033033033033033O

3303301700

170O

33Of 7tO.D

330170O1700330T T«*33O

330

(CC/MS DATA REVIEWER)

18756 d? SPMPLE DPTP PPCKPGE

COMPUCHEM * 009689 FILE: OH009689C2O COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE

CMP« M/E F

417 204432 16648O 138467 188 I604 198443 169414 248433 284609 266444 178403 178426 149431 202459 240 I445 2O2415 149423 252405 228413 149418 228497 264 I429 149407 252409 252406 252437 276419 278408 276619 112 S612 99 S447 82 S448 172 S628 330 S496 244 S471 212 S456 216CHECKSUMS:

820

1058

COMPOUND NAME SCAN

4-CHLOROPHENYL PHENYL ETHERFLUOR ENE < 0.3*18)4-NITROANILINE (03*19)D10-PHENANTHRENE (IS*4>4,6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE (04*4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENE (04*5)PENTACHLOROPHENOL (04*6)PHENANTHRENE (04*7)ANTHRACENE (O4*8)DI-N-BUTYL PHTHALATE (Q4*9)FLUORANTHENE (04*10)D12-CHRYSENE (IS*5)PYRENE (05*3)BUTYLBENZYL PHTHALATE (05*43,3'-DICHLOROBENZIDINE (05*BENZO(A)ANTHRACENE (05*6)BIS(2-ETHYLHEXYL) PHTHALATECHRYSENE (05*8)D12-PERYLENE (IS*6)DI-N-OCTYL PHTHALATE (06*2)BENZO(B > FLUORANTHENE (06*3>BENZO(K)FLUORANTHENE (Q6*4)BENZO(A)PYRENE (06*5)INDENO(1,2,3-C,D)PYRENE (06DIBENZO(A, H)ANTHRACENE (O6«BENZO(G,H, I)PERYLENE (06*8 >2-FLUOROPHENOL (SS*1>D5-PHENOL (SS*2)D5-NITROBENZENE (SS*3)2-FLUOROBIPHENYL (SS*4)2,4,6-TRIBROMOPHENOL (SS*5)D14-TERPHENYL (SS*6)D10-PYRENE1,2,3,4-TETRACHLOROBENZENE

1225

AREA

488OOO

315OOO

248000

QUANTREPORTVALUE

14. 8Sr 540. 0

*•» f\ —mi. Ui-A — =91 wl A

-W22TS-v-^ 2+7-3

2. 16. 140. 06. 9•i-r-t5 >-»

hr »

> L '•2. 3

A^ -Sr-8-40.01 11 «

79. 380. 533. 132. 283. 538. 441. 2

REPORTEDAMOUNT< UC/KC)

BDLf7-49O

ZBOJ

O/w

BDLBDLBDL

Jsi 7PO>° -820**/ OJ

j x~ aeoj

•-' 7'-i-830'Jy i

• rt ,1 t\i\l

'•* *~ ' B DL^ -76U73 -430 J

*37 J__ .

BDLBDLBDLBDLBDL

79.80.66.64.83.77.82.

DETECT.LIMIT(UG/KG)

33C33C170C

^330330170033033033033O

330330J.-7 f\O r \J

33033O330

330

330330330330330

%7."f.7.7.7.X

BDL 33

13335. 4741 2414OOO. 1968. 7 45490.


DATE

(GC/MS DATA REVIEWER)

18756 d? SPMFLE DPTP PPCKPGE

COMPUCHEM * 009689 FILE: GH009689C20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE

QUANTCC REPORT

NO ID* SURROGATE COMPOUND VALUE

72 619 2-FLUOROPHENOL (SS*1) 79.373 612 D5-PHENOL (SS«2) 80. 574 447 D5-NITROBENZENE (SS«3) 33. 175 448 2-FLUOROBIPHENYL (SS*4) 32.276 628 2, 4,6-TRIBROMOPHENOL (SS*5) 83.577 496 D14-TERPHENYL (SS*6) 38. 478 471 D10-PYRENE 41.2

QUANTREPORTAMOUNT 7. +* CONTROLSPIKED RECOVERY RANGE

100. 0100. 050. O50. 010O. 050. 050. 0

7980.6664.83.77.82.

25-12124-11323-1203O-11519-12218-13717-125*

* ADVISORY SURROGATE ONLY++ % RECOVERY - OUANT REPORT VALUE / QUANT REPORT AMOUNT SPIKED X 100 Y.

CORRECTION FACTOR CALCULATION:

FINAL EXTRACT VOLUME (ML) 3O. OG DRY GC/MSX X WEIGHT X DILUTION X 33. 3 =

O.9 ML AMOUNT EXTRACTED(G) FACTOR FACTOR

i-*O. 9ML 30.00 1-r-Co' 1.0 i X <•

X X X X 33. 3 = ,33r-3OO"~~0. 9 ML 30. 000

QUANT REPORT AMOUNT SPIKED CONVERSION FACTOR:

1000 UL FINAL EXTRACT VOL (ML) GCMSx X DILUTION =

AMOUNT SURROGATE ADDED (UL) SPLIT FACTOR FACTOR

1000 UL 0. 9ML 1. 0X X 2. 000

5OO UL 0. 9 ML

VERSION 8


DATE


18756 07 SPMPLE DPTP PPCKPGE 5 2 5

IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS

Lab Code: COMPU Case No.: 18756

Matrix: (soil/water) SOIL

Sample wt/vol: 30.0 (g/mL) G

Level: (low/med) LOW

% Moisture: not dec. 14 dec.

Extraction: (SepF/Cont/Sonc) SONC

GPC Cleanup: (Y/N) H pH: 7.7

B202BDLContract: (2-88i-REVS

SAS No.: SDG No. : 07

Lab Sample ID: 309689

Lab File ID: GD009689A20

Date Received: 12/20/89

Date Extracted: 12/21/89

Date Analyzed: 12/22/89

Dilution Factor: 5.0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

f.1 — 1 *5_1 _ _ _ _ _ _

a Q-.~j £, — £.— _ ___.

95-95-4

O /•»!• 1 W*hW**T

1 "5 r%4 W T «*««.*W

- - — . . . * «

— . - * . •

• •) i». 4 w 1 w«k If . » ^ • 1

W 4 f -I «-«l_ 1 ' T \ Tt Am 1.

v j . y f . _.. yk ^ .

nujCaLJllXu L OB XlclllB. - . j^ •_ ,

^ . - . . . .

Q . - • »

1 1 J> m ' W T W n •» i

J _. . ' 1 •

-- . « . . J .

•J , - 1 . J .

* . - _ , . , * WA*%A!

1 XT ' 4» ' T '

— . • . . •• T*W W 1 ^

- W*-W 1

. f —^ t . . , -

92019001900190019001900190022001900

1200019001900190019001900730093001900190019001300190019001900180019001900930019009300190019001900

DJUUUUUUDUDUUUUUDUuuuDJUuuDJUUUUUuuu

FORM I SV-1 1/87 Rev.

18756 07 5PMPLE DPTP PPCKPGE 524

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.




Sample wt/vol: 30.0 (g/mL) S




GPC Cleanup: (Y/N) Ii pH: 7.7

B202BDLContract: (2-88.-REVS







Dilution Factor: 5. 0


99-09-2 3-Nitroaniline83-3 2 -9 -———Acenaphthene51-28-5 2 , 4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-01-6 4-Nitroaniline534-52-1 4, 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3, 3'-Dichlorobenzidine56-55-3 Benzo (a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b) Fluoranthene207-08-9 Benzo(k) Fluoranthene50-32-8 Benzo(a) Pyrene193-39-5 Indeno (1,2, 3-cd) Pyrene53-70-3 Dibenzo( a, h) Anthracene191-24-2 Benzo (g,h, i) Perylene

;i) - Cannot be separated from Diphenylamine

930022093009300660190019001900580930093001900190019009300900200200260260190038001900190019001900190019001900190019001900

UDJUUDJUUUDJUUUUUUDJDJDJDJDJUUUUUUUUUUUU


18756 07 SPMPLE DflTfl PPCKPGE

IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.








GPC Cleanup: (Y/N) H pH: 7_._

Number TICs found: 20

B202BDLContract: (2-88.-REVS

SAS No.: SDG No.: 07







CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

CAS

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.

NUMBER

621-27-22416-94-6

4453-90-1

569-41-5

54105-67-8629-78-754105-67-8

544-76-3

629-97-0

COMPOUND NAME

DIMETHYLPHENOL ISOMERPHENOL , 3 -PROPYL-PHENOL, 2 , 3 , 6-TRIMETHYL-TJNKNOWN1,4-METHANONAPHTHALENE, 1,4-UNKNOWNNAPHTHALENE, 1, 8-DIMETHYL-UNKNOWNHEPTADECANE, 2 , 6-DIMETHYL-HEPTADECANEHEPTADECANE, 2 , 6 -DIMETHYL-UNKNOWNHEXADECANEPENTACOSANE ISOMERPENTACOSANE ISOMERDOCOSANEPENTACOSANE ISOMERUNKNOWNUNKNOWNUNKNOWN

RT

7.708.478.598.979.059.549.8510.0010.9211.5512.1512.5012.7013.2513.7714.2714.7515.1916.0416.50

EST. CONC.

64003500170016001600210021002100250031002300190031002700390087003100600062002900

Q

JJJJJJJJJJJJJJJJJJJJ

FORM I SV-TIC 1/87 Rev.

18756 07 SPMPLE C'PTP PPCKPGE 522

COMPUCHEM LABSRIC COMPUCHEM DATA: GD009689A20 SCANS 305 TO 160012/22/89 18:47:00 OUT OF 305 TO 1600SAMPLE: 1UL CCI309689 ID#B202B-DL CSI18756-7 ON 20CONDS.: EXTRACTED 12-21-89 1: 5 DILUTION 2096630

ISI1 IS#2

SSI3 '

IS«3 SSf5 SSI6

SSI4 D3tl ISI4 SSi?

ISIS

ISI6

IO

UJ

RIC '

1516

octCLctKct

UJ-JCL

r.'5

infv-

•JO

i4006:04

T6809:05

80012:07

I86015:09

120018:11

140021:13

160024:14

SCANTIME

QUANTITATION REPORT FILE: GDO09689A20DATA: GD009689A20. TI12/22/89 10:47:00 - / 'SAMPLE: 1UL CC*3O9689 ID*B202B-DL CS*18756-7 ON 2OCONDS.: EXTRACTED 12-21-89 1: 5 DILUTIONSUBMITTED BY: 2O ANALYST: 643

AMOUNT»AREA * REF. AMNT/(REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHLOROBENZENE (IS*1)2 61O PHENOL (Ql*3) <108-95-2>3 411 B IS (2-CHLOROETHYL) ETHER (Ql*5) Oll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-B>5 421 1.3-DICHLOROBENZENE (Ql*7) <541-73-l>6 422 1.4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-51-6>8 420 1.2-DICHLOROBENZENE (Ql*10> <95-50-l>9 620 2-METHYLPHENOL (01*11) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL-(01*13) <106-44-S>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (IS*2)16 438 ISOPHORONE (02*2) <78-59-l>17 6O6 2-NITROPHENOL (02*3) <B8-75-5>18 603 2,4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZOIC ACID (02*5) <65-85-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1,2, 4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (Q2*12) <59-50-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 *495 D10-ACENAPHTHENE (IS*3)29 435 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4,6-TRICHLOROPHENOL (03*3) <88-O6-2>31 626 2, 4, 5-TRICHLOROPHENOL (03*4) <95-95-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-58-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 4605 2, 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7O05-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>

18756 07 SPHPLE C-PTP PPCKPGE 52Q

NO474849505152535455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME*467 D10-PHENANTHRENE (IS*4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <534-52-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-3O-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLOROBENZENE (04*5) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <85-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*459 D12-CHRYSENE (IS*5)445 PYRENE (05*3) <129-OO-0>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3,3'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO(A)ANTHRACENE (05*6) <56-55-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (Q5#7> <ll7-61-7>418 CHRYSENE (05*8) <218-01-9>*497 D12-PERYLENE (IS*6)429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO(B)FLUORANTHENE (06*3) <205-99-2>409 BENZO(K)FLUORANTHENE (06*4) <207-O8-9>406 BENZO(A)PYRENE (06*5) <50-32-8>437 INDENOd, 2. 3-C, D)PYRENE (06*6) <193-39-5>419 DIBENZO(A,H)ANTHRACENE (06*7) <53-70-3>408 BENZO(C, H, DPERYLENE (06*8) <191-24-2>*619 2-FLUOROPHENOL (SS*1)*612 D5-PHENOL (SS#2)*447 D5-NITROBENZENE (SS*3)«448 2-FLUOROBIPHENYL (SS*4)*628 2, 4,6-TRIBROMOPHENOL (SS*5)*496 D14-TERPHENYL (SS#6)*471 D10-PYRENE456 1,2,3,4-TETRACHLOROBENZENE

M/E SCAN TIME152 419 6:2194 395 5:5993 NOT FOUND128 NOT FOUND146 NOT FOUND146 NOT FOUND108 NOT FOUND146 NOT FOUND108 443 6:4345 NOT FOUND108 456 6:5470 NOT FOUND117 NOT FOUND77 NOT FOUND136 528 8:0082 NOT FOUND139 NOT FOUND107 501 7:35122 511 7:4493 511 7:44162 NOT FOUND

REF RRT METH1 1.000 A BB1 0. 943 A BB

AREA(HGHT)227320.42252.

AMOUNT4O.OOO NG4. 720 NC

%TOT7. 050. 83

1 1.057 A BB

1 1. 088 A BV

15 1. 000 A BV

15 0. 949 A BB15 0. 968 A VV15 0. 968 A VV

68400.

410954.

677341.

255641.273494.31070.

11. 508 NG

64. 268 NG

40.000 NG

37.784 NG88.745 NG3. 873 NC

2. 03 7'

11. 33 -r

7. 05

6. 66-.15. 65 <

0. 6S_i:

18756 07 SflMPLE DPJP PPCKPGE 51 9

NO M/E22 1802324

128127

25 22526 10727 14228 16429 23730 19631 19632 16233 65

163152138153

3435363738 18439 1094041

168165

42 16543 14944 20445 16646 13847 18848 19849 16950 24851 28452 266"53 178

17855 14956 20257 24058 20259606162

149252228149

63 22864 26465 14966 25267 25268 25269 27670 27871 27672 11273 9974 8275 17276 33O77 244

SCAN TIMENOT FOUND529 8:01NOT FOUNDNOT FOUNDNOT FOUND590 8:56685 10:23NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND646 9: 47NOT FOUNDNOT FOUNDNOT FOUND688 10:25NOT FOUND696 10:33702 10:38707 10:43NOT FOUNDNOT FOUNDNOT FOUND733 11: 06NOT FOUND816 12:22NOT FOUND740 11:13NOT FOUNDNOT FOUNDNOT FOUND818 12:248L8?>12:24871 13:12925 14:011053 15:57945 14:19NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND1218 18:27NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND320 4:51394 5:58467 7: O4624 9:27756 11:27958 14:31

REF RRT METH

15 1. 002 A VV

15 1.117 A*BB28 1.000 A VB

28 0. 943 A VB

28 1.004 A BV

AR EA(HGHT) AMOUNT

14554O. 6.927 NG

103868.355172.

B56O.

11809.

282828

28

47

47

A —* /

4747475757

1. 0161.0251. 032

1.070

1.000

0. 9O7

I rtA^. UU«t

1. 0021. 0671. 1341. 0000. 897

A VVA VBA VB

A VV

A VV

A*BV

A BM x*T ' LiBV f >>"?A BV /->-«•A BB•A*VVA BVA BV

3288.53O64.3852.

37188.

417154.

10777.

17508.12220.234108.12516.

9. 345 NG40.OOO NG

2.O43 NG

1. 108 NG

1.254 NG3. 378 NG1.297 NG

2.987 NG

4O.OOO NG

1.8O3 NG

•*+: NGNG

1. 054 NC1. 363 NG

40.OOO NG1. 336 NC

64 1.000 A BB 205116. 40.000 NC

XTOT

1. 22

1. 65 V7.05'

0. 36

0.20 7"

0. 22 =O. 6O -~0.23

0. 53

7. 05

0. 32

0.0. 2447. 050. 24

7. 05

11

15282857

0.0.0.0.1.0.

76494O884911104910

AAAAA

BVBVVVBBBB

A*BV

109987.100291.67161.88736.19132.53O52.

13.11.6.6.15.7.

402678952924428726

NGNGNGNCNGNG

2.2.1.1.2.1.

360623227236

18756 07 SPttPLE DPTP PPCKPGE 5 1 5

NO M/E SCAN TIME REF RRT78 212 944 14: 18 57 0. 89679 216 NOT FOUND

NO12345678910111213141516171819202122232425262728293031323334353637383940414243444546474849505152

7:7:

RET(L)6: 226: 006: 046: 096: 196: 246: 346: 376: 446: 466: 556: 567: 027:078: 027: 257: 337: 367: 457: 44

5158

8:038:088: 188:488: 5810: 259: 179: 249:269: 389: 4810: O510: 1310: 2210: 2710: 3010: 3510: 4110: 4310: 11

04090912

12: 2511:1611: 1811: 4812: 0112: IS

RATIO1. 001. 00

11111111

1. 00

1. 00

1. 00

1. 001. 001. 00

1. 00

1. 001. 00

1. 00

1. 00

1. 001. 001. 00

1. 00

1. 00

0. 99

RRT(L)10. OOO10. OOO10. 00010. 00010. 00010. 00010. 00010. OOO10. 00010. 00010. 00010. 00010. OOO10. 00010. 00010. 00010. 00010. 00050. OOO10. 00010. 00010. OOO10. 00010. 00010. 00010. OOO10. OOO10. 00010. 00010. 00050. OOO10. 00050. 00010. 00010. 00050. 00010. OOO50. 00050. OOO10. 00010. OOO10. 00010. 00010. 00010. 00050. 00010 00050. 00010. OOO10. 00010. OOO5O. OOO

RATIO0. 10O. 09

METHA*BV

AMNT40. 004. 72

0. 11

0. 11

0. 10

0. 090. 020. 10

0. 10

0. 110. 10

0. 02

O. 1O

0. 02O. 100. 1O

0. 11

0. 10

0. 09

11. 51

64. 27

40. OO

37. 7888. 753. 87

6. 93

9. 3540. 00

2. 04

1. 11

1. 253. 381. 30

2. 99

40. 00

1. 80

AREA(HGHT)56799.

AMNT < L )4O.50.50.50.50.50.5O.50.50.50.50.50.50.50.40.5O.50.50.50.50.50.50.50.50.5O.50.50.40.50.50.5O.50.50.5O.50.50.5O.50.50.5O.50.50.50.50.50.50.40.50.50.50.50.5O.

OO000000000000000000000000000000000000OO00000000000000000000000000000000000000000000000000000000000000OO

R.1.o.

0.

1.

1.

0.o.o.

0.

0.1.

0.

0.

0.0.0.

0.

1.

0.

AMOUNT7. 699 NG

FAC R. FAC(L)OOO149

241

446

000

302323037

172

123OOO

019

O27

007120009

084

000

O2 1

1.1.1.1.1.1.0.1.1.1.1.0.0.0.1.0.0.0.O.0.0.0.1.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.0.0.1.0.1.0.1.0.0.0.0.0.

0005754194265746357484930460471259298735740007812184001824743273892413322223616560003744053993184725698072572OO139295769335269417659402216000130573252280130

XTDT1. 36

RATIO1.0.

0.

1.

1.

0.1.0.

0.

0.1.

0.

o.

0.0.0.

0.

1.

0.

0009

23

29

00

767708

14

1900

04

O2

030703

06

00

04

18756 07 SPHPLE D-PTP PPCKPGE 51 7

NO535455565758596061626364656667686970717273747576777879

RET(L)12:12:13:14:16:14:15:16:16:16:16:18:17:17:17:18:21:21:22:4:5:7:9:

11:14:14:9:

273116060425190103O6O639015053324448415259053030372339

RATIO RRT(L)1. 000. 990. 990. 990. 990. 99

0. 99

1. 001. 001. 001. 001. 000. 990. 99

10.10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.10.0.0.0.0.1.0.10.1.

000000000000000000000000000000OOOOOOOOO000OOO000OOOOOO0007429488759O6118907000OOO

RATIO0.0.0.0.0.O.

O.

1.O.1.1.0.1.O.

101011111009

10

0399Ol019900O9

AMNT5.6.1.1.

40.1.

40.

13.11.6.6.15.7.7.

974605360034

00

40689592437370

AMNT(L)50.50.50.50.40.50.50.50.50.50.50.40.5O.50.50.50.50.50.50.50.50.50.50.50.50.50.50.

0000000000000000000000000000OO000000000000000000000000

R.0.o.0.0.1.o.

1.

o.o.o.0.0.0.o.

FAC R. FAC(L)145145034023000043

000

387353079200043181194

1.1.1.0.1.1.0.0.1.1.1.1.2.1.1.1.1.1.1.1.1.0.1.0.1.1.0.

217123593860OOO600828194091619ISO000207157271009218047027444511571443140173260631

RATIO0. 120. 130. 020. 031. 000. 03

1. 00

0. 270. 230. 140. 140. 310. 150. 15

18756 07 SPMPLE &PTP PPCKPGE 516

CCI1PUCHEI-1 LABS, INC. HID LIBRARY SEARCHDATA: GD6o9b89A28 * 395

12/22/85 10!4?5Ui3 t 5! 55 ENHANCED a 06 2N 8T>SAMPLE; 1UL CC*309£89 ID*62826-DL CS*18?5b~? OH 20

j i. f. r,ii iiTTriu

10*-H

10BASE H/2: 94RICs 1

11*0

SAMPLE

•

r

ii ill

uunuo-, « L.-. IT.HL, ic.u , <. j_i~c-J * « o uiuui *un

UJl

i

.. |

UJ<D1

OC6.HS.U 6ly PHENOL r:Ql#3: <lB8-95-2>* IJ:

Bid1!]'RANK 1 ,« 2PUR 53 i •

1 ll

1145 Y

y

-1145

I

, 11, ,JH

+ ' 1

H/2 50

il II t

r "•ct

•iCj

UJ-JII

SAMPLE HINUS LIBRARY ' ?

uh , ill In , t i .1 . . .

* 1. r * 1 - T • | i | I ' 1 - 1 1 T > t " W + " | - t W T ' T i | i y I - I | • T - t • 1

r 'I

'/I

TV

'S

10r.CO

Jyy I5y 200 250 3uo

tir.i

MID DUAL MASS SPECTRUM DATA; GD005S85A20 *395 BASE H/2: 54/ 9412/22/89 lS;47;yy t 5;59 ENHANCED U0B 2H 8T: RIC; 148223,.-' I7y75l.SECOND SPECTRUM DATA; UHENHANCED *395 COHPUCHEM LABS, INC,SAMPLE; 1UL CC*389689 IO*B202B-OL CS#18756-7 OH 28

, 610 PHENOL <wi*3> <i0s-95-2>•JS.-Ji- I

\ !*?.a: . 1 ii

•1 L

Ilii, 1,, !• • M l T

180,8 -j

1 i-i ;

5y.a -

•

1,1. II

I 'ill ill ilii.iiUiiiiy• I — i -| — r- | — • — r

M/2 5055.9-]

-

47.9-

-

•

lyy. y ~i

56. w -

-T-J--I -J— I- p T-

/ •-,"! - s -

_^^

ilu,1 i ' l

(I

,!

-UJ

r CD; i

^ ctr 15595. CL

aW_pP*p**p-y*4,- —

: ah 1

C.

UJ" -J

1OT 150 200 250 309 £- 17320. Ct

'. \~- o

•D; in

I | , , , , , t , , , , , - | - T i | , ! . , • y , | , , , , . f , | i , . T . , , , , | - i . T , , ffj

r^ 1 ^-*\^iK - - - - - - ^^

• f | - i | i • t | r j i | i ] i j-ff i | l | i | i •[• r |"t (• t j t [ i j i ] ' t | t | i | i "| i | t j -T

400 45y 5oo ^SR KRR


12/22/85 10!47j00 + 6j-SSAMPLE; 1UL CCt389689 IDt6202B-DL

MID LIBRARY SEARCHOATH? GD009689A20 * 443ENHANCED O0B 2N 8T>

CS*18756-7 OH 28

10

BASE M/Z; 188RIC; 247059,

1030

SAMPLE

CONDS. ; EXTRAC1

11jl

ll1 ,1,, ,111 . ! \

C7.H8.0 620 2-HETHYLPH&103d l

H HT IBS6 PK 10sXHNK ^PUR 886

i

1 , 1 Ji 1 ll

ED 12-21-89 1; 5 DILUTION

.

!. H1 — u~, . ' • - 1 . r- . t '-i , 1 ' - ' ' ' • ' ' ' • • ' — ' ' ' 1 ' ' — ' lf " ''

UJCD•1

OIOL (Ql#ll) <95-48-7>* ?

Q>

Ct

ct

UJ-Jfi

SAMPLE HIHUS LIBRARY ' S10'30 1

*

0

-1030 •

,,.. lllil 1 i,J ii,. .

T - T | | |

M--2 5fl 100

. , I I . . .

'/I

NQ

•-£•10

CO••—I

150 200 250 300

''t

10MID DUAL MASS SPECTRUM DATA: GD009685A20 #443 BASE M/2: 108/ 18812/22/89 10;47;«y t g; 43 ENHANCED (106 2H 0T> RIC; 266239,.-' 292351,SECOND SPECTRUM DATA: UNEHHANCED #443 COMPUCHEM LABS, INC,SAMPLE: JUL CC*389689 ID*B202B-DL CS*18756-7 OH 28

628 2-METHYLPHEHOL <61#11> <55-48-7>3S.3

45,4

100,0

50,0

M/298,9

49.4

180,8

56,0

H--2

1i

JJ1 I 1

1 'I

•

.1Hi ' ii,. 1, l li .1, 1"'|" I I - | ' | ' 1 |

11

•1

1

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, , , -j , | r~| -. ,— | y

50i

J*

-

.

•

—

-i

' ' ' 1 ' ' i

T (•• l | 1 | ' I ' '|

?5fl

- 33232.

II(I

HL• I • i - i * I i l • 1 ' i < l i l - i - 1 i i i l - i T i ' 1 i l ' i - i i l i 1 T i - i i iii

..... f L Ii . . . i . i i . . . , , , , , ,

.

hi**j

'. cto("T"

- 33530, CL

cth-ctG

UJ-J

I— p-T-T • | i | i | • | • 1 < | i | • | < | i | i | • ( • | • | i f • I • I i | i | • T ' 1 ' 1 f.

100 150 20d 250 300 £(- 33232. -1

i | . T . 1 i | i | • 1 - I • | > 1 ' I • I ' 1 ' 1 • T • T ' | ' 1 • I • 1 ' I ' | ' 1 • 1 ' 1

Ul

'. r-.Q

•D10f-

r 39680. 2

-

r j r fr-f i | i -| i | • t ' i ' i T i T y ' i ' i * T T T ' | ' i T I ' 1 i I > | ' I ' I i400 458 588 550 600


12/22/89 10« 47; 88 t 6:54SAMPLE: 1UL CCi389689 IOtB202B-OL

MID LIBRARY SEARCHDATA: GD009689A20 * 456ENHANCED <186 2N 8T>

CS#18?56-7 OH 28

\r>

BASE H/2: 107RIC! 1212410,

1863

SAMPLE

•

C7.H8.01863 i

M WT logB PK 187SfiNK I# 12PUR 873

COHDS,: EXTRACTED 12-21-89 1: 5 DILI

1 ,1j | l ,1,!, , . il,.

622 4-r-lETHYLPHENGL <Q1*13> <186-44-5>r

ill"I1 •

JTJON

j

t

i, - - | . . . . - . . | . . . . . . | f . . , . j - . , . . - j „ . /

UJCD•1

OctCL

ctp-ct

UJ-jCL

SfiHPLE MINUS LIBRARY £1063i

0

_ 1 OiT-'J

r

i ..,, ilnl, i ,.

r Ct'/i

r.

'•£"10

CO*-»

H/2 100 128 140 168 200

MID DUAL MASS SPECTRUM DATA: GD009689A20 #456 BASE H/2: 107/ 18?12/22/85 10:47:00 t 6:54 ENHANCED (106 2N 0T> RIC: 1302520./ 1331190.SECOND SPECTRUM DATA: UHEHHAHCED #456 COMPUCHEM LABS, INC,

D1UL CC*309£89 ID#B202B-OL CS*18756-7 OH 28622 4-METHYLPHENOL <Q1»13> <106-44-5>

•J3.U -

.

•

49.5-

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„

-

.

V_^/

1

111. .11 |

I

, ll1

100. 0-j

50.8-

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III.. . ll. .lli — i -- » — t i —

M-'H 50

!

L. .1,' I "

. ...Ii.. , 1

- 29, 872.

UJCDct

Oct0.

ctKctCt

UJ-J

1 1 1 i 1 1 I l l i l l l T 1 i | l | i l l l l LL.i

llln. . ,1,•9—f -*- • , 1 ,

-J 1

\\

1.

r 203320. E:•11/1

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•£«IOr>CO

188 158 2yy


12/22/89 18: 47; 08 +

a-.

10MID LIBRARY SEARCHDATA: GD809689A20 * 581 BASE M/2; 107

7:35 ENHANCED <10B 2N 0T> RIC; 647167,SAMPLE: 1UL CCS389689 ID#B282B-DL CS#18756-7 OH 28

1888

SAMPLE

CONDS,: EXTRACTED 1

1! i 'll i

A lli l,ii Jl , .1 .J .1

2-21-89 1: 5 DILUTION

i

UJ'ict

i ....... OC8.H18.0 ' 603 2,4-Dlr€THYLPHENCl\e2#4>1 <105-67-9>* ' ?

R WTlf5| '§ PK 187SANK 1£ 4PUR 888

r

1ll , 11 1I I I I l l i 1 1 i

aK<T•*.

Ci

UJ-Ju

SAMPLE MINUS LIBRARY . . . . _,1000 '

-1000 •

r

il 1(1 1 1 ii .M i i.l nit i. 1 1 ,

I T 1 T | \ • J T K

M/2 50 188

^--,----, T . 1 , T . ,— -, T-— , 1~-|- ^ -j-,—^™, . , T - - -T - - - ' 1— I T — 1 T*— ' T~" y « 1 • T— ' ,-"-- -T ! [ T -i I - T •

r •*•'/l

f -Q

10

CO•V•—•»

156 200 258 300 350

MID DUAL MASS SPECTRUM

*,}

48, 7 —

•

100.0-

\

.

58.8-

M/297.4-

f

'

48.7-

.

100,0-

50,0-

L"~-|

f

H--2

12/22/8SECONDSAMPLE;

683L^

,

!, pl-| ,4 *• | ' 1 n i *

^ Bf^yl50

' 1 ' i • i •

r- T-, i i . , -350

9 18:

'Jj

\T>DATA: GD009685A28 #501 BASE M/2: 187/ 18?

47:08 t 7:35 ENHANCED U8B 2N 8T> RIC: 692223,-' 739327.SPECTRUM

1ULDATA: UHEHHANCED *501 COMPUCHEM LABS, INC,

CC*309689 IMB262B-DL CS*18756-7 OH 28I2-4-DIMETHYLPHEHOL <G2*4> <105-67-9>

, 1i ,1

u

-p-n'T

ii Jit1 1 '

*T*100

! ji ' i

L . -L."I *T

- | • i • i

• | ' T •

400

> i . i ! 1 • i i i i i ' i • 1 > i > i ' i • i i 1 > i • i i i i i 1 ' i ' i i i

"' r ' i ' | • i • i ' i • i • j ' i ' i ' i T i ' | ' i • i • i • i ' | ' i ' r • i150 200 250 300

- 113152.

UJ7 CD

cto

- 115224. CL

^ ctKCt

'. ujQ.

r 113152. ctj; '/i

"T'T T-| i" j" f"|""T"i-|-|'-»""f» | M ' T" r"l' r T i" | "">""[' ' t r T ' I f '| ' "T ' ••f-r—[J

; r.Q

IOr.

r 116224. *

~

450 588 550 £00

1836

SAMPLE


12/22/89 18:47;88 t 8:81SAMPLE: 1UL CC»389e89 IO*B282B-OLCONDS.s EXTRACTED 12-21-89 1:

MID LIBRARY SEARCHDATA: GD885689A28 * 529ENHANCED O8B 2N 8T>

CS*18756-7 OH 20

BASE M/Z: 128RIC: 354815.

5 DILUTION

C18.H8

XAHK 1* 3

786 -

435 NAPHTHALENE f:G!2 <5l-20~3>*

i ll .Ji . Ilil, .. ..IT 1 ' ' ' ~ T- . ,/ - ^ j

1836

y •


III ..lil i,,ill

100 158i *

286

MID DUAL MASS SPECTR.Uf'

'•£.'5

DATA: GD06S6SSA28 *525 BASE M/2: 128/ 12812/22/89 ld;47;uu t 8:6i ENHANCED (18B 2H 8T-1 RIC: 423423, / 589951.SECOND SPECTRUMSAMPLE i 1UL CCS389689

DATA: UHEHHANCED »525 COMPUCHEM LABS, INC.IOHB282B-OL CS*18756-? OH 28

435) NAPHTHALENE ':«2*9> <91-26-3>

""i45, 8 H

i .In jL, in.., ilili,, JT 1 t 1 1 1 I-™1"-!"-! . " ' I '1"*-

188.8-j ' ' • . •

3

58.0-

- i Lii k _ , fr j• r~> | • i • i • i • i | • T •

H/2 50 10055. b-|

]*

49.8 ~-•*

....T,.., ..,. ... t..y , ! , . , . . , , , ,,...„., f..T...

100,0^

'

50. 0 ~

[]••?, 350 400

t

1

|

J,.1 UJ

CD'1

Oo-

r ??52e* Q-

j dlli ,[1,1

•I

h <iCi

'. UJ

• | 1 1 +\ ' 1 ' 1 ' 1 • 1 ' | ' I ' I ' 1 • 1 > | ' I • 1 ' T ' I " | ' 1 ' 1 ' I £,

150 200 250 300 £r ?7335. "I

' I ' l f [ T t ' I I ' I ' I ' l T I T I ' I ' l T l ' l ' 1 ' [ T T * T '

'. '-f<'. f -- Q

•£.10r.i"iTi

[ — ?S/5'x*?$

*-**

-' ! I'l ' I ' ! i 1 "'I' 1"' r •'' j i | i ' | T"i i"t i |-T-| • • T " | - t T i •( • • ! • | -T-T-T-, •••• r-f

458 566 55? P-00

IO

1855

SAMPLE


12/22/85 18:4?:68 t- 8:56SAMPLE: ILL CC*309689 IDSB202B-DLCOHDS,; EXTRACTED 12-21-89 1: •

MID LIBRARY SEARCHDATA: G0089685A28 * 550ENHANCED U86 2H 8T>

CS#18756-7 OH 28

BASE I1/Z; 142RIC: 275455,

DILUTION

Il.>.-i,I * T r -----1

C11.H10

Itf!"1

PUR 774 .

477 2-HETHYLNAPHTHftLEHE <Q2il3) <91-57-6>

1059

y •


M i.;l .. ,A nil i i. k <,i ^n I ...i|> . ..I

-1059M/2 58 100 158

t -•200

*T7~360 400

-.*-,'• 1

;

49,6-•

-

186,0-

:.,

56.6-

-

M/299.7-

-

49.8-•*

186,8-

5o,0-

H/2

MID DUAL MASS SPECTRUM DATA: GD069685A26 »558 BASE M/2: 142/ 1412/22/89 18; 47; 06 + 8:56 ENHANCED aefi 2H 0T: RIC: 29388?. / 36SECOND SPECTRUM DATA: UHENHAHCED *598 COMPUCHEM LABS, INSAMPLE: 1UL CC»339£89 ID#B282B-DL CS* 18756-7 ON 28

d??\2-METHYLNAPHTHALEHE <62*13> Ol-5?-6>! / i

'

h

ll. li . .11.1 ..L.l|... ill . ...I.., , , lliil. ^T ' l ' l I ' i ' I ' | T l I ' l ' l | ' ! ' | ' | T I T J ' l ' l T ! * T ' | ' | " I r | i | i J T I ' i ' |

J^ |j|f. .ll,L.Lj|ll. lIL^mjinliiirfil- | »i,- l,\ h* d

50 100 158 208 250 300

' "T "'• | ' 1 ' I ' 1 1 1 I | ' T '"I""l 1 l r j r T" ("-| ' i . t ] i j i | i | t rt | i y I | i 1 ' 1 I | I | T [ i , i [

' f r y T 1 > [ t" • ( • -T")" i •(•• t t ' l"i"| '"'1 | 'T'T | ' i 1 ' 1 ' '1 i 1 i l ' " ' " l ' 1 < '[ i | ' 1 ' T" i | '-T-|--T T~f T f 1

356 400 456 566 550 £00

As

515C,

r

:-

•

•

-

.

-

-

~

•

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-~

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t

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1,

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55132. 2

-I

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UJ-JLL

55000. Ct

r.'S

'£>IOr.

55192. °"J

COMPUCHEM I"??- INC.

12/22/8? ).?J4~J0? * 10! 25

MID LIBRARY SEARCHGD993683&20 9CFQ <10B 2H 0T>

10

8«SE M/H: 187R!C; 45375.

j I1.11. CCi s •'•£ "\f -' - '*• - ' ' '-"' ' ~ •"-' &"

•XoMfM C j** ~ " 1

<

C12.H101000 1

M WT 154tf,K 153

PIJP .35

1000 '

0 •

M--Z

i , 1 . . I i ! . ll i 1 l 1 i i . i

401 HCEHHPHTHENE <G31H0> <83-32-3>*

i .. . i. ,1 1SAMPLE MINUS LIBRARY

r

, - , ... „

4R 66

, ., ... .... i . .1

' , . - - - , - • , • , . . . , . — , . ,yy 166 126 140

.-, 1

• • - - * r- —186

1 1 ,

l

i i . . . i

1 86 200

42,0-

I

100.0-1

MID DUAL MASS SPECTRUM!2-'22--83 1.0? 47? 00 + 10525SECOND SPECTRUM

Ii

H---Z

<83-32-3>

OATAs GD003683A20 #688 BASE M/Zi 187-- 187ENHANCED i'10B 2N 0T) RIC: 46713. / 233193,DATAj UHENHANCED #688 COMPUCHEM LABS-

CS»18755-7 W 20

IO

- J166

Jf

* 1 ~>O1 A,^.

' 1 T T ' T T T' r 8488.

t-t* ' I ' I ' I ' T

156 200

UJ'-)'I^o•1LL

•IK•1

UJ-JLLz:•i

r.

r.co

250

1000

COMPUCHEM LABS.. IHC.

12/22/83 10s 47s 00 * 10s 388755-7

MID LIBRARY SEARCHDATAj GD893683A20 9 792ENHANCED O0B 2N 0T>

H

BASE M/CJ 168RIC; 125823,

• PIHH

•

C12.H8.0

B PK 1?|SANK 1

PUR 57"! •

'.•."Ui1. r C~-t .*""-• l _ , l£~'£l~'*S i i v L'iL'JIlv'

ii,, ii, i|,i, i iiii | , , . , ! ( . . i. i.476 DIBEHZOFURAH (Q3#13> <132-64-3> *

1 ll h 1 .hi . Il

... 1. 1, .. ,• * • • • • T • 'i • ' • • • • * • '

1 . . . 1


.ill i . i,,, I . i i ii 1 1 ,,,i ill , Ii , , .,

56 106 150 200

in

33.01

43,5 H

100.0

50.0-

M/Z

MID DUAL MASS SPECTRUM12'-'22'-'83 19:47? 09 + 19? 38SECOND SPECTRUM

iin_ CCf32968? IP#B2?2B-Dl475 PIBEHZOe-'jtJpH <<23*13) <132-64-3>

DATAs GD003683A20 #702 BASE M/Z: 168/ 168ENHANCED U9B 2H 0T>DATAj IJHEHWAHCED #702

CSK18755-7 OH 20

RIC; l 37727, / 265215,COMPUCWPM LABS.-

. ,. , ..ll... i 1 ili.lJllL..|.i., . rL ..ill '_ > r~i i i i F I i i i i i i i i ' i i i i U. . Ii ,r ^ ' i i

JinlLj

T | ' I ( I T T T - | " |1 ' - 28544.

I ' I i 1 i100 156

10

UJ

octCL

ctKctCi

UJ

K.

•o10rvoo

a.COMPUCHEM LABS.- INC.

12--22/83 10s47;00 * 11:96SAMPLE! 11"- CC»3?3589 IMB282B-DL

MID LIBRARY SEARCHDATA: GD085685A20 * 733ENHANCED U0B 2N 0T>

CS*l8?56-7 OH 28

BASE M./Z: 167RIC: 178455,

im-

:,uMP"

cis. Hie

I jl| '

^UR 5.! § .

1.909 "

M--Z

CWS,s EXTRACTED 12-21-89 1: 5 DILUTION

<

id il h i|il ll ii 1 1 , HI , . 1 ill i H ,.l . , u 1 h432 FUJORENE <Q3f 18) <36-73-7> *

1 i . II.,, . .il .1 ll


III! (Ill llll ,.!..! , HI 1,,, III 1 M M , , , | ,|! ....

1

II i . Ii , . T, , . , . . . ,

rr1

• - . . | - . - i > ' - I - . » • - . - ( ' I

(

1 .11 . I

t ^ - - - - V " •"•*•"-! •> '1*™*- -•"-+ ^ ---•* >-Y--«^«-Tr-1-*- »"'-~»-'1-,r"11* T11"1"* • • ' ' f ' *' T™1"*1 r— • r— T • 1— -» 1 -• 1 • T 1 • 1 — -T- — j r— — - - -T 1— i '—j T - - --T •-- i

50 100 159 200 250 306

'7.

100.0

MID DUAL MASS SPECTRUM12--22/83 10:47? 09 + U?96SECOND SPE

CS#1875S-7

DATA; GD003683A29 #733ENHANCED (19B 2H 0T>DATAj UNEHHAHCED #733

OH 20

BASE M/Z; 167/ 167RIC? 20493 1,/ 393615,COPP'JCHEM LABS- !kC,

- 26432.

r 26888.

M-Z T.y 100i T i I 'i I i I i I ' I ' I i I M '

UJ<D•I

OCtCk

CtKCtO

UJ-JCL

ct

r--Q

••a10fvco

jyy

a,

1822

SAMPLE


12/22-'85 18:47; 66 + 12:24SAMPLE: 1UL CC«38%89 ID*B282B-DLCOHDS.: EXTRACTED 12-21-85 1: !

CSB18756-7

MID LIBRARY SEARCHDATA: GD805685A28ENHANCED U0B 2H 0T>

OH 28'

BASE H/Z: 178RIC: 118355,

DILUTION

JLC14.H18

*AHK j

PUR ^2 \

444 PHEHANTHRENE <Q4#7> <85-0i-8>

il

1622

y

-10;M/2 60


166 126 140 160 186 200 220

*•'!

48,4-

100.01

50,0"

M/Z

MID DUAL MASS SPECTRUM12/22/83 19:47?99 + 12;24SECOND SPECTRUMC^Mpt p. iin rr^-jftOCRO IO#g'?P2B~DL

444 WEHFWrHRir£\Q«7r<85-01-8>

DATA; GD003683A20 #818 BASE M/Z: 178/ 178ENHANCED (106 2H BT> RIC; 113423,/ 279847,DATAj IIHPHWMHCED #«18 COMPHCMFM LAB^- IHC,

CS#187?6-7 04 29l 444v_y

i | , i, i i |

[JJIj liij' ,-^y-|l!j!NlTi1iVl!t 1 J^5f) 100 15«

1.1.nil,...!.... ....- i~-fJ—* -™

- 39888.

<7.t

UJCD1

OCtQ.

Cth-CtO

UJ-J

10F-00

1166

SAMPLE

S'l.H10

IN?\JR 449

1166

COMPUCHEM LABSLIBRARY SEARCH12/22/89 10:47:80 + 12:27SAMPLE: 1UL CC#309689 ID#B202B-DL CSI18756-7

DATA: GD009683A20 9 822ENHANCED (196 2N 0T>

ON 20

BASE M/E: 178RIC: 42111.

I lli .11. i 111 i >.l l.l i ..L jJ .ill ..l. jlllil -I . ..!•—•, 1 , - , • - I - i - . - . i . - T - r - . . -^ , - . r , r .

483 ANTHRACENE <Q4i8) <128-12-7>

ill j]SAMPLE MINUS LIBRARY

JL Jl

I ,ll I ,. 1 1 1 l.i I ly I I, k I -i,.li jJ ...i ili I!„,,.,11 I . I

-1166 J>——rM/E 59 199 159 298 250 380

ITt«J.

UJCD•1

OCt

UJ-JCLE

Q

•X.IOr.co

a.

C16.H22.D4

M UTB PK2AW

PIJR

1.022

-1022M/Z

COMPUCHEM LABS.. IHC, MID LIBRARY SEARCHDATA; GD093683A29 # 871

12/22/83 10!47;00 * 13;12 ENHANCED (108 2H 0T>: i'.'L CC#303683 !D#B202B-DL CS#18756-7 O1' 20

BASE M/Z; 149RIC: 37115,

11

1. , iii i f .ii 1 hi. . il .. ,. \ , . l ..., , 1 i - , ..i i . i i . i ,426 DI-N-BUTYL PHTHALATE (0419) <84-74-2> *

f't '"i475.

"

| l ll 1 1. i Ii i,.

!

.

iSAMPLE MINUS LIBRARY

, ! . , , ! , .ll I , , , l l i , ll ,, I .1,1 I I,., I . . . I . ,1 I , 1 .. I . I . .

100

"1—'—I-156 200

—,—,25P

MID DUAL MASS SPECTRUM DATA; GD003683A20 #871 BASE M/Z: 143/ 14312/22/83 10:47:09 + 13:12 ENHANCED «10B 2H 0n RIC: 37433,/ 122233,SECOND SPECTRUM DATftj UHENHANCED #871 COMPUCHEM LABS/ INC.S<W.E» i'JL CC#??3683 1D#?202B-DL CSI18756-7 OH 20

PHTHALATE (Q4#3> <84-74-2>

f)•7.t

U30.0 -i

\i

•

50.0-

4i

"

-

„

1 , 1,III.1

100.0-

•

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M/H 56 100 150 266 250 366 356

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COMPUCHEM LABS, INC. MID LIBRARY SEARCHDATA; GD903683A20 * 313

12/22/83 10:47:00 * 13:58 EHHpNCEO <10B 2H 0T>SAMPLE: 1'JL CC-*3?3583 ID*B202B-DL CS* 18755-7 ON 20CO'-JDS.: EXTR-CTEC 12-21-83 1: 5 DILUTION

BA^E M/Z; 43RIC: 184063,

,1|L .I. . . iJ _.jj. jt>ENTHCOSANE *

HEXATRIACONTAHE *

II 1

HEPTADECANE.. 2,6-DIMETHYL-*

100 156

523-33-2

CAS* 530-05-8

CAS* 54105-57-8

200 300 -^SR

tF-

COMFUCHEM LABS. INC.

12/22/83 10:47:00 + M:20SAMPLE: i'JL CC*3P9689 !D*B2?2B-DL CS*18755-~C7NOS,: EXT«-HCTET 12-21-33 1:

MID LIBRARY SEARCHDATA; QD003683A2? 9 346ENHANCED i'10B 2H 0T*

OH 20

F-t

BA^E M/Z; 43RIC: 137119,

A VV »

t)MP| CT

C22.H45

* WT 310B FK 57RANK 1If 3PM -ftPUR"652

C25.H521000 «

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i, ll L J.I. .|J. . ll. . .J.. .i« . ,.J .. . . .1. ^ .. . _ _ _

DOCOSANE* CAS* 523-37-0

1 i

11 l l .1 J • . - . - .

PENTACOSANE * CAS* 623-33-2

iUu J l l -I -I . . , . . . . , - - - .

HEXATRIACONTAHE * CAS* 630-06-8

56 166 150 266 256 300 356 466

•T>0

•

1'

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C13,H401000^

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12/22/83 10:47:00 * Ml 43 ENHANCED (10B 2H 0T> RICf 130047.SAMPLE: I'.'L CC*3?3683 ID*B202B-DL CS*l»7W-7 nN 2PCONDS.: EXTRACTED 12-21-33 Is 5 DILUTION

1l> L 1 1 1 .

i .1 . . . , . , t .. r r ., r T . .HEPTADECANE, 2.-6-QIMETHYL-* CAS* 54105-67-8

l| J .1 .d , v .., ^ r ,

OCTACOSANE* CAS* 630-02-4

l| j •! i , . . (. ...

100 150 286 256 366 356 466

04F-

Ul

•1

OCt

ctKCt

UJ_JCLz:

NQ

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CO

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COMPUCHEM LAB2, IHC.

12/22/83 10:47!06 + 15:15cttMpij:. JML rcJ>3836-Q !D*B2£2B-DL C-*l«755-7

r CWS.; EXTRACTED 12-21-33 If 5 DILUTION

MID LIBRARY SEARCHDATA; GD003583A20 K1007ENHANCED (IBB 2N 0T)

B«SE M/Z: 43RIC: 208533,

1C12.H25.0

.1 UT 1856 PK 43RANK ^ I

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1-OCTANOL, 2-BUTYL- *

k 1

CAS* 3313-02-8

C16.H33.CL1000

K WT 2503 *K *iEAKK iI -JdCCJSPUR" 6T*

HEXADECANE.. 1-CNLORO- *

ll. , ll . M , MI ' ' • ^^ I-'-'-^------\ (-

CAS* 4850-03-1

C18.H351000

M WT 2526 PK 412«HK^ t3

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\ n

ill ,., ...i.j

CAS* 7206-13-1

56 100 156 266 250 300

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COHPUCHEH LABS, INC.

12/22/89 18; 47: 66 + 16s 87SAMPLE; 1UL 00*309689 IO*6282B-DL

HID LIBRARY SEARCHDATA; GD889G89A26 #1664ENHANCED <18B _H 8T>

CS*18756-7 OH 28

BASE M/Z: 43RIC! 193279.

130? •

S<*FLE

C22.H46.01980 i

•-I MT 325B PK 43RANK 1§ 31572FUR 618

C17.H36.01080

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C28.H481080 i

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1-C OCOSANOL * CAS* 661-19-8

I

1 11 1 1f Ifl ill I. k .. ..

1-HEXADECAHOL, 2-HETHYL-* CAS* 2490-48-4r

HJ, ,5-EICOSEHE, 'EJ-* CAS* 74685-38-6

r

. j, J i l . , .50 166 150 266 250 366 350

C;OMPI

.1 WT 252j? PK 41RHNK 19 23346F! IR 639

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COMPUCHEM LABS.- INC,

12/22/83 10:47:00 * 15:35S»MDI_E: 1'JL CC*3?36?3 IP*B2?2B-[)LC7NDS.: EXTRACTED"l2-2l-«3~ 1? ~5

MID LIBRARY SEARCHDATA; GD093683A20 #1035 BASE M/Z: 43ENHANCED (10B 2N 0T> RlCj 123303,

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CAS* 7296-13-1

JL.3-OCTADECE»-€.. <E>- CAS* 7205-25-3

JL5-OCTADECENE, <E'-* CAS* 7206-21-5

UT100 156 400

•J;•0

RECEIPT PATE

VEMlrVO-ATILECC/HS WORKSHEET COHPUCHEM:

SAS: DUEOATE

JC 3 RC 3 DC<-T C

Jtt 3 R£E 3 DEC 3 C :t>

LOU LEVEL SOLID.EPA SOU E/SSSaaplo Prep Code- — -717Instrument Code-- ~ — -255.-•pound Li*t — — -497Surrogate Std—— --- 393Internal Std——— — 035

SDC. EPA* Dry Ut. Factor. X Moisture /_

«C/HS ANALYSISVolume* mixed: SNInternal Standard Volume Added.

Sample Volume Injected.-Ul

TDate of Sample Bottle Ana 1 vied /-. / J^/ / ftDFTPP Filename Tl^G / J-1f fi 2-f) Disk C ^Standard Filename H^ ?4 ' ~i.it &*-'? Pimk tSample Filename ^TWfci^Pg? /h*~V Disk C 3

ANALYST(S): Injection. Work-up

CC/HS REVIEU

CONDITIONCODE

Entry Code* OK,EA,JA, ES,AL,AH,PL,PH,FL,SBFH,NL,NH,YL,$L,SH,5M,YH

Non-Entry Code* IM,IL,IH.$0,01,0$,PC,OT,DAEO,IF.LA,DI.CO,MN,DU,NS

earc.VRe.ult«>Di*po*ition:

« of Peak* raund

« of Hit*: _

f of Surrogate Outlier*:

Quality Assurance Notice(*)>

« Notice* Required

«C/«S Review A^A Date //^ /

1 ^ 3 Complete

C 3 Reinjection required

C 3 Reestraction required

C 3 Dilute ( :M

C 3 Reinject Neat

C 3 Send to QA

t ll Auditor. .Date.

REPORT INTEGRATION rFinal Reportable Paekaaetal: 6 //

Total • of Inject ion* t(/ f, r> f -^

QA COMMENTS:

Initial*.

Initial*.

Date.• ••••iDate.FINAL REVIEW:

EPAIOOt (03/89)

18756 07 SPHPLE OPTP PPCKPGE 46S

ASSIGNED TO:

EXTRACTION WORKSHEETSemi Volaliles/Miscellaneous

CompuChem Laboratories Inc. DATE ASSIGNED \J • *^

PAGE OF

SAMPLENUMBER

3/0/7^

PREPCODE

CASE CLIENT

3-S*~

OC SAMPLE

TYPE

ss

ORIGNO

SAMPLEWEIGHT (g)

VOLUME (ml)

so.o

3o.o

•3,0.0

^o.o

3o o

30.0

30. 0

30-O

lo.o

30.0

FINAL EXTRACT VOL (MLSI

/NAQD PEST

AOJUSTEOPH

B/N ADATE

COMPT

At

--»

.11

JH

a

COMMENTS

US6"

V*M

SURROGATE

SPIKE

NO

AMTLOT

NO

AMTLOT

S-Vol Acid B/N Pert. Other Other

393

OS ml.3611O

3012 202110ml 10 ml

^ofeis Sofioi

MANUAL COUNTER t3<0/JO 8

FINAL VOLUME VARIFIED

SUPERVISOR REVIEWED


r.•o

UJCDcc;

oa:a.

LU-jLL21•1

rv

inF-.CO

COMPUCHEM * 009689 FILE: GD009689A20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE

CMP*

4946104116014214224744206204126224424364404604386O6603625410602446439475434608477495435611626416478425402479401605607476427428424

M/E

1529493128146146108146108451087011777136821391071229316218012812722510714216423619619616265163152138153184109168165165149

F

I

I

I

COMPOUND NAME SCAN

528

D4-1,4-DICHLOROBENZENE (IS* 419PHENOL (Qltt3>BIS(2-CHLOROETHYL)ETHER <Q12-CHLOROPHENOL (01*6)1,3-DICHLOROBENZENE (Ql«7>1,4-DICHLOROBENZENE (Ql»8>BENZYL ALCOHOL < 0.1*9 >1,2-DICHLOROBENZENE (QlttlO)2-METHYLPHENOL (Ql#ll)BIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOL <_1#13)N-NITROSO-DI-N-PROPYLAMINEHEXACHLOROETHANE (QlttlS)NITROBENZENE (31*16)OS-NAPHTHALENE <IS«2)ISOPHORONE (02*2)2-NITROPHENOL <Q2#3)2,4-DIMETHYLPHENOL (02*4)BENZO1C ACID (02*5)BIS(2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENOL (02*7)1,2,4-TRICHLOROBENZENE (02*NAPHTHALENE (02*9)4-CHLOROANILINE (02*10)HEXACHLOROBUTADIENE (02*11)P-CHLORO-M-CRESOL (02*12)2-METHYLNAPHTHALENE (Q2*13)D10-ACENAPHTHENE (I8*3)HEXACHLOROCYCLOPENTADIENE (2.4,6-TRICHLOROPHENOL (03*32, 4, 5-TRICHLOROPHENOL (03*42-CHLORONAPHTHALENE (Q3*5)2-NITROANILINE (03*6)DIMETHYL PHTHALATE (03*7)ACENAPHTHYLENE (03*8)3-NITROANILINE (03*9)ACENAPHTHENE (03*10)2.4-DINITROPHENOL (03*11)4-NITROPHENOL (03*12)DIBENZOFURAN (03*13)2,4-DINITROTOLUENE (03*14)2,6-DINITROTOLUENE (03*15)DIETHYL PHTHALATE (03*16)

685


DATE

AREA

227OOO

677OOO

355000

ID BY

QUANTREPORTVALUE

40. 04. 7

11. 5

64. 3

40. 0

37. 8go -T3 JO

6.9

9. 340. 0

2 A

1. 1

4 *"1

3. 4. O

X

REPORTEDAMOUNT(UC/KG)

•'•" -78OJBDLBDLBDLBDLBDLBDL

l^ -4-900vBDL

/ ""l-tOOOBDLBDLBDL

BDLBDL

•7 63001BOOOA5OJ

BDL,BDL

•'' 1-26OUBDLBDLBDL

"ty 1AOOJ

BDLBDLBDLBDL3DOJ

BDLBDLBDL

/*/- -tSOJBDLgnn i

2 |-> i^.U\J

BDLBDL

DETECT.LIMIT(UC/KS)

l7QQ

170017001700170017001700170017001700170017001700

170017001700

'-//•' B30O/ _v^ VXJ1

17OO4. / V/Vy

17001700170O1700170017001700

17001700830017OO93 OOOw WU

17001700830017008300Q'Qrsrs17004 "7f\f\i /UO

17001700


18756 87 Sfl/IPLE &PTP PPCKPGE 466

COMPUCHEM * 009689 FILE. GD009689A20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

CMP* M/E F

417 204432 166480 138467 188 I604 198443 169414 248433 284609 266444 178403 178426 149431 202459 240 I445 202415 149423 252405 228413 149418 228497 264 I429 149407 2524O9 252406 252437 276419 278408 276619 112 S612 99 S447 82 S448 172 S628 330 S496 244 S471 212 S456 216CHECKSUMS:

COMPOUND NAME

4-CHLOROPHENYL PHENYL ETHERFLUORENE (Q3*18)4-NITROANILINE (03*19)D10-PHENANTHRENE (18*4)4,6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE <O4*4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENE (04*5)PENTACHLOROPHENOL (04*6)PHENANTHRENE (04*7)ANTHRACENE (04*8)DI-N-BUTYL PHTHALATE (04*9)FLUORANTHENE (Q4«10)D12-CHRYSENE (18*5)PYRENE (05*3)BUTYLBENZYL PHTHALATE (05*43.3'-DICHLOROBENZIDINE (05*BENZO(A)ANTHRACENE (05*6)BIS(2-ETHYLHEXYL) PHTHALATECHRYSENE (05*8)D12-PERYLENE (18*6)DI-N-OCTYL PHTHALATE (06*2)BENZO(B)FLUORANTHENE (06*3)BENZO(K)FLUORANTHENE (Q6*4)BENZO(A)PYRENE (06*5)INDENO(1,2,3-C.D)PYRENE (06DIBENZO(A,H)ANTHRACENE (06*BENZO(G.H,I)PERYLENE (06*8)2-FLUOROPHENOL (88*1)D5-PHENOL (88*2)D5-NITROBENZENE (88*3)2-FLUOROBIPHENYL (88*4)2.4,6-TRIBROMOPHENOL (SS*5)D14-TERPHENYL (88*6)D10-PYRENE1.2,3.4-TETRACHLOROBENZENE

SCAN

816

1053

1218

AREA

417000

234OOO

2050OO

QUANTREPORTVALUE

3. 0

40. 0

IT-B-

'/.J -6r-51. 01. 4

40. 01. 3

40. 0

13. 411. 77. 06. 915. 47. 77. 7

REPORTEDAMOUNT(UG/KG)

BDLseouBDL

BDL3OOJBDLBDLBDL

, V WOJ^ 70-J

,- "-..30 J

* <° eojBDLBDLBDLBDLBDL

BDLBDLBDLBDLBDLBDLBDL

67.58.70.69.77.77.77.

%V.7.V.V.7.%

PAGE 2

LIMIT<UG/KG)

17OO17003300

830O17OO170O17008300170O170017001700

1700170O

1700170O1700

170017001700170O170017OO1700

BDL 17O

13335. 4719 2115000. 566. 9 43945.


DATE


18756 &7 SPMPLE DtfTfl PPCKPGE 465

COMPUCHEM * OO9689 FILE: CD009689A20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PACE 3

QUANTCC REPORT


72 619 2-FLUOROPHENOL (SS*1) 13.473 612 D5-PHENOL (SS*2) 11.774 447 D5-NITROBENZENE (SS*3) 7. O75 448 2-FLUOROBIPHENYL (SS*4) 6.976 628 2, 4. 6-TRIBROMOPHENOL (SS*5) 15.477 496 D14-TERPHENYL (SS*6) 7. 778 471 D10-PYRENE 7. 7

QUANTREPORTAMOUNT 7. ++ CONTROLSPIKED RECOVERY RANGE

20. 020. 010. 010. 020. 0IO. 010. 0

67.58.70.69.77.77.77.

25-12124-11323-12030-11519-12218-13717-125*

* ADVISORY SURROGATE ONLY++ 7. RECOVERY - QUANT REPORT VALUE / QUANT REPORT AMOUNT SPIKED X 100 '/.


FINAL EXTRACT VOLUME (ML) 30. OC DRY CC/MSx X WEIGHT X DILUTION X 33. 3

0.9 ML AMOUNT EXTRACTED(O) FACTOR FACTOR

>y>0. 9ML 30. OO -ffoO 5. 0 ^ *^'

X X X X 33. 3 « «»T-OUD0. 9 ML 30. 000

assmm^mmmmmmmaammmmmmmmmmmmmmmmmmmmmmatxmmmmmmmmmmmmmmmmmmmm*m*'S99mmmx9m»xst3t?zx^ =


1000 UL FINAL EXTRACT VOL (ML) CCMSX X DILUTION =


1000 UL 0. 9ML 5. 0X X » 10. OOO

500 UL 0. 9 ML


DATE

VERSION 8

(GC/MS/DATA REVIEWER)

18756 87 SPMPLE DPTP PPCKPGE 464


EPA SAMPLE NO.




Sample wt/vol: 30.0 (g/mL) £



Extraction: (SepF/Cont/Sonc) SONG

B202CContract: (2-881-REVS


GPC Cleanup: (Y/N) E pH: 8.2


Lab File ID: GH009690A20






108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 i,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol39638-32-9 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Methane120-83-2 2 , 4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2 , 4 , 6-Trichlorophenol95-95-4 2 , 4 , 5-Trichlorophenol91-58-7 2-Cnloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethyl Phthalate208-96-8 Acenaphthylene606-20-2 2 , 6-Dinitrotoluene

3803803803803803803803803805103803803803803801400180038038038013038038038014038038018003801800380380380

FORM I SV-1 1/87 Rev,



EPA SAMPLE NO.




Sample wt/vol: 30.0 (g/mL) £




GPC Cleanup: (Y/N) Ii pH: 8.2

B202CContract: (2-88)-REVS









99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2, 4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-01-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (l) _101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo (a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b) Fluoranthene207-08-9 Benzo (k) Fluoranthene50-32-8 Benzo(a) Pyrene193-39-5 Indeno (1,2, 3-cd) Pyrene53-70-3 Dibenzo (a, h) Anthracene191-24-2 Benzo (g,h, i) Perylene

180038018001800

3938038038059

18001800380380380180038038028038038038076038038077380380380380380380380

(1) - Cannot be separated from Diphenylamine


18756 07 SPttPLE DPTfl PPCKPGE 462



EPA SAMPLE NO.








GPC Cleanup: (Y/N) fi pH: 8.2


B202CContract: (2-88.-REVS









CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11.12.13.

COMPOUND NAME

ALDOLDIMETHYLPHENOL + UNKNOWNDIMETHYLPHENOL ISOMERDIMETHYLPHENOL ISOMERTRIMETHYLPHENOL ISOMERETHYLMETHYLPHENOL ISOMERTRIMETHYLPHENOL ISOMERETHYLMETHYLPHENOL ISOMERTRIMETHYLPHENOL ISOMERUNKNOWNUNKNOWNUNKNOWNUNKNOWN

RT

5.627.257.757.858.108.258.358.528.649.009.099.209.30

EST. CONC.

3803101000150110310310840460230190270540

Q

AJJJJJJJJJJJJJ

FORM I SV-TIC 1/87 Rev.

18756 07 SPttPLE DPTP PPCKPGE 461

-t_5v-&

COMPUCHEM LABSRIC COMPUCHEM DATA: GH6ei9e90A28 SCANS 307 TO 166012/22/89 9:25:08 OUT OF 307 TO 1600SAMPLE: 1UL CC*389690 JD*B202C CStl8756-7 OH 20COND5.: EXTRACTED 12-21-89 UNDILUTED ^056630

'-J'•£>1-

15*1 15*2

55*2- 55*3 ]

396 '.

15*3 55*5

55*4 031t 15*4

RIC

628

514

469

4J.

565 760

wUoj

820

55*6 15*5

55*7 15*6

963

875

1058

1225

1333 1503

UJ

<1

OCC

Cth-

Q

UJ

rv

•oinr.co

4906:04

6009:05

80612:07

109015:09

120018:11

140021:13

160024:14

SCANTIME

QUANTITATION REPORT FILE: GHOO9690A20DATA: GH009690A20. TI12/22/89 9:25:OO / /SAMPLE: 1UL CC*3O969fr ID*B202C CS*18756-7 ON 20CONDS.: EXTRACTED 12-21-89 UNDILUTEDSUBMITTED BY: 20 ANALYST: 643

AMOUNT=AREA * REF. AMNT/<REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHLOROBENZENE (18*1)2 610 PHENOL (Ql*3) <!O8-95-2>3 411 BIS(2-CHLOROETHYL)ETHER (Ql*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-B>5 421 1,3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1,4-DICHLOROBENZENE (01*8) <lO6-46-7>7 474 BENZYL ALCOHOL (01*9) <100-51-6>8 420 1,2-DICHLOROBENZENE (01*10) <95-5O-l>9 620 2-METHYLPHENOL (Ql*ll) <93-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (Ql»12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2.4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZO1C ACID (02*5) <65-85-0>20 410 BIS(2-CHLOROETHOXY)METHANE (O2«6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1,2, 4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (Q2*12) <59-50-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 *495 D10-ACENAPHTHENE (18*3)29 435 HEXACHLOROCYCLOPENTADIENE (Q3*2) <77-47-4>30 611 2,4,6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 5-TRICHLOROPHENOL (03*4) <95-95-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-58-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 8605 2,4-DINITROPHENOL (03*11) <51-28-S>39 6O7 4-NITROPHENOL (03*12) <10O-O2-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2,6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (Q3*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (Q3*17> <7O05-72-3>45 432 FLUORENE (Q3*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>

18756 07 SPHPLE OPTP PPCKPGE 459

NO474849505152535455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME*467 D10-PHENANTHRENE (IS#4)604 4, 6-DINITRO-2-METHYLPHENOL (Q4*2) <534-52-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-3O-6>414 4-BROMOPHENYL PHENYL ETHER <Q4#4) <101-55-3>433 HEXACHLOROBENZENE (04*5) <118-74-1>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <B5-01-8>4O3 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*459 D12-CHRYSENE (18*5)445 PYRENE (05*3) <129-00-0>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3,3'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO(A)ANTHRACENE (05*6) <56-55-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (05*7) <117-81-7>418 CHRYSENE (05*8) <218-01-9>»497 D12-PERYLENE (18*6)429 DI-N-OCTYL PHTHALATE (06*2)407 BENZO(B)FLUORANTHENE409 BENZO(K)FLUORANTHENE406 BENZO(A)PYRENE (O6*5) <50-32-8>437 INDENOd, 2, 3-C, D)PYRENE (Q6«6) <193-39-5>419 DIBENZO<A, WANTHRACENE (06*7) <53-70-3>408 BENZO(C, H, DPERYLENE (06*8) <191-24-2>#619 2-FLUOROPHENOL (88*1)#612 D5-PHENOL (88*2)#447 D5-NITROBENZENE (88*3)#448 2-FLUOROBIPHENYL (88*4)#628 2, 4, 6-TRIBROMOPHENOL (88*5)*496 D14-TERPHENYL (88*6)*471 D1O-PYRENE456 1, 2, 3, 4-TETRACHLOROBENZENE

<117-84-0>(O6*3) <2O5-99-2>(06*4) <207-08-9>

M/E SCAN TIME152 421 6:2394 NOT FOUND93 NOT FOUND128 NOT FOUND146 NOT FOUND146 NOT FOUND108 NOT FOUND146 NOT FOUND108 NOT FOUND45 NOT FOUND108 458 6:5670 NOT FOUND117 NOT FOUND77 469 7: 06136 530 8:0282 NOT FOUND139 NOT FOUND107 5O3 7:37122 514 7:4793 514 7:47162 NOT FOUND

REF1

RRTOOO

METHA BV

AREA(HGHT)305844.

AMOUNT40.OOO NG

XTOT4. 67

1.088 A BB

1515

151515

0.1.

0.0.0.

885000

94997O970

A VBA BV

A*VBA VVA VV

115088.

14380.837149.

3O6476.3O8836.28304.

13.377 NG

1. 196 NG40.OOO NG

36.650 NG81.O83 NG2. 855 NC

1. 56 /-

0. 14:4. 67

4. 28 '>'9. 46..£-0. 33 i-

18756 07 SHMPLE DflTfi PPCKPGE 45S

NO2223242526272829303132333435363738394041424344454647484950515253545556575859606162636465666768697071727374757677

M/E180128127225107142164237196196162651631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522522522762782761129982172330244

SCAN TIMENOT FOUND532 8:04

NOT FOUNDNOT FOUNDNOT FOUND593 8: 59688 10:25

NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND649 9: 50NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND705 10:41NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND736 1 1 : 09NOT FOUND820 12: 25NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND875 13: 15NOT FOUND1058 16:02NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND1060 16:03NOT FOUND1225 18:33NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND322 4 : 53396 6 : 00469 7:06628 9:31759 11:30963 14:35

REF

15

1528

28

28

28

47

47

57

57

64

11

15282857

1.

1.1.

0.

1.

1.

1.

1.

1.

1.

1.

0.0.0.0.1.0.

RRT

OO4

119000

943

025

070

OOO

067

000

002

000

765941885913103910

METH

A

AA

A

A

A

A

A

A

A

A

AAAAAA

VV

BBVV

BV

BB

BB

VV

BV

W

VV

BB

BBBVBVBBBBVV

AREA(HGHT) AMOUNT

89824. 3. 459 NG

50412.421308.

13580.

18928.

22836.

442338.

130770.

264128.

21369.

212820.

971O18.9934O4.515126.652436.144668.416500.

3. 67O NG40.OOO NG

2.733 NG

1.016 NG

1.546 NG

4O.OOO NG

7. 425 NC

4O.000 NG

1.999 NG

40.000 NG

87.942 NC85.977 NC43.143 NC42.916 NC98.348 NG53.764 NC

XTOT

0. 40

O. 434. 67

0. 32 ,

0. 18

4. 67

0. 87

4. 67

10. 2610. 035. 035. 01

11. 486. 27

18756 07 SAMPLE DPTP PPCKPGE 457

NO M/E SCAN TIME REF RRT METH78 212 948 14:22 57 0.896 A VV79 216 NOT FOUND

NO RET<L) RATIO RRT(L) RATIO AMNT1 6:22 1.00 10.000 0.10 40.002 6. OO 10. OOO3 6:04 10.0004 6: 09 10. 0005 6: 19 10. 0006 6: 24 10. 0007 6: 34 10. 0008 6:37 10.0009 6.44 10.00010 6:46 10. OOO11 6.55 1.00 10. OOO 0.11 13.3812 6: 56 10. 00013 7:02 10.00014 7:07 1.00 10. OOO 0.09 1.2015 8:02 1.00 10. OOO 0.10 40.0016 7: 25 10. 00017 7:33 10.00018 7:36 1.00 10.000 0.09 36.6519 7:45 l.OO 50. OOO 0.02 81.0820 7:44 1.01 10. OOO 0.10 2.8521 7: 51 10. 00022 7: 58 10. 00023 8: O3 1. OO 10. OOO 0. 10 3. 4624 8:08 10. OOO25 8: 18 10. 00026 8:48 10.00027 8:58 1.00 10.000 0.11 3.6728 1O:25 l.OO 10. OOO 0.10 40. OO29 9: 17 10. 00030 9. 24 10. OOO31 9: 26 50. 00032 9: 38 10. OOO33 9: 48 1. 00 50. OOO 0. O2 2. 7334 10: 05 10. OOO35 10: 13 10. 00036 10:22 50.00037 10:27 10.00038 10:30 50.00039 10.35 50.00040 10:41 l.OO 10.000 0.10 1.0241 10:43 10.00042 10: 11 10. 00043 11: 04 10. 00044 11: 09 10. OOO45 11:09 1.00 10.000 0.11 1.5546 11: 12 5O. OOO47 12:25 1.00 10. OOO 0.10 40.0048 11: 16 50. 00049 11: 18 10. 00050 11: 48 10. 00051 12: 01 IO. OOO52 12: 15 50. OOO

AREA(HCHT)398030.

AMNT < L )40.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.5O.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.50.50.5O.

0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000OO00

R.1.

0.

0.1.

0.0.0.

0.

0.1.

0.

0.

0.

1.

AMOUNT47. 823 NG

FAC R. FAC(L)000

3O1

014000

293295027

086

048000

026

036

043

000

1.1.1.1.1.1.0.1.1.1.1.0.0.0.1.0.0.0.0.0.0.0.1.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.0.0.1.0.1.0.1.0.0.0.0.0.

000575419426574635748493046O47125929873574OOO7812184001824743273892413322223616560003744O5399318472569807257200139295769335269417659402216000130573252280130

XTOT5. 58

RATIO1.

0.

0.1.

0.1.0.

0.

0.1.

0.

0.

0.

1.

00

27

02OO

736206

07

0700

05

O2

03

00

18756 Q7 SHMPLE DPTP PPCKPGE 456

NO535455565758596061626364656667686970717273747576777879

RET(L)12:2712:13:14:16:14:15:16:16.16:16:18:17.17:17:18:21:21:22:4:5:7:9:

11:14:14:9:

3116060425190103060639015O53324448415259053O30372339

RATIO RRT(L)10. 000

1.

1.

1.

1.

1.1.1.1.1.1.1.

00

00

00

00

00000000000000

10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.10.0.0.0.0.1.0.10.1.

OOOOOO000OOO000000000000000000000000OOO000000OOOOOO000742948875906118907000000

RATIO

0.

0.

0.

0.

1.0.1.1.0.1.0.

11

10

10

10

O3990101990009

AMNT

7.

40.

2.

40.

87.85.43.42.98.53.47.

42

00

00

OO

94981492357682

AMNT(L)50. 0050.50.50.40.50.50.50.5O.50.50.40.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.

00000000000000OO0000000000000000000000000000000000OO

R.

0.

1.

0.

1.

2.2.0.1.0.1.1.

FAC R. FAC(L)1. 217

237

OOO

065

000

540598492239275262206

1.1.0.1.1.0.o.1.1.1.1.2.1.1.1.1.1.1.1.1.0.1.0.1.1.0.

12359386000060082819409161918000020715727100921804702744451157144314017326O631

RATIO

O. 15

1. OO

0. 04

1. 00

1. 761. 720. 860. 861. 971. 080. 96

18756 07 SAMPLE &PTP PPCKPGE 455

IT'

1131

COMPUCHEM LHBS; IHC.

i2-'22-'83 3i25{99 * 6; 56S'JIPLEj IL'L CC*3_'??9p"!6lfB2?2CCO S.'. EXT06CTE6" 12-21-83""

MID LIBRwRt 5EHRCHOwTw; GH00363.tH20 If 458EHHwNCEO a96 2H 0T>

OH 29

B«SE M.-c; 197R!Cs 394127

C7.H8.0

PUR $?9 .

522 4-METHrlPHEHOL (Ql*13> <195-44-5> *

1191SHMPLE MINUS LIBRARY

-1101loo 15o

nin

1 -

43,9-

100,9-1

59,9-

M-

MID DUHL MuSS SPECTRUM).2--22--83 3:25:99 + 6:56SECOND SPECTRUM

QHTH; QH993639H29 #458 BASE M.-c: 197--' 197ENHANCED l'19B 2H 9T> RIC: 339233,-- 353423,OATH; UHEHH«NCED #458 COMPUCHEM (.»<*$. INC,

HI.

Hi.

(Ql*13>

1 I l I 1 I 1 i I

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10

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r


12/22--83 3s 25s 99 * 7; 37

*~W 12-21-33 UNDILUTED

MID LIBRARY SEARCHDATA; GH993639A29 9 593ENHANCED (19B 2N

CSI1S7SS-7 OH 29

> ,M .Mil, . .,lm. T»in.l! In. ... , ,. ».-,.,.S93 2/4-DIMETHYLPHEHOL (Q2H> <195-?7-3>*

BASE M/Z: 197RICs 788473.

C8.H19.0M l-r

i9 4PUR 837

1992

o •


.,1,1 I H.I ll.,,, .11,1 ..II ,,

-1992 '. • , • r-M--Z So 199 150 299

IOt

MID DUAL MASS SPECTRUM DATA: QH993639A29 #593 BASE M/Zs 197-- 19712--22--83 3:25:99 + 7:37 ENHANCED a 98 2N an RIC: 843775,-- 884735,SECOND SPECTRUM DHTPJ UNENHuHCED #593 COMPUCHEM LABS; INC,SAMPLE:)" i'-'l CC&393S39 IP&B292C CS&1875E--7 0UJ 29

/ ??7 2.-4-DIMETHY!.PHEHOL (Q2»4> <195-£7-3>

3"r]

143.4-

199.9-

59.9-

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1 1 ' T ^ 1 ' ' rT"'T'~|

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1

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12/22/33 3?25s00 * 3;94SAM°LE: I'JL CC&309E-30 !DftB202CCO^DS.J E'XTDpCTED 12-21-83" WDI LUTED

C-$»1875E--

MID LIBRARY SEARCHDATA: GH903630A29 9 532ENHANCED (10B 2N 0T>

ON 20

BASE M/Z; 128RICs 188327.

C10.H8100Rs &m699

433 NAPHTHALENE <G2I3> <31-20-3>*

1998

-1998M/Z 40


199 129 140 160 189

33.6 ~

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43.8-

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100.0-*

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MID DUAL MttSS SPECTRUM12/22/83 3:25:00 + 8:94SECOND SPECTRUM«jK(pi c. mi fxcii'5(*ocjOR T r)a{}'W?r.y™1" <92>9> *"**

i i ii i,iii. .i i ,i u i i , , , i , .,i ... i.> i i 1 1 1 1 1 1 1 1 1 1 1 1 ii i

i ii l l . iij,l.,lldU,fc i.i,t p. i p. _ j — ._-j ..fj-j — i_-j. ._ ji. 1 ,,-f. f |_ |.

DATA: GH993639A29 #532 BASE M/Z: 128/ 12ENHANCED a 06 2N 0T> RIC; 13251 1./ 31DATA- IJHENHANCED #532 COMPUCHEM LABS- IN

f c;iii $5— <?C— 7 OH "JP

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?_-?,_aq

MID LIBRARY SEARCHDATA: GH003639A29 9 533ENHANCED <10B 2N 0T?

CSI187K-7 OH 20

BASE M/Z; 142RIC: 158207,

r .-.' «. _ . , C« • ^n.-'CU J.i ii— SJ 'jnuiUviSl'

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1 ll, ,,|l.l. ,r Ml ,1,1 .„. 1 , ,-,- 1,,

477 2-METHY1NAPHTHALENE (02113) <91-57-6> *


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"i "•'"60 100

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120 140• t '

169 ISo•"i '••20y

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100.0

50,0-

100.0

59.0-

MID DUHL MwSS SPECTRUM DATA: GH903630A20 #533 BASE M/Z: 142/ 142

SECOND SPECTRUM '" DATA: UNENHANCEO #533 COMPUCHEM UBS.. INC,SAMPLE:\111 CC#303S30 ID#5202C CS# 18755-7 OH 20

477]2-METHVLNH»MTHALENE (G2#13) <31-57-5>— •>. •>•-

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476 JDIBENZOFURfcH <Q3#13> <132-64-3>

DATH: GH003630A20 #705 BASF M/Z: 168/ 168ENHANCED (1.9B 2N 9T> RIC; 71673,/ 15564DH.TM. UNENHpHCED #705 COMPI'CWEM LABS- INC.

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LAB INSTRUCTIONS

RECEIPT DATE 12/20/89 CASE* 18756 7

SEMI-VOLATILEGC/MS UCRkSHEET COMPUCHEM*: 309690

DUE DATE

JC 3 R C 3 DC ] C

J£ C 3 Re C ] D2 C . {

GC/MS, S-V, LL S/S; SOU 2/83

SAMPLE ID*: B202C Dry Ut . ./ >\"

GC/MS ANALYSIS ___-—-.A? " --- _Volumes m i x e d ; BN ' u 1 Acid ulInternal Standard Volume Added.M i x e d Sample Volume Injected_

Sample P •? p Code • ' ~Instrument C c c e i E rCompound List 1 ? ~Surrogate Std 7?"Internal Std 03:

'/. Moist LI re

Date of Sample Bottle Ana 1 v zedDFTPP FilenameStandard F i 1 enameSample Filename

ul//

Disk C }Disk C >

Disk C }

DEC 2 7 1989 !j1L 1 1 i v^^v . ~- .. i

ANALYST(S):

GC/MS REVIEU

CONDITIONCODE

Injection

Codes OK,EA,JA, ES,AL,AH,PL,?H,FL, "FH,NL,NH,YL,SL,SH,SM ,YH

n-Entry Codes IM,IL,IH,SU,CT,CS,°C,OT D/ED, IF-, LA , DI , CO, RN , DU, Ni

Di spos i t i onExtrarieous Peak Search Results:

* of Peaks Found: ( /:?-

* Of Hits: ''

# of Surrogate Outliers:.

Q u a l i t y Assurance Notice(s)

* Notices Required

GC/'MS Review xV"7M Date 2.2-/

C ] Comp let e

[ ] Re i n j e c t i o n required

C ^TR eextraction ~eq.i:rei

C ] Dilute f 1 )

C ] Rein j ect Neat

[ 3 Send to QA

Auditor t'">"*•- Date / L / ' / "*'/

REPORT INTEGRATIONF i n a l Reportable Package's)

Total of

QA COMMENTS

FINAL REVIEW

I n i t i a l s ,

I n i t i a l s

Dat e.

Dat eA C 1 0 •". '^ < 0 :

18756 07" SAMPLE DflTrt PPCKPGE 42'

ASSIGNED TO

SAMPLENUMBER

3/0/76

PREPCODE

. O.rO.V

EXTRACTION WORKSHEETSemi - Volaliles/ Miscellaneous

CompuChem Laboratories Inc. DATE ASSIGNED U

PAGE OF

CASE1

8 act A

530IB

CLIENT

*

TA*

Baoaa

OC SAMPLE

TYPE

5£.

15S

B

ORIGNO

SAMPLEWEIGHT (g)

VOLUME (ml)

3.QQ

20. 0

10.0

•30.0

•30.0

30.0

30.0

30 O

30.0

FINAL EXTRACT VOL (MLS)

sv/N

05,,

ACID PEST

ADJUSIIDPH

B/NDATE

COMPT

JLl

O -

COMMENTS

SURROGATE

SPIKE

NO

AMTLOT

NO

AMTLOT

S Vc4 Acid B/N Pe*t Other Otter

393

05 mlJOT TO

3012 2021

10ml 10ml.SOfclS 3O809

MANUAL COUNTER

FINAL VOLUME* VARIFIED

SUPERVISOR REVIEWED


'M

UJ(0a

ctCL

1K1

UJ-JCLEl•I'/l

r.

•£•IT^f -•JO

COMPUCHEM # OO9690 FILE: GHOO9690A20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE 1

CMP*

494610411601421422474420620412622442436440460438606603625410602446439475434608477495435611626416478425402479401605607476427428424

M/E

1529493128146146108146108451087011777136821391071229316218012812722510714216423619619616265163152138153184109168165165149

F

I

I

I

COMPOUND NAME SCAN

530

D4-1,4-DICHLOROBENZENE (IS* 421PHENOL (01*3)BIS(2-CHLOROETHYL)ETHER (Ql2-CHLOROPHENOL (Ql*6>1,3-DICHLOROBENZENE (01*7)1,4-DICHLOROBENZENE (Q1#S>BENZYL ALCOHOL (Ql*9>1,2-DICHLOROBENZENE (QlttlO)2-METHYLPHENOL (Qlttll)BIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOL <Q1#13>N-NITROSO-DI-N-PROPYLAMINEHEXACHLOROETHANE (Ql*15>NITROBENZENE (Ql»16>D8-NAPHTHALENE (15*2)ISOPHORONE (Q2»2>2-NITROPHENOL <Q2«3;2,4-DIMETHYLPHENOL <Q2*4>BENZOIC ACID <Q2«5>BIS < 2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENOL <Q2#7>1, 2, 4-TRICHLOROBENZENE <Q2«NAPHTHALENE (Q2#9>4-CHLOROANILINE (Q2tlO>HEXACHLOROBUTADIENE (Q2#l1)P-CHLORO-M-CRESOL «J2#12)2-METHYLNAPHTHALENE (Q2#13>D10-ACENAPHTHENE (IS«»3)HEXACHLOROCYCLOPENTADIENE <2,4,6-TRICHLOROPHENOL (Q3#32,4,5-TRICHLOROPHENOL (03#42-CHLORONAPHTHALENE (Q3#5)2-NITROANILINE (Q3«6>DIMETHYL PHTHALATE (Q3#7)ACENAPHTHYLENE (03*8)3-NITROANILINE (Q3#9)ACENAPHTHENE (Q3*10>2,4-DINITROPHENOL (Q3#ll)4-NITROPHENOL (Q3*12)DIBENZOFURAN (Q3#13)2,4-DINITROTOLUENE (Q3#14)2,6-DINITROTOLUENE (Q3#15)DIETHYL PHTHALATE (Q3*16)

688


AREA

306000

837000

421000

:D BY

QUANT REPORTEDREPORT AMOUNTVALUE (UG/KC)

40. 0BDLBDLBDLBDLBDLBDLBDLBDLBDL

13. 4 -' *TOBDLBDL

-l.-g 4QJ40. 0

BDLBDL

36. 6 / *"• :^2QQ81. 1 Z7QO

BDLBDL

3. 4 f"*^ -HrOJBDLBDLBDL

3. 7 /*•'-• tSOJ40. 0

BDLBDLBDLBDL

2 *7 OA I. r VUU

BDLBDLBDLBDLBDLBDL

1.0 V -3SJBDLBDLBDL

s?^

DETECT.LIMIT(UG/KG)

33C33033033033033033033033033033033O330

33033033O

33033033033033O330330330

3303301700330170033033O170O33O1700170O330330330330

(GC/MS DATA REVIEWER)/

DATE -A i, -'rf

18756 97 SHMPLE C-PTP PPCKPGE 423

COMPUCHEM tt 009690 FILE: GH00969OA20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE

CMP* M/E F COMPOUND NAME SCAN

417 204 4-CHLOROPHENYL PHENYL ETHER432 166 FLUORENE (03*18)480 138 4-NITROANILINE (03*19)467 188 I D10-PHENANTHRENE (IS*4) 820604 198 4,6-DINITRO-2-METHYLPHENOL443 169 N-NITROSODIPHENYLAMINE (04*414 248 4-BROMOPHENYL PHENYL ETHER433 284 HEXACHLOROBENZENE (04*5)609 266 PENTACHLOROPHENOL (04*6)444 178 PHENANTHRENE (04*7)403 178 ANTHRACENE (04*8)426 149 DI-N-BUTYL PHTHALATE (04*9)431 202 FLUORANTHENE (04*10)459 240 I D12-CHRYSENE (IS*5) 1058445 202 PYRENE (05*3)415 149 BUTYLBENZYL PHTHALATE (05*4423 252 3,3'-DICHLOROBENZIDINE (Q5#405 228 BENZO(A)ANTHRACENE (05*6)413 149 BIS(2-ETHYLHEXYL) PHTHALATE418 228 CHRYSENE (05*8)497 264 I D12-PERYLENE (IS*6) 1225429 149 DI-N-OCTYL PHTHALATE (06*2)407 252 BENZO(B)FLUORANTHENE (06*3)4O9 252 BENZO(K)FLUORANTHENE (06*4)406 252 BENZO(A)PYRENE (06*5)437276 INDENO(1,2, 3-C,D)PYRENE (06419 278 DIBENZO(A,H)ANTHRACENE (06*408 276 BENZO(C,H,I)PERYLENE (06*8)619 112 S 2-FLUOROPHENOL (SS*1)612 99 S D5-PHENOL (SS*2)447 82 S D5-NITROBENZENE (SS*3)448 172 S 2-FLUOROBIPHENYL (SS#4)628 330 S 2, 4,6-TRIBROMOPHENOL (SS*5)496 244 S D14-TERPHENYL (SS*6)471 212 S D10-PYRENE456 216 1,2,3,4-TETRACHLOROBENZENECHECKSUMS:

13335. 4742

AREA

442000

264OOO

213000

QUANTREPORTVALUE

1. 5

4O. 0

7. 4

40. 0

2. 0

40. 0

87. 986. 043. 142. 998. 353. 847 8

REPORTEDAMOUNT(UG/KC)

BDL>- 5OJBDL


• -,- -esojBDL

BDLBDLBDLBDL

77 -6TJBDL


88.86.86.86.98.108.96.

BDL

DETECT.LIMIT(UG/KG)

3303301700

170033033O3301700330330330330

330330

•;v-r7e33033O33O

33033033O33033033O330

7.'/.'/.7.'/.V.7.

33

2483000. 856. 6 5851.


DATE


1S756 87 SPMPLE C-PTP PPCKPGE

COMPUCHEM * OO9690 FILE: GH009690A20 COMPOUND LIST 172SEMI-VOLATILE - LOW LEVEL SOLID

PAGE 2

QUANTCC REPORT


72 619 2-FLUOROPHENOL (SS*1) 87.973 612 D5-PHENOL <SS*2) 86.074 447 DS-NITROBENZENE (SS*3) 43. 175 448 2-FLUOROBIPHENYL (SS*4) 42.976 628 2,4,6-TRIBROMOPHENOL (SS«5) 98.377 496 D14-TERPHENYL (SS*6) 53. 878 471 D10-PYRENE 47. 8

QUANTREPORTAMOUNT % +•»• CONTROLSPIKED RECOVERY RANGE

100 01OO. 05O. 050. 0

1OO. O50. 050. 0

88.8686.86.98.108.96.

25-12124-11323-12030-11519-12218-13717-125* X

* ADVISORY SURROGATE ONLY•»••»• % RECOVERY - QUANT REPORT VALUE / QUANT REPORT AMOUNT SPIKED X 1OO '/.


FINAL EXTRACT VOLUME (ML) 3O. 00 DRY GC/MSX X WEIGHT X DILUTION X 33. 3 =

0.9 ML AMOUNT EXTRACTED(G) FACTOR FACTOR

0. 9ML 30. OC -4-rtJO 1.0 3*x X X X 33. 3 - .33r-300

0. 9 ML 30. OOC


1000 UL FINAL EXTRACT VOL (ML) GCMSx X DILUTION =


1000 UL 0. 9ML 1. 0x X = 2. 000

500 UL 0. 9 ML

VERSION 8


DATE




EPA SAMPLE NO.





Level: (low/med) MED


Extraction: (SepF/Cont/Sonc) SONG

GPC Cleanup: (Y/N) N. pH: 8.5

B202TARContract: (2-88)-REVS



Lab File ID: GRD09687A08




Dilution Factor: 5 . 0


i nQ_Qcr_o_____

111-44-495-57-8541-73-1106-46-7100-51-6

95-48-7

106-44-5621-64-767-72-1

78-59-1Q Q_'7 C_C______

105-67-9

1 1 1 — Q 1 — 1 .......

120-82-1

- n*r_y,i-7_Q_____1UO — ** /— O— — — — —

59-50-791-57-6

"7 "7 /1"7—/1— — — — — —Q Q n£_. o _ ___

Q C QK — yl— — — _ — —

•~t A Q Q £ _ Q _ _ _ _ _

— — — Phenolbis (2-Chloroethyl) Ether

---2-Chlorophenol---1 f 3-Dichlorobenzene— -1 f 4-Dichlorobenzene

Benzyl Alcohol— — — 1 r 2—Dichlorobenzene— -2-Methylphenol——•bis ( 2— Chloroisopropyl ) Ether___4 -Me thy Iphenol

N— Mi t" T"o^o— Di — n— PT*O.QVI Ami ne— -Hexachloroethane———Nitrobenzene---Isophorone— — — 2— Nitrophenol---2 f 4-Dimethylphenol

, . . _ j-»,u T ^ .U \ \M 4- W

_ . _ . , . , •.

--— 1 , 2 , 4-Trichlorobenzene

A r* iW T ' 1 '— — — 4— cnioroanii ins__ , - i ,. , .

— — — 4— chloro— 3 —Me thy Iphenol— —2 -Methyl naphthalene

• i v i c m ' K ' l v^ T— — — 2 , 4 / o— i ricnioropnenoi

_ - _ . . • T '— — i — Nitroann me_ _ _ n i -me^¥ Y\\j 1 DH +• H a 1 a -t- £a

_ , . , ^— — — Acenapntny iene_ _ _ . . . ,_ -.— i , b uini trotoiuene

330000280000280000280000280000280000280000110000028000014000002800002800002800002800002800002000000130000028000028000028000034000028000028000028000056000028000028000013000002800001300000280000280000280000

UUUUUU

U

UUUuu

uuuu

uuu

uuuuuuuu

FORM I SV-1 Rev.

IS 756 97 SPMPLE C'PTP PPCKPGE 4 2 0


EPA SAMPLE NO,








GPC Cleanup: (Y/N) N pH: 8_-_










99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2 , 4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-01-6 4-Nitroaniline534-52-1 4 , 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 ButylbenzylphthalateJ91-94-1 3 , 3*-Dichlorobenzidine56-55-3 Benzo (a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b) Fluoranthene207-08-9 Benzo (k) Fluoranthene50-32-8 Benzo (a) Pyrene193-39-5 Indeno(l, 2 , 3-cd) Pyrene53-70-3 Dibenz o( a, h) Anthracene191-24-2 Benzo(g,h, i) Perylene

13000002800001300000130000051000280000280000280000100000130000013000002800002800002800001300000280000280000280000280000280000280000550000280000280000280000280000280000280000280000280000280000280000

(1) - Cannot be separated from Diphenylamine

FORM I SV-2

IS'756 97 SPMPLE L'PTP PPCKPGE 41 •=•



EPA SAMPLE NO.








GPC Cleanup: (Y/N) E pH: 8.











CAS

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.

NUMBER

620-14-4

104-55-2

28715-26-6

24599-58-4

544-76-3

544-76-3629-78-754105-67-8544-76-3

COMPOUND NAME

BENZENE, 1 -ETHYL- 3 -METHYL-UNKNOWN2-PROPENAL, 3-PHENYL-UNKNOWNUNKNOWNBENZOFURAN, 4 , 7 -DIMETHYL-UNKNOWNBENZENE, l,4-DIMETHOXY-2-METDIMETHOXYPHENOL + UNKNOWNUNKNOWNDODECANE + UNKNOWNUNKNOWNHEXADECANEUNKNOWNUNKNOWNHEXADECANEHEPTADECANEHEPTADECANE , 2 , 6-DIMETHYL-HEXADECANEUNKNOWN

RT

7.138.358.608.999.209.529.849.9910.5210.6710.7511.2211.4511.7712.0012.1212.7713.3713.9416.60

EST, CONC.

11000001800000120000012000001900000140000013000003300000120000012000001100000150000017000003300000100000016000002100000120000011000003300000

Q

JJJJJJJJJJJJJJJJJJJJ

FORM I SV-TIC 1/87 Rev

1S756 07 SPMPLE C'PTP PPCKPGE 4 1 S

f-

125.9

COMPUCHEM LABSRIC COMPUCHEM DATA: GRD09687A98 SCAMS 399 TO 13W81/10/96 12:26:00 OUT OF 396 TO 1808SAMPLE: ILIL CCI309S87 IDfB202TAR CS* 18756.7 OH 8CONDS.: EXTRACTED 12/28/89 1: 5 DILUTIOH 2821119

IS#1 ISI2 ISI3 SSf5 SS#6

SS#2 SS*3 SS*4 D3tl 15*4 SS#7

IS#5

IS#b

12:131000

15:16120018:19 1:23 24:26

1800SCAN27:231ME

Ul'i•IiO•ILL

h-•IC.

Ul-JCL

•1'/i

r.

r.

QUANTJTAT ION REPORT FILE: SRD09687A08DATA: GRD09687A08. TI01/10/90 12:26:00 / X x

SAMPLE: 1UL CC*3O9687 ID*B202TAR / CS*1B756. 7 ON 8CONDS.: EXTRACTED 12/28/89 1: 5 DILUTIONSUBMITTED BY: 8 ANALYST: 1090

AMOUNT-AREA * REF.AMNT/<REF.AREA)* RESP.FACT)RESP FAC FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHLOROBENZENE <IS#1>2 610 PHENOL (01*3) <108-95-2>3 411 BIS(2-CHLOROETHYL)ETHER <Q1#5> <lll-14-4>4 601 2-CHLOROPHENOL <Q1*6> <95-57-8>5 421 1,3-DICHLOROBENZENE <Q1*7> <541-73-l>6 422 1,4-DICHLOROBENZENE (Ql#8) <106-46-7>7 474 BENZYL ALCOHOL <Q1#9) <100-51-6>8 420 1-2-DICHLOROBENZENE <Q1#10) <95-50-l>9 620 2-METHYLPHENOL <Q1#11> <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (Qltl3) <106-44-5>12 442 N-NITROSO-DI-N-PROPYLAMINE <Q1#14) <621-64-7>13 436 HEXACHLOROETHANE <G1*15> <67-72-l>14 440 NITROBENZENE <Q1#16) <9B-95-3>15 *460 D8-NAPHTHALENE <IS*2>16 438 ISOPHORONE <Q2#2) <7B-59-l>17 606 2-NITROPHENOL <Q2#3) <B8-7S-3>18 603 2, 4-DIMETHYLPHENOL <Q2#4) <10S-67-9>19 625 BENZOIC ACID <Q2#5) <65-85-O>20 410 BIS<2-CHLOROETHOXY)METHANE (Q2#6) <111-91-1>21 602 2, 4-DICHLOROPHENOL <Q2#7> <120-83-2>22 446 1. 2,4-TRICHLOROBENZENE <Q2#8) <120-B2-1>23 439 NAPHTHALENE (Q2#9) <91-20-3>24 475 4-CHLOROANILINE <Q2#10) <106-47-8>25 434 HEXACHLOROBUTADIENE <02#11) <87-68-3>26 608 P-CHLORO-M-CRESOL <G2*12) <59-5O~7>27 477 2-METHYLNAPHTHALENE (Q2013) <91-57-6>28 *495 D10-ACENAPHTHENE (IS#3)29 435 HEXACHLOR'OCYCLOPENTADIENE <Q3#2) <77-47-4>30 611 2, 4,6-TR1CHLOROPHENOL (Q3#3> <88-06-2>31 626 2,4,5-TRICHLOROPHENOL (Q3t4) <95-95-4>32 416 2-CHLORONAPHTHALENE <Q3t5) <91-58-7>33 478 2-NITROANILINE <Q3*6) <88-74-4>34 425 DIMETHYL PHTHALATE <Q3#7) <131-11-3>35 402 ACENAPHTHYLENE (Q3#B) <208-96-8>36 479 3-NITROANILINE <Q3t9) <99-09-2>37 401 ACENAPHTHENE <Q3#10) <83-32-9>38 ®605 2, 4-DINITROPHENOL <Q34»11) <51-28-5>39 607 4-NITROPHENOL <Q3*12> <100-02-7>40 476 DIBENZOFURAN <Q3*13) <132-64-9>41 427 2, 4-DINITROTOLUENE (Q3#14) <121-l4-2>42 428 2,6-DINITROTOLUENE <Q3#15) <606-20-2>43 424 DIETHYL PHTHALATE <Q3#16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (Q3*17) <7005-72-3>45 432 FLUORENE <03*18) <86-73-7>46 480 4-NITROANILINE (Q3#19) <100-01-6>

IS'756 Q7 SflMPLE D'PTP PPCKPGE 416

NO474849505152535455565758596061626364656667686970717273747576777879

NO123456.tyB.9101 1121314151617IB192021

NAME*467 D10-PHENANTHRENE (IS#4>604 4,6-DINITRO-2-METHYLPHENOL <Q4#2> <534-52-l>443 N-NITROSODIPHENYLAMINE (Q4K3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER <Q4#4) <101-55-3>433 HEXACHLOROBENZENE <Q4#5> <118-74-O6O9 PENTACHLOROPHENOL <Q4#6> <87-86-5>444 PHENANTHRENE <Q4#7> <:85-01-8>403 ANTHRACENE (Q4#8) <120-12-7>426 DI-N-BUTYL PHTHALATE <Q4#9> <B4-74-2>431 FLUORANTHENE <Q4#10) <206-44-0>*4S9 D12-CHRYSENE <IS<*5>445 PYRENE <QS#3> <129-OO-0>415 BUTYLBENZYL PHTHALATE «_5#4> <85-68-7>423 3,3'-DICHLOROBENZIDINE <QS*5) <91-94-l>405 BENZO(A)ANTHRACENE (Q5*6> <56-55~3>413 BISC2-ETHYLHEXYL) PHTHALATE <Q5#7) <117-81-7;>418 CHRYSENE <Q5*8> <I218-01-9>*497 D12-PERYLENE429 DI-N-OCTYL PHTHALATE <Q6#2> <117-84-0>407 BENZO(B>FLUORANTHENE <Q6#3> <205-99-2>409 BENZO(K)FLUORANTHENE <06#4> <207-Q8-9>406 BENZO(A)PYRENE (Q6#5) <50-32-8>437 INDENOd, 2, 3-C, D)PYRENE (Q6#6) <l93-39-5>419 DIBENZO(A, H)ANTHRACENE <Q6#7> <53-70-3->408 BENZO(C, H, DPERYLENE (06*8) <191-24-2>t619 2-FLUOROPHENOL (SS#1)41612 D5-PHENOL (SStt2)*447 D5-NITROBENZENE (SS«3)*448 2-FLUOROBIPHENYL (SS#4)*628 2,4,6-TRIBROMOPHENOL (SS«5)#496 D14-TERPHENYL <SS#6)#471 D10-PYRENE456 1,2,3,4-TETRACHLOROBENZENE

M/E SCAN TIME152 505 7:4394 474 7:1493 NOT FOUND128 NOT FOUND146 NOT FOUND146 NOT FOUND108 523 7:59146 NOT FOUND108 523 7:5945 NOT FOUND108 534 8:0970 NOT FOUND117 NOT FOUND77 NOT FOUND136 614 9:2382 NOT FOUND139 NOT FOUND107 580 8:51122 590 9:0193 590 9 01162 599 9:09

REF RRT METH1 1. 000 A BB1 0. 939 A BB

1 1. 036 A BV

1 1. 036 A BV

1 1 057 A VV

15 1. 000 A VV

15 0. 945 A VV15 0. 961 A VV15 0. 961 A VB15 0. 976 A BB

AREA<HCHT) AMOUNT168220. 40. 000 NG91608. 11 942 NG

218064.

218064.

265080.

571156.

434274.205040.1414246952.

69. 837 NG

40.749 NC

50. 553 NC

40. 000 NG

70. 297 NG78. 407 NC1. 881 NC9. 476 NG

y.TOT5. 641 68

9. 84

5. 74 T

7. 13 '1

5. 64

9. 9i -r-11. 05 •0. 271 34 ,

13756 87 SPMPLE C'PTP PPCKPGE 415

NO2223242526272829303132333435363738394041424344454647484950515253545556575859606162636465666768697071727374757677

M/E180128127225107142164237196196162651631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522522522762782761129982172330244

SCAN TIMENOT FOUND616 9:24

NOT FOUNDNOT FOUND657 10:02676 10: 19771 11:46

NOT FOUND704 10: 45704 10: 45

NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND775 11:50775 1 1 : 50775 11:50788 12:02NOT FOUND755 11:32NOT FOUNDNOT FOUND819 12: 30NOT FOUND905 13: 49NOT FOUND824 12:35

NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND1151 17:35NOT FOUNDNOT FOUND1 1 38 1 7 : 23NOT FOUNDNOT FOUNDNOT FOUND1363 20:49NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND405 6: 11473 7: 13553 8: 27707 10 48842 12: 511043 15 56

REF

15

151528

2828

28282828

28

28

47

47

57

57

64

11

15282857

1.

1.1.1.

0.0.

1.1.1.1.

0.

1.

1.

0.

1.

0.

1.

0.0.0.0.1.0.

RRT

003

070101000

913913

005005005022

979

062

000

910

000

989

000

802937901917092906

METH

A VV

A VBA BVA VB

A*BVA BV

A BVA BVA VBA BB

A*VB

A BV

A VV

A«VV

A VB

A*BV

A BV

A BVA BVA VVA BVA BBA VV

AREA(HGHT

182556.

55/77.216612.307046.

3680.3528.

1 8850.5292.11069.20627.

5117.

31515.

457B16.

26460.

306164.

1564.

290573.

77752.90536.5193795298.7444.

76801.

) AMOUNT

12.

9.20.40.

1.1.

2.2.6.1.

2.

3.

40.

5.

40.

1.

4O.

10.11.8.10.6.9.

161

437108000

167161

529364643833

460

715

000

093

000

070

000

512725638183279946

NG

NGNGNG

NGNG

NGNGNGNG

NG

NG

NG

NG

NG

NG

NG

NGNCNGNGNGNG

'/.TOT

1

1.2.5.

0.0.

0.0.0.0.

0.

0.

5.

0.

5.

0.

5.

1.1.1.10.1.

71 -^

33 83 •y~64 '

16/>16 cs

36 >-33 £"94

26 /35 fy

52- "

64

72 >-

64

15

64

486522448840

1S756 87 SfiMPLE C'PTP PPCKPGE 41 4

NO7879

NO12••3

45678910111213141516171819202122232425262728293031323334353637383940414243444546474849305152

M/E SCAN TIME REF212 1035 15:48 57216 NOT FOUND

RET(L)7.7:7.7:7:7:7:7:7:8:8:8:8:8:9:8:P-8:B:8:9.9:9:9:9:10:10:11:10:10:10:11:11:11:11:11:11:11:11:12:12:11:12:12:12:12:13:12:12:13:'13:13:

42132229404451585803091422282345525057391018242736021947374246000822354250505003023019283133493638082336

RATIO RRT(L)1.1.

1.

1.

1.

1.

1.1.1.1.

1.

1.1.1.

1.1.

1.1.1.1.

1

1.

1.

1.

0000

02

OO

00

00

00010000

00

000000

0000

0000OO00

00

00

00

00

1010.10.1010.1010.10.1010.10.10.10.10.10.10.10.1050.10.1010.10.10.10.10.10.10.10.10.50.10.50.10.10.50.10.50.50.10.10.10.10.10.1050.10501010.10.50

OOO000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

Rl0. 8'

RATIO0.0.

0.

0.

0.

0.

0.0.0.0.

0.

0.0.0.

0.0.

0.0.0.0.

0.

0.

0.

0

1009

10

10

11

10

09021010

10

1111IO

0902

IO020210

10

11

10

09

METHA BV

AMNT4O. OO11. 94

69. 84

40. 75

50. 55

40. 00

70. 3078. 411. 889. 48

12. 16

9. 4420. 1140. 00

1. 171. 16

2. 532. 366. 641. 83

2. 46

3. 71

40. 00

5. 09

AREA<HGHT) AMOUNT89516.

AMNT(L)40. 0050. 0050. 0030. 0050. 0050. 0030. 0030. 0030. 0030. 0050. 0050. 0050. 0030. 0040. OO30. 0030. 0050. 0030. 0030. 0050. 0030. 0050. 0050. 0050. 0050. 0050. 0040. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0030. OO50. 0050. 0050. 0050. 0050 0030. OO40 0050 0050. 0050. 0050 0050. 00

9.

R. FAC1. OOO0. 436

1. 037

1. 037

1. 261

1. 000

0. 6080. 2870. 0200. 066

0. 256

0. 0780. 3031. 000

0. 0100. OO9

0. 0490. 0060. 0290. 054

0. 013

0 082

1 000

0. 046

307 NG

R. FAC(L)1. OOO1. 8241. 7581. 5411. 7661. 5140. 7421. 4701. 2721. 6371. 2471. 0880. 8330. 4291. 0000. 8380. 2100. 4330. 1830. 5260. 3470. 4091. 0510. 4540. 2240. 4140. 7541. 0000. 3760. 4110. 3961. 2980. 2781. 4711. 6600. 2460. 9710. 1260. 2171. 4660 3720 2711. 4890 6081 1050. 2141. 0000 1250. 4540. 2430. 2720. 139

'/.TOT1. 31

RATIO1. 000. 24

1. 40

0. 81

1. 01

1. 00

1. 411. 570. 040. 19

0. 24

0. 190. 401. OO

0. 020. 02

0. 050. 050. 130. 04

0. 05

0 07

1. 00

0. 10

IS 756 Q7 SPMPLE C'PTP PPCKPGE 41 3

NO535455565758596061626364656667686970717273747576777879

RET(L)13: 3113. 5514:3013:17:15:16:17:17:17;17:20:18:19:19:20:24:24:25:6:7:8:10:12:15:15:11.

303550342533223831274731414241541012264952564800

RATIO RRT(L)10. 00010. 00010 000

1

1.

1.

1.1.1.1.1.1.1.

00

00

00

00000000000000

10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.10.0.0.0.0.1.0.10.1.

000000000000OOOOOO000000000000000000000000000000742948875906118907OOO000

RATIO

0.

0.

0.

1.0.1.1.0.1.0.

10

05

10

08990301980009

AMNT

40.

1.

40.

10.11.8.10.6.9.9.

00

07

00

51726418289531

AMNT(L)50. 005O. 0050. 0050.40.50.50.50.50.50.5O.40.50.50.50.50.50.50.50.50.50.50.50.50.30.30.30.

000000000000OO000000000000000000000000000000OOOO

R.

1.

0.

1.

0.0.0.0.0.0.0.

FAC R. FAC(L)0 9980. 9361. 643

000

OO4

000

370431073248019201234

1.1.1.0.0.1.1.0.1.2.1.0.1.1.0.1.1.1.0.1.0.1.1.0.

127000405863191094242979000334242864136262922113759836421219154009257540

RATIO

1. 00

0. 02

1. 00

0. 210. 230. 170. 200. 130. 200. 19

IS 756 87 SPNPLE L'PTP PPCKPGE 412


91 '10'.* 12s26s00 + 7«14SAMPLE: 1UL CCK303687 !D*B202TAR

MID LIBRARY SEARCHDATA: GRD09687A08 9 47«EHHANCED U0B 2H 0T>

CS»18756.7 OH 8

BASE M/Z: 94RICi 166911.

IVVV -

C6.H6.0

M L-JT "54B PK 94RANK 1It 3PUR 431 .

r

r

VVr<w'J» .

|

610 PHEh

1

Crt i r.

1 l l

H'^ICU li' O-

, 1

M 1. J U.LUI I'jn

1 l . i . . .1 , . .OL (Ql»3> <198-95-2>*

i . . . 1SAMPLE MINUS

1000 i

0

-1000M/Z

r

40

1, i i

50

. 1

60

1

1 - i iLIBRARY

1 , 1 , , l . i , , l , . . 1 . . .

• • ! - • - - , • - • • f - • - - , - - • • I - • - - . . - - . | • T . . , , , , , | i . l . . . . . T - . , . - . . , - . -J - ,. 1

70 80 90 100 110 120 130

38.6-1

49.3-

100.0H

50.0-

MID DUAL MASS SPECTRUM81/10/90 12:26:00 + 7:14SECOND 5f ECTRUMSAMPLE: lUL CC*309687 IDIB202TAR/ 610/PHENOL (Qlf3) <108-95-2>

DATA: GRD03687A08 *474ENHANCED <10B 2N 0T)DATAj IJNENHANCEO #474

CSI18756.7 OH 8

BASE M/Z: 94/ 94RIC: 176127,/ 213303.COMPUCHEM LABS, INC.

- 41472.

r 42048.

Ul

•I

•Iu.

cth-•ICj

UJ-JLL

•I'/i

r _Q

••£>inr.co

M/Z

III.. . ijlil.I... .illr~ ' ~r *" r~" "•50-n.ijil .i,.!.!... l.l| J L

100


01-'10/99 12s 2?s00 + 7»59SAMPLE; 1UL CC*303S87 ID*B202TAR

1102 CONDS.: EXTRACTED 12/28/89 It 5 DILUTION

MID LIBRARY SEARCHDATA: GRD03687A08 * 523ENHANCED <19B 2N 0T>

CS*18736.7 ON 8


620 2-METHYLPHENOL (QUID <95-48-7>*


I,,. Mill) I I III, l ... Il i I.

-1102 •. • .M/Z 59 100

-r—•• •-"—--r-

150-? ' ' ' r-

iT.

'Hi

t

250

'.0

93.1 -

49.6-

100.9-1

50.9-

MID DUAL MASS SPECTRUM01/10/90 12:26:09 + 7:59SECOND SPECTRUMSAMPLE: 1UL CC*309687 ID#B202TAR

620 -METHYLPHENOL (Ql*ll) <95-48-7>

DATA: GRD09687A08 t523 BASE M/Z: 108/ 108ENHANCED <10B 2N 0T) RIC: 980991. / 1016830.DATAj UNENHANCED #523 COMPUCHEM LABS, INC.

CS*13756.7 ON 8

M/Z

v_^-r

11,1 IL.I illlib , ,1,f 1 1 1 1 1 I '

, ik1 f!i| ^

5

I Iu Jl L, ,i,i r i i ~

0

fl-«U llJ.n- . • '_ !

| , 1 1 . .

1 1 1 1 1 1 1 ' '

"T'l t-f f-

100

•

1 ....~| 1 | l- | I | 1 | 1 | 1 f i I l | 1 | 1 | I | I | l |

150 200 250

- 128896.

•

Ul(0'1

O•ILL

•I

•ICi

LU-JLL

- 139048. ^

f -Q

'£•IOf -Vj»— i

•

f-

1055

SAMPLE

COMPUCHEM LABS, INC. MID LIBRARY SEARCHDATA: GRD09687A08 tt 534

01/19/90 12i26s00 + 8J09 ENHANCED (18B 2N 9T)SAMPLE: 1UL CCK303687 !D*B292TAR CSI1375S.7 ON 8CONDS.: EXTRACTED 12/28/89 Is 5 DILUTION


C7.H8.0M UT1?!PK 197 ,

113

PUR 871 .

622 4-METHYLPHENOL (Qlfl3) <196-44-3> *

4i I

1035

-1055M/Z


1 1 1 1

46~T '

60 80 100 126 140

98.7

49.4-

109.0-1

50.9-

11/2

MIO DUAL MflSS SPECTRUM DATA: GRD09b87A08 *534 BASE PI/2: 107/ 10791/18/98 12:26:60 t 8:09 ENHANCED (106 2N 8T> RIC: 823295.' 874495,SECOND SPECTRUM DfiTfll UNENHAHCED 1534 COMPUCHEM LABS- INC.SAMPLE: 1UL CCI399687 ID*B292TAP. 05*18756.7 OH 8/ 622 i-METHYLPHENOL <Q1*13> <196-44-5>

1 , 1 .llilii. .1. -r—

r 178432.

> lia **•

r 130736.

100 150

UliTi

O•1LL

Ul-JLL

•1

r.

10F-co

in

1912

-AMPLE


01/10/90 12:26:00 + 8:51SAMPLE: 1UL CC*389687 IDIB292TARCOHD5.: EXTRACTED 12/28/89 1: 5 DILUTION

05*18756.7

MID LIBRARY SEARCHDATA: GRD69687H68 * 580ENHANCED <10B 2H 9T)

OH 8

BASE n/Z: 167RIC: 1144830.

h.il I IC8.H19.0

XANK! iPUR 858

693 2,4-DIHETHYLPHENGL <Q2*4) <ie5-67-9>*


I, .11 iH.ii .ii, I,.

-1012H/2 50 100 150 200

MID DUAL MASS SPECTRUM DATA: GRD09687A08 #580 BASE 11/2: 167/ 10701--16/96 12:26:66 + 8:51 ENHANCED (166 2N 8T) RIC: 1222656./ 1312766.SECOND SPECTRUM DATA: UNENHftHCED *586 COMPUCHEM LABS- INC.SAMPLE: 1UL CC»3e9687 ID*B292TAR CS*18756.7 OH 8

693y2-4-DlMETHYLPHENOL <Q2*4) <185-67-9>

ot

Sb.2 -

49.1-

160.0-

50.6-

•

M/298.2-

49.1-

100.0-

56,0-

<v ..--

.1, lllll ..J.L. .^11.. . JL Jh1 | 1 | 1 | 1 | 1 | 1 T"l |"»

1 Ii , ,lj, 4. JL iv j,

• / - - 1 | 1 -I ' i T 1 • 1 T , -1

50 100

• I , , , , . , . , , , , , .

11 T"«f

.

' 1 ' 1 ' | ' I ' 1 ' 1 ' I ' | ' 1 ' 1 ' 1 ' 1 ' | ' 1 ' I ' 1 ' 1 ' | • 1 ' I ' 1

• ! "1 , • | < | > | > | • | • | i | < | ' | < | , | , | • | < | , | i | ' | • | , |

159 299 250 300

i | i | i | i i i i i i • i i | i i i i i i i i i | i i i i i i i i , | • i , i i i

- 244480.

r 240128.

M/2"•» r-' | "'-"I » t-T

350 400T450

T ? '"i "T"VI i » i ' j i ] ' i ' j ' i i •] i •] T r T• T-t-T506 550 600

r 244480.

LU'-0

O•ICL

CTK•1C,

UJ-JLL

'1

r.

vo10r-'jj

•s

1002

CQMPUCHEM LABS, INC.

01/10/30 12s26s00 + 3s24SAMPLES 1UL CC*309637 IDIB202TARCONDS.s EXTRACTED 12/23/33 Is 5 DILUTION

CS»13756.7

MID LIBRARY SEARCHDATA: GRD03687A08 #616ENHANCED <19B 2N 0T)

ON 3


jil. i J L l

C10.H8

UK 12jt -PUR 53? J

433 NAPHTHALENE <Q2t9> <91-20-3>*

•"

1002 i

-1002M/Z


, 1,1 ,.1.1 , ,1.1 ll

r*100 150 200 250

• i •300

MID DUAL MASS SPECTRUM01/10/90 12:26:00 + 9:24SECOND SPECTRUMSAMPLESNlUL CC#399637 1D#B202TAR

'NAPHTHALENE <Q2#9> <9i-20-3>

DATA: GRD09687A08 #616 BASE M/Z: 128/ 123ENHANCED <106 2N 0T) RICs 404391./ 658431,DATAj UNENHANCED #616 COMPUCHEM LABS, INC.

CS«18756.7 ON 3

37. a -

43.0-

-

100.0-

50.0-

M/Z37.9-

49.0-

•

100.0-

50.0-

. II. .y, ,|l. (_.L .1, |l- , • i • . ' i - i ' . • i • i - i

Ji iLi .In... Jill. . . Li_ . 1 1 ... LL< 1 ' | ' 1 ' 1 r "1' T * p^^^FT

59 199

,1

J

• • ,

I

LuL ....

150 200 259 399

- 114176.

UJ

O£T

- 116698. U.

1KctG

Ul-JCL

r 114176, ct'/i

f -O

'•Ct10f -

- 116608. ^

-

M--Z 350 400 450| ' I ' I " I i I '• | ' I ' I ' I ••'• • 1 ' I ' T ' I

500 550 660

1053


01/10/99 12s26s00 * 10!19SAMPLE: 1UL CC#303637 1D#B292TAR CS»18756.7

MID LIBRARY SEARCHDATA: GRD09687A08 # 676ENHANCED <10B 2N 9T)

ON 3


CONDS.s EXTRACTED 12/28/89 Is 5 DILUTION

..J . Jilt. I . i• • " " I " •

C11.H10

Mm PK 142SANK if 13PUR 761

477 2-METHYLNAPHTHALENE (Q2I13) <91-57-6> *

J .1 .

1059 rSAMPLE MINUS LIBRARY

..i I ,,i .1. ,, 1 1 n! J.,1,. I. I.I.

-1053 *--M/Z 50 100 150 200 250 300

99.7-

HID DUAL MASS SPECTRUM61/16/96 12:26:06 + 10:19SECOND SPECTRUMSAMPLE., 1UL CC*399e87 IDIB282TAR CS*18756.7

(477)2-HETHYLNAPHTHALENE (Q2*13) <91-57-6>

DATA: GRD69687H08 «676ENHANCED (16B 2N 6T>DATA: UNENHANCED *676

OH 8

BASE M/2: 142/ 142RIC: 641623,/ 911359.COMPUCHEn LABS- INC.

49.9-

109.91

r 129920.

50.9-

I ' I ' I ' 1 « T T I ' I ' I ' I ' I ' I ' I

M/2

r 130394.

T ' I

256 300

UJCDIX.OCTCL

UJ-Ja.z:ct

K.O

•10r_,co

1128

SAMPLE


01/10/30 12s26s00 + 12J02SAMPLES 1UL CC#309637 ID#B202TARCONDS.s EXTRACTED 12/28/89 Is

CStl8756.7DILUTION

MID LIBRARY SEARCHDATA: GRD03687A08 # 788ENHANCED (10B 2N 9T>


ON 8

4- — 1 • • • »476 DIBENZOFURAN <Q3#13) <132-64-9> *

1 1

B PK IL.SANK i* i AIt 1-3PUR 34*


-1128M/Z

.1.

• i —•-60

1 i ' * • • i100 120 140 160 180 200

a-,•7.

COft;

63.7 n

30.4-

100.01

50.0-

MID DUAL MASS SPECTRUM91/10/90 12:26:00 + 12:02SECOND SPECTRUMSAMPLEr-lUL CC#303687 ID#B202TAR

, 476/OIBENZOFURAN (Q3#13) <132-64-9>

DATA: GRD09637A03 #788 BASE M/Z: 168/ 106ENHANCED (108 2N 0T> RIC: 64127./ 380927.DATAj IJNENHANCED #788 COMPUCHEM LABS, INC.

CS#13756.7 ON 3

11 I 1 1 ! | 1

l l l l' 1 | 1 | 1 1 1 | 1 |

11 '

|

' 1l , l | l| 1

1 . , 1 . 1 .I 1 1 1 1 1 | 1 | ' 1 > I ' 1

."7

I |

, j Ikilli! Ik,]•-] ~+- -f* t • j i '• hlJM/Z 50 100

t^-

- 10960.

18948.

LUCDCt

ctCL

ctGUJ-jCLcct'/I

10NCO

200 so

r-.

1028

COMPUCHEM LABS, INC. MID LIBRARY SEARCHDATA: GRD09687A08 # 819

01/10/99 12s26s90 * 12j30 ENHANCED <10B 2N 0T>SAMPLE: 1UL CC#303637 ID#B202TAR CS#13756.7 OH 3


1028

SAMPLE

CONDS.s EXTRACTED 12/28/89 Is 5 DIU.ITION

1 | 1 ill |l l|lll 1 II |h i1 - i

[ 1 ill ! I,', I l<l 1 1 I I I ,

C13.H19 432 FLUORENE <Q3#18> <86-73-7> *1023 i

M HT IBB PK 166SANK i9 18PUR 267

, , . II.,, • ' .1 .ll 1


M/Z

l l 1

40

1 n l , i l , ll i| i |

60 80

M M l , , 1 i l l

• —- • ! • - • - • i - , - . . - ,

100 120

1 , , . l l

140

III 1 .... 1 1 i , , i i . . i . , .

166 180 200 220

'•ft•7.

93.0-1

46.3-

100.9 ~

50.9 —

MID DUAL MASS SPECTRUM01/10/90 12:26:00 + 12:30SECOND SPECTRUMSAMPLE: 1UL CC#303637 ID#B292TAR/ 43£ FUJORENE <Q3#18> <36-73-7>

DATA: GRD03687A08 #813 BASE M/Z: 166/ 155ENHANCED U0B 2N 0T) RIC: 232703,/ 383113.DATAs UNENHANCED #813 COMPUCHEM LABS, INC.

CS#13756.7 OH 3

11, 1 III llLilLlI .L l . , l lr i i i i i i i i | iLul i, , i iT V i i | 4) |i' ir ,i 1 , 1 ll[**S | i ll 1 . J , „ . .. 1 . L .r1! i i i i | i i i i i i i i i |

M/Z

11. Jill I III, .Ll....i I ' i

14448.

15536.

LU<sct

ICL

1G

UJ-Ja.s:ct

r..Qo10Kco

200 250


0!/10-'90 12:26:00 + 7s 11SAMPLE: 1UL CCI309537 ID#B202TAR

MID LIBRARY SEARCHDATA; GRD03687A08 # 470ENHANCED (108 2N 0T)

CS#18756.7 OH 8

IOa,t't


1055 ]

SAMPLE

C9.H121055 i

M UT 120B PK 195RANK 1# 3036PUR 981

C3.H121055 i

M UT 126B PK 10$RANK 29 3095PUR 875

C3.H121955 i

M l-JT 120B PK 105RANK 3ft 3037PUR 874

M/2

CONDS.s P EXTRACTED 12/29/83 Is 5 DILUTION

ll - , . t , i , ||l , •BENZENE, 1-ETHYL-3-METHYL-* CAS» 620-14-4

r

1 1 i 1 1 I I I I 1

BENZENE, 1-ETHYL-2-METHYL-* CAS# 611-14-3r

1 1 L 1 t 1 I I I I 1 I

BENZENE, 1-ETHYL-4-METHYL-* CAS# 622-36-8r

1 1 i l l 1 1 I I I l

3w 40 50 60 70 80 90 loo

I I i i i i

J i t i

1 i » 1

110 120

COMPUCHEH LABS- INC.

61/19/99 12:26:06 + 8:24SAMPLE: 1UL CCt389687 ID*B202TAR

HID LIBRARY SEARCHDATA: GRD69687A68 ft 556ENHANCED (196 2N 9T)

CS»18756.7 OH 8

BASE f1/Z: 169RIC: 562175.

1233 j

SAMPLE

C12.H20.01233 i

1 UT 180

1 13130PUR 592

C8.H12.01233 i

M WT 124? PK 103toNK 2» 3406PUR 4§5

C11.H14.0:1293 i

M UT 134B PK 124*ANK 3ft 15367?UR 492

M/Z

ccINOS. : EX

h

TRf

||

iCTED 12/5

M i .

>8/89 1: 5 (

j , 1 ,5-OCTYN-4-ONE, 2,2,7,7-TETRAHETHYL-

r

1 I l

ETHANONE- 1-U-CYCLOHEXEN-l-YL)-*r

'i

i i

BUTYRIC ACID-r

i40

l l

P-METHOXYPHENYL ESTER

i t

60 80

JILUTION

. 1 1 | u

*| 1

CAS*

iCAS*

* CAS*

1

100

|i .1.1. .28884-89-1

i

932-66-1

14617-95-9

120 140 160 180

ncr.

COHPUCHEM LABS- INC.

91/10/98 12:26:99 + 8:39SAMPLE: 1UL CC*399687 ID»B202TftR

MID LIBRARY SEARCHDATA: GRD09687A08 ft 566ENHANCED <19B 2N 9T)

CS«18756.7 OH 8

BASE n/Z: 131RIC: 763993,

1908 i

SAMPLE

C9.H8.01999

.1 HT 132B PK 131RANK 1* 4683PUR 900

C9.H8.01999

M WT 132

r\Hf >«* £

* 4£86 -PUR 869

C9.H8.01039

M WT 132B PK 132SANK 39 4b89PUR 859

M/Z

CONDS.: EXTRACTED 12/28/89 1» 5 DILUTION

,1, ... , ,.,!, .,12-PROPENAL, 3-PHENYL- * CAS* 184-55-2

r

1 ,1, . ,.,ll .h

BENZOFURAN- 2-METHYL- * CAS* 4265-25-2r

BENZOFURAN. 7-HETHYL- * CAS* 17859-52-8r

I 1 1 i 1 i f | II , 1 1 1 1

40 60 39 100 120

1

,I " ' " " 1 * ' '

1

140 160

•"Ia.


01/10/90 12s26s00 + 9j82SAMPLES 1UL CC»309637 ID#B202TAR

MID LIBRARY SEARCHDATA: GRD6968?ft08 * 59iENHANCED <19B 2N 6T>

CS»1875e.7 ON 8

BASE M/Z: 115RIC: 559163.

1114

SAMPLE

COHDS.S EXTRACTED 12-

,. iL ill) II. . -J . . JL

'23/89 Is 5 DILUTION

ll 1.1C10.H10 1H-INDENE, 3-METHYL-* CAS* 767-69-2

1114 i1 WT 1303 PK 130?ANK 1» 4 36PUR *11

r i

, ,. , ii. JLC18.H10 BENZENE; a-METHYL-2-CYCLOPRQPEN-l-YU- * CASft 65951-83-4

1114 iM WT 130S PK 13§SANK I

Pw 1-?

r

j d, .< , , , J,C10.H10 1H-IHOENE, 1 -METHYL-* CAS* 767-59-9

1114 iM WT 130B PK 130?ANK 3

*UR 4Il3

r

11

J lli ,,i , i

J

ll, Jl

M--Z 50 100 150 200 250 300

'7.

1283


81/10/90 12J26S09 * 9s15SAMPLE: 1UL CC#309637 ID#B202TARCOHDS.s EXTRACTED 12/28/89 Is 5

, i I. J L u ..[ . 1» MMplOT««« » m« »«MMMM B IMMM ^

CS#13756.7DILUTION

MID LIBRARY SEARCHDATA: GRD89687A08 * 666ENHANCED (18B 2N 9T)

OH 8

BASE n/Z: 43RIC: 721919.

C13.H231289

.1 UT 184B PK 43RANK T# 13882PUR S51

C12.H261289

M WT 17

UNDECANE, 4,7-DIMETHYL- * CAS* 17381-32-3

17043.IANK

UNDECANE, 2-METHYL- * CAS« 7045-71-8

C11.H241289

M UT 156B PK 43SANK 3ft 8716pi IR 523

M/Z

UNDECANE*

• "i • ''166

CAS* 1129-21-4

156 260 25o Mf)

•T.


91/10/30 12s26s00 + 3s34SAMPLE: 1UL 001389687 ID»B202TAR

MID LIBRARY SEARCHDATA: GRD09687A08 # 627ENHANCED C10B 2N 0T>

CS«18756.7 OH 8

BASE M/Z: 145RICs 1105910.

1055

SAMPLE

C10.H18.01855 i

,1 UT 146B FK 146RANK 1ft 6898PL*? 837

C18.H10.01055 i

M WT 146B PK 143&ANK |# 678§PUR 819

C3.H19.H21055 i

M UT 146B PK 146SANK 3ft 7006PUR 731

M/Z

CONDS.: .EXTRACTED 12/28/89 If 5 DILUTION

BENZQFURAN, 4,7-DIMETHYL- * CAS# 28715-26-6r

| 'I I 1 ' 1 'I 1 I'l 1)

2-PROPENAL, 2-METHYL-3-PHENYL- * CAS» 101-39-3r

1 1 |l ,1 1 ,| t 1 . | , ,

l ,

1

i1H-BEHZIMIDAZOLE, 3,6-DIMETHYL- * CAS# 582-60-5

r

I I I i i l l i. K 1 . i20 40 60 30 100 120 140 160


81/18/90 12s26s00 + 9s54SAMPLES 1UL CC#303637 ID#B292TAR

MID LIBRARY SEARCHDATA: GRD09687A98 # 648ENHANCED (10B 2N 8T?

CS»18736.7 OH 3

a.COn


1173 •

SAMPLE

C9.H12.021179

-1 UT 152B PK 13?RANK 1# 8814FUR 485

C3.H12.021179-

M UT }52

9 '803$ •PUR 470

C3.H12.021173

M UT 152B PK 13?SANK 3

PUR °440

M/Z

TONQS. '. E;*TR

il

ACTED

I

12/28/89 Is 5 D

ll. .i.ll,

I

PHENOL, 4-ETHYL-2-METHQXY-*r

1 1

LUTION

I 1

1

||li III i, i 1

PHENOL, 5-METHOXY-2.-3-DIMETHYL- *r

, , ,,

BENZENE, 1 , 4-DIMETHOXY-2-METHYL-*r

20T-1"

40

M

60,,80

CAS« 2785-89-9

I I

CAS« 34383-01-7

I I

CAS# 24599-58-4

i 1100 120

,1

1

140

1 .1 i .1.

1 l

, — , — , — U-. . -T . - - -160

COCO


01/19/30 12:26:00 + 18:82SAMPLE: 111 CC*303S37 ID#B262TAR CS#13755.7

MID LIBRARY SEARCHDATA: GRD09687A08 # 657ENHANCED C18B 2N 0T>

OH 3

BASE M/Z: 137RICs 1773710.

1168 •

SAMPLE

C9.H12.021160

,1 UT 132B PK 137RANK 1

IU T3S

C8.H8.031160 i

M UT 152B PK 137RANK_ n2

PUR 652

C10.H16.01168 i

M WT 152B PK 137SANK 39 7875PUR 539

M/Z

CONDS.s EXTRACTED 12/23/33 Is 3 DILUTION

, l i |lil l , l i . . . 1,1,1 1 , 1 , .,.,) r|BENZENE, l,4-DIMETHOXY-2-METHYL-* CAS» 24399-58-4

r

i iETHANONE.. l-(2,4-DIHY1DROXYPHENV>L)-* CAS» 89-84-9

r

1-PROPENE, l-METHOXYfl-METHYL-2-CYCLOPENTEH-l-* CAS» 74753-29-0r

,..., I l l 1 t | 1 | 1 1 I I I

20 4o 60 80 100 120 140 160 180


01/18/38 12s26s00 * 10,34SAMPLES 111 CC#363637 !D#B202TAR


CS#13756.7 OH 3

COn


1234

SAMPLE

C8.H10.031234 •

,1 UT 154B PK 154RANK 1# 8432FUR 645

C8.H10.031234

M WT 154B PK 134RANK 29 8435 •PUR 545

C18.H12.01234 i


*

r 1-

4J

ONUS. S EXi

llll 1 ,

IRACTEO 12/28/

,,l 1.1,1 1.

«

PHENOL, 2,6-DIMETHOXY- *

I I I 1 I IPHENOL, 3,4-DIMETHOXY- *

r

ll| 1 1

» 15 5

,111,

ni *

iiPHENOL, 2,6-DIMETHOXY-, ACETATE *

r

( 1 , 1

DILUTION

, 1 ,-OAS«

CASft 2

I'l ' - , -31-10-1

,

«33-89-8

CASft 344-39-0

, » . . *M/Z 100 150 250

'•ftCO

COflPUCHEM LABS, INC.

61/10/96 12:26:68 + 19:43SAMPLE: 1UL CC*389687 ID*B292TftR

MID LIBRARY SEARCHDATA: GRD99687A08 * 702ENHANCED 09B 2N 9T)

CS*18756,7 OH 8

BASE M/Z: 137RIC: 1927670.

1999]

SAMPLE

C19.H14.01088

.1 HT 166B PK 137RANK 1* 18516PUR 614

C19.H12.0-1999

H WT 196B PK 137RANK 2* 15783PUR 566

C11.H15.0-1909

M WT 225B PK 137XAHK 39 26331PUR 554

H/2

CONDS.: EXTRACTED 12/28/89 1: 5 OIL

, ,1,1 Ml|i- .1,1. .,1 J, ,1 (JU L *4

JTION

2 BENZENEHETHANOL> . ALPHA. -ETHYL-4-METHOXY- * CAS* 5349-68-8r

. . . 1 , J 1. .. |l .ilt BENZENEACETIC ACID- . ALPHA. -HYDROXY-3-HETHOXY-* CAS* 54845-40-8r

1 1 .,1 I.I 1 ll („ 1*.H L-T>('ROSir€- 3-METHOXY-. METHYL ESTER* CAS* 78148-37-5r

i M i .LU. •...—5o 160 150 200 250

inCO


91/19/38 12s26s00 + 10s49SAMPLE: 1UL CC#309637 !D#B282TAR

MID LIBRARY SEARCHDATA: GRD83687A08 # 708ENHANCED (18B 2N 8T)

CS#13756.7 OH 3

BASE M/Z; 43RICs 334311.

1342

SAMPLE

C12.H261342 j

1 WT 178B PK 57SANK itt 11444PUR 623

C13.H281342 i

M WT 184J PK 43>AHK 2[ 13332* UK o 0o

C12.H261342 I

M UT 1783 PK 43?ANK 31 11452PUR 601

CONOS.: EXTRACTED 12/28/89 Is 5 DILUTION

I , , 1 1 i . iDOOECANE* CAS» 112-48-3

r

|

JL

i IUNDEI

r

1

l| 1 i . . . .;ANE, 4. -DIMETHYL- * CAS« 17301-32-3

n 1 i . . . . . . . .UNDECANE, 2-METHYL- * CAS# 7045-71-8

r

1 il n iM/Z 40 60 80 100 120 I4o 160 180

COCOMPUCHEM LABS, INC.

01/10/90 12s26s09 + 111 15SAMPLES 1UL CC#303637 ID#B202TAR


CS#18756.7 OH 8


1050

SAMPLE

C8.H8.0410501

.1 UT 168B PK 168D/kUir 4rxFirWS 1

# 11172'FUR 518

C9.H12.0310501

M UT 16g

Wai

C8.H8.041050 i


M/Z

IM

1

JDS.s

ll

EXTRAC

il i i

TED 12/2

III 1,

3/83 Is

ill ,

5 DILU

,1 1

II

BENZOIC ACID, 4-HYDROXY-3-METHOXY-*r

,11BENZENE,r

J ,1ETHANONEr

40

1 1l.-2,3-TRIMETHOXY-*

1 i .1. l-(2,3,4-TRIHYDROXYPHENYD- *

601 ' '

30

i

100

ON

, . ... 1 1 n

CAS* 121-34-6

1

CAS« 634-36-6

•

CAS» 528-21-2

iL . .120 140

i • , . . . . , . , . .

1- 1 - . - i • • i - . . . . • j i

•• I ' 1 - 1 . , . , , . . . , . ,

16o 180 200

1328

SAMPLE

C16.H341323

.1 UT 226

K

C13.H281328

M UT 184PK 43

•\LII/ o

« 1PUR

C14.H381328 i

M UT 138B PK 43SANK 3ft 16282FUR 785

M--Z


01/10/30 12j26s00 + Ilj31SAMPLES 1UL CC#303637 IDftB202TARCONDS.s EXTRACTED 12/28/89 Is

CS#13756.7DILUTION

MID LIBRARY SEARCHDATA: GRD89687A88 # 754ENHANCED <10B 2N 0T>

ON 3


HEXADECANE*

1UNDECANE; 4.-7-DIMETHYL- *

DODECANE, 4,6-DIMETHYL- *

CASt 544-76-3

CASft 17381-32-3

CAS# 61141-72-8r

1 ll J40 60 30 100 120 140 160 188 299 220

COn

coCOMPUCHEM LABS, INC.

01/19/30 12J26S08 + Ils58SAMPLES 1UL CC#303537 1D#B202TAR


CS#18756.7 ON 3


1008

SAMPLE

C3.H10.041000 i

,1 WT lg

# 13627PUR 542

C11.H18.0:1000 '

M WT 182B PK 125RANK 2

C3.H14.021089 1


M--Z

r OT-I05.S EXTRACTED 12/23/39 Is 5 DILUTION

h |lil| ..(II. Ill, , ,.i,|. il.. . hi., ,..., , ,.„.BENZOIC ACID; 3.-4-DIMETHOXY-* CASft 93-87-2

r

| 1 | , 1 1 , |, . 1 . 1 , , ,

. CYCLOPROPANECARBOXYLIC ACID; 2;2-DIMETHYL-3-<2* CASft 5468-63-9r

.SI SILAHE, DIMETHOXYMETHYLPHENYL- * CASft 3827-21-2r

1 I , II i l. . 1 1 1 i. i i50 100 158 200 250

CO


01/10/30 12s25s09 + 12s84SAMPLES 111 CC#383587 ID#B202TAR

MID LIBRARY SEARCHDATA: GRD09687A08 ft 730ENHANCED (108 2N 0T>

CS#13756.7 ON 8

BASE M/Z: 106RIC: 414207.

1000 •

SAMPLE

r CONDS.s EXTRACTS

t

1 lllll .1,1 , il .

D 12/:.8/83

, J

Is

.,

5 DILUTION

, ,C10.H8.03 2H-1-BENZOPYRAN-2-ONE, 7-METHOXY- * CAS« 531-59-9

100014

.1 UT 176B PK 176RANK !* 12376PUR 332

l

C12.H15.0 PHENOL,

aX

=CO

£C

#

19801

rfT 176?K 175UK 2

12427PUR 383

r

i li ulC12.H16.0 PHENOL,

1009 '

M UT 176B PK 107SANK 3ft 12423PI IR 3K3

r

ll l

, l i . . . , 14-CYCLOHEXYL- *

I..

.

2-CYCLOHEXYL- *

ll, I ,

i

CAS« 1131-68-8

CAS« 113-42-6

i

M/Z 50 100 150 200 250 oo

QCO


01/18/30 12s26s00 + 12s11SAMPLE: 111 CC#303537 IDftB202TAR

MID LIBRARY SEARCHDATA: GRD89687A88 ft 798ENHANCED (188 2N 0T>

CS»13756.7 ON 8


1362

SAMPLE

C16.H341362

.1 WT 2g5B PK 57RANK 1# 20624PUR 882

C17.H361352 i

M UT 240B PK 3?RANK 29 22433PUR ?I§

C13.H281362 i

M WT 184B PK 57SANK 3ft 13875PUR 703

M/Z

rTONDS.S EXTRACTED 12/28/83 Is 5 DILUTION

, ,ll .11HEXADECANE* CASft 544-76-3

r

ll ll i .1 >i .j .1 .1 . . .HEPTADECANE * CASft 629-78-7

r

1 llUHDECANE

r

•1 n .1 a .. . . . .2,3-DIMETHYL- * CASft 17301-26-7

ii50 100 150 200

COMPUCHEM LHBS, INC.

01/10/30 12:26s00 + 12s50SAMPLES 111 CC#30?537 1D#B2P2TAR


CSI18756.7 OH 3

'7,r.r;


l-iiv

SAMPLE

C17.H361310'

'I UT 2403 PK 57?AHK 1ft 22453PUR 807

C15.H341318 i

M UT 2263 PK 5?-ANK 2f 20524PUR 7§i

C13.H281318 i

M WT 1343 PK 43?AHK 3ft 13882PUR 758

M/Z

f'.-'jriL'a. . ZA i r.n_. i c.L' It- 4.W3 l. -J L'lL'.'l JL'Jn

HIr

, .1iPTADECi

||

, ,1)*NE *

iHEXADECANE*r

u»r

|| n

,1

CAS# 629-78-7

J ., .. f

CAS» 344-76-3

• ,1 .1 . . . . . . .CECANE. 4,7-DIMETHYL- * CAS# 17381-32-5

IIT • . , - • . -

5o 100 150 200 259

CO

COMPUCHEM LABS, INC. MID LIBRARY SEARCHDATA: GRD03S87A08 # 880

01/10/30 12s26s00 + 13:26 ENHANCED <10B 2N «T>SAMPLE: 111 CC#30?5S7 1P#B202TAR CS#13755.7 OH 3


r V - 1 <

.1

JJ. . w« 1 r.wv l CU1 JL~- -W 7J J.. -J L'J.I_'-M i'.'H

, JL J. J. j. .JL . . .. ._ _ ..C19.H40 HEPTADECANE; 2.-6-DIMETHYL-* CAS# 54105-67-8

1212 1 r

.-I HT 268B PK 57RANK 1ft 25363PUR 803

1

I

J J „ ,C17.H35 HEPTAQECAHE * CAS# 523-78-7

1212 J r

M UT 249S PK 57RANK 2* 22453PUR ,-33

u Il 1 J ll .1 u"*' *' *r - , - , - . , . T - T - . - . - i • i - r - , • i - . • . - | - . • i - i • i - , - , . , . , . , • | • i • • i • i •- T - i

C25.H52 PENTACOSANE * CAS# 623-33-21212 i

M UT 352B PK 43SANK 3ft 33538PUR 7$?

r

l 1y u j i, „M/Z 50 100 150 200 250 JOO fl

f.


01/10/30 12s26!80 + 14:90SAMPLES 1UL 001369587 ID»B202TAR

MID LIBRARY SEARCHDATA: GRD09687A08 #917ENHANCED U0B 2H 0T>

CS»13756.7 OH 8

BASE M/Z: 57RICs 470527

1135 •

C15.H341195 i

.1 UT 226B PK 57RANK 1# 20624PUR ?28

C17.H361195 i

« 1-iT 2483 PK 57RANK 2ft 22453PUR 827

C21.H14.0-1135 i

M UT 338B PK 57SAHK 3ft 36165PUR 81 1

M/Z

v.rnjs*

, J

. C'> 1

I Jl

r.H'j i cu

..y

i^f.'s-'is i; ^ L'.L.'i -ijn

. - il . . J. . j. . -. ..

HEXADECANE* CASft 544-76-3r

i d i ll J J 4

HEPTADECANE * CASft 629-78-7r

15.N2.FEIRON,

r

1

4 D ll J J - . -.

TRICARBOHYL[N-(PHENYL-2-PYRIDIHYLMETHYLE* CAS# 74764-1 1-7

II to ll J J a -. ,» . .. ... ... ... . _i

50 100 150 200 259

••ftI-


01/10/90 12:26:00 * 15s41SAMPLE: 1UL 001309687 ID#B202TAR CS#18756.7

MID LIBRARY SEARCHDATA; GRD03687A08 #1033ENHANCED <10B 2N 8T>


ON 3IglHPI

C18.H241000

,1 UT 240B FK 240RANK i# 22460FUR 500

C13.H2419801

M UT 240B FK 24*RANK 29 22453 •PUR 420

C15.H16.01000 1

M UT 240B PK 134SANK 39 22417 •PUR 392

M--Z

r '-r'-'nu'.?. . C»> l ~ wv : cu Ii- iC- 13 1. 2 'J i L'J I 1 'JH

1 I I I|l| Ji| I Ji ,,|ll Inj illj. , , il,|h L. 1. ,., .jl. ....

TRIPHENYLENE; 1; 2; 3.- 4, 3, 6, 7.- 8; 9; 18; 11; 12-DODEC* CAS# 1510-39-5r

. J , | i j, ,„ L Ji ilCHRYSENE; 1 .- 2.- 3.- 4; 4A; 7; 3; 9; 10; 1 1 ; 12; 12A-QOOECA* CAS# 1610-22-6

r

u 1 i| , ,1 1 1 II y, > | i Ii 1 ,1N2 UREA, N,N'-DIMETHYL-N,H'-DIFHEHYL-* CAS# 611-32-7

r

1 1. u| l|l 1. 1 1 . . , L | ,, - - 1

50 100 150 200

,

250 390

LAB INSTRUCTIONS:

PRIORITYRECEIPT DATE DUE DATE:

SEMI-VOLATILEGC/MS WORKSHEET COMPUCHEM*:.

men i crwei em TH 9/00 GnuntU LbvtL OULlU, C/0O 9UW

- - J C 3 R e )f 3 D C y 3 CO :'

J2C 3 RaC 3 DSC 3 C :1

"1f':5&*- .v-fr-i"'! Sample Prep Code 1

>54pec

^70

393, A T C

SAMPLE ID#: Dry Ut '

CC/MS ANALYSISVolumes mixed: BN ulInternal Standard Volume AddedMixed Sample Volume Injected.Date of Sample Bottle Analyzed IT. / ^ /DFTPP Filename Ifc-q o a 1 1 oC o Disk

DiskDisk C

Standard Filename /U.t±<?o o 1 1 o <?Sample Filename 6* £>o °i £ f 7 /4-e g

INAL

A N A L Y S T ( S ) : Injection. Work-up.

CC/MS REVIEW

CONDITIONCODE

Entry Codes OK.EA.JA, ES,AL,AH,PL,PH,FL,JSFH , NL , NH, YL , SL , SH , SM, YH

Non-Entry Codes IM,IL,IH,SW,CT,CS,PC,OT,DAED,IF,LA,DI,CO,RN,DU,NS

Disposit ion:Extraneous Peak Search JL*sul ts .

tt of Peaks Found: (

# of Hits

* of Surrogate Outliers-'

Quality Assurance Notice(s):

* Notices Required C/ J

CC/MS Review

C t^D Complete

C D Reinjection required

[ ] Reextraction required

C ] Dilute ( : 1 )

C ] Reinject Neat

C 3 Send to QA

Auditor Date

REPORT INTEGRATIONFinal Reportable Package(s):.

Total # of Injections

QA COMMENTS:

FINAL REVIEW:

Initials.ES3SSS3KV1

Init ials

Date.t*as = :

DateAC1009 (05/89)

18756 e? SHMPLE &PTP PPCKPGE 375

ASSIGNED TO

! SAMPir

NUMBER

3o9(,Ul

Jo?****

3MU,tf*

3>1**?

z*umMO IK

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/

SURROGATE

SPIKE

NO

AMT

LOT

NO

AMT

LOT

CASE

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/

Ifl+i,•7

/

CLIENT

rcrp

6f*£

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EXTRACTION WORKSHEETSemi Volahles/ Miscellaneous

CompuChem Laboratories Inc.

QC SAMPLE

TYPE

^

^

as

±s>s-s65

e.

ORIGNO

vu,,

»o-M

vm.n

^.,7

SAMPLE

WEIGHT (g)VOLUME (ml)

\ c

\ c

1 c.

\ c1 f1 0

1 0

1 C

1 o

FINAL EXTRACT VOL (MLSI

/B/N

1 ^

\ L

\ c

l .o

1 C

^ C'

a c

\ 0

, L'

ACID PEST

1

S Vo4 AcM B/N Pest Othei Olhef

393j !/ml.A-^1

3012 2021

10ml. 10ml

M/

Fit

SL

EX

ADJUSTtUPM

B/N A

OATE ASSIGNED Ll L^_..'j_' J

PAGE OF

COMMENTS

j/;%H

< '

f

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\NUAL COUh

>JAL VOLUME

IPERVISOR P

TRACTS RE(

C.V.W>1 ^-gColvevTo,^

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t-cAJi. 3o<lle>87 (ni.Qc.

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COMPUCHEM * DO9687 FILE: GRD09687AO8 COMPOUND LIST 171SEMI-VOLATILE - MEDIUM LEVFL SOLID

PAGE

CMP*

49461O41160142142247442O6204126224424364404604386O660362941O6O244643V4754346O8477495435611626416478425402479401605607476427428424

M/E

15294931281461461081461084510870117771368213910712293162ISO12812722410714216423719619616265163152138153184109168165165149

F

I

I

I

COMPOUND NAME SCAN

614

D4-1,4-DICHLOROBENZENE (IS# 505PHENOL <Q1*3>BIS(2-CHLOROETHYL)ETHER (Ql2-CHLOROPHENOL (Ql#6>1>3-DICHLOROBENZENE <Q1*7>1.4-DICHLOROBENZENE <Q1*8>BENZYL ALCOHOL <Q1#9>1,2-DICHLOROBENZENE (QlttlO)2-METHYLPHENOL <-l#ll>BIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOL (Ql#13)N-NITROSO-DI-N-PROPYLAMINEHEXACHLOROETHANE (Qltl5>NITROBENZENE (Qlttl6>DS-NAPHTHALENE <IS*2>ISOPHOPONE <Q2«2>2-NITROPHENOL <Q2*3>2,4-DIMETHYLPHENOL (Q2#4)BENZOIC ACID (Q2ttS>BIS < 2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENOL <Q2#7>1,2,4-TRICHLOROBENZENE (Q2ttNAPHTHALENE <Q2#9>4-CHLOROANILINE (Q2*10)HEXACHLOROBUTADIENE (Q2#ll)P-CHLORO-M-CRESOL (021*12)2-METHYLNAPHTHALENE <Q2#13>D10-ACENAPHTHENE (IS#3>HEXACHLOROCYCLOPENTADIENE <2, 4,6-TRICHLOROPHENOL (Q3#32,4,5-TRICHLOROPHENOL <Q3#42-CHLORONAPHTHALENE (Q3t5)2-NITROANILINE <Q3#6)DIMETHYL PHTHALATE (Q3#7)ACENAPHTHYLENE (Q3#8)3-NITROANILINE <Q3#9)ACENAPHTHENE <03*10)2,4-DINITROPHENOL (03*11)4-NITROPHENOL (03*12)DIBENZOFURAN (03*13)2,4-DINITROTOLUENE (03*14)2,6-DINITROTOLUENE (03*15)DI ETHYL PHTHALATE (03*16)

771

AREA

168000

571000

307000

QUANTREPORTVALUE

40. 01 . 9

6Q Q

4O. 7

40. 0

70. 3

1-3-9- .§-

12. 2

7 .

20. 140. 0

tv2~

2. 5? A

6L /I

1. 8

REPORTEDAMOUNT(UC/KG)

7 — .*~L.fc_~ _\l /

1 m*^J^J^jQ N

BDLBDLBDLBDL

- BDL/ i f (itT.410000

BDLBDLBDL

BDL

7500OJ

ISO OOOBDLBDL

"'.aoeeeo

BDL1200O~J20OOJBDLBDLBDLBDLBDL

^66OOOJ

BDL

BDL

DETECT.LIMIT(UG/KG)

.j -fCC*' '

1 OOOOO1 OOOOO10000()1 OOOOO100000

1 OOOOO100000100000

1 OOOOO1000001 OOOOO

1000001 OOOOO

/y<_ i5°r°C)(l

1 OOOOO1000001 OOOOO1000001000001 OOOOO1 OOOOO100000

100000i ooooo50000010000050OOOO1000001 OOOOO50000O

5OOOOC5OOOOO1000001 OOOOO100000100000


DATE


18756 87 SAMPLE DPTP PPCKPGE

COMPUCHEM * D09687 FILE: CRD09687A08 COMPOUND LISTSEMI-VOLATILE - MEDIUM LEVEL SOLID

171 PAGE

CMP* M/E F

417 204432 16648O 138467 188 I6O4 198443 169414 248433 2836O9 266444 1784O3 178426 149431 202459 240 I445 202415 149423 252405 228413 149418 228497 264 I429 149407 2524O9 252406 252437 276419 278408 276619 112 S612 99 S447 82 S448 172 S628 330 S496 244 S471 212 S456 216CHECKSUMS:

9O5

1151

COMPOUND NAME SCAN

4-CHLOROPHENYL PHENYL ETHERFLUORENE (Q3*18)4-NITROANILINE (Q3*19)D10-PHENANTHRENE (IS*4)4, 6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE (04*4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENE (04*5)PENTACHLOROPHENOL (04*6)PHENANTHRENE (04*7)ANTHRACENE (04*8)DI-N-BUTYL PHTHALATE (04*9)FLUORANTHENE (04*10)D12-CHRYSENE (IS*5)PYRENE (Q5*3)BUTYLBENZYL PHTHALATE (05*43, 3'-DICHLOROBENZIDINE (05*BENZO(A)ANTHRACENE (05*6)BIS(2-ETHYLHEXYL) PHTHALATECHRYSENE (05*8)D12-PERYLENEDI-N-OCTYL PHTHALATE (06*2)BENZO(B)FLUORANTHENE (06*3)BENZO(K)FLUORANTHENE (06*4)BENZO(A)PYRENE (Q6*5)INDENO(l/2,3-C,D)PYRENE (Q6DIBENZO(A,H)ANTHRACENE (06*BENZO(G,H,I)PERYLENE (06*8)2-FLUOROPHENOL (SS*1)D5-PHENOL (SS*2)D5-NITROBENZENE (SS*3)2-FLUOROBIPHENYL (SS*4)2,4,6-TRIBROMOPHENOL <SS#5)D14-TERPHENYL (SS*6)D10-PYRENE1,2-3, 4-TETRACHLOROBENZENE

1363

QUANT REPORTEDREPORT AMOUNT

AREA VALUE (UG/KG)

t.t.-^-BDL3. 7 Li' 9700QJ

BDL58000 40 0

BDLT— 1 51 OOOJ


IO6OOO 40. 0BDLBDL

1 1 1 1 nnn iBDLBDLBDL

!9OOOO 4O. 0BDLBDLBDLBDLBDLBDLBDL

10. 5 5211.7 58.8. 6 86.10. 2 102.6. 3 32.9. 9 99.9. 3 93.

BDL

DETECTLIMIT(UG/KG)

1000001 OOOOO5000OO

500000* **^rt/~l/\/\1 OOOOO1000001000005000001000OO1000OO1000001000OO

1 OOOOOLOOOOO

10000010OOOO1 OOOOO

1000001000001 OOOOO1000001000OO1000001 OOOOO

y.y.y.y.y.%y.

10000

13334. 5309 2100000. 709 4 40295?;


DATE


//

18756 87 SAMPLE C'PTP PPCKPGE

COMPUCHEM * D09687 FILE: CRD09687A08 COMPOUND LIST 171SEMI-VOLATILE - MEDIUM LEVEL SOLID

PAGE

QUANTCC REPORT


72 619 2-FLUOROPHENOL (SS*1) 10.573 612 D5-PHENOL <SS*2) H.774 447 OS-NITROBENZENE (SS*3> 8. 675 448 2-FLUOROBIPHENYL <SS*4) 10.276 628 2, 4, 6-TRIBROMOPHENOL <SS*5) 6.377 496 D14-TERPHENYL (SS#6) 9.978 471 D10-PYRENE 9. 3

QUANTREPORTAMOUNT y. ++ CONTROLSPIKED RECOVERY RANGE

20. 020. 010. 010. 020. 010. 010. 0

52.58.86.102.32.99.93.

25-12124-11323-12030-11519-12218-13717-125* X

* ADVISORY SURROGATE ONLY«•+ •/. RECOVERY = QUANT REPORT VALUE / QUANT REPORT AMOUNT SPIKED X 100 '/.


FINAL EXTRACT VOLUME (ML) LOG DRY GC/MSx X WEIGHT X DILUTION X 2000

SPLIT FACTOR (*> AMOUNT EXTRACTED(O) FACTOR FACTOR

;**1. OML 1. OC i 6o 5. 0 J /f..' - /

X X X — X 2000 »-iOQQO. Q—1. 0 ML 1. 000


1000 UL FINAL EXTRACT VOL (ML) GCMSx x DILUTION X 2 =


1000 UL 1. OML 5. 0X X X 2 - 10. 000

1000 UL 1. 0 ML

VERSION

CORRECTED/REVIEWED BY(GC/MS DATA REVIEWER)

/DATE ' /"

18756 87 SAMPLE DATA PPCKPGE 371

Chem IDS 309537 Client IQt ECeiMatr i.- Spike ' MS ' 31 3757

Matr-iv Spike Duplicate *'MSO'< 3105^5BlanK Spike ( BS) 31057.Method Blank * 3'148'

Case: 18756.7Method: Semi v o l a t i l e

Matr i< : So 11

The semivolatile fraction of the samples shown above requi^ec!preparations and analyses. Due to high levels of organic componentsoriginal sample matrix. Medium Level Solid, as well as Low Level, prejwere required. Further dilution was required of the Medium Level _ - t r a c 4

concentrations of target compounds which exceeded the analytical angeinstrument. The method blank associated with the above samples from triee-traction failed to meet surrogate recovery criteria. Since all the saas well as the blank spike, met all surrogate and QC criteria, weconcluded that the unacceptable surrogate recovery in the method blankisolated situation relating to an error in the addition of the surspiking standard. Results indicate the standard was inadvertently e.ddeaTaking this into account and adjusting the results to reflect theaddition, surrogate recoveries fall within the acceptance l i m i t s . Fsample preparation could not be performed within holding t i m e , thereforare reporting these data with reference to this quali fying notice.

-a t i c " =4 ~ - f-

- f • t-e

* h i .•—'

"Dies ,'n? v _

was er

5IE S. BVPD, Employee 1.0. «524, 6C/MS Semivolatile Data ReviewerM/90

Approval *]029

i l l ' / A s s u r a n c e S p e c i a l i s t

18756 87 SAMPLE DATA PPCKPGE

C. STANDARDS DATA

(1) Initial Cattbratton Data (Form VI SV-1 ,SV-2)-to order by Instrumentif more than one Instrurnent used.

(a) BNA standard (s) reconstructed ion chromatograms andquanthatton reports (or legtoto facsknle) for theInitial (five point) caHbratton. Spectra are notrequired.

(b) AH Initial caltoratfon data must by Included, reganJessof when It was performed and for which case. When morethan one initial calibration Is performed, the data mustbe put in chronological order, by Instrument.

(2) Continuing CaHbration (Form VII SV-1 , SV-2) - In order by instrument,If more than one instrument used.

(a) BNA standard (s) reconstructed ion chromatograms andquantttation reports (or legMe facsimile) for allcontinuing (12 hour) caHbrattons. Spectra are not required.

(b) When more than one continuing caflbratton is performed.forms must be in chronological order, within fraction andInstrument.

(3) Internal Standard Area Summary (Form VIII SV-1 , SV-2) - in order byinstrument, If more than one Instrument used.

When more than one continuing caflbratton is performed, formsmust be In chronological order, by Instrument.

1S756 87 SAMPLE DATA PACKAGE 36*

(1) Initial Calibration Data (Form VI SV-1 ,SV-2)-to order by instrumentIf more than one instrument used.

(a) BNA standard (s) reconstructed ion chromatograms andquantttatkxi reports (or legMe facsimile) for theinitial (five point) caflbratton. Spectra are notrequired.

(b) AH Initial canbration data must by included, regardtessof when It was performed and for which case. When morethan one initial caflbration is performed, the data mustbe put to chronological order, by instrument.

18756 07 SAMPLE DATA PACKAGE 36S

6BSEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: COMPUCHEM LABS Contract: r2-88.-REVS

Lab Code: COMPU Case No.: 18756 SAS No.: SDG No. : 07

Instrument ID: 08

Min RRF for SPCC(#) = 0.050

Calibration Date(s): 11/21/89 11/21/89

Max %RSD for CCC(*) = 30.0^

LAB FILE ID: RRF20RRFfiO — HHRQ1 1 ? 1 Af)8 RRFT?f

COMPOUND

Phenol *bis ( 2 -Chloroethyl ) Ether2-ChloroDhenol1 , 3-Dichlorobenzene

= HK891121A08 RRF50 = HG891121A08)= HI891121A08 RRF160= HJ891121A08

RRF20

* 1.9551.9011.4681.682

1 . 4-Dichlorobenzene * 1.515Benzyl Alcohol1 , 2-Dichlorobenzene2-Methvlohenolbis(2-Chloroisopropyl) Ether4 -Methy IphenolN-Nitroso-Di-n-Propylamine_HexachloroethaneNitrobenzeneIsophorone

0.8551.5091.2402.7791.244

\ 1.3770.8250.6201.150

2-Nitrophenol * 0.2322 , 4 -Dimethy IphenolBenzoic Acidbis ( 2-Chloroethoxy ) Methane_2 , 4-Dichlorophenol '1 , 2 , 4-TrichlorobenzeneNaphthalene4-Chloroaniline

0.4680.1140.589

* 0.3210.3791.1250.416

Hexachlorobutadiene * 0.2224-Chloro-3-Methylphenol * 0.3862-Methylnaphthalene 0.720Hexachlorocyclopentadiene # 0.3132 , 4 , 6-Trichlorophenol * 0.3912,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethyl PhthalateAcenaphthylene2 , 6-Dinitrotoluene3-Nitroaniline

0.3971.3120.4081.3871.7660.2480.236

Acenaphthene * 1.1702 , 4-Dinitrophenol4-Nitrophenol

1 0.103» 0.153

RRF50

1.7441.7061.3911.5851.4080.8651.3881.1802.6801.2621.3490.8310.6271.1490.2440.4150.1790.6070.3350.3661.0650.3420.2200.4780.7190.3590.3850.3751.1440.5071.3911.5390.2670.2181.1140.1010.193

RRF80

1.6781.7701.4001.6351.4190.8901.4191.1422.5311.2171.2560.8840.5581.0950.2360.4440.1860.5760.3250.3661.0010.4570.2150.4340.6810.4060.4000.3831.2150.5321.4431.5680.2820.2351.1220.1150.212

RRF120

1.5021.6801.3331.5191.4000.8451.3801.0592.5281.1631.2390.8470.5260.9960.2160.4120.2090.5310.3080.3360.9510.4280.2020.4270.5990.4110.4000.3701.1430.5481.3401.4350.2720.2681.0620.1190.228

RRF160

1.3591.6721.3451.4551.3840.8411.3551.0502.6141.1621.2320.8840.4950.9540.2100.4000.2070.5150.2910.3240.8270.4190.1950.4100.5430.4190.3900.3841.1100.5601.3371.3980.2780.2741.0730.1120.215

RRF

1.6481.7461.3871.5751.4250.8591.4101.1342.6261.2101.2910.8540.5651.0690.2280.4280.1790.5640.3160.3540.9940.4120.2110.4270.6520.3820.3930.3821.1850.5111.3801.5410.2690.2461.1080.1100.200

%RSD

13.9*5.43.95.73.6*2.34.27.14.03.85.2*3.3

10.28.46.2*6.5

21.66.95.4*6.511.510.35.6*8.0*

12.011.8*1.7*2.76.8

11.93.29.44.99.73.9*7.0*14.6*

FORM VI SV-1 1/87 Rev.

18756 07 SAMPLE DATA PACKAGE

6CSEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS


Instrument ID: 08

Min RRF for SPCC(#) - 0.050


Max %RSD for CCC(*) = 30.0%

LAB FILE ID: RRF20 = HK891121A08 RRF50 = HG891121A08RRF80 = HH891121A08 RRF120= HI891121A08 RRF160= HJ891121A08

COMPOUND

Dibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenylether_Fluorene4-Nitroaniline4 , 6-Dinitro-2-Methylphenol_N-Nitrosodiphenylamine (!)_'4-Bromophenyl-phenyletherHexachlorobenzene

RRF20

1.5970.3241.3590.5981.2150.1930.092

* 0.5530.2450.299

Pentachlorophenol * 0.082PhenanthreneAnthraceneDi-n-Butvlchthalate

1.0661.0261.399

Fluoranthene * 0.969PvreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo (a) AnthraceneChrvsenebis ( 2-Ethylhexyl ) Phthalate_Di-n-Octyl Phthalate 'Benzo (b) FluorantheneBenzo (k) Fluoranthene

1.4550.7090.2061.0761.0150.992

^ 1.6121.2141.094

Benzo (a) Pyrene * 1.004Indeno (1.2. 3-cd) PyreneDibenzo ( a , h) AnthraceneBenzo (a . h . i ) Perylene

Nitrobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d52-Fluorophenol2.4. 6-Tribromophenol

1.2111.0241.034

0.6021.3921.1201.8181.6320.144

RRF50

1.4720.3221.4170.5591.0120.2020.1030.4470.2230.2580.1150.9600.9361.4410.9581.2540.7850.1191.0890.7561.0391.8071.3030.7850.9251.0820.8850.888

0.6001.1301.0031.8111.6270.160

RRF80

1.5180.3451.5370.5721.0100.1580.1110.4690.2360.2730.1131.0031.0241.5140.9591.2860.7940.1381.1500.8771.0591.9371.3320.8711.0371.2521.0021.043

0.5641.1491.0311.8291.6870.178

RRF120

1.4120.3331.4690.5450.9410.1570.1130.4370.2220.2570.1200.9610.9211.3340.9311.2400.8220.1221.1450.9241.0441.9941.1641.0491.0141.1760.9050.962

0.5631.0831.0341.6411.6790.174

RRF160

1.4300.3221.4060.5420.9110.1790.1180.4410.2330.2630.1230.9730.9801.4160.9431.3240.8750.1201.1840.8851.0881.9571.2580.9471.0011.1830.9300.981

0.5121.0301.1061.6481.6010.174

RRF

1.4860.3291.4380.5631.0180.1780.1070.4690.2320.2700.1110.9930.9771.4210.9521.3120.7970.1411.1290.8911.0441.8611.2540.9490.9961.1810.9490.982

0.5681.1571.0591.7491.6450.166

%RSD

5. 03.04 .74.1

11.711.49.5

10. 3*4.16.4

14.8*4.55.04.61.6*6. 67.6

26.44.0

10.53.38.4*5.4

13.34.2*5.36.46.4

6.412.04.85.52.28.5

;i) Cannot be separated from Diphenylamine


18756 87 SAMPLE DATA PPCKPGE obb

COMPUCHEM LrtBSRIC11--21/89 ll:49:oo

: lUL SEHI2

COHPUCHEM OrtTA: Hh'.39112irt83 SCW5 345 TO 1?00OUT OF 345 TO 17u6

1(3 fv

1147

IJJ'J

15:16

—IHIM21:23

1218559.

— " isn'. SS92

-

J. RIC

463

ISI2

SSI3

1'54

593

7

ISI3 SSI5 SSI6 IStS

SSI4 D3I1 IS44 SSI7 . 1516

7

664

773 . . !

i

'. • 9-

»:

4

.

J8.

•

7 ;

12«8

J

—IJMMJ24:26

IT'•£•n

LU

•1CL

•IK1

LU-J0.

'/I

inr.•X"

TIME

QUANTITATION REPORT FILE. HK891121AOBDATA: HKB91121ACB. I I11/21/39 11:49:00SAMPLE: 1UL SEMI2 bSTDOSO 30406(2364) ONttOSCONDS. :SUBMITTED 3Y: OS ANALYST: 1090

AMOUNT-.'.REA • REh . A^T/CREF. AREA)* RESP. FACT)RESP. FA'. FROM LI«R~RY ENTRY

NO NA!--r1 »494 D4-l,4-DICHi.OFfOBENZENE (15*1)2 610 PHENOL (01*3) C10B-95-2>3 411 BIS<2-CK.03GETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHCNOL (01*6) <95-57-B>5 421 1,3-DlCHLOROLENZENE (01*7) <541-73-l>6 422 1,4-DICKLOSQIiENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (Qlf9> <100-5l-6>8 420 l,2-DICN_0*3DENZENE (01*10) <95-50-l>9 620 2-METH'rL PHENOL (Ql*ll> <95-48-7>

10 432 BIS(2-CHL090ISOPROPYL)ETHER (01*12) <39638-32-9>11 6?2 4-METHViPHCNOL (01*13) <106-44-5>12 4^2 N-NITROSO-n-N-PROPYLAMlNE (01*14) <621-64-7>13 436 HEXACHLCr70tTHANE (01*15) <67-72-l>14 440 NITRODBMZtrNE (01*16) <98-95-3>15 »46C D8-NAPHTHALENE <IS*2)16 439 ISOPHORC^E (QI«2) <78-S9-l>17 606 2-NlTRC»HENO:_ <Q2*3) <BB-75-S>IB 603 2.4-DlMs.THVLPHENOL (02*4) <105-67-9>19 625 BENZO1C ACID (02*5) <65-B5-0>20 410 B1S<2-CHLORO£THOXY)HETHANE (02*6) <111-91-1>21 602 2,4-DlCHLC!»OPnENOL (02*7) <120-B3-2>22 446 1,2. 4-TRlCK.O»OBENZENE (02*8) <120-B2-1>23 439 NAPHTHALENE <OI*9) <91-20-3>24 475 4-CHLOROAML1NE (02*10) <106-47-8>25 434 HEXACHwO^ODUTAMENE (02*11) <87-68-3>26 608 P-CHLOFO M CRcSOL (02*12) <59-50-7>27 477 2-T1ETHvi NAPHTHALENE (02*13) <91-57-6>26 »495 DIO-ACPNAPHTHENE (IS«3)29 435 HEXACHLOSCCYCLOPENTADXENE (03*2) <77-47-4>30 611 2, 4, 6-TP1CHLWCPHENOL (03*3) <88-06-2>31 626 2,4,5-TRICHLDfcDPHENOL (03*4) <95-95-4>32 416 2-CHLORC:-IAPHTHALENE (03*5) <91-5B-7>33 478 2-N1TROAMLINE (03*6) <88-74-4>34 425 DIMETHVL FHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYi EXE (03*8) <208-96-8>36 479 3-N1TROAN1I INE (03*9) <f9-09-2>37 401 ACENAPHTHtNE (03*10) <B3-32-9>38 €605 2. 4-D1NITROPHENOL (03*11) <51-2B-5>39 607 4-N1TROPHENOL (03*12) <100-02-7>40 476 DIBENZCFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE <03tl4) <121-14-2>42 42B 2,6-DINITROTOLUENE (03*15) <606-20-2>43 424 DJETHYL PHTHALATE (03*16) <B4-66-2>44 417 4-CHLORDr'Ki.NYL PHENYL ETHER (03*17) <7005-72-3>45 431 FLUOPEN- <G3*16) <B6-73-7>46 480 4-NITRO v >!I i 1NE (03*19) <100-01-6>

1S756 07 SAMPLE DATA PPCKPGE 564

NO474849505152535455565758596061626364656667666970717273747576777E79

NO1234c.

67891011121314151617IE192021

604 4. 6-DINIlRO-2-«ETHYLPHENOL (04*2) <534-52-O443 N-NirRCSODlKHE.r,YLAMINE (04*3) <86-30-6>414 4-BROttC'PHENYu PHENYL ETHER (Q4*4) <10l-55-3>433 HEXACHLOSOBENZENE (04*5) <118-74-l>609 PENTACH.J3ROPHENOL (04*6) <87-86-5>44«! PH£NANTH«E*F (04*7) <85-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUIVL PHTHALATE (04*9) <84-74-2>431 FLUOR AMTHENJ- (04*10) <206-44-0>*4S9 D12-CHSYSEKE (IS*5)443 PYRENS <Q3*3/ <129-00-0>413 BOTVLBEUZYL PHTHALATE (05*4) <85-68-7>423 3. 3'-DICHLOR08ENZIDINE (05*5) <91-94-l>405 BENZO (A) ANTHRACENE (05*6) <56-55-3>413 BIS(2-£THVLH£WL> PHTHALATE (05*7) <117-8l-7>418 CHRYSEK't (Q9«S> <21S-01-9>*497 D12-PEKYLFWE429 DI-N-OCli'L PHTHALATE (06*2) <117-B4-0>40? B£NZO<3)FLIJ3«ANTHENE (06*3) <205-99-2>409 BENZO (*)FL'->39AKTHENE (06*4) <207-08-9>406 BENZO(A)PYR£^e (06*5) <50-32-8>437 1NDENO <1, 2, 3-C-D) PYRENE (06*6) <193-39-5>419 D 1BEMZCK A, H) ANTHRACENE (Q6*7) <53-70-3>40S BENZOC3.H, I)FEFYLENE (06*8) <191-24-2>*619 2-FLUO*OFH£\3L (SS*1>*61=» DS-PHECOL (SS«2>*4-r,7 DS-NITP.OBENZEfcE <SS*3>

*62S 2. 4. 6-TRI_R_rOPHENOL (8S*5> l/ -**U96 D14-TERPHEUVL (SS*6) (•*»!** ''

4*6 1,2,3. 4-TE i RACHLCROBENZENE

M/E152949212E146146106146109451067011777136621391071 ?293162

SCAN469440447453466 -471 s483,-483"'495 <-498508 /510518525593547 f556560568 "569560

Tir.£7: 106: 436: 506: 557:U77: 127: 237:277:347:367:457: 477:556:019:036: 218:296: 326: 408: 416: 51

REF1111111111111

1515151515151515

RRT1. 0000. 9380. 9530. 9660 9941. 0041. 0301. 0411.0551. 0621.0631 0871 1040 6651. 0000. 9220 9380. 9440 9580. 9600 978

METHA B3A 3VA BVA BBA BVA VBA BVA BBA VCA BBA BBA BVA BBA WA BVA BVA BBA BVA VVA BWA BB

AREA < HGHT )192028187684.182520.140980.161536.145428.62116.144932.119056.266844119436.13216479176.172084.555500.319436.64520129996.31578.163556X89284.

AMOUNT40.28.22.21.2321.20.22.23.21.21.22.18.25.40.24.22.23.10.22.22.

000777745842123889338276623263412345657043000102075408989886117

NGNGNGNGNGNCNGNGNC-NGNGNGNCNGNGNGNGNGNGNGNG

XTOT2. 241. 611. 271. 221. 291. 221. 141. 251. 321. 191. 201. 251 041. 402 241. 351. 231. 310. 611. 281. 24

18756 07 SAMPLE DATA PPCKPGE ..- b o

NO22232425262726293031323334353.37383940414243444546474849SC-SI5253545556575859606162626465666768697071727374757677

M/EISO12812722?1071421642371961961626516315213S1531841091651651651492041661381SS19816924828426617617814<?2022402021492?=>22814*22S26414925'2522522762782761127?8217232024'!

SCAN583595'601613650664773 -688695'699 x

714727748757769776779786793795*755-820828829-63292783884C878895913929"934"990105612081080-11471202I206-"12091210'-137312711323"1325"136515J315551608360439

TIN:8: 599: 059: 119: ?29: 5610:0811:4810:3010: 3710:4010: 5411:0611:2511: 3411:4511:5111:5412: CO12: 07I?: 0311:3212: 31)2:391^:4012: *214:091=-:4SIS: 5013:2413 4013: 5£14: 1114: 1615: 0716:0716:2716:2917:3116 21IS 2516 26IS: 29SO: 5819:2420: 1220. 1420: 5123:4323: 4524:335:306:<*2

523 , 7: 59703 10: 448551094

13: 0316: 42

REF1515151515152628IB2628282828282828282828181-6282828474747474747*74747*7••75757575757?7646464646464646411

15282357

RRT0 9921. 0031. 0131 0341. 0961. 1201. 0000. 8900 8990 9040 9240. 9400.9680. 9790 9951 0041. 0081 0171. 0261.0280. 9771 0611. 0711.0721 0761. 0000 9040. 9060 9470. 9650. 9851 0021. 0031. 0681. 1391 0000. 8940 9500. 9950. 9981 0011. 0021. 0000 9260. 9640. 9650. 9941. 1311. 1331 1710 7680. 9360. 6820 9091. 1060 906

METHA KBA BVA VBA BBA BbA VVA -BA 85A BVA VVA RBA BVA B3A 96A BVA BBA 8VA VVA BBA BBA BDA BVA BBA BBA BVA 8BA BBA EBA BBA 83A BBA BVA VBA BBA BBA BVA BBA UDA BBA BVA BVA VVA 8VA BVA 8VA VVA BVA EBA PBA BVA BVA BVA BVA BBA LBA 8V

AREA<HGHT)105216.312456.115504.61668107108.199868.282576.44292.551BB<"56073.165412.57652.195964.249500.33296.165340.14496.21664.225576.'"45736.35008.192024.644B8.171596.27316.375412.17344.103848.45936''56124.15384.

200184.192576.262556.181956.243876.181060.8826425624X

133904.123403.126360.194076.156404.117764.106136.97392.117524.99340 /100348156715.174564.167104.196664.20334139340

AMOUNT23.27.19.22.18.26.40.14.20.20.23.14.20.25.17.21.18.14.22.20.17.19.22.26.21.40.15.25.20.22.13.21.20.19.20.40.21.16.34.18.18.22.40.16.19.23.20.20.22.21.20.22.23.27.16.20.

401213872764808491000978047662641563741265184603350262330111834330083675584000628080964705305924934760553000985219264179223950000469293102053477012075395067504019596254

NGNCNCNGNGNGNGNGNGNGNGNGNGNCNGNCNCNGNCNGNGNGNGNGNCNGNGNGNCNGNGNGNGNGNGNGNGNGNGNGNGNGNCNCNGNGNGNGNGNGNGNGNGNCNCNC

XTCT1. 311 521 111. 271 051. 482 240. 841. 121. 161. 320. 811. 161. 410. 961. 221. 030. BO1. 251. 131. 001. OS1. 241. 491 212. 240. 871. 401. 171. 270. 741. 231. 171. 111. 152. 241. 230. 911. 921. 021. 021. 282. 240 921 081. 291. 121. 151. 231. IB1. 141. 231. 311 510 931. 13

18756 07 SAMPLE DATA PPCKPGE _> 6

NC7879

NO1234567B910111213141516171619202122232425262726293031323334353637363940414243444546474849505152

M/E SCAN TI;',ir REF RRT KETH21? 1078 16:23 57 0.692 A B V216 715 10:55 28 0.925 A BB

RET<L)7: 126:476:536: 567: 107: 147:267:317:377:407 507: 527:576:059:078: 268: 338:37B: 508:458: 559:029:099 149 259:5910: 1211: 5110: 3410: 4010: 4410: 5811: 0911: 281 1 3711:4711: 5511 5712 0312 0912: 1111: 3412: 3412:4012 4112: 4514: 1012: 5012: 5113 2613 4113 57

RATIO RRTvL)0. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990.990. 990. 990. 990. 990. 990. 990. 990. 980. 990. 990. 990. 990. 990. 990. 990. 991. 000. 990. 990. 990. 991. 001. 000. 991. 000. 990. 99. 00. 00. 00. OO. 00. 00

1. 001. 001. 001. 001. OO1. 001. 001 00

10. 00010. OC'O10. 00010. 00010. OOd10. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00050. OCO10. OC'C10. 00010. 00010. 00010 00010. OOC10. 00010 00 D10. 00010. 00010. 00050. 00010. OC'O50 0 010. OSO10. 00050. OCO10. OC'O50. 00050 00010. OOO10. 00010. 00010. 00010. 00010. 00050. 00010. 00050 00010. 00010. OC>010. OC'O50. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100 100. 110. 110. 110. 110. 110.090. 100 090. 090. 090. OS0. 100. 100. 100. 100. 100. 100. 110. 110. 100.090. 090. 020. 090. 020. 100. 100. 020. 100. 020.020. 100. 100. 100. 110. 110. 110.020. 100. 020. 090. 090 100. 02

AM\T40.26.22.21.23.21.20.22.23.21.21.22.18.25.40.24.22.23.10.22.22.23.27.19.22.16.26.40.14.20.20.23.14.20.25.17.21.18.14.22.20.17.19.22.26.21.40.15.25.20.22.13.

0078746412893426622641346604001008419969)240218776814900980566645674271860352633116333066756006308967031

AREA(HGHT) AMOUNT146908. 18. 491 NC45840. 25. 232 NG

ANNT(L)40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160160160.160.160

00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)1. 0000. 2440.2380. 1840. 2100. 1B90. 1070. 1890. 1550. 3470. 1550. 1720. 1030. 0771. 0000. 1440. 0290. 0590. 0140. 0740. 0400. 0470. 1410. 0520. 0260. 0450. 0901. 0000. 0390. 0490. 0500. 1640. 0510. 1730. 2210. 0290. 1460. 0130. 0190. 2000. 0400. 0310. 1700. 0750. 1520. 0241. 0000. 0120. 0690 0310. 0370. 010

1. 0001. 3591. 6721. 3451. 4551. 3840. 8411. 3551. 05C2. 6141. 1621. 2320. 8640. 4951. 0000. 9540. 2100. 4000. 2070. 5150. 2910. 3240. 8270. 4190. 1950. 4100. 5431. 0000. 4190. 3900. 3841. 1100. 5601. 3371. 3960. 2741. 0730. 1120. 2151. 4300. 3220. 2781. 4060. 5420. 9110. 1791. 0000. 1180. 4410. 2330. 2630. 123

XTOT1. 031. 41

RATIO1. CO0 160. 140 140. 140. 140. 130. 140. 150. 130. 130. 140. 120. 161. 000. 150. 140 150. 070. 140. 140. 150. 170. 120. 140. 120. 171. 000 090. 130. 130. 150. 090. 130 160 110. 140. 110. 090. 140. 130. 110. 120. 140. 170. 131. 000. 100. 160. 130. 14o. oe

1S756 07 SAMPLE DATA PPCKPGE 361

NO535455565756596061626364656667686970717273747576777679

RtT<L)14: 1214: 1715 0816: 0718 2816 3017.3218:2218: 2618 2818:2920:5819:24SO: 1320 1620: 5223: 4623 4624:355: 336:468:0310 4813:0516 4316: 2910: 59

RATIO RRT%L>1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 00.00.00.00. 00.00. 00

1. 001. 000. 990. 990. 990. 991. 001. 001. 000. 99

10 00010. 00010. 00010. 00010. 00010. 00010. 00020. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. OOC10. 00010. 00010. 0000. 7410. 9-5 S0. 6750. 9061 1160. 90-10. 0001 . 000

RATIO0. 100. 100. 110. 110. 100. 090.090. 050. 100. 100. 100. 100. 090. 100. 100. 100. 110. 110. 121. 030. 991. 011. 000. 991. 000. 090. 92

ANNT21.20.19.20.40.21.16.34.161622.40.16.19.23.20.20.22.21.20.22.23.27.16.20.18.25.

929376550099?22618?29500472910054801084007500260254923

AMNT(L)160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160160.160.

000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)0. 1330. 1280. 1750. 1211. 0000. 1820. 0890. 0260. 1350. 1240. 1271. 0000. 2010. 1520. 1370. 1250. 1510. 1280. 1290. 2040.2270. 0750. 1740. 0180. 1400. 1480. 041

0. 9730. 9801. 4160. 9431. 0001. 3240.8750. 1201. 1841. 0860. BBS1. 0001. 9571. 2580. 9471. 0011. 1830. 9300. 9811. 6011. 6480. 5121. 0300. 1741. 1061. 2770. 257

RATIO0. 140 130 120. 131. 000. 140. 100. 210. 110. 110. 141. 000. 100. 120. 140. 130. 130. 140. 130 130. 140. 150. 170. 100. 130. 120. 16


COMPUCHEMRIC11/21/89 8:32:00SAMPLE: 1UL SEMI 2 SSTH850 3ti40rC2365> GN*08COHOS.:

COI1F-IJCHEI1 DATA: Hr_89_121ft06 SCftMS 332 TO 1832OUT OF 332 TO 2200

IS til IS* 2

SS»2 SS93

I $13 SS#5

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RIC COMPUCHEM DATA: HG891.21IW8 SCANS 1832 TO 2200 n

11/21/89 8:32:00 OUT OF 332 TO 2200SAMPLE: 1UL SEMI2 5STD650 30407X2365> OMWfiCONOS.: 272E.956.

1972 20711 ' I

2666 2266 SCnH38:32 33:36 TIME

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QUANTITATION REPC'T FILE HG891121AOBDATA: H5B9 1121 ACS. T I11/21/89 8:32:00SAMPLE: 1UL SEKI2 bSTDOSQ 30407(2365) ON*08CONDS. :SUBMITTED BY: OS ANALYST: 1090

AMOUNT-AREA * REt- . A./ T/ (REF. AREA)* RESP. FACT)RESP FAC. FRCtt LlbRARv ENTRY

NO NA.-C1 *494 D4-1, 4-DICHLDROBENZENE (IS*1>2 630 PHENOL <G1*3> <108-95-2>3 411 BIS(2-CHLOSO£THYL)ETHER (Ql*5) <lll-44-4>4 601 2-CHLOROPHCNOL <G1*6> <95-57-8>5 421 1,3-DICKLOPOBENZENE (01*7) <541-73-l>6 4=>2 1, 4-DICK.030BENZENE <Q1*8> <106-46-7>7 474 BENZYL ALCOi'.CL <G1*9> <100-51-6>S 420 1,2-DICHLORCr.ENZENE <Q1*10) <95-50-l>9 620 2-METH-iLPKlNDL <G1#11) <95-48-7>

10 412 BIS<2-CI-^C!ROI5DPROPYL)ETHER <_1*12) <39638-32-9>11 6?2 4-METHvLPHsNOL (01*13) <106-44-5>12 442 N-NITROBCf-DI-N PROPYLAMINE «il#14) <621-64-7>13 436 HEXACHLC^CiTH^NE (Q1H15) <67-72-l>14 440 NITROBFNZfcNE ( 01*1 6) <98-95-3>15 *460 DS-NAPHTHALEN'E <IS*2)16 435 ISOPHORC;JE <G£»2) <78-59-l>17 606 2-NITRC'HEriOL (G2#3) <S3-75-5>18 603 2- 4-Dlr^STHYLrriENC1.. <Q2*4) <105-67-9>19 62? BENZO 1C ACID (&2*5) <65-85-0>20 410 BIS<2-Ci-iLC~;0£Ti-loXY)nCTHANE <«2#6) <111-91-1>21 602 2, 4-DICr,LCt?OPHcNOL <Q2*7) <120-83-2>22 JAA. 1, 2. 4-TRICHLGrODENZENE <02#8) <120-82-l>23 439 NAPHTHA" ENC <Qr#9) <91-20-3>24 475 4-CHLDPCAi-iIL:NE <Q2*10) <106-47-S>25 434 HEXACHLC.^OD'J'AI IEN£ <Q2#11) <67-68-3>26 60S P-CHLOKO M-CRESOL < 02*12) <:59-5O-7>27 477 2-MtTH¥L?iAPH7HALENE < 02*13) <91-57-6>

2s? 43; uerVACHi_0"OCYCLGPENTADIENE (Q3«2) <77-47-4>30 611 2 - 4 . 6-":_ CHLD»:_PHEN2L <Q-3#3) <B8-06-2>31 62o 2, <», 5-TRICK.ncn.PHENOL (Q3#4) <95-95-4>32 416 2-CHLCrw.-<-»K:HALENE <Q3t5) <91-58-7>33 47s 2-NITRO->NILI'.E (Q3*6) <88-74-4>34 425 DIMETHfL PHTHALATE <Q3*7) <131-ll-3>35 402 ACENAPHiHYLENE (03*8) <20B-96-B>36 479 3-NITROA?!It. 1NE (03*9) <99-09-2>3 401 ACENAPHTHPNE s_3*10) <83-32-9::-36 «±05 2. 4-DIMTROPHENOL (.3*11) <51-28-5>39 607 4-NnRCr-!!ENDL, (03*12) <100-02-7>40 476 D1BENZC; URAN (03*13) <132-64-9>41 427 2- 4-DINITROTO' UENE (03*14) <121-14-2>*2 425 2, 6-DI.MTROTOL'JENE «_3*15) <606-20-2>43 424 DIETHYL PHIHALATE (03*16) <84-66-2>-14 417 4-CHLDPC'='Hi.NYi. PHENYL ETHER (Q3#17) <7005-72-3>4? 432 FLUORENE (G3»»J8) <B6-73-7>46 460 4-NITRD-v;iLlNE <Q3*19) <lOO-01-6>


NC474849505152535455565758596061626364636667686970717273747376777879

NO1234567e91011121314151617IB192021

NAI1S*467 DlO-PricNANtHPENE (13*4)604 4, 6-DI.NlI i^C-i-KETHYLPHENOL (Q4*2) <534-52-l>443 N-NITRCrQDIP.-iEKYLAKINE (Q4*3) <86-30-6->414 4-BROMC'PHDJYL PHENYL ETHER (Q4*4> <101-55-3>433 HEXACHLOÔDENZENE (Q4*5) <118-74-l>6C9 PENTACr!; OROPHENOL (04*6) <87-86-5>444 PHENANTHKEJxc (34*7) <8S-01-8;>403 ANTHRACtME (Q4»8> <120-12-7.>426 DI-N-B'JM'L PHTHALATE (Q4*9) <84-74-2>431 FLUQRAU i HEN'-.. <Q4*10> <206-44-0>*459 D12-CH*YS£NE (IS#5)445 PYRENS (05*3) <129-00-0>415 BUTYLSE^ZYL PHTHALATE (Q5*4> <85-68-7;>423 3. 3'-DICHLC30BENZIDINE (Q5*5) <91-94-l>405 B£NZO(A)A?41HRACENE <_5*6) <56-55-3>413 BIS(2-ETHYLHS.jrYL) PHTHALATE (0.5*7) <117-81-7>418 CHRYSE?;- (03«G) <218-01-9>

429 DI-N-OCTYL PHTHALATE (Q6*2) <117-84-0:>40 / BENZO(3)FLi;OffAUTHENE (Q6#3) <203-99-2>409 BENZO (jOFLUOFANTHENE (Q6*4) <207-08-9>406 BENZO(A>PYS£'<£ (06*5) <50-32-8>437 INDEM3 (1, 2, 3-C. DJPYREKE (Q6*6> <193-39-5>419 D I BENZO ( A, H) ANTHRACENE (36*7) <53-70-3>403 BENZO (S.H, I JPE? YLENE (Q6*8) C191-24-2>*619 2-FLU09CPK-.UOL (SS*1)*61=> DS-PHEÔL <3S«2> A,/,*4-:7 DS-NiTrosEîerrÊ (ss*3> lylAlo*-*-*448 2-FLUCROSIPHI-.NYL (SS*4) , /*62S 2, 4, 6-TRI3RDr'!aPHENOL (SS*5) //f^f^l*496 D14-TE9PHSNVL (SS*6)*471 DlO-PYIcENt4?6 1,2,3, 4-TE 1 RACHLOROSENZENE

M/E152949312814614610314610B45108701177/13652

13'-?107

12'93162

SCA-N472444450456469-"474467491'493 '502512 '514521328596551 '560563373 '572383

TirE7:6:6:6:7:7:7 :7:7:77:7:7:8:9:888.8:B8:

1247?256101426203640493137040£253336434454

REF1111111111111

1515151513151515

1.0.0.00.1.11.1.1.1.1.1.o.1.0.0.0.000

RRT000941933966994004032040055064085089104886000924940945961960978

METHAA

BBBV

A*BVAAAAAAAAAAAAAAAAAA

BBBVVD3VBBVVBVVVBVBBBVBVBVBtJBVVVBVBB

AREA(HCHT) AMOUNT240624.524552.513012.413263476664.423564.260150.417330.354955805952y379540.405728.249804.554711.7073081015710.215328.367108.157944.536432. /296612.

40.64.31.31.54.50.51.51.56.51.54.54.46.63.40.60.57.51.43.56.57.

000183013714453860419195206251300742975399000189861916166952705

NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG

'/.TOT1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.11.1.11.

016329313B29303042303339196101524731094946

18756 87 SAMPLE DATA PACKAGE 356

NO2223242526272829303132333435363738394O41424344434647464950515253345536575839606162636463666768697071727374757677

M/E180125127225107142164237196196162651631351361531S4109168163165149204166138IBB19316924328426617617814920524020214923222S1492582641492?5

2322522762782761129982172330244

SCAN592398 x-604 x-616653667776 -691699'702 x

7177307517617727807637SV796798'736 '823631832'836930641843881896916932-937-9931058 'J2101082 x

11491204120812101213 x-137312731323'1328/136815591560161536444352770685B1096

T I ' '•-..9:059: 039: 139: 249: 5810: 1111: 5110: 3310: 4010: 4310: 5711:0911: 261 1 3711: 4711: 5511: 3715; 03

12: 0915; H

11: 3412: 3412: 4115; 42

12: 4614: 1212: 3112: 3513: 2713: 4313: 5914: 1414: 1815: 10'16: 09IS: 29'16: 3117.33IS: 2316: 2716: 2916 3121 : CO19. 2620: 1420; 17

20: 5323: 4623: 4924: 405: 336: 46B: 0310 4713: 0616: 'i4

REF131315151515282828282828282828282828282828£8262828*7474747474747474747575737?7575737646464646464646411

1523IB"7

RRT0. 9931. 0031. 0131. 0341. 0961. 1191.0000. 8900. 9010 9050. 9240. 9410 9680. 9810. 9951 005I. 0091. 0171. 0261. 0280. 9771 0611 0711. 0721 0771. 0000 9040. 9060. 9470. 9660 9851 0021. 0081. O6S1 1381 0000. 8940. 9500. 9950 9981. 0001. 0021. 0000.9260. 9640. 9660 9951 1341 1351 1750. 7710 9390 8640. 9101 1060 906

KETHA BBA SVA V8A BBA BBA VVA BtiA UDA 3VA VVA BBA BVA BOA SBA BVA BBA BBA BVA BBA 32A BBA BVA D3A S*A VVA 30A 3DA 8VA BBA BBA BBA BVA VfcA BVA B3A 3DA BVA BBA BBA 3VA VVA VBA BVA BVA BVA VBA BVA BVA BBA 3VA BBA DVA DVA 3BA SBA DD

AREA<HGHT323352.941220.302744.194196422328.635708.408392.183720.196864.191600.584524.259156.710924.786584.111392.569356.51536.98480.752468.164648.136348.724132.285788.517476.103306.572664.73608.319628.1 59308.184324.82364.666862.670141.1031670.686097.398417.624754.390736.39124.342183.517323.376750.324103.732042.527708.318000.374617438322.358530.359597.48V375.544660.530552.577656.61616499565.

) AMOUNT56.64.40.56.58.66.40.42.49.48.51.45.52.55.39.51.45.44.31.30.48.50.51.55.56.40.43.50.47.48.46.49.47.50.50.40.47.44.49.45.47.42.40.4651.41.46.45.47.45.50.54.58.54.45.45.

517380906261242174000934420791506240000046729885084804478034072377622592412OOO461636662936698313755899804000363854385979721744000157769447188732571224826947609846921361

NGNGMSNGNGNGMGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNCNGNGNGNGNGNGNGNGNGMGNGNGNGNGNGNGNGNGNGNGNGNGNCNCNGNGNGNGNGNGNG

V.TOT1.1.11.1.1.1.11.1.1.1.11.1.1.111.11.1.1111.1.1.1.1.1.1.1.1.1.1.11.1.111.1.

- 1.1.1.1.11.1.1.1.11.1.1

4363044347630109252430153239013114133027222B31414301102321241325212929012014251621090117

310517162015293948391615


NC7679

NO1234567S91011121314131617IS19202122232425262728293031323334353637383940414243444546474849505132

M/E SCAN Tim KEF RRT ME1H212 1060 16:2? f7 0.693 A BV216 716 10: 56 IS 0. 925 A BB

RET(L)7: 126:476:336: 387. 107: 147:267:317:377: 407: 307:327: 378:039:078:268:338:378: 308:438: 339:029: 099. 149:239: 3910: 1211: 3110 3410: 4010: 4410: 3811 0911:2811:3711 4711: 3511: 3712:0312: 0912 1111-3412:3412: 4012: 4112: 4314; 1012 3012 3113:2613: 4113. 37

RATIO RRT(L>1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 000. 991. 001. 001. 001. 001. 001. 001.001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 00

10. 00010. 00010. 00010. 00010. OOC10. OCO10. OOC10. 00010. 00010. 00010. 00010. 00010. 000.10. 00010 00010. OCO10. OCO10. OCO30. 00010. 0.:-G10. 00010. 00010. 00010. 00010. 00010. OCO10. 00010. 00010. 00010. 00030. 00010. 00050 OC-C10. 00010. OOC30. 00010. 00030. 00030. 00010. 00010. 00010. 00010. 00010. OCO10. 00030. 00010. 00030. OOC10. 00010 00010. 00030. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090. 100 090. 090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090 090. 100 02

AKN ]40.64.51.51.54.30.31.51.56.51.54.34.46.63.40.60.37.31.43.58.37.56.64.40.56.38.66.40.42.49.48.31.45.52.33.39.51.43.44.51.30.48.30.31.33.36.40.4330474846

0018027145S34220212*307497400019869*179570523891232417CO9342795124CO057389088048030733623941004864669470

AREA(HGHT) AMOUNT578624. 45. 495 NG132800. 50. 517 NG

AMNT(L)40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160160.160160.160.160.160.160.160.160.16O.160.160160.40.160.160160.160.160.

000000000000000000000000000000000000000000000000000000000000000000000000000000000000OO000000000000000000

R. FAC R. FAC(L>1. 0000. 5450. 5330. 4350. 4950. 4400. 2700. 4340. 3690. 8370. 3940. 4220. 2600. 1961. 0000. 3390. 0760. 1300. 0560. 1900. 1050. 1140. 3330. 1070. 0690. 1490. 2251. 0000. 1120. 1200. 1170. 3570. 1580. 4350. 4810 0680. 3480. 0320. 0600. 4600. 1010. 0830. 4430. 1730. 3160. 0631. 0000. 0320. 1400. 0700. 0810. 036

1. 0001. 3591. 6721. 3451. 4551. 3840. 8411. 3551. 0502. 6141. 1621. 2320. 8840. 4951. 0000. 9540. 2100. 4000. 2070. 5150. 2910. 3240. 8270. 4190. 1950. 4100. 3431. 0000. 4190. 3900. 3841. 1100. 5601. 3371. 3980. 2741. 0730. 1120. 2151. 4300. 3220 2781. 4060 3420. 9110. 1791. 0000. 1180. 4410. 2330. 2630. 123

XTGT1. 151 28

RATIO1. 000. 400. 320. 320. 340. 320. 320. 320. 350 320. 340. 340. 290. 401. 000 380. 360. 320. 270. 370. 360. 350. 400. 260. 350. 360. 411. CO0. 270. 310. 300 320. 280. 330. 340 250 320. 280. 280 320 310. 300. 310 320. 350 351 000. 270 320 300. 310 29


NO53343356575S596061626364656667686970717273747376777879

REl (D14: 1214: 1719: 0816:0713: 2816:3017:3218: 2218.2618:2818:2920: 3819:2420: 1320: 1620: 3223: 4623: 4624:353:336: 468 0310: 4813:0316: 4316:2910: 39

RATIO RflT.i.;1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 00

10 G'.O10. 00010. 00010. 00010. 00010. 00010. 00020. 00010 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 0000. 7+Z0. 9450. 8730. 90S1. 1180. 90710 0001. 000

' RATIO0. 100. 100. 110. 110. 100. 090. 090. 050. 100. 100. 100. 100. 090. 100. 100. 100. 110. 110. 121. 040. 991. 011. 000. 99

" 1. 000. 090. 93

Ar4947.30.50.40.4744.49.45.47.42.40.46.51.41.46.45.47.45.50.54.53.54.43.43.43.30.

'XT317690800033653993727400167/43197337258395618392364935

AMNT(L)160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160160.160.160.

000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)0. 3000. 2930. 4500. 3001. 0000. 3920. 2450. 0370. 3400. 3250. 2361. 0000. 5650. 4070. 2450. 2890. 3380. 2770. 2770. 3080. 5660. 1880. 3330. 0300. 3130. 3630. 081

0.01.0.1.1.0.0.1.1.0.1.1.1.0.1.1.0.0.1.1.0.1.0.1.1.0.

973980416943000324875120184088885000957253947001163930981601648312030174106277257

RATIO0 310. 300. 320. 321. 000. 300. 280. 310. 290. 300. 271. 000. 290. 320. 260. 290. 290. 300. 280. 320 340. 370. 340. 290. 280. 280. 32


COMPUCHEM Lri65PIC CONPUCHEM DATA: HH831121v*3 SCANS 3-45 TO 134511/21/89 9:17:00 OUT OF 345 TO 2200SAMPLE: 1UL 5EMI2 SSTD08B 30408(2366) OHI08COHOS.:

•NU".'

IS«1 IS*2 IS«3 SS*5 SSI6 15*5

SS#2 SS#3 SS#4 D3»l

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132*;i:366 «««

1 16U9

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10 1400 1600 lb'00

15:16 18:19 21:23 24:26 27:29

UJto.o1

UJ-J0.

r..Q•oinr.oo

COMPUCHEM LABS ^PIC CONPUCHEM DATA: HH33U21AU3 SCANS 1345 TO 22m *'*>11/21/89 9:17:00 OUT OF 345 TO 2200SAMPLE: 1UL SEMI2 SSTD080 3w4ti8'.23bb> OHM?.CONDS': 3435519.

21 131 - ' - 1 -

2000 2200 StnN30:32 33:36 TIME

UJ(01

*OICL

•IC.

UJ-JLL

Q••ft10r.•DO

QUANT I TAT ION REPORT FILE: HH891121A03DATA: K!891121AOB. TI11/21/89 9: 17: 00SAMPLE: 1UL SEMI2 S5TD080 30408<2366) ON#OBCONDS. :SUBMITTED BY: 08 ANALYST: 1090

AMOUNT-AREA * REF.A^NT/(REF.AREA)* RESP FACT)RESP. FA-. FROM LI5RAPV ENTRY

NO NAI-.-E1 »494 04-1,4-DICHLORODENZENE <IS#1)2 610 PHENOL «J1#3> <108-93-2>3 411 B IS <2-C<r-:LO?rOETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROr-HCNCL (Ql#6) <95-57-6>5 421 l,3-DICHLOr?ODENZENE <Q1#7) <541-73-l>6 4?2 1.4-DICHLORODENZENE <Q1#8> <106-46-7>7 474 BENZYL ALCOHOL <Q1#9) <100-51-6>8 4PO 1,2-DICKJDP:ODENZENE <Q1*10) <95-50-l>9 620 2-METH%rLPHLNOL <G1«11) <95-48-7>

10 412 BIS<2-CK.Gn01SQPROPYL)ETHER <Q1#12) <39638-32-9>11 6?2 4-METHYi PHENOL <Q1#13) <106-,4-5>12 442 N-NITRHSO-I'l-N-PROPYLAMINE <Q1*14) <621-64-7>13 436 HEXACHLO^O-ETHANE (Ql#15) <67-72-l>14 440 NITRODi-NZtNE (Ql#16> <98-95-3>15 *460 D8-NAPHTHALEME (IS#2)16 436 ISOPHORO;-;E <Q2#2) <7B-59-l>17 606 2-NITROrHFNOL <Q2#3> <B8-75-5>16 603 2. 4-DI*_;THYLPHENOL (Q2*4) <105-67-9>19 625 BENZO1C ACID (02*5) <65-85-0>20 410 B18(2-CHLOROETHOXY)METHANE <G2*6> <111-91-1>21 602 2, 4-DKHLCROPHENOL (Q2#7) <120-83-2>22 446 1.2,4-TRICHLORODENZENE <Q2#B> <120-82-l>23 439 NAPHTH.M ENC (Q2#9) <91-20-3>24 475 4-CHLOFOAN'ILlNE (Q2*10) <106-47-8>25 434 HEXACHLOlrOD'JTADIENE <Q2#11) <87-68-3>26 606 P-CHLORO M CRESOL (02#12> <59-50-7>27 477 2-METH'rl NAPHTHALENE <Q2#13) <91-57-6>26 *4V5 D10-ACENAP!!THENE (IS#3)29 435 HEXACHLCrtOCYCLDPENTADIENE <03*2) <77-47-4>30 611 2>4,6-iRICHLOROPHENOL <Q34»3) <88-06-2>31 626 2, 4, 5-TRICHLOROPHENOL <Q3t4) <95-95-4>32 416 2-CHLOPO:'iAPHTHALENE <G3#5) <91-58-7>33 478 2-NITROA?JILINE <Q3«6) <88-74-4>34 4?5 DIMETHYL PHTHALATE <03#7) <131-ll-3>35 402 ACENAPHTHYLENE (Q3*8) <208-96-8>36 479 3-NITROANILINE (Q3t9) <99-09-2>37 401 ACENAPHTHENC <03*10) <83-32-9>36 €605 2,4-DINITROPHENOL <Q3#11> <51-2B-5>39 607 4-NITROrHENOL <Q3#12) <100-02-7>40 476 DIBENZCrURAN <03#13> <132-64-9>41 427 2.4-DINITROTDLUENE (03*14) <121-14-2>42 428 2,6-D1NITROTOLUENE <Q3tl5) <606-20-2>43 424 DIETHYL PHTHALATE (Q3«16) <84-66-2>44 417 4-CHLORCr>K_:NYL PHENYL ETHER <Q3*17) <7005-72-3>45 432 FLUOREM (C3«18) <86-73-7>46 480 4-NITRC.^NILlNE (Q3tl9> <100-01-6>


NO474849505152535455565738596061626364656667636970717273747376777879

NO1234567891011121314131617IB192021

NAf-E»467 DIO-PK^NAU'IHRENE (IS*4>604 4, 6-DINI 1 RC-S-r.ETHYLPHENOL (Q«*2> <334-S2-l>443 N-NITROcGDIPHEMYLAMINE (04*3) <86-30-6>414 4-BRCf1Q?HEN!YL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLCS03ENZENE (04*5) <118-74-l>609 PENTACH'. OROPHENOL (Q4*6> <87-86-5>444 PHENANTHXEK'c. (Q4#7) <85-01-8>403 ANTHRACtNE (34*8) <120-12-7>426 DI-N-BUTvL PHTHALATE (Q4*9) <84-74-2>431 FLUOR ANTHER (04*10 > <206-44-0>*459 D12-CHKYSEME (IS*3)445 PYRENE (05*3) <129-00-0>415 BUTYLSENZVL PHTHALATE (03*4) <85-68-7>423 3. S'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO(A)AK'THRACENE (QS*6> <56-55-3>413 8IS(2-ETHYLH6:XYL> PHTHALATE (Q5#7> <117-81-7>418 CHRYSEKf (03»£> <2l8-01-9>*497 D12-PERYLFNE429 Dl-N-OCTYL PHTHALATE (06*2) <117-84-0>40/ BENZO(3)FL'JO«ANTHENE (06*3) <205-99-2>409 BENZO (JOFLiJOSAf-THENE (06*4) <207-08-9>406 BENZO(A)PYREN£ (Q6*5) <30-32-8>437 INDENOd. 2-3-C. DJPYRENS (06*6) <193-39-5>419 DI BENZO ( A, H) ANTHRACENE (06*7) <53-70-3>408 BENZO(G, H, I ) PER YLENE (Q6*8) <191-24-2>*619 2-FLUORGPHENQL (SS#1)*612 D5-PHCr:QL (35*2)*4--7 OS-NITROBENZENE (SS*3) tilbtfix^.*4'-3 2-FLUQSQB I PHENYL (SS*4) |6*ut

*628 2. 4. 6-TRISROMOPHENOL (SS*3) ///2./r>*496 D14-TEKPHENYL (SS*6) ' '*471 D10-PVKENF456 1 , 2, 3, 4-TE 1 RACHLOROBENZENE

M/E152949312614614610614610645108701177/1368213910712?93162

SCAN469441447453466 471 ,483^-486 /495496509 'Sll518526593548557560572 '569580

TItfL7: 106: 446: 506: 557: 077: 127: 237: 277: 347: 367:467: 487: 358:029: 038:258: 306: 338: 446: 418: 51

REF1111111111111

1515151515151515

RRT1 0000 9400. 9530 9660 9941 0041. 0301. 0411. 0551. 0621.0851. 0901. 1040. 8871. OCO0.9240. 9390 9440. 9650. 9600 978

ME1HA*DBA 3VA DVA DCA BVA VSA DVA BBA VVA BVA VVA VVA B8A 3VA BVA BVA BBA DVA VVA 3VA BB

AREA < HOHT )195364.655604.691548.546976.638652.554340.347820.554320.446025.988768. /475389.490612.345284.669715.600560.1315090.282864.533263.223b44.69206SX390452.

AMOUNT40.98.84.83.89.62.84.83.86.77.83.81.79.90.40.91.89.88.72.89.69.

000805706295857012673744989444769531972149000781518818056575463

NGNGNCNGNGNGNGNCNGNGNGNGNGNGNGNGNGNGNGNGNG

%TOT0. 631. 561. 341. 311. 421. 291. 341. 321. 371. 221. 321. 291. 261. 420. 631. 451. 411 401. 141. 411. 41


NC22232425262723293031323334333637383940414243444546474649505152333455565738396061626364656667686970717273747?7677

M/E130123127225107142Ii423719619616265163132136153184109168165165149204166138163198169248284266178178149202240202149252226149226264149232252232276278276112993217233024'!

SCAN539S95x-601 x-613650664774 ""668696'700'7147277437387/0777780766793796 /755'821828

Tl!,>

9:009:059: 119:229: 5_10:0311: 4910:3010:3310: 4110: 5411: 0611:251 1 : 3«!11: 4511: «211: 33IP: 0012:0712:09It: 3212:3212: 39

829X15; 40833927838841879896914930 x935 x991

12:4314:0912; 42

12: 3113: =>513.4113:3714: 1214: 1715: 08

1056 x-16: 0712081080 x

114812031206-12091211 X137312711324x1326X

13661555135616093604403247038561093

18:2716: 2917: 3216: ?218:2718:2318: 2920: 5819: 2420: 1320: 1520: 5223:4523: 4624:343:306: 438:0010: 4'!13: 0416 43

REF1515151515152823S328282826£8282828282828282828232847474747474747474747J7575757373757646464646464646411

15282837

RRT0. 9931. 0031.0131. 0341 0961. 1201.0000. 8890. 8990. 9040. 9220. 9390. 9660. 9790. 9951. 0041. 0081. 0161.0251. 0280.9751. 0611. 0701.0711. 0761.0000. 9040. 9070. 9480. 9670.9861.0031. 0091. 0691. 1391.0000. 8940. 9500. 9960. 9981. 0011 0021. 0000. 9260. 9640. 9660. 9951. 1331. 1331. 1720. 7680. 9380. 8840. 9081 1060 906

METHA 33A BVA VBA BBA BVA VVA 3*A SBA BVA VVA BBA BVA 33A BBA BVA UBA BBA BVA BBA BBA SflA BVA B*A EBA VVA EBA BVA DBA BBA BBA B3A BVA VBA BBA BBA BBA SVA 3VA BVA BVA 3VA VDA BBA BVA BVA VVA BBA BBA BVA BBA BBA BVA 3VA 3VA 33A BV

AREA(HGHT)439180.1201810.548631.257760.521600.818540.316344.256848.253304. '"242312.76S504.336260.912924.992100.148392.710108.72838.134132.960352.x

218372.178212972«:80.361928.639044.100050.455936.101032.427856.214880.X248616.102804.914980.933944.1380680.874040.292132.751563.463964.80732.671636.618740.512178.256215.992400.682760.446160. y531413X

641412.S13463X534443.639313.714549.677804727020.112644.602331.

AMOUNT90.96.87.87.84.100.40.77.82.79.67.75.86.89.68.83.82.78.84.85.81.87.84.83.70.40.74.85.80.82.73.82.83.85.81.40.77.72.91.77.77.79.40.79.84.73.82.84.86.85.84.88.83.89.81.74.

350816307967718351000385192757528876311739409644418877920773095429501737617000960082748814209508594557291000738634968680842250000154726560880654180023339787184222920597

NGNGNGNGNGNGNGNGNGNCNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNCNCNGNGNGNGNGNCNGNGNGNGNGNGNGNCNCNGNGNGNGNGNGNGNGNGNGNGNG

%TOT1. 421. 531. 381. 391. 341. 580. 631. 221. 301. 261. 381. 201 361. 421. 081. 321. 301. 241 341. 351. 281. 381. 331. 401. 110. 631. IS1. 341. 271. 311. 151. 301. 321. 351. 280. 631. 231. 151. 451. 221. 231. 250. 631. 251. 341. 161. 311. 331. 361 341. 331. 401. 391. 411 291. IS

18756 87 SAMPLE DATA PPCKPGE 34S

NO7879

NC12345678910111213141516171619202122232425262726293031323334353637363940414243444546474849505152

M/E SCAN Tlii.- REF RRT METH212 1078 16:23 37 0.892 A BV216 713 10:33 23 0.924 A 3B

RtT(L)7: 126: 476: 536: 587: 107: 147: 267: 317:377 407:507:527: 578: OS9: 078: 268:338: 378 508: 456 559 029 099: 149: 2S9 5910: 1211: 5110: 3410-4010: 4410: 5811:0911: 2811: 371 1 4711 5511: 5712: 0312: 0912: 1111: 3412: 3412. 4012: 4112: 4514: 1012 5012 5113 2613: 4113 57

RATIO RRT-.L)0. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 991. 000. 991. 001. 000. 991. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001 00

10. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00050. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. OCO10. 00050. 00010. 00050. 00010. 00010. 00050. 00010. 00050. 000SO 00010. 00010. 00010. 00010. 00010. 00010. 00050. 00010. 00050. 00010. 00010 00010. 00050 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090. 100. 090. 090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100 020. 090. 090 100. 02

A.MNT40.98.84.63.8982.84.83.8677.83.81.79.90.40.91.89.86.72.89.69.90.96.87.87.84.100.40.77.82.79.87.75.86.89.66.83.82.78.84.85.81.87.84.88.70.40.74.85.80.82.73.

00Bl7130860167749944773397150078*28206SB463582319-7723500561976538631744164428892770943SO7462009606758121


AMNT < L )40.160.160.160.160.160.160.160.160160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.16O.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160

00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)1. 0000. B390. 8850. 7000. 8170. 7090. 4450. 7090. 5711. 2650. 6080. 6280. 4420. 2791. 0000. 5470. 1180. 2220. 0930. 2880. 1630. 1830. 5000. 2260. 1070. 2170. 3411. 0000. 2030. 2000. 1910. 6070. 2660. 7210. 7840. 1170. 5610. 0580. 1060. 7590, 1730. 1410. 7680. 2860. 5050. 0791. 0000. 0550. 2350. 1180. 1360. 056

1. 0001. 3591. 6721. 3451. 4551. 3840. 8411. 3551. 0502. 6141. 1621. 2320. 8640. 4931. 0000. 9540. 2100. 4000. 2070. SIS0. 2910. 3240. 8270. 4190. 1950. 4100. 5431. 0000. 4190. 3900. 3841. 1100. 5601. 3371. 3980. 2741. 0730. 1120. 2151. 4300. 3220. 2781. 4060. 5420. 9110. 1791. 0000. 1180. 4410. 2330. 2630. 123

7. TOT1. 181. 35

RATIO1. 000. 620. 530. 520. 560. 510. 530. 520. 540. 480. 520. 510. 500. 561. OO0. 570. 560. 560. 450. 560. 560. 560. 610 550. 550. 530. 631. 000. 460. 510 500. 550. 470. 540. 560. 430. 520. 320. 490. 530. 540. 510. 550. 530. 550. 441. 000. 470 330 300. 520. 46


NO335455565758596061626364656667666970717273747576777879

RtT(L)14 1214: 1715: 0816 0716 2816: 3017: 3216: 2218:26IS: 2818: 2920: 5819: 2420: 1320: 1620: 5223: 4623: 4624: 355: 336: 468: 0310: 4813: 0516: 4316: 2910: 59

RATIO RRT'.L>1. 001. 001. 00. 00. 00. 00. 00. 00. 00. 00. 00

1. 001. 001. 001. 001. 001. 001. 001. 000. 990. 990. 990. 991. 001. 001. 000. 99

10. 00010. 00010. 00010. 00010. 00010. 00010. 00020. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 0000. 7420. 9490. 8750. 9061. US0. 90~10. 0001 . OOC

RATIO0. 100. 100. 110. 110. 100. 090. 100. 050. 100. 100 100. 100. 090. 100. 100. 100. 11O.'ll0. 121. 030. 991. 011. 000. 991. 000. 090. 92

AMNT82.83.85.81.40.77.72.91.77.77.79.40.79.84.73.82.84.86.85.84.88.88.89.81.74.74.85.

51395629007463976884230015735688651802347918?292609354

AMNT ( L )160160.160.160.40.160.160.160.160.160.160.40.160.160-160.160.160.160.160.160.160.160.160.160.160.160.160.

000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)0. 5020. 5120. 7570. 4791. 0000. 6430. 3970. 0690. 5750. 5300. 4361. 0000. 9680. 6660. 4350. 3190. 6260. SOI0. 5210. 8440. 9140. 2820. 3750. 0890. S160. 5980. 137

0. 9730. 9801. 4160. 9431. 0001. 3240. 8750. 1201. 1641. 0880. 8831. 0001. 9571. 2580. 9471. 0011. 1830. 9300. 9811. 6011. 6480. 5121. 0300. 1741. 1061. 2770. 257

RATIO0 520 520. 530. 511. 000. 490. 450. 570. 490. 490. 301. 000. 490. 330. 460. 520. 530. 340. 530. 530. 550. 550. 560. 510. 470. 470. 53


COMPUCHEM LrtBSRIC COMPUCHEM DATA: (.1331121003 SCANS 356 TO 170611/21/89 10:12:00 OUT OF 350 TO 1700SAMPLE: 1UL SEHI2 SSTD120 30409(23£7> OWKtiCONOS.: 4786150.

IS*2

SS*2 SS#3

444

RJC

513

552

15*3 SS»5

SS»4 03*1 ; IS*4

831 !

668 788

718

S5«6

SS»7

15*5

I Sib

400

6:866609:16

1218

1658 ; 1149

11000

15:16

1272

132S

1363

i120013:19

1400

21:23

1556

1612

160024:26

SCfiNTIME

IOtt't

UJ<01-£O•Ia.

ctoUJ

K.

•f)IOr--.oo

QUANTITATION REPC^T FILE: HI891121A08DATA: HI691121AC6. 1111/21/89 10:12:COSAMPLE. 1UL SEMI2 SSTD120 30409(2367) ON*08CONDS. :SUBMITTED BY: 08 ANALYST: 1090

AMOUNT-AREA * RE»-. A.-.XT/ (REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHwORODENZENE (IS*1)2 610 PHENOL <Q1«3) <108-95-2>3 411 BIS(2-CH.OROETHYL)ETHER «J1*S) <lll-44-4>4 601 2-CHLOROrHLNDL <Q1*6) <95-57-8>5 421 1,3-DICHLOKOoENZENE <Q1*7) <541-73-l>6 422 1.4-DICHLORODeNZENE (Gl*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-51-6>6 420 l,2-DICHLOr!OBENZENE (01*10) <95-50-l>9 620 2-ME1HYLPHENOL (Gl#ll) <95-4B-7>

10 412 B1B(2-CK.OR01SQPROPYL)ETHER (0,1*12) <3963B-32-9>11 622 4-METHYLPHENO-. (01*13) <106-14-5>12 442 N-N1TRC~D-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLG3CETHANE (01*15) <67-72-l>14 440 NITROBtNZENS <01*16) <98-95-3>15 *460 OS-NAPHTHALENE (IS*2)16 438 ISOPHOROME (22*2) <7B-59-l>17 606 2-NITRCrHHNOL <Q2*3) <88-75-5>18 603 2. 4-DI^e.THYLPHENOL (02*4) <105-67-9>19 62S BENZOIC ACID <02*5) <65-B5-0>20 410 B.S(2-CHLOROZTKQXY)METHANE («2*6) <111-91-1>21 602 2,4-DICHLOROeHENOL (02*7) <120-B3-2>22 446 1,2, 4-TRICHLOI?OBENZENE (Q2*8) <120-B2-1>23 439 NAPHTHALENE <02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-B>25 434 HEXACHLOrtODUTADIENE (02*11) <B7-68-3>26 608 P-CHLORO-M-CRESOL (02*12) <S9-SO-7>27 477 2-HETHYI NAPHTHALENE (02*13) <91-57-6>28 *495 D10-ACE?iAPHTHENE (IS*3)29 435 HEXACHLO^OCYCLOPENTADIENE (03*2) <77-47-4>30 611 2,4,6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 5-TRKHLOROPHENOL (03*4) <95-.95-4>32 416 2-CHLORC:>IAPHTHALENE (Q3*5> <91-58-7>33 478 2-NITROAMTLINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (Q3*8) <208-96-8>36 479 3-NITRC>NII. INE (03*9) <99-09-2>37 401 ACENAPHTHENiZ (03*10) <83-32-9>36 «605 2.4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHFNOL (Q3*12) <100-02-7>40 476 DIBENZOrURAM (03*13) <132-64 ?>41 427 2.4-DINITROTDLUENE (03*14) <121-14-2>42 428 2,6-DIN1TROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROrv:rNyL PHENYL ETHER < 03*17) <7005-72-3>45 432 FLUORENE (Q3»18) <B6-73-7>46 460 4-NITRCANILINE <Q3*19) <100-01-6>


NG4748495051525354553637S3596061626364636667666970717273747376777879

NO1234*.67891011121314151617IS192021

NA:IE*467 DlO-P'ricNANlHRENE (IS*4)604 4, 6-DINI I RO-*-METHYLPHENOL (04*2) <534-52-l>443 N-NITR030DIPHENYLAMINE (Q4*3) <S6-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLOROBENZENE (04*5) <118-74-l>609 PENTAC!iU3RO?HENOL (04*6) <87-86-5>444 PHENAMTHKEME (Q4*7) <83-01-8>403 ANTHRACENE (04*8) <120-12-7>426 Dl-N-BUiYL PHTHALATE (04*9) <84-74-2>431 FLUOR AH i HE'- > (G4*10> <206-44-0>•439 D12-CHRYSENE (IS*5)443 PYRENE (03*3) <1 29-00- 0>41 S B'JTYLBEMZYL PHTHALATE (03*4) <85-68-7>423 3, 3'-DICHLOROBENZIDINE (Q3*5) <91-94-l>405 BENZO ( A) ANTHRACENE (05*6) <36-5S-3>413 BI8(2-ETHYLHEXYL) PHTHALATE (05*7) <117-Bl-7>418 CHRYSEivE (OS*8> <218-01-9>*497 D12-PERYLENE429 DI-N-OCTYL PHTHALATE (Q6*2) <117-84-0>40 / BENZO(S) FLUORANTHENE (06*3) <20S-99-2>409 BENZO(K) FLUORANTHENE (06*4) <207-08-9>406 BENZO(A>PVRtN£ (.6*3) <30-32-8>437 1NDEN-K1.2, 3-C. DJPYREME (06*6) <193-39-3>419 DIBENZO ( A, H) ANTHRACENE (06*7) <33-70-3>408 BENZO(G. H, I > PEA YLENE (Q6*8> C191-24-2>*619 S-FLUuROPHtNOL (SS*l)*612 DS-PHE-:OL (SS*2)*4-!7 OS-NITROBENZENE (SS*3) C\llltl»^-*4-!S 2-FLUO»OB I PHENYL (88*4) [JW^*628 2. 4, 6-TR I aROMQPHENOL (SS*5) /|W?7 •*496 D14-TESPHENYL (SS*6) I'l l

*471 D10-PYKEUF4S6 1 , 2, 3. 4-TE 1 RACHLOROBENZENE

M/E132949312314614610614610645103701177/136321391U712?93162

SCAN473445451457470475 s487 '492 /499'502^13^313322329396352360564377 "573583

TIMH7: 136: 486: S36: 597: 117: 157: 267: 317: 377:407: 307: 527: 538:039.066:268: 338: 378: 498 458: 34

REF1111111111111

1515151515151515

RRT1. 0000. 9410. 9530. 9660. 9941 0041 0301 0401. 0551. 0611. 0851.0891. 1040.8881. 0000. 9260. 9400. 9460. 9680. 9610. 978

METHAAAAAAAAAAAAAAAAAAAAA

BBBVBVBBDVVBDVSBVVDVVVVVBBBVBVBVBVBVVVBV36

AREA < HCHT ) AMOUNT17996B.811044.906780.719836.820172.756100.456400.745196.571611.1365010.627912.668334.457232.912124.577992.1727660.373932.714300.362416.920744. '333688.

40.132.120.118.125.121.120.122.121.116.120.120.114.127.40.125.122.123.121.123.127.

000688571997269432611212020058111665960573000283966651207826056

NGNCNGNGNGNGNGNGNCNCNGNGNGNGNGNGNGNGNGNGNG

'/.TOT0. 441. 471 331. 311. 381. 341. 331. 351. 341. 281. 331. 331. 271. 410. 441. 381. 361. 371 341. 371. 40


NO2223242526272329303132333435363738394041424344454647464930513253545556575859606162636465666768697071727374757677

M/E1801281272251071421642371961961626516315213615318410916616516514920416613818819616924823426617817814920224020214923222314922826414923223225227627827611299821723302*, 4

SCAN'392399603 x

616653668776 x

691699 •"703 <"717730751761772780783789796793 /758 /8ZJ831

TIKc9:029: 099: 149: 249: S310: 1211: 5110:3;.10: 40JO: 4410: 5711: 0911: 23It: 3711:4711:5511: 5712:0312: 0912.ll11:3412; 3s'

12; 41832 X12: 42836929841843881897913932'936x9921058"12101082 x

114912041208^12101213137412721323'-1328X

13661357155816113644445267068561096

12: 4614: 1112: 5112; 55

13: 2713: 4213: 3314: 1414: 1815: 0916: 0918 2916: 3117: 3316: 2J18:2716: 2913:312 : 3919:2320: 1420: 1720: 3323 : 4623: *724: 365: 336. 476: 0410: 4713 0616 14

REF151315151515282328262828282828282828282828282828284747474747474747474757573737375737646464646464646411

15282357

0.1.1.11.1.1.0.0.0.0.o.o.0.0.1.1.111.0.1.1.1.1.1o.o.o.0.o.1.1.1.1.1.0.00.0.1.1.1.0.0.0.0.1.1.1.0.000.1.0

RRT993003013034096121000890901906924941963981995005009017026028977061071072077000905907948966985003003068139000894950995998000002000926964967996133134172770939866910106906

METHAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAAA

BaBVVSDDBBVVBEBB3VVVI'DDVBBEBDVBDBBBVDVSBBBBVBbBVDVDDDDBVUD33svDVVBBBBVDVDVDVBBVVBVVBBBBB3VVBBDBBDDDVbDBVDVDVDDDD

AREA(HGHT) AMOUNT583288.1649710.742062.349600.740532.1039360.295224.364276.354 168327984.1012460.485140.1186490.1270690.237364.940932.105032.201760.125021 OX294520.240764.1300730.482V 12.833704.13654443 1084.146372.564644.2871 80. x

332116.154630.1242790.1190800.1725090.1203420.272036.1012100.67121599440/934408.851731.754188.222996.1333830.778856.701852.67P643.787062.605720-64 861.906649.886135.975960.958776.15--94B.843779

124.133.122.123.124.132.40.117.123.115.123.117.120.123.117.118.127.127.118.123.117.123.120.124.105.40.114.118.114.117.116.116.112.113.118.40.112.112.121.116.115.125.40.122.111.132.121.119.116.117.125.119.131.126.119.112.

682087699967973399000906141679563295201162264761261134460959397331813049009000860757138006501529729062378000421842648055070317000235049954610351809689900527933081968209

NGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNCNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG

7. TOT1 331. 331. 361. 371. 331. 460. 441. 301. 361. 281. 361. 301. 331. 361. 301. 311. 411. 401. 311. 371. 301. 381. 331. 371. 160. 441. 271. 311. 261. 291. 291. 311. 251. 251. 310. 441. 241. 251. 341. 281. 271. 380. 441. 351. 231. 471. 341. 321. 291. 301. 391. 321. 461. 391. 331. 24

18756 87 SAMPLE DATA PACKAGE '42

NO7679

NO12345673910111213141316171819202122232423262723293031323334333637383940414243444546474849505152

M/E SCAN TlrC PEF RRT METH212 10SO 16:29 57 0.893 A DV216 718 10: 38 28 0. 925 A DD

REl (L)7: 1?.6:476: 536: 387: 107: 147:267:317:377: 407: 307: 327: 378:039:073:268:338:378: 308:458: 559: 029: 099: 149:239: 3910: 1211: 3110 3410: 4010: 4410: 3811: 0911: 2811: 3711 4711: 331 1 : 3712:0312 O912: 1111: 3412 3412: 4012: 4112: 4514: 1012 3012 3113 2613: 4113: 37

RATIO RRT(L>1. 001.001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 00I. 001. 001. 001.001. 001. 001. 001. 001. 001. 001 001. 001. 001. 001. 00

10. 00010. OGO10. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00010. 00030. 00010. 00010. OCO10. 00010. 00010. OOC10. 00010. 00010. 00010. 00010. OOC10. 00030. 00010. 00030. 00010. 00010. OCO30. 00010. 00030. 00030. 00010. 00010. 00010. 00010. 00010. 00010. 00030. 00010. 00030. 00010. 00010. 00010. 000SO 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090 100. 090. 090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090 020. 090. 020. 100. 100. 020. 100. 020. 020 100. 100. 100 110. 110. 110. 020. 100. 020. 090 090 100. 02

AMNT40.132.120.119.123.121.120.122.121.116.120.120.114.127.40.123.122.123.121.123.127.124.138.122.123.124.132.40.117.123.113.123.117.120.123.117.118.127.127.118.123.117.123.120.124.105.40.114.118.114.117116.

006957CO274361210206116796370028976321830668097099974000911468363020162676261346964033810501008676140130


AMNT(L)40.160.160.160.160.160.160160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160160.160.160.160.160.160.160.160.40.160.160.160.160.160.

00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L>1. 0001. 1271. 2601. 0001. 1391. 0500. 6341. 0350. 7941. 8960. 8720. 9290. 6350. 3931. 0000. 7470. 1620. 3090. 1370. 3980. 2310. 2520. 7140. 3210. 1310. 3200. 4501. 0000. 3080. 3000. 2780. 8370. 4111. 0051. 0760. 2010. 7970. 0390. 1711. 0590. 2490. 2041. 1010. 4090. 7060. 1161. 0000. 0850. 3270. 1670. 1930. 090

1. 0001. 3591. 6721. 3451. 4551. 3340. 8411. 3551. 0502. 6141. 1621. 2320. 8840. 4951. 0000. 9540. 2100. 4000. 2070. 5150. 2910. 3240. 8270. 4190. 1950. 4100. 3431. 0000. 4190. 3900. 3841. 1100. 5601. 3371. 3980. 2741. 0730. 1120. 2151. 4300. 3220. 2781. 4060. 5420. 9110. 1791. 0000. 1180. 4410. 2330. 2630. 123

V.TCT1. 201. 34

RATIO1. CO0. 830. 750. 740. 780. 760. 750. 760. 760. 730. 750. 750. 720. 801. 000. 780. 770. 770. 760. 770. 790. 790. 860. 770. 770. 780. 831. 000 740. 770. 720. 770. 730. 750. 770. 730. 740. 800. 790. 740. 770. 730. 780. 760. 780. 661. 000. 720. 740 710. 730. 73


NO533453363758596061626364656667686970717273747376777879

RE! (L)14 1214: 1715: 0816:0713:2816:3017:3213:2213:2613:2818 2920: 5819:2420: 1320: 1620: 5223:4623:4624:353:336: 463:0310: 4813: OS16: 4316 2910: 39

RATIO RRT(LJ1.1.1.1.1.1.1.1.1.1.

t

1.1.1.1.1.1.1.1.1.1.1.1.

00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 20.00 10.00 1000 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00 0.00 0.00 0.00 0.00 1.00 0.00 10.00 1.

000000000000OOC000000000000OOGOCO0000000000000000000000007*294837;906113907000000

RATIO0. 100. 100. 110. 110. 100. 090. 090. 030. 100. 100. 100. 100. 090. 100. 100. 100. 110. 110. 121. 040. 991. 011. 000. 991. 000. 090. 93

A!118.112.113.11840.112.112.121.116.115.125.40.122.111.132.121.119.116.117.123.119.131.126.119.112.108121.

•;NTS37306330042846503073200230395613581699033930897218720

AttNTCL)160.160.160.160.40.160.160.160.160.160160.40.160.160.160.160.160.160.160.160.160.160.160160.160.160.160.

000000000000000000000000000000000000000000000000000000

R.0.0.1.0.1.0.0.0.0.0.0.1.1.0.0.0.0.0.0.1.1.0.0.0.0.0.0.

FAC R. FAC(L>721691000698000930617091859783693000495873787761882679722239231422812130773869195

0.0.1.0.1.1.0.0.1.1.0.1.1.1.0.1.1.0.0.1.1.0.1.0.1.1.0.

973930416943000324875120184088865000957258947001183930981601648512030174106277257

RATIO0. 740 700 710. 741. 000. 700. 710. 760. 730. 720. 781. 000. 760. 690. S30. 760. 750. 730. 740. 790. 750 820. 790. 750. 700. 680. 76


II"-..

CONPUCHEH LABSPIC COMPUCHEN DATA: HJ3'31121A03 SCAMS 343 TO 170011/21-89 11:13:00 OUT OF 348 TO 1700SAMPLE: 1UL SEMI 2 SSTDlbO 30410'.23b8:/ OM#ti8CONOS.: 5201910.

IS»1 IS*2

SS*2 SS»3

443

RIC

IS»3 55*5

55*4 03*1 '. 15*4

830

654

55*6

SS»7

IS*5

15*6

335

1289

991

11481879 1271

6:96 12:13 15:16 18:13

IHUt)21:23

1556

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CtKCt

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24:26 TIME

QUANTI TAT ION REPORT FILE: HJB91121A08DATA: HJ691121ACB. TI11/21/39 11: 13: COSAMPLE: 1UL SEMI2 S3TOJ60 30410(2368) ON*08CONDS. :SUBMIT!ED DY: 06 ANALYST: 1090

AMOUNT«AREA * RE»-. Ai'iMT/ (REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NA-NE1 *494 D4-1.4-DICHL0RODENZENE <IS*1)2 610 PHENOL (01*3) <lC8-9S-2>3 411 B1S(2-CHLCPOETHYL)ETHER (Ql*3) <lll-44-4>4 601 2-CHLORCr'HrNOL (01*6) <95-57-B>5 421 1,3-DICHLORODENZENE <Q1*7) <541-73-l>6 422 1,4-DICHLCRODENZENE (Ql*8) <106-46-7>7 474 BENZYL ALCOHOL (Ql»9> <100-Sl-6>B 420 1.2-DICHLOPODENZENE «il*10) <95-50-l>9 6?0 2-METHYLPHCNOL (Ql*ll) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER <Q1*12) <39638-32-9>11 622 4-METHVLPHENOL (01*13) <106-44-5>12 442 N-NITRCSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLO:70ETHAfiE (01*15) <67-72-l>14 440 NITRODtNZtNE <Q1*16> <98-95-3>15 *460 D8-NAPHTHALENE (IS»2)16 433 ISOPHQRCi-iE <Q2«2> <78-S9-l>17 606 2-NITROPHENOL <Q2*3> <6S-75-5>16 603 2,4-DI>!rTHYLPHENOL (Q2*4) <105-67-9>19 625 BENZOIC ACID (Q2*5> <6S-85-0>20 410 BIS(2-CHLGROeTHOXY>HETHANE (02*6) <111-91-1>21 602 2. 4-DICHLOROPHr.NOL (Q2#7) <120-83-2>22 446 1.2.4-TRICHLORODENZENE (02*8) <120-82-l>23 439 NAPHTHA' ENC (02*9) <91-20-3>24 475 4-CHLORCANILINE (Q2*10> <106-47-8>25 434 HEXACHLOHODUTADIENE (G2*ll) <B7-6B-3>26 608 P-CHLORO-M-CRESOL (02*12) <59-50-7>27 477 2-METHYl NAPHTHALENE (0,2*13) <91-57-6>26 *495 D10-ACENAPHTHENE (IS*3)29 435 HEXACHLOnOCYCLOPENTADIENE <Q3*2) <77-47-4>30 611 2,4.6-TRICHLOROPHENOL (Q3*3) <88-06-2>31 626 2,4,5-TSICHLORDPHENOL (03*4) <95-95-4>32 416 2-CHLORO;-iAPHTHALENE <Q3*5) <91-58-7>33 478 2-NITROA?nLlNE (Q3*6) <B8-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHVLENE <Q3*B) <208-96-B>36 479 3-NITROANILINE <Q3*9) <99-09-2>37 401 ACENAPHIHtNC (G3*10) <83-32-9>3B *605 2,4-D1NITROPHENOL (03*11) <51-28-S>39 607 4-NITROPHENOL (Q3*12) <100-02-7>40 476 DIBENZCFURAM (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <12l-l4-2>42 426 2,6-DINITROTOLUENE (03*15) <606-20-2>43 424 DlETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROr>H_:r,>VL PHENYL ETHER (03*17) <7005-72-3>45 432 FLUOREM <Q3»16) <B6-73-7>46 450 4-NITRO.-VJTLINE <G3*19) <100-01-6>


NO474B495051525354555657S339606162636463666763697O717273747376777879

NO12w

4567891011121314151617IS192021

NA!1£»467 DlO-PHtUANTHRENE (IS*4)604 4. 6-DINI 1 RC-2-METHYLPHENOL (Q4*2) <334-52-l>443 N-NITROSCDIPHENYLAMINE (Q4#3> <86-30-6>414 4-BROMGPHENYL. PHENYL ETHER <Q4*4) <101-55-3>433 HEXACHLORODEK'ZENE (Q4#5) <118-74-l>609 PENTACHi OROPHENOL (Q4*6) <87-86-5>44-* PHENANTHKEKc (Q4*7) <85-01-8:>403 ANTHRACENE «J4#8> <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2:>431 FLUOR AN l HE. <F (Q4*10) <206-44-0>*4S9 D12-CHRYSENE (IS*3>445 PYRENE (03*3) <:i29-00-0>413 BUTYLBE.VZYL PHTHALATE (05*4) <85-68-7>423 3, 3'-DICHL030BENZIDINE (Q3*S> <91-94-l>403 BENZO ( A) ANTHRACENE «J5#6> <36-53-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (Q5*7) <117-Sl-7>418 CHRYSEfCE (Q3»3> <218-01-9>*497 D12-PERYLCNE429 DI-N-OCiYL PHTHALATE (Q6*2) <117-84-0>407 BENZO(3)FLUOPANTHENE (06*3) <205-99-2>409 BENZO (K)FLUORAKTHENE (Q6*4> <207-08-9>406 BENZO (A /PYRENE (Q6*3> <30-32-8>437 INDENQd, 2-3-C. D)PYREN£ (Q6*6) <1 93-39- 5>419 DIBEN'ZOCA, HJ^s'THRACENE (Q6*7) <33-70-3>408 BENZOtG. H, I>P£«?YLENE (06*8) <191-24-2>*619 2-FLUC30PHEN-3L (SS*1)*612 DS-PHE* OL (S£»2>*447 D3-NITR03ENZET.E (SS*3) CVtilP^*4<-8 2-FLUOSOSIPHENYL (SS*4) *-"*623 2, 4. 6-TKl3ROr.3PHENQL (SS*3) /.l^jf^7

*496 014-TE^PHENfL (SS*6> III*11

*471 DIO-PYKEU'F436 1,2, 3, 4-TEJRACHLCR08ENZENE

M/E13294931261461461081461064510870117771366213910712293162

SCAN472444451456469474 '487 •'492 '499 /502513 /515521529597552 '56056457B/573384

TiNC7.6:6:6:

' 7:7:

' 77

7.7B:9

^ B6:8:8:88:

1247335610142631374050t>2570507263337504535

REF1111111111111

1515151315151515

1.0.0.0.0.11.1.1.1.1.1.1.010000.00.

RRT000941956966994004032042057064087091104886000925933945963960978

METHAAAAAAAAAAAAAAAAAAAAA

BBBVDVBBDVVBDVDDVD3VDVDVDDBVDBBV3VBVVVDVBB

AREA(HCHT) AMOUNT173212.941272.1158140.931540.1008240.958848.582722.938988.727357.ISlllBOXBO 5041.853632.612460.1130000.5709362179480.?480636. '9132SO.472S68.1175190. "663860.

40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.

^ 160.160.

/ 160160.160.

000000000000000000000000000000000000000000000000000000000000000

NGNCNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNG

y.TDT0. 341. 341. 341. 341. 341. 341 341. 341. 341. 341. 341. 341. 341. 340. 341. 341. 341. 341. 341 341. 34


NO222324252627282930313233343336373339404142434445464746495051525354S356575859606162636463666766697071727374757677

M/E180128127225107142164237196196162631631321381331841091681631651492041661361381931692432842661781781492022AO2021492322261492232641492522322522762762761129962172330244

SCAN592599 •"605 x-617654668776 /692699 x703 '718730751761772780783789796798x73BX

823830831 X835926840842880896914930935 '99110561209108 lx

114812031207 <"12091211 X13731271

Tli-iF9: 029: 099: 149: 259: 5910: 1211: 5110: 3410: 4010: -1410: 5311: 0911:2611:37J 1: 4711:5511: 5712; 0312:0912; 1111: 3412;3<!12: 4012; 4112: 4514: 1012: 5012; 5113:2613:4113: 5714: 1214: 1713:0316:0716: k'S16: 3017:3218:2?IB: 2618: 2818: 2920; S319:24

1324 20: 131327 13661556155716103634435277078571095

20: 1620: 5223: 4623: -.624: 355: J36: 468: 0310: 4813: 0516: 43

PCF1515151515152828282828282628282828282S2828£828«8184747474747474747474757573737575737646464646464646411

15282837

RRT0. 9921. 0031. 0131 0341. 095I. 1191 . 0000. 8920. 9010. 9060. 9250. 9410. 9680. 9810. 9951 0051. 0091.0171. 0261.0280. 9771. 0611 0701.0711. 0761. 0000. 9050. 9070. 9480. 9660. 9851 0021.0031. 0681. 1381 0000. 8940. 9300 9930. 9981. 0001.0021.0000. 9260.9640. 9660 9931. 1331. 1341. 1730. 7690. 9390. 8830. 9111. 1040. 906

KETHA 33A BVA VVA DDA BVA VVA BBA BDA BVA VVA 5BA BVA DBA 3VA DVA BBA 38A VVA BBA BBA BDA BVA t)3A BVA DBA 3DA 3VA BSA BBA B3A BB

BVVBVflBBBVBV

A 33A BVA DVA DDA VEA BVA BVA BVA V2A DVA DBA P3A DDA BDA DVA 3VA DVA DDA BB

AREACHGHT739J76.1888170.955636.445636.936508.1240700.277096.463972.431920,X

425791.1230510.621133.1482370.1549390.304008.1189820.123*44.238326.15B4930X356808.307988.1558570.600276.1009290.198563.377620.17B60B.666392.352644.-x

397828.186088.1469550.1480530.2138310.1424820.228660.1210770.799970.1 09936. -/

1082320.995464.809381.201304.1376090.1013020.762464.806027952189.748962. "790191.1108960.1141660.1169130.1141990.192712.

1011310.

) AMOUNT160.160.160160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160160.160.160.

000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000001000000000000000000000000000

NGNGNGNGNCNGNGNCNGNCNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNGNCNGNGNGNGNGNGNGNGNG

'/.TOT1. 341. 341 341. 341 341. 340. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 340. 341. 341. 341. 341. 341. 341. 341. 341. 341. 340. 341. 341. 341. 341. 341. 341. 340. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 341. 34

18756 87 SAMPLE DATA PACKAGE •_> o b

NO7879

NO12345678910111213141516171619202122232425262726293031323334353637363940414243444546474649505152

M/E SCAN TI!<£ PEF212 1079 16:29 37216 719 10: 39 28

RtT(L)7:66:6:7:7:7:7:7:7:7:7:7:6:9:6:B:8:8:8B:9:9:9:9:9:10:11:10:10:10:10:11:11:11:11:11:11:12:12:12:11:12:12:12:12:14:12:12:131313

12475358101426313740505257050726333750455502091425591251344044580928374755570309113434404145105051264157

RATIO RKT<:L>1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001 001. 001. 001. 00

10.10.10.10.1010.10.10.10.10.10.10.10.10.10.10.10.1050.10.10.10.10.10.10.1010.10.10.10.50.10.50.10.10.50.10.50.50.10.10.10.10.10.10.50.10.501010.10.5>0

000000000000000000000000000000000000000000000000000000OOO000000000000000000000000000000000000000000000000000000OOCOCO000000000000000000000000000000000000000

RRT METH0. 892 A BV0. 927 A BB

RATIO0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.

10091010101010101111111111091009090902101010101010111110090902090210100210020210101011111102100209091002

AKNT40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.

0000000000CO00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

AREA(HGHT)1167900.283040.

AMNT i40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160160.

ID00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

R.1.1.1.1.1.1.0.1.1.2.1.1.0.o.1.0.0.0.0.0.0.0.0.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.0.0.1.0.0.0.1.0.0.0.0.0.

AMOUNT160. 000160. 000

NGNS

FAC R. FAC(L)0003596723454553848413550506141622328844950009542104002075152913248274191954105430004193903B4110560337398274073112215430322278406542911179000116441233263123

1.1.1.1.1.1.0.1.1.2.1.1.0.0.1.0.0.0.0.0.0.0.0.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.0.0.1.0.0.01.0.0.0.0.0.

000359672345455384841353050614162232684495000954210400207315291324827419195410543000419390384110560337398274073112215430322278406542911179000118441233263123

'/.TOT1. 341. 34

RATIO1.1.1.1.1.1.1.1.11.1.1.11.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.111.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.11.

00000000CO00000000000000CO00000000CO0000000000000000000000000000000000CO00COCO00000000000000000000CO0000


NC535455565756596061626364656667686970717273747576777679

RtT(L)14:14:1516:1616:17:16:IB:16:18:20:1920:20:20:23:23:24:5:6:S:10:13:16:16:10:

121708072830322226282958241316524646353346034805432959

RATIO RRT(L)1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.

000000000000000000000000000000000000000000000000000000

1010.10.10.10.10.10.2010.10.1010.10.10.10.10.1010.100.0.0.0.1.0.101.

000000000000000000000000000000000000000000000000000000000742946e7*906115907000000

RATIO0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.1.0.1.1.0.1.0.0.

101011111009090510101010091010101111120499010199000993

Af:N'T160.160.160.160.40.160160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

000000000000000000000000000000000000000000000000000000

AMNT < L )160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

000000000000000000000000000000000000000000000000000000

R.0.0.1.0.1.1.0.0.1.1.0.1.1.1.0.1.1.0.0.1.1.0.1.0.1.1.0.

FAC R. FAC(L)973960416943000324875120184083835000957258947001183930981601648512030174106277257

0.0.1.0.1.1.0.0.1.1.0.1.1.1.0.1.1.0.0.1.1.0.1.0.1.1.0.

973980416943000324875120184038885000957238947001183930981601648512030174106277257

RATIO1.1.1111.1.1.11.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.1.

00000000000000000000000000000000000000CO00000000000000


COMPUCHEM LABORATORIES. INC.GC/MS ANALYSIS LOG

RUN LOO

INITIAL TIME OF TUNE

TIME TUNE EXPIRES ->o-' '

PREVENTIVE MAINTENANCE

ANALYSIS TYPE

FILE NAME DATE TIME EPA ID CASE NO STD ID • AMOUNIINJtCIH) COMMENTS (Lot • s, DiapoaMon. Etc )

nron

L*L Kfio/D90

±1 2*74

f° Itl'M

UJ(0ct'*oQCL

ctc,UJ_Ja.z:

r.Q

'•ftIOr-co

/toft it. IL -2Z2£

Piwcf- OS- Uux J»

10

u12

13

14

15

16

17

18

19

2O

21

22

23

24

?

SUPERVISOR APPROVAL



Lab Code: COMPU

Instrument ID:

Case No.: 18756 SAS No.: SDG No.: 07

08




LAB FILE ID: RRF20 = HG900102B08 RRF50 = HH900102B08RRF80 = HJ900102B08 RRF120= HI900102B08 RRF160= HK900102B08

COMPOUND

Phenol *bis (2-Chloroethyl) Ether2-Chloroiohenol1 , 3-Dichlorobenzene

RRF20

* 1.3181.1601.2891.488

1 , 4-Dichlorobenzene * 1.438Benzyl Alcohol1 , 2-Dichlorobenzene2 -Methvlohenolbis (2-Chloroisopropyl) Ether4 -Methy IphenolN-Nitroso-Di-n-Propylamine_:HexachloroethaneNitrobenzeneIsochorone

0.5401.3980.9280.8390.817

I 0.5810.5700.2780.540

2-Nitrochenol * 0.2132 . 4-DimethylphenolBenzoic Acidbis ( 2-Chloroethoxy ) Methane_2 , 4-Dichlorophenol <1 , 2 , 4-TrichlorobenzeneNaphthalene4-Chloroaniline

0.3030.1560.323

» 0.2890.4061.0530.418

Hexachlorobutadiene * 0.2274-Chloro-3-Methylphenol * 0.2702 -Methylnaphthalene 0.679Hexachlorocyclopentadiene # 0.4342 , 4 , 6-Trichlorophenol * 0.4312,4, 5-Trichlorophenol '2-Chloronaphthalene2-NitroanilineDimethyl PhthalateAcenaphthylene2 , 6-Dinitrotoluene3-Nitroaniline

0.4071.3310.1821.4121.6110.2660.228

Acenaohthene * 1.0582 , 4-Dinitrophenol4-Nitrochenol

¥ 0.162If 0.179

RRF50

1.5801.4201.4401.6841.4460.7071.4991.0851.2551.0470.8740.7430.3710.7530.2200.4130.2130.4390.3600.4271.0870.2800.2350.3770.7690.4540.4550.4191.3660.2361.3871.6720.2700.1691.0480.1480.227

RRF80

1.4241.3441.4871.7041.5290.6851.6771.0691.0411.0940.8280.7590.3300.6920.2250.4140.2140.4250.3850.4361.0870.4320.2430.3920.7880.4570.4240.4031.3180.2091.4231.6670.2740.2401.0410.1460.201

RRF120

1.6281.5531.5391.8341.6910.7521.6321.1311.2231. 1051.0000.8340.3610.7240.2050.3970.2270.4520.3630.4191.0690.4400.2340.4150.7140.5030.4260.4091.3280.2781.4591.6690.2910.2711.0370.1550.227

•RRF160

1.5961.5921.5381.7981.5960.8061.6440.9961.5131.1551.0550.9180.3590.7090.1920.4020.2280.4480.3390.3830.9100.4390.2030.4170.5950.4940.4260.4071.2500.3521.4081.5690.2910.2740.9710.1420.212

RRF

1.5091.4141.4591.7021.5400.6981.5701.0421.1741.0440.8680.7650.3400.6840.2110.3860.2080.4170.3470.4141.0410.4020.2280.3740.7090.4680.4320.4091.3190.2511.4181.6380.2780.2361.0310.1510.209

%RSD

8.8*12 . 37. 17.96.9*

14.37.57.7

21.512.721.3 =16.911.112.26.2*

12. 114.312.910.5*5.07.2

17 . 16.7*

16.2*10.96.2 =3.0*1.53.2

26.51.92.84. 318.03.3*5.2:

9.6-

FORM VI SV-1 1/87 Rev,

18756 87 SPMPLE DPJP PPCKPGE


Lab Name: COMPUCHEM LABS Contract: (2-88,-REVS

Lab Code: COMPU Case No.: 18756 SAS No.: SDG No.: 07

Instrument ID: 08



Max %RSD for CCC(*) = 30.0!

LAB FILE ID: RRF20 = HG900102B08 RRF50 = HH900102B08RRF80 = HJ900102B08 RRF120= HI900102B08 RRF160= HK900102B08

COMPOUND

Dibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenylether_Fluorene4-Nitroaniline4 , 6-Dinitro-2-Methylphenol_N-Nitrosodiphenylamine (!)_'4-Bromophenyl-phenyletherHexachlorobenzene

RRF20

1.4770.3381.3810.5891.1290.2050.135

k 0.4580.2330.287

Pentachlorophenol * 0.134PhenanthreneAnthraceneDi-n-Butylphthalate

1.0810.9751.222

Fluoranthene * 0.929PyreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo (a) AnthraceneChrysenebis (2-Ethylhexyl) Phthalate_Di-n-Octyl Phthalate 'Benzo (b) FluorantheneBenzo (k) Fluoranthene

1.5160.5490.1541.0590.8990.730

k 1.5651.3850.719

Benzo(a) Pyrene * 1.005Indeno (1.2. 3-cd) PyreneDibenzo (a , h) AnthraceneBenzo (q.h. i) Perylene

Nitrobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d52 -Fluorophenol2,4, 6-Tribromophenol

1

1.2310.8820.998

0.3601.3701.0551.1921.2290.161

RRF50

1.4250.3581.3920.5641.0810.1770.1470.2500.2570.2980.1661.0570.9911.4670.9741.7350.7670.0551.1030.9771.0342.2941.5070.8641.0831.1660.8720.938

-— — — — as— =0.4691.2841.1641.7401.5180.161

RRF80

1.4180.3681.4080.5731.0690.2180.1450.4890.2710.3120.1621.1191.0411.4911.0681.5800.7900.1531.2071.0361.1092.2161.5520.7491.1231.4461.0671.152

0.4331.1831.0881.7051.5020.164

RRF120

1.3900.4111.5250.5781.0160.2700.1390.4540.2680.2870.1701.0460.9551.5551.0901.3530.8550.1891.1921.0251.2372.3621.4720.8651.1601.5271.1371.188

0.4521.0920.9851.7941.6940.186

RRF160

1.3220.3991.4510.5470.9310.2420.1450.4700.2580.2790.1701.0100.9211.6031.0701.3380.9060.1851.2141.0391.2692.4341.6390.7341.1991.5451.1471.249

0.4661.0181.0211.7661.7790.174

RRF

1.4060.3751.4310.5701.0450.2220.1420.4240.2570.2930.1601.0630.9771.4681.0261.5040.7730.1471.1550.9951.0762.1741.5110.7861.1141.3831.0211. 105

0.4361. 1891.0631.6391.5440. 169

\RSD

4 .08. 04. 12.87.216.03.5

23 .2*5.84.49.5*3.84 .610.06.9*11.017 . 736.96.06.0

20. 016. 1*6.29.26.7*12.613.211.9

10. 311.96.4

15.413.76.4

[1) Cannot be separated from Diphenylamine

FORM VI SV-2 1/37 Rev,

18756 87 SWMPLE DPTP PPCKPGE

125.9

COMPUCHEM LABSRIC ^cUUwho CONPUCHEH DATA: HG998192B98 SCANS 382 TO 185991/92/99 23:45:99o9-° WT OF 382 TO 1859SAMPLE: 1UL SSTD-939 39829-2364 ON 88CONDS.: 984329.

ISfl ISi2 ISf3 SSt5

SSi2 SSi3 5514 0311 . ISM

SSK

SSI7

ISIS

RIC

IStS

13831658

1435 1545 16171743_ A _

6989:19

169615i 17

129918t29

149821:23

169824:26

189SCAN27:3HHE

UJ<o•Ii-TOCtCL

ctKct

UJ-JCLE•1

Q

•-0IOKCO

-UANTITATION REPORT FILE: H0900102B08DATA: H0900102B08. TI01/02/90 23:49:00 -SAMPLE: 1UL SSTD-O9O 30620-2364 ON 08CONDS. : °*° «LA .IfkoSUBMITTED BY: 08 ANALYST: 16O1

AMOUNT-AREA » REF.AMNT/(REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1. 4-DICHLOROBENZENE (ISttl)2 610 PHENOL <Q1«3> <108-99-2>3 411 B IS (2-CHLOROETHYL) ETHER (Qlt9) <Hl-44-4>4 601 2-CHLOROPHENOL (01*6) <99-97-8>3 421 1.3-DICHLOROBENZENE (01*7) <941-73-l>6 422 1. 4-DICHLOROBENZENE (Qlt8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-91-6>B 420 1.2-DICHLOROBENZENE (QltlO) <99-9O-l>9 62O 2-METHYLPHENOL (01*11) <99-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (Qlttl3) <106-44-9>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*19) <67-72-l>14 440 NITROBENZENE (01*16) <98-99-3>19 »46O D8-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-99-l>17 606 2-NITROPHENOL <Q2*3) <B8-79-9>IB 6O3 2,4-DIMETHYLPHENOL (02*4) <109-67-9>19 629 BENZO1C ACID (02*9) <69-89-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1.2.4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-2O-3>24 479 4-CHLOROANILINE (02*10) <106-47-8>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 60B P-CHLORO-M-CREBOL (02*12) <99-9O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>2B «499 D1O-ACENAPHTHENE (18*3)29 439 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4. 6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2< 4, 9-TRICHLOROPHENOL (03*4) <99-99-4>32 416 2-CHLORONAPHTHALENE (03*9) <91-98-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 429 DIMETHYL PHTHALATE (03*7) <131-ll-3>39 402 ACENAPHTHYLENE (03*8) <2O8-96-8>36 479 3-NITROANILINE (03*9) <99-O9-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 ft609 2,4-DINITROPHENOL (03*11) <91-28-9>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2. 4-DINITROTOLUENE (03*14) <121-l4-2>42 428 2.6-DINITROTOLUENE (03*19) <6O6-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7009-72-3>49 432 FLUORENE <Q3*18) <86-73-7>46 480 4-NITROANILINE <Q3*19) <100-Ol-6>

18756 87 SAMPLE DHlH PPCKPGE

NO474849909192939499969798996O61626364696667686970717273747976777879

NO123496789101112131413161718192021

NAME•467 D10-PHENANTHRENE (IS«4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <934-92-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-99-3>433 HEXACHLOROBENZENE (04*9) <1 18-74- 1>609 PENTACHLOROPHENOL (04*6) <87-B6-9>444 PHENANTHRENE (04*7) <89-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*499 D12-CHRYSENE (IS»9)449 PYRENE (03*3) <129-OO-0>419 BUTYLBENZYL PHTHALATE (09*4) <89-68-7>423 3. 3'-DICHLOROBENZIDINE (09*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-99-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PER YLENE429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO (B)FLUORANTHENE (06*3) <203-99-2>409 BENZO(K) FLUORANTHENE (06*4) <207-08-9>406 BENZO ( A) PYRENE (06*9) <90-32-8>437 INDENO (1, 2. 3-C.D) PYRENE (06*6) <l93-39-9>419 D I BENZO ( A, H) ANTHRACENE (06*7) <93-70-3>400 BENZO (0, H, I) PER YLENE (06*8) <191-24-2>•619 2-FLUOROPHENOL (S8*l)•612 D9-PHENOL (88*2)*447 D9-NITROBENZENE (88*3)•448 2-FLUOROB I PHENYL (SS*4)•628 2, 4, 6-TRIBROMOPHENOL (88*9)•496 D14-TERPHENYL (88*6)•471 D10-PYRENE496 1,2,3. 4-TETRACHLOROBENZENE

M/E SCAN TIME REF RRT METH AREA(HOHT)192 497 7:36 1 1. OOO ABB 109840.94 466 7: 07 1 0. 938 A BB 72376.93 ' 474 7: 14 1 0. 994 A BB 63684.128 482 7: 22 1 0. 970 A BB 70784.146- 494 7:33 1 0.994 A BV 81736.146 498 7:36 1 1.002 A VB 7896O.108 5O6 7:44 1 1.018 ABB 29640.146X 314 7:91 1 1.034 ABB 7678O.108 ' 313 7:32 1 1.036 ABB 30940.49 ' 319 7: 96 1 1 . 044 A BB 46O92.108 326 8:02 1 1.098 ABB 44860.70 330 8:06 1 1.066 ABB 31912.117 341 8:16 1 1.089 ABB 31320.77 346 8: 2O 13 0.901 ABB 447OO.136 606 9:13 13 1. OOO ABB 322OO8.82 363 8:38 13 0.932 ABB 86984.139 373 8:43 13 0.946 A B B 34216.107' 372 8:44 13 0.944 ABB 48744.122 376 8:48 13 0.990 A VB 29184.93- 380 8:32 13 0.937 ABB 32024.162- 393 9:03 13 0.979 AB B 46600.

AMOUNT40. 000 NO16. 319 NO14. 364 NO16. 738 NO16. 593 NO18. 016 NO13. 387 NO17. 010 NO18. 620 NO11. 094 NO14. 149 NO11. 019 NO12. 430 NO19. 472 NO40. OOO NO19. 237 NO22. 161 NO13. 079 NO13. 699 NO14. 431 NO17. 093 NO

XTOT2. 601. 070. 991. 091. 081. 170. 871. 111. 210. 720. 920. 720. 811.012.600. 991. 440. 980. 890. 941. 11


NO222324292627282930313233343936373839404142434449464748499O9192939499969798996O6162636469666768697071727374737677

M/E180128'127229107'142'164237196'196'16269163192X

138193184109'168169"169'149-204166138188198169'24B284266178 "178'149-202240202'149-292'228149'228'264149 x292 -292'292'276'278"276'1129982/172330244

SCAN60260861162269066876368869469771272173773179876876776878278074480O810813813899818.82089487188990190694910111191103210811140114911381134138212191307131113711638163817423974633447008361040

TIME9: 129: 179:209: 309:9610: 1211:4110:3110:3610: 3910:9311:0111: 1911:2811:3911:4411:4311:4411:9711:9911:2212: 1312:2212:2312:2913:4412:3012:3213:0313: 1813:3113:4613: 9014:2619:2717:3919:4616: 3117:2917:3317:2317:3821:0718:3419:982O:0220: 9729:2029: 2O26:376:047:068: 1910: 4212: 4613: 33

REF131319131919282828282828282828282828282828282828284747474747474747474797979797979797646464646464646411

19282837

RRT0. 9931.0031.0081.0261. 0731. 1021. 0000. 8990. 9070.9110. 9310. 9420. 9630.9820.9911.0041. 0031. 0041.0221.02O0.9731. 0461.0991.0631.0631. 0000.9100.9120.9900. 9690. 9841.0021.0081. 0911. 1291. 0000. 8970. 9390. 9900.9980. 9891.0031. 0000.8790. 9460. 9490. 9921. 2001. 2001. 2600. 7990. 9360. 8980. 9191. 0930. 904

METHA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BVA BBA VBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BB

AREA(HOHT) AMOUNT69408.169472.67396.36608.43424.109312.164896.39792.39900.33992.109716.19008.116408.132816.188OO.87278.13392.14764.121784.27904.21932.113892.48996.93044.16916.238290.16064.94916.27736.34148.19936.128744.116168.149988.110624.192692.1 1 3776.41876.11784.80896.99724.68608.114244.894OO.79140.41O64.97396.70312.30372.36992.67472.63464.37984.

1 1 2976.13264.80324.

21.23.19.22.12.22.40.17.2O.19.21.10.20.20.16.21.22.16.22.16.18.19.21.24.16.40.18.19.18.20.19.21.21.19.17.40.22.12.16.17.11.17.40.12.16.19.16.19.19.19.13.13.19.26.18.20.

236140041370928809000990238996292394093337649784819890349964296043990247943000340478021318769397190243361000661103718431303303000860906600737931373970810303443926430636

NONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONONO

XTOT1.381. 301.241. 430. 841. 482.601. 141. 321. 301. 380. 671. 301.341. 081. 421. 481. 101. 431. 101. 191. 241. 401. 381. 102.601.211.271. 171. 331. 031. 391. 380. 991. 132. 601. 470. 791. 091. 130. 731. 132. 600. 841. 101.271. 091. 041. 001. 040. 9O0. 881. 001. 731. 201.34


NO7879

NO1234967B910111213141916171819202122232429262728293O31323334393637383940414243444546474849503132

M/E SCAN TIME REF212 1031 13:43 37216 713 10:33 28

RET(L)7:337:O37: 137: 197:307:347:427:487:497:948:008:O98: 138: 189: 138:338:428:418:318:909:019:089: 149: 179:279: 9310:0911:3710:2710:3310:3610: 3010: 3811: 1211: 2611: 3211:4011:4011:4111:3311: 9211: 1912: 1012: 1912:2212:2213:4012:2612: 2812: 3913: 1313:28

RATIO RRT(L)1. 011. 001. 001. 011. 011. 01. 00. 01. 01. 00. 00

1. OO1. 011. 011. OO1. 011. 011. 010. 991. 001. 011. 011. 001. 001. 001. OO1. OO1. 011. 011. 001. 001. 001. 001. 011. 001. 001. 011. 001. 001. 011. 001. 001. 011. 001. 001. 001. 001. 001. 001. 001. 001. 00

10. OOO10. 00010. 00010. 00010. 00010. 00010. 00010. 00010. OOO10. 00010. 00010. OOO10. 00010. 00010. OOO10. OOO10. 00010. OOO30. OOO10. 00010. 00010. 00010. 00010. 00010.00010. OOO10. OOO10. 00010. 00010. OOO30.00010. 00030. 00010. 00010. 00030. OOO10. 00030. 00030. OOO10. 00010. 00010. 00010. OOO10. 00010. 00050. 00010. 00050. OOO10. 00010. 00010. 00050. 000

RRT0. 8960.932

RATIO0.0.0.0.0.0.0.o.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.o.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.

100910101010101010101111110910090909021010101010101111 -10090902090210100210020210101010111102100209091002

METHA BBA BB

AMNT40. 0016. 3214. 3616. 7616. 33iao213.3917. 01ia 6211.0914. 1311.0112.4313. 4740. OO13.2422. 1615.0813.7014. 4317. 1021.2423. 1419. 0422.3712.9322.8140. OO17. 3920.2420.0021.2910.3320.0620. 3416.6321.7822.8216.8922.3316.96ia 2619. 0421. 3324. 2316.9440.00ia 3419. 48ia 0220. 3213.77

AREA(HOHT) AMOUNT91376. 18. 317 NO38336. 29. 399 NO

AMNT(L)40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.

00OO0000000000OO0000OOOO00OO000000OO000000OO00000000OO0000OO0000000000000000000000OO00OO000000000000OO00

R. FAC R. FAC(L)1. 0000. 1630. 1430. 1610. 1860. 1800.0670. 1730. 1160. 1030. 1020. 0730. 0710.0331. OOO0. 0680.0270. 0380. 0200. 04O0. 0360. 0310. 1320. 0320. 0280.0340. 0831. OOO0. 0340. 0940. 0910. 1660. 0230. 1760. 2010. 0290. 1320. 0200. 0220. 1890. 0420. 0330. 1730. 0740. 1410. 0261. 0000. 0170. 0970. 0290. 0360. 017

1. 0001. 9961. 9921. 9381. 7981. 5960. 8061. 6440. 9961. 5131. 1531. 0330. 9180.3991. OOO0. 7090. 1920. 4020. 2280. 4480. 3390. 3830. 9100. 4390. 2030. 4170. 9991. 0000. 4940. 4260. 4071. 2900. 3921. 4081. 5690. 2740. 9710. 1420. 2121. 3220. 3990. 2911. 4510. 5470. 9310. 2421. OOO0. 1490. 4700. 2980. 2790. 170

XTOT1.201.92

RATIO1. 000. 100. O90. 100. 100. 110. 080. 110. 120. 070. 090. 070. 080. 101. 000. 100. 14O. 090. 090. 090. 110. 130. 140. 120. 140. 080. 141. 000. 110. 130. 120. 130. 060. 130. 130. 100. 140. 140. 110. 140. 110. 110. 120. 130. 190. 111. 000. 120. 120. 110. 130. 10


NO939499969798996061626364696667686970717273747976777879

RET(L)13:4313:4714:2219:2317:3019:4316:2717: 2017: 2817: 1717: 3420:3718:2619:9119: 9420:4829:0929:0726:256:017:04B: 1710:3912:4315:9015:4110: 91

RATIO RRT(L)1. 001. 001. 001. 001. 001. 001. 001. OO1. 001. 011. 001. 011. 011. 011. 011. 011. 011. 011. 01. 01. 00. 00. 00. 00. 00. 00

1. 00

10. OOO10. 00010. OOO10. 00010. 00010. 00010. OOO20. OOO10. 00010. 00010. OOO10. 00010. 00010. OOO10. 00010. OOO10. OOO10. 00010. OOO0. 7420. 9480. 8790. 9061. 1180. 90710. OOO1. 000

RATIO0. 100. 100. 110. 110. 100. 090. 090. 090. 100. 100. 100. 100. 090. 090. 090. 100. 120. 120. 131. 080. 991. 031. 010. 981. 000. 090.93

AMNT21.21.15.17.4O.22.12.16.17.11.17.40.12.16.19.16.15.15.15.13.13.15.26.ia20.ia29.

40192536006611724591310086916O769337978190499349669260

AMNT(L)160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

000000OOOO0000000000000000000000000000000000000000OO00

R. FAC R. FAC(L)0. 1330. 1220. 1330. 1161. OOO0. 1900. 0690. 0190. 1320. 0910. 1121. OOO0. 1960. 1730. 0900. 1260. 1340. 1100. 1230. 1340. 1490. 0430. 1710. 0200. 1320. 1300. 089

1. 0100. 9211. 6031. 0701. 0001. 3380. 9060. 1831. 2141. 2691. 0391. 0002. 4341. 6390. 7341. 1991. 5491. 1471. 2491. 7791. 7660. 4661.0180. 1741. 0211. 2930. 480

RATIO0. 130. 130. 100. 111.000. 140. 080. 100. 110. 070. 111. OO0. 080. 110. 120. 100. 100. 100. 100. 090. 080. 100. 170. 120. 130. 120. IB


COMPUCHEH LABSRIC COHPUCHEH DATA: HH909182B88 SCANS 383 TO 185881/92/99 29:91:98 OUT OF 383 TO 1859SAMPLE: 1UL SSTD 959 39821-2365 ON 98

1564158.

ISI1 ISt2 IS13 SStS SS«6

SSI2 SSI3 SSI4 D311 ISM SSi7

1515

ISt€

1638

1419 15671722

6999:19

129818:29

149821:23

169824:26

18905CAN27:3H ME

UJ'.DCt'X.O•ICL

•1

UJ-JCL2Z•I'/l

r.CD

•ftIOf -

JUANTITATION REPORT FILE: HH900102B08DATA: HH900102B08. TI01/02/9O 20:01:00SAMPLE: 1UL SSTD 050 30821-2369 ON OBCONDS. :SUBMITTED BY: 08 ANALYST: 1601

AMOUNT-AREA * REF. AMNT/(REF. AREA)» RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1, 4-DICHLOROBENZENE (IS*1>2 610 PHENOL (01*3) <108-99-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-8>5 421 1.3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1, 4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <10O-51-6>8 420 1,2-DICHLOROBENZENE (01*10) <99-90-l>9 620 2-METHYLPHENOL (01*11) <99-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-9>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*19) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 OS-NAPHTHALENE (I8*2)16 438 ISOPHORONE (02*2) <78-99-l>17 6O6 2-NITROPHENOL (02*3) <88-73-9>IB 603 2, 4-DIMETHYLPHENOL (02*4) <109-67-9>19 629 BENZO1C ACID (02*9) <65-89-O>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2, 4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1,2,4-TRICHLOROBENZENE (02*8) <12O-B2-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 479 4-CHLOROANILINE (02*10) <106-47-B>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (02*12) <99-90-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-37-6>28 »495 D10-ACENAPHTHENE (IS*3)29 433 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4,6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2. 4, 5-TRICHLOROPHENOL (03*4) <95-93-4>32 416 2-CHLORONAPHTHALENE (03*3) <91-38-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 423 DIMETHYL PHTHALATE (03*7) <131-ll-3>33 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 «603 2, 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2, 4-DINITROTOLUENE (03*14) <121-l4-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7O05-72-3>45 432 FLUORENE <03*1B) <B6-73-7>46 4BO 4-NITROANILINE (Q3»19> <100-01-6>


NO474849303132333439969798996061626364696667686970717273747976777879

NO1234967891011121314191617IB192021

NAME*467 D10-PHENANTHRENE (IS*4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <934-32-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-33-3>433 HEXACHLOR08ENZENE (04*9) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-9>444 PHENANTHRENE (04*7) <89-01-8>4CO ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <B4-74-2>431 FLUORANTHENE (04*10) <206-44-0>»439 D12-CHRYSENE (IS*9)449 PYRENE (09*3) <129-00-0>413 BUTYLBENZYL PHTHALATE (03*4) <83-68-7>423 3, 3'-DICHLOROBENZIDINE (09*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-99-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>»497 D12-PER YLENE429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO (B)FLUORANTHENE (06*3) <209-99-2>409 BENZO (K)FLUORANTHENE (06*4) <207-Q8-9>406 BENZO(A)PYRENE (06*9) <90-32-8>437 INDENO (1, 2, 3-C'D) PYRENE (06*6) <l93-39-3>419 D I BENZO ( A, H) ANTHRACENE (06*7) <33-70-3>408 BENZO ( 0, H, I) PER YLENE (06*8) <1 91-24- 2>«619 2-FLUOROPHENOL (SS«1)*612 D9-PHENOL (SS*2)«447 OS-NITROBENZENE (SS«3)•448 2-FLUOROB I PHENYL (SS»4)*628 2, 4, 6-TRIBROMOPHENOL (8S«3)•496 D14-TERPHENYL (SS*6>*471 D10-PYRENE496 1 , 2, 3, 4-TETRACHLOROBENZENE

M/E19294931281461461081461084910870117771368213910712293162

SCAN492461469477489493302509510515521526536541601559368567573373387

TIME7: 317:037: 107: 177:287:327:407:477:477: 527: 388:02B: 118: 169: 118:328: 41B: 408:438: 478: 38

REF1111111111111

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1.0.0.O.0.

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1.1.0.1.0.0.0.0.0.0.

RRT000937933970994002020039037047099069089900000930949943993997977

METH

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BBBBBBBBBVVBBBBBBBBBBBBBBBBBBBBBBBBB

A«VBAABBBB

AREA(HCHT) AMOUNT106016.209420.188212.190816.223128.191632.93716.198684.143720.166296.138788.1 1 9808.98444.1502O4.323776.304884.88964.166968.86324.177300.143772.

40.49.44.46.46.45.43.43.34.41.43.41.40.31.40.33.37.31.46.48.33.

000 NO321 NO394 NO804 NO817 NO302 NO833 NO603 NO428 NO469 NO340 NO413 NO478 NO707 NO000 NO116 NO303 NO377 NO700 NO967 NO184 NO

XTOT1. 071. 321. 191. 231. 231. 211. 171. 221. 431. 101. 211. 101. 081. 381. 071. 421. 331. 371. 241. 301. 42

IS'756 87 S A M P L E D A T A P A C K A G E

NO2223242926272829303132333439363738394041424344494647484990319293949996979839606162636463666768697071727374757677

M/E1BO1281272291071421642371961961626916319213819318410916816916914920416613818819816924828426617817814920224O202149292228149228264149292292292276278276112998217233O244

SCAN596602602616644662757681687691706714730744730761760760774773737792802806806891810812B4686387789389793710021142102410731131114011281149136812031299129813971638163817223914605396948281031

TIME9:069: 129: 129:259:9010:0711:3410:2410:3010: 3310:4710: 9411:0911:2211:27J 1 : 3711:3711:3711:4911:4811: 1912:0612: 1912:1912: 1913:3712:2212:2412:9913: 1113:2413:3813:4214: 1919: 1817:2719:3916:2317: 1717:2917: 1417:292O:3418:2319:4719:9020:4429:0129:0126: 189: 987:028: 1410: 3612: 3913:45

REF151515151919282828282828282828282828282828282828284747474747474747474797979797979797646464646464646411

15282857

RRT0. 9921.0021. 0021.0251. 0721. 1011. OOO0. 9000.9080. 9130. 9330.9430.9640.9830. 9911. 0091.0041. OO41. 0221. 0210. 9741. 0461. 0991.0691.0691.0000.9090.9110. 9490.9690.9841.0O21.0071.0921. 1291.0000.8970. 9400. 9900. 9980. 9881.0031.0000.8790.9470. 9490.9921. 1971. 1971.2990. 7990. 9390. 8970. 9171. 0940. 903

METHA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BVA BBA BBA BVA BBA BBA BVA BVA VBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BB

AREA(HOHT) AMOUNT172704.439904.113416.94976.192600.311396.172412.97788.98104.90196.294344.90948.298896.360280.36924.229792.31936.48848.307012.77120.98168.3OOOOO.121916.232972.38072.220884.40624.68916.71024.82200.49728.291864.273936.403032.268900.120672.261712.1 1 3720.8240.

166404.135B96.147412.77148.221192.149324.83344.104440.112432.84064.90416.201176.230996.189680.276788.34796.175536.

55.59.31.97.49.64.40.49.93.91.94.33.49.93.30.33.92.93.93.44.46.47.91.98.36.40.90.26.49.93.48.92.93.49.49.40.64.42.14.49.40.47.40.47.49.98.49.37.37.37.42.49.50.63.46.56.

7667388877191836100009624914106326162442819289220494478868393089749380664700009669997702688023138197499140008163287924447290490001169739O9193723992919662270249092290975


XTOT1. 491. 590. 891. 341.201. 721. 071. 221. 431. 371. 460. 901. 311. 420.821. 44I. 391. 421. 441. 191. 231. 281. 371. 990. 971. 071.390. 711. 331. 421. 301. 391. 431. 221.211. 071. 731. 130. 391. 211. 091. 291. 071.261.221. 971. 201. 011. 011.00I. 141. 311. 341. 681. 231. 52


NO7879

NO12349678910111213141916171819202122232423262728293O31323334393637383940414243444546474849503132

M/E SCAN TIME REF212 1022 15:37 57216 706 10:47 28

RET(L)7:337:037: 137: 197:307:347:427:487:497:948:008:098: 138: 189: 138:338:428:418:918:909:O19:089: 149: 179:279:9310:091 1 : 3710:2710:3310:3610: 9010: 9811: 1211:2611:3211:401 1 : 4011:4111: 9311: 9211: 1912: 1012: 1912:2212:2213:4012:2612:2812: 3913: 1313:28

RATIO RRT(L)1. 000. 990. 991. 001. 001. OO1. 001. 001. OO1.000. 990. 991. 001. 001. 000. 991. 001. OO0. 990. 99O. 991. OO1.000. 991.001. 001. 000. 991. 000. 991. OO1. 000. 991. 000. 990. 991.000. 990. 990. 990. 990. 990. 991. 001. OO1. 001. 001. 001. 001. 001. 000. 99

10.00010. OOO10. OOO10. 00010. 00010.00010. 00010. OOO10. OOO10. 00010. 00010. OOO10. 00010. OOO10. OOO10. 00010. OOO10. 00090.00010.00010. OOO10.00010. OOO10. OOO10.00010.00010. OOO10.00010. OOO10.00090. OOO10.00090. OOO10. OOO10.00030. OOO10. 00030. OOO30. OOO10.00010. 00010. OOO10. OOO10. OOO10.00030. 00010.00030. 00010. 00010. 00010. 00030. OOO

RRT0. 8990. 933

RATIO0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.o.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.0.

1009IO10IOIO10IO101011111109100909090210101010IO10111110O9090209021010021002021010101011110210020909IO02

METHA BBA BB

AMNT40.0049. 9244. 9946. 8046. 8243. 3043.8343. 6134.4341. 4743.3441. 4140.4831. 7140. OO93. 1237. 3131.3846.7048. 9733. 1833.7739.7431.8937.7243. 1864. 6140. 0043.9633.4931.4134.6333. 6249.2493. 2830-9333.9232.0353. 4333. 8944.8446. 3147.9731. 5438.0736.4740. OO30. 3726. 3649. 7733. 2748. 80

AREA(HGHT) AMOUNT221836. 36. 889 NO12/744. 61. 779 NO

AMNT(L)40.160.160.160.16O.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.

00OOOO0000000000000000000000000000000000000000000000OO00000000000000000000000000OO00000000000000OO000000

R. FAC R. FAC(L)1. OOO0. 4940. 4440. 4300. 9260. 4920. 2210. 4690. 3390.3920. 3270.2730. 2320. 1161. 0000.2390. 0690. 1290. 0670. 1370. 1130. 1330. 3400.0880. 0730. 1180. 24O1. 0000. 1420. 1420. 1310.4270.0740. 4330. 9220. 0930.3270.0460. 0710. 4490. 1120. 0840. 4390. 1760. 3380. 0991. OOO0. 0460. 0780. 0800. 0930. 032

. 000

. 396

. 392

. 338

. 798

. 3960. 8061. 6440. 9961. 3131. 1331.0990. 9180.3991.0000. 7090. 1920. 4020. 2280. 4480. 3390.3830. 9100. 4390.2030. 4170. 9991. 0000. 4940. 4260. 4071.2900. 3921. 4081. 3690.2740. 9710. 1420.2121. 3220. 3990. 2911. 4910. 947O. 9310. 2421. 0000. 1490. 4700. 2980. 2790. 170

XTOT1. 921. 63

RATIO1.000.310.280.290.290.280.270.290.340.260.280. 260. 230.321. OO0.330. 360. 320.290.310.330.330.370.200. 360.280. 401.000.290.330.320.340. 210.310. 330. 190. 340.330. 330. 340.280. 290.300.320. 360.231. 000. 320. 170. 310. 330. 31


NO939499969798996061626364696667686970717273747976777879

RET(L)13:4313:4714:2219:2317:3019:4316: 2717:2017:2817: 1717:3420:9718:2619:9119:9420:4829:0929:0726:296:017:048: 1710:3912: 4319: 9O19:4110:91

RATIO RRT(L)0. 990. 991. 001. 001. 001. 001. OO1. 001.001. 001. 001. 001.001. 001.001. 001.001. 001.000. 990. 990. 991. 001. 001.001. 000. 99

10. 00010. 00010. 00010. 00010.00010.00010. 00020.00010. OOO10. OOO10. 00010. 00010. OOO10. OOO10. 00010. OOO10. 00010. OOO10. 0000. 7420.9480. 8790.9061. 1180. 90710. OOO1.000

RATIO0. 100. 100. 110. 110. 100. 090. 090. 090. 100. 100. 100. 100. 090. 090. 090. 100. 120. 120. 131.070. 991.021. 010. 981. 000. O90.93

AMNT92.3193.8149.7449. 9140. 0064.8242. 3314. 7949. 4440. 7347.094O. 0047. 1249.979a9149. 1937.7237.9937. 3242. 6649. 2730.2363.0946.2936. 9836.8961.78

AMNT(L)160.160.160.160.40.160.160.160.160.160.160.40.16O.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

0000000000OO0000000000OOOO0000OO00000000OOOO000000OO00

R. FAC R. FAC(L)0. 3300. 3100. 4980.3041.0000. 9420. 2400. 0170.3430. 3230. 3O31. OOO0. 7170. 4710.2700.3380. 3640.2720. 2930. 4740. 3440. 1460. 4010.0300. 364O. 46O0. 183

1.0.1.1.1.1.0.0.1.1.1.1.2.1.0.1.1.1.1.1.1.0.1.0.1.1.0.

010921603070000338906183214269039000434639734199345147249779766466018174021293480

RATIO0.330. 340. 290.281. 000. 410. 260. 090. 280.290. 291. 000. 290.290. 370. 280.240. 240. 230. 270. 310. 310.390.290. 360.360.39

18756 87 SAMPLE DATA PACKAGE 3 1 '?

CO

COMPUCHEM LABSRIC COMPUCHEM DATA: HJ996192B68 SCANS 384 TO 185991/92/99 23:61:99 OUT OF 384 TO 1859SAMPLE: ILL SSTD 989 39822-2366 ON 98CONDS.: 2414878.

ISil ISt2

SSt2 SS*3

ISt3 SStS SSK

SSI4 D3f 1 IS*4 SSt7

IS13

IS*6

516RIC

1989

1211

1383

1256 11425 1519

1646

1 1739

A129918:29

149921:23

I169824:26

i18983CAN27:311 ME

uiCDcto'I0.

'I

UJ-JCL

r.

•ftIOr.co

JUANTITATION REPORT FILE: HJ900102B08DATA: HJ900102B08. TI01/02/90 23:01: OOSAMPLE: 1UL SSTD 080 30622-2366 ON 08CONDS. :SUBMITTED BY: 08 ANALYST: 1601

AMOUNT-AREA » REF. AMNT/(REF. AREA)« RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 «494 04-1, 4-DICHLOROBENZENE (IS*D2 610 PHENOL (01*3) <108-93-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <99-57-8>9 421 1,3-DICHLOROBENZENE (01*7) <341-73-l>6 422 1, 4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <10O-31-6>8 420 1,2-DICHLOROBENZENE (01*10) <95-50-l>9 620 2-METHYLPHENOL (01*11) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (Q1»12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*13) <67-72-l>14 44O NITROBENZENE (01*16) <98-93-3>19 «460 D8-NAPHTHALENE (I5*2)16 438 ISOPHORONE (02*2) <78-99-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2, 4-DIMETHYLPHENOL (02*4) <103-67-9>19 629 BENZO1C ACID (02*5) <69-B9-O>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1.2, 4-TRICHLOROBENZENE- (02*8) <120-B2-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 479 4-CHLOROANILINE (02*10) <106-47-8>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 6O8 P-CHLORO-M-CRESOL (02*12) <99-9O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>28 *499 D10-ACENAPHTHENE (IS*3)29 433 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4,6-TRICHLOROPHENOL (03*3) <88-Q6-2>31 626 2, 4, 5-TRICHLOROPHENOL (03*4) <95-95-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-58-7>33 476 2-NITROANILINE (03*6) <88-74-4>34 423 DIMETHYL PHTHALATE (03*7) <131-ll-3->33 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 *603 2,4-DINITROPHENOL (03*11) <31-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-l4-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 01ETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (Q3*17) <7005-72-3>45 432 FLUORENE <Q3*1B) <86-73-7>46 48O 4-NITROANILINE <Q3*19) <10O-01-6>


NO474849909192939439969798996O61626364696667686970717273747976777879

NO1234967B9101112131413161718192021

NAME*467 D10-PHENANTHRENE ( IS«4)604 4.6-DINITRO-2-METHYLPHENOL (04*2) <334-52-l>443 N-NITROSODIPHENYLAMINE (04*3) <B6-30-6>414 4-8ROMOPHENYL PHENYL ETHER (04*4) <101-59-3>433 HEXACHLOROBENZENE (04*9) <118-74-l>6O9 PENTACHLOROPHENOL (04*6) <B7-86-9>444 PHENANTHRENE (04*7) <83-Ol-6>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <B4-74-2>431 FLUORANTHENE (04*10) <206-44-0>•439 D12-CHRYSENE (IS*3)449 PYRENE (05*3) <129-00-O>419 BUTYLBENZYL PHTHALATE (09*4) <89-68-7>423 3, 3'-DICHLOROBENZIDINE (03*5) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <36-3S-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PER YLENE429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO (B)FLUORANTHENE (06*3) <209-99-2>409 BENZO (K)FLUORANTHENE (06*4) <207-08-9>406 BENZO(A)PYRENE (06*9) <90-32-B>437 INDENO(1,2, 3-C,D)PYRENE (06*6) <l93-39-9>419 D I BENZO ( A, H) ANTHRACENE (06*7) <93-70-3>408 BENZO (O.H, I) PER YLENE (06*8) <191-24-2>•619 2-FLUOROPHENOL (SS*1)•612 D9-PHENOL (88*2)«447 OS-NITROBENZENE (SS*3)•448 2-FLUOROB I PHENYL (88*4)•628 2, 4, 6-TRIBROMOPHENOL (88*9)•496 D14-TERPHENYL (SS«6>*471 D10-PYRENE496 1,2. 3, 4-TETRACHLOROBENZENE

M/E SCAN TIME REF RRT METH AREA(HCHT)192 499 7: 37 1 1. 000 A BB 96360.94 468 7:09 1 0.938 ABB 280144.93 476 7: 16 1 0. 994 A BB 264468.128 484 7:24 1 0.970 ABB 2926O8.146 496 7:39 1 0.994 A BV 339192.146 300 7: 38 1 1 . 002 A VB 300648.108 3O9 7:47 1 1.020 ABB 134768.146 316 7: 53 1 1. 034 A BB 3299OO.106 517 7:54 1 1.036 ABB 210392.49 321 7:38 1 1.044 ABB 204800.108 328 8:04 1 1.098 ABB 219196.70 333 8:09 1 1.068 ABB 162972.117 543 8:18 1 1.088 AB B 149260.77 346 8.22 13 0.901 ABB 201784.136 608 9:17 15 1.000 ABB 309644.82 366 8:39 15 0.931 ABB 423032.139 373 8:47 13 0.946 ABB 1374O8.107 374 8:46 13 0.944 A B B 233O08.122 581 8:32 13 0.996 A VB 131004.93 582 8:53 15 0.957 A B B 260180.162 394 9:04 15 0.977 A B B 235652.

AMOUNT4O.71.67.77.75.76.67.81.89.99.79.62.66.73.4O.78.93.82.75.75.91.

000402945398796636971618879046774818130336000020700407027984017

NONONONONONONONONONONONONONONONONONONONONO

XTOT0. 671. 191. 121.291.261. 261. 131. 361. 430. 921. 261.031. 101. 220.671.301. 961. 371. 291. 271. 52

18756 87 SAMPLE DATA PACKAGE 3 1 6

NO2223242926272829303132333439363738394O414243444946474849909192939499969796996O6162636469666768697071727374797677

M/E1801281272291071421642371961961626916319213819318410916816916914920416613818819816924828426617817814920224O2021492922281492282641492922922922762782761129982172330244

SCAN603609612623691669765688694698713721737752738768767768782780744BOO809813813899818.82O83487188990190994410101149103210801138114711361192137912111302130613691646164617303994673467018361039

TIME9: 139: IB9: 219:319: 3710: 1311:4110:3110:3610: 4010: 3311:0111: 1311:2911:391 1 : 4411:4311:4411: 5711: 5511:2212: 1312:2112:2312: 2313:4412:3012:3213:0313: IB13:3113:4613:4914: 2313:2617:3313:4616:3017:2317:3117:2117:3621:OO18:3019: 3319: 3720: 3123:0923:0926. 266:067:088:2010:4212:4613: 32

REF131315151515282828282828282828282828282828282828264747474747474747474757575797979797646464646464646411

19282837

RRT0. 9921. 0021. 0071.0291. 0711. 1001. 0000.8990.9070. 9120. 9320. 9420. 9630. 9830.9911. O041. 0031.0041. 0221. 0200. 9731. 0461.0961. 0631. 063l.OOO0. 9100. 9120. 99O0. 9690.9841.0021. 0071. 0901. 1231. 0000. 8980. 9400. 9900. 9980. 9891.0031.0000.8810. 9470. 99O0. 9931. 1971. 1971. 2960. 8000. 9360. 8980. 9161. 0930. 904

METHA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBBBBBBBBBBBBB

A BBA BBA BBA BVA VBA BBA BBA BBA BVA BBA BBA BVA BVA VBA BBA BBA BVA WA BBA BBA BB

BBBBBBBBBBBB

A BB

AREA(HOHT) AMOUNT266680.664724.264480.148912.239664.481916.178928.163140.191936.143728.470666.74968.90796O.999240.8986O.371664.92184.71812.9O6420.131316.9/740.502972.204960.381724.77940.218296.63380.213432.118920.136148.70932.488924.494448.690696.466180.138912.437792.218860.42332.334298.307144.287042.112880.900192.390468.169O96.293952.326368.240996.260044.299432.339480.264648.422546.38404.3013OO.

91.93.78.93.73.103.40.74.79.79.84.47.80.83.70.83.82.73.83.73.73.77.83.91.72.40.79.83.84.89.76.88.90.74.79.4O.94.69.66.79.69.79.40.72.73.81.74.74.74.73.67.77.74.93.73.83.

228360719346122833000033794116369315831013215732130882840735146615796882102000826217037273597600460376841000452744203337908814OOO819774686920843440731326273220017034200


XTOT1. 321. 591. 311. 991. 251. 760.671. 231.33. 32. 41

0. 79. 35. 42. 17

1. 431. 371.261. 431. 231. 231. 291. 401. 331. 20O. 67. 33. 39. 40. 49. 28. 48. 91

1. 241. 330. 671. 971. 161. 101. 321. 161.330.671. 21. 26. 36. 29. 29. 24. 23. 12. 29. 24

1. 951. 251. 42

IS'756 87 SAMPLE DATA PACKAGE Z15

NO7879

NO12345678910111213141516171819202122232425262728293031323334393637383940414243444946474849305132

M/E SCAN TIME REF RRT METH212 1030 19: 44 97 0. 896 A BV216 713 10: 93 28 0. 932 A BB

RET(L)7:337:097: 137: 197:307:347:427:487:497:948:008:098: 136: 189: 138:396:428:418:918:90:01.08: 14: 17:27:93

10:0911:3710:2710:3310:3610:9010:9811: 1211:2611: 3211:4011:4011:4111: 9311: 9211: 1912: IO12: 1912:2212:2213:4012:2612:2812: 9913: 1313:28

RATIO RRT(L)1. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011.011. 011.011. 011. 011. 001.011. 011. 011. 011. 011. 011.011. 011.011. 011. 001. Ol1. 011. OO1. 011. 011. 001. 011. 001. OO1. 011. 001. 001. 011. 001. OO1. 001. 001. 001. 001. 001. 001. 00

10.00010. 00010. 00010. 00010. OOO10. 00010. OOO10. OOO10. OOO10. OOO10. 00010. OOO10. 00010. OCOIO. OOO10. 00010. OOO10. 00050. 00010. 00010. OOO10.00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. 00010. 00030. 00010. OOO90. 00010. OOO10. 00090. OOO10. 0009O. OOO50.00010.00010. OOO10. OOO10. OOO10. 00010. OOO50. 00010. OOO50. OOO10. 00010. 00010. OOO50. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 100. 100. 110. 110. 110. 090. 100. 090. 090. 090. 020. 100. 100. 10O. 100. 100. 100. 11O. 110. 100. O90. 090. 020. 090. 020. 100. 100. 020. 100.020. 020. 100. 100. 100. 100. 110. 110. 020. 100. 020. 090. 090. 100. 02

AMNT40.71.67.77.75.76.67.81.85.55.79.62.66.73.4O.78.93.82.79.79.91.91.99.7a99.79.109.4O.74.79.79.84.47.80.89.7O.89.82.79.89.73.73.77.83.91.72.4O.79.83.84.89.76.

0040343680669762880377821334OO02704103980223367233128300037912373283012173138884731361BO8810OO8322042760

AREA(HOHT) AMOUNT392688. 87. 724 NO193176. 90. 222 NO

AMNT(L)40.160.160.160.160.16O.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.

0000000000OO00OOOO0000000000OO0000000000OO00OO0000000000OO0000000000OO0000OOOO00000000OO000000000000OO00

R. FAC R. FAC(L)1. 0000. 7120. 6720. 7440. 8320. 7650. 3430. 8390. 5350. 5210. 3470. 4140. 3790. 1631. OOO0. 3460. 1120. 2070. 1070. 2130. 1930. 2180. 3430. 2160. 1210. 1960. 3941. 0000. 2280. 2120. 2010. 6390. 1040. 7110. 8340. 1200. 3200. 0730. 1010. 7090. 1840. 1370. 7040. 2860. 5350. 1091. 0000. 0730. 2440. 1360. 1560. 081

1. 0001. 5961. 5921. 5381. 7981. 5960. 8061. 6440. 9961. 5131. 1591.0990.9180. 3991. OOO0. 7090. 1920. 4020.2280. 4480. 3390. 3830. 9100. 4390.2030. 4170. 3931. OOO0. 4940. 4260. 4071. 2300. 3321. 4081. 3690. 2740. 9710. 1420. 2121. 3220. 3990. 2911. 4310. 5470. 9310. 2421. 0000. 1450. 4700. 2560. 2790. 170

XTOT1. 461. 30

RATIO1. 000. 430. 420. 460. 470. 480. 420. 510. 540. 340. 470. 390. 410. 461. OO0. 490. 590. 520. 470. 470. 570. 570. 600. 490. 6O0. 470. 661.000. 460. 3O0. 490. 530. 300. 510. 530. 440. 540. 510. 470. 540. 460. 470. 490. 320. 370. 431. OO0. 3O0. 920. 930. 960. 48

18756 87 SAMPLE DATA PACKAGE 31 4

NO939499969798996061626364696667686970717273747976777679

RET(L)13:4313:4714:2219:2317:3019:4316:2717:2017:2617: 1717:3420:9716:2619:9119:9420. 4829:0929:0726:236:017:04B: 1710:3912:4313:3019:4110:91

RATIO RRT(L)1. 001. 001. 001. 001. 001. 001. OO1. OO1. 00. 00. 00. 00. 00. 00. 00. 00. 00

1. OO1. 001.011.011. 011. 011. OO1. OO1. 001. 00

10. 00010. 00010. OOO10. OOO10. 00010. 00010. OOO20. 00010. 00010. 00010. OOO10. 00010. 00010. OOO10. OOO10. OOO10. 00010. OOO10. 0000. 7420.9480. 8790. 9061. 1180. 90710. 0001. 000

RATIO0. 100. 100. 110. 110. 100. 090. 090. 090. 100. 100. 100. 100. 090. 090. 090. 100. 120. 120. 131. 080. 991. 031. 010.981.000.090. 93

AMNTBB,90.74.79.40.94.69.66.79.69.79.40.72.79.81.74.74.74.73.67.77.74.93.79.89.87.90.

604638840049742094918100827769928444733327220203207222

AMNT(L)160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)0. 3990. 9200. 7490. 9341. 0000. 7900. 3990. 0760. 6030. 9940. 9181.0001. 1080. 7760. 3790. 9620. 7230. 9340. 9760. 7910. 8930. 2160. 9920. 0820. 9440. 7O90. 271

1. 0100. 9211. 6031. 0701. 0001. 3380. 9060. 1891.2141. 2691. 0391. 0002. 4341. 6390. 7341. 1991. 5451. 1471. 2491. 7791. 7660. 4661. 0180. 1741. 0211. 2930. 480

RATIO0. 330. 370. 460. 301. 000. 390. 440. 410. 300. 440. 301. 000. 460. 470. 310. 470. 470. 470. 460. 420. 480. 460. 380. 470. 330. 330. 36

1S756 87 SAMPLE DATA PACKAGE 313

COHPUCHEM LABSRIC COHPUCHEH DATA. HI998192B98 SCANS 383 TO 179881/92/96 21:28:68 OUT OF 383 TO 1799SAMPLE: ILL SSTD 129 39823-2367 ON 98CONDS.: 2949118.

15*1 IS*2 IS13 SS*5 SS*6 IS*5

SS*2. SS*3 S5I4 D3fl '. 15*4 SSi7 IS«6

1135

1219

1392

13641645

1419A

6989:19

129918:29

149821:23

169924:26

SCANTIME

UJ

•I

OaCL

aK•i

UJ-JCL

•1

r.

••ft10r.co

JUANTITATION REPORT FILE: HI9OO102B06DATA: HI900102B08. TI01/02/90 21: 28:OOSAMPLE: 1UL SSTD 120 30823-2367 ON 08CONDS. :SUBMITTED BY: 08 ANALYST: 1601

AMOUNT-AREA » REF.AMNT/(REF. AREA)» RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1, 4-DICHLOROBENZENE (IS»1)2 610 PHENOL (01*3) <108-93-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-8>3 421 1,3-DICHLOROBENZENE (01*7) <341-73-l>6 422 1,4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <10O-31-6>8 420 1,2-DICHLOROBENZENE (01*10) <93-3O-l>9 620 2-METHYLPHENOL (01*11) <93-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-3>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*13) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>13 *460 D8-NAPHTHALENE (I3*2)16 438 ISOPHORONE (02*2) <78-99-l>17 6O6 2-NITROPHENOL (02*3) <86-73-9>16 603 2,4-DIMETHYLPHENOL (02*4) <103-67-9>19 629 BENZO1C ACID (02*9) <63-83-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1.2, 4-TRICHLOROBENZENE (02*8) <120-82-l>23 439 NAPHTHALENE (02*9) <91-20-3>24 473 4-CHLOROANILINE (02*10) <106-47-6>29 434 HEXACHLOROBUTADIENE (02*11) <87-66-3>26 606 P-CHLORO-M-CRESOL (02*12) <99-9O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>28 *499 D10-ACENAPHTHENE (I8*3)29 439 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4, 6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 9-TRICHLOROPHENOL (03*4) <99-99-4>32 416 2-CHLORONAPHTHALENE (03*9) <91-98-7>33 478 2-NITROANILINE (03*6) <B8-74-4>34 429 DIMETHYL PHTHALATE (03*7) <131-ll-3>39 402 ACENAPHTHYLENE (03*6) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 «609 2, 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <1OO-02-T>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-l4-2>42 428 2,6-DINITROTOLUENE (03*13) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7003-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>


NO474849909192939499969798996O61626364696667686970717273747976777879

NO123496789101112131419161718192021

NAME•467 D10-PHENANTHRENE (IS«4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <934-32-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-33-3>433 HEXACHLOROBENZENE (04*9) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-S6-9>444 PHENANTHRENE (04*7) <89-01-6>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>«499 D12-CHRYSENE (IS«9>449 PYRENE (09*3) <129-OO-O>413 BUTYLBENZYL PHTHALATE (03*4) <83-68-7>423 3, 3'-DICHLOR01ENZIDINE (03*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-39-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PER YLENE429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO(B) FLUORANTHENE (06*3) <209-99-2>4O9 BENZO(K)FLUORANTHENE (06*4) <207-08-9>4O6 BENZO(A)PYRENE (06*9) <9O-32-B>437 INDENO (1, 2, 3-C.D) PYRENE (06*6) <l93-39-9>419 DIBENZO(A.H) ANTHRACENE (06*7) <93-70-3>4O8 BENZO(0, H, DPERYLENE (06*8) <191-24-2>«619 2-FLUOROPHENOL (SS«1)•612 D9-PHENOL (88*2)•447 D3-NITROBENZENE (S8*3)•448 2-FLUOROBIPHENYL (SS*4>•629 2, 4, 6-TRIBROMOPHENOL (SS*3>•496 D14-TERPHENYL (SS«6)•471 D10-PYRENE496 1,2, 3, 4-TETRACHLOROBENZENE

M/E SCAN TIME REF RRT METH AREA(HOHT)152 497 7:36 1 1. OOO ABB 92332.94 466 7: 07 1 0. 938 A BB 490964.93 474 7: 14 1 0. 994 A BB 430144.128 482 7: 22 1 0. 970 A BB 426296.146 494 7:33 1 0.994 A BV 908O12.146 498 7:36 1.002 A VB 468416.108 506 7:44 1.018 A BV 208308.146 514 7:91 1.034 BB 492168.108 519 7:92 1.036 W 313416.49 919 7:96 1.044 BB 338628.108 326 8:02 1.098 VB 306140.70 331 8:07 1 1.068 BB 277072.117 341 8:16 1 1.089 BB 230940.77 346 8:20 13 0.902 ABB 339432.136 60S 9:14 13 1. OOO ABB 313788.82 369 8:38 19 0.934 ABB 681636.139 572 8:44 13 0.949 ABB 193148.107 372 8:44 13 0.949 ABB 373428.122 580 8:52 IS 0.999 A VB 2140OO.93 38O 8:52 15 0.999 A B B 429844.162 392 9:03 13 0.979 ABB 342032.

AMC40.122.117.120.122.127.111.119.136.96.114.113.109.120.40.122.128.118.119.121.128.

UNT000444021049389143920171283939833770031368000332373330437217768


XTOT0. 441. 341.283134392230

1. 491.061. 261.231. 191.320. 441.341. 411. 301. 311. 331. 41

18756 87 SAMPLE DATA PACKAGE 31 0

NO2223242926272829SO31323334393637383940414243444946474849909192939499969796996O6162636469666768697071727374737677

M/EISO1281272291071421642371961961626916319213819318410916616916914920416613818819616924828426617817814920224O2021492922261492282641492922922922762782761129982172330244

SCAN6016076106216496677636876936967117207397907977677667677807797437988088128128968178188928698649OO90494310091149103110791138114711341192137412101302130613641649164417283974633446998331038

TIME9: 119: 169: 199:299:5910: 1111:3910:3010:3910:3810:9211:0011: 1411:2711:3411:4311:4211:4311: 9911: 9411:2112: 1112:2112:2412:2413: 4312:2912: 3O13:0113: 1613:3013:4913:4914:2419:2917:3319:4916:2917:2317:3117: 1917:3620: 9918:2919: 9319:9720: SO23:0823:0726:246:047:068: 1910:4112:4313: 31

REF131315151513282828282828282828282828282828282828284747474747474747474757575737373797646464646464646411

13282837

RRT METH0. 993 BB1.003 BB1.008 BB1. 026 BB1.073 BB1. 102 BB1.000 BB0. 900 BB0. 908 BV0. 912 VB0. 932 BB0. 944 A BB0. 963 A BB0. 983 A BB0. 992 A BV1. 0031.0041. 0031. 0221. 0210.9741.0461. 0391. 0641. 0641. 0000.9100.9110. 9490.9680. 9841.0021. 0071.0901. 1241.0000.8970. 9390.9900.9980. 9871.0031.0000.8810.9460. 991

BBBB•BBBBBBBBBBBBBBBBBBBBBVBBBBBBBVVBBBBBBBWBVBVBVBVVBBBWBVVB

0. 993 A BV1. 197 A BB1. 197 A BV1. 298 A BB0. 799 A BB0. 936 A BB0. 899 A BB0. 916 A BB1 . 094 A BB0. 903 A BB

AREA(HOHT) AMOUNT394060.10063OO.414364.220940.390452.672224.172188.239616.220248.211136.68616O.143668.793904.861920.139772.939792.803OO.117236.717816.212164.130320.787888.298344.324764.139432.238380.99348.324744.191960.2O4912.121416.747968.683164.1112710.779740.168066.662392.431064.99108.600673.623464.916681.144O64.1020660.636179.373630.901268.660053.491464.913489.469396.496892.429920.963872.96088.496736.

131.141.120.138.119.143.40.122.120.120.127.94.124.127.118.128.131.128.126.123.119.126.126.130.133.40.114.119.124.123.120.124.124.116.122.40.121.113.122.117.116.118.40.116.107.141.116.118.118.114.114.121.116.128.127.119.

292004208293287916000184249900920917319633912133034442192929986198701968797000989990383042067229930389291000344209989820990402000426773422099993990106283914319698994762


XTOT. 44. 94.32. 91. 31

1. 980. 441. 341. 321. 321. 401. 041.361. 401. 301. 401. 431. 411. 38. 39.31.38.39. 43. 46

0. 441. 291. 271.361.391. 311.361.361.271.340. 441. 331. 241.341. 291. 281. 300.441.271. 181. 991. 271. 301. 301. 291. 291. 331.271. 411. 401.27

IS'756 87 SAMPLE D A T A PACKAGE

NO7879

NO12349676910111213141916171819202122232429262726293031323334393637363940414243444346474649909192

M/E SCAN TIME REF RRT METH212 1029 19:43 97 0.896 A BV216 712 10: 93 28 0. 933 A BB

RET(L)7:337:097: 137: 197:307.347:427.487:497:348:008:038: 13B: 189: 136:398:428:418:916:909:019:069: 149: 179:279:9310:091 1 : 3710:2710:3310:3610:9010:9811: 1211: 2611:3211:4011:4011:4111: 931 1 : 9211: 1912: 1012: 1912:2212:2213:4012: 2612: 2812: 9913: 1513:28

RATIO RRT(L)1.011.001. 001.011.011. 011. 001.011. 011.001. OO1. OO1.011.011. 001. 011. 001.011. 001. 001. 001.011. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. OO1. OO1. 00. 00. 00. 00. 00. 00. 00

1. 001. 001. 001. 001. 001. 001. 001. 001. 00

10. 00010. 00010. OOO10. OOO10. OOO10. OOO10. 00010. 00010. 00010. 00010. OOO10. OOO10. OOO10. 00010. 00010. OOO10. 00010.00030. 00010. 00010.00010. 00010. 00010. 00010. OOO10. 00010. OOO10. 00010. OOO10. OOO50. 00010. 00030. OOO10.00010. 00030. 00010. 00030. 00050. OOO10. 00010. 00010. 00010.00010. 00010. OOO50. 00010. OOO50. OOO10. 00010. 00010. OOO30. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 100. 100. 110. 110. 110. 090. 100. 090. 090. 090.020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 100. 110. 110. 020. 100. 020. 090. 090. 100. 02

AMNT40.122.117.120.122.127.111.119.136.96.114.113.109.120.40.122.12a118.119.121.12a131.141.120.isa119.143.40.122.120.120.127.94.124.127.na128-131.12a126.123.119.126.126.130.133.40.114.115.124.123.120.

00440203391492172896837703370093379946227729002129299200182990929232639113034419939916709776009893380407

AREA(HGHT) AMOUNT6332OO. 116. 946 NO270236. 130. 870 NO

AMNT(L)40.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.160.160.160.160.

0000000000000000000000000000000000OO0000000000OO000000000000OO0000000000OO0000000000000000OO000000000000

R. FAC R. FAC(L)1.0001. 2211. 1631. 1541. 3761. 2680. 3641. 2240. 8490. 9170. 8290. 73O0. 6230. 2701. 0000. 5430. 1340. 2980. 1700. 3390. 2730. 3140. 8020. 33O0. 1760. 3110. 3361. 0000. 3770. 3200. 3070. 9960. 2O91. 0941. 2310. 2030. 77B0. 1170. 1701. 0420. 3080. 219I. 1440. 4330. 7620. 2021. 0000. 1040. 3410. 2010. 2150. 127

1.0001. 5961. 5921. 5381. 7981. 5960. 8061. 6440. 9961. 5131. 1531. 0330. 9180. 3391. 0000. 7090. 1920. 4020. 2280. 4480. 3390. 3830. 9100. 4390.2030. 4170. 3931. OOO0. 4940. 4260. 4071. 2300. 3321. 4O81. 5690. 2740. 9710. 1420. 2121. 3220. 3990. 2911. 4510. 5470. 9310.2421. OOO0. 1450. 4700. 2580. 2790. 170

XTOT1.281. 43

RATIO1. 000. 770. 730. 730. 760. 790. 700. 740. 830.610. 720. 710.660. 731. OO0. 770. 600. 740. 750. 760. BO0. 820. 880. 750. 860. 750. 9O1. OO0. 760. 750.750. 800. 590. 780. SO0. 740.800. 820. 800. 790. 770. 750. 790.790.820.841.000. 720. 720.780. 770. 73


NO333453363738396061626364636667666970717273747376777879

RET(L)13:4313:4714:2219:2317:3019:4316:2717: 2017:2817: 1717:3420:3718:2619:3119:3420:4623:0925:0726:296:017:046: 1710:3912:4319: 9019:4110:91

RAT 1C1. 001. 001. 001. 001. 001. 001. OO1. 001. 001. OO1. 001. 001. 001. 001.001. 001. 001. 001. 001. 01.00. 00. 00. 00. OO. 00. 00

) RRT(L)10. 00010. 00010. 00010. 00010. 00010. 00010. OOO20. 00010. 00010.00010. 00010. OOO10. 00010.00010.00010. OOO10. OOO10.00010. OOO0. 7420. 9480. 8790. 9061. 1180. 9O710. OOO1. 000

RATIO0. 100. 100. 110. 110. 100. 090. 090.090. 100. 100. 100. 100. 090. 090. 100. 100. 120. 120. 131. 080. 991.031. 010. 981. 000. 090. 93

ftf124.124.116.122.40.121.113.122.117.116.118.40.116.107.141.116.iiaiia114.114.121.116.i2a127.119.116.130.

INT229339290034213982934000437742033993112891327099769387

AMNT(160.160.160.160.40.160.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.

L)0000000000000000000000000000000000000000OO000000OO0000

R. FAC f0. 7840. 7161. 1660. 8181. OOO1. 0130. 6410. 1410. 8940. 9270. 7691. OOO1. 7711. 1040. 6480. 8701. 1490. 8930. 8911. 2711. 3490. 3390. 8190. 14O0. 7390. 9490. 392

». FAC(L)1. 0100.9211. 6031. 0701. 0001. 3380. 9060. 1891. 2141. 2691. 0391. 0002. 4341. 6390. 7341. 1991. 9491. 1471. 2491. 7791.7660. 4661. 0180. 1741. 0211. 2930. 480

RATIO0. 780. 760.730.761.000. 760.710.770. 740.730. 741. 000. 730. 670. 880. 730. 740. 740. 710. 710. 760. 730. 800. BO0. 720. 730. 62

1S'756 87 SAMPLE DATA PACKAGE 30 r

COMPUCHEM LABSRIC COMPUCHEM DATA: HK969192B98 SCANS 379 TO 185991/92/99 22:26:99 OUT OF 379 TO 1859SAMPLE: ILL SSTD 169 39824-2368 ON 68CONDS.: 3619839.

IStl IS12 IS*3 SS*5

S5i2 S5I3 SS§4 D311 . ISt4

SSI6 ISI5

IS*6

1132

. 1297

1299

1246 II NL

1645

1729

1421 1 Jl 1787

12:13199915:17

129618:26

I48621:23

169924:26

189SCAN27:38 HE

UJCD•I

O

o.•IK•1

Ul-JCL

r.

••ft10r -

OUANTITATION REPORT FILE: HK900102B08DATA: HK900102B08. TI01/02/90 22:26:00SAMPLE: 1UL SSTD 160 30824-2368 ON 08CONDS. :SUBMITTED BY: 06 ANALYST. 1601

AMOUNT-AREA * REF. AMNT/<REF. AREA)* RESP. FACT)RE8P. FAC. FROM LIBRARY ENTRY

NO NAME1 »494 D4-1, 4-DICHLOROBENZENE (19*1)2 610 PHENOL (01*3) <108-93-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 6O1 2-CHLOROPHENOL (01*6) <95-37-8>9 421 1,3-DICHLOROBENZENE (01*7) <941-73-l>6 422 1,4-DICHLOROBENZENE (01*6) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-91-6>8 420 1,2-DICHLOROBENZENE (01*10) <99-90-l>9 62O 2-METHYLPHENOL (01*11) <99-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-9>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*19) <67-72-l>14 440 NITROBENZENE (01*16) <98-99-3>19 *460 OS-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-39-l>17 606 2-NITROPHENOL (02*3) <88-79-9>16 603 2,4-DIMETHYLPHENOL (02*4) <109-67-9>19 629 BENZO1C ACID (02*9) <69-B5-O>20 410 BIB(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-B3-2>22 446 1.2,4-TRICHLOROBENZENE (02*8) <12O-B2-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 479 4-CHLOROANILINE (02*10) <106-47-8>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 606 P-CHLORO-M-CRESOL (02*12) <99-9O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>28 *499 D10-ACENAPHTHENE (I8*3)29 435 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 511 2,4,6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 3-TRICHLOROPHENOL (03*4) <93-93-4>32 416 2-CHLORONAPHTHALENE (03*9) <91-98-7>33 476 2-NITROANILINE (03*6) <68-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*6) <208-96-8>36 479 3-NITROANJLINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 -6O5 2,4-DINITROPHENOL (03*11) <51-28-9>39 607 4-NITROPHENOL (03*12) <100-O2-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <B4-66~2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <70O5-72-3>45 432 FLUORENE (03*18) <86-73-7>46 48O 4-NITROANIL1NE (Q3»19) <lOO-Ol-6>

'56 07 SAMPLE DATA PACKAGE 305

NO474849909192939499965798996061626364696667686970717273747976777879

NO123496789101112131419161718192021

NAME•467 D10-PHENANTHRENE (IS*4)6O4 4, 6-DINITRO-2-METHYLPHENOL (04*2) <934-92-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-99-3>433 HEXACHLOROBENZENE (04*9) <1 18-74-1 >609 PENTACHLOROPHENOL (04*6) <87-B6-9>444 PHENANTHRENE (04*7) <89-01-6>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*459 D12-CHRYSCNC (IS»5)449 PYRENE (09*3) <129-OO-0>419 BUTYLBENZYL PHTHALATE (05*4) <83~68-7>423 3, 3'-DICHLOROBENZIDINE (09*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-99-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PERYLENE429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO(B)FLUORANTHENE (06*3) <209-99-2>409 BENZO (K)FLUORANTHENE (06*4) <2O7-Q8-9>406 BENZO(A)PYRENE (06*9) <90-32-8>437 INDENO (1, 2, 3-C.D) PYRENE (06*6) <l93-39-3>419 D I BENZO ( A, H) ANTHRACENE (06*7) <S3-70-3>408 BENZO(0, H, DPERYLENE (06*8) <l91-24-2>«619 2-FLUOROPHENOL (SS«1)•612 D3-PHENOL (88*2)•447 OS-NITROBENZENE (SS*3)•448 2-FLUOROB I PHENYL (SS«4)•628 2, 4, 6-TRIBROMOPHENOL (88*3)•496 D14-TERPHENYL (SS*6)•471 D10-PYRENE496 1 , 2, 3, 4-TETRACHLOROBENZENE

M/E SCAN TIME REF RRT METH AREA(HOHT)192 494 7:33 1 1. OOO ABB 92192.94 464 7:09 1 0.939 BB 968392.93 472 7: 13 1 0. 999 BB 987232.128 479 7: 19 0. 970 BB 967248.146 491 7: 30 0. 994 BV 663120.146 499 7: 34 . 002 VB 988964.106 504 7:42 . 02O BV 297344.146 311 7:48 .034 BB 6O6164.108 312 7:49 .036 W 367396.49 317 7: S4 . 047 A BB 357952.106 524 8:00 1.061 A VB 4259OO.70 329 8:09 1.071 ABB 389068.117 338 8:13 1 1.089 AB B 338384.77 343 8: 18 IS 0. 9OO A BB 473836.136 603 9:13 15 1. OCO A B B 331476.82 362 8:33 IS 0.932 AB B 940240.139 370 8:42 IS 0.949 AB B 29430O.107 369 8:41 13 0.944 A B B 532404.122 579 8:31 15 0.960 A W 302788.93 578 8:30 13 0.939 A B B 393776.162 390 9:01 13 0.978 ABB 448972.

AMOUNT40.160.160.160.160.160.160.160.160.160.160.160.16O.160.40.160.160.160.160.160.160.

COOCOO000COO000COOCOO000000000OOO000000000coocoo000coocoo000OOO


XTOT0. 341. 341. 3434343434343434343434

1. 340.341. 341. 341. 341. 341. 341. 34

1 8 756 SAMPLE DATA PACKAGE 3 0 4

NO22232429262726293031323334393637383940414243444946474649SO919293949996979899606162636469666766697071727374797677

M/E160126127229107142164237196196162691631921361931841091661691691492041661381661981692482642661781781492022402021492922281492282641492922922922762782761129982172330244

SCAN39860960661964766976168469169470971873374679976476476977877774179680681081089981481683O86788289890294110071146102910771133114411321130137112071299130313621646164417293944633426978321036

TIME9:089: 149: 179:279: S310:0911:3710: 2710:3310: 3610: 3010:5811: 1211:2611:3211:4011:4011:4111: 5311: 5211: 1912: 1012: 1912:2212:2213:4012:2612:2812: 5913: 1313:2613:4313:4714:2213:2317:3013:4316: 2717:2017:2817: 1717:3420: 3718:2619: SI19: 5420:4825:0925: 0726:256:017:048: 1710: 3912: 4313: 30

REF1313IS13131328282828282828282B282828282826262828284747474747474747474737575757379797646464646464646411

15282837

RRT METH0. 992 A BB. 003 A BB. 006 A BB. 027 A BB. 073 A BB. 103 A BB. 000 A BB

0. 899 A BB0. 908 A BV0. 9120. 9320. 9430. 9630.9830. 992

VBBBBBBBBBBV

1. 004 A BB1. 004 A BB1.009 A BB1. 022 A BB1. 021 A BB0. 974 A BB1. 046 A BB1. 0991. 0641. 0641. 0000. 9090.9120.9900. 9690. 989

BBBVBVBBBBBBBBBBBB

1. 003 A BV1. OO8 A VB1. 091 A BV1. 1291.0000. 8980. 94O0.9900. 9980. 9881. 0031. 0000. 88O0. 9470.9900. 9931. 2011. 1991. 2610. 798

BVBBBVBVBBBVBVVBBBVBBVVBBVBBBBBBBB

0. 937 A BB0. 899 A BB0. 916 A BB1 . 093 A BB0. 904 A BB

AR EA ( HOHT ) AMOUNT907296. 160. 0001206240. 160. 000962620.269940.993236.789480.170904.337432.290880.278296.894906.240372.962936.1072440.167296.664008.97320.144992.903624.272780.199220.991792.373944.636332.169968.218976.127432.41 1640.226396.244772.148628.884996.806304.140490O.937132.144212.772O64.922792.106916.700162.731892.999100.124376.1210960.819398.364944.996639.766614.970790.621614.696116.691080.618328.699792.1 1 9220.389 108.

160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.160.16O.160.160.160.160.160.160.160.40.16O.160.160.160.160.160.40.160.160.160.160.160.160.160.160.160.160.160.160.160.

000000OOOOOOOOOOOO000OOO000000OOO000000000000000000coo000coocoo000000OOO000000000coo000OOO000OOO000000000000000OOOcoocooOOO000001001001000000000000000cooOOO000000


XTOT1. 341. 341. 341.341.341. 340. 341. 341. 341. 341. 341. 341. 34. 34. 34. 34. 34. 34. 34

1. 341. 341. 341. 341. 341. 340. 341. 341. 341.341. 341. 341. 341.341. 341. 340. 341. 341. 341.341.341. 341.340. 341. 341. 341.341. 341. 341.341.341. 341. 341. 341. 341. 341. 34


NO7879

NO123496789

101112131419161718192O2122232429262728293031323334393637383940414243444946474849903132

M/E SCAN TIME REF RRT METH212 1027 15:41 57 0.696 A BV216 710 10:51 28 0.933 A B B

RET(L)7:337:057: 137: 197:307:347:427:487:497:948:008:098: 138: 189: 138:398:428:418:918:90

:01:08: 14: 17:27:S3

10:0911:3710:271O:3310:3610:9010: 9811: 1211:2611:3211: 4O11:4011:4111:9311:9211: 1912: 1012: 1912:2212:2213:4012:2612:2812:9913: 1513:28

RATIO RRT(L)1. 001.001. OO1. 001. 001. 001. 001. CO1. 001.001. CO1. 001. 001. 001. OO1. 001. 001. CO1. 001. CO1. 001. 001. 00l .OO1.001.001. CO1. OO1. 001. 001. 001. 001. 001. 001. 001. 001. OO1. OO1. 001. 001. OO1. OO1. 001. 001. OO1. 001. 001. 001. 001. 001. 001. 00

10. 00010. 00010. OOO10. 00010. OCO10. OCO10. OCO10. 00010. 00010. 00010. OOO10. 00010. OOO10. OOO10. OCO10. 00010.00010. OCO30.00010. OOO10. OCO10. 00010. 00010. OOO10. OOO10. 00010. OOO10. OOO10. 00010. OOOSO. 00010. 000SO. OOO10. 00010. 000SO. 00010. 000SO. OOOSO. OOO10.00010. OOO10. OOO10. OCO10. 00010. OOO30. OOO10. OOO30. OCO10. OOO10. OCO10. OCO30. OOO

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 100. 100. 110. 110. 110. 090. 100. 090.090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 100. 110. 110. 020. 100. 020. 090. 090. 100. 02

AMNT40.

160.160.160.160.160.160.160.160.16O.160.160.160.160.40.

160.160.160.160.160.160.160.160.16O.160.160.160.

4O.160.16O.16O.160.160.160.16O.160.16O.16O.16O.16O.16O.16O.160.160.16O.160.40.

160.160.160.16O.160.

CO00000000CO0000COCOCOCOCOCO00CO00COCO0000CO00CO00COCOCO00OOCOCOCOCOCOOO0000CO00000000COCO00COCOCOCO00CO

AREA(HOHT) AMOUNT743696. 160. OOO NO327948. 160. 000 NO

AMNT(L)40.

160.160.160.160.160.160.160.160.160.160.160.160.160.40.

160.160.160.160.160.160.160.160.160.160.160.160.40.

160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.160.40.

160.160.160.160.160.

0000CO00OO00000000OOCOCOCOCOCO00OO00OO00OOCOCOCOCOCO00CO00COCO00COCOCO00CO0000COCOCOCOCOCOCOCOOOCOCO00CO

R. FAC R. FAC(L)1. 0001. 3961. S921. 3381. 7981. S960. 8061. 6440. 9961. 3131. 1591. 0990. 9180. 3991. COO0. 7090. 1920. 4020. 2280. 4480. 3390. 3830. 9100. 4390.2030. 4170. 9991. 0000. 4940. 4260. 4071. 2900. 3921. 4081. 9690. 2740. 9710. 1420. 2121. 322O. 3990. 2911. 4910. 5470. 9310. 2421. COO0. 1450. 4700. 2580. 2790. 170

1.0001. 5961. S921. 3381. 7981. 3960. 8061. 6440. 9961. 3131. 1331. OSS0. 9180. 3391. 0000. 7090. 1920. 4020.2280. 4480. 3390. 3830. 9100. 4390.2030.4170. S9S1. COO0. 4940. 4260. 4071. 2300. 3321. 4081. 3690. 2740. 9710. 1420. 2121. 3220. 3990. 2911. 4310. 5470.9310. 2421. OOO0. 1430. 4700. 2380. 2790. 170

XTOT1. 341. 34

RATIOl .OOl.OO1. OO1. 001. CO1. 001. OO1.001. 001.001. CO1. 001. 001. 001. OO1. 001. OO1. OO1. CO1. 001. OO1. OO1. CO1. 001.001.001. OO1. CO1. OOl.OO1. 001. 001. 001. 001. CO1. 001. 001. OO1. 001. 001.001. 001.001. CO1. 001.001. 001.001. CO1. CO1. CO1. CO

1S756 07 SAMPLE DATA PACKAGE

NOS354S3963738996061626364636667686970717273747376777879

RET(L) R.13:13:14:19:17:19:16:17:17:17:17:20:18:19:19:2O:29:29:26:6:7:8:10:12:19:19:10:

434722233043272O28173497269194480907290104173943904191

111111111111111111111111111

RATIO R R T ( L )1. 00 10. OOO1. 00 10. OOO1. 00 10. OOO1.00 10. OOO1. 00 10. OOO1. 00 10. 0001. 00 10. OCO1.00 20. OOO1. 00 10. OOO1. 00 10. OOO1. 00 10. OCO1. 00 10. OOO1. 00 10. 0001.00 10.0001. 00 10. OOO1. 00 10. OCO1. 00 10. 0001. 00 10. 0001. 00 10. OOO1. OO 0. 7421. OO O. 9481.00 0.8791.00 0.9061. CO 1. 118l .OO 0.9071. 00 10. OOO1.00 1. OOO

RATIO0. 100. 100. 110. 110. 100. 090. 090. 090. IO0. 100. 100. 100.090.090. 100. IO0. 120. 120. 131. 080. 991. 031.010.981. CO0.090. 93

AMNT160.00160. CO160. CO16O. OO40.00

160. OO160. OO16O. CO160. OO16O. CO16O. OO40. CO

160. OO160. OO160.00160. OO160. OO160. CO160. OO160.0016O. CO160.0016O. CO16O. CO160. 00160.00160. 00

AMNT(L)160. CO160.00160. CO160. 0040.00

160.00160.00160.00160. 00160.00160. CO40. CO

160.00160.00160.00160.00160. CO160. CO160.00160. CO160. CO160. 00160.00160.0016O. OO160. CO160. CO

R. FAC F1. 0100.9211. 6031. 0701. 0001. 3380. 9060. 1891.2141.2691. 039l.OOO2. 4341.6390. 7341. 1991. 9491. 1471. 2491. 7791. 7660. 4661.0180. 1741. 0211. 2930. 480

». FAC(L)1. 0100. 9211. 6031. 0701. COO1. 3380.9060. 1891. 2141. 2691. 0391. OOO2. 4341. 6390. 7341. 1991. 9431. 1471.2491. 7791. 7660. 4661. 0180. 1741. 0211. 2930. 480

RATIO1. 001.001.001.001.00. OO.CO.00.00.00. 00

1.00l.OO1. 001. 001. CO1. OO1. 001. 001. 001. 001.001.001.001. 001. 001. OO

1.9756 87 SAMPLE D A T A PACKAGE 3 0 1

COMPUCHEM LABORATORIES. INC.GC/MS ANALYSIS LOG

RUN LOG

INITIAL TIME OF TUNE

TIME TUNE EXPIRES _

-. n SHIFT(S| (A)

.£ PREVENTIVE MAINTENANCE

.5.08 DATE ol/of/fO.(B).

ANALYSIS TYPE

UJtoct*octCL

•I

UJ-JCL

10IV00


Lab Name: COMPUCHEM LABS Contract: (2-88) -REVS

Lab Code: COMPU Case No.: 18756 SAS No.: SDG No. : OJ7

Instrument ID: 20

Min RRF for SPCC(#) - 0.050



LAB FILE ID: RRF20 = HJ891221A20 RRF50 = HH891221A20RRF80 - HL891221A20 RRF120= HK891221A20 RRF160- HI891221A20

COMPOUND

Phenol ^bis ( 2-Chloroethyl ) Ether2 -Chlorophenol1 , 3-Dichlorobenzene

RRF20

* 1.4041.3651.2041.450

1.4-Dichlorobenzene * 1.529Benzyl Alcohol1 . 2-Dichlorobenzene2 -Methy Iphenolbis ( 2-Chloroisopropy 1 ) Ether4 -Methy IphenolN-Nitroso-Di-n-Propylamine_'Hexachloroe thaneNitrobenzeneIsophorone

0.5941.3470.8610.9740.888

i 0.8560.7270.4940.784

2-Nitrophenol * 0.1972 . 4-DimethylphenolBenzoic Acidbis ( 2-Chloroethoxy ) Methane_2 . 4-Dichlorophenol <1,2, 4-TrichlorobenzeneNaphthalene4-Chloroaniline

0.4010.1250.400

» 0.2620.3131.0130.372

Hexachlorobutadiene * 0.2034 -chloro-3 -Methy Iphenol '2-Methylnaphthalene

* 0.2400.530

Hexachlorocyclopentadiene # 0.3212 , 4 , 6-Trichlorophenol * 0.3452 t 4 , 5-Trichlorophenol2 -Chloronaphthalene2-NitroanilineDimethyl PhthalateAcenaphthylene2 . 6-Dinitrotoluene3-Nitroaniline

0.3201.1790.3911.1091.5720.1960.185

Acenaphthene * 1.0612 . 4-Dinitrophenol4 -Nitrophenol

# 0.072f 0.161

RRF50

1.6521.4871.3911.6061.6040.7971.4741.0891.2201.1201.1290.8260.5960.9610.2370.4120.2030.4950.3390.3681.2710.3190.2060.4170.7250.3650.3490.3611.3690.4761.3991.6820.2960.2361.2990.1240.294

RRF80

1.5331.4001.3791.5411.-5950.7891.4301.0391.1021.1051.0360.8040.6520.9610.2400.5030.2240.5350.3290.3591.3930.5590.2260.4550.7010.4700.4050.4301.4430.5161.5282.0410.2980.2881.4140.1480.307

RRF120

1.6391.4821.5161.6291.7160.8951.4951.1791.2221.3681.1490.9220.5621.0200.2460.5170.2310.5650.3420.3951.3830.5840.2530.4410.7950.5890.5600.5531.8530.6511.7092.4210.3590.3211.7570.1750.342

RRF160

1.8591.5451.4811.7291.7630.8681.5771.2601.2681.2531.2320.9340.5871.0530.2610.5420.2100.5140.3490.4001.3560.4770.2290.3990.7500.6380.5390.5831.9950.6831.8482.5570.3650.3411.6550.1420.341

RRF

1.6171.4561.3941.5911.6410.7891.4651.0861.1571.1471.0800.8430.5780.9560.2360.4750.1990.5020.3240.3671.2830.4620.2230.3900.7000.4770.4400.4491.5680.5431.5192.0550.3030.2741.4370.1320.289

%RSD

10.4*5.08.76.55.8*14.95.814.010.315.713.3*10.29.910.910.1*13.521.412.511.0*9.512.424.99.1*22.3*14.528.8*23.5*25.821.922.518.821.222.523.319.4*29.0*25.8*






Instrument ID: 20

Min RRF for SPCC(#) » 0.050



LAB FILE ID: RRF20 = HJ891221A2Q RRF50 - HH891221A20RRF80 = HL891221A20 RRF120- HK891221A20 RRF160- HI891221A20

COMPOUND

Dibenzofuran2 , 4-DinitrotolueneDiethylphthalate4 -Chi oropheny 1 -pheny lether_Fluorene4-Nitroaniline4 , 6-Dinitro-2-Methylphenol_N-Nitrosodiphenylamine (!)_'4-Bromophenyl-phenyletherHexachlorobenzene

RRF20

1.2470.2621.1730.5031.1140.1300.069

* 0.5350.2130.276


0.9460.9281.328

Fluoranthene * 0.637PyreneButylbenzylphthalate3,3' -DichlorobenzidineBenz o ( a ) AnthraceneChrysenebis ( 2 -Ethy Ihexy 1 ) Phthalate_Di-n-Octyl Phthalate 'Benzo (b) FluorantheneBenzo (k) Fluoranthene

1.5100.8710.1891.0520.9231.209

« 2.0331.4010.894

Benzo (a) Pyrene * 0.973Indeno (1,2,3 -cd ) PyreneDibenzo (a . h) AnthraceneBenzo fa . h . i , Perylene

Nitrobenzene-d52-FluorobiphenylTerphenvl-dl4Phenol -d52-Fluorophenol2.4. 6-TribromoDhenol

0.9480.7930.780

0.4871.2191.0281.2311.2600.111

RRF50

1.5460.3681.4580.6181.4420.2150.1200.5760.2480.2730.1241.2641.1061.6490.9341.4430.8990.1601.0341.1841.7542.5991.4131.1541.0381.2401.0610.985

0.6221.2881.0261.4721.4560.125

RRF80

1.714'0.4271.6720.7381.4930.2530.1440.7120.2630.3040.1511.3571.4431.8181.1411.5940.8890.2161.1371.2581.8362.6201.5591.1391.1461.3721.1991.090

0.6121.4351.1641.3421.3740.148

RRF120

2.0570.4431.8710.9361.9430.3110.1310.7430.2630.3410.1471.5671.5532.1141.0721.8790.9490.1861.1381.4972.1133.2551.5931.2581.1801.4041.2771.134

0.6091.8461.2641.5691.4290.170

RRF160

2.0510.4411.9560.9291.9060.2360.1670.9190.3000.3890.1601.6391.6082.4281.2861.7610.9880.1921.1991.5092.1833.1901.7391.3241.3401.4271.2791.105

0.6452.1271.2781.6341.5450.147

RRF

1.7230.3881.6260.7451.5800.2290.1260.6970.2570.3170.1341.3551.3281.8671.0141.6370.9190.1891.1121.2741.8192.7391.5411.1541.1351.2781.1221.019

0.5951.5831.1521.4501.4130.140

%RSD

20.019.819.625.622.028.828.921.8*12.215.421.0*20.322.322.724.3*11.05.2

10.56.119.121.218.3*9.114.212.5*15.518.214.2

10.424 .610.611.37.5

16.3

(1) Cannot be separated from Diphenylamine


18756 87 SAMPLE DATA PPCKPGE ^ y o

r -•T-.

i-Sr*

COMPUCHEM LABSRIC COMPUCHEM DATA: HJ891221A26 SCANS 387 TO 165612/21/89 18:51:99 -r v OUT OF 307 TO 1658SAMPLEi 1 UL 38654-12364 28 NG/UL SEMI2 STD. (SSKD820)

693768.

IStl ISI2

SS92 SSI3

421

ISI3 SSI5

SS14 D3I1 ISt4

652

SSI6

SSI7

ISt5

ISI6

1863

4086:84

88812:87

1

LJL"-T*

1123

1

•

J J 1314 1?7 4 1683l

188815:89

i ' l '1288 148818:11 21:12

i168824:14

SCANTIME

UJcoct__•octCLctKaoUJ_jCLCctv\

r\-

•-ftLOl\.CO

QUANTI TATION REPORT FILE: HJ891221A20DATA: HJ891221A2O. TI12/21/89 18:51:00 TSAMPLE: 1 UL 30654-*2364 20 NG/UL SEMI2 STD. (SS*D020)CONDS. :SUBMITTED BY: 20 ANALYST: 873

AMOUNT-AREA * REF. AMNT/(REF. AREA)• RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHLOROBENZENE (IS»1)2 610 PHENOL (01*3) <108-9S-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-S7-8>5 421 1.3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1.4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-Sl-6>8 420 1,2-DICHLOROBENZENE (01*10) <95-50-l>9 620 2-METHYLPHENOL (01*11) <9S-48-7>10 412 BIS(2-CHLOROI8OPROPYL)ETHER (Ql«12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITR08O-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (Ql»15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (IS*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2.4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZOIC ACID (02*5) <65-85-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2.4-D1CHLOROPHENOL (02*7) <120-83-2>22 446 1,2,4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRE80L (02*12) <59-5O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 «495 D10-ACENAPHTHENE (IS*3)29 435 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4,6-TRICHLOROPHENOL (03*3) <88-O6-2>31 626 2,4,5-TRICHLOROPHENOL (03*4) <9S-95-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-58-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 .605 2. 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2,6-DINITROTOLUENE (03*15) <606-2O-2>43 424 DIETHYL PHTHALATE (Q3*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7005-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>


NO474849505152535455565758596061626364656667686970717273747576777879

rW123456789101112131415161718192021

NAME•467 D10-PHENANTHRENE (IS»4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <534-52-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLOROBENZENE (04*5) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <85-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>•459 D12-CHRYSENE (13*5)445 PYRENE (05*3) <129-00-0>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3, 3'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO (A) ANTHRACENE (05*6) <56-55-3>413 BI8(2-ETHYLHEXYL) PHTHALATE (05*7) <117-81-7>418 CHRYSENE (05*8) <218-01-9>*497 D12-PERYLENE (IS»6)429 DI-N-OCTYL PHTHALATE (06*2) <117-84-0>407 BENZO(B)FLUORANTHENE (06*3) <205-99-2>409 BENZO(K) FLUORANTHENE (06*4) <207-08-9>406 BENZO (A) PYRENE (06*5) <5O-32-8>437 INDENOd, 2,3-C, D)PYRENE (06*6) <1 93-39- 5>419 DIBENZO(A.H) ANTHRACENE (06*7) <53-70-3>408 BENZO(0, H. DPERYLENE (06*8) <191-24-2>*619 2-FLUOROPHENOL (8S*1)•612 D5-PHENOL (SS*2>*447 D5-NITROBENZENE (SS*3)*448 2-FLUOROBIPHENYL (SS*4)«628 2, 4, 6-TRIBROMOPHENOL (35*5)•496 D14-TERPHENYL (S8»6)*471 D10-PYRENE456 1. 2, 3. 4-TETRACHLOROBENZENE

M/tT15294931281461461081461084510870117771368213910712293162

-VAN421396401406418422433437445447457458464470530490498502509510518

nva-r6:236:006:046:096:206:246:346:376:446:466: 596: 567:027:078:027:257: 337:367: 437: 437: 51

tfk>-11

11515151515151515

1.0.0.0.0.1.1.1.1.1.1.1.1.0.1.0.0.0.0.0.0.

KKTOOO941952964993002029038057062086088102887OOO925940947960962977

METR' AKEATHWHTT AMOUNTAAAAAAAAAAAAAAAAAAA

BBBBBBBBBVVBBBBBBBVBBBBBBBBBBBBBBBBBBB

A*BBA BB

113660.79796.77560.68412.82428.86920.33732.76556.48956.55336.50464.48624.41328.73144.295900.116028.29188.59284.18500.59172.38692.

40.16.18.17.18.19.14.18.15.15.15.15.17.16.4O.16.16.19.12.16.15.

OOO NO997 NO359 NO304 NO062 NO071 NO886 NO275 NO824 NO966 NO860 NO154 NO616 NO581 NO000 NO322 NO674 NO447 NO320 NO150 NO421 NO

2. 751. 171. 261. 191. 241. 311. 021. 2509100904

1. 211. 142. 751. 121. 151. 340. 851. 111. 06

1S756 87 SAMPLE DATA PPCKPGE 2 9 5

NO2223242526272829303132333435363738394041424344454647484950515253545556575859606162636465666768697071727374757677

M/E180128127225107142164237196196162651631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522522522762782761129982172330244

SCAN52653153754858159268761362062363664766667368369069269970570667172973573673882074374677979380982282687693010609511010105610591063106312311123117611791222143514381496322395468627759964

TIME7:588:038:088: 188:488:5810:24

: 17:23:26:38: 48

10:0510: 1210:2110:2710:2910:3510. 4110:4210: 1011:0311:0811:0911: 1112:2511: 1511: 1811:4812:0112: 1512:2712:3113: 1614:0516:0314:2415: 1816:0016:0216:0616:0618:3917:0117:4917: 5118:3121:4421: 4722:404: 535: 597: 059:30

11: 3014: 36

REF151515151515282828282828282828282828282828282828284747474747474747474757575757575757646464646464646411

15282857

RRT0. 9921. 0021. 0131. 0341.0961. 1171.0000.8920. 9020.9070. 9260.9420. 9690. 9800. 9941. 0041. 0071. 0171. 0261. 0280. 9771. 0611. 0701. 0711. 0741. 0000. 9060. 9100. 9500. 9670.9871.0021.0071. 0681. 1341. 0000. 8970. 9930. 9960. 9991. 0031. 0031. 0000. 9120. 9990. 9980.9931. 1661. 1681. 2150. 7650. 9380. 8830. 9131. 1050. 909

METHA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BB

BBBBBBBBBVVB

A BBA BBA BBA BBA BBA BBA BVA BBA VBA BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA VBA BBA BBA BB

AREA(HGHT) AMOUNT %TOT46320.149828.S5O64.30020.35488.78436.119632.19188.20636.19124.70496.23396.66320.94O60.11072.63472.4288.9616.7462O.1 5664.11748.70172.30108.66648.778O.

121324.4200.32444.12912.16744.5496.57372.56268.80540.38628.60128.45396.26176.5684.31616.36340.27760.45O16.45764.31524.20116.21892.21340.17852.17564.71620.69932.71992.72936.6612.30892.

17.15.23.19.11.14.40.17.19.17.17.16.15.18.15.16.11.10.16.14.13.16.16.19.12.40.11.18.17.20.14.14.16.16.13.40.20.19.23.20.13.19.40.15.19.15.18.15.14.15.17.16.15.18.17.20.

013935333698512627000563754730220439852698693334980949140249281O88295453077OOO942583181188481962773103637000922365586348785601000648822491734286949840317724641935672032

NONGNGNGNGNONGNGNGNONGNGNGNGNGNONGNONONONGNGNGNONONGNGNGNONONONONONGNONONONONONGNONGNONGNGNGNGNGNGNONONONONGNONG

1. 171. 091. 601. 350. 791. 002. 751.211. 361. 221. 181. 131. 091. 281. 081. 120. 800. 751. 110. 980. 911. 101. 121. 060. 832. 750. 791. 281. 181. 390. 991. 031. 151. 110. 942. 751. 441. 331. 621. 400. 951. 072. 751. 071. 361. 061. 291. 051. 031. O91. 191. 151. 071. 301. 211. 38


NU7879

NO123456789101112131415161718192O212223242926272829303132333435363738394O414243444546474849505152

n/fc SCAN TIME REF RRT METH212 949 14: 22 57 0. 895 A BB216 636 9: 38 28 0. 926 A BB

RET(L) RATIO RRT(L)6:215: 586: 036: 076: 186:226:336:366:436:446: 53

. 00

. 01

. 01

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 006: 59 1. 007:00 17:058: OO7:247: 317: 347:437: 427: 507: 568:028.078: 168:468:5710:239: 169:22

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

.00

. 00

. 00

. 009:29 1.009: 36 19:46 !10:04 ]10:11 110:21 110:26 110:29 110:34 110:40 J10:41 110: 091 1 : 03 !11: 0711: 0711: 1112:2411: 1411:17 :11:4712:00 112: 14 ;

I. 00t. 00t. 00L. 00L 00L 001. 00I. 001. 00L 00L 00L 00L. 001. 00I. 001. 001. 00I. 00I. 001. 001. 00

10. 00010. 00010. OOO10. OOO10. 00010. 00010. OOO10. OOO10. OOO10. OOO10. 00010. 00010. 00010. OOO10. OOO10. OOO10. OOO10. OOO9O. OOO10. OOO10. OOO10. OOO10. OOO10.00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO50. OOO10. OOO90. OOO10. OOO10. 00050. OOO10. OOO50. OOO50. 00010. OOO10. 00010. OOO10. OOO10. OOO10. OOO90. OOO10. OOO50. 00010. OOO10. 00010. 00050. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090. 100. 090. 090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 10O. 100. 100. 110. 110. 110. 020. 100. 020. 090. 090. 100. 02

AMNT40.17.18.17.18.19.14.18.15.15.15.19.17.16.40.16.16.19.12.16.15.17.15.23.19.11.14.40.17.19.17.17.16.15.18.19.16.11.10.16.14.13.16.16.19.12.40.11.18.17.20.14.

00003630060789278297861962980032674932194201933370916300967973224489706933589514292809294908009458181948

AREA(HGHT) AMOUNT34236. 18. 89033964. 18. 361

AMNT(L)40. 0050. 0050. 0050.0090. 0090. 0090. 0090. 0090. 0090. 0050. 0090. OO90. 0090. 0040. 0050. 0050. 0050. 005O. 0050. 0050.0050. 0050. 0050. OO50. 0050. 0050.0040. 0050. 00SO. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050.0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0040. 0050. 0050. 0090. 0090. 0050. 00

NGNG

R. FAC R. FAC(L)1. 0000. 5620. 9460. 4820. 580O. 6120. 2370. 5390. 3450. 3890. 3550. 3420. 2910. 1981. 0000. 3140. 0790. 1600.090O. 1600. 1090. 1290. 4090. 1490. 0810. 0960.2121. 0000. 1280. 1380. 1280. 4710. 1960. 4430. 6290. 0740. 4240.0290. 0640. 4990. 1090.0790. 4690. 2010. 4460. 0921. 0000. 0280. 2140. 0890. 1100. 036

1.1.1.1.1.1.0.1.1.1.1.1.0.0.1.0.0.0.0.0.0.0.1.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.0.0.1.0.1.0.1.0.0.0.0.0.

0006524873916066O4797474089220120129826596OOO961237412203495339368271319206417725OOO365349361369476399682236299124294546368296458618442215000120576248273124

XTOT1. 301. 26

RATIO1. 000. 340. 370. 350. 360. 380. 300. 370. 320. 320. 320. 300. 350. 331. OO0. 330. 330. 390. 250. 320. 310. 340. 320. 470. 390. 230. 291. 000. 350. 400. 350. 340. 330. 320. 370. 310. 330. 230. 220. 320. 280. 270. 320. 330. 310. 241. 000. 230. 370. 340. 400. 29


NO535455565758596061626364656667686970717273747576777879

RET(L) RATIO RRT(L)12: 2612:3013: IS14: 0916:0414:2419: IB16:0116:0216: 0616: 0618:3917:0117: 9017: 5118:3121:4921:4722: 414: 515:577:049:2911:2914: 36

. 00

. 00

. 00

. OO

. 00

. 00

. 00

. 00

. 00

. 00

. OO

. 00

. 00

. 00

. 00

. 00

. OO

.00

. OO

. 01

. 01

. 00

. 00

. 00

. OO14:22 l.OO9:37 1.00

10. 00010. OOO10. 00010. OOO10. 00010. 00010. 00020. 00010. 00010. OOO1 0. 00010. 00010. OOO10. 00010. OOO10. 00010. 00010.00010. OOO0. 7420. 9480. 8750. 9O61. 1180. 90710. 0001. OOO

RATIO0. 100. IO0. 110. 110. 100. 090. 100. 050. 100. 100. IO0. 100. 090. 100. 100. 100. 120. 120. 121. 030. 991. 011. 010. 991. OO0. 090. 93

AMNT14.16.16.13.40.20.19.23.20.13.15.40.15.19.15.18.15.14.15.17.16.15.18.17.2O.18.18.

967710640092375935796000658249732995843272649367038936

AMNT(L)50.SO.SO.SO.4O.50.50.50.50.SO.SO.40.50.SO.SO.50.50.50.50.SO.50.50.SO.50.SO.SO.SO.

000000000000000000000000000000OO000000000000OO00000000

R. FAC R. FAC(L)0. 3780. 3710. 5310. 25S1. 0000. 6040. 3480. 0760. 4210. 4840. 3691. 0000. 8130. 5600. 3S70. 3890. 3790. 3170. 3120. 5040. 4920. 1950. 4880. 0440. 4110. 4560. 227

1.2641. 1061. 6490. 9341. OOO1. 4430. 8990. 1601. 0341. 7541. 1841. 0002. 5991. 4131. 1341. 0381. 2401. 0610. 9851. 4561. 4720. 6221. 2880. 1251. 0261. 2060. 618

RATIO0. 300. 34C. 320. 271. 000. 420. 390. 470. 410. 280. 311. 000. 310. 400. 310. 370. 310. 300. 320. 350. 330. 310. 380. 350. 400. 380. 37


a,

RIC12/21/89 17i35:88

COMPUCHEM LABSCOMPUCHEM DATA: HH891221A28 SCANS 305 TO 1688

OUT OF 305 TO 1680SAMPLE: 1 UL 38655-12365 50 NG/UL SEMI2 STD. (SSTD858)CONDS.i 1828158.

ISfl ISI2 ISI3 SSt5 SSt6 ISf5

SS*2 SSf3 SSM 0311 '. ISt4 SSf7

1063

1516

428

8751818

1188815:89

1123

11801223

i1282 1348

1438| 1498

JLL120018:11

—I148821:12

—I160824:14

SCANTIME

UJCOctiioctCL

CtO

UJ-Ja.E•I'/l

fv

Q

••ftinr\-co

QUANTITATION REPORT FILE: HH891221A20DATA: HH891221A20. TI12/21/89 17:35:00SAMPLE: 1 UL 30655-*2365 5O NO/UL SEMI2 STD. (S8TD05O)COND8.:SUBMITTED BY: 20 ANALYST: 875

AMOUNT-AREA » REF. AMNT/(REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1. 4-DICHLOROBENZENE (IS»1)2 610 PHENOL (01*3) <108-9S-2->3 411 BIS(2-CHLOROETHYL)ETHER (Ql»5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-B>5 421 1.3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1.4-DICHLOROBENZENE (Ql«8) <106-46-7>7 474 BENZYL ALCOHOL (Ql*9) <lOO-51-6>B 420 1,2-DICHLOROBENZENE (01*10) <95-50-l>9 620 2-METHYLPHENOL (01*11) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-N1TROPHENOL (02*3) <88-75-5>18 603 2, 4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZOIC ACID (02*5) <65-85-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2.4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1,2, 4-TRICHLOROBENZENE (02*8) <12O-82-l>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <B7-68-3>26 608 P-CHLORO-M-CRESOL (02*12) <59-5O-T>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 *495 D10-ACENAPHTHENE (18*3)29 435 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4, 6-TRICHLOROPHENOL (03*3) <88-O6-2>31 626 2,4, 5-TRICHLOROPHENOL (03*4) <95-95-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-58-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 4605 2, 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <1OO-02-T>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2, 4-DINITROTOLUENE (03*14) <121-14-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <B4-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7O05-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <10O-01-6>


NO474849505152535455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME•467 D10-PHENANTHRENE (IS*4)604 4, 6-D1NITRO-2-METHYLPHENOL (04*2) <534-52-l>443 N-NITROSOD1PHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-59-3>433 HEXACHLOROBENZENE (Q4*3) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <8S-01-B>403 ANTHRACENE (04*8) <12O-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*459 D12-CHRYSENE (IS*5)445 PYRENE (05*3) <129-00-0>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3, 3'-DICHLOROBENZIDINE (Q3*S) <91-94-l>405 BENZO( A) ANTHRACENE (05*6) <56-55-3>413 BI8(2-ETHYLHEXYL) PHTHALATE (05*7) <117-81-7>418 CHRYSENE (05*8) <218-01-9>•497 D12-PER YLENE (IS*6)429 DI-N-OCTYL PHTHALATE (O6*2) <117-84-0>407 BENZO(B) FLUORANTHENE (06*3) <205-99-2>409 BENZO (K)FLUORANTHENE (06*4) <2O7-08-9>406 BENZO(A)PYRENE (06*5) <5O-32-8>437 INDENO (1. 2. 3-C.D) PYRENE (06*6) <1 93-39- 5>419 DIBENZO( A. H) ANTHRACENE (06*7) <53-70-3>408 BENZO(G, H, DPERYLENE (06*8) <191-24-2>*619 2-FLUOROPHENOL (88*1)*612 D5-PHENOL (38*2)»447 D9-NITROBENZENE (SS»3)*448 2-FLUOROB I PHENYL (88*4)•628 2. 4, 6-TRIBROMOPHENOL (38*9)»496 D14-TERPHENYL (38*6)*471 D10-PYRENE456 1.2, 3. 4-TETRACHLOROBENZENE

M/E15294931281461461081461084510870117771368213910712293162

SCAN419394399404416420432436443445455457462468528489496500510508517

TIME6:215:586:036:076. 186:22:33.36:43:44:S3: 537:007:058:007:247: 317:347:437: 427: 50

REF1111111111111

1515151515151515

1.0.0.0.0.1.1.1.1.1.1.1.1.0.1.0.0.0.0.0.0.

RRTOOO940952964993002031041057062086091103886000926939947966962979

METHAAAAAA

AAAAAAAA

BBBVBBBBBVVBBVBBVBBBBBBBBBVBBBBBBBBBWBBBB

AREA(HOHT) AMOUNT154692.319480.287488.269040.310352.310156.194204.285076.210536.235848.216524.218344.159648.309168.414760.498204.122684.213652.105240.256788.175840.

40.42.38.46.51.48.41.49.42.20.42.36.51.51.40.47.50.54.42.40.52.

000 NO622 NG620 NO886 NO386 NO686 NG761 NG813 NO673 NG468 NG244 NO751 NO227 NO343 NO000 NO966 NG333 NO190 NO133 NG966 NO107 NO

XTOT1. 081. 151.04263831123415

1.1.1.1.1.1.0. 551. 140. 991. 381. 381. 081. 2935461310

1. 40


NO2223242326272829303132333433363738394041424344434647484950515253545556575859606162636465666768697071727374757677

M/E180128127225107142164237196196162631631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522522522762782761129982172330244

SCAN5245305365465795916866126186226346456656726836896926987O470567072973473473881974274377879280882182387393010619511010105710591063106312311123117711791223143614381498320393467626758964

TIME7: 568:028:078: 168:46B: 5710:239: 169:229:259:369:4610:0410: 1110:2110:2610:2910: 3410:4010:4110:0911:0311: 0711:0711: 1112:2411: 1411: 1711:4712:0012: 1412:2612:3013: 1514:0516:0414:2415: 1816:0116:0216:0616:0618:3917:0117: 5017: 5118:3121:4521:4722: 414: 515: 577: 049: 2911:2914: 36

REF151515IS1515282828282828282828282828282828282828284747474747474747474757575757575757646464646464646411

15282857

RRT0.9921. 0041. 0151. 0341.0971. 1191. 0000.8920. 9010.9070. 9240. 9400. 9690. 98O0. 9961. 004. 009. 017. 026. 028

0. 977. 063. 070.070.076. OOO

0. 9060. 9100. 95O0. 9670. 9871. 0021. 0071. 0681. 1361. 0000. 8960. 9520. 9960. 9981.0021. 0021.0000.9120.9560. 9980. 9941. 1671. 1681. 2170. 7640. 9380. 8840. 9131. 1090. 909

METHA BB

BVBBBBBVBBBB

A BBA BVA VBA BBA BBA BBA BBA BVA BBA BBA BVA BBA BBA BBA BVA BBA BBA BBA BBA BBA BBA BBA BBA BBA BVA VBA BBA BVA BBA BVA BBA BBA BVA BVA VBA BBA BVA BVA WA BVA BBA BVA BBA BBA BVA VBA BBA BBA BV

AREA(HOHT190812.658980.165396.106808.216052.375824.208724.95308.91132.94096.357120.124156.364972.438836.61548.338992.32304.76612.403316.95900.77168.380512.161186.376240.36196.223216.33476.160612.69136.76300.3466O.332732.308604.460O88.260568.160284.289204.180164.32120.207092.351356.237168.113728.369438.200896.164036.147616.176344.1 50848.140072.281448.284548.322584.336032.32640.205540.

) AMC54.34.46.56.49.50.40.51.42.41.53.44.47.47.37.S3.33.86.47.41.46.30.33.36.33.40.39.30.33.32.44.31.49.47.32.40.45.49.42.45.64.65.40.46.29.24.50.46.46.45.50.42.53.48.40.52.

NJNT793092551680329791000995357527407899394112718480836922843Bll234987237969371OOO21197384689796166955410077900043459S872731632094OOO103497085300187397OSS797891336850248188

NGNONGNGNGNGNONONGNGNGNONGNONGNONONONCNGNGNGNCNONONGNONGNONONGNGNONONGNGNONONONONGNGNONONGNGNGNONONONONONONONONO

XTOT1. 471. 451. 251. 521. 331. 371. 081. 401. 141. 121. 441. 211. 271. 271. 011. 490. 912. 341. 291. 121. 241. 371. 431. 530. 951. 081. 051. 371. 451. 421. 211. 391. 331. 271. 421. 081. 221. 331. 151. 231. 741. 751. 081. 240. 790. 651. 351. 241. 251. 211. 371. 151. 431. 311. 081. 40


NU7879

NO123456789101112131415161718192O2122232425262728293031323334353637383940414243444546474849503132

n/6 SCAN TIME REF RRT METH212 949 14: 22 57 0. 894 A BB216 635 9: 37 28 0. 926 A BB

RET(L)6:215: 116: 146: 186:296:226: 436:476: 536: 557:056: 557: 127: 178:007:357:317:457:557:537: 508:088: 138: 188: 168:469:0910:239: 169:259:369: 489: 5810: 1510:2310:3210:2610:2910:3410: 5110: 5310:2111: 1311: 1911: 2O11:2212:2411:2611: 171 1 . 5812: 1112: 14

RATIO RRT(L)1.001. 150.970.970.971.000.970. 970. 980. 970.971. 000.970. 971.000. 981.000.980. 980. 981. 000. 980.980. 981.001.000.981.001.000.990. 980.980. 980.980. 980. 981. 001. 001. 000. 980. 980. 980. 980. 980. 980. 981. 000. 981.000. 980. 981. 00

10.00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10.00010. OOO10.00010. OOO10. OOO10. 00010. 00010. 00010. OOO10. 00010. OOOSO. OOO10. OOO10. OOO10. OOO10. 00010.00010. OOO10. 00010. OOO10. OOO10.00010. 00050. OOO10. OOO50.00010. OOO10. 00050. 00010. OOO50. OOO50. 00010. OOO10. 00010. OOO10. OOO10. OOO10. OOO50.00010. 00050. OOO10. OOO10. OOO10. 00050. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090. 100. 090. 090.090. 020. 100. 100. IO0. 10O. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090. 090. 100. 02

AMNT4O.42.38.46.51.48.41.49.42.20.42.36.51.51.40.47.50.54.42.4O.52.54.54.46.56.49.50.4O.52.42.41.53.44.47.47.37.5S.33.86.47.41.46.50.S3.56.35.40.39.50.53.52.44.

OO626289396976816747247523340097331913971179095568337900003653419039117248849284812399249737002197859096

AREA(HCHT) AMOUNT241568. 52. 889 NG161364. 55. 567 NG

AMNT(L)40.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.SO.50.50.50.50.50.50.SO.50.50.40.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.50.30.50.

0000000000000000000000000000000000000000000000000000000000000000000000000000000000000000OO00000000000000

R. FAC R. FAC(L>1. OOO1.6321. 4871. 3911. 6O61. 6O40. 7971. 4741.0891. 22O1. 1201. 1290.826O. 5961. OOO0. 9610. 2370. 412O. 2O30. 4950. 3390. 3681. 2710.3190.2060. 4170. 7251. OOO0. 3650. 3490. 3611. 3690. 4761. 3991. 6820. 2361. 2990. 1240.2941. 5460.3680. 2961. 4580. 6181. 4420. 2151. OOO0. 12OO. 5760. 248O. 273O. 124

1. OOO1. 9381. 9251. 4841. 5631. 6470. 9531. 4801. 2762. 9801. 3231. 5360. 8O60. 5811. OOO1.OO20. 2350. 38O0. 2410. 6050. 3250. 3361. 1750. 3430. 1820. 4220. 7141. OOO0.3510. 4120. 4341. 2810. S3O1. 4761.7850. 3131. 1710. 1830. 1691. 6160. 44O0. 3201. 4300. 5801.2660. 3041. 0000. 1530. 3650. 23O0. 2580. 138

XTOT1. 421. 49

RATIO1. 000. 850. 770. 941. O30. 970. 841. OO0. 850. 410. 840. 741. 021. 031. 00O. 961. 011. 080.840. 821. 041. 101. 080. 931. 130. 991. 021. 001. 040. 850.831. 070. 900. 930. 940. 751. 110. 681. 740. 960. 840. 921. 021. 061. 140. 711. 000. 781. O21. 081. O60. 90


NO535455565758596061626364656667686970717273747576777879

RET(L)12: 3812:4213:2514:0516:0414:3615:2816: 1016: 1416: 1516: 1618:3917:0118:0918:0918:3122: 1522: 1823: 165:016:087: 158:4111:4014: 4714:359:49

RATIO RRT(L)0. 980. 980. 991. 001. 000.990. 990.990. 990. 990. 991. 001. 000. 980. 981.000.980. 980. 970.970. 970.971. 090. 980.990. 990. 98

10.00010. OOO10.00010. 00010. 00010. 00010. 00020. OOO10. OOO10. 00010. OOO10. 00010. 00010. 00010. OOO10. OOO10. 00010. 00010. 0000. 7420. 9480.8750. 9061. 1180.90710. 0001. 000

RATIO0. 100. 100. 110. 110. 100. 090. 100. 050. 100. 100. 100. 100. 090. 100. 100. 100. 120. 120. 121.030. 991.011. 010. 991. OO0. 090. 93

AMNT51.49.47.52.40.45.49.42.45.64.65.40.46.29.24.30.46.46.43.30.42.S3.48.40.52.52.5S.

67351078OO436O8773630900103008301940038089348323198957

AMNT(L)SO.30.50.50.40.50.50.50.50.50.SO.40.50.50.50.50.50.SO.SO.50.50.50.50.50.50.50.50.

OO0000OO0000000000OO00000000OOOO00OO000000OO00OO000000

R. FAC R. FAC(L)1. 2641. 1O61. 6490. 934l.OOO1. 4430.899O. 1601.0341.7541. 1841. OOO2. 5991. 4131. 1541. 0381.2401. 0610.9851. 4561.472O. 6221.288O. 1251.0261. 2060. 618

1.2231. 1161. 75O0.8831. OOO1. 5890. 9070. 1871. 1301. 3570. 9091. OOO2. 8182. 3952. 3951. 0321. 3431. 1441. 0931. 4331. 7150. 5831. 3180. 1550.9831. 1400. 557

RATIO1. 030.990. 941. O61. 000. 910. 990. 860. 911. 291. 301. 00O. 920. 590. 481. Ol0. 920. 930. 901. 020. 861. O70. 980. 801. 041. 061. 11


10'JO

COMPUCHEM LABSRIC12/21/89 19:54:88

COMPUCHEM DATA: HL891221A28 SCANS 382 TO 1608OUT OF 382 TO 1600

SAMPLE: 1 UL 30656-12366 80 HC/UL SEMI2 STD. (SSTD080)CONDS.i 3097590.

IS«1 ISI2

SS12 SSI3

ISI3 SSI5

SSI4 D3I1 . ISM

SSI6 ISIS

SSI7 ' IStG

RIC

391. 1058

74 1341

1434

A4006:04

I148821:12

160024:14

SCANTIME

UJtoct:_-octCL

•Ic.

UJ_jCL£•1i/i

r-»•S)

•oinr->co

DATA: HL891221A2O. Tl12/21/89 19:54:OOSAMPLE: 1 UL 306S6-*2366 80 NG/UL SEMI2 STD. (S8TDO8O)CONDS. :SUBMITTED BY: 20 ANALYST: 873


NO NAME1 *494 D4-1,4-DICHLOROBENZENE (IS»1)2 610 PHENOL (01*3) <108-95-2>3 411 B13(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 6O1 2-CHLOROPHENOL (01*6) <95-57-8>5 421 1,3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1,4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <10O-Sl-6>8 420 1,2-DICHLOROBENZENE (01*10) <95-50-l>9 620 2-METHYLPHENOL (01*11) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <l06-44-5>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (IS*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2, 4-DIMETHYLPHENOL (02*4) <105-67-9->19 625 BENZO1C ACID (02*5) <65-85-O>20 410 BIS(2-CHLOROETHOXY)METHANE (O2*6) <111-91-1>21 602 2i 4-DICHLOROPHENOL (02*7) <12O-83-2>22 446 1,2. 4-TRICHLOROBENZENE (Q2*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-2O-3>24 475 4-CHLOROANILINE (02*10) O06-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRE3OL (02*12) <39-3O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 »495 D10-ACENAPHTHENE (18*3)29 435 HEXACHLOROCYCLOPENTADIENE (O3*2) <77-47-4>30 611 2,4, 6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 5-TRICHLOROPHENOL (03*4) <95-95-4.>32 416 2-CHLORONAPHTHALENE (Q3*3) <91-38-7>33 478 2-NITRQANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <2O8-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 -60S 2. 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2. 4-DINITROTOLUENE (03*14) <121-14-2>42 428 2i 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7005-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>


NO474849505152533455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME*467 D10-PHENANTHRENE (IS«4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <534-52-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-3O-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLOROBENZENE (Q4*S) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <83-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <84-74-2>431 FLUORANTHENE (04*10) <206-44-0>*459 D12-CHRYSENE (IS«5)445 PYRENE (05*3) <129-OO-O>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3, 3'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO < A) ANTHRACENE (05*6) <56-SS-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (05*7) <117-81-7>418 CHRYSENE (05*8) <21B-01-9>»497 D12-PERYLENE (IS*6)429 DI-N-OCTYL PHTHALATE (06*2) <117-B4-0>407 BENZO(B)FLUORANTHENE (06*3) <2OS-99-2>409 BENZO<K)FLUORANTHENE (06*4) <207-08-9>406 BENZO(A)PYRENE (06*3) <30-32-8>437 INDENOd. 2,3-C. D)PYRENE (06*6) <193-39-5>419 DIBENZO(A, H) ANTHRACENE (06*7) <53-70-3>408 BENZO < 0, H, I) PER YLENE (06*8) <191-24-2>*619 2-FLUOROPHENOL (SS*1)«612 D5-PHENOL (33*2)#447 D5-NITROBENZENE (33*3)*448 2-FLUOROB I PHENYL (SS*4)*628 2. 4, 6-TRIBROMOPHENOL (SS«5)•496 D14-TERPHENYL (33*6)*471 D10-PYRENE456 1 . 2, 3, 4-TETRACHLOROBENZENE

M/E15294931281461461081461084510870117771368213910712293162

SCAN415391396401412417428432439442452453459465524485492497507505513

TIME6:5:6:6:6:6:6:6:6:6:6:6:6:7:7:7:7:7:7:7:7:

175500041419293339425152570356212732413946

REF1111111111111

1515151515151515

1.0.0.0.0.1.1.1.1.1.1.1.1.0.1.0.0.0.0.0.0.

RRT000942954966993005031041058065089092106887000926939948968964979

METHA BBA BBA*BBA BBA BVA VBA BBA BBA BBA BBA BBA BBA BBA BBA BBA BVA BBA BBA VVA«BBA BB

AREA ( HGHT ) AMOUNT109596.335992.306824.302276.337784.349652.173036.313404.227788.241496.242268.227180.176204.378104.290176.557976.139148.291840.130251.310268.191052.

40.74.75.79.76.79.79.77.76.72.78.73.77.87.40.80.81.97.88.86.77.

OOO NG221 NG320 NG292 NO762 NG561 NG192 NG587 NO357 NG264 NO965 NG430 NO892 NG402 NO000 NG041 NO058 NO621 NO451 NG351 NG650 NG

XTOT0. 611. 121. 141. 201. 161. 201. 201. 171. 161. 0919111832

0. 611. 211. 231. 481. 341. 311. 17


NO22232425262728293031323334353637383940414243444546474849SO515253545556575859606162636465666768697071727374757677

M/EISO128127225107142164237196196162651631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522522522762782761129982172330244

SCAN52152653254357558768260861561863064166066867868568869469970166672473073073481473B741773787803816821870925105594610051051105410S7105712261117117111741218143114351493317390463621753959

TIME7: 537: 588:038: 138:438:5310:209: 139: 199:229:339:4310:0010: 0710: 1610:2310:2510:3110:3510:3710:0510: 581 1 : 0311:0311:0712:2011: 1111: 1311:4211:5512: 1012:2212:2613: 1114:0115: 5914:2015: 1315:5515: 5816:0116:0118:3416: 5517:4417:4718:2721:4021:4422: 374:485: 547: 019:24

11: 2414. 32

REF151515151515282828282828282828282828282828282828284747474747474747474757575757575757646464646464646411

15282857

RRT0. 9941.0041. 0151. 0361.0971. 1201. OOO0. 8910. 9020. 9O60. 9240. 9400. 9680. 9790. 9941.0041.0091.0181.0251.0280.9771. 0621.0701.0701. 0761.0000.9070. 9100.9300.9670. 9861.0021.0091. 0691. 1361.0000.8970.9330. 9960. 9991.0021.0021.0000.9110. 9330. 9580.9931. 1671. 1701. 2180. 7640. 9400. 8840. 9111. 1040. 909

METHA BBA BVA BBA BBA BB

BBBBBBBVVBBB

A BBA BBA BBA BVA BBA BBA BVA BBA BBA BBA BVA BB

BBBVBBBBBBBBBBBBBVVBBV

A BVA BBA BVA BBA BBA BVA BVA VVA BBA BVA BVA VBA BVA BVA BBA BBA BBA BVA BBA*BBA BBA BB

AREA(HGHT) AMOUNT208456.808636.324644.131368.263860.406704.136800.128728.110704.117776.394800.141072.418068.558452.78756.386752.4O5O4.83864.468892.116788.81596.457460.201788.408376.69096.149516.43076.212852.78512.90792.43132.403880.431592.543632.341196.110672.352916.196704.47756.251748.406296.278480.81168.425323.253044.184636.186048.222684.194632.176963.301072.294164.35S364.392604.40608.257620.

78.87.140.87.87.77.40.103.92.95.84.86.87.97.97.87.95.83.88.92.80.91.95.82.93.4O.96.98.84.88.97.85.104.88.97.40.88.79.107.88.83.85.4O.80.88.78.88.88.9O.88.75.72.78.89.94.90.

0756972779O1281339000039672486337682386082617036633309692904663715503804800OOO053925769824199894395201744OOO367062665029737028000655243941297467391508495959729132912763

NONGNONONGNGNONGNONONGNGNGNGNCNONONGNONGNGNGNGNGNONONGNONGNGNONGNGNGNONONGNONONGNGNGNONONGNONGNGNONGNONONONGNONO

7.TOT1. 181. 332. 121.331. 321. 170. 611. 561. 401. 441. 281. 311. 321. 471. 481. 321. 451. 261. 341. 411. 221. 391. 441. 251. 420. 611. 451. 501. 281. 341. 471. 301. 581. 331. 480. 611. 341. 201. 631. 331. 271. 290. 611. 221. 331. 191. 341. 341. 371. 341. 141. 101. 191. 351. 441. 37


NO7879

NO12345678910111213141516171819202122232425262728293031323334353637383940414243444546474849505132

M/E SCAN212216

RET(L>6:215: 586:036:076: 186:226:336:366:436: 446: 536: 557.007:038:OO7:247:317:347:437:427:307: 368:028:078: 168:468:3710:239: 169:229:239:369:4610:0410: 1110:2110:2610: 2910:3410: 4O10: 4110:0911:0311: 0711:0711: 1112:2411: 1411: 1711: 4712: 0012: 14

TIME REF RRT944 14: 18 37 0. 895631

RATIO0. 990. 990.990.990. 990.990. 990.990. 990.990. 990.990.990.990. 990.990.990.990. 990.990.990. 990.990. 990. 990.990.990. 990.991.000.990. 990.990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990. 990.990. 990. 990. 990.990. 990. 99

9: 33 28 0. 925

RRT(L)10. 00010. 00010. OOO10.00010. 00010. OOO10. OOO10. 00010. OOO10. OOO10. OOO10.00010.00010. OOO10. OOO10. OOO10. OOO10. OOO50. 00010. OOO10.00010.00010. OOO10.00010.00010. OOO10. 00010. OOO10. 00010. OOO50. OOO10. OOO50. OOO10. OOO10. 00050. OOO10. 00050. 00050. 00010. OOO10. OOO10. OOO10. 00010. 00010. OOO50. OOO10. OOO50. OOO10. OOO10. OOO10. OOO50. OOO

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110- 110. 110. 110. 110. 090. 100. 090.090. 090.020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 100. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090. 090. 100. 02

METHA BBA BB

AMNT40. 0074.2275.3279.2976. 7679. 3679. 1977. 5976. 3672.2678.9673. 4377.8987.4040.0080.0481.0697. 6288. 4586.3577.6578.0887. 70140.2887.9087.2877.344O. 00103.0492. 6795. 4984. 3486. 6887. 3997. 0897. 6287.0495. 6583. 5188. 6992.9080. 6791.7295. 5082. 8093. 8040. 0096. 0598. 9384. 7788. 8297. 20

AREA(HCHT) AMOUNT289488.189904.

AMNT(L)40.80.80.8O.80.80.80.80.80.80.80.8O.SO.80.40.80.80.8O.80.80.8O.80.80.80.80.80.80.4O.80.80.80.80.80.80.80.80.80.80.80.80.80.80.80.80.80.80.40.80.80.80.80.80.

00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

86.89.

R. FAC1. OOO1. 5331.4001. 3791. 5411. 5950.7891. 4301. 0391. 1021. 1O51.0360. 8O40. 6521. OOO0. 961O. 24OO. SO30.2240. 5350.329O- 3591.393O. 559O. 2260. 4550. 7011. OOO0. 4700. 4O50. 43O1. 4430. 5161. 5282. 0410. 2881. 4140. 1480. 3O71. 7140. 4270. 2981. 6720. 7381. 4930. 2531. OOO0. 1440. 7120. 2630. 3O40. 151

779781

NONO

R. FAC(L)1.1.1.1.1.1.0.1.1.1.1.1.0.0.1.0.0.0.0.0.0.0.1.0.0.0.0.1.0.0.0.1.0.1.1.0.1.0.0.1.o.0.1.0.1.0.1.0.0.0.0.0.

OOO65248739160660479747408922012O129826596OOO961237412203495339368271319206417725000365349361369476399682236299124294546368296458618442215000120576248273124

XTOT1. 311. 36

RATIO1. 000. 930. 940. 990. 96O. 990. 990. 970. 950. 900. 990. 920. 971. 091. OO1. 001. 011. 221. 111. 08O. 970. 981. 101. 751. 101. 090. 971. 001. 291. 161. 191. 051. 081. 091. 211. 221. 091. 201. 041. 111. 161. 011. 151. 191. 041. 171. 001. 201. 241. 061. 111. 21


NO535455565758596061626364656667686970717273747576777879

RET(L)12:2612:3013: 1514:0516:0414:2415: 1816:0116:0216:0616:0618:3917:0117: 5017: 5118:3121:4321:4722:414: 313:577:049:2911:2914:3614:229:37

RATIO RRT(L)0.991. OO0.990.990. 990.991.000.991.000.990. 991. 000. 990. 991. 001.00l.OO1.001.000. 990.990.990.990.990.990.990.99

10. 00010.00010. OOO10. 00010.00010. 00010.00020. OOO10. OOO10. 00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10.00010. OOO10. OOO0. 7420.9480. 8730.9061. 1180.90710.0001.000

RATIO0. 100. 100. 110. 110. 100. 090. 100. 030. 100. IO0. 100. 100. 090. 100. 100. 100. 120. 120. 121. 030.991. 011.000. 99l.OO0. O90.93

AMNT85.1O4.88.97.40.88.79.107.88.83.85.40.80.88.78.88.88.9O.88.75.72.78.89.94.9O.86.89.

893920740037066603740300652494304739514996731391767878

AMNT(L)80.8O.80.80.40.80.80.80.80.80.80.40.80.80.80.80.80.BO.BO.80.80.80.80.80.80.80.80.

OOOOOO00OOOO00OOOOOOOOOOOO0000OOOOOOOO00OOOOOO00OOOO00

R. FAC R. FAC(L)1.3571. 4431. 8181. 1411. OOO1. 5940. 8890. 2161. 1371.8361. 2581. 0002. 6201. 5591. 1391. 1461.3721. 1991. 09O1. 3741.3420. 6121. 4350. 1481. 1641. 3080. 694

1. 2641. 1O61. 6490. 9341. OOO1. 4430. 8990. 16O1. 0341. 7541. 1841. OOO2. 5991. 4131. 1541. 0381. 24O1.0610. 9831. 4361. 4720. 6221. 2880. 1231. 0261.2060. 618

RATIO1. 071. 301. 101. 221. 001. 100. 991. 331. 101. O31. O61. OO1. 011. 100. 991. IO1. 111. 131. 110. 940. 910. 981. 111. 191. 131. 081. 12


RIC12/21/89 19:21:00

COMPUCHEM LABS

SAMPLE: 1 UL 30657-12367 120 NG/UL SEMI2 STD. (SSTD120)CONDS.:

COMPUCHEM DATA: HK891221A28 SCANS 389 TO 1650OUT OF 389 TO 1658

5253118.

ISI1 ISI2 ISI3 SSt5 SSI6 I SI 5

SSt2 SS*3 SSI4 D3tl ISM SSI7 ISt6

•7.r.•M

UJ<0Ct

738

RIC398

4886:84

1 878825

1965

953

1125

1183

1226

i1443

1338 1577

108815:89

128818:11

140821:12

168824:14

SCANTIME

ctQ.ctKCt

UJ-JCLEct'/i

LOr..co

dUANTITATION REPORT FILE: HK891221A20DATA: HK891221A20. TI12/21/89 19:21:OOSAMPLE: 1 UL 30657-W2367 120 NG/UL SEMI2 STD. (SSTD120)CONDS. :SUBMITTED BY: 20 ANALYST: 875

AMOUNT-AREA * REF. AMNT/(REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1,4-DICHLOROBENZENE (IS*1)2 610 PHENOL (01*3) <10B-95-2>3 411 B18(2-CHLOROETHYL)ETHER (Ql*5) Oll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-B>5 421 1.3-DICHLOROBENZENE (01*7) <541-73-l>6 422 1.4-DICHLOROBENZENE (01*8) <lO6-46-7>7 474 BENZYL ALCOHOL (Ql*9) <!OO-31-6>8 420 1,2-DICHLOROBENZENE (01*1O) <93-50-l>9 620 2-METHYLPHENOL (Ql*ll) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITROBO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 44O NITROBENZENE (01*16) <98-95-3>15 *460 D8-NAPHTHALENE (13*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2, 4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZO1C ACID (02*5) <65-8S-O>20 410 B18(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-B3-2>22 446 1.2,4-TRICHLOROBENZENE (02*8) <12O-82-l>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-B>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (O2*12) <59-SO-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-57-6>28 »495 D10-ACENAPHTHENE (13*3)29 433 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2, 4,6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2,4,5-TRICHLOROPHENOL (03*4) <95-9S-4>32 416 2-CHLORONAPHTHALENE (03*5) <91-5B-7>33 478 2-NITROANILINE (Q3*6) <8B-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-B>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 t605 2, 4-DINITROPHENOL (03*11) <51-28-5>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2, 4-DINITROTOLUENE (03*14) <121-14-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7005-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>


NO474849505152535455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME*467 D10-PHENANTHRENE (IS*4)604 4, 6-DINITRO-2-METHYLPHENOL (04*2) <534-52-l>443 N-NITROSODIPHENYLAM1NE (04*3) <86-3O-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>433 HEXACHLOROBENZENE (04*5) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-5>444 PHENANTHRENE (04*7) <85-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (04*9) <B4-74-2>431 FLUORANTHENE (04*10) <206-44-0>»459 D12-CHRYSENE (IS*5>445 PYRENE (05*3) <129-00-0>415 BUTYLBENZYL PHTHALATE (05*4) <85-68-7>423 3, 3'-DICHLOROBENZIDINE (05*5) <91-94-l>405 BENZO ( A) ANTHRACENE (05*6) <56-53-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (03*7) <117-81-7>418 CHRYSENE (03*8) <218-01-9>»497 D12-PERYLENE (13*6)429 DI-N-OCTYL PHTHALATE (06*2) <117-B4-0>407 BENZO (B)FLUORANTHENE (06*3) <20S-99-2>409 BENZO (K)FLUORANTHENE (06*4) <207-08-9>406 BENZO (A)PYRENE (06*5) <50-32-8>437 INDENO (i. 2, 3-C.D) PYRENE (06*6) <193-39-5>419 D IBENZO( A. H) ANTHRACENE (06*7) <33-70-3>408 BENZO(G, H, DPERYLENE (06*8) <191-24-2>«619 2-FLUOROPHENOL (38*1)»612 DS-PHENOL (SS*2)*447 DS-NITROBENZENE (33*3)•448 2-FLUOROB I PHENYL (33*4)•628 2, 4, 6-TRIBROMOPHENOL (33*5)*496 D14-TERPHENYL (38*6)*471 D10-PYRENE456 1, 2, 3. 4-TETRACHLOROBENZENE

M/E15294931281461461081461084510870117771368213910712293162

SCAN422398403408419424436439447449459461466472532493500504516312521

TIME6:246:026:066: 116:216:256:366:396: 466:486: 576: 597:037:098:037:287: 347: 387: 497: 457: 33

REF1111111111111

1515151515151515

RRT1. 0000. 9430. 95S0. 9670. 9931.0051. 0331.0401.0591.0641. 0881. 0921. 1040.8871. 0000. 9270. 9400. 9470. 9700. 9620. 979

METHA BBA BVA BBA BBA BVA VBA BVA BBA VBA BVA BVA BVA BBA VBA BBA BVA BBA BVA WA BBA BB

AREA(HOHT) AMOUNT128892.633716.573084.586100.629720.663524.346196.577924.455740.472500.328884.444232.356700.616172.365688.1118980.270024.566680.253219.619400.375524.

40.119.119.130.121.128.134.121.129.120.146.122.134.113.40.127.124.150.136.136.121.

000032622727682377722653898221577090076022000372816413449789109

NGNONONONONONONGNONONONGNGNGNONGNONONONGNG

XTOT0. 371. 101. 111. 211. 121. 191. 241. 121. 201. 111. 351. 131. 241. 040. 371. IB1. 151. 391. 261. 261. 12


NO22232423262726293031323334353637383940414243444546474849505152S3545556575859606162636465666768697071727374757677

M/E180128127225107142164237196196162651631521381531841091681651651492041661381881981692482842661781781492022402021492522281492282641492522322322762782761129982172330244

SCAN52853353955056359469061562262563864966867666669269570170770967473273773874282274674976179S81182382687893210639331012103610611063106312341125118011631226143714431503324398471629760967

TIME8:008:048: 108:208: SO9:0010: 279: 199:259.289:409: 5010:0710: 1410:2310:2910:3210:3710:4310:4410: 1311:0511: 1011: 1111: 1412:2711: 1811:2111: SO12:0212: 1712:3012:3213: 1814:0716:0614:2615:2016:0116: 0416:0816:0818:4117: 0217: 5217: 5518:3421:4621: 5122: 464: 546:027 089:3211.3114:39

REF151515151515282828282828282828282828282828282828284747474747474747474757575757575757646464646464646411

15282837

RRT0.9921. 0021. 0131. 0341. 0961. 1171. OOO0. 8910. 9010. 9060. 9230. 9410. 9660. 9800. 9941.0031.0071. 0161.0231. 0280. 9771.0611.0661.0701. 0731. 0000. 9060. 9110.9500. 9670.9871. 0041. 0071.0681. 1341. 0000. 8970. 9520. 9950. 9981. 0021.0021. 0000. 9120. 9560.9S90. 9941. 1651. 1691.2180. 7660. 9430. 8850. 912I. 1010. 910

METHA BBA BVA VBA BBA BBA BBA BBA BBA BVA VBA BBA BBA BBA BBA BVA BBA BBA WA BBA BBA BBA BVA BBA BBA WA BBA BBA BBA BBA BBA BBA BVA VBA WA VVA BBA BVA BBA BBA BVA BBA VVA BBA WA BVA WA BVA*BVA BVA BVA BBA BVA VBA BBA BBA BB

AREA(HGHT) AMOUNT432832.151738O.640860.277372.483352.871756.153792.271926.256472.25S04O.854924.300392.788396.1117070.148236.610816.B0772.137656.948960.204428.165728.863176.431664.896496.143504.193066.76164.430472.152172.197580.65220.907744.899516.1224590.620745.129204.72845S.367960.72066.440932.819136.580252.66404.643646.412957.326001.305907.363826.331128.293920.552656.606636.667776.851664.78388.490088.

128.13O.219.147.126.131.40.193.192.183.162.164.146.172.163.162.169.139.159.144.145.153.181.161.173.40.131.154.127.149.142.148.166.153.137.40.156.126.139.132.144.151.40.ISO.139.130.136.139.144.138.117.127.117.171.162.147.

6385817322726715430006124659274511835867394363O9673644666634736936728693287000509920224678119751480847699000237683210066608756000323262793383781464096834976394988970898

NONONONGNONONONONGNONONONONONGNONONONGNGNGNGNGNGNONONONONONONONGNGNONONONONONONCNGNONONONONONONGNONGNONONGNGNONO

•XTOT1. 191. 212. 031. 361. 171. 220. 371. 791. 781. 701. 501. 521. 351. 601. 511. 501. 571. 291. 481. 341. 351. 421. 681. 491. 6O0. 371. 221. 431. IB1. 381. 311. 371. 561. 421. 270. 371. 441. 171. 291. 221. 341. 400. 371. 391. 251. 211. 261. 251. 331. 281. 091. 181. 081. 591. 511. 37


NO7879

NO1234567a910111213141516171819202122232425262728293031323334353637383940414243444546474849303152

M/E SCAN TIME REF RRT METH212 952 14:25 57 0.896 A BV216 639 9: 41 28 0. 926 A BB

RET(L)6:215: 586:036:076: 186:226:336:366:436:446:536:557: 007:058: OO7:247:317:347:437:427: 507:568:028:078: 168:468: 5710:239: 169:229:259:369.4610:0410: 1110:2110: 2610:2910: 3410: 4010: 4110: 0911: 0311: 0711: 0711:1112: 2411: 1411: 1711: 4712:0012: 14

RATIO RRT(L)1.011. 011. 011. 011.011. 011.011.011. 011.011.011. 011. 011. 011. 011. 011. 011. 011. 011.011.01I. 01.01.01. 01. 01.01. 01. 00

1. 011. 001.011. 011. 001. 011. 001. 001. 001. 001. 001. 011. 011. 001. 001. 011. 011. 001. 011. 011. 001. 001. 00

10. 00010. 00010. OOO10. 00010. 00010. 00010. 00010. 00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. OOOSO. 00010.00010. OOO10. 00010. OOO10. OOO10. 00010. 00010.00010. OOO10. OOO10. OOO50. OOO10. OOO50. OOO10. OOO10. 00050. OOO10. OOO50. OOOSO. OOO10. OOO10. OOO10. 00010. 00010. OOO10. OOO50. OOO10. OOO50. OOO10. OOO10. 00010. OOO50. 000

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110. 090. 100. 090. 090. 090. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. O90.020. 090. 020. 100. 100. 020. 100. 020.020. 100. 10O. 100. 110. 110. 110. 020. 100. 020. 090. 100. 100. 02

AMNT40.119.119.130.121.128.134.121.129.120.146.122.134.113.40.127.124.150.136.136.121.128.130.219.147.126.131.40.193.192.183.162.164.146.172.163.162.169.139.159.144.145.153.181.161.173.40.131.154.127.149.142.

00036273683872659022580908020037824145791164567327875400614693451859744431676467657494736929005192226812

AREA(HGHT) AMOUNT550244. 141. 287 NG393472. 165. 469 NO

AMNT(L)40.50.50.50.50.50.50.50.50.50.50.SO.SO.SO.40.SO.SO.30.SO.30.30.30.30.30.SO.SO.30.40.SO.30.30.50.SO.50.50.50.50.50.50.50.50.50.30.30.50.50.40.50.50.50.50.50.

0000000000OO000000OO00000000OO0000000000OO00000000000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)1. 0003.9333. 5573. 6383. 9094. 1182. 1493. 5872. 8292.9333. 2832.7972. 2141. 3461. 0002. 4460. S911. 24O0. 3541.3550.8220.9473. 3201.4020. 6071. 0571. 9O71. OOO1. 4191. 3491.3274. 4471. 5634. 1015. 8110. 7714. 2180. 4200. 8204. 9361. 0630.8624. 4902. 24S4. 6630. 7461. OOO0.3161. 7840. 6300. 8190. 353

1. OOO1.6521. 4871. 3911. 6061. 6O40. 7971. 4741. 0891. 2201. 1201. 1290. 8260. 5961. OOO0. 9610. 2370. 4120. 2030. 4950. 3390. 3681. 2710. 3190. 2060. 4170. 7231. 0000. 3630.3490. 3611. 3690. 4761. 3991. 6820. 2361. 2990. 1240. 2941. 3460. 3680. 2961. 4380. 6181. 4420. 2151. 0000. 1200. 3760. 2480. 2730. 124

XTOT1. 311. 33

RATIO1. 002. 382. 392. 612. 432. 572. 692. 432. 602. 402. 932. 442. 682. 261. 002. 332. 303. 012. 732. 742. 422. 372. 614. 392. 932. 542. 631. 003. 873. 833. 683.233. 282. 933. 433. 273. 253. 392. 793. 192. 892. 913. 083. 633. 233. 471. 002. 633. 102. 342. 992. 84

18756 07 SAMPLE DATA PPCKPGE '75

NO333455565758596061626364656667686970717273747576777879

RET(L)12:2612:3013: 1514:0516:0414:2415: 1816:0116:0216: 0616:0618:3917.0117: 5017: 5118.3121:4521:4722: 414: 515:577:049:2911:2914:3614:229:37

RATIO RRT(L)1. 001. OO1. 001.001. 001. 001. OO1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 011. 011. 011. 001.001. 001. OO1. 01

10. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. 00020. OOO10. OOO10. 00010. 00010. 00010. OOO10. OOO10. 00010. OOO10. 00010. 00010. OOO0. 7420. 9480. 8750. 9061. 1180. 90710. OOO1.000

RATIO0. 100. IO0. 110. 110. 100. 090. 100.050. 100. 100. 100. 100. 090. IO0. 100. 100. 120. 120. 121. 040.991.011.010. 991. OOO. O90.93

AMNT148.168.153.137.4O.156.126.139.132.144.151.40.150.135.130.136.135.144.138.117.127.117.171.162.147.141.165.

754885700024682107617600322879387846108398399997902947

AMNT(L)50.50.50.50.40.50.50.50.50.50.50.40.50.50.50.SO.5O.50.50.5O.50.50.50.50.50.50.50.

000000000000000000000000OO000000000000OO000000OO00OO00

R. FAC R. FAC(L)3. 7613. 7275. 0742. 5721. OOO4. 5102.2780. 4462.7305. 0723. 5931. OOO7. 8133. 8233. 0182.8323. 3693. 0662.7213. 4303. 7661. 4614. 43O0. 4083. 0353. 4072.047

1. 2641. 1061. 6490. 9341. OOO1. 4430. 8990. 16O1. 0341. 7541. 1841. OOO2. 5991. 4131. 1541. 0381. 24O1. 0610. 9851. 4561. 4720. 6221. 2880. 1251. 0261. 2O60. 618

RATIO2. 983.373. 082. 751. 003. 122. S32. 782.642.893. 041. 003. 012. 712. 622. 732. 722. 892. 762. 362. 562. 333. 443. 262. 962.833. 31


COMPUCHEM LABSRIC12/21/89 18:15:00

COMPUCHEM DATA: HI891221A28 SCANS 308 TO 1600OUT OF 308 TO 1680

SAMPLEt 1 UL 30658-12368 160 NG/UL SEMI2 STD. (SSTD168)CONDS.i 4797438.

IStl ISI2 ISff3 SSf5

SSt2 SSI3 5SI4 D3I1 ISM

SS§6

SS17

ISI5

ISt6

1865

RIC

1362

1443

JL888

12:87188815:89

120018:11

148021:12

l168024:14

SCANTIME

nf -•'••I

UJ(0Ct'X.octCL

Ct

UJ-JCLHCtI/I

Q

•Dinr^CO

QUANTITATION REPORT FILE: HI891221A20DATA: HI891221A2O. TI12/21/89 18:13:OOSAMPLE: 1 UL 30638-*2368 160 NG/UL SEMI2 STD. (SSTD160)CONDS. :SUBMITTED BY: 20 ANALYST: 875


NO NAME1 *494 D4-1,4-DICHLOROBENZENE (IS*1)2 610 PHENOL (01*3) <108-95-2>3 411 B13(2-CHLOROETHYL)ETHER (01*5) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <95-57-8>3 421 1,3-DICHLOROBENZENE (01*7) <341-73-l>6 422 1,4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-51-6>B 420 1,2-DICHLOROBENZENE (01*10) <95-50-l>9 620 2-METHYLPHENOL (01*11) <95-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-5>12 442 N-NITR080-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*15) <67-72-l>14 440 NITROBENZENE (01*16) <98-95-3>15 »460 D8-NAPHTHALENE (IS*2)16 438 ISOPHORONE (02*2) <78-59-l>17 606 2-NITROPHENOL (02*3) <88-75-5>18 603 2,4-DIMETHYLPHENOL (02*4) <105-67-9>19 625 BENZOIC ACID (02*5) <6S-85-0>20 410 BIS(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <12O-83-2>22 446 1.2. 4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-20-3>24 475 4-CHLOROANILINE (02*10) <106-47-8>25 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (02*12) <59-3O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-37-6>28 »493 D10-ACENAPHTHENE (13*3)29 435 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2,4, 6-TRICHLOROPHENOL (03*3) <88-O6-2>

'31 626 2, 4, 5-TRICHLOROPHENOL (03*4) <93-93-4>32 416 2-CHLORONAPHTHALENE (03*3) <91-38-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 425 DIMETHYL PHTHALATE (03*7) <131-ll-3>35 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-O9-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 «605 2, 4-DINITROPHENOL (03*11) <51-2B-5.>39 607 4-NITROPHENOL (03*12) <100-O2-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2, 6-DINITROTOLUENE (03*15) <606-2O-2>43 424 DIETHYL PHTHALATE (03*16) <B4-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7005-72-3>45 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-Ol-6>


NO474849505152535455565758596061626364656667686970717273747576777879

NO123456789101112131415161718192021

NAME•467604443414433609444403426431*459445415423405413418»497429407409406437419408*619*612*447*448«628

D10-PHENANTHRENE (13*4)4, 6-DINITRO-2-METHYLPHENOL (04*2) <534-52-l>N-NITROSODIPHENYLAMINE (04*3) <86-3O-6>4-BROMOPHENYL PHENYL ETHER (04*4) <101-55-3>HEXACHLOROBENZENE (04*5) <118-74-l>PENTACHLOROPHENOL (04*6) <87-86-5>PHENANTHRENE (04*7) <85-Ol-8>ANTHRACENE (04*8) <120-12-7>DI-N-BUTYL PHTHALATE (04*9) <84-74-2>FLUORANTHENE (04*10) <2O6-44-O>D12-CHRYSENE (13*5)PYRENE (05*3) <129-OO-0_>BUTYLBENZYL PHTHALATE (05*4) <85-68-7>3. 3'-DICHLOROBENZIDINE (05*5) <91-94-l>BENZO ( A) ANTHRACENE (05*6) <56-55-3>BIS(2-ETHYLHEXYL) PHTHALATE (05*7) <117-81-7>CHRYSENE (05*8) <218-01-9>D12-PER YLENE (IS«6)DI-N-OCTYL PHTHALATE (O6*2) <117-84-0>BENZO (B)FLUORANTHENE (06*3) <205-99-2>BENZO(K) FLUORANTHENE (06*4) <207-08-9>BENZO (A)PYRENE (06*3) <50-32-B>INDENO (1, 2, 3-C.D) PYRENE (Q6*6) <193-39-5>DIBENZO(A.H) ANTHRACENE (06*7) <53-70-3>BENZO(G, H, DPERYLENE (06*8) <191-24-2>2-FLUOROPHENOL (SS»1)D5-PHENOL (83*2)DS-NITROBENZENE (83*3)2-FLUOROB I PHENYL (33*4)2, 4. 6-TR IBROMOPHENOL ( SS*5 )

*496 D14-TERPHENYL (38*6)*471456

M/E15294931281461461081461084510870117771368213910712293162

D10-PYRENE1, 2. 3, 4-TETRACHLOROBENZENE

SCAN TIME REF RRT METH AREA(HGHT)422 6:24 1 1.000 A B B 117452.398 6: 02 1 0. 943 A BB 873592.403 6:06 1 0.955 A B B 725740.408 6:11 1 0.967 A BB 695880.42O 6:22 1 0.995 A BV 812496.424 6:25 1 1.005 A VB 828372.436 6:36 1 1.033 A BV 407560.439 6:39 1 1.040 A BB 740680.447 6:46 1 1.059 A VB 591724.449 6:48 1 1.064 A VB 595920.459 6: 57 1 1. 088 A BV 588S92.461 6:59 1 1.092 A BB 579020.466 7:03 1 1.104 A B B 438984.472 7:09 15 0.887 A W 7835S4.532 8:03 15 1. OOO A BB 333972.493 7:28 15 0.927 A BV 1406700.5OO 7:34 15 0.940 A BB 348176.504 7:38 15 0.947 A BB 723628.516 7:49 15 0.970 A VB 280456.512 7:45 15 0.962 A BB 686648.520 7.53 15 0.977 A BB 466348.

AMOUNT40.180.166.170.172.175.174.171.185.166.179.174.181.157.40.175.176.210.165.166.164.

000070241332292883050099085392014635077373OOO329225312478041683

NONONGNGNONGNONGNONONONONONONONGNONONONONG

XTOT0. 271. 231. 13161820191726142219

1. 241. 070. 271. 201. 201. 441. 131. 131. 12


NO22232425262728293031323334353637383940414243444546474849505152535455565758596O6162636465666766697071727374737677

M/E1601281272231071421642371961961626316313213813318410916816316314920416613816819816924828426617817814920224O202149292228149228264149232232252276278276112998217233O244

SCAN52853453955058259468961562262563864966867968669269970170770867473273773874162274974878179981182482887793210629931012105610611065106512331125117911631226144214441SOS323398471629760966

TIME8:OO8:058: 108:206:499:0010:269: 199:259:289:409: 5010:0710: 1310:2310:2910:3210:3710:4310:4310: 131 1 . 0511: 1011: 1111: 1312:2711: 1711:2011: SO12:0212: 1712:2912:3213: 1714:0716:0514:2615:2016.0116:0416:0816:0818:4117:0217:5117: 5316:3421:5021:5222:464: 546:027:089:3211:3114.38

REFISIS19191919262828282828282828282828282828262828284747474747474747474797979797979797646464646464646411

19262857

RRT METH0. 992 A BB1. 004 A BV1.013 A BB1. 034 A BB1. 094 A BV1. 117 A VB1. 000 A BB0. 893 A BB0. 903 A BV0. 907 A VB0. 926 A BB0. 942 A BB0. 970 A BB0. 960 A BB0. 996 A BV1. 004 A BB1. 009 A BB1.017 A W1. 026 A BB1. 028 A BB0. 978 A VB1. 062 A BV1.070 A BB1.0711.0751. OOO0. 9060. 9100. 99O0.9670.9871.0021. 0071. 0671. 1341.0000. 8970. 9530. 9960. 9991. 0031.0031. 0000. 9120.9960.9990. 9941. 1701. 1711. 2210. 769

BBBVBBBBBBBBBBBVBVVBBBWBBWBVBVBVWWBBBVBVVBWBBBBBBBB

0. 943 A BV0. 669 A VB0. 913 A BB1. 103 A BB0. 910 A BB

AREA(HOHT) AMOUNT934692.1611030.637286.306364.933972.1002490.119196.293920.248204.268468.918784.314472.891140.1177810.196900.762196.69272.196940.944636.202980.168120.901096.428064.877776.108720.119920.80212.440676.143836.186920.76776.786004.771492.1164660.616623.99892.703672.394612.76612.479104.872166.603067.66260.649496.460968.390906.399216.378167.339116.292876.729744.767464.861896.979884.67680.510708.

174.170.239.178.153.165.40.279.246.258.233.229.211.243.231.2O3.183.183.212.191.197.214.24O.211.175.4O.223.255.193.227.206.207.232.233.220.40.19S.175.191.185.199.204.40.196.196.183.206.184.192.179.169.177.165.264.187.199.

067653258113353636000483828569161546348239028756116649263818441605687434331OOO002355627512156388666593314000207613859608150004000407919566513039928439810615901272917346

NONGNONONONONGNGNONONONONGNGNGNONGNGNGNONGNGNONGNGNGNGNONONGNGNONGNGNGNONONONONONONONONONGNONGNGNGNGNONONONONGNG

XTOT1. 191. 161. 631. 221. 051. 130. 271. 911. 681. 761. 591. 571. 441. 661. 581. 391. 251. 271. 451. 311. 351. 461. 641. 441.200. 271. 521. 741. 321. 551. 411. 421. 591. 611. 300. 271. 331. 201. 311. 271. 361. 390. 271. 341. 341. 251. 411. 261. 321. 221. 161. 211. 131. 801. 281. 36


NO7879

NO12343678910111213141316171819202122232423262728293031323334353637383940414243444546474849305132

M/E SCAN TIME REF RRT METH212 951 14:24 57 0.895 A BV216 639 9:41 28 0.927 A BB

RET(L)6:215: SB6:036:076: 186:226:336:366:436:446: S36:557:007:058:007:247:317: 347:437:427: 507: 568:028:078: 168:468: 5710:239: 169:229:259:369: 4610: 0410: 1110: 2110: 2610:2910:3410: 4010: 4110:0911:0311: 0711:0711: 1112:2411: 1411: 1711: 4712: 0012: 14

RATIO RRT(L)1. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011. 011.011. 01I. 011. 011. 011. 011. 011. 011. 011. 001. 001. 011. 001. 011. 011. OO1. 001. 001. 001. 001. OO1. 001. 001. 011. 001. 001. 011. 001. 001. 001. 001. 001. 001. 00

10. 00010. 00010. 00010. 00010. OOO10. OOO10. 00010. 00010. 00010. OOO10. 00010. OOO10. OOO10. 00010. 00010. OOO10. 000IO. OOO50.00010. OOO10.00010. OOO10. 00010. OOO10. OOO10.00010. 00010. OOO10. OOO10. OOO50. OOO10. OOO50. 00010. OOO10. 00050. 00010. OOO50. 00050. OOO10. 00010. 00010. 00010. 00010. 00010. 00050. 00010. 00050. 00010. 00010. 00010. 00050. 000

RATIO0. 100. 090. 100. 100. 100. IO0. 100. IO0. 110. 110. 110. 110. 110. 090. 100. 090. 090. 090.020. 100. 100. 100. 100. IO0. IO0. 110. 110. 100. 090. 090. 020. 090. 020. 100. 100. 020. 10O. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090. 100. 100. 02

AMNT40.180.166.170.172.175.174.171.185.166.179.174.181.157.40.175.176.210.165.166.164.174.170.239.178.153.165.40.279.246.258.233.229.211.243.231.203.183.185.212.191.197.214.240.211.175.40.223.255.193.227.2O6.

00072433298805100839016308370033223148046807652611356400488357165535240376126526624460694333000036635116

AREA(HGHT) AMOUNT546SO8. 181. 303 NG4O8712. 229. 345 NO

AMNT(L)40.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.50.50.50.5O.SO.SO.SO.SO.50.50.40.50.50.50.5O.50.50.50.50.50.50.50.50.50.50.50.50.50.50.40.50.50.50.50.50.

00000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

R. FAC R. FAC(L)1. 0005. 9504. 9434. 7405. S34S. 6422. 776S. 0454. 0304. 0594. OO93.9442. 99O1.8771. OOO3. 3700. 8341. 733O. 6721. 6451. 1171. 2814. 3381. 5270. 7341. 2782. 4011. OOO2. 0421. 7241.8656. 3832. 1855. 9138. 1821. 0905. 2950. 4531. 0906. 5621. 4101. 1666. 2602. 9746. 0980. 7551. 0000. 5352. 9400. 9601. 2440. 512

1. 0001. 652. 487. 391. 606. 604

0. 797. 474. 089

1. 2201. 1201. 1290. 8260. 5961. OOO0. 9610. 2370. 4120. 2030. 4950. 3390. 3681. 2710. 3190. 2060. 4170. 7251. OOO0. 3650. 3490. 3611. 3690. 4761. 3991. 6820. 2361. 2990. 1240. 2941. 5460. 3680. 2961. 4580. 6181. 4420. 2151. 0000. 1200. 5760. 2460. 2730. 124

XTOT1. 241. 57

RATIO1. 003. 603. 323. 413. 453. 523. 463. 423. 703. 333. 583. 493. 623. 151. 003. 513. 524. 213. 313. 323. 293. 483. 414. 793. 563. 073. 311. 005. 594. 945. 174. 664. 594. 234. 864. 624. 083. 663. 714. 253. 843. 954. 294. 814. 233. 511. 004. 465. 113. 874. 554. 12

1S756 87 SAMPLE DATA PACKAGE 269

NO53545336575859606162636465666768697O717273747376777879

RET(L) RATIO RRT(L)12:12:13:14:16:14:13:16:16:16:16:18:17:17:17:18:21:21:22:4:3:7:9:

11:14:14:9:

26 1. 0030 l.OO13 1.0003 1. 00042418010206063901303131

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. 00

. OO

. 00

. 0043 1.0047 1.0041 1.0031 1.0137 . 0104 . 0129 . 0029 . 0036 . 0022 . 0037 . 01

10. 00010. OOO10. 00010. 00010. 00010. 00010. OOO20. OOO10. 00010. OOO10. OOO10. OOO10. OOO10. OOO10. OOO10. 00010. OOO10. 00010. 0000. 7420. 9480. 8750. 9061. 1180. 90710. 0001. 000

RATIO0. 100. 100. 110. 110. 100. 090. IO0. 050. 100. 100. 10O. IO0. 090. IO0. 100. 100. 120. 120. 121. 030. 991. 011. 010. 991. OO0. 090. 93

AMNT207.232.235.220.40.195.175.191.165.199.204.40.196.196.183.206.184.192.179.169.177.165.264.187.199.181.229.

396759310021818661150000419259510493448162902792355054

AMNT(L)SO. 0050. 0050. 0050. 0040. 0050. 0050. 0050. 0050. 0050. 0050. 0040. 0050. 0050. 0050. 0050. 0050. OO50.00SO. OO50.0050. 0050. 0050. 0050.0050.0050.0050. 00

R. FAC R. FAC(L)5. 2445. 1477. 7704. 1151. 0005.6353. 1620. 6153. 8376. 9654. 8301. 000

10. 2O85. S664. 2374.2894. 5664. 0943. 5364. 9435.2272. 0646. 8O70.4704. 0904. 3772. 839

1. 2641. 1061. 6490. 9341. 0001. 4430. 8990. 1601. 0341. 7541. 1841. 0002. 5991. 4131. 1541.0381. 2401. 0610. 9851. 4561. 4720. 6221. 2880. 1251. 0261. 2060. 618

RATIO4. 154. 654. 714. 411. 003. 903. 523. 843. 713. 984. 081. 003. 933. 943. 674. 133. 683. 863. 593. 403. 553. 325. 293. 763. 993. 634. 59

18756 07 SAMPLE DATA PACKAGE 26S

COMPUCHEM LABORATORIES. INC.INITIAL TIME OF TUNE SHIFT(S) (A| (B) |C|

1

2

3

4

5

6

7

e

9

10

11

12

13

14

15

16

17

18

19

20

2,

22

23

24

nEJECIEO

/

GC/MS ANALYSIS LOG

RUN LOG

FILE NAME

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DATE

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COMMENTS (Lot »'s. Disposition. Etc )

'

\ VFRIFIFD v <r „ \ v. c ^ l -_,Uv 1 y "v £**-v

f-•£ir-4

UJCDCt'.*Oct0.

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SUPERVISOR APPROVAL


Lab Name: COMPUCHEM LABS Contract: (2-88) -REVS


Instrument ID: 21



Max %RSD for CCC(*) = 30.0^

LAB FILE ID: RRF20 - HH891030C21 RRF50 = HG891030C21RRF80 = HI891Q30C21 RRF120= HJ891030C21 RRF160= HK891030C21

COMPOUND

Phenolbis ( 2-Chloroethyl ) Ether2-Chlorophenol1 , 3-Dichlorobenzene

RRF20

* 1.4911.3501.3441.578

1 . 4-Dichlorobenzene * 1.624Benzyl Alcohol1 . 2-Dichlorobenzene2 -Methylphenolbis(2-Chloroisopropyl) Ether4 -Methy IphenolN-Nitroso-Di-n-Propylamine_jHexachloroe thaneNitrobenzeneIsophorone

0.7391.4521.0400.7131.074

1 0.7670.7140.3820.685

2-Nitroohenol * 0.1832 , 4 -Dimethy IphenolBenzoic Acidbis (2-Chloroethoxy)Methane_2 , 4-Dichlorophenol '1,2, 4-TrichlorobenzeneNaphthalene4-Chloroaniline

0.3080.1740.430

* 0.2710.3481.1300.342

Hexachlorobutadiene * 0.2094-Chloro-3-Methylphenol * 0.2662-Methylnaphthalene 0.566Hexachlorocyclopentadiene # 0.3622 ,4 .6-Trichlorophenol * 0.3532,4, 5-Trichlorophenol2-chloronachthalene2-NitroanilineDimethyl PhthalateAcenaphthylene2 , 6-Dinitrotoluene3-Nitroaniline

0.3831.2310.2181.2981.6210.2020.207

Acenaphthene * 1.179! 2 , 4-Dinitrophenol', 4-Nitrophenol

„ 0.118H 0.168

RRF50

1.6881.3631.3411.4701.5690.7351.4260.9710.7771.1100.9380.6900.4460.8010.2130.3310.2170.4550.3080.3821.2450.3010.2180.2950.6480.3460.3990.4151.4480.2601.4661.8670.2590.2241.4360.1300.234

RRF80

1.6501.4231.3711.5861.6970.7811.5831.1690.8241.2190.9910.7370.4170.7120.1960.3380.2030.4620.2920.3701.1940.2750.2070.2970.6210.4210.4490.4831.5850.2651.5341.9070.2760.2011.4770.1220.208

RRF120

1.6701.3691.5231.5911.6520.8131.4991.0520.7571.2500.9280.7150.4340.7890.2140.3670.1950.4730.3210.3931.2670.3590.2230.3270.6550.4560.4600.4781.6270.3091.6312.1370.2850.2441.5820.1320.224

RRF160

1.5901.4491.4161.6861.7510.8571.5381.1260.9991.2841.0300.7800.4800.8440.2200.3970.2380.5220.3190.4161.2790.3460.2290.3500.6920.4650.4970.5171.6830.3881.7762.1060.3410.2751.7220.1480.252

RRF

1.6181.3911.3991.5821.6590.7851.5001.0720.8141.1870.9310.7270.4320.7660.2050.3480.2050.4680.3020.3821.2230.3250.2170.3070.6360.4100.4320.4551.5150.2881.5411.9280.2730.2301.4790. 1300.217

%RSD

4.9*3.15.44.8 i4.2*6.6)4.27.213.67.7

10.8=!4.78.48. 67.5*9.911.77.26.9*6.65.010.84.3*10.5*7.413.2 =13.0*12.011.922.411.610. 818.313.113 . 6i8.9 =14.7 =




Lab Name: COMPUCHEM LABS Contract: (2-88^-REVS


Instrument ID: 21




LAB FILE ID: RRF20 = HH891030C21 RRF50 = HG891030C21RRF80 = HI891030C21 RRF120= HJ891030C21 RRF160= HK891030C21

COMPOUND

Dibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenylether_Fluorene4-Nitroaniline4 , 6-Dinitro-2-Methylphenol_N-Nitrosodiphenylaroine (l)_j4-Bromophenyl-phenyletherHexachlorobenzene

RRF20

1.5160.3021.3340.5391.0900.1570.093

* 0.5580.2350.322


1.0941.0441.282

Fluoranthene * 0.862PyreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo (a) AnthraceneChrysenebis ( 2 -Ethylhexyl ) Phthalate_Di-n-Octyl Phthalate <Benzo (b) FluorantheneBenzo ()_) Fluoranthene

1.4600.5750.1490.9821.0600.963

" 1.4480.9901.228

Benzo (a) Pyrene * 0.981Indeno ( 1 , 2 , 3-cd) PyreneDibenzo ( a , h) AnthraceneBenzofq.h, i) Perylene

Nitrobenzene-d52-FluorobiphenylTerphenyl-dl4Phenol-d52-Fluorochenol2,4, 6-Tribromophenol

0.9910.7140.864

0.3771.3560.9871.4201.3060.137

RRF50

1.7280.3661.5800.6131.3020.1670.1110.5970.2420.3470.1301.2361.1351.5541.0541.5150.6560.1521.0611.0321.1781.8931.2021.1800.8731.2110.8661.022

0.4421.4620.9691.4031.3340.172

RRF80

1.7890.3471.6030.6441.4330.1210.1180.6230.2690.3640.1311.2941.2211.5941.0361.5770.6300.1271.0500.9661.1811.9921.3281.2631.0351.1830.8300.986

0.4201.5671.0721.4321.4500.177

RRF120

1.9670.3991.6920.6961.4850.1880.1260.7050.3010.3870.1501.4141.3191.6351.1581.4950.6290.1271.0021.0061.1421.8771.2051.3691.1471.1940.8341.003

0.4261.5840.9921.4571.3880.184

RRF160

2.0540.4401.9430.7421.7310.1560.1380.6410.2770.3420.1601.3841.3211.7131.1681.5920.7260.1331.1540.9951.3742.1431.2481.2131.1001.0990.7990.959

0.4631.6481.0091.5911.3670.210

RRF

1.8110.3711.6300.6471.4080.1580.1170.6250.2650.3520.1341.2841.2081.5561.0561.5280.6430.1381.0501.0121.1681.8711.1951.2511.0271.1360.8090.967

0.4261.5231.0061.4611.3690.176

%RSD

11.614.113.512.016.815.414.48.7*10.16.9

16.9*10.09.910.511.7*3.68.58.86.43.5

12.513.8*10.55.8

10.4*8.17.26.4

7.57.63.95.24.0

14 . 9

(1) Cannot be separated from Diphenylamine



RIC19/38/89 4i44:96SAMPLE! 1UL SSTD82e HG/UL LOTI2364CONDS.:

COMPUCHEM LABSCOMPUCHEM DATA: HH891638C21 SCAHS 356 TO 1656

OUT OF 356 TO 2898

1511 1512 ISI3 5515

SSI2 5513 5St4 D3tl . 1514

SSI6 1515

SSI7 ISIS UJ<£•

_ RIC

1146

942 100

1882

12981216 129

JLJl1361

i

l 1448 1588 A 1812

a:CL

ctK<ta

UJ

s:cc

rv

•oinr-.CO

14:59

T128817:59

148828:59

168823:59

188826:59

QUANTITATION REPORT FILE: HH891O30C21DATA: HH89103OC21. TI10/30/89 4:44:OOSAMPLE: 1UL S8TD020 NO/UL LOT*2364CONDS. :SUBMITTED BY: 21 ANALYST: 619

AMOUNT-AREA » REF. AMNT/(REF. AREA)» RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1. 4-DICHLOROBENZENE (IS*1>2 61O PHENOL (01*3) <108-99-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*9) <lll-44-4>4 601 2-CHLOROPHENOL (Qlt6) <99-97-8>5 421 1,3-DICHLOROBENZENE (01*7) <941-73-l>6 422 1,4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-91-6>8 420 1.2-DICHLOROBENZENE (01*10) <93-90-l>9 620 2-METHYLPHENOL (01*11) <99-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <lO6-44-9>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*19) <67-72-l>14 440 NITROBENZENE (01*16) <98-99-3>19 »460 D8-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-99-l>17 606 2-NITROPHENOL (02*3) <88-79-9>18 603 2,4-DIMETHYLPHENOL (02*4) <109-67-9>19 629 BENZO1C ACID (02*9) <69-89-O>20 410 B18(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2. 4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1.2, 4-TRICHLOROBENZENe (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-2O-3>24 479 4-CHLOROANILINE (02*10) <106-47-8>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORQ-M-CRESOL (02*12) <99-9O-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>28 »499 D10-ACENAPHTHENE (IS*3)29 439 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2. 4. 6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2. 4.9-TRICHLOROPHENOL (03*4) <99-99-4>32 416 2-CHLORONAPHTHALENE (03*9) <91-98-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 429 DIMETHYL PHTHALATE (03*7) <131-ll-3>39 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-O9-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 t609 2. 4-DINITROPHENOL (03*11) <91-28-9>39 607 4-NITROPHENOL (03*12) <100-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2i6-DINITROTOLUENE (03*19) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <S4-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER <Q3*17) <7009-72-3>49 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <10O-01-6>


NO474849909192939499969798996061626364696667686970717273747976777879

NO12349678910U12131419161718192021

NAME*467 D10-PHENANTHRENE (IS*4)604 4. 6-DINITRO-2-METHYLPHENOL (04*2) <934-92-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-30-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-99-3>433 HEXACHLOROBENZENE (04*9) <1 18-74-1 >609 PENTACHLOROPHENOL (04*6) <87-86-9>444 PHENANTHRENE (04*7) <89-01-8>403 ANTHRACENE (04*8) <120-12-7>426 DI-N-BUTYL PHTHALATE (O4*9> <84-74-2>431 FLUORANTHENE (04*10) <206-44-O>«499 D12-CHRYSENE (13*9)449 PYRENE (09*3) <129-OO-O>419 BUTYLBENZYL PHTHALATE (09*4) <89-68-7>423 3, 3'-DICHLOROBENZIDINE (09*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-99-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PER YLENE (18*6)429 DI-N-OCTYL PHTHALATE (06*2) <117-84-O>4O7 BENZO(B)FLUORANTHENE (06*3) <209-99-2>409 BENZO(K)FLUORANTHENE (06*4) <207-O8-9>406 BENZO(A)PYRENE (06*9) <9O-32-8>437 INDENO (1. 2. 3-C.D) PYRENE (O6*6) <193-39-9>419 D I BENZO ( A, H) ANTHRACENE (06*7) <93-70-3>408 BENZO(0, H, DPERYLENE (O6*8) <l91-24-2>•619 2-FLUOROPHENOL (88*1)•612 D9-PHENOL (88*2)*447 D9-NITROBENZENE (SS«3)#448 2-FLUOROB I PHENYL (SS«4)•628 2. 4. 6-TRIBROMOPHENOL (88*9)•496 D14-TERPHENYL (SS«6) . /*471 D10-PYRENE /A IU496 1.2. 3, 4-TETRACHLOROBENZENE /k'^-U

M/E19294931281461461081461084910870117771368213910712293162

SCAN4704464904964674724844884964979089O9919922984943991999963962973

TIME7:036:416:496: 907:007:O47: 197: 197:267:277: 377:387:437: 498:498:088: 198. 198:268: 298.39

REF1111

1919191919191919

RRT1. OOO0. 9490. 9970. 9700.9941.004.030. 038. 099. 097. 081. 083

1. 0960.8941. OOO0. 9300. 9430. 99O0. 9640. 9620. 981

METHA BBA BVA BVA BBA BVA VBA BVA BBA VBA BBA BVA BVA BBA BBA BBA BBA BBA BBA VBA BBA BB

/to}Ui

'fAREA(HCHT) AMOUNT126184.94048.89172.84800.99988.102440.46601.91640.69624.44964.67796.48408.49072.70092.367436.129920.33664.96980.31944.79036.49716.

40.17.19.20.21.20.20.20.21.IB.19.16.20.17.4O.17.17.18.16.18.17.

000662819046476698108371428339341393710108OOO119204989026913993

NONCNONONONONONONONONONONONONONCNONCNONCNC

<7

5CTOT2. 991. 12. 26. 28.37. 32. 28.30. 36

1. 171. 231. 041. 321. 092. 991. 091. 101. 181. 021. 201. 12


NO2223242926272829303132333439363738394O41424344494647484990919293949996979899606162636469666768697071727374797677

M/E180128127229107142164237196196162691631921381931841091681691691492041661381881981692482842661781781492022402021492922281492282641492922922922762782761129982172330244

SCAN98098699260263764974867O67868269470672473474979179476176676873179079779880288780680984389887988989394210O11141102310821134113911391143136112161290129413901628163317113714499216848231039

TIME8:428:478:929:019:339:4411: 1310. 0210: 1010: 1310:2410:3910:9111:0011: 1011: 1911: 181 1 : 2411:2911:3110:9711:9011:9711: 9812:0113: 1812:0912:0712: 3812:9113:0713: 1913:2314:0719:0017:0619:2016: 1317:0017:0417:0417:0820:2418: 1319: 2O19: 2420: 1424:2424:2829:389: 346: 407: 4810: 1912:2019.31

REF191919191919282828282828282828282828282828282828284747474747474747474797979797979797646464646464646411

19282897

RRT t0. 993 t1. 0031.0141. 0311. 0911. Ill1. 0000. 8960. 9060.9120. 9280. 9440. 968O. 9810. 9961.0041. O081.017.024.0270.977. 096. 066. 067.072. 000

O. 9090. 9120. 99OO. 967 /0. 986 *1. 002 /1 . 007 /1.062 t1. 129 /1.000 t0. 897 /0. 9480. 9940.9980. 9981.0021. OOO0.893 t0. 948 i0. 991 iO. 992 t1. 196 i1. 20O i1.297 t0. 789 /0. 947 i0. 892 /0. 914 /1. 100 t0. 907 /

1ETHH BBBVBBBBBBBBBBBBBVVBBBBBBBBBBBBBBBBBBBBBBBBVBBBBBBBBBBBBBB

S BB\ BBt BVX VB* BB\ BBX BBt BBBBBBBVBBVBBB

)» BB\ BV\ VV* BV\ BB* BBit BBK BB\ BV\ BB\ BB\ BB\ BB

AREA(HCHT63872.207676.62804.38440.48892.103912.199864.28196.27476.29868.99924.17028.101196.126332.1616O.91920.9196.13080.118112.23912.19792.103992.41984.84996.12236.191980.8888.93472.22932.30872.9688.

104788.100048.122848.826O4.124892.91172.39932.9328.61296.6014O.66184.100176.72944.49604.61932.49148.49644.39760.43284.82372.896OO.69180.109668.10664.61636.

) AMC18.18.22.19.IB.17.40.20.17.18.16.16.17.17.18.16.18.14.17.16.19.16.17.16.18.4O.16.18.19.18.19.17.18.16.16.40.19.17.19.18.16.20.40.19.16.20.22.16.16.16.19.20.17.18.19.20.

IUNT184169677239010498000913669497997784706363992422196341940469616893988743821OOO696696412999926697409907367OOO277932633496392937000306474829481371486918979238024946870366

NONCNCNCNCNONCNCNCNCNONONCNONONCNCNCNCNCNCNCNCNCNONONCNCNCNCNCNCNONGNCNCNCNCNONCNONCNONCNONCNCNONCNCNCNCNONONONC

XTOT1. 161. 161. 441. 221. 191. 112. 991. 331. 131. 181. 081. 071. 131. 111. 181. 091. 160. 911. 121. 090. 991. 081. 121. 071. 202. 991. 061. 191. 241. 180. 991. 131. 171. 091. 042. 991. 231. 121. 291. 181. 041. 312. 990. 971. 091. 331. 431. 041. 091. 081. 291. 291. 081. 181. 011. 30


NO7879

NO12349678910111213141916171819202122232429262728293031323334393637383940414243444946474849909192

M/E SCAN TIME REF RRT METH212 1021 19:18 97 0.895 A B B216 699 10: 29 28 0. 929 A BB

RET(L)7:046:426:466:917:017:047: 167:207:267:287:387:387: 447:908:498:088: 198: 198:298:268:398:428:478: 939:019:349:4411: 1310:0310: 1010: 1410:2910:3610: 9211:0111: 1111: 1611: 1911:2911: 3011: 3110: 9811: 9111: 9811: 9812:0213: 1812:0612:0712:3912: 9213:07

RATIO RRT(L)1. 001.001.00. 00. 00.00.00.00.00.00.00.00

1. OO1. 001.001. OO1. 001.000.991.001.001. 001.001.001.001.001.001. 001.001. 001. 001. OO1. 001. 001. 001. 001. 001. 001.00l.OO1. 001. 001. OO1. 001.001. 001. 001. 001. 001. 001. 001. 00

10. OOO10.00010.00010. OOO10. 00010.00010. 00010. OOO10.00010. OOO10.00010. OOO10.00010. OOO10.000IO. OOO10. OOO10. OOO90. OOO10. OOO10.00010. OOO10.00010. 00010.00010. OOO10.000IO. OOO10. OOO10. OOO90.00010. 00090. 00010. OOO10. 0009O. 00010. OOO90. OOO90.00010. OOO10. OOO10. 00010. OOO10. 00010. 00090. 00010. 00090. 00010. OOO10. 00010. OOO90. OOO

RATIO0. 100.090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110.090. 100.090. 090. 100. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100. 090. 090. 020.090. 020. 100. 100.020. 100. 020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090. 100. 100. 02

AMNT4O.17.19.20.21.20.20.20.21.18.19.16.20.17.40.17.17.18.16.18.17.18.18.22.19.18.17.40.20.17.18.17.16.17.17.18.16.18.14.17.16.19.16.17.16.18.40.16.18.19.18.19.

OO66820948701137433434397111OO122099039199181768230146OO916946007871369942163494476289997482007070419693

AREA(HOHT) AMOUNT71460. 19. 972 NC26764. 18. 724 NC

AMNT(L)40.90.90.90.90.90.90.90.90.90.90.90.90.90.40.90.90.90.90.90.90.90.90.90.90.90.90.40.90.90.90.90.90.90.90.90.90.9O.90.90.90.90.90.90.90.90.40.90.90.90.90.90.

0000000000000000OOOO0000OOOOOOOO00000000OO000000000000000000000000000000000000000000OO0000000000000000OO

R. FAC R. FAC(L)1. OOO0. 9960. 94O0. 9380. 6310.6490.2990. 9810. 4160.289O. 43O0. 3070. 286O. 1931. OOO0. 274O. 0730. 123O. 0700. 1720. 1O80. 1390. 4920. 1370.0840. 1060.2261. OOO0. 1490. 1410. 1930. 4920.0870. 9190. 6480. 0830. 4720. 0470.0670. 6060. 1210.0810. 9340.2190. 4360. 0631. OOO0. 0370. 2230. 0940. 1290. 040

1. 0001. 6881. 3631. 3411. 4701. 9690. 7391. 4260.9710. 7771. 1100.9380. 69O0. 4461. 0000. 8010.2130. 3310. 2170. 4990. 3O80. 3821. 2490. 3010. 2180. 2990. 6481. OOO0. 3460. 3990. 4191. 4480. 2601. 4661. 8670. 2241. 4360. 13O0. 2341. 7280.3660. 2991. 9800. 6131. 3020. 1671. 0000. Ill0. 9970. 2420. 3470. 130

7.TOT1. 271. 19

RATIO1. OO0. 390. 4OO. 4O0. 43O. 410. 40O. 410. 430. 370. 39O. 330. 410. 341. 000.340.340. 370. 320. 380. 39O. 360. 360. 490. 380. 360. 391. OO0. 420. 390. 37O. 340. 340. 390. 390. 370. 330. 360. 290. 390. 330. 310. 340. 390. 330. 381. 000. 330. 370. 390. 370. 31

18756 07 SAMPLE DATA PACKAGE ^ t' u

NO939499969798996061626364696667686970717273747976777879

RET(L)13:2013:2414:0819:0117:0619:2116: 1417:0117:0917:0917.0920: 2918: 1419:2119:2420: 1624:2824:3229:429:346:417:4810: 1612: 2O19:3219: 1910:26

RATIO RRT(L>1. 001. 001.001.001.001. 001. 001. 001. 001.00l.OO1.001. 001.001. 001. 001. 00l.OO1.001. 001. 001. 001. 001. 001. 001. 001. OO

10. 00010. 00010. 00010.00010. OOOIO. OOO10.00020. 00010. 00010. 00010.00010.00010. OOOIO. OOO10. 00010. OOO10.00010. OOO10.0000. 7420. 9480. 8790. 9061. 1180.90710. OOO1. OOO

RATIO0. 100. 100. 110. 110. 100. 090.090. 090. 100. 100. 100. 100.090. 090. 100. 100. 120. 120. 131.06l.OO1.021.010. 981.000. 090.93

AMNT17.18.16.16.4O.19.17.19.18.16.2O.4O.19.16.20.22.16.16.16.19.20.17.18.19.20.19.18.

704O91370028936390399400314783483749929824029987379772

AMNT(L)90.90.90.90.40.9O.90.90.90.90.90.40.90.90.90.90.90.90.90.90.90.90.90.90.90.90.90.

0000000000000000000000000000000000000000OO000000000000

R. FAC R. FAC(L>0. 4380. 4180. 9130.3491. 0000. 9840.2300. 0600.3930.3890. 4241.0000.9790.3960.4910.3920.3960.2860. 3460. 9220. 9680. 1910. 9420. 0990.3990. 4980. 137

1.2361. 1391. 9941.0941. OOO1. 9190. 6960. 192.061. 178. 032. OOO.893.202

1. ISO0.8731.2110. 8661. 0221. 3341. 4030. 4421. 4620. 1720. 9691. 1460. 367

RATIO0. 390.370. 330. 331. 000. 390. 390. 390. 370. 330. 411. OO0. 310. 330. 420. 490. 330. 330. 340. 390. 4O0.340. 370. 320. 41O. 400. 37


in

RIC18/38/89 3:24:88SAMPLE: 1UL SSTD058 NC/UL LOTt2365CONDS.:

COMPUCHEM LABSCOMPUCHEM DATA: HG891838C21 SCANS 356 TO 1856

OUT OF 356 TO 2888

•4_5ra1511 1512

5512 5513

IS13 5515

5514 0311 '. ISM

5516

SSI7

ISi5

ISI6

695 . 1148

1824

1983

1217

1295

1443 1515/, 1715

JLJL198814:59

128817:59

148820:59

168823:59

188826:59

1

a

UJ_ja.•I

inr.

QUANTITATION REPORT FILE: HC891030C21DATA: HC891030C21. TI10/30/89 3:24:00SAMPLE: 1UL S8TD090 NO/UL LOT*2369CONDS. :SUBMITTED BY: 21 ANALYST: 619

AMOUNT-AREA * REF. AMNT/(REF. AREA)* RESP. FACT)RESP. FAC. FROM LIBRARY ENTRY

NO NAME1 *494 D4-1, 4-DICHLOROBENZENE (18*1)2 610 PHENOL (01*3) <108-99-2>3 411 BIS(2-CHLOROETHYL)ETHER (01*9) <lll-44-4>4 601 2-CHLOROPHENOL (01*6) <99-97-8>9 421 1,3-DICHLOROBENZENE (01*7) O41-73-O6 422 I,4-DICHLOROBENZENE (01*8) <106-46-7>7 474 BENZYL ALCOHOL (01*9) <100-91-6>8 420 1'2-DICHLOROBENZENE (01*10) <99-9O-l>9 620 2-METHYLPHENOL (01*11) <99-48-7>10 412 BIS(2-CHLOROISOPROPYL)ETHER (01*12) <39638-32-9>11 622 4-METHYLPHENOL (01*13) <106-44-9>12 442 N-NITROSO-DI-N-PROPYLAMINE (01*14) <621-64-7>13 436 HEXACHLOROETHANE (01*19) <67-72-l>14 440 NITROBENZENE (01*16) <98-99-3>19 *460 D8-NAPHTHALENE (18*2)16 438 ISOPHORONE (02*2) <78-99-l>17 6O6 2-NITROPHENOL (02*3) <88-79-9>18 603 2,4-DIMETHYLPHENOL (02*4) <109-67-9>19 629 BENZOIC ACID (02*9) <69-89-0>20 410 B18(2-CHLOROETHOXY)METHANE (02*6) <111-91-1>21 602 2,4-DICHLOROPHENOL (02*7) <120-83-2>22 446 1-2, 4-TRICHLOROBENZENE (02*8) <120-82-1>23 439 NAPHTHALENE (02*9) <91-2O-3>24 479 4-CHLOROANILINE (02*10) <106-47-8>29 434 HEXACHLOROBUTADIENE (02*11) <87-68-3>26 608 P-CHLORO-M-CRESOL (02*12) <99-90-7>27 477 2-METHYLNAPHTHALENE (02*13) <91-97-6>28 »499 D10-ACENAPHTHENE (18*3)29 439 HEXACHLOROCYCLOPENTADIENE (03*2) <77-47-4>30 611 2. 4, 6-TRICHLOROPHENOL (03*3) <88-06-2>31 626 2, 4, 9-TRICHLOROPHENOL (03*4) <99-99-4>32 416 2-CHLORONAPHTHALENE (O3*9) <91-98-7>33 478 2-NITROANILINE (03*6) <88-74-4>34 429 DIMETHYL PHTHALATE (03*7) <131-ll-3>39 402 ACENAPHTHYLENE (03*8) <208-96-8>36 479 3-NITROANILINE (03*9) <99-09-2>37 401 ACENAPHTHENE (03*10) <83-32-9>38 t609 2. 4-DINITROPHENOL (03*11) <91-28-9>39 607 4-NITROPHENOL (03*12) <10O-02-7>40 476 DIBENZOFURAN (03*13) <132-64-9>41 427 2,4-DINITROTOLUENE (03*14) <121-14-2>42 428 2,6-DINITROTOLUENE (03*19) <606-20-2>43 424 DIETHYL PHTHALATE (03*16) <84-66-2>44 417 4-CHLOROPHENYL PHENYL ETHER (03*17) <7009-72-3>49 432 FLUORENE (03*18) <86-73-7>46 480 4-NITROANILINE (03*19) <100-01-6>


NO474849509192939499969798996O61626364696667686970717273747976777879

NO123496789101112131419161718192021

NAME•467 D10-PHENANTHRENE (IS«4)604 4. 6-DINITRO-2-METHYLPHENOL (04*2) <934-92-l>443 N-NITROSODIPHENYLAMINE (04*3) <86-3O-6>414 4-BROMOPHENYL PHENYL ETHER (04*4) <101-99-3>433 HEXACHLOROBENZENE (04*9) <118-74-l>609 PENTACHLOROPHENOL (04*6) <87-86-9>444 PHENANTHRENE (04*7) <89-01-B>403 ANTHRACENE (04*8) <120-12-7>426 Dl-N-BUTYL PHTHALATE (04*9) <B4-74-2>431 FLUORANTHENE (04*10) <206-44-O>*499 D12-CHRY8ENE (IS*9)449 PYRENE (09*3) <129-00-0>419 BUTYLBENZYL PHTHALATE (09*4) <89-68-7>423 3, 3'-DICHLOR08ENZIDINE (09*9) <91-94-l>409 BENZO ( A) ANTHRACENE (09*6) <96-99-3>413 BIS(2-ETHYLHEXYL) PHTHALATE (09*7) <117-81-7>418 CHRYSENE (09*8) <218-01-9>•497 D12-PER YLENE (IS»6)429 DI-N-OCTYL PHTHALATE (06*2) <117-B4-0>407 BENZO(B)FLUORANTHENE (06*3) <2O9-99-2>409 BENZO(K) FLUORANTHENE (06*4) <207-O6-9>406 BENZO(A)PYRENE (06*9) <50-32-8>437 INDENO(1,2, 3-C, D) PYRENE (06*6) <1 93-39- 9>419 D I BENZO ( A. H) ANTHRACENE (06*7) <93-70-3>408 BENZO(C.H. DPERYLENE (06*8) <191-24-2>*619 2-FLUOROPHENOL (SS«1)«612 D9-PHENOL (S8*2)•447 D9-NITROBENZENE (SS*3)*448 2-FLUOROB I PHENYL (SS*4)*628 2.4. 6-TRIBROMOPHENOL (SS«9)*496 D14-TERPHENYL (SS*6)*471 D10-PYRENE496 1,2,3, 4-TETRACHLOROBENZENE

M/E SCAN TIME REF RRT METH AREA(HOHT)192 471 7:04 1 1. OOO A BB 120292.•94 447 6. 42 1 0. 949 A BB 293816.93 491 6: 46 1 0. 998 A BV 204880.128 497 6: 91 1 0. 970 A BB 201640.146 468 7:01 1 0.994 A BV 221028.146 472 7: 04 1 1. OO2 A VB 239908.108 489 7:16 1 1.030 A BV 110468.146 489 7:20 1 1.038 A BB 214428.108 496 7:26 1 1.093 A VB 149979.49 498 7.28 1 1. O97 A BB 116864.108 909 7:38 1 1.081 A BB 166979.70 909 7:38 1 1.081 A BB 141096.117 916 7:44 1 1.096 A BB 103736.77 923 7:90 19 0.896 A VB 180980.136 984 8:49 19 1.000 A BV 324624.82 943 8:08 19 0.930 A BB 324996.139 991 8:19 19 0.943 A BB 86440.107 999 8: 19 19 0. 990 A BV 134496.122 966 8:29 15 0.969 A W 88048.93 963 8:26 19 0.964 A BB 1846OO.162 973 8:39 19 0.981 A BB 124832.

V i

A7//y) /

AMOUNT40.90.90.90.90.90.90.90.90.90.90.50.9090.40.90.90.9O.90.9O.9O.

OOO000OOOOOOOOOOOO000000OOO000000000000OOOOOO000000OOO000000000

NONONCNCNCNCNCNONCNCNCNCNONCNCNONONONCNCNO

XTOT1. 031. 291. 2929292929

1.291. 291. 291. 291. 292929032929292929

1. 29


NO2223242926272829303132333439363738394041424344494647484990919293949996979899606162636469666768697071727374797677

M/E180128127229107142164237196196162691631921381931841O91681691691492041661381881981692482842661781781492022402021492922281492282641492922922922762782761129982172330244

SCAN981986993602638690749671678683699707729739746792799762767769732791798799803887807809844899879890894943100211411024108311391140114O1144136312171291129913921633163717193714469216898231036

TIME8:428:478:939.019:349:4411: 1310:0310: 1010: 1410:2910:3610:9211:0111: 1111: 1611: 1911:2911:3011.3110:9811:9111: 9811: 9612:0213: 1812:0612:0712:3912:9213:0713:2013:2414:0819:0117: O619:2116: 1417:0117:0917:0917:0920.2918: 1419:2119:2420: 1624:2824:3229: 429: 346:417:4810: 1612:2019:32

REF19191919191928282828282828282828282828282828282828474747474747474747479797979797979764646464646464641119282897

RRT METH0. 999 A BB1. 003 A BV1.019 A BB1.031 A BB1. 092 A BB1. 113 A BV1. 000 A BB0. 896 A BB0. 909 A BV0. 912 A VB0. 928 A BB0. 944 A»BB0. 9680. 9810.9961. 0041. 0081. 0171.0241. 0270. 9771.0961.0691.0671.072l.OOO0.9100.912

BBBBBBBBBBBBBBBBBBBVBBBBVBBBBBBB

0. 992 A BB0. 968 A BB0. 986 A BB1. 003 A BV1. O08 A VB1. 0631. 1301. OOO0.8970. 9490. 9990.9990.9991.0031.0000. 8940. 9480. 9910. 9931. 1991.202

BVBBBBBVBBBBBVBBVBBBBBBVVBBBBBBB

1. 299 A BB0. 788 A BB0. 947 A BB0. 892 A BB0. 919 A BB1. 099 A BB0. 908 A BB

AREA(HCHT) AMOUNT199164.909032.122340.88280.119824.262936.141160.61092.70392.73280.299964.49940.258700.329468.39444.293460.22936.4130O.304932.64664.49676.278792.108096.229772.29440.190196.26420.141940.97604.82972.30968.293896.269780.369343.290468.192884.289476.129444.29080.202838.229104.197293.117008.2768OO.179891.172996.127677.177096.126680.149420.200976.211028.1799O8.298012.30428.189240.

90.9O.9O.90.9O.90.4O.90.90.90.90.9O.90.9O.9O.90.9O.90.9O.90.9O.90.90.90.9O.40.9O.90.9O.90.90.90.9O.90.9O.40.90.90.90.90.90.90.40.90.90.90.90.90.90.90.9O.90.9O.90.90.9O.

000000000000OOOOOOOOOOOO000000000OOO000000000000000000000OOOOOO000000OOO000OOOOOOOOOOOOOOO000OOOOOOOOOOOO000000OOOOOO000000OOOOOO000OOOOOO000000000OOO000000OOO000000OOO

NCNCNCNCNCNONCNONONONONONCNONCNCNCNONONCNONCNONCNCNONONCNONONCNCNCNONONONONONCNONONCNCNONCNCNCNCNCNCNCNCNONONCNC

XTOT1. 291.291. 291. 291. 291. 291. O3I. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291.291. 291. 291. 031. 291. 291. 291. 291. 291.291. 291.291. 291. 031. 291. 29I. 291. 291. 291. 291. 031. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 291. 29


NO7879

NO1234967891011121314191617181920212223242926272829303132333439363738394O414243444946474849909152

M/E SCAN TIME REF RRT METH212 1022 19: 19 97 0. 896 A BV216 696 10:26 28 0.929 A BB

RET(L)7:046:426:466.917:017:047: 167:207:267:287:387:387:447: 908:498:088: 198: 198:298:268:398:428:478:939:019:349:4411: 1310: 0310: 1010: 1410:2910:3610: 9211.0111: 1111: 1611: 1911:2911:3011: 3110: 9811: 91115811: 9812: 0213. 1812: 0612: 0712:3912: 9213:07

RATIO RRT(L). 00.00.00.00.00. 00

1. 001.001.001.001.001. 001. 001. 001. 001.001.001. 001.001. 001.001.001.001.00. 00. 00.00. OO.00

1. 001. 001. 001.001. 00.1.001. 001. OO1.001. 001. OO.00.00.00. 00. 00. 00.00.00. 00

1. 001. 001. 00

10.00010. 00010. 00010. OOO10.00010. 00010. 00010. OOO10. 00010. OOO10.00010. 00010. 00010. 00010. OOO10. 00010. OOO10.00090. 00010. OOO10.00010. OOO10. 00010.00010. OOO10. OOO10.00010. 00010.00010. 00090. 00010. OOO90. 00010. OOO10.00090. OOO10. OCO90.0009O. OOO10.00010.00010. OOO10. 000IO. OOO10. 00090. 00010. 00090. OOO10. OOO10. 00010. 00090. OOO

RATIO0. 100. 090. 100. 100. 100. 100. 100. 100. 110. 110. 110. 110. 110.090. 100.090.090. 100. 020. 100. 100. 100. 100. 100. 100. 110. 110. 100.090.090. 020. O90. 020. 100. 100.020. 100.020. 020. 100. 100. 100. 110. 110. 110. 020. 100. 020. 090. 100. 100. 02

AMNT40.90.90.90.90.90.90.90.90.90.90.50.9O.90.40.90.9O.90.9O.90.90.90.90.90.90.90.90.40.90.50.90.90.90.90.90.90.90.9O.90.90.90.90.90.90.90.90.4O.90.9O.9O.90.9O.

000000COCOCO000000000000000000000000000000000000000000000000000000000000OOOO0000OO00000000000000OO000000

AREA(HGHT) AMOUNT219O03. 90. OOO NC64728. 90. OOO NC

AMNT(L)40.90.90.90.90.90.90.90.90.90.90.90.9O.9O.40.9O.90.90.90.90.50.90.90.90.90.90.90.4O.9O.90.90.90.90.90.90.90.90.90.90.90.90.90.90.9O.90.90.4O.90.90.90.90.90.

0000000000000000000000000000000000000000000000000000000000OO00000000OO0000000000OO00OO000000000000000000

R. FAC R. FAC(L)1.0001. 6681. 3631. 3411. 4701. 9690. 7391. 4260.9710. 7771. 1100.9380. 69O0. 4461. OOO0. 8010.2130.3310.2170.4990. 3O80. 3821.2490. 3O10.2180. 2990.646l.OOO0. 3460. 3990. 4191.4480.2601. 4661.8670.2241. 4360. 13O0. 2341.7280. 3660.2991. 9800.6131. 3020. 1671. 0000. Ill0. 9970. 2420. 3470. 130

l.OOO1.6881. 3631. 3411. 4701. 9690. 7351. 4260. 9710.7771. 1100.938O. 69O0.4461. 0000. 8010. 2130.3310. 2170. 4990. 3060. 3821. 2450. 3010.2180. 2950.6461. OOO0. 3460. 3990. 4151. 4480. 2601. 4661. 8670. 2241. 4360. 13O0. 2341. 7280. 3660. 2991. 98O0. 6131.3020. 1671. 0000. Ill0. 9970. 2420. 3470. 13O

XTOT1. 291. 29

RATIO1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. OO1.001. 001. 001. 001. 001. 001.001. 001. 001. 001. 001. OO1. OO1. 001. 001. 001. OO1. 001. 001. 001. 001. 001. 001. 001. OO1.001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. 00


NO939499969798996O61626364656667666970717273747576777879

RET(L) f13: 20 I13:2414: 0815:0117:0615:2116: 1417:0117:0517:0517:09 120: 25 318: 14 ]19:21 119: 24 ]20: 16 324:28 ;24: 32 325: 42 ;5: 34 36:41 37:48 3

10: 16 312: 20 315:32 315: 19 310: 26 3

IATICL. 00. 00. 00.00.00.00. 00. 00. 00.00

L. 00L. 00L.OOL.OOL.OOL.OOt. 00L. 00L.OOI. OOL.OOL.OOL.OOL.OOL. 00L.OOL.OO

) RRT(L)10. 00010.00010. 00010.00010.00010. OOO10.00020. 00010. OOO10. OOO10.00010.00010. OOO10. OOO10.00010. 00010. 00010. OOO10.0000. 7420. 9460. 8750. 9O61. 1180.90710. 0001.000

RATIO0. 100. 100. 110. 110. 100. O90.090.050. 100. 100. 100. 100.090.090. 100. 100. 120. 120. 131.06l.OO1.021.010.98l.OO0.090.93

AT50.50.50.50.4O.50.50.50.50.50.50.40.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.

INT000000000000OOCO00CO00000000000000000000000000CO000000

AMNT(50.50.90.90.40.50.50.50.50.50.50.40.50.50.50.50.50.50.50.50.50.50.50.50.50.50.50.

L)00000000000000000000000000OO0000OO000000000000OO000000

R.FAC f1.2361. 1351. 5541.0541. OOO1. 5150.6560. 1521.0611. 1781.0321.0001.6931. 2021. 1600.8731.2110.8661.0221. 3341. 4O30. 4421. 4620. 1720. 9691. 1460.367

«.FAC(L)1.2361. 1351. 5541. 0541.0001. 5150. 6560. 1521.0611. 1781.0321. OOO1. 8931.2021. 1600.8731.2110.8661.0221. 3341. 4O30. 4421. 4620. 1720. 9691. 1460. 367

RATIO1. 001. 001.001. 001. 001. 001. 001. 001. OO1. 001. 001. 001. 001. 001. 001. 001. 001. 001. 001. OO1.001.001. 001. OO1. OO1. 001. 00


RIC18/38/89 3:22:88SAMPLE! 1UL SST0888 NG/UL LOT123S6CONDS.t

COMPUCHEM LABSCOMPUCHEM DATA: HI891839C21 SCANS 355 TO 1855

OUT OF 355 TO 2808

IStl 1512 1513 SStS SSt6 1515

SSI2! 5513 5514 0311 ISM SSI7 1516

RIC

693 ..

649 .

798

7! 1149889

I

9421923

19821217

1295

13311635

1444 J326 A 1715A

898Ili59

199914:59

129917.59

149828:59

168923:59

189826:59

r-4in'"4

UJ•-D1XOd0.

aoUJ-jCL

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SAMPLE DATA PACKAGE

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