NUS - US Environmental Protection Agency
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NUS . CORPORATION A MaiiiDunon Company REMEDIAL INVESTIGATION/ FEASIBILITY STUDY REPORT D-31-3-5-1 DRAFT TC-.tt-RI/FS-D(2HV VOLUME IV APPENDICES TYBOUTS CORNER LANDFILL NEW CASTLE COUNTY, DELAWARE EPA WORK ASSIGNMENT NUMBER 07-3L09.0 CONTRACT NUMBER 68-01-6699 NUS PROJECT NUMBER S716 JUNE 1985 0039U rssjfc!|^ww!(easww^««KSM^^ U
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Transcript of NUS - US Environmental Protection Agency
NUS. CORPORATION
A MaiiiDunon Company
REMEDIAL INVESTIGATION/FEASIBILITY STUDY REPORT
D-31-3-5-1DRAFTTC-.tt-RI/FS-D(2HV
VOLUME IVAPPENDICES
TYBOUTS CORNER LANDFILLNEW CASTLE COUNTY, DELAWARE
EPA WORK ASSIGNMENTNUMBER 07-3L09.0
CONTRACT NUMBER 68-01-6699
NUS PROJECT NUMBER S716
JUNE 1985
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NUS PirK Will TwoClllf Mine Road
CORPORATION 412-788-i'oeo
D-31-3-S-1DRAFT
REMEDIAL INVESTIGATION/FEASIBILITY STUDY REPORT
VOLUME IVAPPENDICES
TYBOUTS CORNER LANDFILL .NEW CASTLE COUNTY, DELAWARE
EPA WORK ASSIGNMENTNUMBER 07-3L09.0
CONTRACT NUMBER 68-01-6690
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NUS PROJECT NUMBER S716
JUNE 1985
SUBMITTED FOR NUS BY: APPROVED:
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GEORQE D. GARDNER, P.E. DAVID MaclNTYRE, PEPROJECT MANAGER REGIONAL MANAGER
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ID GOC?'Oi>QA Halliburton Company
. DRAFT
CONTENTS
APPENDICES
H MANUAL WATER LEVEL MEASUREMENTS
I APRIL-MAY 1983 SAMPLING ANALYSIS ANDJAN-FES 19B4 SAMPLING ANALYSIS
J MAY 1984 SAMPLING ANALYSIS
K JANUARY 1985 SAMPLING ANALYSIS
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APPENDIX J
MAY 1984 SAMPUNG ANALYSIS ' '
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MONITORING WELL ANALYSIS
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TYBOUTS CORNER LANDFILL MICROBIOLOGICAL ANALYSES
DRINKING HATER SUPPLIES AND MONITORING. HELLS
004112000198
ft:&'!£• '•
'•,:/•
'^ ^ 8 ^7 s UNITES STATSS ENVIRONMENTAL PROTECTION AGENCY.._' ' \tjiiai'f REOIQiMlllx V, ,.!••" CENTUM, REBIONAL LABORATORY
'""' 939 96STQATS ROAD 39I.!M>!740ANNAPOLIS, MARYLAND 81401 FTS,932'37S2
DATi : June 11, 1384su'SJHCT: tj,1crob1olog1cal Analyses on Drinking Water Supplies and Monitoring Wells
Surrounding Tybouts Landfill, Superfund Remedial, 840502-13 - 22,840503-07 - 22, 840507-10 - 15, 840508-01 -02
FROM : Bettlna B. FletcherpS?Environmental Scientist
TO : Daniel K. Donne!lyCMef, Lab Section
/£-i E. Ramona Trovato'^"Team Leader, Inorganic Section
Samples 840502-13 - 22 and 840503-07 -22 were analyzed for Total Col 1 form,Fecal CoHform and Fecal Streptococcus by the membrane filtration procedure,Membrane filtration Is the method of choice since It provides a directcapture and,count,of organisms present In the sample. However, limitationsto this method .exist 1n the Interferences posed by samples with heavysolids, high color and high background growth. Where these Interferencesare present, samples become difficult and even Impassible to analyze bythe membrane filtration method. When samples were found t'o be unsuitablefor analysis by the membrane filtration (MF) procedure, a resampling wasrequested and further analyses were performed by the Most Probable Number 'Method. The Most Probable Number (MPN) procedure detects and estimatesthe organisms through a tube dilution method using a nutrient-rich mediumwhich Is better suited for examination of troublesome water 'Samples asdescribed above.Samples 840507-10 - 15 and 840508-01 - 02 from the landfill monitoringwells and those drinking water samples evidencing problems with analysisby the MF procedure were analyzed Initially or on resampling by the MPNprocedures for each of the subject organisms. Field blanks were processedfrom each site to detect problems with sample handling procedures.Closely sequentially sampled allquots were analyzed on each of themonitoring wells. Duplicate plantings were performed In the laboratoryon each sample set. Routine quality control procedures were In effectthroughout the analytical series with acceptable performance. . . • .BBFsad ' ' ' ' '"'cc: P. J. Krantz '
QAO, CRL
Sample Description!Lab No.. Description840502-13 Tybouts, Ty-PH-000
-14 Tybouts, Ty-PW-001 ftwORS-»S-15 Tyoouts, Ty-PH-002 foao-15 Tybouts, Ty-PW-003 ""-17 Tybouts, Ty-PW-004 .-18 Tybouts, Ty.-PW-OQ5 •.-19 Tybouts, Ty-PW-006-20 Tybouts, Ty-PW-007-21 Tybouts, Ty-PH-008-22 Tybouts, Ty-PH-009
840503-07 Tybouts, Ty-PW-010-08 Tybouts, Ty-PH-011 OPMATIMI. SCUO-L. &ncn-09 Tybouts, Ty-PW-012 offeMnoa H.'.iivi/i,-10 Tybouts, Ty-PW-013-11 Tybouts, Ty-PW-014 •-12 Tybouts, Ty-PW-015-13 Tybouts, Ty-PW-016 6.C. .. ....14 Tybouts, Ty-PW-017 ttiV6ntK&- ' &&•-15 Tybouts, Ty-PH-018 t_C fJef&MJ ;-16 Tybouts, Ty-PW-019 wo t*s/*MJ . ^-17 Tybouts, Ty-PH-020 KWoifK ' -"•''-18 • Tybouts, Ty-PH-021 uu BStaf
• -19 • Tybouts, Ty-PH-022 TON'S*•20, Tybouts, Ty-PH--21 Tybouts, Ty-PH- _.-22 Tybouts, Ty-PW-Q25
840507-10 Tybouts, Sta. TY-HW-20S-11 Tybouts, Sta. TY-MW-202-12 Tybouts, Sta. TY-MW-201-13 Tybouts, Sta. TY-HW-210-14 Tybouts, Sta. TY-MW-208-15 Tybouts, Sta. TY-W-026
840508-01 Tybouts, Sta. TY-PW-027-02 Tybouts, Sta. TY-PW-028
Pa9e__L-°<_JL_ . .004114
t
is 000200
••\ M NM%#\''r-- : mm :•" " ' m*t:..'.}t:
MF MethodTotal Conform Fecal Col 1 form Fecal Streptococcus
Organisms Organisms OrganismsLab No. Par 100 mL _ Per 100 mL . Per 100 ml
<1 s*Invalid Sample Due to Heavy Solids - ResampleTNTC with 45 <l. <1total conformorganisms
19jae 3 of,OCOT
$fr..
.„-10 <1 <1 N*
-11 <1 <1 "' .. <1-12 ; <i <i • • • • < ! • •-13' • <1 ' . ' .<! ' <1-14 <r <i <i-15 <1 <1 <1 • ' •-16 <1 <1 <1-17 <1 <1 <1-18 <1 <1 1-19 <!** <1 <1-20 10*** <1 <1-21 <1 <1 1
. • MPN Method '
840507-10 9 <2 30-11 80 <2 1000-12 29 5 340-13 ' 6 <2 290 .
..v.;:S. -14 ;../'•..'. <3 'i..:''••"••...'. <2 ,'• .•-•••'• 160.'••" .•IS.'" "2 <2 ' 19
840508-01 ,4 <2 20 If?-02 <2 ' <2 <2 . **''
TNTC • Too Numerous To Count*Sol1ds • Orange 1n color and very heavy - Difficult to analyze by membranefiltration. Recommend resampling and analysis by the tube methods
"Background growth questionable - suggest resampling to be run by MPN, also _4<cStandard Plate Count , 00411"
***Background growth present - Significance Undetermined
\- DRAFT
ii
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t• APPENDIX K H';
'JANUARY less SAMPUNQ ANALYSIS
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UNITED STATES ENVIRONMENTAL. PROTECTION AGENCYREGION III
CENTRAL REGIONAL LABORATORYSM flBSTOATB ROAD
ANNAPOLIS, MARYLAND 81401
DATE i February 7, 1985SUBJECT: Tybouts Corner: Hater Samples for VOC Analysis by GC/MS
Superfund Remedial 5TFA03RH09, (1/17/85 - 1/29/85), 850117-01 - 08;850118-01 - 06; 850122-01 - 08
FRO'M ; R1ck Drelsch-. Chuck SandsChemist "p Chemist
TO ! Daniel K. DonnellyChief, Annapolis Lab
THRU : John Austin MTeam Leaders/Organic Analysis Section
The above samples were analyzed'for volatile organic compounds amenable tothe purge and trap technique and Identifiable by GC/MS. The nominaldetection limit for all runs was l.ppb (ug/L).
a blank. Each shipment .should have had a representative blank. The analyseswere'performed despite this error. ' .Samples 850117-01, -06; 350118-02.- 06 and 850122-01 - 03, -OS, -06 exhibitedno reportable volatile organic compounds.
OA SummaryAverage S Recovery
1/17 1/22 1/24 1/24
Bromochloromethane 106 t 5 103 + 11 109 * 9 114 * 10l,4-D1chlorobutane 112 t 1 102? 9 117 ~ 13 1017 7para-Bromofluorobenzene 10478 10778 110 710 9676
n «
RD:adcc: P. J. Krantz, OAO
Diana Plckens
00411?
1 la 000204
if-''il:
ifet.
itiThe .samples arrived In three sepirate shipments. Only one shipment contained ,' •fevl
xiAWwa../. nz"5 3/ii»i"»i-iir-UNITED STATES ENVIRONMENTAL, PROTECTION AGENCY
flEQION IIICENTRAL REGIONAL LABORATORY
"""" 333 8ESTQATB ROAD JOI'234,2740ANNAPOLIS, MARYLAND 81401 FT5'9JW73Z
DATE : February 13, 1986SUBJECT: Tybouts Dat, RepoPt5 •
FROM : Daniel K. Donnelly (3ES21)9''"i?Chief, Annapolis Lab
TO : Abraham Ferdas (3HH21)Site Response Section
Enclosed are 4 of the Tybouts organlcs data reports. They are for:
1. Volatlles2. Extractables3. PCB/Pest1ddes4. Chlorides and 1^3
There 1s one PCB/pest1cide, report remaining and 1t should be 1n the mall. by about the 20th.. • . ' . l ...A.. , • par
•DKD'sad . ' . . ' . ' • . ' . &.'
Enclosures'a/s
%•
MS:
0041131000203 I1
JA
Samp1enDeser1pt1on!850117-01 Tybouts Corner Landfill, Location 13, TY-GH-119A
•02 Tybouts Corner Landfill, Monitoring Hell 1105, TY-GH-105-03 Tybouts Corner Landfill, Location 13, TY-GW-119B-04 Tybouts Corner Landfill, Location 13, TY-GH-119B-D-05 Tybouts Corner Landfill, Location 14, TY-GM-120B-06 Tybouts Corner Landfill, Location 14, TY-GH-120A-D•07 Tybouts Corner Landfill, Location 14, TY-GH-120A•08 Tybouts Corner Landfill, Monitoring Hell 1205, TY-GW-205
850118-01 Tybouts Corner Landfill, Lab + Trailer 81k., TY-GH-OQO-02 Tybouts Corner Landfill, Location 17, TY-GH-122-03 Tybouts Corner Landfill, Location 16, TY-GH-118A-04 Tybouts Corner Landfill, Location 16, TY-GH-118B-05 Tybouts Corner Landfill, Location 16, TY-GH-11BB-D-06 Tybouts Corner Landfill, Location 15, TY-QH-117A
850122-01 Tybouts Corner Landfill, Location II, TY-GH-121A•02 Tybouts Corner Landfill, Location II, TY-GM-121B-03 Tybouts Corner Landfill, Location 12, TY-GH-116A•04 Tybouts Corner Landfill, Location 12, TY-GH-116A-D•05 Tybouts Corner Landfill, Location 12, TY-GW-llfiB•06 Tybouts Corner Landfill, Location 15, TY-RH-117B•07 Tybouts Corner Landfill, Location 12, TY-GH-116C-08 Tybouts Corner Landfill, Corner of Bean Field, TY-GH-114
Page 2 of 6QQ4119
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-, «ilA .UNITED STATES ENVIRONMENTAL. PROTECTION AGENCY
REGION III'*, ..I?' CENTRAL REQIONAL LABORATORY"*>" 839 BE8TOATE ROAO 30M24-2740
ANNAPOLIS, MARYLANO 21401 FTM8J.3TS!
DATE : February 7, 1985SUBJECT! PCB/Pest1dde Results for Tybouts Corner Landfill
Superfund Remedial, 850117-01 - 08 and 850118-01 - 06FROM ! James Barren §& • Gregory Rodgers^j/f.
Chemist j ChemistTO , : Daniel K. Donnelly
Chief, Annapolis LabTHRU : John Austin/^
Team Leader/Organic Analysis Section
Two sets of samples were received for PCBs and Pesticides, as noted below.No pesticides or PCBs were noted at the levels attached. 01 butylChlordenate was added as a surrogate. Matrix spikes were also run asattached. Matrix spike duplicate sample 850118-05 MSD was lost, however
• since.the samples were run. as a set It was felt sufficient AQC data was•• provided with three'spikes. ' • ,Sample Description and Results;Lab No. Description Results
cc: P. J. KrantzQA Officer
0002.10
P
Tybouts Corner Landfill, Location 13, TY-GW-119A N.D.d)Tybouts Corner Landfill, Monitoring Well 1105, TY-GW-105 N.D.Tybouts Corner Landfill, Location #3, TY-GH-119B N.D.Tybouts Corner Landfill, Location *3, TY-GW-119B-D N.D.Tybouts Corner Landfill, Location 14, TY-GH-120B N.D. ;.,Tybouts Corner Landfill, Location 14, TY-GW-120A-D N.D. ';Tybouts Cornar Landfill, Location 14, TY-GH-120A N.D. |.';Tybouts Corner Landfill, Monitoring Hell #205, TY-GH-205 N.D. h,Tybouts Corner Landfill, Lab + Trailer Blk., TY-GW-000 N.D. b*Tybouts Corner Landfill, Location #7, TY-GH-122 N.D. pi;'Tybouts Corner Landfill, Location 16, TY-GH-118A N.D. : ,Tybouts Corner Landfill, Location 16, TY-GH-11BB N.D. !;.,Tybouts Corner Landfill, Location #6, TY-GH-118B-D N.D.Tybouts Corner Landfill, Location 15, TY-GH-117A ' N.D. U
N.D. • None Detected f:'/..(ilSee attached Detection Limits. • [v
!'•"''JB/GR':ad ('••.'
Surrogate % Recovery - D1butyl ChlordenateLab No. ' Recovery
114.086.057.088.097.0119.079.0131.0132.0120.0128.089.0130.0100.4
850117-04 .USD 48.0850117-04 MSD-2 78.0
850118-05 MS 117.0 '850118.05 MO . L.A.
Matrix Spikes . . 850117-04' 850117-04 850117-04 . MS, MSD 850118-06
MS' % MSD * , ReL.X MSCone, ng Cone, ng Recovery Cone, ng Recovery Difference Cone, ng
Page_J_of 2_
0002.U
ff
iLlndane 0.05 0.034 68.0 0.047 94.0 31.0 0.04 &Heptachlor 0.05 0.033 66.0 0.047 94.0 35.0 0.044Dleldrn 0.105 0.067 63.0. 0.1Q6 100.3 45.0 0.098Endrln 0.209 0.133 64.0 0.217 103.8 48.0 0.93DOT 0.2Q3 0.1Q9 54.0 0.219 108.0 62.8 0.20
\-f#£
Detection Lialca*Low water6 Low Soil/Sedlaent'
____Pea t iej.de s__________GAS Number_____ug/L_______yg/Xg______
104. nlpha-BHC 319-84-6 0.05 2.0105. bata-BHC 319-85-7 0.05 2.0
106. delca-BHC 319-86-fl 0.09 2.0107. gaana-SHC (Lindane) 58-89-9 0.05 2.0108. Hepcachlor 76-44-8 0.05 2.0109. jUdrin 309-00-2 0.05 2.0110. Hepcachlor Epoxide 1024-57-3 0.05 2.0
Ul. EndoauUan I . 959-98-8 0.05 2.0112. Dieldrin . 60-57-1 0.10 4.0113. 4,4'-DDE • 72-55-9 0.10 4.0114. Endrin 72-20-8 - 0 . 1 0 4.0115. Endooulfan II 33213-65-9 0.10 4.0
116. 4,4'-DDD . 72L54-8 0.10 4.0117. Endrin Aldehyde 7421-93-4 ' 0.10 4.0118. Endoiulian Sulface 1031-07-8 0.10 4.0U9.'4,4'-DDI 50-29-3 0.10 • 4.0120..Endrin KBton* 53494-70-5 . ,0.10 4.0
121. MMhoxyctdor ' ' 7?-43-5 0.5 • 20.0122. Chlordane ' 57-74-9' '0.5 20.0123. loitaphene • 8001-35-2 1.0 40.Q124. AROCLQR-1016 12674-11-2 0.5 20.0125. AHOCLOR-1221 11104-28-2 0.5 20.0
126. AROCLOR-1232 11141-16-5 0.5 20.0127. AROCLOR-1242 ,(>3469-21-9 0.5 20.0128. A80CLOR-124B 12672-29-6 0.5 20.0129. AROCLQR-1254 11097-69-1 1.0 40.0'130. AROCLOR-1260 11096-S2-5 1.0 40.0
"Medium Mater Contract Required Detection Liotcs (CRDL) for PeaclcidR HSLCompounds are 100 tines the individual Low Hat.r CROL.
^Mediua Soil/Sediment Contract Required Detection limits (CRDL) for PesticideHSL compounds are 60. tines the individual Low Soil/Sediment CRDL.
•Detection Units listed Cor noil/sedlnenc arc based on wet weight. The.detec-tion limits calculated by the laboratory foe soil/sediment, calculated on dryweight basis, as required by the contract, will be higher.
** Specific detection Halts are highly matrix dependent. The detectionHalts listed herein are provided for guidance and nay not always beachievable.
C-6 10/84 Rev
. Jfc 0002,12
m
UNITED STATES ENVIRONMENTAL PROTECTION AOENCY is, '«RK1IONIII \ Sife '
CENTRAL RCOIONAL LABORATORY feviii» B68TQATE ROAO 901.2244740 Ir <
ANNAPOLIS, MARYLAND 21401 FTS.J2J.ar821 ,;
DATE : February 13, 1985SUBJECT; Tybouts Corner Landfill Analyses for Chloride and NHa .
Superfund Remedial, 850117-01 - 08; 850118-01 - 06; 850122-01 - 0811 £&FROM • Norman Frltsche /W- D1ane S1ms *&
Environmental Scientist Laboratory Scientist ;£X
TO : Daniel K. Donnelly \$*Chelf, Annapolis Lab l:?;;v
Received 22 samples from Tybouts Corner Landfill for chloride and NH3analyses.Sample Description!Lab No. Description850117-01 Tybouts Corner landfill, Location 13, TY-GH-119A
-02 Tybouts Corner Landfill,. Monitoring Well #105, TY-GH-105-03 .,Tybouts Corner Landfill* Location 13, TY-8H-1WB•04 , Tybouts Corner Landfill, Location 13, TY-GH-119B-D .-05 Tybouts Corner Landfill, Location 14, TY-GH-120B .-06 Tybouts Corner Landfill, Location 14, TY-GH-120A-D-07 Tybouts Corner Landfill, Location 14, TY-GH-120A-08 Tybouts Corner Landfill, Monitoring Hell 1205, TY-GM-2Q5
850118-01 Tybouts Corner Landfill, Lab + Trailer Blk., TY-GH-000-02 Tybouts Corner Landfill, Location 17, TY-GH-122-03 Tybouts Corner Landfill, Location 16, TY-GH-118A-04 Tybouts Corner Landfill, Location 16, TY-GH-118B-05 Tybouts Corner Landfill, Location #6, TY-GW-llSrD-06 Tybouts Corner Landfill, Location #5, TY-GM-117A
850122-01 Tybouts'Corner Landfill, Location #1, TY-GH-121A-02 Tybouts Corner Landfill, Location II, TY-GH-121B-03 Tybouts Corner Landfill, Location 12, TY-GM-116A-04 Tybouts Corner Landfill, Location 12, TY-GH-116A-D 3f•05 Tybouts Corner Landfill, Location 12, TY-GH-116B•06 Tybouts Corner Landfill, Location 15, TY-GM-117B-07 Tybouts Corner Landfill, Location 12, TY-GH-116C-W£ Tybouts Corner Landfill, Corner of Bean Field, TY-I
Additional quality control data are available upon request.NF/DS:adcc: P. J. Krantz
QAO, CRL
1500021-3
Results for Tybouts Corner Landfill!Lab No. Chloride (mg/L)
2.62 .041369 . 160 + .03
"6'.39 (77X) " •"• ' .U55 "6.24 .0413.74 • <.022.48 .0422.48 .039 + .001 (107S)254 90 + 701 (92X)1.63 " 7030
2.08 + .09 (85*) <.02* (116%)1.02 .07450.3 " . ' " .02046.1 .026 "~3.41 .133 '38.6 ,088'3'.29 """"" " " .098 '
.099 ""•.082 + .007 (935)
"" " . """ .1T2 _.__,„.._._..... «Mo——...... no+.or •;;;—
^Samples analyzed 1n duplicates, both values below detection Units.
Page..
000214
,•«*;.\&Pi?.
I
:tf a:lfifi.___•:'•. »'.*«&tM*'A ;;$P°;->
,V\(mj\-XUNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REdlQN IIICENTRAL REGIONAL LABORATORY
M»BE3TOATEROAO 301.224.2740ANNAPOLIS, MARYLAND 21401 IT8.922.37S2
DATE ! February 13, 1985SUBJECT: GC/MS Analysis of Tybouts Corner Landfill
Superfund Remedial, 850117-01 - 08; 850118-01 - 06; 850122-01-08
FROM i John Aust1n>Jp,UQt ' Joseph L. Slayton *V_»Chemist w C V Chemist 0
TO •. Daniel K. DonnellyChief, Annapolis Lab
The samples were examined for the presence of organic compounds listed asextractable Priority Pollutants and Hazardous Substance List Compounds,using fused silica capillary column/gas chromatography/mass spectrometry.Concentrations of these compounds were determined using the relativeresponse,of authentic standards to the Internal standard.The samples were also examined for the presence of compounds 1n additionthose on the priority pollutant 11st. Tentative Identification of'these•compounds was made on the comparison of sample spectra to the EPA/NIHMASS Spectral Library. Concentrations for those compounds were estimated
. _ based on the response of the Internal standard. 'All sample extracts have been corrected for any blank contamination.
JA/JS:adcc: P. J, Krantz •
QAO, CRL
004129
1
Sample Description!850117-01 Tybouts Corner Landfill, Location 03, TY-GH-119A
•02 Tybouts Corner Landfill, Monitoring Hell 0105, TY-GW-105•03 Tybouts Corner Landfill, Location 03, TY-GH-119B-04 Tybouts Corner Landfill, Location 03, TY-GH-119B-D-05 .Tybouts Corner Landfill, Location 04, TY-GM-120B•06 Tybouts Corner Landfill, Location 04, TY-GH-120A-D •-07 Tybouts Corner Landfill, Location 04, TY-GH-120A-08 Tybouts Corner Landfill, Monitoring Hell 0205, TY-GH-205
850118-01 Tybouts Corner Landfill, Lab + Trailer Blk., TY-GH-000-02 Tybouts Corner Landfill, Location 07, TY-GH-122-03 Tybouts Corner Landfill, Location 06, TY-GH-118A-04 Tybouts Corner Landfill, Location 06, TY-GH-118B•OS Tybouts Corner Landfill, Location 06, TY-GM-118-0-06 Tybouts Corner Landfill, Location 05, TY-GH-117A
850122-01 Tybouts Corner Landfill, Location 01, TY-GH-121A•02 Tybouts Corner Landfill, Location 01, TY-GH-121B•03 Tybouts'Corner Landfill, Location 02, TY-GH-116A-04 Tybouts Corner Landfill, Location 02, TY-GH-U6A-D•05 Tybouts Corner Landfill, Location 12, TY-GH-U6B-06 Tybouts Corner Landfill, Location 05, TY-GW-117B-07 Tybouts Corner Landfill, Location 02, TY-GH-116C•08 Tybouts Corner Landf1.ll, Corner of Bean Field, TY-GH-114
Page 2 of 0041.30
j 000216
Region IIICentral Regional Laboratory
(intractable Organlcs Analysis Data SheetSample No. Lab Blank
Units: Hater • ug/LSoil • mg/kg (wet)
Senvlvolatlle CompoundsActual Detection Limit • ( 1 ) x NDL
IUL
>-.
,11
,U111
CASNumber62-75-8108-95-262-53-3'1U-44-V95-57-ti541-73-1'106-46-7. ..00-51-6
• *
:u
.0oLU
ill;illI 1 11lu'11111 "111I"3uT111I."
95-50-195-43963106-
3-1l-.i.D4-5
621-64-767-72-198-95-378-59-188-75-5105-67-965-85-U111-91-1120-83-212Q-B.-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-7BB-74-4131-11-3
10 208-96-8: &-03-2 ..
N-N1 trosodlmethyl ami nePhenolAnlbis
neZ-Chloroethyl (Ether
2-Chl orophenol,-•T*"enz,_-
"-•Met
) cil orobenzene) ci orobenzenei A conoi)• ch orobenzenehyl phenol
b1s(2-chlorolsopropyl J.theri •ie• W1exaikn
hyl phenolro-01-n-Propylam1ne.hloroethanebenzene
"Isopnorone2-Nlt2,'-l
~Eenzc~~iftt
rophenol1 methy)1c Ad
1 phenold
^Ci oroethoxvlMethaneici orophenol
1,.,4-TrcmorobenzeneNapht2f-Oi
haleneoroanmne
exachlorobutadlene~4-Chl oro-3-Metfiyl phenol2 -MetHexac
nyi naphthaleneiloroc
2,4,6-Trtch2,4?5-Tr1tf
'dopentadleneorophenolorooneno
2-Chloronaphthalene2-N1troanll1neDimethyl PhthalateAcehapnthy3-Nltroanl
eneIne
•'
NDL
10bllbll111111I)UU
bllbll111111111bll111.11II1111bll1111112 11111111111111111,11UD,0111
CAS 'Number
83-32-951-28-5100-02-7132-6121-1
4-9* -I
606-20-284-66-270.5-7Z-386 7!100-0
-71-b
543-52-186-30-6101-55-3118-74-187-8685-0;120-
-b-8
Acenaphthene2.4-D1n1trophenol4-N'ifroi01 lenzp2, 4-D2,'6-DDiet•4-Cl
nn
henolurantrototroto
ueneuene
ylphthaiateoronhenyl-phenyietner
Fluorene4-N1troan1llne' ,6-oinltro-2-MethyN-N1trosod1phenylam4-Bromophenyl
phenolne(l)
•phenyl etherHexachlorobenzene'entachloropnenol'henanthrene
2-7 Anthracene84-74-2206-44-092-87-5129-QO-O85-68-79b,-94-15-55-3
"T17-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70•31 51 -24-2
(D
D' -n-Butyl phthalate• uoranthene!enz1d1nePyreneButylberizy'lpn3,j"-DlctiloroEenzo(a)Antb1s(2-EthylChrysene01-n-Qctytenzolenzo
i, t
Benzol aF'
:halate3enz1d1ne
iraceneiexy)PhthalatePhthalateuorantheneuoranthene
^reneIndeno(lj2.3-cd)PyreheD1banz(a,h)Anthrace.na^Benzofq,h 1 ttftftteJA
' Cannot be separated
•
.31
from dlphenylamlneNDL • Nominal Detection Limit IL
, .••'•'.'I; '
V ,
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850117-01
Units: Hater • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
NDL
IUill
1I
111"1. r111111
1J
111"1
1IUIII
1.J111
10I I I
1IUId
Jn
CASNumber62-75-8108-95-2'62-53-34111-44-495-57-8541-73-1IU6-4(J-/,00-51-695-50-195-4839631
-7-32-9
106-44-5621-64-767-7298-9578-59
-1-3-1
88-75-5105-67-965-85-011-91-120-83-220-62-191-20-3106-47-887-6659-5091-57
-3-7-6
77-47-488-06-295-95-491-58-788-74-4
u 131-11-3°. "Q8-9
J9-09
NDI. "
O-ti-2
N-N1trosod1methy1am1nePhenol
ThT 'bis 't2-C 11,3-1.4-Benzj1.2-1
ne•Chloroethyll.therorophenolITcf1ci
•A•ch
1 orobenzeneorobenzenecoitol
l orobenzeneZ-Methyl phenolb1 s (2-chl orol sopropy l l-ther4-Met'-Nit
hylro-
&henol1-n-Propylamlne
•exachloroethaneNitrobenzeneIsophorone2-Nltroohenol2,4-1;Benzo
methylphenolc Acid
b1s(2-Ch2,4-Dlch1,2,4-Tr
oroethoxy Methaneorophenolchlorobenzene
NaphthaTene3-ChloroanmneHexacniorobutadlene4-Chloro-3-Methylphenol2-MetHexac2.4.0
lylnaohthalenei procyclopentac-Trichioropneno
2,4,5-irlcnioroonenolene
.-Chloronaohthalene2-N1troan111neDimethyl PhthalateAcenaonthylene3-Nitroanlline
,
Nominal Detection Limit
NDL
10allbll111
in1111bllbl)I)11
111bll11.011
111bll111111dllU1111U11
111111u.u111
CASNumber83-32-951-28-500-02-732-64-921-14-2606-20-284-66-270U.-7Z-386-73-7100-01-6543-52-186-30-6101-55-3,18-74-187-85-5. 85-01-8120-12-784-74-2' 206-44-082-87-5129-00-0B5-68-791-94-156-55-31 7-81-72, 8-01-91 7-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenanhthene2,4
~~i -1-01n1trophenolItropnenol
JTbenzofuran~2,4-0' l2.6-lT
Urotolr troto
ueneuene
Di ethyl phthalate4-Chl oropneny l -phenyi etnerFluorene~jI -N1troan1l1ne,6-Dln1tro-2-Methy
~N-N1trosod1pnenylam~~iphenolne(l)
-Bromophenyl -phenyi etherexachlorooenzene'entachloropnenol'henantnreneAnthracenenI n-Butyl phthalateuorant heneenzldlneyreneutyl benzyl phthalate,3'-D1chlorobenzldlne
~Benzo(a)Anthraceneb1 s ( 2-Ethy 1 hexy ) Phthal ateChrysene
~lH-n-Octy Phthalatelenzol
"BenzoBenzo iIndenoUibenz
• uorant1 uorant
leneiene
'yrene,,2.3-cd)Pyrenea.hiAnthracene
Benzo(g,h.1)Pervlene(1) •• Cannot be s
"Not detected afterblank.
eparated fromcorrectloirtl
»
dlphenylamlne
'pi
Page 4 of 32_
is .0002.1.8__.._.......
Region IIICentral Regional Laboratory
Extra-table Qrganlcs Analysis Data SheetSample No... 850117-02 __
Units: Mater - ug/LSoil • mg/kg (wet)
Semi volatile Compounds' Actual Detection Limit • ( 10 ) x NDL
IDL
,u,11
11
.1]1 f\
,Lf,U
.11
,U,11
. w
.U
.U,n
. w,ll
>Ll
9.U.l)_I
CASNumber •
62-75-8108-95-262-53-34 •111-44-495-57-8541-73-1"06-46-7iflO-bl-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47 '438-06-295-95-491-58-788-74-4131-11-3"'08-96-8-J9-09-2 ,
N-N1trosod1methylam1nePhenolAnilineb1s(2-Chloroethyl)Ether2-Chlor1,3-01 C1.4-D1CBenzyl1.2-U1C
ophenoltil orobenzenetil orobenzeneAlcoholhi orobenzene
2-Methyl phenolb1 s (2-chlorol sopropyl (Ether4-Methyl phenolN-N1tro-D1-n-PropylamlneHexachloroethaneNitrobenzeneIsophorone2-Nltrophenol2,4-DlmethylphenolBenzole Addbis(Z-C2,4-01c
hloroethoxylMethanehi orophenol
1 , 2 ,4-Tr1 chl orobenzeneNaphthalene3-Chloroan1l1neHexachlorobutadlene4-Chl oro-3-Metnyl phenol2-MethyHexachl2.4.6-T
1 naphthaleneorocyclopentadlener1 cm orophenol
2,4,5-Trlchloropnenol2-Chloronaphthalene2-Nltroani lineDimethyl PhthalateAcenaonthylene•3-Nitroanillne
,
544
34
NDL
10MbllID111111111111IUbllbll111IU111bllIUIUIUIUblJIUIU.uIU111IUIUIUIUIUIUIU111
CASNumber83-32-951-28-5100-02-7132-64-9121-14-2606*20-284-6..Z7005-7.-3B6-/.-7100-01-6543-52-186-30-6101-55-3118-74-187-86-585-01-812U-12-784-74-2206-44-09Z-tJ7-5129-QO-O85-68-791-94-156-56-3117-81-7218-01-9117-84-0205-99*2207-08-9DO-32-8193-39-553-70-3191-24-2
Acenaohthene2,4-olnltroohenoi4-mtrophenolOlbenzofuran2,4-D1n1trotoluene2,6-D1n1trotoluene01 ethyl phthai'ate4-Ch l oronheny l -phenyi etnerFluorene4-Nltroan1llne4 ,6-01 n1t ro-2-Methyl phenolN-N1trosod1pnenylam1ne(l)4-Bromoohenyl-onenyletherHexachl orobenzenePentachloropnenolPhenanthreneAnthraceneD1-n-Butyl phthalateFl uorantheneBenzldlnePyreneButylbenzylphthalate3,3'-DlchlorobenzldlneBenzo(a)Anthracenebi s ( 2-Ethyl hexy ) Phthal ateChrysene01-n-Octyl PhthalateBenzo b Fl uorantheneBenzo k Fl uorantheneBenzo a PyreneIndenol ,2.3-cdlPyreneDlbenzla .hiAnthracene
,M_,
K
Benzolg.n.l IPerylene i(1) • Cannot be separated fr<ft@*|fe&«>i1>ine
, , . •- , . , *Not detected after correctl6rTfor laboratory ["NDL • Nominal Detection Limit blank. ' \
'oiW-
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850117-03
Units: Hater • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
IUL
, .
.11'1i
111r
iU
LUIII
.uIU1IUI I I .;luLU1LU1"I •3UIU1.'lu
CASNumber62-75-8108-95-262-53-34111-44-495.57.8541-73-1106-46-/100-51-695-50-195-4396!
8-78-32-9
106-44-5621-64-y67-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-4)1-11106-87-6
2-1-3 '7-8-3
59-50-791-57-6177-47-488-05-295-95-491-58-788-7131-
-41-3
206-96-815-09-2 ,,
N-N1trosod1methy1am1nePhenolAn1 inebis 2-Ch
, 2-Chion.3-01C
~1T4-0'CBenzy J
,2-D' Ct
loroethyl (Etherhenolorobenzeneoro lenzenecohoiorobenzene
~2-Methyl phenolb1 s ( 2-ch 1 orol soprppy l ) Ether4-Methyl PhenolN-N1 tro-bl -n-Propyl ami neHexachl oroethaneNitrobenzeneIsophorone2-Nltrophenol2, 4-0' meBenzo cb1s(2-Ch2,4-01chl,2,4-Tr
thy) phenolAddoroethoxy (Methaneoroonenolchlorobehzene
Naphthalene3-Chloroamnne
~Fi exachlorobutadlene•Chloro".-MethylHexach o2,4,6- r2,4,5-Tr
-3"Methylphernaphthalene
Ol
roc;'dopentadlenec"i oroph'eno1cn oropnenol
2-Chloronaphthalene2-N1troan1l1ne •Dimethyl Phthalate
"^cenaprit'nylene3-N1troan1l1ne
NDL
10bUbUIU
LUI)bUbllIUIUIUbU.U.,11u111bULULU2(1UULULuLI
,,uLuLULU
CASNumber83-32-951-28-5100-02-7132-64-9121-14-2606-20-28'/I-66-2Ob-72-3
•S.-73-7• 100-01-6543-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791-S4-156-55-3117-81-721LJ8-01-97-84-0
205-99-2207-08-950-32-8193-39-553-70-3191-24-2
(D •
Acenaphthene2,<-D1n1trophenol4- itroonenol01 >enzofuran2,4-H.,6-)Ti
r trotov troto
ueneuene
Jlethyl phthalate .•Chl oropneny 1 -phenyi ether
"Vluorene.-NttroanlUne,6-D1n1tr'o-2-Methy•Nltrosodlphenylam-Brombphenyl-pneny
phenolne(l)ether
exachl orobenzeneentachloronhenol
"PhehanthreneAnthraceneD1-n-8utyl phthalateFl uorantheneIenz1d1ne'yreneiutyl ie
"i '-l1nzyl phthalatechlorobenzldlne
len'zo(a)Anthracene>1s(2-Ethylhexy)PhthalateChrysene01-n-OelenzoBenzoBenzo a
ty Phthalate" F uorant
•1 uorantienelene
) 'yreneIndeno(l,2.3-cd)Pyrene)1benz(a,h)Anthracene'6nzo(g,n,1 (Perylene
Cannot be separated from
.
K
dlphenylamine*Not detected after correiQ04-?34aboratory
NDL • Nominal Detection Limit blank vv-_*
Region IIICentral Regional Laboratory
Extractable Organic: Analysis Data SheetSample No. 850117-05
Units: Hater « ug/LSoil • nig/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
iDL
3II
ID'UUiUIU0IU'Uu10LUU
.11IUIIj1(1
IIIIIJIU
IIJ
LU"II
3ULU
1i
LU"7
CASNumber
62-75-8108-95-262-53-34111-44-495-57-8541-73-106-46-700-51-695-50-195-48-7•39638-32-9106-44-5621-64-767-72-19i)-95-37B-59-188-75-5105-67-965-85-0111-91-120-83-220-82-191-20-3106-487-6i
7-8-3
59-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-U-3208-96-8.99-09'-2 .
N-N1trosod1methy1am1nePhenolAnilineb1Tf2-Chloroethyl (Ether2-Chl orophenol1.3-D1,4-Dflenz:1,2-2-Me
•chlorfctf
Ach
oro lenzenei lenzene
coholorobenzene
hyl phenolbls(2-chloro1sppropyl (Ether4-Methyl-Nltro-t
HexacN1tro
JhenoliT-'n -P ropy 1 ami ne
hloroethanelenzene
Isophorone2-N1trophenol2,4-Qienzcbls(2
•metnylphenol• c Acid•CRI
2 -01 ch1.2,4Nap it3-Ch!
oroethoxy (Methaneorophenol
-f rich 1 orobenzenefialeneoroanlllne
Hexachl orobutadleneWHiloro-l-2 -MetHexac2,4,6
hylnaphi oroc•Tr
2,4,5-TrlCIch
ethyl phenolthaleneclopentadleheorop'hlnoorooheho
S-J'hloronauhthalene2-N1troan1l1neDimethyl PhthalateAcenapncnylene3-lm roam line
NDL
10bUbULUUI)
i1)11IUbUblIUIUIUbULUUULUbULULU,iUUILULUUUIUIULULU
CASNumber83-32-951-2100-132-
3-bI.-/W-tl
121-14-2606-20.-284-66-2~7005-7Z-36-73-7100-01-6543-52-186-30-6101-55-3118-74-187-86-585-0120-
-U.-I1
84-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
(1) • Ci
Acenaphthene2,4-Dlnltropnenol4-NltroohenolDlbenz2.4-D12.6-11
"lie ; ly4-C ilo
>"urann1 trotom troto
ueneuene
phthalate•ophenyl -phenyi ether
•Fluorene4-NltroanHlne4,6-oln1trb-2-Methj;lRhenolN-N1tr'6sod1phenylam4-Bromophenyl-pheny
ne(l)ether
Hexachl orobenzenePentachl orophenolPhenantnreneAnthraceneDI-n-Butyl phthalate•1 uoranthenelenziainePyreneButyl benzyl phthalate3,3'-D1chlorobenzldlneBenzo (a (Anthraceneb1s(2-Ethylhexy)PhthalateChryseneD1-n-0cty PhthalateBenzoBenzoBenzoIndeno
) F uoranthenet • uoranthenej 'vrene,,2.3-cd)Pyrene
Dibenzla.nlAnthraceneBenzo ( g., n.DPery lene
nnot be separated tr
u
oixM phenyi ami ne*Not detected after cMceatlw •for laborator>
NDL • Nominal Detection Limit blank.of 32
Region IIICentral Regional Laboratory
Extractive Organlcs Analysis Data SheetSample No. ..850117-06
Units: Hater • ug/LSoil » mg/kg (wet)
Semi volatile CompoundsActual Detection Limit « ( i .. ) x NDL
NOL
).JIU"Jj
lUr
LU"1yLUHIJ
.JIU
JI
IU"II
LllLU1
. Ilu
3UIU..10 '
CASNumb ftp
62-75-8108-95-262-53-34111-44-495-57-8541-73-1106-46-7iQO-51-695-50-195-48-7139638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2,20-82-191-20-3106-47-887-68-39-50-791-57-6 .77-47-488-06.-295-95-491-58-788-74-4131-11-3'408-96-8
N-N1trosod1 methyl ami nePhenolAnilineb1sf2-Chloroethyl (Ether2-cnioro,3-F;,4"-!lenzy1.2-D
CICIAch
henolorooro
tenzenelenzene
cohoiorobenzene
2-Methyl phenolb1s(2 •chlorolsopropyl (Ether4-Methylphenol-N1 t ro-D1 -n-Propyl ami neexacN1tro
iloroethanejenzene
Isophorone2-N1tronhenol2,4-DBenzo
methyl phenolc Add
b1s(2-Ch2,4-Dlcfi1.2.4'• Ir
oroethoxy (Methaneorophenolchlorooenzene
Naphthalene!"Chloroan1l1heHexachl orobutadlene4-Cnloro»3-Methylphenol2-Methylnaphthalenehcxaci2, 4,6-
orocyclopentadleneTrlchloropheno
2,4,5-Trlcnlorooneno2-Chloronaontha'lene2"N1troan1l1neOlmethyl PhtnalateAcehaonthylene
r*~ /-9-09-2 3-N1troan1l1ne
,
NDL » Nominal Detection Limit
NDL
10bUbU. )U.UuLULUbUbUIUIUIUbUIUIULUIUbULUIUill)IUIUu,uuuLUU,u
CASNumber83-32-951-28-5100-02-7132-64-9121-14-2
T>1W6-20-2-00-2
7005-86-7*1Cb'
I -I
/-•J.71-6
' 52-186-30-6101-55-3118-74-187-86-585-01 -U120-12-784-74•i"206-44-092-87-5129-00-085-68-79b1..L.
-M-bb
-1-Ii
7-81-78-01-9V-84-0
205-99-2207-08-950-32-8193-39-553-70-3191-24-2
(1) •*Not
bla
Acenaohthene2,4-111
.jkInltrophenol'ophenol
jenzofuran2,4-12.6-1
nitrotonltrotb
ueneuene
Diethyl phthalate4-Chlorophenyl-phenyletherFluorene4-N1troan1l1ne' ,6-Dln1tro-2-MethylphenolN-Nltrosodlphenylam*'•Brombphenyl-pneny
ne(l)ether
lexachlorobenzene'entachlorophenolPhenanthreneAnthraceneW-n-Butyl phthalatePi uorantheneBenzldlnePyreneButyl benzyl phthalate3,3'-Q1cniorobenz1d1neBenzolalAnthraceneb1s(2 •Ethylhexy)PhthalateChryseneDl-n-Octylenzoenzo
bk
enzolaIndenDiben
}
F!•Phthalateuorantuorant
tenelene
l^rene,k.3-cdlPyrene
i a, h (AnthraceneBenzo(g,n
*
DPerylene iCannot be separafl /|r|ijdetected after correctionnk.
lOphenylamlnefor laboratory
Li,
k JI
Region III VCentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850117-08.
Units: Hater • ug/LSoil « mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
IDL
1 W
,U
iUIIIMuurt
uU
IUJ1 '"lu"LUli ~IUL"I "sUill:
CASNumber62-75-8108-95-262-53-34111-44-495-57-854. -73-1106-46-710(1-51-6 .95-50-195-48-739638-32-9"106-44-5621-64-767 72-198-95-378-59-188-75-5105-67-965-85-0111-91-120-83-220-82-191-20-3106-47-887-68-359-51-791-57-677-47-488-05-295-95-491-58-788-74-4
L I 131-11-310 208-96-8
55-U3-2 .
N-N1trosod1methylam1nePhenolAril mebis 2-Chloroethyl (Ether2-Chl orophenolP!-J chiorj4-l chlor
i lenzenei lenzene
l e'nzy ft cohol1,2-0 ch orobenzene2-Methyl phenolbls(2-chlorolsopropyl)Ether4-Methyl phenolN-Nltro-Dl-n-PropylamlneHexacnioroethaneNltrooenzeneIsophorone2-N1trophenol2,4-Dliiiethylphenollenzo1 c Addb1 s ( 2-Ch I oroethoxy (Methane2,4-Dfch orophenol1 , 2 , 4-TD chl oroPenzeneNapithalene3-Chloroan1l1neHexachl orobutadlene'-Chloro-3-Mcthylpnenol.2-Meth: n naphtha 1 eneHexach oroq.f4f.« r' ch2,4,5-Tr cn
clopentadleneoroporoo
rtenolhenol
2-Chloronaoht halene2-N1troan1l1neDimethyl PhtnalateAcenaon'th'y3-Nltroani '
;nene
43] 5
J1JL
19,9
9.3
35.8
2.9
23.8
NDL
10bUblL
J,UULU111IU.bUbllUI11bULUUU11)bUU.UauLUUIUUU
LUUULU
CASNumber83-32-951-28-5,00-02-732-64-9121-14-2606-20-28' -66-2710S-/2-386-73-7100-01-6543-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-930-32-8193-39-553-70-3
10 191-24-2
Acenaohthene2.4-D1n1trpphenbl4-iltroohenolD1 mnzofuran2,4-D1 n1 troto uene.2.6-0' nltroto ueneDiethyiphthalate ,4-Chloroohenyl-phenyletherFluorene4-Nltroah1l1ne',6-D1n1tro-2-MethylphenPll-Nltrosod1phenylam1ne(l|' -Brompphenyl -pnenyl etherI'exachlorobenzenePentacnl orophenolPhenanthreneAnthraceneD1 -h-Butyl phthalate: uorantheneienzldlnePyreneButylbenzylphthalate3,3'-D1chlorobenz1d1neBenzo(a)Antiraceneb1s(2-Ethyl iexy)PhthalateChryseneDl-n-Uctyl Phthalatelenzol »F uorant lenelenzo ; F uorant leneBenzo (a PyreneIndeno ' ,2.3-cd)PyreneDlbenz a.htAnthraceneBenzo(g,h,1)Perylene
_____
*
,
(1) • Cannot be separated-fum d1 phenyi ami ne
a.
„. . -- *Not detected aftetfUtArfbalfcn for laboratoryNOL • Nominal- Detection Limit blank.Page 9 of 32
* 1*000223
..J
U.S. Environmental Protection Agency, Region 3, Central Regional Lab-.,
Project Name: Tybouts Corner Landfill___________________Sample Number: 8S0117_-01_
Combined ExtractOTHER COMPOUNDS""———"——' Estimated Cone.
Scan No. Tentative Identification pobNone Identified
Sample Number: BS0117-02Combined Extract
OTHER COMPOUNDS~"————— |( Estimated Cone.
Scan No. Tentative Identification ppti899 l,3,3-Tr1methy1-2-Oxab1cyc1oC2.2.2]
'octane ' Trace (9)980 . ' l,3,3-Tr1methylb1cyclo[2.2,l]
heptane-2-one • 281050 ' alpha.alpha.4-Tr1methylcyclottexane-
methandl • 2601059 l,7,7-Tr1methylbycyc1o[2.2.l]
heptan-2-one 1401066 4-Methyl-l-(l-methylethy1)cyc1ohexanol 321186 Hexahydro-2H-azep1n-2-one 2701204 l,7,7-Tr1methylb1cyc1o[2.2.l]
heptane-2,5-d1one Trace (7)1239 Hexamethylphosphoric trlamlde 110
Sample Number: 850117-03ComMned Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. 'Tentative Identification ppbNone Identified
Page 10 oT _3j
000234it,
•&>
V -.V" U.S. Environmental Protection Agency, Region 3, Central Regional Lab .
Project Name: Tybouts Corner Landfill_____________Sample Number: 850117-05
Combined ExtractOTHER COMPOUNDS
Estimated Cone.Scan No. Tentative Identification ppb
None Identified
Sample Number: 850117-06•Combined Extract
OTHER COMPOUNDS.' Estimated Cone.
Scan No. Tentative Identification ppbNone Identified
Sample'Number*' 'Bsbw-oa ' ' ' • • _•,1.;$
Combined ExtractOTHER COMPOUNDS
Estimated Cone.Scan No. Tentative Identification ppb
897 l,3,3-Tr1methyl.2-oxab1cycloC2.2.2]octane Trace (4)
1048 alpha.alpha.4-Tr1methylcydo-hexanemethanol • 140
1057 l,7l(7-Tr1methylb1cycloC2.2.rjheptan-2-one 71
1053 4-Methyl-l.(l-methylethyl)cyc1bhexanol 141182 Hexahydro-2H-azep1n-2-one 1501201 l,7,7-Tr1methy1b1cyclo[2.2.l]
heptane-2,5-d1one Trace (9)1238 Hexamethylphosphorlc trlamlde 44
004139Page 11 of 32
000225
'••lf,ft-
NDL
I.J"10Trij"nr
JUT
nrIT
kvTITr10"Irio"10i.r10i •50"in
Region IIICentral Regional Laboratory
Extractable Qrganlcs Analysis Data SheetSample No. flfiOTis.Ol
Units: Mater " ug/LSoil <• mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
CASNumber62-75-8108-95-262-53-34TU-44-495-57-8541-73-1106-46-7
1 T .00-51-6'.r ———95-5JM
396; 8-32-9106-44-5621-64-767-72-198-5-378-59-18B-/5-b105-67-965-85-011-91-120- 3-22091-2T06-i 7-887-68-3
12-1-3
- - 791-57-677-47-488-06-2g-95-91-58-788-74-4
ID ' <Uo-9o-a
N-N1trosod1methy1am1nePhenolmn Tnebl5T2-Ch1oroethyl (Ether-Clilorophenol1.3-D enloro lenzene1,4-U chloro lenzeneBenzyl Alcoholr.2-D1ch1orofaenzene2-Hethy phenolbl5(2-c 1 prol soprpjiy 1,,/ctner•|| ethyl phenor^1trp-01-n-Propy1 amineexac iToroethaneNitrobenzeneIsophorone2-N1trophenp1274-0'methyl phenolienzo c Ada
2-C iloroethoxy(Methane2.4-01ciloropnenolI72.4^Tr1cnlorQpenzeneNaphthalene3-Chlorpan1l1neHexacnlorooutadlene4-Chloro-3-Hel:hylpheno12-Methl naphthaleneHexachloroc 'c1opentadleneiiV ,6-Tr ch oropheno
,S-Tr1en orooheno2-Chloronaphthalene2"N1troan1l1neOlmetnyl PhtnaiateAcenaontny3-N1troan1
eneine
NDL
10
U
CASNumber83-32-9.1-2B-5100-02-7132-64-9
606-20-2U4-66-27005-72-386-73 7100-0i>6543-52-185-30-6"
-55-3IB-74-187-86-585-01-820-12-784-74-2206-44-092-87-5129-00-085-68-791-94-1•55-3-88-0 -9
U7-84-02(-99-2207-08-950-32-319-39-553-70-3191-24-2
Ac&naohthene2.4-Dlnltropnenol4-ntropJenplDl lenzofuran2,4-D1n1trotoiuene2,6-)1n1troto ueneethyl phthill ate
' -Chlorophenyl-phenyiethepFluoreneNltroanHlne,6-Dl n1tro-2-He ;hy_ phenol
N-NltrosodTpneny am1 n¥(l)'-Bromophenyl-phenyTetherf exachl orobenzeneentachlorophenolhenantrene
Anthracene) -n-Butylphthalateuoranthene
Benzldlne'yrenelutyl benzyl phthalate3,3'-D1chlorobenz1d1neenzo(a)Anthracene.b1s(2-Ethylhexy)PhthalateChrysene
Benzou Pyrene
D1-n-0cty PnthalateBenzo b F uorant leneBenzo K Fluorant leneIndenod. 2. 3-cd (Pyrene)1benz(a,h (Anthraceneienzoig.h.1(Perylene
(1) « Cannot be separated from dlphenylamlne"Not detected after correction for laboratory
NDL • Nominal Detection Limit blank, 004140P.M6, 12"of 32
_- .__._... J 9_-_-.._________••
.">•'•'..''1 •'; n'
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. asona-Qg
Units: Hater • ug/LSoil *mg/kg (wet)
Semlvolatlle CompoundsActual Detection Limit » ( 1 ) x NDL
NDL
3.11LUUUlUIU.ffLU
11il
LU"Jj
ulIU11
IU"1I
iULU...jJLU
30
LU
CASNumber62-75-8108-95-26.-61111-
-344-4
95-57-fl541- 73-1)6-4b-/10-51-fi'
95-50-195-'•3963
-7-32-9
106-44-5621-64-767-72-198-95-378-59-18' 1-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3308-96-8.9-09-2
NDL *
N-N1trosod1methylam1nePhenolAh1bis2-ch
' I'"2"
Ine2-Chloroethyl (EtherorekiHci
Benzyl fl1. 2-01 ell
nenolorooro
lenzenelenzene •
coholorobenzene
2 -Methyl phenolbls(2-chloro1sopropyl (Ether4-Methyl(•Nltro-
Shenol1- i•Propylamlne
lexachloroethaneNitrobenzeneIsophorone
~!£FT2.4-Benz
irophenolllmethy 1 phenoli c Acid
•>ls(2-Ch2,4-D1ch
oroethoxy (Methaneorophenol
1,2,4-TrlchlorobenzeneNaphthalene3-Chlproamnne(•exachlorobutadlenei -Oil oro-3-2-Me1Hexa2,4,2,4,
.vlnapisthy phenolvthalene
:ilorocyclopentadlener- rlchloropi- rlchlorop
tienoheno
z-Cmoronaohthalene2-N1troan1^1neDimethyl PhthalateAcenaoiithyiene3-N1troan1l1ne
Nominal' Detection Limit
NDL
10bUbUI11IIU
blbliUUUbUuuuubU,1IU
u,uuIu,1u,u
CASNumber83-32-9SRI: •b00-02-732-6_T-1
' -9'•It1
606-20-2.1 -66-2"7105-7Z-386-71!•110D-01-6543-52-186-30-6101-55-3118-74-187-8685-01120-84-7'
-b-Ui-'l-I
206-44-092-87-b129-00-085-68-7,91-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaphtnene<j,4-LH.r
-Dt
4-DinltrophenolUtrophenollenzor4-BlivPei
iran:ro
1n1troyip
4 Chl oroFluorene4-
:o:o
ueneuene
nhaiate) lenyl -phenyi ether
«t roam lineT^-Dlnltro-2-Nethy-•<1trosod1 phenyi am'Brombphenyl •phenyi
phenolne(l)ether
exacnlorobenzene'entachl orophenol'henanthreneAnthraceneTF•n-Butuorant
Mphthalatetene
fenzldlne'yrenelutyl3,3'-
benzyl phthalateHchlorobenzldlne
)e'n'zb(a)Antris(2-EthylChryseneD1 -n-UctBenzo (blenzojklenzo(a)Indeno 1Dlbenz a
iracenelexy (Phthalate
if Phtha• uorant; uorant
atelenetene
'yrene,2,3-cd)Pyrene.n) Anthracene
Benzo(g,n,1 'Perylene(1) • Cannot be separated from*Not detected after correction
blank.UV™f7'ltllfor labora
*
Inetory
Page J3_, of 32
Region IIICentral Regional Laboratory
Extractable Organic: Analysis Data SheetSample No. B50118-03....
Units: Hater • ug/LSoil • mg/kg (wet)
Semi volatile.CompoundsActual Detection Limit • ( ] ) x NDL
u)L
3J
LU'0j
iiiIU •T
IU"1D
iOIU1
.1LU"11
iULU1JLU
II
Idi i i
ijjLUi
•^
CASNumber62-75-8 •108-95-262-53-34111•44-495-57-854IUVIt)b-yb-
•73-1•46-7•51-6il-lIt -7
39638-32-9106-44-5.621•64-767-72-198-95-378-59-1 '88-75-5 -105-67-965-85-0111 •91-1120-83-2120•82-191-20-3106 •47-837-68-359-50-791-57-677-'BB-'
7-46-2
95-95-491-58-788-74-4131-11-3208•96-89-09-2 ..
N-N1trosod1methylam1nePhenolAn1'bis
ne2-Chloroethyl Ittner
2-Chloro,3-,4-enzj,Z-j
J'ch1 chf A1'ch
2-Wethylb1s(2-ch
henoloror
ibenzenejpenzene
cohol • •orobenzene .ihenollordsopropyl (Ether
4-MethylohenolN-N1 tro-01 -n-Propy 1 ami neHexachl oroethaneNitrobenzeneIsoohorone2-N1tropnenol2, 4-01 methyl phenolBenzole Addb1s(2-Ch2,4-D1chl,2.4-Tr
oroethoxy (Methaneorophenolchlorobenzene
Naphthalene3-Chloroanll1nehexachlorobutadlene4-Ch2 -MetHexai2,4j2,4,!
oro-3-Methy ipnenoilylnaphthaleneii oroc
j-Tr• Ir
CIch
^clopentadleneoroooroo
mnolhenol
2-Chloronapntnalene2-Nltroanil1neDimethyl PhthalateAcenabnfnylene3-NltroaniHne
.'
NDL * Nominal Detection Limit
NDL
10bUbiI,UU
111 'IUlUbUbULUIUIUbULIIUIUILbllIUIU-Uuuuu.uuLULULULU
CASNumber83-32-951-28-5100-02-7132-6121-1
4-9-H .
606-20-284-66-27005-72-386-73-7100-01-6"543-52-186-30-601-55-318-74-187-86-5
' 85-01-8120-,84-74
l-l•i
206-44-092-87-5129-00-085-68-19 -94-156-55-3117-8218-0
-1•y117-84-0205-99-2207-08-950-32•H193-39-553-70-3191-24-2
Acenaohthene2,4-D1n1trophenol4-Ulmropnenolbenzofuran
2,4-D12.6-D1Dlethy4-Ch o
n' troton1 troto
ueneuene
l phthalaterophenyl -phenyi ether
Fluorene4-Nltroanillne4,6-D1n1tro-2-MethyN-4-
NUrosodlphenylam1aromophenyl
phenolhe(l)
•phenyi etherHexachlorobenzene'entachloroohenolPhenanthreneAnthraceneDl •n-Butyl phthalatePI uorantheneBenzidine'yreneButyl3,3'-)
enzyl phthalate1chlorobenzldlne
BenzolalAntb1s(2-Ethyl
iraceneiexy)Phthalate
ChryseneHi"•n-Octyl Phthalate
riehzolenzoiehzoIndenoDlbenz
D hk !•
uorantuorant
lenelene
a) Pyrenel,2.3-cd)Pyrenea. n (Anthracene
Benzolg.h(1) • Ciinnot be*Not detected af
blank.
1separatedter corrq
IPerylene
fromm dli
K
C 17
henylamlne"^aooratory
___ 32UUrjtTTJ—3?
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850118-04
t
Units: Water • ug/LSoil. • mg/kg (rat)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
CASL Number »
62-75-8108-95-262-53-3411 1-44-495-57•8
HP1 -?3-l1, i-46-71 J -51-fi
- 95-50-195-4639631
-7-32-9
106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3! 06-47-8(7-68-359-5Q•791-57-677.47.488-06-295-95-4
r~ 91-58-788-74-4lHl-11-3208-96-839-09-2
NDL •
N-N1trosod1methy1am1nePhenolAn'1bis
ne2-Cliloroethyl)Etner
2-Chloroohenol,3-.4-
1 enz1,2-2-Me
J1ciJ1c<
J'ch
orobenzeneorobenzenecohol ,orobenzene •
: yTphenolb1s(2-chlorolsoprapy4-Methyl-Nltro-
(Ether8 henol1-n-Propylamlne
lexachloroetnaneItrobenzenesophorone2-N12,4-lenz
trophenoi31 methyl phenolr c Add
)1s"(2"Ch2.4-D1C11,2,4-Tr
~tapi"~"""c>
oroethoxylMethaneorophenolchlorobenzene
ihaleneoroanlllne
HeTachlorobutadlene4-Chloro-3"Mettiyl Phenol2-MeHexa
thy 1 naphtha! enenlorpc:
2 4, 6-T rich2j4,5-Tr1cJi
clopentacorophenoorooheno
1ene
2-Chloro'naohthalene2-N1troanl'llneDimethyl PhthalateAcenaontnyiene3-Nitroamline
Nominal Detection Limit
NDL
10bUbUUU]UIDLUbUbULUUU
bULULULULUbUiUUuuIULULUUUUU
LUIULU
CASNumber83-32-9 A51•28-5 2100-02-7 4132-64-9 D121-14-2 ~_606-20-2 2T
/II-66-2 D05-V.-3 «
".B-73-7 F100-01-6 4543-52-1 '86-30-6 N101-55-3 4118-74-1 H87•86-5 '35-01-8 '120-12-7 A84-74-2 D206-44-0 f92-B7-5 B129-00-0 P85-68-791-94-1 356-55-3 o117-81-7 t218-01-9 1J117-84-0 D205-99-2 :207-08-9 T50-32-8 B193-39-553-70-3191-24-2 1
*Notbl
cenaphthene,4-Dlnltropnenol-NltrophenolIbenzofuran,4-Oln t.6-01 nie';h'£lp" C iloro")luorene
rotoroto
uene •uene
thai atelenyl -phenylether
•lilt roam line,6-oinltro-2-Methy-Nltrosodlpheny am
phenolne(ll
-Bromopheriyl -phenyletherexachlorobenzeneentachl orophenollenanthrenenthracene•n-Butyl phthalateuorantneneenzldlneyreneutyiaenzyiphthalate,3'-DicniorobenzldlneenzolalAnthracenels(. -Ethyl nexylPhtnal atehrysene1-n-Oct]e"nzd i Ijnzo ;
Phthalateuorantuorant
lenelene
enzo a 'yrenefideno ,1benz a,
2.3-cd)PyrenehlAnthracene
snzolg.h.l IPerylene
ff
2. 2"
Cannot be separated from d1 phenyi ami nedetected after correction for laboratoryank- . Q04143
H3A ni9Q)YL3219
Region IIICentral Regional Laboratory
Extract:1'e Organlcs Analysis Data SheetSample No. 850118-06
Units: Hater » ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 . ) x NDL
NDL
,.„ll)1 1
l10""Luun
uU
iu1"IluIU1 "1."LU1I ':0In
L"*
• M
CAS.Number62-75-8108-95-262-53-3'111-44-'95-57-8541-73-1
rfl.16-46-70-51-6
91-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-011-91-120-83-2120-82-191-20-3106-47-887-68-359-50-791•57-fr77-47-488-06-295-95-491-58-788-74-4131-11-3ftjB-96-B,9-09-2 .
NDL
^
N-N1trosod1methy1am1nePhenol
Tivlbis
me2-Chloroethyl (Ether
~Z-v,hloroDlienolT;J
•U-U
enzy_2-D'
CICIAch
orobenzeneorobenzenecohol.orobenzene
2-Hethyl Phenolb1s(2-chlorolsopropyl (Ether4-Methyl PhenolN-N1 tro-Dl -n-Propyl ami neHexacnioroethanef UrobenzeneIsophorone2-NUrophenol2,4-Dltnethy phenolBenzole Acidb1s(2-Ci2,4-Dlci1,2Nap3-C
,4-lroroethoxy (Methaneoroonenolcm orobenzene
it ha leneiloroanlUne
Hexachl orobutadlene4-Chloro2-MethylnapHexachl oroc2,4..4
,6-lr.0'Ir
chcn
lethvi pnenoinnaieneclopenta'dleneoropnenoorooneno
2-Chloronaohthaiene2-N1troan1HneDimethyl PhtnalateAcenaohtnylene3-N1troanll1ne
0.5 J
• Nominal Detection Limit
NOL
10bUbUUIIUu.uubUbUIUIUIUbUIUIUIUIUbUIUIUUUIU
,uLUUuuuLU
CASNumber83-32-951-2100-
l-aI.-/
132-6421-1'
-9-i
606-20-28' -66-27005.
. 86-7lOO-i
•/.-J1
1-6543-52-186-30-6101-55-3118-74-187-86'b85-01-8120-12 784-74-2206-44-092-87-5129-00-085-6H-791-94-156-55-31! 7-81-72.. 8-01-9117-84-0205-99-2207-Q8-950-32-8193-39-553-70-3191-24-2
(1) - C«•Not de
blan
Acenaonthene2,4-D1nltrophenol4-LH
<1troohenolbenz
2,4-D'2.6 )'DietW
)"uranr trotolueneiVtrotolueneohihalate
4-Chlorophehyl -phenyletherFluorene-N1troan1l1ne.6-01 mtro-4-
-.-MeNltrosodlpheny
;hyam1
phenolne(r)
iromophenvl -phenyletherHexachlorooenzene'entachl orophenol'henanthreneAnthracene31-n-Butylphthalate•1 uorantheneJenz1d1ne
"PyreneButylbenzylphthalate3,3'-D1chlorobenz1d1neenzo(a)A'nt
HuslZ-EthylChrysene
iraceneiexy]Phthalate
)1-n-0ct' Phthalateenzolenzoenzo c
Tndeno)1benz
i)' uoranthene• uoranthene'yrene
1, 2. 3-cd) Pyrenea, h (Anthracene
ienzo(g,h,1IPerylene
IT
S.3
nnot be separated from dlphenylamlne;ected after correctlpnQfjir ljtjiratoryt,
J a Estimated concentration below limits of . , . _ , , „accurate quantltatlon. PageJ6_of__2_
3-: ':!'&$ jS6:rSil
U.S. Environmental Protection Agency, Region 3, Central Regional Lab9
Project Name: Tybouts Corner Landfill_____________Sample Number: 850118-01 •
Combined ExtractOTHER COMPOUNDS
Estimated Cone.Scan No. Tentative Identification ppbNone Identified
Sample Number: 850118-02Combined Extract •
OTHER COMPOUNDSi Estimated Cone.
Scan No. Tentative 'Identification ppbNone Identified
Sample Number: ', • '•850118.03 '_•Combined Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. Tentative Identification ppbNone Identified
Sample Number: 850118-04 '• Combined Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. Tentative Identification ppbNone Identified
Sample Number: 850118-06Combined Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. Tentative Identification __ppbNone Identified nnno.L 004145
i .J.B OOU<:-l|'ageJ7_ofj___f
...._.....' '. ». ....i«..._..___„.___
•i&
I'.;;•'»",'
•
•if'.Ci:
..ffi•;!;?!§V:
Region III ,Central Regional Laboratory
Extractable Organks Analysis Data. Sheet 'Sample No. Laboratory Blank
Units: Mater • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit * ( 1 ) x NDL
iUL
, ..Un
.u
.il
0nwU
Un
uU,
.0
)U
.
.ur~
CASNumber62-75 •8108-95-262-53-34111-44-495-57-8541-73-1i 06-46-7.00-51-695-50-195-48"39638-
•1•U.-D
106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-"965-85-,11-91120-8:
U•1•i
2--82-191-20-3106-47-887-68-59-50-
i1
91-57-677-47-488-06-295-95-491-58-788-74-4131-11-31Q8-96-89-69-2
N-N1trosod1 methyl ami nePhenolAn1bis
1ne2-Chloroethyl (Ether
PChloro,3-01 ch.4-01 cnlenzyl Aj,2-D1ch
henolorobenzeneorobenzenecoholorobenzene
2-Methyl phenolb1 s ( 2-chl orol sopropyl (Ether'•Hf.f ethyl phenol
ltro-01-n-PropylamlneHexachloroethaneMtrobenzeneIsophorone2-Nltrophenol2,4-D1metnylphenolBenzole Acidb1s(2-Chl2,4•U1ch1,.,4-Tr1
oroethoxy (Methaneorophenolchl orobenzene
Naphthalene3-Chloroan1l1neHexachl orobutadl ene4-Chl orb-3-MethyTpfienbl2,-MethylnaphthaleneHexacm orocycl opentadlene1,4,6 -Tr2,4,5-Tr1
etlorophenocnlorbohenol
2-Chlorbnaohthalene2-NUroanlllneDimethyl PhthalateAcenapntnylene3-N1troan111ne
NDL
10bUbUIULL
11
LU.11KbUbUIUIULUbULUUULUbULUUUULUULUIUuu,uuIUIU
CASNumber83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-2700586-731QD-I
72-3-71-6
543-52-186-30-6101-55-3118-74-1.7-86-585-01-8120-12-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
s
Acenaohthene2,4-D1n1trophenpl4-N1trophenolDlbenzofuran2. 4-Dln1 trotoluene2,6- in1 trotolueneDlethyl phthalate4-Chlorop lenyl-phenyl etherFluorene4-N1troan1Hne4 , 6-D1 n1 t ro-2-Methy l phenolN-N1trosod1phenylam' ned!'-Bromopnenyl-pheny etherexacn I orobenzene'entachl orophenolPhenanthreneAnthraceneD'-n-Butyl phthalateF uorantheneBenz1d1ne'yreneButyl benzyl phthalate3,3'-D1chiorobenzldlneBenzo(a)Ant iraceneb1s(2-Ethyl lexy (PhthalateChrysene •D1-n-0ctyl PhthalateBenzo b • uoranthenelenzo k • uorantheneienzo a PyreneIndeno : .2. 3-cd) PyreneDibenz a, n (Anthracene
1.0
Benzo(g,n.1IPervlene !
(1) • Cannot be separa@j)4i_)n>9l phenyi ami ne
Ci';
"Not detected after correction for laboratoryNDL • Nominal Detection Limit blank.
32
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850122-01
Units: Hater • ug/LSoil -mg/kg (wet)
Semi volatile CompoundsActual Detection Limit « ( 1 ) x NDL
CASL Number
62-75-8108-95-262-53-34111-44-495-57-8541-73-1105-46-7100-51-695-5195-41 -739638-32-9106-44-5621-64-767-72-198-95-37B-59-188.75-5105-67-965-85-0111-91-112Q-E120-f
3-22-1
91-20-3106-"'67-61
7-8-3
59-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3',08-96-8
.-J9-09-2
NDL •
N-N1 trosodlmethy 1 ami nePhenolAnl Iii'bis 2-2-Ch o1,3-D1.4-0Benzy1,2-01
!Jhloroethyl (Etherromenol:i br'oberizene:i orobenzene •A cohol:h orobenzene •
2-Methyl phenolb1s(2-chlorolsopropyl (Ether4-Methyl phenolN-N1 tro-DI -h-Prbpyl ami neHexachl orbethaneNitrobenzeneIsophorone
. 2-N1trophenol2,4-Dlmethyl phenolienzolc Acidbls(2-(2,4-DI'
;nioroethoxy (Methane: iloroph'e'nol •
1, 2, 4-Trlchl orobenzeneNaphthalene3-ChloroanlHneHexachl orobutad! ene4-Ch loro-3-Met hyl phenol2-Met nHexachl2,4,6-12,4.5-
'Inaphthaleneorocyclopehtadlenerr chloropFr cnloroo
nenorteno
2-dhloronaohthalene2-Nltroan1l1neDimethyl PhtnalateAcenapntnylene3-N1troan111ne
Nominal Detection Limit
NDL
10bUbUIUUu.UIU11)bllbll.UuIUbUIUu'1IUbUU11dUHiIUIUIUuu0uuu
CASNumber83-32-951-28-5100-02-732-64121-11
•9•i
606-20-284-66-27005-72-3
. 86-73-1: 00-01-6543-52-186-30-6101-55-311B-74-187-86-585-01-8: 20-12-7£4-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-8]• I2; 8-01-9I, 7-84-0205-99-2
• 207-08-950-32-8193-39-lT53-70-3191-24-2
(1) > Can*Not dete
blank.
Acenaphthene2,4-Dln1trophenol4-N1trophenoiDlbenzofuranz,*-U12.6-)'Diet iy_
r trotoT troto
ueneuene
Phtnalate4-Chlorpphenyl-phenyletherFluorene4-N1troani1me4, 6-D1n1tro-2-MethyJ phenol~H1 -
N1trpspd1 phenyi amtromophenyl-pheny
ne(l)ether
exachl orobenzene'entachl orophenol'henanthreneAnthraceneD' -n-Butyl phthalate• uprantheneBenzldlne'yreneiutyl i"3,3'-)
snzylphthalatechlorobenzldlne
lenzo(a)Amiis(2-EthylChryseneD1-n-0ctylBenzolBenzoBenzoIndenoDibenz
iracenelexy) PhthalateWthalate
j, ; uorant< • uorant
lenelene
aT'yrene1,2.a.h
Benzolg.n,
3-cd (PyreneAnthracene(Perylene
not be separated fromcted Ertncjfnfejl n
it
26.0
dl phenyi ami nefor laboratory
•
Page 19 of 3200023,9
-Zis.
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850122-02
Units: Water « ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit •( 1 . ) x NDL
NDLjluIU'ill1 •lu"IU1LUi"1 '10LU1 "'.*LU1I '10"111I."LU1r "uUlu
fc' j
CASNumber62-75-8108..95-262-53•34111-44-495-57,,.541-73-1'06-46-7100-51-695-50-195-48-73963E106-'
•32-94-b
621-64-767-72-198-95
"7 -59•3-1
88-75-5105-67-965-85111-9,2o-0
-0•13-2
20-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-5B-788-74•4131-11-3'1)8-96-8
-J9-09 •2 .
N-N1trosod1methy1am1nePhenolAnilineb1s(2-Chloroet hyl (Ether2-Chlorb1,3-C1.4-CBenzy1,2-02 -Met
CIct
cli
ihenol00obenzeneobenzene
cohol .orobenzene
iyTohenolb1s(2-chlorolsopropyl (Ether4-N-
eu•h
lylro-
8 henol1-n-Propylam1ne
HexachloroethaneNitrobenzeneIsophorone2-Nltroohenol2,4-D1methyBenzoleb1s(2-Ch2,4-blcil,Z,4-Tr
1 phenold
1 oroethoxy (Methaneorophenolchl orobenzene
Naphthalene3-Chl oroanlllneHexachlorobutadlene4-Chloro2-MetHexac
-3-Methyl phenolwlnaphthaleneiloroc
2,4,6-Trlch2,4,3-Tricn
'dopentadleneoroohenoloropnenol
2-Chloronaohthalene2-Nltroan1l1neDimethyl PhtnalateAcenaontnyiene3-N1troan1l1ne
NDL • Nominal Detection
.
NDL
10aUbU111
11bbUIUIUIUbUIUIUIUIUbULULU.UJ UIUuu
LU.11Ui)U
(:*NLimit
CASNumber83 3251
-9•28-5
~ Ifo-02«7~32-6121-160
-§iD-2
'•tf4-liU-li
7S&"-2"Tffos-86IUb4.6
li-i•73-70-01-6! -52-1-30-6
101-55-3118-74-187-86-585-01120-184-7'
-U£-1-2
206-44-092•al-b"T29-00-085-6B-791-94-1.6-55-3117-81-7218-01-9117-84-0205-99-2207-08-9.0-32-8193-39-553•70-3191-24-2
Acenaphthene2,4-01t -Nr:r
nltrophenoiiphenol
ibenzofuran" Ifi- )•2.6-1
n1 trotor troto
ueneuene
uietnyiohthaiate4-cnl oropneny I -pheny l etherHuorene-Nltroanll1ne,6-D1n1trb-2-Methy-Nitrosodlpheny.lam•Bromophenyl -pneny
phenolne(l)ether
exachl orobenzeneentachl orophenolhenanthrene
"Anthracene"1 ' -n-Butyl phthal ate
uoranthene~Benzld1ne'yreneutyl benzyl phthal ate,3'-D1cniorobenzld1neenzo a (Anthracene
^ n s ( 2-Ethyl hexy (Phthal ateChryseneQT-n-0Benzolenzoenzondeno)ibenz
:t •'> •i •
Phthalateuorantheneuoranthene
alPyrenel,2.3-cd)Pyrenea, hi Anthracene
)enzo(q,n) • Cannot be separatot detected after cwrblank.
DPerylene
M
,
*
17.8
•o*Q|1 phenyi ami neorrfor laboratory
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850122-03
Units: Hater • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ..) x NDL
!DL
,UU
,Uw-
u0„
U
UnuU
U'
.u,u
.1
id. p
.u
.Ur
CASNumber62-75-8108-95-262-53-34111-44-496-57-8541-73-1'06-46-7
, j.00-51-695-50-r •
• 95-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-1B8-75-5105-67-965-85-011-91-1,20-83-2120-82-19!, -20-311 6-47-887-68-359-50-791-57-677-4/-488-05-295-95-491-58-788-74-4131-11-308-96-8
-. /9-09-2 „
N-N1trosod1methylam1nePhenolAn1bis
me"2-Chloroethyl (Ether
2-Chl oroonenol1,3-01'1',4-D'Benzy1,2-D1
:iCIAch
orobenzeneorobenzenecoholorobenzene
2 -Methyl phenolbls(2-441 4
chlorolsopropyl (Etheretnyl1trO"l
inenolH-n-ProoyVamine
HexacnloroethaneNitrobenzeneIsophorone2-N1tropnenoi2,4-OlmetnylphenolBenzole Addb1s(2-Ch2,4-D1ch1,2Nap3-C
,4-rroroethoxy (Methaneorophenolchl orobenzene
htnaleneiloroanlllne
Hexacnlorobutadlene4-Chloro"3-MethylohenPl2-Met •Hexac i2,4.0-
l naphtha) eneorocyclopentadleneTrlcnlorooheno
(STr, 5 -Tr1 chl bropheno2-Chloronaphthalene2-N1troan1nneDimethyl PhtnalateAcenaontny3-N1troan1
eneme
NDL10bUbUIUUU1)1,
IUbUbUIUIUIUblIUIUIUIUbUIULUi!U111IULU;.UUIULuUUIU
CASNumber83-32-951-28-5~K1.0-02-72-6"Tii-i
606-2
-9-2-H
B4-66-Z7005-72-386-73-7100-01-6543-52-186-30-6101-55-3118-74-187-8685-01120-
•b•Ui-l
84-74-2206-44-092-87-5129-00-035-68•191-94-156-55-31].1
l-s.-U
-/,-0
7-84-0"265-99-2207-08-950-32-3193-39-553-70-3191-24-2
(D •
Acenaphthene2,4-D4-fii
imtroohenol•oohenol
Dl lenzoruran2,4-12.6-1
n1 trotoluenem irotoluene
lethyipithalate' -Chlorophenyl-phenyletnerFluorene'•NltroaniUne .4,6-0N-Nl:
1n1trb-2-Methy•osod! phenyi am
phenolne(l)
4-Bromophenyl -phenyletherHexachl orobenzenePentachl orophenolPhenanthreneAnthraceneD' -n-ButylpnthalateF uorantheneBenz1d1ne'yreneButylbenzylphthalate3,3'-Benzo
)1chlorobenzld1neDAnt
b1s(2-EthylChrysene11-n-OctylenzoBenzolenzo
iracenelexy (Phthal atePhthalate
i F uorant( Fl uorant
lenelene
a Pyrenendenol ,2.Hoenzla.ht)enzo(g,h,
i Cannot be separatee
3-cd (PyreneAnthracene(Perylenefrom
*
7.0
dlphenylamlneNDL » Nominal Detection Limit blank,
Page 21 of 32
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850122-05
Units: Mater • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 .. ) x NDL
SOL
IUIU
1JLU"1TiU111i.jLUi
iLU"1
ijULU
il
LUi n
1lULU. .SUi "
IU,UI.
CASNumber62-75-8108-95-262-53-34111-44-495-57-8541-73-1JB-46-700-51-695-50-195-'39631106-
-7B-32-94-5
621-64-767-72-198-95-378-59-188-75-5105-67-9
nJ5--5-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-320S-96-8
..-59-09-2 .
NDL »
N-N1trosod1methy1am1nePhenolAnilineb1s(2-Chloroethyl (Ether2-Chlor±3-0 c,4-0 eenzy5 -U'e
01 henoli orobenzenei orobenzeneA coholh orobenzene
2-Met hylphenolb1s(2-chloro1sopropyl)Ether
~~i~3if-l
ethylphenolitro-Dl-n-Propyiamlne
Hexachl oroethaneNitrobenzeneIsophorone2-f2,'
Urophenol-Olmethy
Benzole Adbls(2-c2,4-D1c1,2,4-1
1 phenold
hi oroethoxy (Methaneil orophenolr cniorobenzene
Naphthalene3-Chloroanl lineHexachlordbutadlene4-Ch or2-Met i:Hexac i2,4,6-7
o-J-InaporocHen
2,4,5-Tricr
Methyl phenolhthalene'dopentadleneloroohenoloropnenol
2-Chloronaphthalene2-NltroanlllneDimethyl PhtnalateAcenaontnyl3-N1troan1
Nominal Detection
eneIne
Limit
NDL
10bUbULUL1)1
.U10',UbUbUIUIUIUbUUuIUIUbULULUIiLILU,uuLULULULULU
CASNumber83-32-951-28-5lOO-oi-7132-64-9121-14-2.606-20-2ll4-66-27005-72-386-73-7100-01-6543-52-186-30-6"101-55-3118-74-187-86-585-0120-84-7'
-82-7•i
206-44-092-87-5129-00-085-68-791-94-1
,56-55-3^nil7-81-78-01-97-84-0
205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaohthene2,4-Dinnropnenol4-NitrophenolDlbenzofuran2,4-012.6-11Dletw
n trotor troto
ueneuene •
Iphthalate .4-Chl oropheny l -pheny let herFluorene .'-N1t roam nne,6-omitro-2-Methy
("Nltrosodlphenylam'•Bromophenyl--pheny
phenolnedlether
exacnlorobenzene'entachl orophenol'henanthreneAnthraceneB1 -n-Butyl phthal ateF uprantneneBenz1d1ne'yrenelutyl i3,3'-)
inzylphthalateichlorobenzldlne
Benzo(a)Anbls(2-Ethy
nracenelexy (Phthal ate
Chrysene1)1 -n-OctyBenzoBenzoBenzolIndenoDibenz
i hPhthalatelorant
t FTuoranttenelene
a Pyrene1.2a.h
BenzolQ.h,3-cd (PyreneAnthracene(Pervlene
,
*
117.1"
(1) • Cannot be separated from d1 phenyi ami ne*Not detected after correctJc.n_fwvi1aboratory
blank. 00415"
i ' , _ i
» la
Region IIICentral Regional Laboratory
Extractable Organlcs Analysis Data SheetSample No. 850122-06
Units: Hater • ug/LSoil • mg/kg (wet)
Semlvolatlle CompoundsActual Detection Limit •( 1 ) x NDL
NDL
lu"iU
IU1"_lu™LUl -
IU
10"
1 •iuU
,u,".u"u:d;"
iu
CAS .Number62-75-8106-95-262-5:111-'95-b4UiOI
-344-4
•57-8•73-1)-46-7 •i-Sl-6
9TT-50-195-48-739638-32-9106-44-5621-64-767-72-198-•95-378-59-188-75-5105-67-965- 85-0111-91-1120-t120-E91-
3-22-1
20-3106-'B7-6E
7-8-3
59-50-791-57-677-47-488-06-295-95-4 •91-58-788-74-4131-11-3
.0' 'J8-96-8S -9-09-2
N-N1 t rosodlmethyl ami nePhenolAnlbis
ne2-Chloroet hyl (Ether
2-Chlorc
1
' •
l'"enri<!-
J'CIJ' Cl' AJ'cli
henoloroorob
enzeneenzene
cohoiorobenzene
'.-Methylphenolb1s(Z-chlorolsopropyl (Ether4-Methylphenol
~I -N1tro-D1-•n-Propyiam1neexachloroethaneItrobenzene
Tsophorone2-Nltrophenol2,4-
~EenzJlmethi1 c Aci
1s(2-CiT.4-D1C11,2,4-Tr
"I apni-Ui
'Iphenolrdoroepro|
:hoxy (Methanelenoi
ch'l orobenzenechaleneoroanlllne
"Hexachl orobutadl ene4-Chloro-3-Metnyi phenol2-Methyl naphtha leneHexach 1 orocycl opentadl ene2, 4, 6-Tr1 chl oroonenol2,4,5-7r1cnloropnenol2-Chloronaphthalene2-N1troan1l1neDimethyl PhthalateAcenaontny3-N1trpan1
eneme
>
NDL
10bUbUUUUu
bbULiLULUbUUUU,UbULULUUULllUULULUUUUuLU
CASNumber83-32-951-28-5100-02-7,32-64-921-14-2
,6CU4H6-20-2-66-205-72-3
SS-73-7100-01-6543-52-186-30-6tal-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0
, 92-87-5r i_9-oo-o85-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-1?207-08-950-32-8193-39-5
r 53-70-3191-24-2
(D •
Acenaohthene2,4-D1n1trophenol4-ntrophenolDl lenzofuran2,4-1 n12.6-) h1Dietiylp4-Chloro[
rotoroto
ueneuene
inautelenyl -pheny letner
Fluorene4-N1troaniilne4,6-01 n1tro-2 •MethylphenolN-N1trosodlphenylam1ne(l)4-Bromophenyl-•phenyletherHexachlorobenzene'entachloropnenol'henanthreneAnthraceneDI-n-Butylphthalater uorantheneienzldlne'yreneiut'yl lenzyl phthal ate3,3'-)lchlorobenz1d1neBenzofal/b1s(2-Eth
n .iraceney lexy (Phthal ate
Chrysene01-n-octylenzo i FSenz'o :Benzo aIndenol ,
Phthalateuorantheneuoranthene
yrene2.3-cdlPyrene
Hbenzla.hlAnthracenelenzo(g.h,1 fjswUelfil
W
3.3
Cannot be separated from dlphenylamlne*Not detected after correction for laboratory
NDL * Nominal Detection Limit blank.
. -It"
Region IIICentral Regional Laboratory
Extractable Organic; Analysis Data SheetSample No. 850122-07
Units: Water • ug/LSoil • mg/kg (wet)
Semi volatile CompoundsActual Detection Limit • ( 1 ) x NDL
IDL
.U
.U
,u-T-1N
,u.0t B
.11,i,0,11,a.U,;.0n,.u.0,.aUL"3IVrr3
CASNumber62-75-8108-95-262-53-3'Ul-44-495-57-8541-73-16-46-7
1DQ-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-212Q-E2-191-20-311 6-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-7U8-/4-4131-11-308-96-8JI9-09-2 .
N-N1trosod1methy1am1nePhenolAnilineb1s(2-Chloroet hyl (Ether2-Chloro henoll.3-D1ch orobenzeneTT-ITci orobenzeneenzy A cohol2",:D' ch orobenzene
2-Met hyl phenolb1s(2-chlorolsopropyl (Ether4-NethylphenolN"N1tro"D1"n-Propylam1neHexachl oroethaneN1tro lenzeneIsophorone2-N1trophenol2, 4-D1metnyl phenolBenzole Addb1s(2-Ch oroethoxy (Methane2 ,4-01 o orophenol1,2,4-Tr chlorobenzeneNaphthalene3-Chloroan1l1neHexachl orobutadl ene4-Chloro-3-MethylphehPl2-MethylnaphthaleneHexac ii oroc2,4,6-7r1ch2.4,5-Tricn
'dopentadleneorobhenoloropnenol
2-Chloronaphthalene2-N1trpanU1neDlmethvl PhthalateAcenapntnyl3-Nltroani
eneme
NDL
10blblIUIUUuuI
blbUIUIUIUbUIUIUIUJUbUIUIU20IULULULULU,U0LULULU
CASNumber83-32-951-2B-510D-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6543-52-186-30-6101-55-3118-74-187-86-5
r B5-0 -8120- 2-784-74-2206-44-092-87-5129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2
Acenaohthene2,4-D1nltrophenol4-<itrophenolDlbenzofuran2,4-)1n1trot6luene2.6-D1n1trotolueneDienylphthaute4-c ilorophenyl-phenyletherFlubrene4-N1troan1l1ne4,6-D1n1tro-2-Methy phenolN-N1trosod1phenylam' ne(l)4-Brompphenyl-onenyletherHexachl orobenzenePent ach I oropnenolPhenanthreneAnthracene01 -n-Butyl phthal ateFl uoranthenelenzldlnePyreneButyl benzyl phthal ate3,3'-D1chlorobenzld1neBenzola (Anthraceneb1s(2-.thylhexy (Phthal ateChryseneDl-n-Octy PhthalateBenzo b)F uorantheneBenzo k)F uorantheneBenzo a (PyreneIndeno(l,2,3-cd)Pyrene
K
14,7
Dlbenzla.n (AnthraceneBenzolo.n.DPerylene
(1) • Cannot be separated from dlphenylamlne*Not detected after correction for laboratory
NDL • Nominal Detection Limit blank. 004152Page .24 .of a;
U.S. Environmental Protection Agency, Region 3, Central Regional Lab.
Project Name; Tybouts Corner Landfill_______________________________Sample Number: 850122-01
Combined ExtractOTHER COMPOUNDS
Estimated Cone.Scan No. Tentative Identification ppb
None Identified • |(j
Sample Number: 850118-02 |§,Combined Extract
OTHER COMPOUNDS""" ' Estimated Cone.
Scan No. Tentative Identification ppbNone1 Identified , ' • |?
f"Sample Number: 850122-03 . ' fy
Combined ExtractOTHER COMPOUNDS
Estimated Cone.Scan No. • Tentative Identlf1cat1on ppbNone Identified
Sample Number: 850118-05Combined Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. Tentative Identification ppb' 882 2-Ethyl-l-hexanol 2.61537 2,4,6-Trlmethyloctane 2.91632 2,4,6-Trlmethyloctane 5.61638 2,7,20-Trlnethyldodecane 3.41722 3,7-D1methylundecane 111731 2,7,10-TMmethyldodecane 7.11784 fl-Decylhydroxylamlne 1.31807 Nonadecane 15 n.tK/i004154
Page 26 of .32
000240
U.S. Environmental Protection Agency, Region 3, Central Regional Lab,. "" ;(|v:I..'.?.'.)
Project Name: Tyfaouts Corner Landfill ___ ______________________ •Sample Number: 850122-05
Combl ned Extract .OTHER COMPOUNDS
Estimated Cone.Scan No. Tentative Identification ppb1911 l-Ethyl-4-methylcyclohexane 2.51960. Undecylcyclohexane 8.7 •1997 Octacosane . J92070 Heptadecane 212141 Hexatrlacontane 17
Sample Number: 850122-06,,
Combined ExtractOTHER COMPOUNDS
Estimated Cone.' ' Scan No. , Tentative Identification ppb '
None Identified ' ' •,%
Sample Number: 850122-07Combined Extract
OTHER COMPOUNDSEstimated Cone.
Scan No. Tentative Identification ppb. 1632 3-Ethyl-2,7-d1methyloctane 1.1 |-r'1722 2,4,6-Trlmethyloctane 1.5 ';';».1732 2,7,10-Trlmethyldodecane 1.3 (_;(.1808 2,7,10-TrlmethyldDdecane 1.8 if:1889 2,7,10-Trlmethyldodecane • 1.7 '1960 Hexylcyclohexane Trace (0.6)2023 2,7,10-Trtmethyldodecane 1.12071 2,7,10-Trlmethyldodecane 2,22114 l-(Ethenyloxy)octadecane 1.32267 2 ,7-Dlmethyl octane 1.82361 2,4,6-Trlmethyloctane 1.9
Page 27 of 32 __004155
is 000241
U.S. Environmental Protection Agency, Region 3, Central Regional Lab.
Project Name:_ Tybouts Corner Landfill_________________Sample Number: 850122-08
Combined ExtractOTHER COMPOUNDS
"~~""""" Estimated Cone.Scan No. Tentative Identification ' ppb
787 (Methylethyl)benzene Isomer 1.1877 l,3-D1ethylbenzene 4.8890 l,3,3-Tr1methy1-2-oxab1cyclo[2.2.2]
octane 4.3896 Sp1ro[2,4]heptan-4-one 7.4970 l,3,3-Tr1methylb1cycloC2.2.1]
heptan-2-one 11987 3,5-D1methylpheno1 1.6991 2-Ethyl-!l,3-d,1methylbenzene 1.2999 D1 ethyl ester' phosphoric add 7.21003 Tetramethylbenzene Isomer 2.41009 Tetramethylbenzene Isomer 4.61034 2,5-D1methylpheno1 • • 261041- a1pha.alpha.,4-Tr1methy1'-
cyclohexanemethanol' ' 1001049 l,7,7-Tr1methylb1cyclo[2.2.1] '
heptan-2-one 481056 4-Methy1-l-(1-methylethyl)cyc1ohexano1 101121 l-(2-Methoxyethoxy)butane 4.61156 2,5,8,11-Tetraoxadodecane 5.01188 Hexahydro-2H-azep1n-2-one 4201194 l,7,7-Tr1methylb1cycloC2.2.l]
heptane-2,5-d1one 2.81210 l-[2-(2-Methoxy-l-methylethoxy)-l"
methylethoxy]-2-propanol 471297 • 1-Phenyl-l-propanone Trace (0.7)1583 2-Methylbenzenesulfonam1de .4.31622 2(3H)-Benzoth1azolone 6.01666 N-Ethy'l-4-methylbenzenesu1fonam1de 8,22048 4,4'-(l-Methy1ethyl1dene)-b1s-phenol 4.0
Page 28 of 32_ 004156000242
Matrix Spike RecoveryI Recovery
Page 29 ..of 320041
000243
Phenol2-Chl orophenol1,4-01 chl orobenzeneN-n1troso-n-propyl-l-propanam1ne1, 2, 4-Trl chl orobenzene'4-Chl oro-3-methyl phenolAcenaphthene
(1,2-Dlhydroacenaphthylene)4-N1trqpheno12,4-D1n1trotoluenePentachlorophenolDlbutylphthalatePyrene
Sample No.Dup. 1Spike35.8 ' '90.8
87.6
91.0
90.0
82.2
92.4
24.1
85.8
82.0
104
95.6
860117-07Dup. 2Spike
35.5
89.4
89.1
92.7
92.8
82.3
95.7
23.3
87.1
80.9
99.3
102
RPD*
0.8
1.5
1.7
• 1.93.1
0.1
3.53.4
,1.5 '
1.3
4.6
6,5
TargetRPD42
40
28
38
. 28
42
3150
'. 38 .
50
40
31
TargetLimitsMater12-8927-123
36-97
41-116
39-98
23-97
46-118
. 10-80
24-96
9-103
11-117
26-127
'>
\-t
]y
'<;.•
\
••
*RPD • Relative X difference: (RepHcatei - Replicate?) x 100
I
Matrix Spike ReepveryS Recovery
Average Replicate
32
00.0244
Phenol2-Chl orophenol1,4-01 chl orobenzeneN-n1troso-n*propy1*l-propanam1ne1,2,4-Trlchlorobenzene4-Chl oro-3-methyl phenolAcenaphthene( 1 ,2-D1hydroacenaphthylene )
4-N1trophenol.2,4-D1h1-trotoluenePentachl orophenolDlbiitylphthalatePyrene
Sample No.Dup. 1Spike35.1
87.1
91.9
89.7
94.0
87.0
94.6
26.4
.89.0
76.1
103
98.6
850122-04DupTTSpike35.586.790.6
91.3
92.9
89.3 •
. 97.0
25.5.94.5
.78.2105
97.6
RPD*
4.7
0.5
1.4
1.8
1.2
2.6
2.5
3.5 •
6.0
2.7
1.9
1.0
TargetRPD
4240
28
38
28
42
31
.50 ,
. ,38' '50
4031
TargetLimitsWater12-8927-123
36-9741-116
39-98
23-97
46-118
10-80
24-96
9-103
11-117
26-127
'"* .'
i;•K'T''.' ' ' '",•f;w't4;?I1.---V :/> '
'At''
-'l-,'''i.^Jt.
'vf
Iv• JE-
ill'\'&;' '•?•'
*RPD • Relative X difference: (RepHcatei - Replicate?) x 100 . (it1.
Surrogate Recovery
X Recovery 2,4,6-2-Fluoro- D5- D5-N1tro- 2-Fluoro Trlbromo- D14-
Sample Wo. phenol Phenol. Benzene l.l'-blphenyl phenol TerphenylTarget Limits
Hater 23-107 15-96 41-120 44-119 20-105 33-128
850117-ReagentBlank 51.0 33.4 88.9 80.3 82.1 97.3-01 48.6 30.7 84.5 86.7 '95.7 99.4-02 * * * * » • *-03 49.3 30.8 83.2 82.0 97.5 96.2-05 46.6 30.9 86.6 85.2 85.0 101-06 48.2 29.7 82.3 82.4 95.3 98.6-07 Spike 1 48.0 32.4 84.8 79.6 89.6 97.2-07 Spike 2 47.9 32.0 ,.86.6 82.4 87.4 101.2•08 49.3 32.3 108.6 • 89.5 104 . 95.8
*Sample required dilution which resulted 1n surrogate compound concentrationsbelow the level of accurate quantltatlon.850118-01 32.0 20.4 83.7 • 95.0 73.0 68.8'
•02 47,0 28.1 90.3 88.7 82.5 104 '•03 42.0 26.4 82.4 87.2 91.0 99.6-04 45.1 28.9 88.6 88.2 91.4 103•06 42.6 27.2 86.3 85.0 108 112
Blank • 48.9 28.4 80.8 84.3 81.2 81.0850122-01 51.3 29.7 86.5 88.9 88.3 91.7
•02 54.9 32.3 91.5 92.6 89.3 90.6•03 54.5 30.7 88.7 92.6 91.5 100.8-04 Dup. 1 52.0 31.9 88.7 90.6 95.0 96.1•04 Dup. 2 51.7 31.5 92.1 95.1 96.3 97.8•05 ' 47.6 26.1 84.6 88,4 81.1 109.9•06 46.2 27.3 77.3 83.0 81.7 89.2•07 58.3 33.4 97.0 95.7 89.4 93.5•08 43.1 26.4 90.8 90.0 88,0 85.9
• »
Page_31_of
lk 000245
Quality Control
1. Before acquisition of any samples the mass spectrometer Iscalibrated using FC43.
2. The calibration 1s verified by obtaining the spectra of a knowncompound (DFTPP). All mass assignments and relative abundances arefound to be 1n acceptable ranges or the Instrument Is adjusted untilsuitable spectra of the known are obtained.
3. Immediately before analysis each sample Is spiked with an Internalstandard DIO-phenanthrene. All quantltatlon or estimates ofconcentration are made 1n comparison to the Internal standard.
4. Mixed standards of extractable Priority Pollutants and HazardousCompound List Substances are analyzed before each group of samples.The relative response of'each compound versus the Internal standardIs determined for use 1n quantltatlon.
5. For each group of samples extracted a method blank Is prepared andexamined for laboratory Introduced contamination.
6. The samples were, spiked with mixture of surrogate compounds prior toanalysis. Recovery for each wa's determined to check for matrix effect.
7. An 'aliquot of samples 850117-07 and 850122-04 were spiked with a .priority pollutant cocktail at 50 ng/ug (1n the extract).and carried .through the extraction'and GC/MS analysis. The recovery for'each1compound was determined to check for matrix effect.
u
APPENDIX L
SAMPLING PROGRAM .
004161,bOOOJM7
_&•
APPENDIX L1
SCOPE OP THE SAMPLING PROGRAM
L1.1 SCOPE OF SAMPLING PROGRAM - NARRATIVEU.?, ' DESCRIPTION OF THE TABLES
Tabla L1-1 Scope of the. Sampling Program,Tabl« LI-2 • Check List of Analyzed Organic ContaminantsTable L1-3 ' Check Uat'of Analyzed Inorganic Contaminants fey
" IIm
* is
004162
000248w
DRAFT
U.I SCOPE OF SAMPLING PROGRAM - NARRATIVE
The RI Sampling end Analysis Program Implemented for the site InvestigationIncluded the following: (See Figure 5-1 for a site map showing all of the samplinglocations)
• Residential Walls - April 1983 sampling episodes
Sixteen wells were sampled In April 1983 and subjected to a full prioritypollutant scan. Table L1-2 and Table L1-3 list all 'of the hazardoussubstances measured In a full priority pollutant scan. The results of thissampling wars discussed In a preliminary health and risk assessment IssuedIn August, 1983 (.),
• Ambient Air - June, 1983
An' ambient air sampling program was 'performid on .unt 24,1.83 ualng' Tanax air' sampling tubaa at eight onslte locations, Absorbed pollutants •were analyzed for volatile organic chemicals,
',1.K
• Residential W'.'lls - July, 1983
DNREC and ,'PA repeated the residential wall sampling to verify the \findings of the above,April sample results. The results ware reported In jthe preliminary health and risk assessment Issued In August, 1983 (2),
X*.. .
« Leachate - April, 1983
• Leachatss (five samples) were collected on April 27,1983 and analyzedfor a full priority pollutant scan.
L1-1 0
•» *»000249
04V**
\- ' DRAFT
• Surface Water - January, 1984
Surface water samples (12 locations) and sediment sample1! (six locations)were collected for analysis In January, 1S84. Analyses covered tha fullpriority pollutant scan and special analysis for phenols, Total OrganicHalogens (TOX), Total Organic Carbon (TOO), and chlorides,
• Subsurface Soils - January, 1984
Subsurface soils (six samples) were collected from tha borings drilledthrough the main landfill for a full priority pollutant scan onJanuary 27,1984,
• Groundwater (Monitoring Walla) - January - February, 1984 "' '
GroundwAter samples ware taken from drilling Phase I and II .monitoringj • walla and iilictad existing walla batwaan, January 16, and
I ' • February 12,1984. Forty-six groundwatar samples ware forwarded toContract Laboratories for a full priority pollutant scan. Conductivity andpH ware measured In the flold.
• Groundwater (Monitoring Wells) - May, 1984
All monitoring wells sampled In January - February, 1984 were resampladfrom May 2 to May 7,1984', Forty-five groundwatar samples were sent toContract Laboratories for a full priority pollutant scan.
• Groundwater (Monitoring Wells) - January, 1985
All drilling Phase III monitoring wells (TY-116 to TY-122) and selectedPhase II wells (TY-105, TY-205 and TY-114) were sampled onJanuary 17, 1985. Seventeen groundwatar samples were forwarded toContract Laboratories for a full priority pollutant scan,
Ll-2
,, 000250
004V*1
••-•t:;MM*DRAFT
LU DESCRIPTION OF THE TABLES
«
Table LI-1 Is the detailed scope of the overall sampling program listingall of the media sampled In chronological order. It segregates the samplesby media In the following rational order ambient air, surface water andsediments, sub-surface soils, groundwater - by aquifer under and aroundthe fill areas, and residential well groundwater. As an adjunct to thesampling scope, check lists of chemical analytical parameters for whichthe samples were tested are appended.
Table LI-2 Is a check list of all the organic contaminants divided Intovolatlles, semi-volatiles (add and base/neutral extra-tables), pesticidesand PCBs, and dloxln.
table L1-3 la a check list of the analyzed Inorganic contaminants listed bytasks which .are relajtad to the chemical analytical methods uaad In thelaboratory. '
0041«5
S.kfi&'•'J&-
000251
il$$i
8Q300Q'r
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!i s il5 1! iilllfi i III ' i?l 1 jjso *1 llolfoa I ••lun
S
, 1 1
*1 ! •^s M #II 1 § §1 -111 fi 1 "a "§ a a So< C l/j <fl U) V)V1 •.!•.
e_ s s s
!'- !- 00416S_ i - £
\~
.«3r
I !
T TJ. ! 1}i R z B iii"! •- S dri _ 2 n .'
- . - .I 3 I S |S |Ii . S . S. Ifo o a a Q Q P £I a a a si as
.•" 11-?;,
l 1 I
004167
\-
u J
:SBl
C « J I J"«_ » 1Be >> C el"" f!fii <"<• '"JIT" * i
13 If S Ijg }ll . J.|f _j._ss*;11 ig n mil5hh ghHh gg g'g, 3g =
.B
o£ 5S o
I 1004168
*
Itassooo
" JH ' ' - -
HI 1 . i !5 11.7 i KQ d • SS 1
p"Ss i sii»i mi £u • u • u 0 » • H « -a
!a.S?! ._ifi ' ' • 5
-"""
f
ii It
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3 !.ls ; ' «sl^ll I g__5£__ § I
0 - 1 >
J J j • fjl II Jj. jI! II II Ji __
i • Ufi • il 1 1 i 11s 15
11004170
.,
DRAFT
TABLE LI-2
CHECKLIST OF ORGANIC CHEMICAL POLLUTANTSANALYZED - FULL PRIORITY POLLUTANT SCAN
EEI CAS* ,_____yolatllas_____ _PP£ CAS # . ,____Pesticides______
(2V) 107-02-8 acroleln (89P) 309-00-2 aldrln(3V) 107-13-1 acrylonltrlle (90P) 60-57-1 dlaldrln(4V) 71-43-2 benzene (91P) 57-74-9 chlordane(6V) 56-23-5 carbon tetrachlorlde (92P) 50-29-3 4,4'-DDT(7V) 108-90-7 chlorobenzene , (93P) 72-65-9 4,4'-DDE(10V) 107-06-2 1,2-dlBhloroethane (B4P) 72-64-8 4,4'-DDD(11V) 71-66-6 1,1,1-trlchloroethane (95P) 116-29-7 -endosulfan(13V) 75-34-3 1,1-dlchloroathane (96P) 116-29-7 -endosulfan(14V) 79-00-5 1,1,2-trlchloroethane (97P) 1031-07-8 endosulfan aulfate(15V) 79-34-5 1,1,2,2-tetrachloroathane (98P) 72-20-8 endrln(16V) 76-00-3 chloroethane (99P) 7421-93-4 endrln aldehyde(19V) 110-75-8 2-chloroethylvlnyl ether (100P) 76-44-8 heptachlor(23V) 67-66-3 chloroform (10'IP) 1024-57-3 heptachlor epoxide(29V) 75-35-4 1,1-dlohloroethene (102P) 319-84-6 -BHC(30V) 166-60-5 tran8-1,2-dlchloroethene (103P) 319-85-7 -BHC'32V) 78-87-5 1,2-dichloropropane (104P) 319-86-8 -BHC3V) 10061-02-6 trans-1,3-dlchloropropene (105P) B8-BB-9 -BHC (llndane) . '
• 10061-01-05 cls-1,3-dlc'hloropropene (106P) 53469-21-8 PCB-1242 • .(3BV) 100-41-4 ethylbenzene (107P) 11097-69-1 PCB-1254 I-(44V) 75-09-2 methylene chloride (108P) 11104-2Q-2 PCB-1221(45V) 74-87-3 chloromethane (109P) 11141-16-5 PCB-1232(46V) 74-83-9 bromomethane (110P) 12672-29-6 PCB-1248(47V) 75-25-2 bromoform (111P) 11096-82-5 PCB-1260(48V) 75-27-4 bromodlchloromethane (112P) 12674-11-2 PCB-1016(49V) 78-69-4 fluorotrlchloromethane (113P) 8001-35-2 toxaphene(50V) 75-71-8 dlchlorodlfluoromethane(51V) 124-48-1 chloradibromomethane(85V) 127-18-4 tstrachloroethene PP # CAS # .____Dloxlns____§(86V) 108-88-3 toluene(87V) 79-01-6 trichloroethene (129B) 1746-01-6 2,3,7,8-tetrachlorodlbenzo-p-dloxin(88V) 75-01-4 vinyl chloride
67-64-1 acetone ,78-93-3 2-butanone76-18-0 carbon dlsulflde519-78-6 2-hexanone108-10-1 4-methyl-2-pentanone100-42-5 styrene108-06-4 vinyl acetate1330-20-7 total xylanes
004171OQoar>7> J>
litDRAFT
TABLE LI-2CHECKLIST OF ORGANIC CHEMICAL POLLUTANTSANALYZED - FULL PRIORITY POLLUTANT SCANPAGE TWO
PP__ CAS # Volatlles_____ PP * CAS i». ____PBStleldaa____
(21A) 88-06-2 2,4,6-trichlorophenol (82B) 87-68-3 hexachlorobutadlane(22A) 59-50-7 p-chloro-m-cresol (53B) 77-47-4 hexachlorocyclopentadlene(24A) 95-57-8 2-chlorophenol (54B) 78-59-1 isophorono(31A) 120-83-2 2,4-dlchlorophenol (55B) 91-20-3 naphthalene(34A) 105-67-9 2,4-dlmethylphenol (56B) 98-95-3 nitrobenzene(57A) 88-75-5 2-nltrophenol .(6IB) 62-75-9 N-nltrosodlmethylamlne(58A) 100-02-7 4-nltrophenol (62B) 86-30-8 N-nltrosodlphenylamlne(59A) 51-28-5 2,4-dlnltrophenol (63B) 621-64-7 N-nltrosodipropylamlne(60A) 534-52-1 4,6-dlnltro-2-methylphenol (66B) 117-81-7 bis (2-ethylhexyl) phthalate(64A) 87-86-5 pentachlorophenol (678) 85-68-7 benzyl butyl phthalate(66A) 108-95-2 phenol (68B) 64-74-2 dl-n-butyl phthalate
65-85-0 benzole add (69B) 117-84-0 dl-n-octyl phthalata95-48-7 2-methylphenol (70B) 84-66-2 dlethyl phthalate108-39-4 4-methylphenol ' (71B) 131-11-3 dimethyl phthalate95-95-4 2,4,5-trlchlorophenol (728) 56-55-3 benzo(a)anthracene
(IB) 83-32-9 acenaphthene (73B) 50-32-8 benio(a)pyrene3) 92-87-5 benzldine • (74B) 205-99-2 benzo(b)fluoranthane
IdB) 120-82-1 1,2,4-trlchlorobenzene • (75B) 207-08-9 benzo(k)fluoranthana •(9B) 118-74-1 hexachlorobenzene (768) 218-01-9 chrysene !•.(12B) • 67-72-1 hexachlorbethane (77B) 208-96-8 acenaphthylene(18B) • 111-44-4 bls(2-chloroethyl)ether (7BB) 120-12-7 anthracene(208) 91-58-7 2-chloronaphthalene (79B) 191-24-2 benzo(ghl)perylen8(25B) 96-50-1 1,2-dlchlorobenzene (BOB) 86-73-7 fluorene(268) 541-73-1 1,3-dlchlorobenzene (BIB) 85-01-8 phananthrene(27B) 106-46-7 1,4-dichlorobenzene (82B) 53-70-3 dlbenzo(a,h)anthracene(28B) ' 91-94-1 3,3'-dlchlorobenzldlne (83B) 193-39-5 lndeno(1,2,3-cd)pyrene(35B) 121-14-2 2,4-dlnltrotoluene (B4B) 129-00-0 pyrene(36B) 606-20-2 2,6-dlnltrotoluene 62-53-3 aniline(378) 122-66-7 l,2-dlphenylhydrazln8 100-61-6 benzyl alcohol(398) 206-44-0 fluoranthene 106-47-8 4-chloroanlline(40B) 7005-72-3 4-chlorophenyl phenyi ether 132-64-9 dlbenzofuran(41B) 101-55-3 4-bromophenyl phanyl ethar 91-57-6 2-methylnaphthalene(42B) 39638-32-9 bis (2-chlorolsopropyl) ether 68-74-4 2-nltroanlllne(438) 111-91-1 bis (2-chloroethoxy) methane 99-09-2 3-nltroaniline
100-01-6 4-nltroanlllne
004172
* 18 000258
n TABLE L1-3
CHECKLIST OF INORGANIC CHEMICAL POLLUTANTSANALYZED - FULL PRIORITY POLLUTANT SCAN
(Elements to be Identified and Measured)
1, Aluminum 1. Arsenic2, Chromium 2, Antimony3, Barium 3, Selenium4. Beryllium 4, Thallium5, Cobalt 5, Mercury6. Coppar 6, Tin r_7, iron .7, Cadmium ' '•'•8, Nickel 8, Lead9, Manganese•10: Zinc1 1 , Bofop ' , . , . . ' J£&!_.12, Vanadium13, silver •!. Ammonia
2, Cyanide3, Sulllde
00
APPENDIX L2
AMBIENT AIR SAMPLING PROGRAM
L2 INTRODUCTION
Table L2-1 Sampling Locations - Ambient AirTable L2-2 Characterizations of Ambient Air Sampling PointsTable L2-3 Ambient Air Samples - Chemical Analytical Results
004174ooosijo
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DRAFTL2 INTRODUCTION
Flgura 6-2 shows the location of the sampling points on a site map sketch thatIncludes the extent of the burled wastes, Flgura 5-1 shows all media samplinglocations,
Table L2-1 Is a tabulated list of the sampling locations and a brief locationdescription, Table L2-2 provides a more detailed description of the samplinglocations listing the attributes expected to Impinge on the air quality,
Chemical analytical results are tabulated In Table U-3, where they are expressedIn volume/volume ratios (ppb) and In mass/unit volume of ambient air(ug/m3 - mlcrograms per cubic meter),
004175 |„ 19 0002G1 I
A -^\- TABLE L2-2
CHARACTERIZATION OF AMBIENT AIR SAMPLING POINTSTYBOUTS CORNER LANDFILL SITE
A-1 Sampling point located near entrance gate In close proximity of the fillboundary and Route 71,
A-2 Sampling point located In an abandoned borehole near Wells TY-102 andTY-202.
A-3 Sampling point located downwind of Monitoring Well MP-2, MP-2 was thesource of organic vapors as measured by an OVA.
A-4 Sampling point located upwind of Monitoring Well MP-2 as described forA-3,
A-5 Sampling point located at prospective field trailer parking area. Sampleswere taken to establish air quality at the sampling area for tho RemedialInvestigation,
A-6 Sampling point located In a ditch containing leachate discharges,A-7 Sampling point located at the toe of the landfill (between TY-303 and
TY-205) In an area containing leachate discharge. ' • •A-B Sampling point located In marsh (east of TY-105) to provide an Indication
of mechanisms acting on .ambient air from the leachate 'discharges andreceiving reservoir,
A-9 Duplicate of A-5,
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APPENDIX 13
SURFACE WATER/SEDIMENT SAMPLING AND ANALYSIS
13 DESCRIPTION OF SURFACE WATER ANDSEDIMENT SAMPLING PROGRAM
Table L3.-.T Surface Water and Sediment Sampling LocationsTable L3-2 Surface Water - Chemical Analytical ResultsTable L3-3 Sediments - Chemical Analytical Results
004180
i
IllL3 DESCRIPTION OF SURFACE WATER AND
SEDIMENT SAMPLING PROGRAM
The surface water and sediment sampling program was designed to provide ageneral overview of the quality of surface water entering, moving through the site,and discharging Into the Red Lion Creek Marsh. Emphasis was directed towardpotential environmental impacts on the marsh rather than determining migrationpaths for onslte contamination, Therefore, selection of the sampling locationsreflects this major objective. Sample locations were clustered around the maindrainage channels leading to the marsh, See Figure 3-1 for a map showing thelocation of the sampling points, Table L3-1 lists the samples, and the character oftheir locations are described.
Six surface water (SW-001 to 004, SW-006, SW-012, and SW-013) and threesediment samples (SW-001, SD-004, and SD-013) were collected from the head ofPigeon Run to its confluence with Red Lion Creek,
One upstream (above the site) surface, water sample (SW-OOS) was collected from • •' , j^yRed Lion Creek. Samples from four springs (SW-007 to SW-010) that feed the, • . pmarsh were collected and analyzed. Sediment samples were collected at the same | >location as some of the surface water samples. \:i$
A sample from one leachate seep flowing Into the marsh (SW-014) and a sediment p-1'sample (SD-014) we're collected and analyzed with this group of environmental i'.;samples, This location (SW-014) was tested by R, E, Wrightl3) during the ;'.development of the RAMP, It Is more appropriate to Include the results for the -leachate seep analysis with the other leachate sample results In Table L4-1, :,
IChemical analytical results reported by the laboratories are listed In Table L3-2 '/,for the surface water samples and Table L3-3 for the sediments, The results arearranged according to the drainage pattern of surface runoff, going from *..'background locations to sampling spots affected by surface drainage, and those r.associated with groundwater discharge,
004181L3-1
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TABLE L3-1 p$-,,
SURFACE WATER AND SEDIMENT SAMPLING LOCATIONS 1 ''>]TYBOUTS CORNER LANDFILL SITE Kfy. I
Sample No,Surface LocationWater Sediment Map.Coordinates .______Remarks _____.
SW-001 SD-001 E 432 560 N 588 060 Pigeon Run-Upgradient of site
SW-002 E 432 390 N 587 275 Pigeon Run
SW-003 E 432 600 N 586 900 Pigeon Run
SW-004 SD-004 E 433 090 N 686 510 Pigeon Run
SW-005 SD-005 E 431 830 N 584 850 Red Lion Creek-Upgradlent of, Site
SW-006 E 439 935 N 565 415 Pigeon Run-Below west fill
SW-OQ7 • E 436 115 N 586 730 Unnamed Creek flowing Into RedLion Marsh (east of site)
SW-008 E 435 830 N 586 810 Spring east of site
SW-009 ' E 435 680 N 586 360 Spring east of site
SW-010 E435 485 N 586 205 Spring east of site
SW-011 E 435 410 N 585 640 Unnamed Creek-Downstream ofSW-Q07 (east of site)
SW-D12 E 433 190 N 585 085 Pigeon Run-Just upstream of, confluence with Red Lion Creek
SW-013 SD-013 E 433 200 N 584 875 Pigeon Run and Red Lion CreekConfluence
SD-Q14 E 433 615 N 586 240 Sedlment-Leachate flow
SW-016 SD-01S E 433 655 N 584 890 Red Lion Marsh
Notes;1, See Figure 5-1 for location of all sample points and the coordinate grid,
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APPENDIX L4
LEACHATE SAMPLING PROGRAM
L4 LEACHATE SAMPLING PROGRAM
Table L4-1 List of Leachate Sample LocationsTable L4-2 Loachates - Chemical Analytical Results
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9
Five leachate samples were collected at a variety of onslte locations. Samplinglocations are tabulated In Table L4-1 by sample numbers and map grid coordinates,Another'sample (SW-014) was collected as part of the surface water samplingprogram, Figure 6-1, showing the general sample locations, Is provided forconvenience In reading the report. • '..".','
ATable L4-2 contained the analytical results of the leachate samples, £j|:v
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LEACHATE SAMPLE LOCATIONS ^TYBOUTS CORNER LANDFILL SITE
LocationSample No. Map Coordinates ______Remarks_________
TCL-1 N 586 510 E 433 445
TCL-2 N 586 390 E 433 360
TCL-3 N 586 450 E 433 335
TCL-4 ' N 685 450 E 433 335 Taken at same location as TCL-3
TCL-5 N 58S 400 E 433 400}'<••(:•
SW-014 N 585 240 E 433 620 | i
Iifm-Notes: . .1, See Figure 5-1.for location of all media sample points and the coordinate grid,
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APPENDIX L5
SUBSURFACE SOILS SAMPLING PROGRAM
L5 SUBSURFACE SOILS SAMPLING PROGRAM
Table L5-1 • Chemical Analytical Results: Subsurface Soil
004192
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p$lL5.1 SUBSURFACE SOILS SAMPLING PROGRAM k ''''
KA'.P!'
During the drilling program, six soil samples were collected from the borings •,through the main landfill (GW-310 to QW-315 Inclusive). Soils were collected fromthe horizon Immediately below the deposited refuse, It was expected that thesamples would Indicate past migration from the waste matrix and would boIndicative of the "worst case* condition of onslte soils, Table L5-1 tabulates the ''•;'••'..results of the chemical analyses, For locations of the sampling points, seo >-Appendix A6 for monitoring wells, ftfy
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APPENDIX L6
GROUNDWATER SAMPLING PROGRAM
Table L6-1 Chemical Analytical Data: Main Fill AreaTable L6-2 Chemical Analytical Data; Western Fill AreaTable L6-3 Chemical Analytical Data: Residential Wells
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L6 GROUNDWATER SAMPLING PROGRAM
A list of the monitoring well locations appears In Table L6-1, Locations aredefined by map grid coordinates (see Figure 5-1) that were surveyed to the nearest0,001 foot; surface elevation surveyed to the nearest 0,1 foot; and the elevation atthe centerllne of the screen, ,
Aquifer designations are Included for further definition of the monitoring points,Exact geometrical spacing can be obtained from the tabulation of grid coordinatesand elevations. Figure 5-1 shows the approximate location of all groundwatermonitoring locations,
For a scope of the groundwater monitoring program, see Appendix LI andTable L1-1, which Itemizes all of the sampling rounds conducted at the TyboutsCorner Landfill Site, •
Chemical analytical data has been arranged. In the components listed In Table L6-2by aquifer location, The' aquifers are divided into three main categories —Columbia, Potomac Sand No,i, and No, 2, It has also been separated for the "mainfill" and "western fill" areas, There are no monitoring wells in the Columbiaformation at the West fill, The following Is a list of tables that follow, containingthe groundwater chemical analytical data:
Title
L6-3 Groundwater in the West Fill Potomac No. 1 Sand
L6-4 Groundwater In the West Fill Potomac No. 2 Sand
L6-5A Groundwater In the Main Fill Columbia Formation
L6-5B Groundwater Below and Upgradient of the Main Fill ColumbiaFormation
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L6-5C Groundwator Downgradlent of the Main Fill Columbia Formation
L6-6A Groundwater Below the Main Fill Potomac No. 1 Sand
L6-6B Groundwater Upgradlent of the Main Fill Potomac No. 1 Sand
L6-6C Groundwater Downgradlent of the Main Fill Potomac No, 1 Sand
L6-7A Groundwater Downgradiant of tha Main Fill Potomac No. 2 Sand
L6-7B Groundwater Upgradlent of the Main Fill Potomuc No. 2 Sand
L6-2
18 QQ02S4
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DRAFT
TABLE L6-1
GROUNDWATER MONITORING POINT LOCATIONTYBOUTS CORNER LANDFILL SITE
Monitoring Location By Grid Coordinates GroundWell No,.,. ~ Y (North) u X (East) , Elevation (ft) Agulfer Daslgnatlon
TY101 588,109,152 435,043,872 58,6 Potomac No, 2 SandTY102 587,157,618 434,430,358 61,9 Potomac No, 1 SandTY103 586,260,969 433,981,807 49,7 Potomac No, 1 SandTY104 586,752,052 433,985.954 37,8 Potomac No, 2 SandTY1Q6 685,414,955 433,476,365 14,0 ' Potomac No, 2 SandTY1Q7 686,292,553 433,312,497 29,6 Potomac No, 2 SandTY 108 587, 321,836 433, 018,425 357 Potomac No, 2 SandTY 110 588,372.389 434,152,586 55,7 Potomac No, 2 SandTY 112 586,699.136 432,963,573 29,0 Potomac No, 2 SandTY 113 585,918,679 432,297,196 19.4 Potomac No, 2 SandTY114 586,469,886 434,677,486 56,0 Potomac No, 1 Sand
TY201 588,088.726 434,983,831 59,1 ColumbiaTY202 ' 587,138,459 434,443.743 62,0 Columbia .TY203 586,248,332 433,959,867 46,7 ColumbiaTY204 585,752.47. 433,979.211 37,8 ' Potomac No, L SandTY205 585,435.913 433,488.679 14.8 Potomac No, 1 SandTY206 684,689,765 433,060.108 19,0 Potomac No, 2 SandTY207 586,254,057 433,291,123 29,7 Potomac No, 1 SandTY208 587,313,813 433,005,337 35,46 Potomac No. 1 SandTY209 587,909,450 433,097,470 36,4 Potomac No, 1 Sand :TY210 588,358,456 434,138,264 55,7 Potomac No, 1 Sand -•TY211 588,285,940 434,525.190 62,81 Potomac No. 1 SandTY212 566,880,108 432,971,239 28,7 Potomac No, 1 SandTY213 585,960,892 432,288,797 20,1 Potomac No, 1 SandTY214 586,486.407 434,675,838 56,6 ColumbiaTY215 587,458,935 434,953,960 60,2 Columbia
DRAFTill
"
TABLE L6-1GROUNDWATER MONITORING POINT LOCATIONTYBOUTS CORNER LANDFILL SITEPAGE TWO
Monitoring Location By Grid Coordinates Ground' Wall No. " Y (North) X (East) ,J3S_S!_D_(1SL_ Aquifer DBslnnallgn
TY 303 585,537,580 433,372,572 19.9 Potomac No, 1 SandTY304 585,381.342 432,736,266 12.4 I'otomac No, 1 SandTY 307 585,724,303 432,459,463 18.1 Potornfic No, 1 SandTY 309 585,683,902 432,6.10,606 Potomac No, 1 SandTY310 586,530,026 433,823,123 62.2 Potomac No, 1 SandTY311 586,801,439 434,053,630 56.1 ColumbiaTy312 587,336.238 434,140,856 57.6 Potomac No, 1 SandTY313 587,882.700 434,043,713 66.9 ColumbiaTY314 588,131,572 434,331,368 63,8 ColumbiaTY315 587,264,123 433,567,076 47,0 ColumbiaP5 587,691,737 434,265,573 58.1 Columbia . i.V;;MP2 587,193,236 433,641.485 50.6 ColumbiaMP3 588,074,048 434,043,742 55,7 ColumbiaMP3A 588,073,927 434,052,984 55.8 Potomac No, 1 SandMP 10 587,570,559 433,110,936 38.4 Columbia ' . '.MP 11 . 587,,922,225 433,610,129 44.2 Columbia
TY. 116A 584,444,782 434,514,638 34.4 Potomac No, 2 SandTY 116B 584,468,902 434,490,072 31.7 Potomac No, 2 SandTY 116C 584,432,837 434,513,174 35,8 Potomac No, 1 SandTY 117A 588,001,202 433,205,615 34,2 Potomac No, 2 SandTY 117B 588,005,082 433, 173,953 34.4 Potomac No, 2 SandTY 118A 586,768,662 435,687,841 28,1 Potomac No, 2 SandTY 118B 586, 810,264 435, 712,495 28.5 Potomac No, 1 SandTY 119A 585,192,848 434,586,481 5,6 Potomac No, 2 Sand
236
DRAFTKip
TABLE L6-1 'GROUNDWATER MONITORING POINT LOCATIONTYBOUTS CORNER LANDFILL SITEPAGE THREE
Monitoring Location By Grid Coordinates GroundWell No. Y (North) X (East) Elevation (ft) Aquifer Designation
TY 119B 585, 207.826 434, 583,336 6,4 Potomac No, 1 SandTY 120A 585,261.665 433,829.887 8,0 Potomac No, 2 SandTY 120B 585,269,622 433,851.418 8.8 Potomac No. 1 SandTY 121A 584,700.232 433,450.945 15.6 Potomac No. 2 SandTY 121B 684,684,232 433,453,224 16,1 Potomac No. 1 SandTY 122 584,829,227 432,436,735 15,8 Potomac No, 2 Sand
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APPENDIX L7
* RESIDENTIAL WELL SAMPLING
L7 RESIDENTIAL WELLS
Table L7-1 Residential Wells - Chemical Analytical Results
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L7 RESIDENTIAL WELLS
Table U~1 shows a tabulation of the results of tha residential wells that wereIncluded In tho sampling program, Table L7-1 In Appendix Includes the samplingdetails end tho scope of the program,
Samples were taken from 9 of the 24 wells during the Remedial Action Master Plan(RAMP) phase of the overall project It was during this sampling that a number ofvolatile organic contaminants were found In the Wagner and Martin wells,
For Inclusion of the chemical data In this risk assessment, the validation protocolscovering the analytical laboratory sample management, methods, and measurementare sufficiently comprehensive and relevant to assure the soundness of the data,Any observations deemed to be acceptable or acceptable with some qualification,have been Included In the tabulations, All other categories of the validation havenot been used. ' •
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