Lake Linden
200
ANALYTICAL REPORT Client: MDNRE Work Order: 1110319 Project: C&H Lake Linden Ops Description: Laboratory Services Client Sample ID: SS-01 Sampled: 10/10/11 14:15 Lab Sample ID: 1110319-01 Sampled By: J. Spielberg Matrix: Soil Received: 10/17/11 17:00 Unit: ug/kg dry Prepared: 10/18/11 By: JDM Dilution Factor: 1 Analyzed: 10/18/11 By: JDM QC Batch: 1111418 Analytical Batch: 1J19045 Percent Solids: 60 Volatile Organic Compounds by EPA Method 8260B (Continued) Analytical CAS Number Analyte Result RL MDL 79-01-6 Trichloroethene 83U 83 9.4 75-69-4 Trichlorofluoromethane 170U 170 12 96-18-4 1,2,3-Trichloropropane 170U 170 68 *526-73-8 1,2,3-Trimethylbenzene 410U 410 9.5 95-63-6 1,2,4-Trimethylbenzene 170U 170 9.4 108-67-8 1,3,5-Trimethylbenzene 170U 170 9.6 75-01-4 Vinyl Chloride 66U 66 11 179601-23-1 Xylene, Meta + Para 170U 170 17 95-47-6 Xylene, Ortho 83U 83 12 Surrogates: % Recovery Control Limits Dibromofluoromethane 104 76-108 1,2-Dichloroethane-d4 103 84-115 Toluene-d8 98 90-107 4-Bromofluorobenzene 99 84-110 *See Statement of Data Qualifications Page 4 of 199 This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested. 5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
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Transcript of Lake Linden
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-01 Sampled: 10/10/11 14:15Lab Sample ID: 1110319-01 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/18/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 60
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 83U 83 9.4
75-69-4 Trichlorofluoromethane 170U 170 12
96-18-4 1,2,3-Trichloropropane 170U 170 68
*526-73-8 1,2,3-Trimethylbenzene 410U 410 9.5
95-63-6 1,2,4-Trimethylbenzene 170U 170 9.4
108-67-8 1,3,5-Trimethylbenzene 170U 170 9.6
75-01-4 Vinyl Chloride 66U 66 11
179601-23-1 Xylene, Meta + Para 170U 170 17
95-47-6 Xylene, Ortho 83U 83 12
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 4 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-01 Sampled: 10/10/11 14:15Lab Sample ID: 1110319-01 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 60 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 5 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02 Sampled: 10/10/11 12:32Lab Sample ID: 1110319-02 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/18/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 100
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 56U 56 6.8
108-86-1 Bromobenzene 110U 110 6.3
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.7
75-25-2 Bromoform 110U 110 8.6
74-83-9 Bromomethane 47J 230 13
104-51-8 n-Butylbenzene 56U 56 5.9
135-98-8 sec-Butylbenzene 56U 56 5.9
98-06-6 tert-Butylbenzene 56U 56 6.3
75-15-0 Carbon Disulfide 280U 280 5.7
56-23-5 Carbon Tetrachloride 56U 56 5.6
108-90-7 Chlorobenzene 56U 56 13
*75-00-3 Chloroethane 280U 280 12
67-66-3 Chloroform 56U 56 6.4
74-87-3 Chloromethane 53J 280 7.5
110-82-7 Cyclohexane 280U 280 7.4
96-12-8 1,2-Dibromo-3-chloropropane 56U 56 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 56U 56 8.4
74-95-3 Dibromomethane 280U 280 6.5
110-57-6 trans-1,4-Dichloro-2-butene 56U 56 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.7
541-73-1 1,3-Dichlorobenzene 110U 110 6.2
106-46-7 1,4-Dichlorobenzene 110U 110 7.5
*75-71-8 Dichlorodifluoromethane 280U 280 8.6
75-34-3 1,1-Dichloroethane 56U 56 5.6
107-06-2 1,2-Dichloroethane 56U 56 6.0
75-35-4 1,1-Dichloroethene 56U 56 8.4
156-59-2 cis-1,2-Dichloroethene 56U 56 7.0
Continued on next page
*See Statement of Data Qualifications
Page 6 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02 Sampled: 10/10/11 12:32Lab Sample ID: 1110319-02 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/18/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 56U 56 6.1
78-87-5 1,2-Dichloropropane 56U 56 7.2
10061-01-5 cis-1,3-Dichloropropene 56U 56 9.2
10061-02-6 trans-1,3-Dichloropropene 56U 56 6.3
100-41-4 Ethylbenzene 56U 56 7.7
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2800U 2800 18
*74-88-4 Iodomethane 120 110 9.0
98-82-8 Isopropylbenzene 280U 280 8.2
*108-20-3 Isopropyl Ether 280U 280 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.7
1634-04-4 Methyl tert-Butyl Ether 280U 280 7.4
75-09-2 Methylene Chloride 110U 110 6.5
78-93-3 2-Butanone (MEK) 840U 840 29
*91-57-6 2-Methylnaphthalene 370U 370 8.6
108-10-1 4-Methyl-2-pentanone (MIBK) 2800U 2800 6.6
*91-20-3 Naphthalene 140J 370 7.7
*994-05-8 tert-Amyl Methyl Ether 280U 280 2.7
*637-92-3 Ethyl tert-Butyl Ether 280U 280 3.9
103-65-1 n-Propylbenzene 110U 110 6.4
100-42-5 Styrene 56U 56 5.9
*75-65-0 t-Butanol 2800U 2800 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 56U 56 13
127-18-4 Tetrachloroethene 56U 56 5.7
109-99-9 Tetrahydrofuran 1100U 1100 37
108-88-3 Toluene 110U 110 8.1
*87-61-6 1,2,3-Trichlorobenzene 370U 370 6.8
120-82-1 1,2,4-Trichlorobenzene 370U 370 7.3
71-55-6 1,1,1-Trichloroethane 56U 56 6.5
79-00-5 1,1,2-Trichloroethane 56U 56 7.5
Continued on next page
*See Statement of Data Qualifications
Page 7 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02 Sampled: 10/10/11 12:32Lab Sample ID: 1110319-02 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/18/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 56U 56 6.4
75-69-4 Trichlorofluoromethane 110U 110 8.3
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 280U 280 6.5
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.4
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.5
75-01-4 Vinyl Chloride 45U 45 7.5
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 56U 56 7.9
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 8 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02 Sampled: 10/10/11 12:32Lab Sample ID: 1110319-02 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 89 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 9 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02D Sampled: 10/10/11 12:32Lab Sample ID: 1110319-03 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 120J 1100 100
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 56U 56 6.7
108-86-1 Bromobenzene 110U 110 6.3
74-97-5 Bromochloromethane 110U 110 6.7
75-27-4 Bromodichloromethane 110U 110 5.7
75-25-2 Bromoform 110U 110 8.5
74-83-9 Bromomethane 53J 220 13
104-51-8 n-Butylbenzene 56U 56 5.8
135-98-8 sec-Butylbenzene 56U 56 5.8
98-06-6 tert-Butylbenzene 56U 56 6.3
75-15-0 Carbon Disulfide 280U 280 5.7
56-23-5 Carbon Tetrachloride 56U 56 5.6
108-90-7 Chlorobenzene 56U 56 13
*75-00-3 Chloroethane 280U 280 12
67-66-3 Chloroform 56U 56 6.4
74-87-3 Chloromethane 54J 280 7.5
110-82-7 Cyclohexane 280U 280 7.4
96-12-8 1,2-Dibromo-3-chloropropane 56U 56 13
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 56U 56 8.4
74-95-3 Dibromomethane 280U 280 6.5
110-57-6 trans-1,4-Dichloro-2-butene 56U 56 4.9
95-50-1 1,2-Dichlorobenzene 110U 110 5.7
541-73-1 1,3-Dichlorobenzene 110U 110 6.2
106-46-7 1,4-Dichlorobenzene 110U 110 7.5
*75-71-8 Dichlorodifluoromethane 280U 280 8.5
75-34-3 1,1-Dichloroethane 56U 56 5.6
107-06-2 1,2-Dichloroethane 56U 56 5.9
75-35-4 1,1-Dichloroethene 56U 56 8.4
156-59-2 cis-1,2-Dichloroethene 56U 56 7.0
Continued on next page
*See Statement of Data Qualifications
Page 10 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02D Sampled: 10/10/11 12:32Lab Sample ID: 1110319-03 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 56U 56 6.1
78-87-5 1,2-Dichloropropane 56U 56 7.2
10061-01-5 cis-1,3-Dichloropropene 56U 56 9.2
10061-02-6 trans-1,3-Dichloropropene 56U 56 6.3
100-41-4 Ethylbenzene 56U 56 7.6
60-29-7 Ethyl Ether 220U 220 11
591-78-6 2-Hexanone 2800U 2800 18
*74-88-4 Iodomethane 150 110 9.0
98-82-8 Isopropylbenzene 280U 280 8.2
*108-20-3 Isopropyl Ether 280U 280 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.6
1634-04-4 Methyl tert-Butyl Ether 280U 280 7.4
75-09-2 Methylene Chloride 110U 110 6.5
78-93-3 2-Butanone (MEK) 840U 840 28
*91-57-6 2-Methylnaphthalene 370U 370 8.5
108-10-1 4-Methyl-2-pentanone (MIBK) 2800U 2800 6.6
*91-20-3 Naphthalene 140J 370 7.6
*994-05-8 tert-Amyl Methyl Ether 280U 280 2.7
*637-92-3 Ethyl tert-Butyl Ether 280U 280 3.9
103-65-1 n-Propylbenzene 110U 110 6.4
100-42-5 Styrene 56U 56 5.8
*75-65-0 t-Butanol 2800U 2800 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 56U 56 13
127-18-4 Tetrachloroethene 56U 56 5.7
109-99-9 Tetrahydrofuran 1100U 1100 37
108-88-3 Toluene 110U 110 8.1
*87-61-6 1,2,3-Trichlorobenzene 370U 370 6.7
120-82-1 1,2,4-Trichlorobenzene 370U 370 7.3
71-55-6 1,1,1-Trichloroethane 56U 56 6.5
79-00-5 1,1,2-Trichloroethane 56U 56 7.5
Continued on next page
*See Statement of Data Qualifications
Page 11 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02D Sampled: 10/10/11 12:32Lab Sample ID: 1110319-03 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 56U 56 6.4
75-69-4 Trichlorofluoromethane 110U 110 8.3
96-18-4 1,2,3-Trichloropropane 110U 110 46
*526-73-8 1,2,3-Trimethylbenzene 280U 280 6.4
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.4
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.5
75-01-4 Vinyl Chloride 45U 45 7.5
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 56U 56 7.9
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 12 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-02D Sampled: 10/10/11 12:32Lab Sample ID: 1110319-03 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 89 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 13 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-03 Sampled: 10/10/11 13:52Lab Sample ID: 1110319-04 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 74
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 220J 1300 120
107-13-1 Acrylonitrile 130U 130 27
71-43-2 Benzene 67U 67 8.1
108-86-1 Bromobenzene 130U 130 7.5
74-97-5 Bromochloromethane 130U 130 8.1
75-27-4 Bromodichloromethane 130U 130 6.9
75-25-2 Bromoform 130U 130 10
74-83-9 Bromomethane 48J 270 16
104-51-8 n-Butylbenzene 67U 67 7.0
135-98-8 sec-Butylbenzene 67U 67 7.0
98-06-6 tert-Butylbenzene 67U 67 7.5
75-15-0 Carbon Disulfide 340U 340 6.9
56-23-5 Carbon Tetrachloride 67U 67 6.7
108-90-7 Chlorobenzene 67U 67 15
*75-00-3 Chloroethane 340U 340 14
67-66-3 Chloroform 67U 67 7.7
74-87-3 Chloromethane 340U 340 9.0
110-82-7 Cyclohexane 340U 340 8.9
96-12-8 1,2-Dibromo-3-chloropropane 67U 67 16
124-48-1 Dibromochloromethane 130U 130 20
106-93-4 1,2-Dibromoethane 67U 67 10
74-95-3 Dibromomethane 340U 340 7.8
110-57-6 trans-1,4-Dichloro-2-butene 67U 67 5.9
95-50-1 1,2-Dichlorobenzene 130U 130 6.9
541-73-1 1,3-Dichlorobenzene 130U 130 7.4
106-46-7 1,4-Dichlorobenzene 130U 130 9.0
*75-71-8 Dichlorodifluoromethane 340U 340 10
75-34-3 1,1-Dichloroethane 67U 67 6.7
107-06-2 1,2-Dichloroethane 67U 67 7.1
75-35-4 1,1-Dichloroethene 67U 67 10
156-59-2 cis-1,2-Dichloroethene 67U 67 8.4
Continued on next page
*See Statement of Data Qualifications
Page 14 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-03 Sampled: 10/10/11 13:52Lab Sample ID: 1110319-04 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 74
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 67U 67 7.3
78-87-5 1,2-Dichloropropane 67U 67 8.6
10061-01-5 cis-1,3-Dichloropropene 67U 67 11
10061-02-6 trans-1,3-Dichloropropene 67U 67 7.5
100-41-4 Ethylbenzene 67U 67 9.2
60-29-7 Ethyl Ether 270U 270 13
591-78-6 2-Hexanone 3400U 3400 22
*74-88-4 Iodomethane 130 130 11
98-82-8 Isopropylbenzene 340U 340 9.8
*108-20-3 Isopropyl Ether 340U 340 2.6
99-87-6 4-Isopropyltoluene 130U 130 9.2
1634-04-4 Methyl tert-Butyl Ether 340U 340 8.9
75-09-2 Methylene Chloride 130U 130 7.8
78-93-3 2-Butanone (MEK) 1000U 1000 34
*91-57-6 2-Methylnaphthalene 440U 440 10
108-10-1 4-Methyl-2-pentanone (MIBK) 3400U 3400 8.0
*91-20-3 Naphthalene 170J 440 9.2
*994-05-8 tert-Amyl Methyl Ether 340U 340 3.2
*637-92-3 Ethyl tert-Butyl Ether 340U 340 4.6
103-65-1 n-Propylbenzene 130U 130 7.7
100-42-5 Styrene 67U 67 7.0
*75-65-0 t-Butanol 3400U 3400 170
630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 67U 67 15
127-18-4 Tetrachloroethene 67U 67 6.9
109-99-9 Tetrahydrofuran 1300U 1300 45
108-88-3 Toluene 130U 130 9.7
*87-61-6 1,2,3-Trichlorobenzene 440U 440 8.1
120-82-1 1,2,4-Trichlorobenzene 440U 440 8.8
71-55-6 1,1,1-Trichloroethane 67U 67 7.8
79-00-5 1,1,2-Trichloroethane 67U 67 9.0
Continued on next page
*See Statement of Data Qualifications
Page 15 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-03 Sampled: 10/10/11 13:52Lab Sample ID: 1110319-04 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 74
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 67U 67 7.7
75-69-4 Trichlorofluoromethane 130U 130 10
96-18-4 1,2,3-Trichloropropane 130U 130 56
*526-73-8 1,2,3-Trimethylbenzene 340U 340 7.8
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.7
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.8
75-01-4 Vinyl Chloride 54U 54 9.0
179601-23-1 Xylene, Meta + Para 130U 130 14
95-47-6 Xylene, Ortho 67U 67 9.4
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 16 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-03 Sampled: 10/10/11 13:52Lab Sample ID: 1110319-04 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 74 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 17 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-04 Sampled: 10/11/11 11:55Lab Sample ID: 1110319-05 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 120J 950 84
107-13-1 Acrylonitrile 95U 95 19
71-43-2 Benzene 47U 47 5.7
108-86-1 Bromobenzene 95U 95 5.3
74-97-5 Bromochloromethane 95U 95 5.7
75-27-4 Bromodichloromethane 95U 95 4.8
75-25-2 Bromoform 95U 95 7.2
74-83-9 Bromomethane 35J 190 11
104-51-8 n-Butylbenzene 47U 47 4.9
135-98-8 sec-Butylbenzene 47U 47 4.9
98-06-6 tert-Butylbenzene 47U 47 5.3
75-15-0 Carbon Disulfide 240U 240 4.8
56-23-5 Carbon Tetrachloride 47U 47 4.7
108-90-7 Chlorobenzene 47U 47 11
*75-00-3 Chloroethane 240U 240 10
67-66-3 Chloroform 47U 47 5.4
74-87-3 Chloromethane 240U 240 6.3
110-82-7 Cyclohexane 240U 240 6.2
96-12-8 1,2-Dibromo-3-chloropropane 47U 47 11
124-48-1 Dibromochloromethane 95U 95 14
106-93-4 1,2-Dibromoethane 47U 47 7.1
74-95-3 Dibromomethane 240U 240 5.5
110-57-6 trans-1,4-Dichloro-2-butene 47U 47 4.2
95-50-1 1,2-Dichlorobenzene 95U 95 4.8
541-73-1 1,3-Dichlorobenzene 95U 95 5.2
106-46-7 1,4-Dichlorobenzene 95U 95 6.3
*75-71-8 Dichlorodifluoromethane 240U 240 7.2
75-34-3 1,1-Dichloroethane 47U 47 4.7
107-06-2 1,2-Dichloroethane 47U 47 5.0
75-35-4 1,1-Dichloroethene 47U 47 7.1
156-59-2 cis-1,2-Dichloroethene 47U 47 5.9
Continued on next page
*See Statement of Data Qualifications
Page 18 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-04 Sampled: 10/11/11 11:55Lab Sample ID: 1110319-05 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 47U 47 5.1
78-87-5 1,2-Dichloropropane 47U 47 6.1
10061-01-5 cis-1,3-Dichloropropene 47U 47 7.8
10061-02-6 trans-1,3-Dichloropropene 47U 47 5.3
100-41-4 Ethylbenzene 47U 47 6.4
60-29-7 Ethyl Ether 190U 190 8.9
591-78-6 2-Hexanone 2400U 2400 15
*74-88-4 Iodomethane 98 95 7.6
98-82-8 Isopropylbenzene 240U 240 6.9
*108-20-3 Isopropyl Ether 240U 240 1.8
99-87-6 4-Isopropyltoluene 95U 95 6.4
1634-04-4 Methyl tert-Butyl Ether 240U 240 6.2
75-09-2 Methylene Chloride 18J 95 5.5
78-93-3 2-Butanone (MEK) 710U 710 24
*91-57-6 2-Methylnaphthalene 310U 310 7.2
108-10-1 4-Methyl-2-pentanone (MIBK) 2400U 2400 5.6
*91-20-3 Naphthalene 310U 310 6.4
*994-05-8 tert-Amyl Methyl Ether 240U 240 2.3
*637-92-3 Ethyl tert-Butyl Ether 240U 240 3.3
103-65-1 n-Propylbenzene 95U 95 5.4
100-42-5 Styrene 47U 47 4.9
*75-65-0 t-Butanol 2400U 2400 120
630-20-6 1,1,1,2-Tetrachloroethane 95U 95 14
79-34-5 1,1,2,2-Tetrachloroethane 47U 47 11
127-18-4 Tetrachloroethene 47U 47 4.8
109-99-9 Tetrahydrofuran 950U 950 32
108-88-3 Toluene 95U 95 6.8
*87-61-6 1,2,3-Trichlorobenzene 310U 310 5.7
120-82-1 1,2,4-Trichlorobenzene 310U 310 6.1
71-55-6 1,1,1-Trichloroethane 47U 47 5.5
79-00-5 1,1,2-Trichloroethane 47U 47 6.3
Continued on next page
*See Statement of Data Qualifications
Page 19 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-04 Sampled: 10/11/11 11:55Lab Sample ID: 1110319-05 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 47U 47 5.4
75-69-4 Trichlorofluoromethane 95U 95 7.0
96-18-4 1,2,3-Trichloropropane 95U 95 39
*526-73-8 1,2,3-Trimethylbenzene 240U 240 5.4
95-63-6 1,2,4-Trimethylbenzene 95U 95 5.4
108-67-8 1,3,5-Trimethylbenzene 95U 95 5.5
75-01-4 Vinyl Chloride 38U 38 6.3
179601-23-1 Xylene, Meta + Para 95U 95 9.6
95-47-6 Xylene, Ortho 47U 47 6.6
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 20 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-04 Sampled: 10/11/11 11:55Lab Sample ID: 1110319-05 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 94 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 21 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-05 Sampled: 10/11/11 11:40Lab Sample ID: 1110319-06 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 130J 1200 110
107-13-1 Acrylonitrile 120U 120 24
71-43-2 Benzene 60U 60 7.2
108-86-1 Bromobenzene 120U 120 6.7
74-97-5 Bromochloromethane 120U 120 7.2
75-27-4 Bromodichloromethane 120U 120 6.1
75-25-2 Bromoform 120U 120 9.1
74-83-9 Bromomethane 50J 240 14
104-51-8 n-Butylbenzene 60U 60 6.2
135-98-8 sec-Butylbenzene 60U 60 6.2
98-06-6 tert-Butylbenzene 60U 60 6.7
75-15-0 Carbon Disulfide 300U 300 6.1
56-23-5 Carbon Tetrachloride 60U 60 6.0
108-90-7 Chlorobenzene 60U 60 14
*75-00-3 Chloroethane 300U 300 13
67-66-3 Chloroform 60U 60 6.8
74-87-3 Chloromethane 300U 300 8.0
110-82-7 Cyclohexane 300U 300 7.9
96-12-8 1,2-Dibromo-3-chloropropane 60U 60 14
124-48-1 Dibromochloromethane 120U 120 18
106-93-4 1,2-Dibromoethane 60U 60 9.0
74-95-3 Dibromomethane 300U 300 7.0
110-57-6 trans-1,4-Dichloro-2-butene 60U 60 5.3
95-50-1 1,2-Dichlorobenzene 120U 120 6.1
541-73-1 1,3-Dichlorobenzene 120U 120 6.6
106-46-7 1,4-Dichlorobenzene 120U 120 8.0
*75-71-8 Dichlorodifluoromethane 300U 300 9.1
75-34-3 1,1-Dichloroethane 60U 60 6.0
107-06-2 1,2-Dichloroethane 60U 60 6.4
75-35-4 1,1-Dichloroethene 60U 60 9.0
156-59-2 cis-1,2-Dichloroethene 60U 60 7.4
Continued on next page
*See Statement of Data Qualifications
Page 22 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-05 Sampled: 10/11/11 11:40Lab Sample ID: 1110319-06 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 60U 60 6.5
78-87-5 1,2-Dichloropropane 60U 60 7.7
10061-01-5 cis-1,3-Dichloropropene 60U 60 9.8
10061-02-6 trans-1,3-Dichloropropene 60U 60 6.7
100-41-4 Ethylbenzene 60U 60 8.2
60-29-7 Ethyl Ether 240U 240 11
591-78-6 2-Hexanone 3000U 3000 20
*74-88-4 Iodomethane 140 120 9.6
98-82-8 Isopropylbenzene 300U 300 8.8
*108-20-3 Isopropyl Ether 300U 300 2.3
99-87-6 4-Isopropyltoluene 120U 120 8.2
1634-04-4 Methyl tert-Butyl Ether 300U 300 7.9
75-09-2 Methylene Chloride 120U 120 7.0
78-93-3 2-Butanone (MEK) 900U 900 30
*91-57-6 2-Methylnaphthalene 400U 400 9.1
108-10-1 4-Methyl-2-pentanone (MIBK) 3000U 3000 7.1
*91-20-3 Naphthalene 400U 400 8.2
*994-05-8 tert-Amyl Methyl Ether 300U 300 2.9
*637-92-3 Ethyl tert-Butyl Ether 300U 300 4.1
103-65-1 n-Propylbenzene 120U 120 6.8
100-42-5 Styrene 60U 60 6.2
*75-65-0 t-Butanol 3000U 3000 150
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 18
79-34-5 1,1,2,2-Tetrachloroethane 60U 60 14
127-18-4 Tetrachloroethene 60U 60 6.1
109-99-9 Tetrahydrofuran 1200U 1200 40
108-88-3 Toluene 120U 120 8.6
*87-61-6 1,2,3-Trichlorobenzene 400U 400 7.2
120-82-1 1,2,4-Trichlorobenzene 400U 400 7.8
71-55-6 1,1,1-Trichloroethane 60U 60 7.0
79-00-5 1,1,2-Trichloroethane 60U 60 8.0
Continued on next page
*See Statement of Data Qualifications
Page 23 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-05 Sampled: 10/11/11 11:40Lab Sample ID: 1110319-06 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 60U 60 6.8
75-69-4 Trichlorofluoromethane 120U 120 8.9
96-18-4 1,2,3-Trichloropropane 120U 120 50
*526-73-8 1,2,3-Trimethylbenzene 300U 300 6.9
95-63-6 1,2,4-Trimethylbenzene 120U 120 6.8
108-67-8 1,3,5-Trimethylbenzene 120U 120 7.0
75-01-4 Vinyl Chloride 48U 48 8.0
179601-23-1 Xylene, Meta + Para 120U 120 12
95-47-6 Xylene, Ortho 60U 60 8.4
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 97 84-110
*See Statement of Data Qualifications
Page 24 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-05 Sampled: 10/11/11 11:40Lab Sample ID: 1110319-06 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 83 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 25 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-06 Sampled: 10/11/11 09:40Lab Sample ID: 1110319-07 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 150J 1100 100
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 57U 57 6.8
108-86-1 Bromobenzene 110U 110 6.3
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.6
74-83-9 Bromomethane 230U 230 13
104-51-8 n-Butylbenzene 57U 57 5.9
135-98-8 sec-Butylbenzene 57U 57 5.9
98-06-6 tert-Butylbenzene 57U 57 6.3
75-15-0 Carbon Disulfide 280U 280 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
*75-00-3 Chloroethane 280U 280 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 280U 280 7.6
110-82-7 Cyclohexane 280U 280 7.5
96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.5
74-95-3 Dibromomethane 280U 280 6.6
110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.2
106-46-7 1,4-Dichlorobenzene 110U 110 7.6
*75-71-8 Dichlorodifluoromethane 280U 280 8.6
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.0
75-35-4 1,1-Dichloroethene 57U 57 8.5
156-59-2 cis-1,2-Dichloroethene 57U 57 7.0
Continued on next page
*See Statement of Data Qualifications
Page 26 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-06 Sampled: 10/11/11 09:40Lab Sample ID: 1110319-07 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.1
78-87-5 1,2-Dichloropropane 57U 57 7.2
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.3
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.3
100-41-4 Ethylbenzene 57U 57 7.7
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2800U 2800 18
*74-88-4 Iodomethane 100J 110 9.1
98-82-8 Isopropylbenzene 280U 280 8.3
*108-20-3 Isopropyl Ether 280U 280 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.7
1634-04-4 Methyl tert-Butyl Ether 280U 280 7.5
75-09-2 Methylene Chloride 110U 110 6.6
78-93-3 2-Butanone (MEK) 850U 850 29
*91-57-6 2-Methylnaphthalene 370U 370 8.6
108-10-1 4-Methyl-2-pentanone (MIBK) 2800U 2800 6.7
*91-20-3 Naphthalene 370U 370 7.7
*994-05-8 tert-Amyl Methyl Ether 280U 280 2.7
*637-92-3 Ethyl tert-Butyl Ether 280U 280 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 5.9
*75-65-0 t-Butanol 2800U 2800 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 110U 110 8.2
*87-61-6 1,2,3-Trichlorobenzene 370U 370 6.8
120-82-1 1,2,4-Trichlorobenzene 370U 370 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.6
Continued on next page
*See Statement of Data Qualifications
Page 27 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-06 Sampled: 10/11/11 09:40Lab Sample ID: 1110319-07 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.4
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 280U 280 6.5
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 45U 45 7.6
179601-23-1 Xylene, Meta + Para 110U 110 12
95-47-6 Xylene, Ortho 57U 57 7.9
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 104 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 28 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-06 Sampled: 10/11/11 09:40Lab Sample ID: 1110319-07 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 88 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 29 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-07 Sampled: 10/10/11 17:40Lab Sample ID: 1110319-08 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 95
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 140J 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.9
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.9
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
74-83-9 Bromomethane 42J 230 13
104-51-8 n-Butylbenzene 57U 57 6.0
135-98-8 sec-Butylbenzene 57U 57 6.0
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
*75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 290U 290 7.7
110-82-7 Cyclohexane 290U 290 7.6
96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.6
110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.7
*75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.1
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 30 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-07 Sampled: 10/10/11 17:40Lab Sample ID: 1110319-08 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 95
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.4
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 110 110 9.2
98-82-8 Isopropylbenzene 290U 290 8.4
*108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.6
75-09-2 Methylene Chloride 110U 110 6.6
78-93-3 2-Butanone (MEK) 860U 860 29
*91-57-6 2-Methylnaphthalene 380U 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.8
*91-20-3 Naphthalene 160J 380 7.8
*994-05-8 tert-Amyl Methyl Ether 290U 290 2.7
*637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 6.0
*75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 72J 110 8.2
*87-61-6 1,2,3-Trichlorobenzene 380U 380 6.9
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.7
Continued on next page
*See Statement of Data Qualifications
Page 31 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-07 Sampled: 10/10/11 17:40Lab Sample ID: 1110319-08 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 95
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.5
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 290U 290 6.6
95-63-6 1,2,4-Trimethylbenzene 22J 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 46U 46 7.7
179601-23-1 Xylene, Meta + Para 58J 110 12
95-47-6 Xylene, Ortho 18J 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 97 84-110
*See Statement of Data Qualifications
Page 32 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-07 Sampled: 10/10/11 17:40Lab Sample ID: 1110319-08 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 95 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 33 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-08 Sampled: 10/10/11 16:02Lab Sample ID: 1110319-09 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 200J 1200 100
107-13-1 Acrylonitrile 120U 120 23
71-43-2 Benzene 19J 58 6.9
108-86-1 Bromobenzene 120U 120 6.5
74-97-5 Bromochloromethane 120U 120 6.9
75-27-4 Bromodichloromethane 120U 120 5.9
75-25-2 Bromoform 120U 120 8.8
74-83-9 Bromomethane 41J 230 13
104-51-8 n-Butylbenzene 7.2J 58 6.0
135-98-8 sec-Butylbenzene 58U 58 6.0
98-06-6 tert-Butylbenzene 58U 58 6.5
75-15-0 Carbon Disulfide 290U 290 5.9
56-23-5 Carbon Tetrachloride 58U 58 5.8
108-90-7 Chlorobenzene 58U 58 13
*75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 58U 58 6.6
74-87-3 Chloromethane 290U 290 7.7
110-82-7 Cyclohexane 58J 290 7.6
96-12-8 1,2-Dibromo-3-chloropropane 58U 58 14
124-48-1 Dibromochloromethane 120U 120 17
106-93-4 1,2-Dibromoethane 58U 58 8.7
74-95-3 Dibromomethane 290U 290 6.7
110-57-6 trans-1,4-Dichloro-2-butene 58U 58 5.1
95-50-1 1,2-Dichlorobenzene 120U 120 5.9
541-73-1 1,3-Dichlorobenzene 120U 120 6.4
106-46-7 1,4-Dichlorobenzene 120U 120 7.7
*75-71-8 Dichlorodifluoromethane 290U 290 8.8
75-34-3 1,1-Dichloroethane 58U 58 5.8
107-06-2 1,2-Dichloroethane 58U 58 6.1
75-35-4 1,1-Dichloroethene 58U 58 8.7
156-59-2 cis-1,2-Dichloroethene 58U 58 7.2
Continued on next page
*See Statement of Data Qualifications
Page 34 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-08 Sampled: 10/10/11 16:02Lab Sample ID: 1110319-09 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 58U 58 6.2
78-87-5 1,2-Dichloropropane 58U 58 7.4
10061-01-5 cis-1,3-Dichloropropene 58U 58 9.5
10061-02-6 trans-1,3-Dichloropropene 58U 58 6.5
100-41-4 Ethylbenzene 58U 58 7.9
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 93J 120 9.2
98-82-8 Isopropylbenzene 17J 290 8.4
*108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 120U 120 7.9
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.6
75-09-2 Methylene Chloride 120U 120 6.7
78-93-3 2-Butanone (MEK) 870U 870 29
*91-57-6 2-Methylnaphthalene 380U 380 8.8
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.8
*91-20-3 Naphthalene 200J 380 7.9
*994-05-8 tert-Amyl Methyl Ether 290U 290 2.8
*637-92-3 Ethyl tert-Butyl Ether 290U 290 4.0
103-65-1 n-Propylbenzene 16J 120 6.6
100-42-5 Styrene 58U 58 6.0
*75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 18
79-34-5 1,1,2,2-Tetrachloroethane 58U 58 13
127-18-4 Tetrachloroethene 58U 58 5.9
109-99-9 Tetrahydrofuran 1200U 1200 38
108-88-3 Toluene 100J 120 8.3
*87-61-6 1,2,3-Trichlorobenzene 380U 380 6.9
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.5
71-55-6 1,1,1-Trichloroethane 58U 58 6.7
79-00-5 1,1,2-Trichloroethane 58U 58 7.7
Continued on next page
*See Statement of Data Qualifications
Page 35 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-08 Sampled: 10/10/11 16:02Lab Sample ID: 1110319-09 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 58U 58 6.6
75-69-4 Trichlorofluoromethane 120U 120 8.5
96-18-4 1,2,3-Trichloropropane 120U 120 48
*526-73-8 1,2,3-Trimethylbenzene 29J 290 6.6
95-63-6 1,2,4-Trimethylbenzene 72J 120 6.6
108-67-8 1,3,5-Trimethylbenzene 13J 120 6.7
75-01-4 Vinyl Chloride 46U 46 7.7
179601-23-1 Xylene, Meta + Para 140 120 12
95-47-6 Xylene, Ortho 100 58 8.1
Surrogates: % Recovery Control Limits
Dibromofluoromethane 105 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 36 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-08 Sampled: 10/10/11 16:02Lab Sample ID: 1110319-09 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 87 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 37 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-09 Sampled: 10/10/11 17:27Lab Sample ID: 1110319-10 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 120J 1100 97
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 55U 55 6.6
108-86-1 Bromobenzene 110U 110 6.1
74-97-5 Bromochloromethane 110U 110 6.6
75-27-4 Bromodichloromethane 110U 110 5.6
75-25-2 Bromoform 110U 110 8.3
74-83-9 Bromomethane 220U 220 13
104-51-8 n-Butylbenzene 55U 55 5.7
135-98-8 sec-Butylbenzene 55U 55 5.7
98-06-6 tert-Butylbenzene 55U 55 6.1
75-15-0 Carbon Disulfide 270U 270 5.6
56-23-5 Carbon Tetrachloride 55U 55 5.5
108-90-7 Chlorobenzene 55U 55 12
*75-00-3 Chloroethane 270U 270 12
67-66-3 Chloroform 55U 55 6.2
74-87-3 Chloromethane 270U 270 7.3
110-82-7 Cyclohexane 270U 270 7.2
96-12-8 1,2-Dibromo-3-chloropropane 55U 55 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 55U 55 8.2
74-95-3 Dibromomethane 270U 270 6.3
110-57-6 trans-1,4-Dichloro-2-butene 55U 55 4.8
95-50-1 1,2-Dichlorobenzene 110U 110 5.6
541-73-1 1,3-Dichlorobenzene 110U 110 6.0
106-46-7 1,4-Dichlorobenzene 110U 110 7.3
*75-71-8 Dichlorodifluoromethane 270U 270 8.3
75-34-3 1,1-Dichloroethane 55U 55 5.5
107-06-2 1,2-Dichloroethane 55U 55 5.8
75-35-4 1,1-Dichloroethene 55U 55 8.2
156-59-2 cis-1,2-Dichloroethene 55U 55 6.8
Continued on next page
*See Statement of Data Qualifications
Page 38 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-09 Sampled: 10/10/11 17:27Lab Sample ID: 1110319-10 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 55U 55 5.9
78-87-5 1,2-Dichloropropane 55U 55 7.0
10061-01-5 cis-1,3-Dichloropropene 55U 55 9.0
10061-02-6 trans-1,3-Dichloropropene 55U 55 6.1
100-41-4 Ethylbenzene 55U 55 7.4
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
*74-88-4 Iodomethane 80J 110 8.7
98-82-8 Isopropylbenzene 270U 270 8.0
*108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.4
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.2
75-09-2 Methylene Chloride 20J 110 6.3
78-93-3 2-Butanone (MEK) 820U 820 28
*91-57-6 2-Methylnaphthalene 360U 360 8.3
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.4
*91-20-3 Naphthalene 140J 360 7.4
*994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
*637-92-3 Ethyl tert-Butyl Ether 270U 270 3.8
103-65-1 n-Propylbenzene 110U 110 6.2
100-42-5 Styrene 55U 55 5.7
*75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 55U 55 12
127-18-4 Tetrachloroethene 55U 55 5.6
109-99-9 Tetrahydrofuran 1100U 1100 36
108-88-3 Toluene 110U 110 7.9
*87-61-6 1,2,3-Trichlorobenzene 360U 360 6.6
120-82-1 1,2,4-Trichlorobenzene 360U 360 7.1
71-55-6 1,1,1-Trichloroethane 55U 55 6.3
79-00-5 1,1,2-Trichloroethane 55U 55 7.3
Continued on next page
*See Statement of Data Qualifications
Page 39 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-09 Sampled: 10/10/11 17:27Lab Sample ID: 1110319-10 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 55U 55 6.2
75-69-4 Trichlorofluoromethane 110U 110 8.1
96-18-4 1,2,3-Trichloropropane 110U 110 45
*526-73-8 1,2,3-Trimethylbenzene 270U 270 6.3
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.2
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.3
75-01-4 Vinyl Chloride 44U 44 7.3
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 55U 55 7.6
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 97 84-110
*See Statement of Data Qualifications
Page 40 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-09 Sampled: 10/10/11 17:27Lab Sample ID: 1110319-10 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 92 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 41 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-10 Sampled: 10/12/11 09:33Lab Sample ID: 1110319-11 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 120J 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.8
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
74-83-9 Bromomethane 230U 230 13
104-51-8 n-Butylbenzene 57U 57 5.9
135-98-8 sec-Butylbenzene 57U 57 5.9
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
*75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 290U 290 7.6
110-82-7 Cyclohexane 19J 290 7.5
96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.6
110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.6
*75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.0
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 42 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-10 Sampled: 10/12/11 09:33Lab Sample ID: 1110319-11 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.4
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 89J 110 9.1
98-82-8 Isopropylbenzene 290U 290 8.3
*108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.5
75-09-2 Methylene Chloride 110U 110 6.6
78-93-3 2-Butanone (MEK) 860U 860 29
*91-57-6 2-Methylnaphthalene 380U 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.7
*91-20-3 Naphthalene 160J 380 7.8
*994-05-8 tert-Amyl Methyl Ether 290U 290 2.7
*637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 5.9
*75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 19J 110 8.2
*87-61-6 1,2,3-Trichlorobenzene 380U 380 6.8
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.6
Continued on next page
*See Statement of Data Qualifications
Page 43 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-10 Sampled: 10/12/11 09:33Lab Sample ID: 1110319-11 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.4
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 12J 290 6.6
95-63-6 1,2,4-Trimethylbenzene 18J 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 46U 46 7.6
179601-23-1 Xylene, Meta + Para 110U 110 12
95-47-6 Xylene, Ortho 22J 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 44 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-10 Sampled: 10/12/11 09:33Lab Sample ID: 1110319-11 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 88 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 45 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-11 Sampled: 10/12/11 15:45Lab Sample ID: 1110319-12 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 140J 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.9
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.9
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
74-83-9 Bromomethane 45J 230 13
104-51-8 n-Butylbenzene 57U 57 6.0
135-98-8 sec-Butylbenzene 57U 57 6.0
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
*75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 290U 290 7.7
110-82-7 Cyclohexane 16J 290 7.6
96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.7
110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.7
*75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.1
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 46 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-11 Sampled: 10/12/11 15:45Lab Sample ID: 1110319-12 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.4
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 98J 110 9.2
98-82-8 Isopropylbenzene 290U 290 8.4
*108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.6
75-09-2 Methylene Chloride 110U 110 6.7
78-93-3 2-Butanone (MEK) 860U 860 29
*91-57-6 2-Methylnaphthalene 380U 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.8
*91-20-3 Naphthalene 170J 380 7.8
*994-05-8 tert-Amyl Methyl Ether 290U 290 2.8
*637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 6.0
*75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 15J 110 8.3
*87-61-6 1,2,3-Trichlorobenzene 380U 380 6.9
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.5
71-55-6 1,1,1-Trichloroethane 57U 57 6.7
79-00-5 1,1,2-Trichloroethane 57U 57 7.7
Continued on next page
*See Statement of Data Qualifications
Page 47 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-11 Sampled: 10/12/11 15:45Lab Sample ID: 1110319-12 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.5
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 9.4J 290 6.6
95-63-6 1,2,4-Trimethylbenzene 14J 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.7
75-01-4 Vinyl Chloride 46U 46 7.7
179601-23-1 Xylene, Meta + Para 110U 110 12
95-47-6 Xylene, Ortho 17J 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 48 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-11 Sampled: 10/12/11 15:45Lab Sample ID: 1110319-12 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 87 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 49 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-13 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 130J 1100 95
107-13-1 Acrylonitrile 110U 110 21
71-43-2 Benzene 53U 53 6.4
108-86-1 Bromobenzene 110U 110 6.0
74-97-5 Bromochloromethane 110U 110 6.4
75-27-4 Bromodichloromethane 110U 110 5.4
75-25-2 Bromoform 110U 110 8.1
74-83-9 Bromomethane 210U 210 12
104-51-8 n-Butylbenzene 53U 53 5.5
135-98-8 sec-Butylbenzene 53U 53 5.5
98-06-6 tert-Butylbenzene 53U 53 6.0
75-15-0 Carbon Disulfide 270U 270 5.4
56-23-5 Carbon Tetrachloride 53U 53 5.3
108-90-7 Chlorobenzene 53U 53 12
*75-00-3 Chloroethane 270U 270 11
67-66-3 Chloroform 53U 53 6.1
74-87-3 Chloromethane 270U 270 7.1
110-82-7 Cyclohexane 28J 270 7.0
96-12-8 1,2-Dibromo-3-chloropropane 53U 53 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 53U 53 8.0
74-95-3 Dibromomethane 270U 270 6.2
110-57-6 trans-1,4-Dichloro-2-butene 53U 53 4.7
95-50-1 1,2-Dichlorobenzene 110U 110 5.4
541-73-1 1,3-Dichlorobenzene 110U 110 5.9
106-46-7 1,4-Dichlorobenzene 110U 110 7.1
*75-71-8 Dichlorodifluoromethane 270U 270 8.1
75-34-3 1,1-Dichloroethane 53U 53 5.3
107-06-2 1,2-Dichloroethane 53U 53 5.6
75-35-4 1,1-Dichloroethene 53U 53 8.0
156-59-2 cis-1,2-Dichloroethene 53U 53 6.6
Continued on next page
*See Statement of Data Qualifications
Page 50 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-13 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 53U 53 5.7
78-87-5 1,2-Dichloropropane 53U 53 6.8
10061-01-5 cis-1,3-Dichloropropene 53U 53 8.7
10061-02-6 trans-1,3-Dichloropropene 53U 53 6.0
100-41-4 Ethylbenzene 53U 53 7.2
60-29-7 Ethyl Ether 210U 210 10
591-78-6 2-Hexanone 2700U 2700 17
*74-88-4 Iodomethane 65J 110 8.5
98-82-8 Isopropylbenzene 270U 270 7.8
*108-20-3 Isopropyl Ether 270U 270 2.0
99-87-6 4-Isopropyltoluene 110U 110 7.2
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.0
75-09-2 Methylene Chloride 110U 110 6.2
78-93-3 2-Butanone (MEK) 84J 800 27
*91-57-6 2-Methylnaphthalene 290J 350 8.1
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.3
*91-20-3 Naphthalene 180J 350 7.2
*994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
*637-92-3 Ethyl tert-Butyl Ether 270U 270 3.7
103-65-1 n-Propylbenzene 110U 110 6.1
100-42-5 Styrene 53U 53 5.5
*75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 16
79-34-5 1,1,2,2-Tetrachloroethane 53U 53 12
127-18-4 Tetrachloroethene 53U 53 5.4
109-99-9 Tetrahydrofuran 1100U 1100 35
108-88-3 Toluene 25J 110 7.7
*87-61-6 1,2,3-Trichlorobenzene 350U 350 6.4
120-82-1 1,2,4-Trichlorobenzene 350U 350 6.9
71-55-6 1,1,1-Trichloroethane 53U 53 6.2
79-00-5 1,1,2-Trichloroethane 53U 53 7.1
Continued on next page
*See Statement of Data Qualifications
Page 51 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-13 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 53U 53 6.1
75-69-4 Trichlorofluoromethane 110U 110 7.9
96-18-4 1,2,3-Trichloropropane 110U 110 44
*526-73-8 1,2,3-Trimethylbenzene 17J 270 6.1
95-63-6 1,2,4-Trimethylbenzene 22J 110 6.1
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.2
75-01-4 Vinyl Chloride 43U 43 7.1
179601-23-1 Xylene, Meta + Para 34J 110 11
95-47-6 Xylene, Ortho 26J 53 7.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 52 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-13 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 94 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 53 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-13 Sampled: 10/12/11 12:15Lab Sample ID: 1110319-14 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 93
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 290J 1100 96
107-13-1 Acrylonitrile 110U 110 21
71-43-2 Benzene 37J 54 6.5
108-86-1 Bromobenzene 110U 110 6.0
74-97-5 Bromochloromethane 110U 110 6.5
75-27-4 Bromodichloromethane 110U 110 5.5
75-25-2 Bromoform 110U 110 8.2
74-83-9 Bromomethane 220U 220 12
104-51-8 n-Butylbenzene 42J 54 5.6
135-98-8 sec-Butylbenzene 19J 54 5.6
98-06-6 tert-Butylbenzene 54U 54 6.0
75-15-0 Carbon Disulfide 270U 270 5.5
56-23-5 Carbon Tetrachloride 54U 54 5.4
108-90-7 Chlorobenzene 54U 54 12
*75-00-3 Chloroethane 270U 270 11
67-66-3 Chloroform 54U 54 6.1
74-87-3 Chloromethane 270U 270 7.2
110-82-7 Cyclohexane 380 270 7.1
96-12-8 1,2-Dibromo-3-chloropropane 54U 54 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 54U 54 8.1
74-95-3 Dibromomethane 270U 270 6.2
110-57-6 trans-1,4-Dichloro-2-butene 54U 54 4.7
95-50-1 1,2-Dichlorobenzene 110U 110 5.5
541-73-1 1,3-Dichlorobenzene 110U 110 5.9
106-46-7 1,4-Dichlorobenzene 110U 110 7.2
*75-71-8 Dichlorodifluoromethane 270U 270 8.2
75-34-3 1,1-Dichloroethane 54U 54 5.4
107-06-2 1,2-Dichloroethane 54U 54 5.7
75-35-4 1,1-Dichloroethene 54U 54 8.1
156-59-2 cis-1,2-Dichloroethene 54U 54 6.7
Continued on next page
*See Statement of Data Qualifications
Page 54 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-13 Sampled: 10/12/11 12:15Lab Sample ID: 1110319-14 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 93
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 54U 54 5.8
78-87-5 1,2-Dichloropropane 54U 54 6.9
10061-01-5 cis-1,3-Dichloropropene 54U 54 8.8
10061-02-6 trans-1,3-Dichloropropene 54U 54 6.0
100-41-4 Ethylbenzene 150 54 7.3
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
*74-88-4 Iodomethane 68J 110 8.6
98-82-8 Isopropylbenzene 65J 270 7.9
*108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 35J 110 7.3
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.1
75-09-2 Methylene Chloride 110U 110 6.2
78-93-3 2-Butanone (MEK) 100J 810 27
*91-57-6 2-Methylnaphthalene 730 360 8.2
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.4
*91-20-3 Naphthalene 780 360 7.3
*994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
*637-92-3 Ethyl tert-Butyl Ether 270U 270 3.7
103-65-1 n-Propylbenzene 75J 110 6.1
100-42-5 Styrene 54U 54 5.6
*75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 16
79-34-5 1,1,2,2-Tetrachloroethane 54U 54 12
127-18-4 Tetrachloroethene 54U 54 5.5
109-99-9 Tetrahydrofuran 1100U 1100 36
108-88-3 Toluene 580 110 7.8
*87-61-6 1,2,3-Trichlorobenzene 360U 360 6.5
120-82-1 1,2,4-Trichlorobenzene 360U 360 7.0
71-55-6 1,1,1-Trichloroethane 54U 54 6.2
79-00-5 1,1,2-Trichloroethane 54U 54 7.2
Continued on next page
*See Statement of Data Qualifications
Page 55 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-13 Sampled: 10/12/11 12:15Lab Sample ID: 1110319-14 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 93
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 54U 54 6.1
75-69-4 Trichlorofluoromethane 110U 110 8.0
96-18-4 1,2,3-Trichloropropane 110U 110 44
*526-73-8 1,2,3-Trimethylbenzene 180J 270 6.2
95-63-6 1,2,4-Trimethylbenzene 460 110 6.1
108-67-8 1,3,5-Trimethylbenzene 77J 110 6.2
75-01-4 Vinyl Chloride 43U 43 7.2
179601-23-1 Xylene, Meta + Para 900 110 11
95-47-6 Xylene, Ortho 640 54 7.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 100 84-110
*See Statement of Data Qualifications
Page 56 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-13 Sampled: 10/12/11 12:15Lab Sample ID: 1110319-14 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 93 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 57 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-14 Sampled: 10/12/11 13:00Lab Sample ID: 1110319-15 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 830J 1200 110
107-13-1 Acrylonitrile 120U 120 24
71-43-2 Benzene 250 61 7.3
108-86-1 Bromobenzene 120U 120 6.8
74-97-5 Bromochloromethane 120U 120 7.3
75-27-4 Bromodichloromethane 120U 120 6.2
75-25-2 Bromoform 120U 120 9.3
74-83-9 Bromomethane 240U 240 14
104-51-8 n-Butylbenzene 91 61 6.3
135-98-8 sec-Butylbenzene 59J 61 6.3
98-06-6 tert-Butylbenzene 61U 61 6.8
75-15-0 Carbon Disulfide 300U 300 6.2
56-23-5 Carbon Tetrachloride 61U 61 6.1
108-90-7 Chlorobenzene 61U 61 14
*75-00-3 Chloroethane 300U 300 13
67-66-3 Chloroform 61U 61 7.0
74-87-3 Chloromethane 300U 300 8.2
110-82-7 Cyclohexane 610 300 8.1
96-12-8 1,2-Dibromo-3-chloropropane 61U 61 15
124-48-1 Dibromochloromethane 120U 120 18
106-93-4 1,2-Dibromoethane 61U 61 9.1
74-95-3 Dibromomethane 300U 300 7.1
110-57-6 trans-1,4-Dichloro-2-butene 61U 61 5.4
95-50-1 1,2-Dichlorobenzene 120U 120 6.2
541-73-1 1,3-Dichlorobenzene 120U 120 6.7
106-46-7 1,4-Dichlorobenzene 120U 120 8.2
*75-71-8 Dichlorodifluoromethane 300U 300 9.3
75-34-3 1,1-Dichloroethane 61U 61 6.1
107-06-2 1,2-Dichloroethane 61U 61 6.5
75-35-4 1,1-Dichloroethene 61U 61 9.1
156-59-2 cis-1,2-Dichloroethene 61U 61 7.6
Continued on next page
*See Statement of Data Qualifications
Page 58 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-14 Sampled: 10/12/11 13:00Lab Sample ID: 1110319-15 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 61U 61 6.6
78-87-5 1,2-Dichloropropane 61U 61 7.8
10061-01-5 cis-1,3-Dichloropropene 61U 61 10
10061-02-6 trans-1,3-Dichloropropene 61U 61 6.8
100-41-4 Ethylbenzene 480 61 8.3
60-29-7 Ethyl Ether 240U 240 11
591-78-6 2-Hexanone 3000U 3000 20
*74-88-4 Iodomethane 72J 120 9.8
98-82-8 Isopropylbenzene 240J 300 8.9
*108-20-3 Isopropyl Ether 300U 300 2.3
99-87-6 4-Isopropyltoluene 76J 120 8.3
1634-04-4 Methyl tert-Butyl Ether 300U 300 8.1
75-09-2 Methylene Chloride 120U 120 7.1
78-93-3 2-Butanone (MEK) 420J 910 31
*91-57-6 2-Methylnaphthalene 910 400 9.3
108-10-1 4-Methyl-2-pentanone (MIBK) 3000U 3000 7.2
*91-20-3 Naphthalene 1100 400 8.3
*994-05-8 tert-Amyl Methyl Ether 300U 300 2.9
*637-92-3 Ethyl tert-Butyl Ether 300U 300 4.2
103-65-1 n-Propylbenzene 230 120 7.0
100-42-5 Styrene 61U 61 6.3
*75-65-0 t-Butanol 3000U 3000 160
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 19
79-34-5 1,1,2,2-Tetrachloroethane 61U 61 14
127-18-4 Tetrachloroethene 61U 61 6.2
109-99-9 Tetrahydrofuran 1200U 1200 41
108-88-3 Toluene 1700 120 8.8
*87-61-6 1,2,3-Trichlorobenzene 400U 400 7.3
120-82-1 1,2,4-Trichlorobenzene 400U 400 7.9
71-55-6 1,1,1-Trichloroethane 61U 61 7.1
79-00-5 1,1,2-Trichloroethane 61U 61 8.2
Continued on next page
*See Statement of Data Qualifications
Page 59 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-14 Sampled: 10/12/11 13:00Lab Sample ID: 1110319-15 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 61U 61 7.0
75-69-4 Trichlorofluoromethane 120U 120 9.0
96-18-4 1,2,3-Trichloropropane 120U 120 50
*526-73-8 1,2,3-Trimethylbenzene 320 300 7.0
95-63-6 1,2,4-Trimethylbenzene 840 120 7.0
108-67-8 1,3,5-Trimethylbenzene 140 120 7.1
75-01-4 Vinyl Chloride 49U 49 8.2
179601-23-1 Xylene, Meta + Para 1800 120 12
95-47-6 Xylene, Ortho 1400 61 8.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 100 84-110
*See Statement of Data Qualifications
Page 60 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-14 Sampled: 10/12/11 13:00Lab Sample ID: 1110319-15 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 82 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 61 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-15 Sampled: 10/11/11 18:52Lab Sample ID: 1110319-16 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 260J 1000 90
107-13-1 Acrylonitrile 100U 100 20
71-43-2 Benzene 45J 51 6.1
108-86-1 Bromobenzene 100U 100 5.7
74-97-5 Bromochloromethane 100U 100 6.1
75-27-4 Bromodichloromethane 100U 100 5.2
75-25-2 Bromoform 100U 100 7.7
74-83-9 Bromomethane 200U 200 12
104-51-8 n-Butylbenzene 29J 51 5.3
135-98-8 sec-Butylbenzene 16J 51 5.3
98-06-6 tert-Butylbenzene 51U 51 5.7
75-15-0 Carbon Disulfide 250U 250 5.2
56-23-5 Carbon Tetrachloride 51U 51 5.1
108-90-7 Chlorobenzene 51U 51 12
*75-00-3 Chloroethane 250U 250 11
67-66-3 Chloroform 51U 51 5.8
74-87-3 Chloromethane 250U 250 6.8
110-82-7 Cyclohexane 220J 250 6.7
96-12-8 1,2-Dibromo-3-chloropropane 51U 51 12
124-48-1 Dibromochloromethane 100U 100 15
106-93-4 1,2-Dibromoethane 51U 51 7.6
74-95-3 Dibromomethane 250U 250 5.9
110-57-6 trans-1,4-Dichloro-2-butene 51U 51 4.5
95-50-1 1,2-Dichlorobenzene 100U 100 5.2
541-73-1 1,3-Dichlorobenzene 100U 100 5.6
106-46-7 1,4-Dichlorobenzene 100U 100 6.8
*75-71-8 Dichlorodifluoromethane 250U 250 7.7
75-34-3 1,1-Dichloroethane 51U 51 5.1
107-06-2 1,2-Dichloroethane 51U 51 5.4
75-35-4 1,1-Dichloroethene 51U 51 7.6
156-59-2 cis-1,2-Dichloroethene 51U 51 6.3
Continued on next page
*See Statement of Data Qualifications
Page 62 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-15 Sampled: 10/11/11 18:52Lab Sample ID: 1110319-16 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 51U 51 5.5
78-87-5 1,2-Dichloropropane 51U 51 6.5
10061-01-5 cis-1,3-Dichloropropene 51U 51 8.3
10061-02-6 trans-1,3-Dichloropropene 51U 51 5.7
100-41-4 Ethylbenzene 60 51 6.9
60-29-7 Ethyl Ether 200U 200 9.5
591-78-6 2-Hexanone 2500U 2500 17
*74-88-4 Iodomethane 46J 100 8.1
98-82-8 Isopropylbenzene 42J 250 7.4
*108-20-3 Isopropyl Ether 250U 250 1.9
99-87-6 4-Isopropyltoluene 17J 100 6.9
1634-04-4 Methyl tert-Butyl Ether 250U 250 6.7
75-09-2 Methylene Chloride 100U 100 5.9
78-93-3 2-Butanone (MEK) 71J 760 26
*91-57-6 2-Methylnaphthalene 620 330 7.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2500U 2500 6.0
*91-20-3 Naphthalene 530 330 6.9
*994-05-8 tert-Amyl Methyl Ether 250U 250 2.4
*637-92-3 Ethyl tert-Butyl Ether 250U 250 3.5
103-65-1 n-Propylbenzene 43J 100 5.8
100-42-5 Styrene 51U 51 5.3
*75-65-0 t-Butanol 2500U 2500 130
630-20-6 1,1,1,2-Tetrachloroethane 100U 100 15
79-34-5 1,1,2,2-Tetrachloroethane 51U 51 11
127-18-4 Tetrachloroethene 51U 51 5.2
109-99-9 Tetrahydrofuran 1000U 1000 34
108-88-3 Toluene 300 100 7.3
*87-61-6 1,2,3-Trichlorobenzene 330U 330 6.1
120-82-1 1,2,4-Trichlorobenzene 330U 330 6.6
71-55-6 1,1,1-Trichloroethane 51U 51 5.9
79-00-5 1,1,2-Trichloroethane 51U 51 6.8
Continued on next page
*See Statement of Data Qualifications
Page 63 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-15 Sampled: 10/11/11 18:52Lab Sample ID: 1110319-16 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 51U 51 5.8
75-69-4 Trichlorofluoromethane 100U 100 7.5
96-18-4 1,2,3-Trichloropropane 100U 100 42
*526-73-8 1,2,3-Trimethylbenzene 130J 250 5.8
95-63-6 1,2,4-Trimethylbenzene 230 100 5.8
108-67-8 1,3,5-Trimethylbenzene 57J 100 5.9
75-01-4 Vinyl Chloride 40U 40 6.8
179601-23-1 Xylene, Meta + Para 430 100 10
95-47-6 Xylene, Ortho 320 51 7.1
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 64 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-15 Sampled: 10/11/11 18:52Lab Sample ID: 1110319-16 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 91 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 65 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-16 Sampled: 10/11/11 17:08Lab Sample ID: 1110319-17 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 86
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 310J 1100 96
107-13-1 Acrylonitrile 110U 110 21
71-43-2 Benzene 86 54 6.5
108-86-1 Bromobenzene 110U 110 6.0
74-97-5 Bromochloromethane 110U 110 6.5
75-27-4 Bromodichloromethane 110U 110 5.5
75-25-2 Bromoform 110U 110 8.2
74-83-9 Bromomethane 41J 220 12
104-51-8 n-Butylbenzene 39J 54 5.6
135-98-8 sec-Butylbenzene 20J 54 5.6
98-06-6 tert-Butylbenzene 54U 54 6.0
75-15-0 Carbon Disulfide 270U 270 5.5
56-23-5 Carbon Tetrachloride 54U 54 5.4
108-90-7 Chlorobenzene 27J 54 12
*75-00-3 Chloroethane 270U 270 11
67-66-3 Chloroform 54U 54 6.1
74-87-3 Chloromethane 270U 270 7.2
110-82-7 Cyclohexane 350 270 7.1
96-12-8 1,2-Dibromo-3-chloropropane 54U 54 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 54U 54 8.1
74-95-3 Dibromomethane 270U 270 6.2
110-57-6 trans-1,4-Dichloro-2-butene 54U 54 4.7
95-50-1 1,2-Dichlorobenzene 39J 110 5.5
541-73-1 1,3-Dichlorobenzene 37J 110 5.9
106-46-7 1,4-Dichlorobenzene 16J 110 7.2
*75-71-8 Dichlorodifluoromethane 270U 270 8.2
75-34-3 1,1-Dichloroethane 54U 54 5.4
107-06-2 1,2-Dichloroethane 54U 54 5.7
75-35-4 1,1-Dichloroethene 54U 54 8.1
156-59-2 cis-1,2-Dichloroethene 54U 54 6.7
Continued on next page
*See Statement of Data Qualifications
Page 66 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-16 Sampled: 10/11/11 17:08Lab Sample ID: 1110319-17 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 86
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 54U 54 5.8
78-87-5 1,2-Dichloropropane 54U 54 6.9
10061-01-5 cis-1,3-Dichloropropene 54U 54 8.8
10061-02-6 trans-1,3-Dichloropropene 54U 54 6.0
100-41-4 Ethylbenzene 100 54 7.3
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
*74-88-4 Iodomethane 63J 110 8.6
98-82-8 Isopropylbenzene 58J 270 7.9
*108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 29J 110 7.3
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.1
75-09-2 Methylene Chloride 110U 110 6.2
78-93-3 2-Butanone (MEK) 140J 810 27
*91-57-6 2-Methylnaphthalene 570 360 8.2
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.4
*91-20-3 Naphthalene 560 360 7.3
*994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
*637-92-3 Ethyl tert-Butyl Ether 270U 270 3.7
103-65-1 n-Propylbenzene 64J 110 6.1
100-42-5 Styrene 54U 54 5.6
*75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 16
79-34-5 1,1,2,2-Tetrachloroethane 54U 54 12
127-18-4 Tetrachloroethene 54U 54 5.5
109-99-9 Tetrahydrofuran 1100U 1100 36
108-88-3 Toluene 500 110 7.8
*87-61-6 1,2,3-Trichlorobenzene 110J 360 6.5
120-82-1 1,2,4-Trichlorobenzene 92J 360 7.0
71-55-6 1,1,1-Trichloroethane 54U 54 6.2
79-00-5 1,1,2-Trichloroethane 54U 54 7.2
Continued on next page
*See Statement of Data Qualifications
Page 67 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-16 Sampled: 10/11/11 17:08Lab Sample ID: 1110319-17 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 86
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 54U 54 6.1
75-69-4 Trichlorofluoromethane 110U 110 8.0
96-18-4 1,2,3-Trichloropropane 110U 110 44
*526-73-8 1,2,3-Trimethylbenzene 160J 270 6.2
95-63-6 1,2,4-Trimethylbenzene 290 110 6.1
108-67-8 1,3,5-Trimethylbenzene 77J 110 6.2
75-01-4 Vinyl Chloride 43U 43 7.2
179601-23-1 Xylene, Meta + Para 580 110 11
95-47-6 Xylene, Ortho 420 54 7.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 100 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 100 84-110
*See Statement of Data Qualifications
Page 68 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-16 Sampled: 10/11/11 17:08Lab Sample ID: 1110319-17 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 86 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 69 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-17 Sampled: 10/11/11 16:52Lab Sample ID: 1110319-18 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 140J 1000 91
107-13-1 Acrylonitrile 100U 100 20
71-43-2 Benzene 51U 51 6.1
108-86-1 Bromobenzene 100U 100 5.7
74-97-5 Bromochloromethane 100U 100 6.1
75-27-4 Bromodichloromethane 100U 100 5.2
75-25-2 Bromoform 100U 100 7.7
74-83-9 Bromomethane 200U 200 12
104-51-8 n-Butylbenzene 6.6J 51 5.3
135-98-8 sec-Butylbenzene 51U 51 5.3
98-06-6 tert-Butylbenzene 51U 51 5.7
75-15-0 Carbon Disulfide 250U 250 5.2
56-23-5 Carbon Tetrachloride 51U 51 5.1
108-90-7 Chlorobenzene 51U 51 12
*75-00-3 Chloroethane 250U 250 11
67-66-3 Chloroform 51U 51 5.8
74-87-3 Chloromethane 250U 250 6.8
110-82-7 Cyclohexane 47J 250 6.7
96-12-8 1,2-Dibromo-3-chloropropane 51U 51 12
124-48-1 Dibromochloromethane 100U 100 15
106-93-4 1,2-Dibromoethane 51U 51 7.6
74-95-3 Dibromomethane 250U 250 5.9
110-57-6 trans-1,4-Dichloro-2-butene 51U 51 4.5
95-50-1 1,2-Dichlorobenzene 100U 100 5.2
541-73-1 1,3-Dichlorobenzene 100U 100 5.6
106-46-7 1,4-Dichlorobenzene 100U 100 6.8
*75-71-8 Dichlorodifluoromethane 250U 250 7.7
75-34-3 1,1-Dichloroethane 51U 51 5.1
107-06-2 1,2-Dichloroethane 51U 51 5.4
75-35-4 1,1-Dichloroethene 51U 51 7.6
156-59-2 cis-1,2-Dichloroethene 51U 51 6.3
Continued on next page
*See Statement of Data Qualifications
Page 70 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-17 Sampled: 10/11/11 16:52Lab Sample ID: 1110319-18 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 51U 51 5.5
78-87-5 1,2-Dichloropropane 51U 51 6.5
10061-01-5 cis-1,3-Dichloropropene 51U 51 8.4
10061-02-6 trans-1,3-Dichloropropene 51U 51 5.7
100-41-4 Ethylbenzene 51U 51 6.9
60-29-7 Ethyl Ether 200U 200 9.6
591-78-6 2-Hexanone 2500U 2500 17
*74-88-4 Iodomethane 68J 100 8.2
98-82-8 Isopropylbenzene 250U 250 7.4
*108-20-3 Isopropyl Ether 250U 250 1.9
99-87-6 4-Isopropyltoluene 100U 100 6.9
1634-04-4 Methyl tert-Butyl Ether 250U 250 6.7
75-09-2 Methylene Chloride 19J 100 5.9
78-93-3 2-Butanone (MEK) 760U 760 26
*91-57-6 2-Methylnaphthalene 340 340 7.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2500U 2500 6.0
*91-20-3 Naphthalene 220J 340 6.9
*994-05-8 tert-Amyl Methyl Ether 250U 250 2.4
*637-92-3 Ethyl tert-Butyl Ether 250U 250 3.5
103-65-1 n-Propylbenzene 7.6J 100 5.8
100-42-5 Styrene 51U 51 5.3
*75-65-0 t-Butanol 2500U 2500 130
630-20-6 1,1,1,2-Tetrachloroethane 100U 100 15
79-34-5 1,1,2,2-Tetrachloroethane 51U 51 12
127-18-4 Tetrachloroethene 51U 51 5.2
109-99-9 Tetrahydrofuran 1000U 1000 34
108-88-3 Toluene 38J 100 7.3
*87-61-6 1,2,3-Trichlorobenzene 340U 340 6.1
120-82-1 1,2,4-Trichlorobenzene 340U 340 6.6
71-55-6 1,1,1-Trichloroethane 51U 51 5.9
79-00-5 1,1,2-Trichloroethane 51U 51 6.8
Continued on next page
*See Statement of Data Qualifications
Page 71 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-17 Sampled: 10/11/11 16:52Lab Sample ID: 1110319-18 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 51U 51 5.8
75-69-4 Trichlorofluoromethane 100U 100 7.5
96-18-4 1,2,3-Trichloropropane 100U 100 42
*526-73-8 1,2,3-Trimethylbenzene 33J 250 5.9
95-63-6 1,2,4-Trimethylbenzene 51J 100 5.8
108-67-8 1,3,5-Trimethylbenzene 14J 100 5.9
75-01-4 Vinyl Chloride 41U 41 6.8
179601-23-1 Xylene, Meta + Para 65J 100 10
95-47-6 Xylene, Ortho 59 51 7.1
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 72 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-17 Sampled: 10/11/11 16:52Lab Sample ID: 1110319-18 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 91 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 73 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-18 Sampled: 10/11/11 15:20Lab Sample ID: 1110319-19 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 190J 1100 95
107-13-1 Acrylonitrile 110U 110 21
71-43-2 Benzene 14J 53 6.4
108-86-1 Bromobenzene 110U 110 5.9
74-97-5 Bromochloromethane 110U 110 6.4
75-27-4 Bromodichloromethane 110U 110 5.4
75-25-2 Bromoform 110U 110 8.1
74-83-9 Bromomethane 210U 210 12
104-51-8 n-Butylbenzene 22J 53 5.5
135-98-8 sec-Butylbenzene 9.2J 53 5.5
98-06-6 tert-Butylbenzene 53U 53 5.9
75-15-0 Carbon Disulfide 270U 270 5.4
56-23-5 Carbon Tetrachloride 53U 53 5.3
108-90-7 Chlorobenzene 53U 53 12
*75-00-3 Chloroethane 270U 270 11
67-66-3 Chloroform 53U 53 6.0
74-87-3 Chloromethane 270U 270 7.1
110-82-7 Cyclohexane 120J 270 7.0
96-12-8 1,2-Dibromo-3-chloropropane 53U 53 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 53U 53 8.0
74-95-3 Dibromomethane 270U 270 6.2
110-57-6 trans-1,4-Dichloro-2-butene 53U 53 4.7
95-50-1 1,2-Dichlorobenzene 110U 110 5.4
541-73-1 1,3-Dichlorobenzene 110U 110 5.8
106-46-7 1,4-Dichlorobenzene 110U 110 7.1
*75-71-8 Dichlorodifluoromethane 270U 270 8.1
75-34-3 1,1-Dichloroethane 53U 53 5.3
107-06-2 1,2-Dichloroethane 53U 53 5.6
75-35-4 1,1-Dichloroethene 53U 53 8.0
156-59-2 cis-1,2-Dichloroethene 53U 53 6.6
Continued on next page
*See Statement of Data Qualifications
Page 74 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-18 Sampled: 10/11/11 15:20Lab Sample ID: 1110319-19 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 53U 53 5.7
78-87-5 1,2-Dichloropropane 53U 53 6.8
10061-01-5 cis-1,3-Dichloropropene 53U 53 8.7
10061-02-6 trans-1,3-Dichloropropene 53U 53 5.9
100-41-4 Ethylbenzene 37J 53 7.2
60-29-7 Ethyl Ether 210U 210 10
591-78-6 2-Hexanone 2700U 2700 17
*74-88-4 Iodomethane 52J 110 8.5
98-82-8 Isopropylbenzene 44J 270 7.7
*108-20-3 Isopropyl Ether 270U 270 2.0
99-87-6 4-Isopropyltoluene 11J 110 7.2
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.0
75-09-2 Methylene Chloride 110U 110 6.2
78-93-3 2-Butanone (MEK) 800U 800 27
*91-57-6 2-Methylnaphthalene 520 350 8.1
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.3
*91-20-3 Naphthalene 440 350 7.2
*994-05-8 tert-Amyl Methyl Ether 270U 270 2.5
*637-92-3 Ethyl tert-Butyl Ether 270U 270 3.7
103-65-1 n-Propylbenzene 42J 110 6.0
100-42-5 Styrene 120 53 5.5
*75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 16
79-34-5 1,1,2,2-Tetrachloroethane 53U 53 12
127-18-4 Tetrachloroethene 53U 53 5.4
109-99-9 Tetrahydrofuran 1100U 1100 35
108-88-3 Toluene 120 110 7.6
*87-61-6 1,2,3-Trichlorobenzene 350U 350 6.4
120-82-1 1,2,4-Trichlorobenzene 350U 350 6.9
71-55-6 1,1,1-Trichloroethane 53U 53 6.2
79-00-5 1,1,2-Trichloroethane 53U 53 7.1
Continued on next page
*See Statement of Data Qualifications
Page 75 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-18 Sampled: 10/11/11 15:20Lab Sample ID: 1110319-19 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 53U 53 6.0
75-69-4 Trichlorofluoromethane 110U 110 7.9
96-18-4 1,2,3-Trichloropropane 110U 110 44
*526-73-8 1,2,3-Trimethylbenzene 92J 270 6.1
95-63-6 1,2,4-Trimethylbenzene 170 110 6.0
108-67-8 1,3,5-Trimethylbenzene 77J 110 6.2
75-01-4 Vinyl Chloride 42U 42 7.1
179601-23-1 Xylene, Meta + Para 210 110 11
95-47-6 Xylene, Ortho 180 53 7.4
Surrogates: % Recovery Control Limits
Dibromofluoromethane 101 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 100 84-110
*See Statement of Data Qualifications
Page 76 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-18 Sampled: 10/11/11 15:20Lab Sample ID: 1110319-19 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 94 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 77 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-19 Sampled: 10/11/11 14:10Lab Sample ID: 1110319-20 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 56
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 180J 1600 150
107-13-1 Acrylonitrile 160U 160 32
71-43-2 Benzene 81U 81 9.8
108-86-1 Bromobenzene 160U 160 9.1
74-97-5 Bromochloromethane 160U 160 9.8
75-27-4 Bromodichloromethane 160U 160 8.3
75-25-2 Bromoform 160U 160 12
74-83-9 Bromomethane 330U 330 19
104-51-8 n-Butylbenzene 81U 81 8.5
135-98-8 sec-Butylbenzene 81U 81 8.5
98-06-6 tert-Butylbenzene 81U 81 9.1
75-15-0 Carbon Disulfide 410U 410 8.3
56-23-5 Carbon Tetrachloride 81U 81 8.1
108-90-7 Chlorobenzene 81U 81 19
*75-00-3 Chloroethane 410U 410 17
67-66-3 Chloroform 81U 81 9.3
74-87-3 Chloromethane 410U 410 11
110-82-7 Cyclohexane 410U 410 11
96-12-8 1,2-Dibromo-3-chloropropane 81U 81 20
124-48-1 Dibromochloromethane 160U 160 24
106-93-4 1,2-Dibromoethane 81U 81 12
74-95-3 Dibromomethane 410U 410 9.4
110-57-6 trans-1,4-Dichloro-2-butene 81U 81 7.2
95-50-1 1,2-Dichlorobenzene 160U 160 8.3
541-73-1 1,3-Dichlorobenzene 160U 160 8.9
106-46-7 1,4-Dichlorobenzene 160U 160 11
*75-71-8 Dichlorodifluoromethane 410U 410 12
75-34-3 1,1-Dichloroethane 81U 81 8.1
107-06-2 1,2-Dichloroethane 81U 81 8.6
75-35-4 1,1-Dichloroethene 81U 81 12
156-59-2 cis-1,2-Dichloroethene 81U 81 10
Continued on next page
*See Statement of Data Qualifications
Page 78 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-19 Sampled: 10/11/11 14:10Lab Sample ID: 1110319-20 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 56
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 81U 81 8.8
78-87-5 1,2-Dichloropropane 81U 81 10
10061-01-5 cis-1,3-Dichloropropene 81U 81 13
10061-02-6 trans-1,3-Dichloropropene 81U 81 9.1
100-41-4 Ethylbenzene 81U 81 11
60-29-7 Ethyl Ether 330U 330 15
591-78-6 2-Hexanone 4100U 4100 27
*74-88-4 Iodomethane 63J 160 13
98-82-8 Isopropylbenzene 410U 410 12
*108-20-3 Isopropyl Ether 410U 410 3.1
99-87-6 4-Isopropyltoluene 160U 160 11
1634-04-4 Methyl tert-Butyl Ether 410U 410 11
75-09-2 Methylene Chloride 160U 160 9.4
78-93-3 2-Butanone (MEK) 1200U 1200 41
*91-57-6 2-Methylnaphthalene 540U 540 12
108-10-1 4-Methyl-2-pentanone (MIBK) 4100U 4100 9.6
*91-20-3 Naphthalene 220J 540 11
*994-05-8 tert-Amyl Methyl Ether 410U 410 3.9
*637-92-3 Ethyl tert-Butyl Ether 410U 410 5.6
103-65-1 n-Propylbenzene 160U 160 9.3
100-42-5 Styrene 81U 81 8.5
*75-65-0 t-Butanol 4100U 4100 210
630-20-6 1,1,1,2-Tetrachloroethane 160U 160 25
79-34-5 1,1,2,2-Tetrachloroethane 81U 81 18
127-18-4 Tetrachloroethene 370 81 8.3
109-99-9 Tetrahydrofuran 1600U 1600 54
108-88-3 Toluene 160U 160 12
*87-61-6 1,2,3-Trichlorobenzene 540U 540 9.8
120-82-1 1,2,4-Trichlorobenzene 540U 540 11
71-55-6 1,1,1-Trichloroethane 81U 81 9.4
79-00-5 1,1,2-Trichloroethane 81U 81 11
Continued on next page
*See Statement of Data Qualifications
Page 79 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-19 Sampled: 10/11/11 14:10Lab Sample ID: 1110319-20 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/18/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111418 Analytical Batch: 1J19045Percent Solids: 56
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 81U 81 9.3
75-69-4 Trichlorofluoromethane 160U 160 12
96-18-4 1,2,3-Trichloropropane 160U 160 67
*526-73-8 1,2,3-Trimethylbenzene 410U 410 9.4
95-63-6 1,2,4-Trimethylbenzene 160U 160 9.3
108-67-8 1,3,5-Trimethylbenzene 160U 160 9.4
75-01-4 Vinyl Chloride 65U 65 11
179601-23-1 Xylene, Meta + Para 160U 160 17
95-47-6 Xylene, Ortho 81U 81 11
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 80 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-19 Sampled: 10/11/11 14:10Lab Sample ID: 1110319-20 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 56 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111475
Page 81 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-20 Sampled: 10/11/11 13:37Lab Sample ID: 1110319-21 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 120J 1200 110
107-13-1 Acrylonitrile 120U 120 24
71-43-2 Benzene 60U 60 7.2
108-86-1 Bromobenzene 120U 120 6.8
74-97-5 Bromochloromethane 120U 120 7.2
75-27-4 Bromodichloromethane 120U 120 6.2
75-25-2 Bromoform 120U 120 9.2
*74-83-9 Bromomethane 70J 240 14
104-51-8 n-Butylbenzene 11J 60 6.3
135-98-8 sec-Butylbenzene 60U 60 6.3
98-06-6 tert-Butylbenzene 60U 60 6.8
75-15-0 Carbon Disulfide 300U 300 6.2
56-23-5 Carbon Tetrachloride 60U 60 6.0
108-90-7 Chlorobenzene 60U 60 14
75-00-3 Chloroethane 300U 300 13
67-66-3 Chloroform 60U 60 6.9
74-87-3 Chloromethane 100J 300 8.1
110-82-7 Cyclohexane 110J 300 8.0
*96-12-8 1,2-Dibromo-3-chloropropane 60U 60 14
124-48-1 Dibromochloromethane 120U 120 18
106-93-4 1,2-Dibromoethane 60U 60 9.0
74-95-3 Dibromomethane 300U 300 7.0
*110-57-6 trans-1,4-Dichloro-2-butene 60U 60 5.3
95-50-1 1,2-Dichlorobenzene 120U 120 6.2
541-73-1 1,3-Dichlorobenzene 120U 120 6.6
106-46-7 1,4-Dichlorobenzene 120U 120 8.1
75-71-8 Dichlorodifluoromethane 300U 300 9.2
75-34-3 1,1-Dichloroethane 60U 60 6.0
107-06-2 1,2-Dichloroethane 60U 60 6.4
75-35-4 1,1-Dichloroethene 60U 60 9.0
156-59-2 cis-1,2-Dichloroethene 60U 60 7.5
Continued on next page
*See Statement of Data Qualifications
Page 82 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-20 Sampled: 10/11/11 13:37Lab Sample ID: 1110319-21 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 60U 60 6.5
78-87-5 1,2-Dichloropropane 60U 60 7.7
10061-01-5 cis-1,3-Dichloropropene 60U 60 9.9
10061-02-6 trans-1,3-Dichloropropene 60U 60 6.8
100-41-4 Ethylbenzene 60U 60 8.2
60-29-7 Ethyl Ether 240U 240 11
591-78-6 2-Hexanone 3000U 3000 20
*74-88-4 Iodomethane 190 120 9.6
98-82-8 Isopropylbenzene 300U 300 8.8
108-20-3 Isopropyl Ether 300U 300 2.3
99-87-6 4-Isopropyltoluene 120U 120 8.2
1634-04-4 Methyl tert-Butyl Ether 300U 300 8.0
75-09-2 Methylene Chloride 22J 120 7.0
78-93-3 2-Butanone (MEK) 65J 900 31
91-57-6 2-Methylnaphthalene 410 400 9.2
108-10-1 4-Methyl-2-pentanone (MIBK) 3000U 3000 7.1
*91-20-3 Naphthalene 260J 400 8.2
994-05-8 tert-Amyl Methyl Ether 300U 300 2.9
637-92-3 Ethyl tert-Butyl Ether 300U 300 4.2
103-65-1 n-Propylbenzene 7.8J 120 6.9
100-42-5 Styrene 6.6J 60 6.3
75-65-0 t-Butanol 3000U 3000 150
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 18
79-34-5 1,1,2,2-Tetrachloroethane 60U 60 14
127-18-4 Tetrachloroethene 60U 60 6.2
109-99-9 Tetrahydrofuran 1200U 1200 40
108-88-3 Toluene 41J 120 8.7
87-61-6 1,2,3-Trichlorobenzene 400U 400 7.2
120-82-1 1,2,4-Trichlorobenzene 400U 400 7.8
71-55-6 1,1,1-Trichloroethane 60U 60 7.0
79-00-5 1,1,2-Trichloroethane 60U 60 8.1
Continued on next page
*See Statement of Data Qualifications
Page 83 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-20 Sampled: 10/11/11 13:37Lab Sample ID: 1110319-21 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 83
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 60U 60 6.9
75-69-4 Trichlorofluoromethane 120U 120 8.9
96-18-4 1,2,3-Trichloropropane 120U 120 50
*526-73-8 1,2,3-Trimethylbenzene 40J 300 6.9
95-63-6 1,2,4-Trimethylbenzene 51J 120 6.9
108-67-8 1,3,5-Trimethylbenzene 19J 120 7.0
75-01-4 Vinyl Chloride 48U 48 8.1
179601-23-1 Xylene, Meta + Para 71J 120 12
95-47-6 Xylene, Ortho 58J 60 8.4
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 100 84-110
*See Statement of Data Qualifications
Page 84 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-20 Sampled: 10/11/11 13:37Lab Sample ID: 1110319-21 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 83 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 85 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-01 Sampled: 10/10/11 17:01Lab Sample ID: 1110319-22 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 66
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1500U 1500 140
107-13-1 Acrylonitrile 150U 150 30
71-43-2 Benzene 76U 76 9.1
108-86-1 Bromobenzene 150U 150 8.5
74-97-5 Bromochloromethane 150U 150 9.1
75-27-4 Bromodichloromethane 150U 150 7.8
75-25-2 Bromoform 150U 150 12
*74-83-9 Bromomethane 120J 300 18
104-51-8 n-Butylbenzene 76U 76 7.9
135-98-8 sec-Butylbenzene 76U 76 7.9
98-06-6 tert-Butylbenzene 76U 76 8.5
75-15-0 Carbon Disulfide 380U 380 7.8
56-23-5 Carbon Tetrachloride 76U 76 7.6
108-90-7 Chlorobenzene 76U 76 17
75-00-3 Chloroethane 380U 380 16
67-66-3 Chloroform 76U 76 8.7
74-87-3 Chloromethane 160J 380 10
110-82-7 Cyclohexane 380U 380 10
*96-12-8 1,2-Dibromo-3-chloropropane 76U 76 18
124-48-1 Dibromochloromethane 150U 150 23
106-93-4 1,2-Dibromoethane 76U 76 11
74-95-3 Dibromomethane 380U 380 8.8
*110-57-6 trans-1,4-Dichloro-2-butene 76U 76 6.7
95-50-1 1,2-Dichlorobenzene 150U 150 7.8
541-73-1 1,3-Dichlorobenzene 150U 150 8.4
106-46-7 1,4-Dichlorobenzene 150U 150 10
75-71-8 Dichlorodifluoromethane 380U 380 12
75-34-3 1,1-Dichloroethane 76U 76 7.6
107-06-2 1,2-Dichloroethane 76U 76 8.1
75-35-4 1,1-Dichloroethene 76U 76 11
156-59-2 cis-1,2-Dichloroethene 76U 76 9.4
Continued on next page
*See Statement of Data Qualifications
Page 86 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-01 Sampled: 10/10/11 17:01Lab Sample ID: 1110319-22 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 66
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 76U 76 8.2
78-87-5 1,2-Dichloropropane 76U 76 9.8
10061-01-5 cis-1,3-Dichloropropene 76U 76 12
10061-02-6 trans-1,3-Dichloropropene 76U 76 8.5
100-41-4 Ethylbenzene 76U 76 10
60-29-7 Ethyl Ether 300U 300 14
591-78-6 2-Hexanone 3800U 3800 25
*74-88-4 Iodomethane 300 150 12
98-82-8 Isopropylbenzene 380U 380 11
108-20-3 Isopropyl Ether 380U 380 2.9
99-87-6 4-Isopropyltoluene 150U 150 10
1634-04-4 Methyl tert-Butyl Ether 380U 380 10
75-09-2 Methylene Chloride 32J 150 8.8
78-93-3 2-Butanone (MEK) 110J 1100 39
91-57-6 2-Methylnaphthalene 500U 500 12
108-10-1 4-Methyl-2-pentanone (MIBK) 3800U 3800 9.0
*91-20-3 Naphthalene 190J 500 10
994-05-8 tert-Amyl Methyl Ether 380U 380 3.7
637-92-3 Ethyl tert-Butyl Ether 380U 380 5.3
103-65-1 n-Propylbenzene 150U 150 8.7
100-42-5 Styrene 76U 76 7.9
75-65-0 t-Butanol 3800U 3800 190
630-20-6 1,1,1,2-Tetrachloroethane 150U 150 23
79-34-5 1,1,2,2-Tetrachloroethane 76U 76 17
127-18-4 Tetrachloroethene 76U 76 7.8
109-99-9 Tetrahydrofuran 1500U 1500 51
108-88-3 Toluene 150U 150 11
87-61-6 1,2,3-Trichlorobenzene 500U 500 9.1
120-82-1 1,2,4-Trichlorobenzene 500U 500 9.9
71-55-6 1,1,1-Trichloroethane 76U 76 8.8
79-00-5 1,1,2-Trichloroethane 76U 76 10
Continued on next page
*See Statement of Data Qualifications
Page 87 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-01 Sampled: 10/10/11 17:01Lab Sample ID: 1110319-22 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 66
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 76U 76 8.7
75-69-4 Trichlorofluoromethane 150U 150 11
96-18-4 1,2,3-Trichloropropane 150U 150 63
526-73-8 1,2,3-Trimethylbenzene 380U 380 8.8
95-63-6 1,2,4-Trimethylbenzene 150U 150 8.7
108-67-8 1,3,5-Trimethylbenzene 150U 150 8.8
75-01-4 Vinyl Chloride 61U 61 10
179601-23-1 Xylene, Meta + Para 150U 150 16
95-47-6 Xylene, Ortho 76U 76 11
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 88 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-01 Sampled: 10/10/11 17:01Lab Sample ID: 1110319-22 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 66 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 89 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-02 Sampled: 10/10/11 16:10Lab Sample ID: 1110319-23 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1300U 1300 120
107-13-1 Acrylonitrile 130U 130 26
71-43-2 Benzene 65U 65 7.7
108-86-1 Bromobenzene 130U 130 7.2
74-97-5 Bromochloromethane 130U 130 7.7
75-27-4 Bromodichloromethane 130U 130 6.6
75-25-2 Bromoform 130U 130 9.8
*74-83-9 Bromomethane 79J 260 15
104-51-8 n-Butylbenzene 65U 65 6.7
135-98-8 sec-Butylbenzene 65U 65 6.7
98-06-6 tert-Butylbenzene 65U 65 7.2
75-15-0 Carbon Disulfide 320U 320 6.6
56-23-5 Carbon Tetrachloride 65U 65 6.5
108-90-7 Chlorobenzene 65U 65 15
75-00-3 Chloroethane 320U 320 14
67-66-3 Chloroform 65U 65 7.4
74-87-3 Chloromethane 99J 320 8.6
110-82-7 Cyclohexane 320U 320 8.5
*96-12-8 1,2-Dibromo-3-chloropropane 65U 65 15
124-48-1 Dibromochloromethane 130U 130 19
106-93-4 1,2-Dibromoethane 65U 65 9.7
74-95-3 Dibromomethane 320U 320 7.5
*110-57-6 trans-1,4-Dichloro-2-butene 65U 65 5.7
95-50-1 1,2-Dichlorobenzene 130U 130 6.6
541-73-1 1,3-Dichlorobenzene 130U 130 7.1
106-46-7 1,4-Dichlorobenzene 130U 130 8.6
75-71-8 Dichlorodifluoromethane 320U 320 9.8
75-34-3 1,1-Dichloroethane 65U 65 6.5
107-06-2 1,2-Dichloroethane 65U 65 6.8
75-35-4 1,1-Dichloroethene 65U 65 9.7
156-59-2 cis-1,2-Dichloroethene 65U 65 8.0
Continued on next page
*See Statement of Data Qualifications
Page 90 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-02 Sampled: 10/10/11 16:10Lab Sample ID: 1110319-23 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 65U 65 7.0
78-87-5 1,2-Dichloropropane 65U 65 8.3
10061-01-5 cis-1,3-Dichloropropene 65U 65 11
10061-02-6 trans-1,3-Dichloropropene 65U 65 7.2
100-41-4 Ethylbenzene 65U 65 8.8
60-29-7 Ethyl Ether 260U 260 12
591-78-6 2-Hexanone 3200U 3200 21
*74-88-4 Iodomethane 200 130 10
98-82-8 Isopropylbenzene 320U 320 9.4
108-20-3 Isopropyl Ether 320U 320 2.5
99-87-6 4-Isopropyltoluene 130U 130 8.8
1634-04-4 Methyl tert-Butyl Ether 320U 320 8.5
75-09-2 Methylene Chloride 130U 130 7.5
78-93-3 2-Butanone (MEK) 81J 970 33
91-57-6 2-Methylnaphthalene 430U 430 9.8
108-10-1 4-Methyl-2-pentanone (MIBK) 3200U 3200 7.6
*91-20-3 Naphthalene 430U 430 8.8
994-05-8 tert-Amyl Methyl Ether 320U 320 3.1
637-92-3 Ethyl tert-Butyl Ether 320U 320 4.4
103-65-1 n-Propylbenzene 130U 130 7.4
100-42-5 Styrene 65U 65 6.7
75-65-0 t-Butanol 3200U 3200 160
630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 65U 65 15
127-18-4 Tetrachloroethene 65U 65 6.6
109-99-9 Tetrahydrofuran 1300U 1300 43
108-88-3 Toluene 130U 130 9.3
87-61-6 1,2,3-Trichlorobenzene 430U 430 7.7
120-82-1 1,2,4-Trichlorobenzene 430U 430 8.4
71-55-6 1,1,1-Trichloroethane 65U 65 7.5
79-00-5 1,1,2-Trichloroethane 65U 65 8.6
Continued on next page
*See Statement of Data Qualifications
Page 91 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-02 Sampled: 10/10/11 16:10Lab Sample ID: 1110319-23 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 65U 65 7.4
75-69-4 Trichlorofluoromethane 130U 130 9.6
96-18-4 1,2,3-Trichloropropane 130U 130 53
526-73-8 1,2,3-Trimethylbenzene 320U 320 7.4
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.4
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.5
75-01-4 Vinyl Chloride 52U 52 8.6
179601-23-1 Xylene, Meta + Para 130U 130 13
95-47-6 Xylene, Ortho 65U 65 9.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Page 92 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-02 Sampled: 10/10/11 16:10Lab Sample ID: 1110319-23 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 77 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 93 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-03 Sampled: 10/10/11 16:00Lab Sample ID: 1110319-24 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 79
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1400U 1400 120
107-13-1 Acrylonitrile 140U 140 27
71-43-2 Benzene 68U 68 8.2
108-86-1 Bromobenzene 140U 140 7.6
74-97-5 Bromochloromethane 140U 140 8.2
75-27-4 Bromodichloromethane 140U 140 7.0
75-25-2 Bromoform 140U 140 10
74-83-9 Bromomethane 270U 270 16
104-51-8 n-Butylbenzene 68U 68 7.1
135-98-8 sec-Butylbenzene 68U 68 7.1
98-06-6 tert-Butylbenzene 68U 68 7.6
75-15-0 Carbon Disulfide 340U 340 7.0
56-23-5 Carbon Tetrachloride 68U 68 6.8
108-90-7 Chlorobenzene 68U 68 16
75-00-3 Chloroethane 340U 340 14
67-66-3 Chloroform 68U 68 7.8
74-87-3 Chloromethane 340U 340 9.1
110-82-7 Cyclohexane 340U 340 9.0
*96-12-8 1,2-Dibromo-3-chloropropane 68U 68 16
124-48-1 Dibromochloromethane 140U 140 20
106-93-4 1,2-Dibromoethane 68U 68 10
74-95-3 Dibromomethane 340U 340 7.9
*110-57-6 trans-1,4-Dichloro-2-butene 68U 68 6.0
95-50-1 1,2-Dichlorobenzene 140U 140 7.0
541-73-1 1,3-Dichlorobenzene 140U 140 7.5
106-46-7 1,4-Dichlorobenzene 140U 140 9.1
75-71-8 Dichlorodifluoromethane 340U 340 10
75-34-3 1,1-Dichloroethane 68U 68 6.8
107-06-2 1,2-Dichloroethane 68U 68 7.2
75-35-4 1,1-Dichloroethene 68U 68 10
156-59-2 cis-1,2-Dichloroethene 68U 68 8.5
Continued on next page
*See Statement of Data Qualifications
Page 94 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-03 Sampled: 10/10/11 16:00Lab Sample ID: 1110319-24 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 79
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 68U 68 7.4
78-87-5 1,2-Dichloropropane 68U 68 8.7
10061-01-5 cis-1,3-Dichloropropene 68U 68 11
10061-02-6 trans-1,3-Dichloropropene 68U 68 7.6
100-41-4 Ethylbenzene 68U 68 9.3
60-29-7 Ethyl Ether 270U 270 13
591-78-6 2-Hexanone 3400U 3400 22
*74-88-4 Iodomethane 140 140 11
98-82-8 Isopropylbenzene 340U 340 9.9
108-20-3 Isopropyl Ether 340U 340 2.6
99-87-6 4-Isopropyltoluene 140U 140 9.3
1634-04-4 Methyl tert-Butyl Ether 340U 340 9.0
75-09-2 Methylene Chloride 26J 140 7.9
78-93-3 2-Butanone (MEK) 1000U 1000 35
91-57-6 2-Methylnaphthalene 450U 450 10
108-10-1 4-Methyl-2-pentanone (MIBK) 3400U 3400 8.0
*91-20-3 Naphthalene 450U 450 9.3
994-05-8 tert-Amyl Methyl Ether 340U 340 3.3
637-92-3 Ethyl tert-Butyl Ether 340U 340 4.7
103-65-1 n-Propylbenzene 140U 140 7.8
100-42-5 Styrene 68U 68 7.1
75-65-0 t-Butanol 3400U 3400 170
630-20-6 1,1,1,2-Tetrachloroethane 140U 140 21
79-34-5 1,1,2,2-Tetrachloroethane 68U 68 15
127-18-4 Tetrachloroethene 68U 68 7.0
109-99-9 Tetrahydrofuran 1400U 1400 45
108-88-3 Toluene 140U 140 9.8
87-61-6 1,2,3-Trichlorobenzene 450U 450 8.2
120-82-1 1,2,4-Trichlorobenzene 450U 450 8.9
71-55-6 1,1,1-Trichloroethane 68U 68 7.9
79-00-5 1,1,2-Trichloroethane 68U 68 9.1
Continued on next page
*See Statement of Data Qualifications
Page 95 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-03 Sampled: 10/10/11 16:00Lab Sample ID: 1110319-24 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 79
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 68U 68 7.8
75-69-4 Trichlorofluoromethane 140U 140 10
96-18-4 1,2,3-Trichloropropane 140U 140 56
526-73-8 1,2,3-Trimethylbenzene 340U 340 7.8
95-63-6 1,2,4-Trimethylbenzene 140U 140 7.8
108-67-8 1,3,5-Trimethylbenzene 140U 140 7.9
75-01-4 Vinyl Chloride 55U 55 9.1
179601-23-1 Xylene, Meta + Para 140U 140 14
95-47-6 Xylene, Ortho 68U 68 9.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Page 96 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-03 Sampled: 10/10/11 16:00Lab Sample ID: 1110319-24 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 79 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 97 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04 Sampled: 10/10/11 18:12Lab Sample ID: 1110319-25 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1400U 1400 120
107-13-1 Acrylonitrile 140U 140 27
71-43-2 Benzene 68U 68 8.2
108-86-1 Bromobenzene 140U 140 7.6
74-97-5 Bromochloromethane 140U 140 8.2
75-27-4 Bromodichloromethane 140U 140 6.9
75-25-2 Bromoform 140U 140 10
*74-83-9 Bromomethane 65J 270 16
104-51-8 n-Butylbenzene 68U 68 7.1
135-98-8 sec-Butylbenzene 68U 68 7.1
98-06-6 tert-Butylbenzene 68U 68 7.6
75-15-0 Carbon Disulfide 340U 340 6.9
56-23-5 Carbon Tetrachloride 68U 68 6.8
108-90-7 Chlorobenzene 68U 68 16
75-00-3 Chloroethane 340U 340 14
67-66-3 Chloroform 68U 68 7.8
74-87-3 Chloromethane 60J 340 9.1
110-82-7 Cyclohexane 340U 340 9.0
*96-12-8 1,2-Dibromo-3-chloropropane 68U 68 16
124-48-1 Dibromochloromethane 140U 140 20
106-93-4 1,2-Dibromoethane 68U 68 10
74-95-3 Dibromomethane 340U 340 7.9
*110-57-6 trans-1,4-Dichloro-2-butene 68U 68 6.0
95-50-1 1,2-Dichlorobenzene 140U 140 6.9
541-73-1 1,3-Dichlorobenzene 140U 140 7.5
106-46-7 1,4-Dichlorobenzene 15J 140 9.1
75-71-8 Dichlorodifluoromethane 340U 340 10
75-34-3 1,1-Dichloroethane 68U 68 6.8
107-06-2 1,2-Dichloroethane 68U 68 7.2
75-35-4 1,1-Dichloroethene 68U 68 10
156-59-2 cis-1,2-Dichloroethene 68U 68 8.4
Continued on next page
*See Statement of Data Qualifications
Page 98 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04 Sampled: 10/10/11 18:12Lab Sample ID: 1110319-25 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 68U 68 7.3
78-87-5 1,2-Dichloropropane 68U 68 8.7
10061-01-5 cis-1,3-Dichloropropene 68U 68 11
10061-02-6 trans-1,3-Dichloropropene 68U 68 7.6
100-41-4 Ethylbenzene 68U 68 9.2
60-29-7 Ethyl Ether 270U 270 13
591-78-6 2-Hexanone 3400U 3400 22
*74-88-4 Iodomethane 130J 140 11
98-82-8 Isopropylbenzene 340U 340 9.9
108-20-3 Isopropyl Ether 340U 340 2.6
99-87-6 4-Isopropyltoluene 140U 140 9.2
1634-04-4 Methyl tert-Butyl Ether 340U 340 9.0
75-09-2 Methylene Chloride 25J 140 7.9
78-93-3 2-Butanone (MEK) 1000U 1000 35
91-57-6 2-Methylnaphthalene 450U 450 10
108-10-1 4-Methyl-2-pentanone (MIBK) 3400U 3400 8.0
*91-20-3 Naphthalene 200J 450 9.2
994-05-8 tert-Amyl Methyl Ether 340U 340 3.3
637-92-3 Ethyl tert-Butyl Ether 340U 340 4.7
103-65-1 n-Propylbenzene 140U 140 7.8
100-42-5 Styrene 68U 68 7.1
75-65-0 t-Butanol 3400U 3400 170
630-20-6 1,1,1,2-Tetrachloroethane 140U 140 21
79-34-5 1,1,2,2-Tetrachloroethane 68U 68 15
127-18-4 Tetrachloroethene 68U 68 6.9
109-99-9 Tetrahydrofuran 1400U 1400 45
108-88-3 Toluene 140U 140 9.8
87-61-6 1,2,3-Trichlorobenzene 450U 450 8.2
120-82-1 1,2,4-Trichlorobenzene 450U 450 8.8
71-55-6 1,1,1-Trichloroethane 68U 68 7.9
79-00-5 1,1,2-Trichloroethane 68U 68 9.1
Continued on next page
*See Statement of Data Qualifications
Page 99 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04 Sampled: 10/10/11 18:12Lab Sample ID: 1110319-25 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 82
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 68U 68 7.8
75-69-4 Trichlorofluoromethane 140U 140 10
96-18-4 1,2,3-Trichloropropane 140U 140 56
526-73-8 1,2,3-Trimethylbenzene 340U 340 7.8
95-63-6 1,2,4-Trimethylbenzene 140U 140 7.8
108-67-8 1,3,5-Trimethylbenzene 140U 140 7.9
75-01-4 Vinyl Chloride 54U 54 9.1
179601-23-1 Xylene, Meta + Para 140U 140 14
95-47-6 Xylene, Ortho 68U 68 9.5
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Page 100 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04 Sampled: 10/10/11 18:12Lab Sample ID: 1110319-25 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 82 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 101 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04D Sampled: 10/10/11 18:12Lab Sample ID: 1110319-26 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1200U 1200 110
107-13-1 Acrylonitrile 120U 120 24
71-43-2 Benzene 62U 62 7.4
108-86-1 Bromobenzene 120U 120 6.9
74-97-5 Bromochloromethane 120U 120 7.4
75-27-4 Bromodichloromethane 120U 120 6.3
75-25-2 Bromoform 120U 120 9.4
74-83-9 Bromomethane 250U 250 14
104-51-8 n-Butylbenzene 62U 62 6.4
135-98-8 sec-Butylbenzene 62U 62 6.4
98-06-6 tert-Butylbenzene 62U 62 6.9
75-15-0 Carbon Disulfide 310U 310 6.3
56-23-5 Carbon Tetrachloride 62U 62 6.2
108-90-7 Chlorobenzene 62U 62 14
75-00-3 Chloroethane 310U 310 13
67-66-3 Chloroform 62U 62 7.0
74-87-3 Chloromethane 310U 310 8.2
110-82-7 Cyclohexane 310U 310 8.1
*96-12-8 1,2-Dibromo-3-chloropropane 62U 62 15
124-48-1 Dibromochloromethane 120U 120 18
106-93-4 1,2-Dibromoethane 62U 62 9.2
74-95-3 Dibromomethane 310U 310 7.1
*110-57-6 trans-1,4-Dichloro-2-butene 62U 62 5.4
95-50-1 1,2-Dichlorobenzene 120U 120 6.3
541-73-1 1,3-Dichlorobenzene 120U 120 6.8
106-46-7 1,4-Dichlorobenzene 120U 120 8.2
75-71-8 Dichlorodifluoromethane 310U 310 9.4
75-34-3 1,1-Dichloroethane 62U 62 6.2
107-06-2 1,2-Dichloroethane 62U 62 6.5
75-35-4 1,1-Dichloroethene 62U 62 9.2
156-59-2 cis-1,2-Dichloroethene 62U 62 7.6
Continued on next page
*See Statement of Data Qualifications
Page 102 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04D Sampled: 10/10/11 18:12Lab Sample ID: 1110319-26 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 62U 62 6.6
78-87-5 1,2-Dichloropropane 62U 62 7.9
10061-01-5 cis-1,3-Dichloropropene 62U 62 10
10061-02-6 trans-1,3-Dichloropropene 62U 62 6.9
100-41-4 Ethylbenzene 62U 62 8.4
60-29-7 Ethyl Ether 250U 250 12
591-78-6 2-Hexanone 3100U 3100 20
*74-88-4 Iodomethane 110J 120 9.8
98-82-8 Isopropylbenzene 310U 310 9.0
108-20-3 Isopropyl Ether 310U 310 2.4
99-87-6 4-Isopropyltoluene 120U 120 8.4
1634-04-4 Methyl tert-Butyl Ether 310U 310 8.1
75-09-2 Methylene Chloride 26J 120 7.1
78-93-3 2-Butanone (MEK) 920U 920 31
91-57-6 2-Methylnaphthalene 410U 410 9.4
108-10-1 4-Methyl-2-pentanone (MIBK) 3100U 3100 7.3
*91-20-3 Naphthalene 170J 410 8.4
994-05-8 tert-Amyl Methyl Ether 310U 310 3.0
637-92-3 Ethyl tert-Butyl Ether 310U 310 4.2
103-65-1 n-Propylbenzene 120U 120 7.0
100-42-5 Styrene 62U 62 6.4
75-65-0 t-Butanol 3100U 3100 160
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 19
79-34-5 1,1,2,2-Tetrachloroethane 62U 62 14
127-18-4 Tetrachloroethene 62U 62 6.3
109-99-9 Tetrahydrofuran 1200U 1200 41
108-88-3 Toluene 120U 120 8.9
87-61-6 1,2,3-Trichlorobenzene 410U 410 7.4
120-82-1 1,2,4-Trichlorobenzene 410U 410 8.0
71-55-6 1,1,1-Trichloroethane 62U 62 7.1
79-00-5 1,1,2-Trichloroethane 62U 62 8.2
Continued on next page
*See Statement of Data Qualifications
Page 103 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04D Sampled: 10/10/11 18:12Lab Sample ID: 1110319-26 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 62U 62 7.0
75-69-4 Trichlorofluoromethane 120U 120 9.1
96-18-4 1,2,3-Trichloropropane 120U 120 51
526-73-8 1,2,3-Trimethylbenzene 310U 310 7.1
95-63-6 1,2,4-Trimethylbenzene 120U 120 7.0
108-67-8 1,3,5-Trimethylbenzene 120U 120 7.1
75-01-4 Vinyl Chloride 49U 49 8.2
179601-23-1 Xylene, Meta + Para 120U 120 13
95-47-6 Xylene, Ortho 62U 62 8.6
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Page 104 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-04D Sampled: 10/10/11 18:12Lab Sample ID: 1110319-26 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 81 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 105 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-05 Sampled: 10/10/11 18:40Lab Sample ID: 1110319-27 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 98
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 55U 55 6.6
108-86-1 Bromobenzene 110U 110 6.2
74-97-5 Bromochloromethane 110U 110 6.6
75-27-4 Bromodichloromethane 110U 110 5.6
75-25-2 Bromoform 110U 110 8.3
*74-83-9 Bromomethane 40J 220 13
104-51-8 n-Butylbenzene 55U 55 5.7
135-98-8 sec-Butylbenzene 55U 55 5.7
98-06-6 tert-Butylbenzene 55U 55 6.2
75-15-0 Carbon Disulfide 270U 270 5.6
56-23-5 Carbon Tetrachloride 55U 55 5.5
108-90-7 Chlorobenzene 55U 55 13
75-00-3 Chloroethane 270U 270 12
67-66-3 Chloroform 55U 55 6.3
74-87-3 Chloromethane 270U 270 7.4
110-82-7 Cyclohexane 270U 270 7.2
*96-12-8 1,2-Dibromo-3-chloropropane 55U 55 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 55U 55 8.2
74-95-3 Dibromomethane 270U 270 6.4
*110-57-6 trans-1,4-Dichloro-2-butene 55U 55 4.8
95-50-1 1,2-Dichlorobenzene 110U 110 5.6
541-73-1 1,3-Dichlorobenzene 110U 110 6.0
106-46-7 1,4-Dichlorobenzene 110U 110 7.4
75-71-8 Dichlorodifluoromethane 270U 270 8.3
75-34-3 1,1-Dichloroethane 55U 55 5.5
107-06-2 1,2-Dichloroethane 55U 55 5.8
75-35-4 1,1-Dichloroethene 55U 55 8.2
156-59-2 cis-1,2-Dichloroethene 55U 55 6.8
Continued on next page
*See Statement of Data Qualifications
Page 106 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-05 Sampled: 10/10/11 18:40Lab Sample ID: 1110319-27 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 55U 55 5.9
78-87-5 1,2-Dichloropropane 55U 55 7.0
10061-01-5 cis-1,3-Dichloropropene 55U 55 9.0
10061-02-6 trans-1,3-Dichloropropene 55U 55 6.2
100-41-4 Ethylbenzene 55U 55 7.5
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
*74-88-4 Iodomethane 110 110 8.8
98-82-8 Isopropylbenzene 270U 270 8.0
108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.5
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.2
75-09-2 Methylene Chloride 22J 110 6.4
78-93-3 2-Butanone (MEK) 59J 820 28
91-57-6 2-Methylnaphthalene 360U 360 8.3
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.5
*91-20-3 Naphthalene 160J 360 7.5
994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
637-92-3 Ethyl tert-Butyl Ether 270U 270 3.8
103-65-1 n-Propylbenzene 110U 110 6.3
100-42-5 Styrene 55U 55 5.7
75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 55U 55 12
127-18-4 Tetrachloroethene 55U 55 5.6
109-99-9 Tetrahydrofuran 1100U 1100 37
108-88-3 Toluene 14J 110 7.9
87-61-6 1,2,3-Trichlorobenzene 360U 360 6.6
120-82-1 1,2,4-Trichlorobenzene 360U 360 7.1
71-55-6 1,1,1-Trichloroethane 55U 55 6.4
79-00-5 1,1,2-Trichloroethane 55U 55 7.4
Continued on next page
*See Statement of Data Qualifications
Page 107 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-05 Sampled: 10/10/11 18:40Lab Sample ID: 1110319-27 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 91
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 55U 55 6.3
75-69-4 Trichlorofluoromethane 110U 110 8.1
96-18-4 1,2,3-Trichloropropane 110U 110 45
526-73-8 1,2,3-Trimethylbenzene 270U 270 6.3
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.3
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.4
75-01-4 Vinyl Chloride 44U 44 7.4
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 55U 55 7.7
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 108 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-05 Sampled: 10/10/11 18:40Lab Sample ID: 1110319-27 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 91 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 109 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-06 Sampled: 10/11/11 09:30Lab Sample ID: 1110319-28 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 97
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 8.6J 55 6.5
108-86-1 Bromobenzene 110U 110 6.1
74-97-5 Bromochloromethane 110U 110 6.5
75-27-4 Bromodichloromethane 110U 110 5.6
75-25-2 Bromoform 110U 110 8.3
*74-83-9 Bromomethane 48J 220 13
104-51-8 n-Butylbenzene 55U 55 5.7
135-98-8 sec-Butylbenzene 55U 55 5.7
98-06-6 tert-Butylbenzene 55U 55 6.1
75-15-0 Carbon Disulfide 270U 270 5.6
56-23-5 Carbon Tetrachloride 55U 55 5.5
108-90-7 Chlorobenzene 55U 55 12
75-00-3 Chloroethane 270U 270 12
67-66-3 Chloroform 55U 55 6.2
74-87-3 Chloromethane 270U 270 7.3
110-82-7 Cyclohexane 270U 270 7.2
*96-12-8 1,2-Dibromo-3-chloropropane 55U 55 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 55U 55 8.2
74-95-3 Dibromomethane 270U 270 6.3
*110-57-6 trans-1,4-Dichloro-2-butene 55U 55 4.8
95-50-1 1,2-Dichlorobenzene 110U 110 5.6
541-73-1 1,3-Dichlorobenzene 110U 110 6.0
106-46-7 1,4-Dichlorobenzene 110U 110 7.3
75-71-8 Dichlorodifluoromethane 270U 270 8.3
75-34-3 1,1-Dichloroethane 55U 55 5.5
107-06-2 1,2-Dichloroethane 55U 55 5.8
75-35-4 1,1-Dichloroethene 55U 55 8.2
156-59-2 cis-1,2-Dichloroethene 55U 55 6.8
Continued on next page
*See Statement of Data Qualifications
Page 110 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-06 Sampled: 10/11/11 09:30Lab Sample ID: 1110319-28 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 55U 55 5.9
78-87-5 1,2-Dichloropropane 55U 55 7.0
10061-01-5 cis-1,3-Dichloropropene 55U 55 8.9
10061-02-6 trans-1,3-Dichloropropene 55U 55 6.1
100-41-4 Ethylbenzene 55U 55 7.4
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
*74-88-4 Iodomethane 100J 110 8.7
98-82-8 Isopropylbenzene 270U 270 8.0
108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.4
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.2
75-09-2 Methylene Chloride 21J 110 6.3
78-93-3 2-Butanone (MEK) 820U 820 28
91-57-6 2-Methylnaphthalene 360U 360 8.3
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.4
*91-20-3 Naphthalene 140J 360 7.4
994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
637-92-3 Ethyl tert-Butyl Ether 270U 270 3.8
103-65-1 n-Propylbenzene 110U 110 6.2
100-42-5 Styrene 55U 55 5.7
75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 55U 55 12
127-18-4 Tetrachloroethene 55U 55 5.6
109-99-9 Tetrahydrofuran 1100U 1100 36
108-88-3 Toluene 31J 110 7.9
87-61-6 1,2,3-Trichlorobenzene 360U 360 6.5
120-82-1 1,2,4-Trichlorobenzene 360U 360 7.1
71-55-6 1,1,1-Trichloroethane 55U 55 6.3
79-00-5 1,1,2-Trichloroethane 55U 55 7.3
Continued on next page
*See Statement of Data Qualifications
Page 111 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-06 Sampled: 10/11/11 09:30Lab Sample ID: 1110319-28 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 92
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 55U 55 6.2
75-69-4 Trichlorofluoromethane 110U 110 8.1
96-18-4 1,2,3-Trichloropropane 110U 110 45
526-73-8 1,2,3-Trimethylbenzene 270U 270 6.3
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.2
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.3
75-01-4 Vinyl Chloride 44U 44 7.3
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 55U 55 7.6
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
Page 112 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-06 Sampled: 10/11/11 09:30Lab Sample ID: 1110319-28 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 92 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 113 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-07 Sampled: 10/11/11 10:15Lab Sample ID: 1110319-29 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.9
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.9
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
*74-83-9 Bromomethane 50J 230 13
104-51-8 n-Butylbenzene 57U 57 6.0
135-98-8 sec-Butylbenzene 57U 57 6.0
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 50J 290 7.7
110-82-7 Cyclohexane 290U 290 7.6
*96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.6
*110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.7
75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.1
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 114 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-07 Sampled: 10/11/11 10:15Lab Sample ID: 1110319-29 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.4
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 100J 110 9.2
98-82-8 Isopropylbenzene 290U 290 8.4
108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.6
75-09-2 Methylene Chloride 24J 110 6.6
78-93-3 2-Butanone (MEK) 860U 860 29
91-57-6 2-Methylnaphthalene 380U 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.8
*91-20-3 Naphthalene 380U 380 7.8
994-05-8 tert-Amyl Methyl Ether 290U 290 2.7
637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 6.0
75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 110U 110 8.2
87-61-6 1,2,3-Trichlorobenzene 380U 380 6.9
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.7
Continued on next page
*See Statement of Data Qualifications
Page 115 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-07 Sampled: 10/11/11 10:15Lab Sample ID: 1110319-29 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 87
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.5
96-18-4 1,2,3-Trichloropropane 110U 110 47
526-73-8 1,2,3-Trimethylbenzene 290U 290 6.6
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 46U 46 7.7
179601-23-1 Xylene, Meta + Para 110U 110 12
95-47-6 Xylene, Ortho 57U 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 99 84-110
Page 116 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-07 Sampled: 10/11/11 10:15Lab Sample ID: 1110319-29 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 87 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 117 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-08 Sampled: 10/11/11 14:55Lab Sample ID: 1110319-30 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 100
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 56U 56 6.8
108-86-1 Bromobenzene 110U 110 6.3
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.7
75-25-2 Bromoform 110U 110 8.6
*74-83-9 Bromomethane 70J 230 13
104-51-8 n-Butylbenzene 56U 56 5.9
135-98-8 sec-Butylbenzene 56U 56 5.9
98-06-6 tert-Butylbenzene 56U 56 6.3
75-15-0 Carbon Disulfide 280U 280 5.7
56-23-5 Carbon Tetrachloride 56U 56 5.6
108-90-7 Chlorobenzene 56U 56 13
75-00-3 Chloroethane 280U 280 12
67-66-3 Chloroform 56U 56 6.4
74-87-3 Chloromethane 75J 280 7.5
110-82-7 Cyclohexane 280U 280 7.4
*96-12-8 1,2-Dibromo-3-chloropropane 56U 56 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 56U 56 8.4
74-95-3 Dibromomethane 280U 280 6.5
*110-57-6 trans-1,4-Dichloro-2-butene 56U 56 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.7
541-73-1 1,3-Dichlorobenzene 110U 110 6.2
106-46-7 1,4-Dichlorobenzene 110U 110 7.5
75-71-8 Dichlorodifluoromethane 280U 280 8.6
75-34-3 1,1-Dichloroethane 56U 56 5.6
107-06-2 1,2-Dichloroethane 56U 56 6.0
75-35-4 1,1-Dichloroethene 56U 56 8.4
156-59-2 cis-1,2-Dichloroethene 56U 56 7.0
Continued on next page
*See Statement of Data Qualifications
Page 118 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-08 Sampled: 10/11/11 14:55Lab Sample ID: 1110319-30 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 56U 56 6.1
78-87-5 1,2-Dichloropropane 56U 56 7.2
10061-01-5 cis-1,3-Dichloropropene 56U 56 9.2
10061-02-6 trans-1,3-Dichloropropene 56U 56 6.3
100-41-4 Ethylbenzene 56U 56 7.7
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2800U 2800 18
*74-88-4 Iodomethane 130 110 9.0
98-82-8 Isopropylbenzene 280U 280 8.2
108-20-3 Isopropyl Ether 280U 280 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.7
1634-04-4 Methyl tert-Butyl Ether 280U 280 7.4
75-09-2 Methylene Chloride 24J 110 6.5
78-93-3 2-Butanone (MEK) 840U 840 29
91-57-6 2-Methylnaphthalene 370U 370 8.6
108-10-1 4-Methyl-2-pentanone (MIBK) 2800U 2800 6.6
*91-20-3 Naphthalene 370U 370 7.7
994-05-8 tert-Amyl Methyl Ether 280U 280 2.7
637-92-3 Ethyl tert-Butyl Ether 280U 280 3.9
103-65-1 n-Propylbenzene 110U 110 6.4
100-42-5 Styrene 56U 56 5.9
75-65-0 t-Butanol 2800U 2800 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 56U 56 13
127-18-4 Tetrachloroethene 56U 56 5.7
109-99-9 Tetrahydrofuran 1100U 1100 37
108-88-3 Toluene 110U 110 8.1
87-61-6 1,2,3-Trichlorobenzene 370U 370 6.8
120-82-1 1,2,4-Trichlorobenzene 370U 370 7.3
71-55-6 1,1,1-Trichloroethane 56U 56 6.5
79-00-5 1,1,2-Trichloroethane 56U 56 7.5
Continued on next page
*See Statement of Data Qualifications
Page 119 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-08 Sampled: 10/11/11 14:55Lab Sample ID: 1110319-30 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 89
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 56U 56 6.4
75-69-4 Trichlorofluoromethane 110U 110 8.3
96-18-4 1,2,3-Trichloropropane 110U 110 46
526-73-8 1,2,3-Trimethylbenzene 280U 280 6.5
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.4
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.5
75-01-4 Vinyl Chloride 45U 45 7.5
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 56U 56 7.9
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Page 120 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-08 Sampled: 10/11/11 14:55Lab Sample ID: 1110319-30 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 89 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 121 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-09 Sampled: 10/11/11 14:08Lab Sample ID: 1110319-31 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 95
107-13-1 Acrylonitrile 110U 110 21
71-43-2 Benzene 53U 53 6.4
108-86-1 Bromobenzene 110U 110 6.0
74-97-5 Bromochloromethane 110U 110 6.4
75-27-4 Bromodichloromethane 110U 110 5.4
75-25-2 Bromoform 110U 110 8.1
74-83-9 Bromomethane 210U 210 12
104-51-8 n-Butylbenzene 53U 53 5.5
135-98-8 sec-Butylbenzene 53U 53 5.5
98-06-6 tert-Butylbenzene 53U 53 6.0
75-15-0 Carbon Disulfide 270U 270 5.4
56-23-5 Carbon Tetrachloride 53U 53 5.3
108-90-7 Chlorobenzene 53U 53 12
75-00-3 Chloroethane 270U 270 11
67-66-3 Chloroform 53U 53 6.1
74-87-3 Chloromethane 270U 270 7.1
110-82-7 Cyclohexane 270U 270 7.0
*96-12-8 1,2-Dibromo-3-chloropropane 53U 53 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 53U 53 8.0
74-95-3 Dibromomethane 270U 270 6.2
*110-57-6 trans-1,4-Dichloro-2-butene 53U 53 4.7
95-50-1 1,2-Dichlorobenzene 110U 110 5.4
541-73-1 1,3-Dichlorobenzene 110U 110 5.8
106-46-7 1,4-Dichlorobenzene 110U 110 7.1
75-71-8 Dichlorodifluoromethane 270U 270 8.1
75-34-3 1,1-Dichloroethane 53U 53 5.3
107-06-2 1,2-Dichloroethane 53U 53 5.6
75-35-4 1,1-Dichloroethene 53U 53 8.0
156-59-2 cis-1,2-Dichloroethene 53U 53 6.6
Continued on next page
*See Statement of Data Qualifications
Page 122 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-09 Sampled: 10/11/11 14:08Lab Sample ID: 1110319-31 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 53U 53 5.7
78-87-5 1,2-Dichloropropane 53U 53 6.8
10061-01-5 cis-1,3-Dichloropropene 53U 53 8.7
10061-02-6 trans-1,3-Dichloropropene 53U 53 6.0
100-41-4 Ethylbenzene 53U 53 7.2
60-29-7 Ethyl Ether 210U 210 10
591-78-6 2-Hexanone 2700U 2700 17
*74-88-4 Iodomethane 74J 110 8.5
98-82-8 Isopropylbenzene 270U 270 7.8
108-20-3 Isopropyl Ether 270U 270 2.0
99-87-6 4-Isopropyltoluene 110U 110 7.2
1634-04-4 Methyl tert-Butyl Ether 270U 270 7.0
75-09-2 Methylene Chloride 23J 110 6.2
78-93-3 2-Butanone (MEK) 65J 800 27
91-57-6 2-Methylnaphthalene 350U 350 8.1
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.3
*91-20-3 Naphthalene 350U 350 7.2
994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
637-92-3 Ethyl tert-Butyl Ether 270U 270 3.7
103-65-1 n-Propylbenzene 110U 110 6.1
100-42-5 Styrene 53U 53 5.5
75-65-0 t-Butanol 2700U 2700 140
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 16
79-34-5 1,1,2,2-Tetrachloroethane 53U 53 12
127-18-4 Tetrachloroethene 53U 53 5.4
109-99-9 Tetrahydrofuran 1100U 1100 35
108-88-3 Toluene 110U 110 7.7
87-61-6 1,2,3-Trichlorobenzene 350U 350 6.4
120-82-1 1,2,4-Trichlorobenzene 350U 350 6.9
71-55-6 1,1,1-Trichloroethane 53U 53 6.2
79-00-5 1,1,2-Trichloroethane 53U 53 7.1
Continued on next page
*See Statement of Data Qualifications
Page 123 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-09 Sampled: 10/11/11 14:08Lab Sample ID: 1110319-31 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 94
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 53U 53 6.1
75-69-4 Trichlorofluoromethane 110U 110 7.9
96-18-4 1,2,3-Trichloropropane 110U 110 44
526-73-8 1,2,3-Trimethylbenzene 270U 270 6.1
95-63-6 1,2,4-Trimethylbenzene 110U 110 6.1
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.2
75-01-4 Vinyl Chloride 43U 43 7.1
179601-23-1 Xylene, Meta + Para 110U 110 11
95-47-6 Xylene, Ortho 53U 53 7.4
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 124 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-09 Sampled: 10/11/11 14:08Lab Sample ID: 1110319-31 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 94 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 125 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-10 Sampled: 10/11/11 11:48Lab Sample ID: 1110319-32 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 76
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1300U 1300 120
107-13-1 Acrylonitrile 130U 130 26
71-43-2 Benzene 66U 66 7.9
108-86-1 Bromobenzene 130U 130 7.4
74-97-5 Bromochloromethane 130U 130 7.9
75-27-4 Bromodichloromethane 130U 130 6.7
75-25-2 Bromoform 130U 130 10
74-83-9 Bromomethane 260U 260 15
104-51-8 n-Butylbenzene 66U 66 6.9
135-98-8 sec-Butylbenzene 66U 66 6.9
98-06-6 tert-Butylbenzene 66U 66 7.4
75-15-0 Carbon Disulfide 16J 330 6.7
56-23-5 Carbon Tetrachloride 66U 66 6.6
108-90-7 Chlorobenzene 66U 66 15
75-00-3 Chloroethane 330U 330 14
67-66-3 Chloroform 66U 66 7.5
74-87-3 Chloromethane 330U 330 8.9
110-82-7 Cyclohexane 330U 330 8.7
*96-12-8 1,2-Dibromo-3-chloropropane 66U 66 16
124-48-1 Dibromochloromethane 130U 130 20
106-93-4 1,2-Dibromoethane 66U 66 9.9
74-95-3 Dibromomethane 330U 330 7.7
*110-57-6 trans-1,4-Dichloro-2-butene 66U 66 5.8
95-50-1 1,2-Dichlorobenzene 130U 130 6.7
541-73-1 1,3-Dichlorobenzene 130U 130 7.3
106-46-7 1,4-Dichlorobenzene 130U 130 8.9
75-71-8 Dichlorodifluoromethane 330U 330 10
75-34-3 1,1-Dichloroethane 66U 66 6.6
107-06-2 1,2-Dichloroethane 66U 66 7.0
75-35-4 1,1-Dichloroethene 66U 66 9.9
156-59-2 cis-1,2-Dichloroethene 66U 66 8.2
Continued on next page
*See Statement of Data Qualifications
Page 126 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-10 Sampled: 10/11/11 11:48Lab Sample ID: 1110319-32 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 76
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 66U 66 7.1
78-87-5 1,2-Dichloropropane 66U 66 8.5
10061-01-5 cis-1,3-Dichloropropene 66U 66 11
10061-02-6 trans-1,3-Dichloropropene 66U 66 7.4
100-41-4 Ethylbenzene 66U 66 9.0
60-29-7 Ethyl Ether 260U 260 12
591-78-6 2-Hexanone 3300U 3300 22
*74-88-4 Iodomethane 100J 130 11
98-82-8 Isopropylbenzene 330U 330 9.7
108-20-3 Isopropyl Ether 330U 330 2.5
99-87-6 4-Isopropyltoluene 130U 130 9.0
1634-04-4 Methyl tert-Butyl Ether 330U 330 8.7
75-09-2 Methylene Chloride 33J 130 7.7
78-93-3 2-Butanone (MEK) 98J 990 34
91-57-6 2-Methylnaphthalene 440U 440 10
108-10-1 4-Methyl-2-pentanone (MIBK) 3300U 3300 7.8
*91-20-3 Naphthalene 180J 440 9.0
994-05-8 tert-Amyl Methyl Ether 330U 330 3.2
637-92-3 Ethyl tert-Butyl Ether 330U 330 4.6
103-65-1 n-Propylbenzene 130U 130 7.5
100-42-5 Styrene 66U 66 6.9
75-65-0 t-Butanol 3300U 3300 170
630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 66U 66 15
127-18-4 Tetrachloroethene 66U 66 6.7
109-99-9 Tetrahydrofuran 1300U 1300 44
108-88-3 Toluene 29J 130 9.5
87-61-6 1,2,3-Trichlorobenzene 440U 440 7.9
120-82-1 1,2,4-Trichlorobenzene 440U 440 8.6
71-55-6 1,1,1-Trichloroethane 66U 66 7.7
79-00-5 1,1,2-Trichloroethane 66U 66 8.9
Continued on next page
*See Statement of Data Qualifications
Page 127 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-10 Sampled: 10/11/11 11:48Lab Sample ID: 1110319-32 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 76
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 66U 66 7.5
75-69-4 Trichlorofluoromethane 130U 130 9.8
96-18-4 1,2,3-Trichloropropane 130U 130 55
526-73-8 1,2,3-Trimethylbenzene 330U 330 7.6
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.5
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.7
75-01-4 Vinyl Chloride 53U 53 8.9
179601-23-1 Xylene, Meta + Para 130U 130 13
95-47-6 Xylene, Ortho 66U 66 9.3
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 99 84-110
Page 128 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-10 Sampled: 10/11/11 11:48Lab Sample ID: 1110319-32 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 76 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 129 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-11 Sampled: 10/11/11 16:30Lab Sample ID: 1110319-33 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.8
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
74-83-9 Bromomethane 230U 230 13
104-51-8 n-Butylbenzene 7.7J 57 5.9
135-98-8 sec-Butylbenzene 57U 57 5.9
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 290U 290 7.6
110-82-7 Cyclohexane 77J 290 7.5
*96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.6
*110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.6
75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.0
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 130 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-11 Sampled: 10/11/11 16:30Lab Sample ID: 1110319-33 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.4
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 71J 110 9.1
98-82-8 Isopropylbenzene 290U 290 8.3
108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.5
75-09-2 Methylene Chloride 27J 110 6.6
78-93-3 2-Butanone (MEK) 69J 860 29
91-57-6 2-Methylnaphthalene 350J 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.7
*91-20-3 Naphthalene 200J 380 7.8
994-05-8 tert-Amyl Methyl Ether 290U 290 2.7
637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 8.9J 110 6.5
100-42-5 Styrene 57U 57 5.9
75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 55J 110 8.2
87-61-6 1,2,3-Trichlorobenzene 380U 380 6.8
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.6
Continued on next page
*See Statement of Data Qualifications
Page 131 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-11 Sampled: 10/11/11 16:30Lab Sample ID: 1110319-33 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.4
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 27J 290 6.6
95-63-6 1,2,4-Trimethylbenzene 42J 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 46U 46 7.6
179601-23-1 Xylene, Meta + Para 78J 110 12
95-47-6 Xylene, Ortho 56J 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
*See Statement of Data Qualifications
Page 132 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-11 Sampled: 10/11/11 16:30Lab Sample ID: 1110319-33 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 88 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 133 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-12 Sampled: 10/11/11 17:04Lab Sample ID: 1110319-34 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 71
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1400U 1400 130
107-13-1 Acrylonitrile 140U 140 28
71-43-2 Benzene 70U 70 8.4
108-86-1 Bromobenzene 140U 140 7.9
74-97-5 Bromochloromethane 140U 140 8.4
75-27-4 Bromodichloromethane 140U 140 7.2
75-25-2 Bromoform 140U 140 11
74-83-9 Bromomethane 280U 280 16
104-51-8 n-Butylbenzene 70U 70 7.3
135-98-8 sec-Butylbenzene 70U 70 7.3
98-06-6 tert-Butylbenzene 70U 70 7.9
75-15-0 Carbon Disulfide 350U 350 7.2
56-23-5 Carbon Tetrachloride 70U 70 7.0
108-90-7 Chlorobenzene 70U 70 16
75-00-3 Chloroethane 350U 350 15
67-66-3 Chloroform 70U 70 8.0
74-87-3 Chloromethane 350U 350 9.4
110-82-7 Cyclohexane 350U 350 9.3
*96-12-8 1,2-Dibromo-3-chloropropane 70U 70 17
124-48-1 Dibromochloromethane 140U 140 21
106-93-4 1,2-Dibromoethane 70U 70 11
74-95-3 Dibromomethane 350U 350 8.2
*110-57-6 trans-1,4-Dichloro-2-butene 70U 70 6.2
95-50-1 1,2-Dichlorobenzene 140U 140 7.2
541-73-1 1,3-Dichlorobenzene 140U 140 7.7
106-46-7 1,4-Dichlorobenzene 140U 140 9.4
75-71-8 Dichlorodifluoromethane 350U 350 11
75-34-3 1,1-Dichloroethane 70U 70 7.0
107-06-2 1,2-Dichloroethane 70U 70 7.5
75-35-4 1,1-Dichloroethene 70U 70 11
156-59-2 cis-1,2-Dichloroethene 70U 70 8.7
Continued on next page
*See Statement of Data Qualifications
Page 134 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-12 Sampled: 10/11/11 17:04Lab Sample ID: 1110319-34 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 71
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 70U 70 7.6
78-87-5 1,2-Dichloropropane 70U 70 9.0
10061-01-5 cis-1,3-Dichloropropene 70U 70 12
10061-02-6 trans-1,3-Dichloropropene 70U 70 7.9
100-41-4 Ethylbenzene 70U 70 9.6
60-29-7 Ethyl Ether 280U 280 13
591-78-6 2-Hexanone 3500U 3500 23
*74-88-4 Iodomethane 91J 140 11
98-82-8 Isopropylbenzene 350U 350 10
108-20-3 Isopropyl Ether 350U 350 2.7
99-87-6 4-Isopropyltoluene 140U 140 9.6
1634-04-4 Methyl tert-Butyl Ether 350U 350 9.3
75-09-2 Methylene Chloride 33J 140 8.2
78-93-3 2-Butanone (MEK) 1100U 1100 36
91-57-6 2-Methylnaphthalene 460U 460 11
108-10-1 4-Methyl-2-pentanone (MIBK) 3500U 3500 8.3
*91-20-3 Naphthalene 460U 460 9.6
994-05-8 tert-Amyl Methyl Ether 350U 350 3.4
637-92-3 Ethyl tert-Butyl Ether 350U 350 4.8
103-65-1 n-Propylbenzene 140U 140 8.0
100-42-5 Styrene 70U 70 7.3
75-65-0 t-Butanol 3500U 3500 180
630-20-6 1,1,1,2-Tetrachloroethane 140U 140 21
79-34-5 1,1,2,2-Tetrachloroethane 70U 70 16
127-18-4 Tetrachloroethene 70U 70 7.2
109-99-9 Tetrahydrofuran 1400U 1400 47
108-88-3 Toluene 140U 140 10
87-61-6 1,2,3-Trichlorobenzene 460U 460 8.4
120-82-1 1,2,4-Trichlorobenzene 460U 460 9.1
71-55-6 1,1,1-Trichloroethane 70U 70 8.2
79-00-5 1,1,2-Trichloroethane 70U 70 9.4
Continued on next page
*See Statement of Data Qualifications
Page 135 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-12 Sampled: 10/11/11 17:04Lab Sample ID: 1110319-34 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 71
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 70U 70 8.0
75-69-4 Trichlorofluoromethane 140U 140 10
96-18-4 1,2,3-Trichloropropane 140U 140 58
526-73-8 1,2,3-Trimethylbenzene 350U 350 8.1
95-63-6 1,2,4-Trimethylbenzene 140U 140 8.0
108-67-8 1,3,5-Trimethylbenzene 140U 140 8.2
75-01-4 Vinyl Chloride 56U 56 9.4
179601-23-1 Xylene, Meta + Para 140U 140 14
95-47-6 Xylene, Ortho 70U 70 9.8
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 103 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 136 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-12 Sampled: 10/11/11 17:04Lab Sample ID: 1110319-34 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 71 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 137 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-13 Sampled: 10/11/11 10:53Lab Sample ID: 1110319-35 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1100U 1100 100
107-13-1 Acrylonitrile 110U 110 23
71-43-2 Benzene 57U 57 6.8
108-86-1 Bromobenzene 110U 110 6.4
74-97-5 Bromochloromethane 110U 110 6.8
75-27-4 Bromodichloromethane 110U 110 5.8
75-25-2 Bromoform 110U 110 8.7
74-83-9 Bromomethane 230U 230 13
104-51-8 n-Butylbenzene 57U 57 5.9
135-98-8 sec-Butylbenzene 57U 57 5.9
98-06-6 tert-Butylbenzene 57U 57 6.4
75-15-0 Carbon Disulfide 290U 290 5.8
56-23-5 Carbon Tetrachloride 57U 57 5.7
108-90-7 Chlorobenzene 57U 57 13
75-00-3 Chloroethane 290U 290 12
67-66-3 Chloroform 57U 57 6.5
74-87-3 Chloromethane 290U 290 7.6
110-82-7 Cyclohexane 73J 290 7.5
*96-12-8 1,2-Dibromo-3-chloropropane 57U 57 14
124-48-1 Dibromochloromethane 110U 110 17
106-93-4 1,2-Dibromoethane 57U 57 8.6
74-95-3 Dibromomethane 290U 290 6.6
*110-57-6 trans-1,4-Dichloro-2-butene 57U 57 5.0
95-50-1 1,2-Dichlorobenzene 110U 110 5.8
541-73-1 1,3-Dichlorobenzene 110U 110 6.3
106-46-7 1,4-Dichlorobenzene 110U 110 7.6
75-71-8 Dichlorodifluoromethane 290U 290 8.7
75-34-3 1,1-Dichloroethane 57U 57 5.7
107-06-2 1,2-Dichloroethane 57U 57 6.0
75-35-4 1,1-Dichloroethene 57U 57 8.6
156-59-2 cis-1,2-Dichloroethene 57U 57 7.1
Continued on next page
*See Statement of Data Qualifications
Page 138 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-13 Sampled: 10/11/11 10:53Lab Sample ID: 1110319-35 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 57U 57 6.2
78-87-5 1,2-Dichloropropane 57U 57 7.3
10061-01-5 cis-1,3-Dichloropropene 57U 57 9.3
10061-02-6 trans-1,3-Dichloropropene 57U 57 6.4
100-41-4 Ethylbenzene 57U 57 7.8
60-29-7 Ethyl Ether 230U 230 11
591-78-6 2-Hexanone 2900U 2900 19
*74-88-4 Iodomethane 74J 110 9.1
98-82-8 Isopropylbenzene 290U 290 8.3
108-20-3 Isopropyl Ether 290U 290 2.2
99-87-6 4-Isopropyltoluene 110U 110 7.8
1634-04-4 Methyl tert-Butyl Ether 290U 290 7.5
75-09-2 Methylene Chloride 23J 110 6.6
78-93-3 2-Butanone (MEK) 860U 860 29
91-57-6 2-Methylnaphthalene 330J 380 8.7
108-10-1 4-Methyl-2-pentanone (MIBK) 2900U 2900 6.7
*91-20-3 Naphthalene 180J 380 7.8
994-05-8 tert-Amyl Methyl Ether 290U 290 2.7
637-92-3 Ethyl tert-Butyl Ether 290U 290 3.9
103-65-1 n-Propylbenzene 110U 110 6.5
100-42-5 Styrene 57U 57 5.9
75-65-0 t-Butanol 2900U 2900 150
630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 57U 57 13
127-18-4 Tetrachloroethene 57U 57 5.8
109-99-9 Tetrahydrofuran 1100U 1100 38
108-88-3 Toluene 22J 110 8.2
87-61-6 1,2,3-Trichlorobenzene 380U 380 6.8
120-82-1 1,2,4-Trichlorobenzene 380U 380 7.4
71-55-6 1,1,1-Trichloroethane 57U 57 6.6
79-00-5 1,1,2-Trichloroethane 57U 57 7.6
Continued on next page
*See Statement of Data Qualifications
Page 139 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-13 Sampled: 10/11/11 10:53Lab Sample ID: 1110319-35 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 88
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 57U 57 6.5
75-69-4 Trichlorofluoromethane 110U 110 8.4
96-18-4 1,2,3-Trichloropropane 110U 110 47
*526-73-8 1,2,3-Trimethylbenzene 23J 290 6.6
95-63-6 1,2,4-Trimethylbenzene 37J 110 6.5
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.6
75-01-4 Vinyl Chloride 46U 46 7.6
179601-23-1 Xylene, Meta + Para 45J 110 12
95-47-6 Xylene, Ortho 42J 57 8.0
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 140 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-13 Sampled: 10/11/11 10:53Lab Sample ID: 1110319-35 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 88 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 141 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-14 Sampled: 10/11/11 18:03Lab Sample ID: 1110319-36 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 84
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1200U 1200 110
107-13-1 Acrylonitrile 120U 120 24
71-43-2 Benzene 60U 60 7.1
108-86-1 Bromobenzene 120U 120 6.7
74-97-5 Bromochloromethane 120U 120 7.1
75-27-4 Bromodichloromethane 120U 120 6.1
75-25-2 Bromoform 120U 120 9.0
74-83-9 Bromomethane 240U 240 14
104-51-8 n-Butylbenzene 60U 60 6.2
135-98-8 sec-Butylbenzene 60U 60 6.2
98-06-6 tert-Butylbenzene 60U 60 6.7
75-15-0 Carbon Disulfide 300U 300 6.1
56-23-5 Carbon Tetrachloride 60U 60 6.0
108-90-7 Chlorobenzene 60U 60 14
75-00-3 Chloroethane 300U 300 13
67-66-3 Chloroform 60U 60 6.8
74-87-3 Chloromethane 300U 300 8.0
110-82-7 Cyclohexane 300U 300 7.9
*96-12-8 1,2-Dibromo-3-chloropropane 60U 60 14
124-48-1 Dibromochloromethane 120U 120 18
106-93-4 1,2-Dibromoethane 60U 60 8.9
74-95-3 Dibromomethane 300U 300 6.9
*110-57-6 trans-1,4-Dichloro-2-butene 60U 60 5.2
95-50-1 1,2-Dichlorobenzene 120U 120 6.1
541-73-1 1,3-Dichlorobenzene 120U 120 6.5
106-46-7 1,4-Dichlorobenzene 120U 120 8.0
75-71-8 Dichlorodifluoromethane 300U 300 9.0
75-34-3 1,1-Dichloroethane 60U 60 6.0
107-06-2 1,2-Dichloroethane 60U 60 6.3
75-35-4 1,1-Dichloroethene 60U 60 8.9
156-59-2 cis-1,2-Dichloroethene 60U 60 7.4
Continued on next page
*See Statement of Data Qualifications
Page 142 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-14 Sampled: 10/11/11 18:03Lab Sample ID: 1110319-36 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 84
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 60U 60 6.4
78-87-5 1,2-Dichloropropane 60U 60 7.6
10061-01-5 cis-1,3-Dichloropropene 60U 60 9.8
10061-02-6 trans-1,3-Dichloropropene 60U 60 6.7
100-41-4 Ethylbenzene 60U 60 8.1
60-29-7 Ethyl Ether 240U 240 11
591-78-6 2-Hexanone 3000U 3000 19
*74-88-4 Iodomethane 74J 120 9.5
98-82-8 Isopropylbenzene 300U 300 8.7
108-20-3 Isopropyl Ether 300U 300 2.3
99-87-6 4-Isopropyltoluene 120U 120 8.1
1634-04-4 Methyl tert-Butyl Ether 300U 300 7.9
75-09-2 Methylene Chloride 26J 120 6.9
78-93-3 2-Butanone (MEK) 890U 890 30
91-57-6 2-Methylnaphthalene 390U 390 9.0
108-10-1 4-Methyl-2-pentanone (MIBK) 3000U 3000 7.0
*91-20-3 Naphthalene 390U 390 8.1
994-05-8 tert-Amyl Methyl Ether 300U 300 2.9
637-92-3 Ethyl tert-Butyl Ether 300U 300 4.1
103-65-1 n-Propylbenzene 120U 120 6.8
100-42-5 Styrene 60U 60 6.2
75-65-0 t-Butanol 3000U 3000 150
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 18
79-34-5 1,1,2,2-Tetrachloroethane 60U 60 13
127-18-4 Tetrachloroethene 60U 60 6.1
109-99-9 Tetrahydrofuran 1200U 1200 40
108-88-3 Toluene 120U 120 8.6
87-61-6 1,2,3-Trichlorobenzene 390U 390 7.1
120-82-1 1,2,4-Trichlorobenzene 390U 390 7.7
71-55-6 1,1,1-Trichloroethane 60U 60 6.9
79-00-5 1,1,2-Trichloroethane 60U 60 8.0
Continued on next page
*See Statement of Data Qualifications
Page 143 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-14 Sampled: 10/11/11 18:03Lab Sample ID: 1110319-36 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 84
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 60U 60 6.8
75-69-4 Trichlorofluoromethane 120U 120 8.8
96-18-4 1,2,3-Trichloropropane 120U 120 49
526-73-8 1,2,3-Trimethylbenzene 300U 300 6.8
95-63-6 1,2,4-Trimethylbenzene 120U 120 6.8
108-67-8 1,3,5-Trimethylbenzene 120U 120 6.9
75-01-4 Vinyl Chloride 48U 48 8.0
179601-23-1 Xylene, Meta + Para 120U 120 12
95-47-6 Xylene, Ortho 60U 60 8.3
Surrogates: % Recovery Control Limits
Dibromofluoromethane 102 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 144 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SB-14 Sampled: 10/11/11 18:03Lab Sample ID: 1110319-36 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 84 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 145 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-01 Sampled: 10/12/11 13:30Lab Sample ID: 1110319-37 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1300U 1300 120
107-13-1 Acrylonitrile 130U 130 26
71-43-2 Benzene 65U 65 7.8
108-86-1 Bromobenzene 130U 130 7.3
74-97-5 Bromochloromethane 130U 130 7.8
75-27-4 Bromodichloromethane 130U 130 6.6
75-25-2 Bromoform 130U 130 9.9
*74-83-9 Bromomethane 54J 260 15
104-51-8 n-Butylbenzene 65U 65 6.8
135-98-8 sec-Butylbenzene 65U 65 6.8
98-06-6 tert-Butylbenzene 65U 65 7.3
75-15-0 Carbon Disulfide 320U 320 6.6
56-23-5 Carbon Tetrachloride 65U 65 6.5
108-90-7 Chlorobenzene 65U 65 15
75-00-3 Chloroethane 320U 320 14
67-66-3 Chloroform 65U 65 7.4
74-87-3 Chloromethane 320U 320 8.7
110-82-7 Cyclohexane 320U 320 8.6
*96-12-8 1,2-Dibromo-3-chloropropane 65U 65 16
124-48-1 Dibromochloromethane 130U 130 19
106-93-4 1,2-Dibromoethane 65U 65 9.7
74-95-3 Dibromomethane 320U 320 7.5
*110-57-6 trans-1,4-Dichloro-2-butene 65U 65 5.7
95-50-1 1,2-Dichlorobenzene 130U 130 6.6
541-73-1 1,3-Dichlorobenzene 130U 130 7.1
106-46-7 1,4-Dichlorobenzene 130U 130 8.7
75-71-8 Dichlorodifluoromethane 320U 320 9.9
75-34-3 1,1-Dichloroethane 65U 65 6.5
107-06-2 1,2-Dichloroethane 65U 65 6.9
75-35-4 1,1-Dichloroethene 65U 65 9.7
156-59-2 cis-1,2-Dichloroethene 65U 65 8.1
Continued on next page
*See Statement of Data Qualifications
Page 146 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-01 Sampled: 10/12/11 13:30Lab Sample ID: 1110319-37 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 65U 65 7.0
78-87-5 1,2-Dichloropropane 65U 65 8.3
10061-01-5 cis-1,3-Dichloropropene 65U 65 11
10061-02-6 trans-1,3-Dichloropropene 65U 65 7.3
100-41-4 Ethylbenzene 65U 65 8.8
60-29-7 Ethyl Ether 260U 260 12
591-78-6 2-Hexanone 3200U 3200 21
*74-88-4 Iodomethane 82J 130 10
98-82-8 Isopropylbenzene 320U 320 9.5
108-20-3 Isopropyl Ether 320U 320 2.5
99-87-6 4-Isopropyltoluene 130U 130 8.8
1634-04-4 Methyl tert-Butyl Ether 320U 320 8.6
75-09-2 Methylene Chloride 24J 130 7.5
78-93-3 2-Butanone (MEK) 970U 970 33
91-57-6 2-Methylnaphthalene 430U 430 9.9
108-10-1 4-Methyl-2-pentanone (MIBK) 3200U 3200 7.7
*91-20-3 Naphthalene 430U 430 8.8
994-05-8 tert-Amyl Methyl Ether 320U 320 3.1
637-92-3 Ethyl tert-Butyl Ether 320U 320 4.5
103-65-1 n-Propylbenzene 130U 130 7.4
100-42-5 Styrene 65U 65 6.8
75-65-0 t-Butanol 3200U 3200 170
630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 65U 65 15
127-18-4 Tetrachloroethene 65U 65 6.6
109-99-9 Tetrahydrofuran 1300U 1300 43
108-88-3 Toluene 130U 130 9.4
87-61-6 1,2,3-Trichlorobenzene 430U 430 7.8
120-82-1 1,2,4-Trichlorobenzene 430U 430 8.4
71-55-6 1,1,1-Trichloroethane 65U 65 7.5
79-00-5 1,1,2-Trichloroethane 65U 65 8.7
Continued on next page
*See Statement of Data Qualifications
Page 147 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-01 Sampled: 10/12/11 13:30Lab Sample ID: 1110319-37 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 65U 65 7.4
75-69-4 Trichlorofluoromethane 130U 130 9.6
96-18-4 1,2,3-Trichloropropane 130U 130 54
526-73-8 1,2,3-Trimethylbenzene 320U 320 7.5
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.4
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.5
75-01-4 Vinyl Chloride 52U 52 8.7
179601-23-1 Xylene, Meta + Para 130U 130 13
95-47-6 Xylene, Ortho 65U 65 9.1
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 148 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-01 Sampled: 10/12/11 13:30Lab Sample ID: 1110319-37 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 77 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 149 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-02 Sampled: 10/12/11 18:00Lab Sample ID: 1110319-38 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 80
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1200U 1200 110
107-13-1 Acrylonitrile 120U 120 25
71-43-2 Benzene 62U 62 7.5
108-86-1 Bromobenzene 120U 120 7.0
74-97-5 Bromochloromethane 120U 120 7.5
75-27-4 Bromodichloromethane 120U 120 6.3
75-25-2 Bromoform 120U 120 9.4
74-83-9 Bromomethane 250U 250 14
104-51-8 n-Butylbenzene 62U 62 6.5
135-98-8 sec-Butylbenzene 62U 62 6.5
98-06-6 tert-Butylbenzene 62U 62 7.0
75-15-0 Carbon Disulfide 310U 310 6.3
56-23-5 Carbon Tetrachloride 62U 62 6.2
108-90-7 Chlorobenzene 62U 62 14
75-00-3 Chloroethane 310U 310 13
67-66-3 Chloroform 62U 62 7.1
74-87-3 Chloromethane 310U 310 8.3
110-82-7 Cyclohexane 310U 310 8.2
*96-12-8 1,2-Dibromo-3-chloropropane 62U 62 15
124-48-1 Dibromochloromethane 120U 120 19
106-93-4 1,2-Dibromoethane 62U 62 9.3
74-95-3 Dibromomethane 310U 310 7.2
*110-57-6 trans-1,4-Dichloro-2-butene 62U 62 5.5
95-50-1 1,2-Dichlorobenzene 120U 120 6.3
541-73-1 1,3-Dichlorobenzene 120U 120 6.8
106-46-7 1,4-Dichlorobenzene 120U 120 8.3
75-71-8 Dichlorodifluoromethane 310U 310 9.4
75-34-3 1,1-Dichloroethane 62U 62 6.2
107-06-2 1,2-Dichloroethane 62U 62 6.6
75-35-4 1,1-Dichloroethene 62U 62 9.3
156-59-2 cis-1,2-Dichloroethene 62U 62 7.7
Continued on next page
*See Statement of Data Qualifications
Page 150 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-02 Sampled: 10/12/11 18:00Lab Sample ID: 1110319-38 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 80
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 62U 62 6.7
78-87-5 1,2-Dichloropropane 62U 62 8.0
10061-01-5 cis-1,3-Dichloropropene 62U 62 10
10061-02-6 trans-1,3-Dichloropropene 62U 62 7.0
100-41-4 Ethylbenzene 62U 62 8.5
60-29-7 Ethyl Ether 250U 250 12
591-78-6 2-Hexanone 3100U 3100 20
*74-88-4 Iodomethane 60J 120 9.9
98-82-8 Isopropylbenzene 310U 310 9.1
108-20-3 Isopropyl Ether 310U 310 2.4
99-87-6 4-Isopropyltoluene 120U 120 8.5
1634-04-4 Methyl tert-Butyl Ether 310U 310 8.2
75-09-2 Methylene Chloride 25J 120 7.2
78-93-3 2-Butanone (MEK) 930U 930 32
91-57-6 2-Methylnaphthalene 410U 410 9.4
108-10-1 4-Methyl-2-pentanone (MIBK) 3100U 3100 7.3
*91-20-3 Naphthalene 410U 410 8.5
994-05-8 tert-Amyl Methyl Ether 310U 310 3.0
637-92-3 Ethyl tert-Butyl Ether 310U 310 4.3
103-65-1 n-Propylbenzene 120U 120 7.1
100-42-5 Styrene 62U 62 6.5
75-65-0 t-Butanol 3100U 3100 160
630-20-6 1,1,1,2-Tetrachloroethane 120U 120 19
79-34-5 1,1,2,2-Tetrachloroethane 62U 62 14
127-18-4 Tetrachloroethene 62U 62 6.3
109-99-9 Tetrahydrofuran 1200U 1200 41
108-88-3 Toluene 120U 120 8.9
87-61-6 1,2,3-Trichlorobenzene 410U 410 7.5
120-82-1 1,2,4-Trichlorobenzene 410U 410 8.1
71-55-6 1,1,1-Trichloroethane 62U 62 7.2
79-00-5 1,1,2-Trichloroethane 62U 62 8.3
Continued on next page
*See Statement of Data Qualifications
Page 151 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-02 Sampled: 10/12/11 18:00Lab Sample ID: 1110319-38 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 80
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 62U 62 7.1
75-69-4 Trichlorofluoromethane 120U 120 9.2
96-18-4 1,2,3-Trichloropropane 120U 120 51
526-73-8 1,2,3-Trimethylbenzene 310U 310 7.1
95-63-6 1,2,4-Trimethylbenzene 120U 120 7.1
108-67-8 1,3,5-Trimethylbenzene 120U 120 7.2
75-01-4 Vinyl Chloride 50U 50 8.3
179601-23-1 Xylene, Meta + Para 120U 120 13
95-47-6 Xylene, Ortho 62U 62 8.7
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 99 84-110
Page 152 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-02 Sampled: 10/12/11 18:00Lab Sample ID: 1110319-38 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 80 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 153 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03 Sampled: 10/12/11 14:15Lab Sample ID: 1110319-39 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 75
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1300U 1300 120
107-13-1 Acrylonitrile 130U 130 26
71-43-2 Benzene 66U 66 8.0
108-86-1 Bromobenzene 130U 130 7.4
74-97-5 Bromochloromethane 130U 130 8.0
75-27-4 Bromodichloromethane 130U 130 6.8
75-25-2 Bromoform 130U 130 10
74-83-9 Bromomethane 270U 270 15
104-51-8 n-Butylbenzene 66U 66 6.9
135-98-8 sec-Butylbenzene 66U 66 6.9
98-06-6 tert-Butylbenzene 66U 66 7.4
75-15-0 Carbon Disulfide 330U 330 6.8
56-23-5 Carbon Tetrachloride 66U 66 6.6
108-90-7 Chlorobenzene 66U 66 15
75-00-3 Chloroethane 330U 330 14
67-66-3 Chloroform 66U 66 7.6
74-87-3 Chloromethane 330U 330 8.9
110-82-7 Cyclohexane 330U 330 8.8
*96-12-8 1,2-Dibromo-3-chloropropane 66U 66 16
124-48-1 Dibromochloromethane 130U 130 20
106-93-4 1,2-Dibromoethane 66U 66 10
74-95-3 Dibromomethane 330U 330 7.7
*110-57-6 trans-1,4-Dichloro-2-butene 66U 66 5.8
95-50-1 1,2-Dichlorobenzene 130U 130 6.8
541-73-1 1,3-Dichlorobenzene 130U 130 7.3
106-46-7 1,4-Dichlorobenzene 130U 130 8.9
75-71-8 Dichlorodifluoromethane 330U 330 10
75-34-3 1,1-Dichloroethane 66U 66 6.6
107-06-2 1,2-Dichloroethane 66U 66 7.0
75-35-4 1,1-Dichloroethene 66U 66 10
156-59-2 cis-1,2-Dichloroethene 66U 66 8.2
Continued on next page
*See Statement of Data Qualifications
Page 154 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03 Sampled: 10/12/11 14:15Lab Sample ID: 1110319-39 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 75
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 66U 66 7.2
78-87-5 1,2-Dichloropropane 66U 66 8.5
10061-01-5 cis-1,3-Dichloropropene 66U 66 11
10061-02-6 trans-1,3-Dichloropropene 66U 66 7.4
100-41-4 Ethylbenzene 66U 66 9.0
60-29-7 Ethyl Ether 270U 270 12
591-78-6 2-Hexanone 3300U 3300 22
*74-88-4 Iodomethane 60J 130 11
98-82-8 Isopropylbenzene 330U 330 9.7
108-20-3 Isopropyl Ether 330U 330 2.5
99-87-6 4-Isopropyltoluene 130U 130 9.0
1634-04-4 Methyl tert-Butyl Ether 330U 330 8.8
75-09-2 Methylene Chloride 26J 130 7.7
78-93-3 2-Butanone (MEK) 1000U 1000 34
91-57-6 2-Methylnaphthalene 440U 440 10
108-10-1 4-Methyl-2-pentanone (MIBK) 3300U 3300 7.8
*91-20-3 Naphthalene 440U 440 9.0
994-05-8 tert-Amyl Methyl Ether 330U 330 3.2
637-92-3 Ethyl tert-Butyl Ether 330U 330 4.6
103-65-1 n-Propylbenzene 130U 130 7.6
100-42-5 Styrene 66U 66 6.9
75-65-0 t-Butanol 3300U 3300 170
630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 66U 66 15
127-18-4 Tetrachloroethene 66U 66 6.8
109-99-9 Tetrahydrofuran 1300U 1300 44
108-88-3 Toluene 130U 130 9.6
87-61-6 1,2,3-Trichlorobenzene 440U 440 8.0
120-82-1 1,2,4-Trichlorobenzene 440U 440 8.6
71-55-6 1,1,1-Trichloroethane 66U 66 7.7
79-00-5 1,1,2-Trichloroethane 66U 66 8.9
Continued on next page
*See Statement of Data Qualifications
Page 155 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03 Sampled: 10/12/11 14:15Lab Sample ID: 1110319-39 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 75
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 66U 66 7.6
75-69-4 Trichlorofluoromethane 130U 130 9.8
96-18-4 1,2,3-Trichloropropane 130U 130 55
526-73-8 1,2,3-Trimethylbenzene 330U 330 7.6
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.6
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.7
75-01-4 Vinyl Chloride 53U 53 8.9
179601-23-1 Xylene, Meta + Para 130U 130 14
95-47-6 Xylene, Ortho 66U 66 9.3
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 156 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03 Sampled: 10/12/11 14:15Lab Sample ID: 1110319-39 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 75 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 157 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03D Sampled: 10/12/11 14:15Lab Sample ID: 1110319-40 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 1300U 1300 120
107-13-1 Acrylonitrile 130U 130 26
71-43-2 Benzene 65U 65 7.8
108-86-1 Bromobenzene 130U 130 7.3
74-97-5 Bromochloromethane 130U 130 7.8
75-27-4 Bromodichloromethane 130U 130 6.6
75-25-2 Bromoform 130U 130 9.9
74-83-9 Bromomethane 54J 260 15
104-51-8 n-Butylbenzene 65U 65 6.8
135-98-8 sec-Butylbenzene 65U 65 6.8
98-06-6 tert-Butylbenzene 65U 65 7.3
75-15-0 Carbon Disulfide 320U 320 6.6
56-23-5 Carbon Tetrachloride 65U 65 6.5
108-90-7 Chlorobenzene 65U 65 15
75-00-3 Chloroethane 320U 320 14
67-66-3 Chloroform 65U 65 7.4
74-87-3 Chloromethane 71J 320 8.7
110-82-7 Cyclohexane 320U 320 8.6
*96-12-8 1,2-Dibromo-3-chloropropane 65U 65 16
124-48-1 Dibromochloromethane 130U 130 19
106-93-4 1,2-Dibromoethane 65U 65 9.7
74-95-3 Dibromomethane 320U 320 7.5
*110-57-6 trans-1,4-Dichloro-2-butene 65U 65 5.7
95-50-1 1,2-Dichlorobenzene 130U 130 6.6
541-73-1 1,3-Dichlorobenzene 130U 130 7.1
106-46-7 1,4-Dichlorobenzene 130U 130 8.7
*75-71-8 Dichlorodifluoromethane 320U 320 9.9
75-34-3 1,1-Dichloroethane 65U 65 6.5
107-06-2 1,2-Dichloroethane 65U 65 6.9
75-35-4 1,1-Dichloroethene 65U 65 9.7
156-59-2 cis-1,2-Dichloroethene 65U 65 8.1
Continued on next page
*See Statement of Data Qualifications
Page 158 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03D Sampled: 10/12/11 14:15Lab Sample ID: 1110319-40 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 65U 65 7.0
78-87-5 1,2-Dichloropropane 65U 65 8.3
10061-01-5 cis-1,3-Dichloropropene 65U 65 11
10061-02-6 trans-1,3-Dichloropropene 65U 65 7.3
100-41-4 Ethylbenzene 65U 65 8.8
60-29-7 Ethyl Ether 260U 260 12
591-78-6 2-Hexanone 3200U 3200 21
74-88-4 Iodomethane 110J 130 10
98-82-8 Isopropylbenzene 320U 320 9.5
108-20-3 Isopropyl Ether 320U 320 2.5
99-87-6 4-Isopropyltoluene 130U 130 8.8
*1634-04-4 Methyl tert-Butyl Ether 320U 320 8.6
*75-09-2 Methylene Chloride 92J 130 7.5
78-93-3 2-Butanone (MEK) 970U 970 33
*91-57-6 2-Methylnaphthalene 430U 430 9.9
108-10-1 4-Methyl-2-pentanone (MIBK) 3200U 3200 7.7
*91-20-3 Naphthalene 430U 430 8.8
994-05-8 tert-Amyl Methyl Ether 320U 320 3.1
637-92-3 Ethyl tert-Butyl Ether 320U 320 4.5
103-65-1 n-Propylbenzene 130U 130 7.4
100-42-5 Styrene 65U 65 6.8
75-65-0 t-Butanol 3200U 3200 170
*630-20-6 1,1,1,2-Tetrachloroethane 130U 130 20
79-34-5 1,1,2,2-Tetrachloroethane 65U 65 15
127-18-4 Tetrachloroethene 65U 65 6.6
109-99-9 Tetrahydrofuran 1300U 1300 43
108-88-3 Toluene 130U 130 9.3
87-61-6 1,2,3-Trichlorobenzene 430U 430 7.8
120-82-1 1,2,4-Trichlorobenzene 430U 430 8.4
71-55-6 1,1,1-Trichloroethane 65U 65 7.5
79-00-5 1,1,2-Trichloroethane 65U 65 8.7
Continued on next page
*See Statement of Data Qualifications
Page 159 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03D Sampled: 10/12/11 14:15Lab Sample ID: 1110319-40 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 77
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 65U 65 7.4
75-69-4 Trichlorofluoromethane 130U 130 9.6
96-18-4 1,2,3-Trichloropropane 130U 130 54
526-73-8 1,2,3-Trimethylbenzene 320U 320 7.5
95-63-6 1,2,4-Trimethylbenzene 130U 130 7.4
108-67-8 1,3,5-Trimethylbenzene 130U 130 7.5
75-01-4 Vinyl Chloride 52U 52 8.7
179601-23-1 Xylene, Meta + Para 130U 130 13
95-47-6 Xylene, Ortho 65U 65 9.1
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 97 90-1074-Bromofluorobenzene 98 84-110
Page 160 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-03D Sampled: 10/12/11 14:15Lab Sample ID: 1110319-40 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 77 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111477
Page 161 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-04 Sampled: 10/12/11 15:15Lab Sample ID: 1110319-41 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 22
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
67-64-1 Acetone 4500U 4500 400
107-13-1 Acrylonitrile 450U 450 89
71-43-2 Benzene 72J 220 27
108-86-1 Bromobenzene 450U 450 25
74-97-5 Bromochloromethane 450U 450 27
75-27-4 Bromodichloromethane 450U 450 23
75-25-2 Bromoform 450U 450 34
74-83-9 Bromomethane 900U 900 52
104-51-8 n-Butylbenzene 90J 220 23
135-98-8 sec-Butylbenzene 85J 220 23
98-06-6 tert-Butylbenzene 83J 220 25
75-15-0 Carbon Disulfide 1100U 1100 23
56-23-5 Carbon Tetrachloride 76J 220 22
108-90-7 Chlorobenzene 220U 220 51
75-00-3 Chloroethane 1100U 1100 47
67-66-3 Chloroform 51J 220 26
74-87-3 Chloromethane 1100U 1100 30
110-82-7 Cyclohexane 1100U 1100 30
*96-12-8 1,2-Dibromo-3-chloropropane 220U 220 54
124-48-1 Dibromochloromethane 450U 450 67
106-93-4 1,2-Dibromoethane 220U 220 34
74-95-3 Dibromomethane 1100U 1100 26
*110-57-6 trans-1,4-Dichloro-2-butene 220U 220 20
95-50-1 1,2-Dichlorobenzene 450U 450 23
541-73-1 1,3-Dichlorobenzene 450U 450 25
106-46-7 1,4-Dichlorobenzene 36J 450 30
75-71-8 Dichlorodifluoromethane 1100U 1100 34
75-34-3 1,1-Dichloroethane 69J 220 22
107-06-2 1,2-Dichloroethane 220U 220 24
75-35-4 1,1-Dichloroethene 220U 220 34
156-59-2 cis-1,2-Dichloroethene 220U 220 28
Continued on next page
*See Statement of Data Qualifications
Page 162 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-04 Sampled: 10/12/11 15:15Lab Sample ID: 1110319-41 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 22
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 98J 220 24
78-87-5 1,2-Dichloropropane 220U 220 29
10061-01-5 cis-1,3-Dichloropropene 220U 220 37
10061-02-6 trans-1,3-Dichloropropene 220U 220 25
100-41-4 Ethylbenzene 81J 220 30
60-29-7 Ethyl Ether 900U 900 42
591-78-6 2-Hexanone 11000U 11000 73
*74-88-4 Iodomethane 170J 450 36
98-82-8 Isopropylbenzene 81J 1100 33
108-20-3 Isopropyl Ether 1100U 1100 8.5
99-87-6 4-Isopropyltoluene 92J 450 30
1634-04-4 Methyl tert-Butyl Ether 1100U 1100 30
75-09-2 Methylene Chloride 150J 450 26
78-93-3 2-Butanone (MEK) 3400U 3400 110
91-57-6 2-Methylnaphthalene 1500U 1500 34
108-10-1 4-Methyl-2-pentanone (MIBK) 11000U 11000 26
*91-20-3 Naphthalene 600J 1500 30
994-05-8 tert-Amyl Methyl Ether 1100U 1100 11
637-92-3 Ethyl tert-Butyl Ether 1100U 1100 15
103-65-1 n-Propylbenzene 90J 450 26
100-42-5 Styrene 29J 220 23
75-65-0 t-Butanol 11000U 11000 570
630-20-6 1,1,1,2-Tetrachloroethane 450U 450 68
79-34-5 1,1,2,2-Tetrachloroethane 220U 220 51
127-18-4 Tetrachloroethene 92J 220 23
109-99-9 Tetrahydrofuran 4500U 4500 150
108-88-3 Toluene 83J 450 32
87-61-6 1,2,3-Trichlorobenzene 1500U 1500 27
120-82-1 1,2,4-Trichlorobenzene 1500U 1500 29
71-55-6 1,1,1-Trichloroethane 100J 220 26
79-00-5 1,1,2-Trichloroethane 220U 220 30
Continued on next page
*See Statement of Data Qualifications
Page 163 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-04 Sampled: 10/12/11 15:15Lab Sample ID: 1110319-41 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: DLVDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111481 Analytical Batch: 1J20035Percent Solids: 22
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 90J 220 26
75-69-4 Trichlorofluoromethane 450U 450 33
96-18-4 1,2,3-Trichloropropane 450U 450 180
526-73-8 1,2,3-Trimethylbenzene 1100U 1100 26
95-63-6 1,2,4-Trimethylbenzene 56J 450 26
108-67-8 1,3,5-Trimethylbenzene 76J 450 26
75-01-4 Vinyl Chloride 78J 180 30
179601-23-1 Xylene, Meta + Para 160J 450 46
95-47-6 Xylene, Ortho 54J 220 31
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Page 164 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-04 Sampled: 10/12/11 15:15Lab Sample ID: 1110319-41 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 22 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111478
Page 165 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-05 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-42 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 26
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 430J 3800 340
107-13-1 Acrylonitrile 380U 380 75
71-43-2 Benzene 190U 190 23
108-86-1 Bromobenzene 380U 380 21
74-97-5 Bromochloromethane 380U 380 23
75-27-4 Bromodichloromethane 380U 380 19
75-25-2 Bromoform 380U 380 29
74-83-9 Bromomethane 240J 760 44
104-51-8 n-Butylbenzene 190U 190 20
135-98-8 sec-Butylbenzene 190U 190 20
98-06-6 tert-Butylbenzene 190U 190 21
75-15-0 Carbon Disulfide 940U 940 19
56-23-5 Carbon Tetrachloride 190U 190 19
108-90-7 Chlorobenzene 190U 190 43
75-00-3 Chloroethane 940U 940 40
67-66-3 Chloroform 190U 190 22
74-87-3 Chloromethane 330J 940 25
110-82-7 Cyclohexane 940U 940 25
*96-12-8 1,2-Dibromo-3-chloropropane 190U 190 45
124-48-1 Dibromochloromethane 380U 380 57
106-93-4 1,2-Dibromoethane 190U 190 28
74-95-3 Dibromomethane 940U 940 22
*110-57-6 trans-1,4-Dichloro-2-butene 190U 190 17
95-50-1 1,2-Dichlorobenzene 380U 380 19
541-73-1 1,3-Dichlorobenzene 380U 380 21
106-46-7 1,4-Dichlorobenzene 380U 380 25
*75-71-8 Dichlorodifluoromethane 940U 940 29
75-34-3 1,1-Dichloroethane 190U 190 19
107-06-2 1,2-Dichloroethane 190U 190 20
75-35-4 1,1-Dichloroethene 190U 190 28
156-59-2 cis-1,2-Dichloroethene 190U 190 23
Continued on next page
*See Statement of Data Qualifications
Page 166 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-05 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-42 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 26
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 190U 190 20
78-87-5 1,2-Dichloropropane 190U 190 24
10061-01-5 cis-1,3-Dichloropropene 190U 190 31
10061-02-6 trans-1,3-Dichloropropene 190U 190 21
100-41-4 Ethylbenzene 190U 190 26
60-29-7 Ethyl Ether 760U 760 36
591-78-6 2-Hexanone 9400U 9400 62
74-88-4 Iodomethane 440 380 30
98-82-8 Isopropylbenzene 940U 940 28
108-20-3 Isopropyl Ether 940U 940 7.2
99-87-6 4-Isopropyltoluene 380U 380 26
*1634-04-4 Methyl tert-Butyl Ether 940U 940 25
*75-09-2 Methylene Chloride 240J 380 22
78-93-3 2-Butanone (MEK) 2800U 2800 96
*91-57-6 2-Methylnaphthalene 1200U 1200 29
108-10-1 4-Methyl-2-pentanone (MIBK) 9400U 9400 22
*91-20-3 Naphthalene 1200U 1200 26
994-05-8 tert-Amyl Methyl Ether 940U 940 9.1
637-92-3 Ethyl tert-Butyl Ether 940U 940 13
103-65-1 n-Propylbenzene 380U 380 22
100-42-5 Styrene 190U 190 20
75-65-0 t-Butanol 9400U 9400 480
*630-20-6 1,1,1,2-Tetrachloroethane 380U 380 57
79-34-5 1,1,2,2-Tetrachloroethane 190U 190 43
127-18-4 Tetrachloroethene 190U 190 19
109-99-9 Tetrahydrofuran 3800U 3800 130
108-88-3 Toluene 380U 380 27
87-61-6 1,2,3-Trichlorobenzene 1200U 1200 23
120-82-1 1,2,4-Trichlorobenzene 1200U 1200 25
71-55-6 1,1,1-Trichloroethane 190U 190 22
79-00-5 1,1,2-Trichloroethane 190U 190 25
Continued on next page
*See Statement of Data Qualifications
Page 167 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-05 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-42 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 26
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 190U 190 22
75-69-4 Trichlorofluoromethane 380U 380 28
96-18-4 1,2,3-Trichloropropane 380U 380 160
526-73-8 1,2,3-Trimethylbenzene 940U 940 22
95-63-6 1,2,4-Trimethylbenzene 380U 380 22
108-67-8 1,3,5-Trimethylbenzene 380U 380 22
75-01-4 Vinyl Chloride 150U 150 25
179601-23-1 Xylene, Meta + Para 380U 380 39
95-47-6 Xylene, Ortho 190U 190 26
Surrogates: % Recovery Control Limits
Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 102 84-115Toluene-d8 97 90-1074-Bromofluorobenzene 99 84-110
Page 168 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SD-05 Sampled: 10/12/11 16:15Lab Sample ID: 1110319-42 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 26 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111478
Page 169 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12D Sampled: 10/12/11 16:15Lab Sample ID: 1110319-43 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B
AnalyticalCAS Number Analyte Result RL MDL
*67-64-1 Acetone 100J 1100 97
107-13-1 Acrylonitrile 110U 110 22
71-43-2 Benzene 54U 54 6.5
108-86-1 Bromobenzene 110U 110 6.1
74-97-5 Bromochloromethane 110U 110 6.5
75-27-4 Bromodichloromethane 110U 110 5.6
75-25-2 Bromoform 110U 110 8.3
74-83-9 Bromomethane 56J 220 13
104-51-8 n-Butylbenzene 6.0J 54 5.7
135-98-8 sec-Butylbenzene 54U 54 5.7
98-06-6 tert-Butylbenzene 54U 54 6.1
75-15-0 Carbon Disulfide 270U 270 5.6
56-23-5 Carbon Tetrachloride 54U 54 5.4
108-90-7 Chlorobenzene 54U 54 12
75-00-3 Chloroethane 270U 270 12
67-66-3 Chloroform 54U 54 6.2
74-87-3 Chloromethane 70J 270 7.3
110-82-7 Cyclohexane 48J 270 7.2
*96-12-8 1,2-Dibromo-3-chloropropane 54U 54 13
124-48-1 Dibromochloromethane 110U 110 16
106-93-4 1,2-Dibromoethane 54U 54 8.2
74-95-3 Dibromomethane 270U 270 6.3
*110-57-6 trans-1,4-Dichloro-2-butene 54U 54 4.8
95-50-1 1,2-Dichlorobenzene 110U 110 5.6
541-73-1 1,3-Dichlorobenzene 110U 110 6.0
106-46-7 1,4-Dichlorobenzene 110U 110 7.3
*75-71-8 Dichlorodifluoromethane 270U 270 8.3
75-34-3 1,1-Dichloroethane 54U 54 5.4
107-06-2 1,2-Dichloroethane 54U 54 5.8
75-35-4 1,1-Dichloroethene 54U 54 8.2
156-59-2 cis-1,2-Dichloroethene 54U 54 6.8
Continued on next page
*See Statement of Data Qualifications
Page 170 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12D Sampled: 10/12/11 16:15Lab Sample ID: 1110319-43 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
156-60-5 trans-1,2-Dichloroethene 54U 54 5.9
78-87-5 1,2-Dichloropropane 54U 54 7.0
10061-01-5 cis-1,3-Dichloropropene 54U 54 8.9
10061-02-6 trans-1,3-Dichloropropene 54U 54 6.1
100-41-4 Ethylbenzene 54U 54 7.4
60-29-7 Ethyl Ether 220U 220 10
591-78-6 2-Hexanone 2700U 2700 18
74-88-4 Iodomethane 110 110 8.7
98-82-8 Isopropylbenzene 270U 270 8.0
108-20-3 Isopropyl Ether 270U 270 2.1
99-87-6 4-Isopropyltoluene 110U 110 7.4
*1634-04-4 Methyl tert-Butyl Ether 270U 270 7.2
*75-09-2 Methylene Chloride 77J 110 6.3
78-93-3 2-Butanone (MEK) 820U 820 28
*91-57-6 2-Methylnaphthalene 310J 360 8.3
108-10-1 4-Methyl-2-pentanone (MIBK) 2700U 2700 6.4
*91-20-3 Naphthalene 190J 360 7.4
994-05-8 tert-Amyl Methyl Ether 270U 270 2.6
637-92-3 Ethyl tert-Butyl Ether 270U 270 3.8
103-65-1 n-Propylbenzene 110U 110 6.2
100-42-5 Styrene 54U 54 5.7
75-65-0 t-Butanol 2700U 2700 140
*630-20-6 1,1,1,2-Tetrachloroethane 110U 110 17
79-34-5 1,1,2,2-Tetrachloroethane 54U 54 12
127-18-4 Tetrachloroethene 54U 54 5.6
109-99-9 Tetrahydrofuran 1100U 1100 36
108-88-3 Toluene 40J 110 7.8
87-61-6 1,2,3-Trichlorobenzene 360U 360 6.5
120-82-1 1,2,4-Trichlorobenzene 360U 360 7.1
71-55-6 1,1,1-Trichloroethane 54U 54 6.3
79-00-5 1,1,2-Trichloroethane 54U 54 7.3
Continued on next page
*See Statement of Data Qualifications
Page 171 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12D Sampled: 10/12/11 16:15Lab Sample ID: 1110319-43 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00Unit: ug/kg dry Prepared: 10/19/11 By: JDMDilution Factor: 1 Analyzed: 10/19/11 By: JDMQC Batch: 1111494 Analytical Batch: 1J20052Percent Solids: 81
Volatile Organic Compounds by EPA Method 8260B (Continued)
AnalyticalCAS Number Analyte Result RL MDL
79-01-6 Trichloroethene 54U 54 6.2
75-69-4 Trichlorofluoromethane 110U 110 8.1
96-18-4 1,2,3-Trichloropropane 110U 110 45
*526-73-8 1,2,3-Trimethylbenzene 25J 270 6.3
95-63-6 1,2,4-Trimethylbenzene 36J 110 6.2
108-67-8 1,3,5-Trimethylbenzene 110U 110 6.3
75-01-4 Vinyl Chloride 44U 44 7.3
179601-23-1 Xylene, Meta + Para 63J 110 11
95-47-6 Xylene, Ortho 43J 54 7.6
Surrogates: % Recovery Control Limits
Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 97 90-1074-Bromofluorobenzene 99 84-110
*See Statement of Data Qualifications
Page 172 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
ANALYTICAL REPORT
Client: MDNRE Work Order: 1110319Project: C&H Lake Linden Ops Description: Laboratory ServicesClient Sample ID: SS-12D Sampled: 10/12/11 16:15Lab Sample ID: 1110319-43 Sampled By: J. SpielbergMatrix: Soil Received: 10/17/11 17:00
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
Analytical Dilution Date Time QC Analyte Result RL MDL Unit Factor Method Analyzed By Batch
Percent Solids 81 0.1 0.1 % 1 USEPA-3550B 10/20/11 13:30 CLB 1111478
Page 173 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260BSample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111418 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank Analyzed: 10/18/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J19045
Acetone 100 J -- 1000 89Acrylonitrile 100 U 100 20Benzene 50 U 50 6.0Bromobenzene 100 U 100 5.6Bromochloromethane 100 U 100 6.0Bromodichloromethane 100 U 100 5.1Bromoform 100 U 100 7.6Bromomethane 200 U 200 12n-Butylbenzene 50 U -- 50 5.2sec-Butylbenzene 50 U 50 5.2tert-Butylbenzene 50 U 50 5.6Carbon Disulfide 250 U 250 5.1Carbon Tetrachloride 50 U 50 5.0Chlorobenzene 50 U 50 11Chloroethane 250 U 250 11Chloroform 50 U 50 5.7Chloromethane 250 U 250 6.7Cyclohexane 250 U 250 6.61,2-Dibromo-3-chloropropane 50 U 50 12Dibromochloromethane 100 U 100 151,2-Dibromoethane 50 U 50 7.5Dibromomethane 250 U 250 5.8trans-1,4-Dichloro-2-butene 50 U 50 4.41,2-Dichlorobenzene 100 U 100 5.11,3-Dichlorobenzene 100 U 100 5.51,4-Dichlorobenzene 100 U 100 6.7Dichlorodifluoromethane 250 U 250 7.61,1-Dichloroethane 50 U 50 5.01,2-Dichloroethane 50 U 50 5.31,1-Dichloroethene 50 U 50 7.5cis-1,2-Dichloroethene 50 U 50 6.2trans-1,2-Dichloroethene 50 U 50 5.41,2-Dichloropropane 50 U 50 6.4cis-1,3-Dichloropropene 50 U 50 8.2trans-1,3-Dichloropropene 50 U 50 5.6Ethylbenzene 50 U 50 6.8
Continued on next page
Page 174 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111418 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/18/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J19045
Ethyl Ether 200 U 200 9.42-Hexanone 2500 U 2500 16Iodomethane 20 J -- 100 8.0Isopropylbenzene 250 U 250 7.3Isopropyl Ether 250 U 250 1.94-Isopropyltoluene 100 U 100 6.8Methyl tert-Butyl Ether 250 U 250 6.6Methylene Chloride 100 U 100 5.82-Butanone (MEK) 750 U 750 252-Methylnaphthalene 330 U 330 7.64-Methyl-2-pentanone (MIBK) 2500 U 2500 5.9Naphthalene 140 J -- 330 6.8tert-Amyl Methyl Ether 250 U 250 2.4Ethyl tert-Butyl Ether 250 U 250 3.4n-Propylbenzene 100 U 100 5.7Styrene 50 U 50 5.2t-Butanol 2500 U 2500 1301,1,1,2-Tetrachloroethane 100 U 100 151,1,2,2-Tetrachloroethane 50 U 50 11Tetrachloroethene 50 U 50 5.1Tetrahydrofuran 1000 U 1000 33Toluene 100 U 100 7.21,2,3-Trichlorobenzene 330 U 330 6.01,2,4-Trichlorobenzene 330 U 330 6.51,1,1-Trichloroethane 50 U 50 5.81,1,2-Trichloroethane 50 U 50 6.7Trichloroethene 50 U 50 5.7Trichlorofluoromethane 100 U 100 7.41,2,3-Trichloropropane 100 U 100 411,2,3-Trimethylbenzene 250 U -- 250 5.81,2,4-Trimethylbenzene 100 U 100 5.71,3,5-Trimethylbenzene 100 U 100 5.8Vinyl Chloride 40 U 40 6.7Xylene, Meta + Para 100 U 100 10Xylene, Ortho 50 U 50 7.0
Method Blank Analyzed: 10/18/2011 By: JDMUnit: ug/L Analytical Batch: 1J19045
Surrogates:Dibromofluoromethane 102 76-108
Continued on next page
Page 175 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111418 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/18/2011 By: JDMUnit: ug/L Analytical Batch: 1J19045
Surrogates (Continued):1,2-Dichloroethane-d4 102 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 97 84-110
Laboratory Control Sample Analyzed: 10/18/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J19045
Benzene 2000 1960 98 85-120 -- 20 50 6.0Chlorobenzene 2000 1950 97 85-113 -- 20 50 111,1-Dichloroethene 2000 2010 101 72-131 -- 20 50 7.5Toluene 2000 1940 97 81-122 -- 20 100 7.2Trichloroethene 2000 1960 98 79-128 -- 20 50 5.7
Laboratory Control Sample Analyzed: 10/18/2011 By: JDMUnit: ug/L Analytical Batch: 1J19045
Surrogates:Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 100 84-110
Matrix Spike 1110319-14 SS-13 Analyzed: 10/19/2011 By: JDMUnit: ug/kg dry Analytical Batch: 1J19045
Benzene 36.8 J 2070 2080 99 83-116 -- 11 54 6.5Chlorobenzene 54 U 2070 2010 97 89-107 -- 16 54 121,1-Dichloroethene 54 U 2070 1960 95 75-118 -- 20 54 8.1Toluene 577 2070 2650 100 82-118 -- 11 110 7.8Trichloroethene 54 U 2070 2150 104 79-121 -- 14 54 6.1
Matrix Spike 1110319-14 SS-13 Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J19045
Surrogates:Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 100 90-1074-Bromofluorobenzene 101 84-110
Matrix Spike Duplicate 1110319-14 SS-13 Analyzed: 10/19/2011 By: JDMUnit: ug/kg dry Analytical Batch: 1J19045
Benzene 36.8 J 2070 2110 100 83-116 2 11 54 6.5
Continued on next page
Page 176 of 199
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111418 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Matrix Spike Duplicate (Continued) 1110319-14 SS-13 Analyzed: 10/19/2011 By: JDMUnit: ug/kg dry Analytical Batch: 1J19045
Chlorobenzene 54 U 2070 2040 98 89-107 1 16 54 121,1-Dichloroethene 54 U 2070 2020 98 75-118 3 20 54 8.1Toluene 577 2070 2690 102 82-118 2 11 110 7.8Trichloroethene 54 U 2070 2200 106 79-121 2 14 54 6.1
Matrix Spike Duplicate 1110319-14 SS-13 Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J19045
Surrogates:Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 101 90-1074-Bromofluorobenzene 101 84-110
QC Batch: 1111481 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20035
Acetone 1000 U 1000 89Acrylonitrile 100 U 100 20Benzene 50 U 50 6.0Bromobenzene 100 U 100 5.6Bromochloromethane 100 U 100 6.0Bromodichloromethane 100 U 100 5.1Bromoform 100 U 100 7.6Bromomethane 46 J -- 200 12n-Butylbenzene 50 U -- 50 5.2sec-Butylbenzene 50 U 50 5.2tert-Butylbenzene 50 U 50 5.6Carbon Disulfide 250 U 250 5.1Carbon Tetrachloride 50 U 50 5.0Chlorobenzene 50 U 50 11Chloroethane 250 U 250 11Chloroform 50 U 50 5.7Chloromethane 250 U 250 6.7Cyclohexane 250 U 250 6.61,2-Dibromo-3-chloropropane 50 U 50 12Dibromochloromethane 100 U 100 15
Continued on next page
Page 177 of 199
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111481 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20035
1,2-Dibromoethane 50 U 50 7.5Dibromomethane 250 U 250 5.8trans-1,4-Dichloro-2-butene 50 U 50 4.41,2-Dichlorobenzene 100 U 100 5.11,3-Dichlorobenzene 100 U 100 5.51,4-Dichlorobenzene 100 U 100 6.7Dichlorodifluoromethane 250 U 250 7.61,1-Dichloroethane 50 U 50 5.01,2-Dichloroethane 50 U 50 5.31,1-Dichloroethene 50 U 50 7.5cis-1,2-Dichloroethene 50 U 50 6.2trans-1,2-Dichloroethene 50 U 50 5.41,2-Dichloropropane 50 U 50 6.4cis-1,3-Dichloropropene 50 U 50 8.2trans-1,3-Dichloropropene 50 U 50 5.6Ethylbenzene 50 U 50 6.8Ethyl Ether 200 U 200 9.42-Hexanone 2500 U 2500 16Iodomethane 61 J -- 100 8.0Isopropylbenzene 250 U 250 7.3Isopropyl Ether 250 U 250 1.94-Isopropyltoluene 100 U 100 6.8Methyl tert-Butyl Ether 250 U 250 6.6Methylene Chloride 100 U 100 5.82-Butanone (MEK) 750 U 750 252-Methylnaphthalene 330 U 330 7.64-Methyl-2-pentanone (MIBK) 2500 U 2500 5.9Naphthalene 130 J -- 330 6.8tert-Amyl Methyl Ether 250 U 250 2.4Ethyl tert-Butyl Ether 250 U 250 3.4n-Propylbenzene 100 U 100 5.7Styrene 50 U 50 5.2t-Butanol 2500 U 2500 1301,1,1,2-Tetrachloroethane 100 U 100 151,1,2,2-Tetrachloroethane 50 U 50 11Tetrachloroethene 50 U 50 5.1
Continued on next page
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111481 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20035
Tetrahydrofuran 1000 U 1000 33Toluene 100 U 100 7.21,2,3-Trichlorobenzene 330 U 330 6.01,2,4-Trichlorobenzene 330 U 330 6.51,1,1-Trichloroethane 50 U 50 5.81,1,2-Trichloroethane 50 U 50 6.7Trichloroethene 50 U 50 5.7Trichlorofluoromethane 100 U 100 7.41,2,3-Trichloropropane 100 U 100 411,2,3-Trimethylbenzene 6.0 J -- 250 5.81,2,4-Trimethylbenzene 100 U 100 5.71,3,5-Trimethylbenzene 100 U 100 5.8Vinyl Chloride 40 U 40 6.7Xylene, Meta + Para 100 U 100 10Xylene, Ortho 50 U 50 7.0
Method Blank Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20035
Surrogates:Dibromofluoromethane 100 76-1081,2-Dichloroethane-d4 99 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 98 84-110
Laboratory Control Sample Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20035
Benzene 2000 2130 106 85-120 -- 20 50 6.0Chlorobenzene 2000 2120 106 85-113 -- 20 50 111,1-Dichloroethene 2000 2190 109 72-131 -- 20 50 7.5Toluene 2000 2100 105 81-122 -- 20 100 7.2Trichloroethene 2000 2100 105 79-128 -- 20 50 5.7
Laboratory Control Sample Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20035
Surrogates:Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115
Continued on next page
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This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111481 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Laboratory Control Sample (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20035
Surrogates (Continued):Toluene-d8 100 90-1074-Bromofluorobenzene 101 84-110
Matrix Spike 1110319-41 SD-04 Analyzed: 10/19/2011 By: JDMUnit: ug/kg dry Analytical Batch: 1J20035
Benzene 71.6 J 8950 9330 103 83-116 -- 11 220 27Chlorobenzene 51.5 J 8950 9290 103 89-107 -- 16 220 511,1-Dichloroethene 220 U 8950 9050 101 75-118 -- 20 220 34Toluene 82.8 J 8950 9190 102 82-118 -- 11 450 32Trichloroethene 89.5 J 8950 9270 103 79-121 -- 14 220 26
Matrix Spike 1110319-41 SD-04 Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20035
Surrogates:Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 101 84-110
Matrix Spike Duplicate 1110319-41 SD-04 Analyzed: 10/19/2011 By: JDMUnit: ug/kg dry Analytical Batch: 1J20035
Benzene 71.6 J 8950 9290 103 83-116 0.4 11 220 27Chlorobenzene 51.5 J 8950 9250 103 89-107 0.5 16 220 511,1-Dichloroethene 220 U 8950 9040 101 75-118 0.1 20 220 34Toluene 82.8 J 8950 9170 101 82-118 0.3 11 450 32Trichloroethene 89.5 J 8950 9120 101 79-121 2 14 220 26
Matrix Spike Duplicate 1110319-41 SD-04 Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20035
Surrogates:Dibromofluoromethane 104 76-1081,2-Dichloroethane-d4 100 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 101 84-110
QC Batch: 1111494 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20052
Acetone 100 J -- 1000 89
Continued on next page
Page 180 of 199
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111494 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20052
Acrylonitrile 100 U 100 20Benzene 50 U 50 6.0Bromobenzene 100 U 100 5.6Bromochloromethane 100 U 100 6.0Bromodichloromethane 100 U 100 5.1Bromoform 100 U 100 7.6Bromomethane 200 U 200 12n-Butylbenzene 50 U 50 5.2sec-Butylbenzene 50 U 50 5.2tert-Butylbenzene 50 U 50 5.6Carbon Disulfide 250 U 250 5.1Carbon Tetrachloride 50 U 50 5.0Chlorobenzene 50 U 50 11Chloroethane 250 U 250 11Chloroform 50 U 50 5.7Chloromethane 250 U 250 6.7Cyclohexane 250 U 250 6.61,2-Dibromo-3-chloropropane 50 U 50 12Dibromochloromethane 100 U 100 151,2-Dibromoethane 50 U 50 7.5Dibromomethane 250 U 250 5.8trans-1,4-Dichloro-2-butene 50 U 50 4.41,2-Dichlorobenzene 100 U 100 5.11,3-Dichlorobenzene 100 U 100 5.51,4-Dichlorobenzene 100 U 100 6.7Dichlorodifluoromethane 250 U 250 7.61,1-Dichloroethane 50 U 50 5.01,2-Dichloroethane 50 U 50 5.31,1-Dichloroethene 50 U 50 7.5cis-1,2-Dichloroethene 50 U 50 6.2trans-1,2-Dichloroethene 50 U 50 5.41,2-Dichloropropane 50 U 50 6.4cis-1,3-Dichloropropene 50 U 50 8.2trans-1,3-Dichloropropene 50 U 50 5.6Ethylbenzene 50 U 50 6.8Ethyl Ether 200 U 200 9.4
Continued on next page
Page 181 of 199
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111494 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20052
2-Hexanone 2500 U 2500 16Iodomethane 100 U 100 8.0Isopropylbenzene 250 U 250 7.3Isopropyl Ether 250 U 250 1.94-Isopropyltoluene 100 U 100 6.8Methyl tert-Butyl Ether 250 U 250 6.6Methylene Chloride 24 J -- 100 5.82-Butanone (MEK) 750 U 750 252-Methylnaphthalene 330 U 330 7.64-Methyl-2-pentanone (MIBK) 2500 U 2500 5.9Naphthalene 130 J -- 330 6.8tert-Amyl Methyl Ether 250 U 250 2.4Ethyl tert-Butyl Ether 250 U 250 3.4n-Propylbenzene 100 U 100 5.7Styrene 50 U 50 5.2t-Butanol 2500 U 2500 1301,1,1,2-Tetrachloroethane 100 U 100 151,1,2,2-Tetrachloroethane 50 U 50 11Tetrachloroethene 50 U 50 5.1Tetrahydrofuran 1000 U 1000 33Toluene 100 U 100 7.21,2,3-Trichlorobenzene 330 U 330 6.01,2,4-Trichlorobenzene 330 U 330 6.51,1,1-Trichloroethane 50 U 50 5.81,1,2-Trichloroethane 50 U 50 6.7Trichloroethene 50 U 50 5.7Trichlorofluoromethane 100 U 100 7.41,2,3-Trichloropropane 100 U 100 411,2,3-Trimethylbenzene 6.0 J -- 250 5.81,2,4-Trimethylbenzene 100 U 100 5.71,3,5-Trimethylbenzene 100 U 100 5.8Vinyl Chloride 40 U 40 6.7Xylene, Meta + Para 100 U 100 10Xylene, Ortho 50 U 50 7.0
Method Blank Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20052
Surrogates:Dibromofluoromethane 103 76-108
Continued on next page
Page 182 of 199
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QUALITY CONTROL REPORT
Volatile Organic Compounds by EPA Method 8260B (Continued)Sample Spike Spike Control RPD
Analyte Conc. Qty. Result % Rec. Limits RPD Limits RL MDL
QC Batch: 1111494 (Continued) 5035A High Concentration (MeOH) - MS/USEPA-8260B
Method Blank (Continued) Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20052
Surrogates (Continued):1,2-Dichloroethane-d4 101 84-115Toluene-d8 98 90-1074-Bromofluorobenzene 98 84-110
Laboratory Control Sample Analyzed: 10/19/2011 By: JDMUnit: ug/kg wet Analytical Batch: 1J20052
Benzene 2000 1960 98 85-120 -- 20 50 6.0Chlorobenzene 2000 1950 97 85-113 -- 20 50 111,1-Dichloroethene 2000 1960 98 72-131 -- 20 50 7.5Toluene 2000 2000 100 81-122 -- 20 100 7.2Trichloroethene 2000 1980 99 79-128 -- 20 50 5.7
Laboratory Control Sample Analyzed: 10/19/2011 By: JDMUnit: ug/L Analytical Batch: 1J20052
Surrogates:Dibromofluoromethane 103 76-1081,2-Dichloroethane-d4 101 84-115Toluene-d8 99 90-1074-Bromofluorobenzene 101 84-110
Page 183 of 199
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QUALITY CONTROL REPORT
Physical/Chemical Parameters by EPA/APHA/ASTM Methods
RL MDLSample Spike Spike Control RPD
QC Type Conc. Qty. Result Unit % Rec. Limits RPD Limits
Analyte: Percent Solids/USEPA-3550B
QC Batch: 1111475 (Method-Specific Preparation) Analyzed: 10/20/2011 By: CLB
Method Blank 0.1 U % 0.1
QC Batch: 1111477 (Method-Specific Preparation) Analyzed: 10/20/2011 By: CLB
Method Blank 0.1 U % 0.1
QC Batch: 1111478 (Method-Specific Preparation) Analyzed: 10/20/2011 By: CLB
Method Blank 0.1 U % 0.1
Page 184 of 199
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STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B
Qualification: The corresponding CCV for this analytical batch had a recovery exceeding the upper control limit of the method. A positive result for this analyte in any associated samples are considered estimated. Non-detectable results are not qualified.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-01 SS-01 1,2,3-Trimethylbenzene1110319-01 SS-01 Chloroethane1110319-01 SS-01 Dichlorodifluoromethane1110319-01 SS-01 Ethyl tert-Butyl Ether1110319-01 SS-01 Isopropyl Ether1110319-01 SS-01 t-Butanol1110319-01 SS-01 tert-Amyl Methyl Ether1110319-02 SS-02 1,2,3-Trimethylbenzene1110319-02 SS-02 Chloroethane1110319-02 SS-02 Dichlorodifluoromethane1110319-02 SS-02 Ethyl tert-Butyl Ether1110319-02 SS-02 Isopropyl Ether1110319-02 SS-02 t-Butanol1110319-02 SS-02 tert-Amyl Methyl Ether1110319-03 SS-02D 1,2,3-Trimethylbenzene1110319-03 SS-02D Chloroethane1110319-03 SS-02D Dichlorodifluoromethane1110319-03 SS-02D Ethyl tert-Butyl Ether1110319-03 SS-02D Isopropyl Ether1110319-03 SS-02D t-Butanol1110319-03 SS-02D tert-Amyl Methyl Ether1110319-04 SS-03 1,2,3-Trimethylbenzene1110319-04 SS-03 Chloroethane1110319-04 SS-03 Dichlorodifluoromethane1110319-04 SS-03 Ethyl tert-Butyl Ether1110319-04 SS-03 Isopropyl Ether1110319-04 SS-03 t-Butanol1110319-04 SS-03 tert-Amyl Methyl Ether1110319-05 SS-04 1,2,3-Trimethylbenzene1110319-05 SS-04 Chloroethane1110319-05 SS-04 Dichlorodifluoromethane1110319-05 SS-04 Ethyl tert-Butyl Ether1110319-05 SS-04 Isopropyl Ether1110319-05 SS-04 t-Butanol1110319-05 SS-04 tert-Amyl Methyl Ether1110319-06 SS-05 1,2,3-Trimethylbenzene1110319-06 SS-05 Chloroethane1110319-06 SS-05 Dichlorodifluoromethane1110319-06 SS-05 Ethyl tert-Butyl Ether1110319-06 SS-05 Isopropyl Ether1110319-06 SS-05 t-Butanol1110319-06 SS-05 tert-Amyl Methyl Ether1110319-07 SS-06 1,2,3-Trimethylbenzene1110319-07 SS-06 Chloroethane1110319-07 SS-06 Dichlorodifluoromethane1110319-07 SS-06 Ethyl tert-Butyl Ether1110319-07 SS-06 Isopropyl Ether1110319-07 SS-06 t-Butanol
Page 185 of 199
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STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The corresponding CCV for this analytical batch had a recovery exceeding the upper control limit of the method. A positive result for this analyte in any associated samples are considered estimated. Non-detectable results are not qualified.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-07 SS-06 tert-Amyl Methyl Ether1110319-08 SS-07 1,2,3-Trimethylbenzene1110319-08 SS-07 Chloroethane1110319-08 SS-07 Dichlorodifluoromethane1110319-08 SS-07 Ethyl tert-Butyl Ether1110319-08 SS-07 Isopropyl Ether1110319-08 SS-07 t-Butanol1110319-08 SS-07 tert-Amyl Methyl Ether1110319-09 SS-08 1,2,3-Trimethylbenzene1110319-09 SS-08 Chloroethane1110319-09 SS-08 Dichlorodifluoromethane1110319-09 SS-08 Ethyl tert-Butyl Ether1110319-09 SS-08 Isopropyl Ether1110319-09 SS-08 t-Butanol1110319-09 SS-08 tert-Amyl Methyl Ether1110319-10 SS-09 1,2,3-Trimethylbenzene1110319-10 SS-09 Chloroethane1110319-10 SS-09 Dichlorodifluoromethane1110319-10 SS-09 Ethyl tert-Butyl Ether1110319-10 SS-09 Isopropyl Ether1110319-10 SS-09 t-Butanol1110319-10 SS-09 tert-Amyl Methyl Ether1110319-11 SS-10 1,2,3-Trimethylbenzene1110319-11 SS-10 Chloroethane1110319-11 SS-10 Dichlorodifluoromethane1110319-11 SS-10 Ethyl tert-Butyl Ether1110319-11 SS-10 Isopropyl Ether1110319-11 SS-10 t-Butanol1110319-11 SS-10 tert-Amyl Methyl Ether1110319-12 SS-11 1,2,3-Trimethylbenzene1110319-12 SS-11 Chloroethane1110319-12 SS-11 Dichlorodifluoromethane1110319-12 SS-11 Ethyl tert-Butyl Ether1110319-12 SS-11 Isopropyl Ether1110319-12 SS-11 t-Butanol1110319-12 SS-11 tert-Amyl Methyl Ether1110319-13 SS-12 1,2,3-Trimethylbenzene1110319-13 SS-12 Chloroethane1110319-13 SS-12 Dichlorodifluoromethane1110319-13 SS-12 Ethyl tert-Butyl Ether1110319-13 SS-12 Isopropyl Ether1110319-13 SS-12 t-Butanol1110319-13 SS-12 tert-Amyl Methyl Ether1110319-14 SS-13 1,2,3-Trimethylbenzene1110319-14 SS-13 Chloroethane1110319-14 SS-13 Dichlorodifluoromethane1110319-14 SS-13 Ethyl tert-Butyl Ether1110319-14 SS-13 Isopropyl Ether
Page 186 of 199
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STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The corresponding CCV for this analytical batch had a recovery exceeding the upper control limit of the method. A positive result for this analyte in any associated samples are considered estimated. Non-detectable results are not qualified.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-14 SS-13 t-Butanol1110319-14 SS-13 tert-Amyl Methyl Ether1110319-15 SS-14 1,2,3-Trimethylbenzene1110319-15 SS-14 Chloroethane1110319-15 SS-14 Dichlorodifluoromethane1110319-15 SS-14 Ethyl tert-Butyl Ether1110319-15 SS-14 Isopropyl Ether1110319-15 SS-14 t-Butanol1110319-15 SS-14 tert-Amyl Methyl Ether1110319-16 SS-15 1,2,3-Trimethylbenzene1110319-16 SS-15 Chloroethane1110319-16 SS-15 Dichlorodifluoromethane1110319-16 SS-15 Ethyl tert-Butyl Ether1110319-16 SS-15 Isopropyl Ether1110319-16 SS-15 t-Butanol1110319-16 SS-15 tert-Amyl Methyl Ether1110319-17 SS-16 1,2,3-Trimethylbenzene1110319-17 SS-16 Chloroethane1110319-17 SS-16 Dichlorodifluoromethane1110319-17 SS-16 Ethyl tert-Butyl Ether1110319-17 SS-16 Isopropyl Ether1110319-17 SS-16 t-Butanol1110319-17 SS-16 tert-Amyl Methyl Ether1110319-18 SS-17 1,2,3-Trimethylbenzene1110319-18 SS-17 Chloroethane1110319-18 SS-17 Dichlorodifluoromethane1110319-18 SS-17 Ethyl tert-Butyl Ether1110319-18 SS-17 Isopropyl Ether1110319-18 SS-17 t-Butanol1110319-18 SS-17 tert-Amyl Methyl Ether1110319-19 SS-18 1,2,3-Trimethylbenzene1110319-19 SS-18 Chloroethane1110319-19 SS-18 Dichlorodifluoromethane1110319-19 SS-18 Ethyl tert-Butyl Ether1110319-19 SS-18 Isopropyl Ether1110319-19 SS-18 t-Butanol1110319-19 SS-18 tert-Amyl Methyl Ether1110319-20 SS-19 1,2,3-Trimethylbenzene1110319-20 SS-19 Chloroethane1110319-20 SS-19 Dichlorodifluoromethane1110319-20 SS-19 Ethyl tert-Butyl Ether1110319-20 SS-19 Isopropyl Ether1110319-20 SS-19 t-Butanol1110319-20 SS-19 tert-Amyl Methyl Ether1110319-40 SD-03D Dichlorodifluoromethane1110319-42 SD-05 Dichlorodifluoromethane1110319-43 SS-12D Dichlorodifluoromethane
Page 187 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The corresponding CCV for this analytical batch had a recovery below the lower control limit of the method. Positive results for this analyte in any associated samples are considered estimated; non-detectable results are considered approximate.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-01 SS-01 1,2,3-Trichlorobenzene1110319-01 SS-01 2-Methylnaphthalene1110319-01 SS-01 Naphthalene1110319-02 SS-02 1,2,3-Trichlorobenzene1110319-02 SS-02 2-Methylnaphthalene1110319-02 SS-02 Naphthalene1110319-03 SS-02D 1,2,3-Trichlorobenzene1110319-03 SS-02D 2-Methylnaphthalene1110319-03 SS-02D Naphthalene1110319-04 SS-03 1,2,3-Trichlorobenzene1110319-04 SS-03 2-Methylnaphthalene1110319-04 SS-03 Naphthalene1110319-05 SS-04 1,2,3-Trichlorobenzene1110319-05 SS-04 2-Methylnaphthalene1110319-05 SS-04 Naphthalene1110319-06 SS-05 1,2,3-Trichlorobenzene1110319-06 SS-05 2-Methylnaphthalene1110319-06 SS-05 Naphthalene1110319-07 SS-06 1,2,3-Trichlorobenzene1110319-07 SS-06 2-Methylnaphthalene1110319-07 SS-06 Naphthalene1110319-08 SS-07 1,2,3-Trichlorobenzene1110319-08 SS-07 2-Methylnaphthalene1110319-08 SS-07 Naphthalene1110319-09 SS-08 1,2,3-Trichlorobenzene1110319-09 SS-08 2-Methylnaphthalene1110319-09 SS-08 Naphthalene1110319-10 SS-09 1,2,3-Trichlorobenzene1110319-10 SS-09 2-Methylnaphthalene1110319-10 SS-09 Naphthalene1110319-11 SS-10 1,2,3-Trichlorobenzene1110319-11 SS-10 2-Methylnaphthalene1110319-11 SS-10 Naphthalene1110319-12 SS-11 1,2,3-Trichlorobenzene1110319-12 SS-11 2-Methylnaphthalene1110319-12 SS-11 Naphthalene1110319-13 SS-12 1,2,3-Trichlorobenzene1110319-13 SS-12 2-Methylnaphthalene1110319-13 SS-12 Naphthalene1110319-14 SS-13 1,2,3-Trichlorobenzene1110319-14 SS-13 2-Methylnaphthalene1110319-14 SS-13 Naphthalene1110319-15 SS-14 1,2,3-Trichlorobenzene1110319-15 SS-14 2-Methylnaphthalene1110319-15 SS-14 Naphthalene1110319-16 SS-15 1,2,3-Trichlorobenzene1110319-16 SS-15 2-Methylnaphthalene
Page 188 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The corresponding CCV for this analytical batch had a recovery below the lower control limit of the method. Positive results for this analyte in any associated samples are considered estimated; non-detectable results are considered approximate.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-16 SS-15 Naphthalene1110319-17 SS-16 1,2,3-Trichlorobenzene1110319-17 SS-16 2-Methylnaphthalene1110319-17 SS-16 Naphthalene1110319-18 SS-17 1,2,3-Trichlorobenzene1110319-18 SS-17 2-Methylnaphthalene1110319-18 SS-17 Naphthalene1110319-19 SS-18 1,2,3-Trichlorobenzene1110319-19 SS-18 2-Methylnaphthalene1110319-19 SS-18 Naphthalene1110319-20 SS-19 1,2,3-Trichlorobenzene1110319-20 SS-19 2-Methylnaphthalene1110319-20 SS-19 Naphthalene1110319-21 SS-20 1,2-Dibromo-3-chloropropane1110319-21 SS-20 Naphthalene1110319-21 SS-20 trans-1,4-Dichloro-2-butene1110319-22 SB-01 1,2-Dibromo-3-chloropropane1110319-22 SB-01 Naphthalene1110319-22 SB-01 trans-1,4-Dichloro-2-butene1110319-23 SB-02 1,2-Dibromo-3-chloropropane1110319-23 SB-02 Naphthalene1110319-23 SB-02 trans-1,4-Dichloro-2-butene1110319-24 SB-03 1,2-Dibromo-3-chloropropane1110319-24 SB-03 Naphthalene1110319-24 SB-03 trans-1,4-Dichloro-2-butene1110319-25 SB-04 1,2-Dibromo-3-chloropropane1110319-25 SB-04 Naphthalene1110319-25 SB-04 trans-1,4-Dichloro-2-butene1110319-26 SB-04D 1,2-Dibromo-3-chloropropane1110319-26 SB-04D Naphthalene1110319-26 SB-04D trans-1,4-Dichloro-2-butene1110319-27 SB-05 1,2-Dibromo-3-chloropropane1110319-27 SB-05 Naphthalene1110319-27 SB-05 trans-1,4-Dichloro-2-butene1110319-28 SB-06 1,2-Dibromo-3-chloropropane1110319-28 SB-06 Naphthalene1110319-28 SB-06 trans-1,4-Dichloro-2-butene1110319-29 SB-07 1,2-Dibromo-3-chloropropane1110319-29 SB-07 Naphthalene1110319-29 SB-07 trans-1,4-Dichloro-2-butene1110319-30 SB-08 1,2-Dibromo-3-chloropropane1110319-30 SB-08 Naphthalene1110319-30 SB-08 trans-1,4-Dichloro-2-butene1110319-31 SB-09 1,2-Dibromo-3-chloropropane1110319-31 SB-09 Naphthalene1110319-31 SB-09 trans-1,4-Dichloro-2-butene1110319-32 SB-10 1,2-Dibromo-3-chloropropane1110319-32 SB-10 Naphthalene
Page 189 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The corresponding CCV for this analytical batch had a recovery below the lower control limit of the method. Positive results for this analyte in any associated samples are considered estimated; non-detectable results are considered approximate.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-32 SB-10 trans-1,4-Dichloro-2-butene1110319-33 SB-11 1,2-Dibromo-3-chloropropane1110319-33 SB-11 Naphthalene1110319-33 SB-11 trans-1,4-Dichloro-2-butene1110319-34 SB-12 1,2-Dibromo-3-chloropropane1110319-34 SB-12 Naphthalene1110319-34 SB-12 trans-1,4-Dichloro-2-butene1110319-35 SB-13 1,2-Dibromo-3-chloropropane1110319-35 SB-13 Naphthalene1110319-35 SB-13 trans-1,4-Dichloro-2-butene1110319-36 SB-14 1,2-Dibromo-3-chloropropane1110319-36 SB-14 Naphthalene1110319-36 SB-14 trans-1,4-Dichloro-2-butene1110319-37 SD-01 1,2-Dibromo-3-chloropropane1110319-37 SD-01 Naphthalene1110319-37 SD-01 trans-1,4-Dichloro-2-butene1110319-38 SD-02 1,2-Dibromo-3-chloropropane1110319-38 SD-02 Naphthalene1110319-38 SD-02 trans-1,4-Dichloro-2-butene1110319-39 SD-03 1,2-Dibromo-3-chloropropane1110319-39 SD-03 Naphthalene1110319-39 SD-03 trans-1,4-Dichloro-2-butene1110319-40 SD-03D 1,1,1,2-Tetrachloroethane1110319-40 SD-03D 1,2-Dibromo-3-chloropropane1110319-40 SD-03D 2-Methylnaphthalene1110319-40 SD-03D Methyl tert-Butyl Ether1110319-40 SD-03D Naphthalene1110319-40 SD-03D trans-1,4-Dichloro-2-butene1110319-41 SD-04 1,2-Dibromo-3-chloropropane1110319-41 SD-04 Naphthalene1110319-41 SD-04 trans-1,4-Dichloro-2-butene1110319-42 SD-05 1,1,1,2-Tetrachloroethane1110319-42 SD-05 1,2-Dibromo-3-chloropropane1110319-42 SD-05 2-Methylnaphthalene1110319-42 SD-05 Methyl tert-Butyl Ether1110319-42 SD-05 Naphthalene1110319-42 SD-05 trans-1,4-Dichloro-2-butene1110319-43 SS-12D 1,1,1,2-Tetrachloroethane1110319-43 SS-12D 1,2-Dibromo-3-chloropropane1110319-43 SS-12D 2-Methylnaphthalene1110319-43 SS-12D Methyl tert-Butyl Ether1110319-43 SS-12D Naphthalene1110319-43 SS-12D trans-1,4-Dichloro-2-butene
Qualification: The analyte concentration in the associated MB was greater than the MDL but less than the RL. The positive sample result, which was less than 5 times the MB value, is considered estimated.
Page 190 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The analyte concentration in the associated MB was greater than the MDL but less than the RL. The positive sample result, which was less than 5 times the MB value, is considered estimated.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-01 SS-01 Acetone1110319-01 SS-01 Naphthalene1110319-02 SS-02 Naphthalene1110319-03 SS-02D Acetone1110319-03 SS-02D Naphthalene1110319-04 SS-03 Acetone1110319-04 SS-03 Naphthalene1110319-05 SS-04 Acetone1110319-06 SS-05 Acetone1110319-07 SS-06 Acetone1110319-07 SS-06 Iodomethane1110319-08 SS-07 Acetone1110319-08 SS-07 Iodomethane1110319-08 SS-07 Naphthalene1110319-09 SS-08 Acetone1110319-09 SS-08 Iodomethane1110319-09 SS-08 Naphthalene1110319-10 SS-09 Acetone1110319-10 SS-09 Iodomethane1110319-10 SS-09 Naphthalene1110319-11 SS-10 Acetone1110319-11 SS-10 Iodomethane1110319-11 SS-10 Naphthalene1110319-12 SS-11 Acetone1110319-12 SS-11 Iodomethane1110319-12 SS-11 Naphthalene1110319-13 SS-12 Acetone1110319-13 SS-12 Iodomethane1110319-13 SS-12 Naphthalene1110319-14 SS-13 Acetone1110319-14 SS-13 Iodomethane1110319-15 SS-14 Acetone1110319-15 SS-14 Iodomethane1110319-16 SS-15 Acetone1110319-16 SS-15 Iodomethane1110319-16 SS-15 Naphthalene1110319-17 SS-16 Acetone1110319-17 SS-16 Iodomethane1110319-17 SS-16 Naphthalene1110319-18 SS-17 Acetone1110319-18 SS-17 Iodomethane1110319-18 SS-17 Naphthalene1110319-19 SS-18 Acetone1110319-19 SS-18 Iodomethane1110319-19 SS-18 Naphthalene1110319-20 SS-19 Acetone1110319-20 SS-19 Iodomethane1110319-20 SS-19 Naphthalene1110319-21 SS-20 1,2,3-Trimethylbenzene
Page 191 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The analyte concentration in the associated MB was greater than the MDL but less than the RL. The positive sample result, which was less than 5 times the MB value, is considered estimated.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-21 SS-20 Bromomethane1110319-21 SS-20 Iodomethane1110319-21 SS-20 Naphthalene1110319-22 SB-01 Bromomethane1110319-22 SB-01 Iodomethane1110319-22 SB-01 Naphthalene1110319-23 SB-02 Bromomethane1110319-23 SB-02 Iodomethane1110319-24 SB-03 Iodomethane1110319-25 SB-04 Bromomethane1110319-25 SB-04 Iodomethane1110319-25 SB-04 Naphthalene1110319-26 SB-04D Iodomethane1110319-26 SB-04D Naphthalene1110319-27 SB-05 Bromomethane1110319-27 SB-05 Iodomethane1110319-27 SB-05 Naphthalene1110319-28 SB-06 Bromomethane1110319-28 SB-06 Iodomethane1110319-28 SB-06 Naphthalene1110319-29 SB-07 Bromomethane1110319-29 SB-07 Iodomethane1110319-30 SB-08 Bromomethane1110319-30 SB-08 Iodomethane1110319-31 SB-09 Iodomethane1110319-32 SB-10 Iodomethane1110319-32 SB-10 Naphthalene1110319-33 SB-11 1,2,3-Trimethylbenzene1110319-33 SB-11 Iodomethane1110319-33 SB-11 Naphthalene1110319-34 SB-12 Iodomethane1110319-35 SB-13 1,2,3-Trimethylbenzene1110319-35 SB-13 Iodomethane1110319-35 SB-13 Naphthalene1110319-36 SB-14 Iodomethane1110319-37 SD-01 Bromomethane1110319-37 SD-01 Iodomethane1110319-38 SD-02 Iodomethane1110319-39 SD-03 Iodomethane1110319-40 SD-03D Methylene Chloride1110319-41 SD-04 Iodomethane1110319-41 SD-04 Naphthalene1110319-42 SD-05 Acetone1110319-42 SD-05 Methylene Chloride1110319-43 SS-12D 1,2,3-Trimethylbenzene1110319-43 SS-12D Acetone1110319-43 SS-12D Methylene Chloride1110319-43 SS-12D Naphthalene
Page 192 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
STATEMENT OF DATA QUALIFICATIONS
Volatile Organic Compounds by EPA Method 8260B (Continued)
Qualification: The analyte concentration in the associated MB was greater than the MDL but less than the RL. The positive sample result, which was greater than 5 times the MB value, is not considered estimated.
Analysis: USEPA-8260B
Sample/Analyte: 1110319-01 SS-01 Iodomethane1110319-02 SS-02 Iodomethane1110319-03 SS-02D Iodomethane1110319-04 SS-03 Iodomethane1110319-05 SS-04 Iodomethane1110319-06 SS-05 Iodomethane1110319-14 SS-13 Naphthalene1110319-15 SS-14 Naphthalene
Page 193 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
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Page 194 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
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I8YISion: 3.0
Page 199 of 199
This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc.Individual sample results relate only to the sample tested.
5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com
MICHIGAN DEPARTMENT OF NATURAL RESOURCES AND ENVIRONMENT
ENVIRONMENTAL LABORATORYP.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Division: RD
Report to: SCOTT CORNELIUS Lab Work Order # : 11000149
MDEQ-RD-LANSING Work Site ID : 45371900
CONSTITUTION HALL Site Name : LAKE LINDEN/TORCH LAKE
525 W. ALLEGAN, LANSING, MI 48909 Received: 10/18/2011
Reported: 11/22/2011
Total: $1,059.00 Collected By: BARB VETORT
Samples Received :
No: Sample ID Sample Description Matrix: Collection Date
01 AB85336 MW 03 WATER 10/12/2011
02 AB85337 MW 05 WATER 10/12/2011
03 AB85338 MW 08 WATER 10/12/2011
04 AB85339 MW 09 WATER 10/12/2011
05 AB85340 MW 10 WATER 10/12/2011
06 AB85341 MW 11 WATER 10/12/2011
07 AB85342 MW 12 WATER 10/13/2011
AB85337 Sample was preserved with HCL.
I certify that the analysis performed by the MDEQ Environmental Laboratory are accurate and that the laboratory
tests were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate
regulatory agencies.
George L. Krisztian,
Laboratory Director
Lab Work Order #: 11000149 Page 1 of 5
MICHIGAN DEPARTMENT OF NATURAL RESOURCES AND ENVIRONMENT
ENVIRONMENTAL LABORATORYP.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB85336 MW 03
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 30 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen 2.7 mg N/L 0.10 D 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus .52 mg P/L 0.010 D 11/02/2011 365.4 LAV
7664-41-7 Ammonia 2.1 mg N/L 0.1 D 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite ND mg N/L 0.1 K 10/24/2011 353.2 MB
7440-44-0 TOC 12 mg/L 0.5 10/31/2011 5310C SM LAV
Sample Number: AB85337 MW 05
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 6.1 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen .50 mg N/L 0.10 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus .063 mg P/L 0.010 11/02/2011 365.4 LAV
7664-41-7 Ammonia .18 mg N/L 0.1 I , P 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite ND mg N/L 0.1 K , P 10/24/2011 353.2 MB
7440-44-0 TOC 3.1 mg/L 0.5 10/31/2011 5310C SM LAV
Sample Number: AB85338 MW 08
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 15 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen 24 mg N/L 0.10 D 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus .29 mg P/L 0.010 D 11/02/2011 365.4 LAV
7664-41-7 Ammonia 23 mg N/L 1.0 D 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite ND mg N/L 0.1 K 10/24/2011 353.2 MB
7440-44-0 TOC 6.7 mg/L 0.5 10/31/2011 5310C SM LAV
Sample Number: AB85339 MW 09
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 15 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen 32 mg N/L 0.10 D 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus .14 mg P/L 0.010 D 11/02/2011 365.4 LAV
7664-41-7 Ammonia 28 mg N/L 1.0 D 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite 2.9 mg N/L 0.1 D 10/24/2011 353.2 MB
7440-44-0 TOC 6.0 mg/L 0.5 10/31/2011 5310C SM LAV
CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts
RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane
ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian
Lab Work Order #: 11000149 Page 2 of 5
MICHIGAN DEPARTMENT OF NATURAL RESOURCES AND ENVIRONMENT
ENVIRONMENTAL LABORATORYP.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB85340 MW 10
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 13 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen .30 mg N/L 0.10 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus 0.13 mg P/L 0.010 11/02/2011 365.4 LAV
7664-41-7 Ammonia .09 mg N/L 0.01 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite ND mg N/L 0.1 K 10/24/2011 353.2 MB
7440-44-0 TOC 4.2 mg/L 0.5 10/31/2011 5310C SM LAV
Sample Number: AB85341 MW 11
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 18 mg/L 5 11/01/2011 410.4 LAV
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen .55 mg N/L 0.10 11/02/2011 351.2 LAV
7723-14-0 Total Phosphorus .25 mg P/L 0.010 11/02/2011 365.4 LAV
7664-41-7 Ammonia ND mg N/L 0.01 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite .48 mg N/L 0.01 10/24/2011 353.2 MB
7440-44-0 TOC 6.9 mg/L 0.5 10/31/2011 5310C SM LAV
CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts
RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane
ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian
Lab Work Order #: 11000149 Page 3 of 5
MICHIGAN DEPARTMENT OF NATURAL RESOURCES AND ENVIRONMENT
ENVIRONMENTAL LABORATORYP.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB85342 MW 12
CAS# Analyte Name Result Unit RL Qualifier Date Tested Method Analyst
COD 14 mg/L 5 11/01/2011 410.4 LAV
Digestion Metals Water Completed 10/26/2011 3010/200 JW
Digestion Mercury Water Completed 10/27/2011 7470/245.1 TB
7439-97-6 Mercury - Total ND µg/L 0.2 10/28/2011 7470/245.1 TS
KN TP - Digestion Completed 11/02/2011 351.2 LAV
TKN Total Kjeldahl Nitrogen 27 mg N/L 0.10 11/09/2011 351.2 LAV
7723-14-0 Total Phosphorus .44 mg P/L 0.010 D 11/02/2011 365.4 LAV
7429-90-5 Aluminium - Total 8500 µg/L 50 D 11/14/2011 6020/200.8 KS
7440-36-0 Antimony - Total 1.1 µg/L 1 11/11/2011 6020/200.8 KS
7440-38-2 Arsenic - Total 220 µg/L 1 11/11/2011 6020/200.8 KS
7440-39-3 Barium - Total 26000 µg/L 5 D 11/14/2011 6020/200.8 KS
7440-41-7 Beryllium - Total ND µg/L 1 11/11/2011 6020/200.8 KS
7440-43-9 Cadmium - Total ND µg/L 0.2 11/09/2011 6020/200.8 KS
7440-47-3 Chromium - Total 9.2 µg/L 1 11/11/2011 6020/200.8 KS
7440-48-4 Cobalt - Total ND µg/L 15 11/11/2011 6020/200.8 KS
7440-50-8 Copper - Total 1200 µg/L 1 D 11/11/2011 6020/200.8 KS
7439-92-1 Lead - Total 310 µg/L 1 11/11/2011 6020/200.8 KS
7439-96-5 Manganese - Total 290 µg/L 5 11/11/2011 6020/200.8 KS
7439-98-7 Molybdenum - Total ND µg/L 25 11/09/2011 6020/200.8 KS
7440-02-0 Nickel - Total 15 µg/L 2.0 11/11/2011 6020/200.8 KS
7782-49-2 Selenium - Total ND µg/L 1 11/11/2011 6020/200.8 KS
7440-22-4 Silver -Total 1.1 µg/L 0.2 11/09/2011 6020/200.8 KS
7440-24-6 Strontium - Total 800 µg/L 5 11/11/2011 6020/200.8 KS
7440-28-0 Thallium - Total ND µg/L 2 11/11/2011 6020/200.8 KS
7440-32-6 Titanium - Total 190 µg/L 10 11/11/2011 6020/200.8 KS
7440-62-2 Vanadium - Total 29 µg/L 2 11/11/2011 6020/200.8 KS
7440-66-6 Zinc - Total 57 µg/L 10 11/11/2011 6020/200.8 KS
7440-42-8 Boron - Total 140 µg/L 20 11/02/2011 6010/200.7 WN
7439-89-6 Iron - Total 4000 µg/L 20 11/02/2011 6010/200.7 WN
7664-41-7 Ammonia 28 mg N/L 1.0 D 10/24/2011 350.1 MB
7727-37-9 Nitrate + Nitrite 1.8 mg N/L 0.1 D 10/24/2011 353.2 MB
7440-44-0 TOC 5.5 mg/L 0.5 10/31/2011 5310C SM LAV
CAS# : Chemical Abstract Service Registry Number ug / L : microgram / liter (ppb) Laboratory Contacts
RL : Reporting Limit mg / L : milligram / liter (ppm) Inorganic Unit Mgr: Kirby Shane
ug / Kg : microgram / kilogram (ppb) Organic Unit Mgr: Carol Smith ND : Not Detectedmg / Kg : milligram / kilogram (ppm) Systems Mgmt Unit: George Krisztian
Lab Work Order #: 11000149 Page 4 of 5
