Experimental Investigation of High Strain-Rate Behaviour of Glass

7
Experimental investigation of high strain-rate behaviour of glass Marco Peroni 1, a , George Solomos 1,b , Valerio Pizzinato 1,c , Martin Larcher 2,d 1 EC Joint Research Centre, IPSC, European Laboratory for Structural Assessment ELSA, Via E. Fermi 2749, 21027 Ispra (VA) Italy 2 Institut für Mechanik und Statik, Universität der Bundeswehr München, 85577 Neubiberg, Germany a [email protected], b [email protected], c [email protected], d [email protected] Keywords: Split Hopkinson Pressure Bar, dynamic glass behaviour, laminated glass, strain-rate Abstract. The purpose of this work is to assess the dynamic mechanical behaviour of a commercial glass similar to that of the laminated glass structures used for protection and security applications in buildings. In particular, the study has been focussed on the influence of the strain-rate on the compressive (standard compression test) and tensile (splitting tensile test) strength of this glass. Tests at different strain-rates have been performed in the range between 10 -3 to 10 3 s -1 using standard test equipment for quasi-static tests and a SHPB equipped with a high-speed camera for the dynamic ones. Test data for compression tend to show that there is no substantial sensitivity to the strain-rate concerning ultimate strength and Young modulus. An appreciable increase in the ultimate tensile strength is revealed at higher strain-rate. Introduction Laminated glass panels are widely used for protection and security applications in buildings. Their dynamic behaviour, e.g. to blast loading, is influenced by the mechanical properties of the two materials normally used to build their sandwich structure: the external glass panes and the polymeric layer (usually PVB Polyvinylbutyral), which binds them together [1, 2]. The technical literature contains plenty of information about the dynamic mechanical properties of many structural materials, especially metals, obtained through different test types (such as Split Hopkinson Pressure Bar techniques, Taylor tests, flyer plate tests, etc.). However, the study of the dynamic mechanical properties of polymers and glassy materials is not as common. In addition, especially for glassy materials, many problems occur during dynamic testing due mainly to their brittle behaviour. For example in these situations it is very difficult for the specimen to reach dynamic equilibrium before crack propagation and failure, and frequently particular elaboration techniques for the experimental data must be developed in order to produce meaningful results. The purpose of this work is to assess the dynamic mechanical behaviour of a commercial glass similar to that used in laminated glass structures. In particular, the study has been focussed on the influence of the strain-rate on the compressive/tensile strength of this glass. Cylindrical specimens have been used both for compression (diameter 5 mm and height 6 mm) and splitting tensile tests (diameter 9 mm and height 5 mm). With reference to the splitting tensile test (Brazilian test) the effect of “bearing strips” has also been evaluated in order to better distribute compression loading and to avoid the propagation of initial cracks. Tests at different strain-rates have been performed in the range between 10 -3 to 10 3 s -1 using standard test equipment for quasi-static tests and a SHPB for the dynamic ones. Strain-rate reported refers to that at maximum stress. For what concerns high strain-rate tests, wave dispersion phenomena and the effect of local punching at the bar/specimen interface have been taken into account in order to improve the accuracy. Further, the deformation and cracking processes of the specimen have been monitored using a high-speed digital camera, which proves to be crucial in aiding in the interpretation of the data. Applied Mechanics and Materials Vol. 82 (2011) pp 63-68 Online available since 2011/Jul/27 at www.scientific.net © (2011) Trans Tech Publications, Switzerland doi:10.4028/www.scientific.net/AMM.82.63 All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTP, www.ttp.net. (ID: 137.193.23.208-16/08/11,10:26:53)

Transcript of Experimental Investigation of High Strain-Rate Behaviour of Glass

Experimental investigation of high strain-rate behaviour of glass

Marco Peroni1 a George Solomos1b Valerio Pizzinato1c Martin Larcher2d 1EC Joint Research Centre IPSC European Laboratory for Structural Assessment ELSA

Via E Fermi 2749 21027 Ispra (VA) Italy

2Institut fuumlr Mechanik und Statik Universitaumlt der Bundeswehr Muumlnchen 85577 Neubiberg

Germany

amarcoperonijrceceuropaeu

bgeorgesolomosjrceceuropaeu

cerminiopizzinatojrceceuropaeu

dmartinlarcherunibwde

Keywords Split Hopkinson Pressure Bar dynamic glass behaviour laminated glass strain-rate

Abstract The purpose of this work is to assess the dynamic mechanical behaviour of a commercial

glass similar to that of the laminated glass structures used for protection and security applications in

buildings In particular the study has been focussed on the influence of the strain-rate on the

compressive (standard compression test) and tensile (splitting tensile test) strength of this glass

Tests at different strain-rates have been performed in the range between 10-3

to 103 s

-1 using

standard test equipment for quasi-static tests and a SHPB equipped with a high-speed camera for the

dynamic ones Test data for compression tend to show that there is no substantial sensitivity to the

strain-rate concerning ultimate strength and Young modulus An appreciable increase in the ultimate

tensile strength is revealed at higher strain-rate

Introduction

Laminated glass panels are widely used for protection and security applications in buildings

Their dynamic behaviour eg to blast loading is influenced by the mechanical properties of the two

materials normally used to build their sandwich structure the external glass panes and the polymeric

layer (usually PVB Polyvinylbutyral) which binds them together [1 2] The technical literature

contains plenty of information about the dynamic mechanical properties of many structural

materials especially metals obtained through different test types (such as Split Hopkinson Pressure

Bar techniques Taylor tests flyer plate tests etc) However the study of the dynamic mechanical

properties of polymers and glassy materials is not as common In addition especially for glassy

materials many problems occur during dynamic testing due mainly to their brittle behaviour For

example in these situations it is very difficult for the specimen to reach dynamic equilibrium before

crack propagation and failure and frequently particular elaboration techniques for the experimental

data must be developed in order to produce meaningful results

The purpose of this work is to assess the dynamic mechanical behaviour of a commercial glass

similar to that used in laminated glass structures In particular the study has been focussed on the

influence of the strain-rate on the compressivetensile strength of this glass Cylindrical specimens

have been used both for compression (diameter 5 mm and height 6 mm) and splitting tensile tests

(diameter 9 mm and height 5 mm) With reference to the splitting tensile test (Brazilian test) the

effect of ldquobearing stripsrdquo has also been evaluated in order to better distribute compression loading

and to avoid the propagation of initial cracks Tests at different strain-rates have been performed in

the range between 10-3

to 103 s

-1 using standard test equipment for quasi-static tests and a SHPB for

the dynamic ones Strain-rate reported refers to that at maximum stress For what concerns high

strain-rate tests wave dispersion phenomena and the effect of local punching at the barspecimen

interface have been taken into account in order to improve the accuracy Further the deformation

and cracking processes of the specimen have been monitored using a high-speed digital camera

which proves to be crucial in aiding in the interpretation of the data

Applied Mechanics and Materials Vol 82 (2011) pp 63-68Online available since 2011Jul27 at wwwscientificnetcopy (2011) Trans Tech Publications Switzerlanddoi104028wwwscientificnetAMM8263

All rights reserved No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTPwwwttpnet (ID 13719323208-160811102653)

Test equipment

Compression tests and splitting tensile tests on glass specimens have been performed with two

different apparatuses Static compression and splitting tensile tests have been performed on the

electro-mechanical universal testing machine Zwick Z100 (maximum force 100 kN and maximum

velocity 300 mmmin) at the Safety and Reliability Laboratory of the Politecnico di Torino High

strain-rate compression and splitting tensile tests have been carried out on a SHPB at the HopLab of

the JRCIspra where maraging steel rods of 10 mm diameter are used With reference to Fig 1a

this equipment generates a compressive pulse by loading in tension a portion of the input bar (1 m)

and rapidly releasing the left end with a fragile that breaks at an established load [3] The

compressive generated pulse travels through the pre-stressed and input bars and loads the specimen

like a conventional SHPB as shown in the Lagrangian waves diagram of the test (Fig 1b) With

this setup long duration compressive pulses can be easily created without the problems related to

projectilerod misalignment inherent in the conventional SHPB

t

x Pre-stressed bar Input bar Output bar

Strain transducers

Reflected wave Transmitted wave

Incident wave

(

(Fragile bolt

Hydraulic actuator

Fig 1 Pre-stressed SHPB setup with Lagrangian waves propagation diagram

The loaddisplacement curves of the specimen can be obtained with standard SHPB procedures

with the only difference that due the longer duration of the incident pulse normally incident and

reflected waves are not separated For this reason it is necessary to separate ascending and

descending waves with an appropriate algorithm [4] Because of the brittle behaviour of the material

tested it is essential to compensate for distortions due to dispersion phenomena [5] and to account

for the effect of local punching at the barspecimen interface [6] in order to improve accuracy To

better evaluate the specimen loading conditions also during the dynamic tests a high speed camera

synchronised with the SHPB acquisition system has been used Reduction of specimen overheating

is achieved by utilizing ldquocoldrdquo LED lights for the illumination

Fig 2 Glass specimens adopted

All experiments have been carried out on high purity optical glass specimens obtained by

grinding The glass with the trade name Optiwhite has a low iron content and in its specifications

includes the following mechanical characteristics density 2500 kgm3 Young Modulus 73 GPa

Poisson ratio 023 compression strength 700-900 MPa and bending (tensile) strength 30 MPa

Cylindrical specimens have been employed for both compression and splitting tensile tests In

64 Performance Protection and Strengthening of Structures under ExtremeLoading

particular their dimensions were for compression tests of 5 mm diameter and 6 mm length and for

splitting tensile tests of 9 mm diameter and 5 or 10 mm length (Figure 2) To obtain reliable

experimental data about 5 repetitions for each type of tests have been performed

Compression tests

Compression tests on glass specimens have been carried out at two strain-rates of about 510-4

s-1

(SC=static compression) and about 1103s

-1 (DC=dynamic compression) Due to the small specimen

sizes it has not been possible to precisely characterize the glass longitudinal elastic modulus using

strain-gages however as shown below reliable estimates of the global mechanical behaviour of the

material have been reached For the static tests deformation has been obtained through cross-head

displacement measurements which have been corrected from the errors introduced by the machine

compliance using a calibrated test In the high strain-rate tests dynamic equilibrium has been

carefully checked and as mentioned before state-of-the-art compensations have been applied to

acquire signals and to improve their accuracy Fig 3a summarizes all compression tests at both

strain-rates and includes also additional dynamic compression test curves where specimens did not

break These latter allow to evaluate the longitudinal elastic modulus with good accuracy by using

both the loading and unloading test phases (DCNF= dynamic compression no fracture)

0 002 0040

500

1000

1500

Stress (MPa)

SC

0 002 0040

500

1000

1500

Strain

DC

0 002 0040

500

1000

1500

DCNF

10-4

10-2

100

102

104

0

500

1000

1500

Strainrate (1s)

Stress (MPa)

SC

DC

DCNF

Fig 3 a) Compression stress-strain curves b) Maximum stress vs strain-rate in compression tests

As easily noted glass maintains a brittle-pure elastic behaviour at both strain-rates and the elastic

longitudinal modulus seems not to be appreciably influenced by the test speed Compression

maximum stresses show also small strain-rate sensitivity (Fig 3b) Table 1 summarizes the

experimental results in terms of maximum stress and longitudinal elastic modulus

Table 1 Experimental compression data

1 2 3 4 5 mean

Standard

deviation

SC

Strain-rate (s-1) 510

-4 510

-4 510

-4 510

-4 510

-4 510

-4 310

-5

Max stress (MPa) 1144 978 1087 1160 1070 1087 72

Young modulus (GPa) 61 58 72 66 79 67 8

DC

Strain-rate (s-1) 1342 947 1055 923 1282 1109 192

Max stress (MPa) 1326 1126 1251 1081 1109 1179 105

Young modulus (GPa) 63 69 51 50 54 58 8

When analysing experimental data both the static and the dynamic standard deviation of the

maximum stress and longitudinal elastic modulus are calculated and found to be quite small

considering the rather large scattering of data usually encountered in brittle materials In addition

since the maximum stress increase under high strain-rate testing is comparable to the standard

Applied Mechanics and Materials Vol 82 65

deviation it can be stated that the analysed glass does not present noticeable strain-rate sensitivity

To conclude the analysis of compression tests it is interesting to observe the image sequence of a

dynamic experiment recorded with the high-speed camera (50000 fps) The specimen was elastically

loaded (for the small size of the specimen the dynamic equilibrium is verified) and some radial

cracks appear in the third image

Fig 4 High speed sequence of compression test (50000 fps)

At this point the specimen loaded in compression collapses and a tensile wave starts to propagate

in the glass Due to the extremely low tensile strength of glass (compared to its compression one)

the whole specimen blows up becoming a fine glass dust as shown in the last picture At this point

the glass is no more able to transmit any compressive load and the transmitted signal vanishes

Splitting tensile test (Brazilian test)

Splitting tensile test or Brazilian test is nowadays a conventional mechanical test for the

investigation of the tensile strength of brittle materials This test is standardized only for concrete

specimens [5] but it is also adopted for other brittle materials such as rocks ceramics or glass [6]

The setup of splitting tensile test is rather simple a cylindrical specimen is loaded in compression

along two opposite generatrices as shown in Fig 5a This compression load generates a particular

stress-strain field with two peaks of compression at the cylinder surface and an interior zone of

almost constant tension (Fig 5a) For the higher compression strength of brittle material the

specimen breaks under tension and the maximum tensile stress can be easily deduced with the well

known analytical expression

Db

P

sdotsdot

sdot=π

σ2

(1)

where σ is the tensile strength P the maximum compression force during the test and b and D are

the specimen height and diameter respectively

compression

tension

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Stress (MPa)

S5

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Displacement (mm)

S5P

Fig 5 a) Brazilian test setup and typical stressstrain field b) static experimental data

For the reduction of local compression peaks small pieces of compliant materials (bearing strips

usually made of plywood for concrete specimens) are used to better distribute compression loading

and to avoid the propagation of initial cracks For the current tests the effectiveness of bearing strips

66 Performance Protection and Strengthening of Structures under ExtremeLoading

to loading the specimens has been evaluated in a preliminary phase For this reason two series of

tests have been performed splitting tests on specimen without (S5) and with paper bearing strips

(S5P)

Table 2 Experimental splitting tensile data

1 2 3 4 5 mean Standard

deviation

S5 Velocity (mms) 0009 0009 0009 0009 0009 0009 1410

-4

Max stress (MPa) 756 546 382 523 861 614 192

S5P

Velocity (mms) 0010 0010 0010 0009 0009 0010 7710-4

Max stress (MPa) 667 473 505 509 574 545 77

D5 Velocity (ms) 550 483 698 599 528 572 064

Max stress (MPa) 998 773 348 475 621 643 254

D5P

Velocity (ms) 767 673 84 742 81 772 067

Max stress (MPa) 871 917 7614 981 947 895 851

As presented in Fig 5b and in Table 2 the series without bearing strips shows a higher scatter of

data results probably due to the effect of damage induced by compression loading plates Using the

paper bearing strips the standard deviation is three times smaller and allows to evaluate more

effectively the mechanical properties of the glass tested

Dynamic tests have been performed directly by loading the specimen with the SHPB bars as in a

standard compression test In this kind of tests specimen-bar alignment is essential to correctly

transfer the compression pulse from the bars to the specimen Also in this case two series of

experiments have been carried out with and without bearing strips (made of papers)

0 01 02 03 040

20

40

60

80

100

120

Stress (MPa)

D5

0 01 02 03 040

20

40

60

80

100

120

Displacement (mm)

D5P

10-6

10-4

10-2

100

102

0

20

40

60

80

100

120

Test speed (ms)

Stress (MPa)

S5

S5P

D5

D5P

Fig 6 a) Dynamic tensile data b) maximum stress vs strain-rate in splitting tensile tests

Preliminary tests have been conducted to ensure dynamic equilibrium and this condition has

been verified for all specimens Fig 6a summarizes the data results obtained by the dynamic

splitting tensile tests Also in dynamic tests data obtained without the bearing strips present high

scattering and this fact prevents the correct evaluation of the glass tensile strength (standard

deviation of D5 is three times greater than standard deviation of D5P) Contrary to the compression

data the tensile strength seems to be substantially influenced by strain-rate with an increase of about

30 MPa when the strain-rate grows by six magnitude orders This phenomenon has also been

noticed in the high strain-rate behaviour of concrete where the tensile strength is more strain-rate

influenced than the compressive strength

Applied Mechanics and Materials Vol 82 67

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

Test equipment

Compression tests and splitting tensile tests on glass specimens have been performed with two

different apparatuses Static compression and splitting tensile tests have been performed on the

electro-mechanical universal testing machine Zwick Z100 (maximum force 100 kN and maximum

velocity 300 mmmin) at the Safety and Reliability Laboratory of the Politecnico di Torino High

strain-rate compression and splitting tensile tests have been carried out on a SHPB at the HopLab of

the JRCIspra where maraging steel rods of 10 mm diameter are used With reference to Fig 1a

this equipment generates a compressive pulse by loading in tension a portion of the input bar (1 m)

and rapidly releasing the left end with a fragile that breaks at an established load [3] The

compressive generated pulse travels through the pre-stressed and input bars and loads the specimen

like a conventional SHPB as shown in the Lagrangian waves diagram of the test (Fig 1b) With

this setup long duration compressive pulses can be easily created without the problems related to

projectilerod misalignment inherent in the conventional SHPB

t

x Pre-stressed bar Input bar Output bar

Strain transducers

Reflected wave Transmitted wave

Incident wave

(

(Fragile bolt

Hydraulic actuator

Fig 1 Pre-stressed SHPB setup with Lagrangian waves propagation diagram

The loaddisplacement curves of the specimen can be obtained with standard SHPB procedures

with the only difference that due the longer duration of the incident pulse normally incident and

reflected waves are not separated For this reason it is necessary to separate ascending and

descending waves with an appropriate algorithm [4] Because of the brittle behaviour of the material

tested it is essential to compensate for distortions due to dispersion phenomena [5] and to account

for the effect of local punching at the barspecimen interface [6] in order to improve accuracy To

better evaluate the specimen loading conditions also during the dynamic tests a high speed camera

synchronised with the SHPB acquisition system has been used Reduction of specimen overheating

is achieved by utilizing ldquocoldrdquo LED lights for the illumination

Fig 2 Glass specimens adopted

All experiments have been carried out on high purity optical glass specimens obtained by

grinding The glass with the trade name Optiwhite has a low iron content and in its specifications

includes the following mechanical characteristics density 2500 kgm3 Young Modulus 73 GPa

Poisson ratio 023 compression strength 700-900 MPa and bending (tensile) strength 30 MPa

Cylindrical specimens have been employed for both compression and splitting tensile tests In

64 Performance Protection and Strengthening of Structures under ExtremeLoading

particular their dimensions were for compression tests of 5 mm diameter and 6 mm length and for

splitting tensile tests of 9 mm diameter and 5 or 10 mm length (Figure 2) To obtain reliable

experimental data about 5 repetitions for each type of tests have been performed

Compression tests

Compression tests on glass specimens have been carried out at two strain-rates of about 510-4

s-1

(SC=static compression) and about 1103s

-1 (DC=dynamic compression) Due to the small specimen

sizes it has not been possible to precisely characterize the glass longitudinal elastic modulus using

strain-gages however as shown below reliable estimates of the global mechanical behaviour of the

material have been reached For the static tests deformation has been obtained through cross-head

displacement measurements which have been corrected from the errors introduced by the machine

compliance using a calibrated test In the high strain-rate tests dynamic equilibrium has been

carefully checked and as mentioned before state-of-the-art compensations have been applied to

acquire signals and to improve their accuracy Fig 3a summarizes all compression tests at both

strain-rates and includes also additional dynamic compression test curves where specimens did not

break These latter allow to evaluate the longitudinal elastic modulus with good accuracy by using

both the loading and unloading test phases (DCNF= dynamic compression no fracture)

0 002 0040

500

1000

1500

Stress (MPa)

SC

0 002 0040

500

1000

1500

Strain

DC

0 002 0040

500

1000

1500

DCNF

10-4

10-2

100

102

104

0

500

1000

1500

Strainrate (1s)

Stress (MPa)

SC

DC

DCNF

Fig 3 a) Compression stress-strain curves b) Maximum stress vs strain-rate in compression tests

As easily noted glass maintains a brittle-pure elastic behaviour at both strain-rates and the elastic

longitudinal modulus seems not to be appreciably influenced by the test speed Compression

maximum stresses show also small strain-rate sensitivity (Fig 3b) Table 1 summarizes the

experimental results in terms of maximum stress and longitudinal elastic modulus

Table 1 Experimental compression data

1 2 3 4 5 mean

Standard

deviation

SC

Strain-rate (s-1) 510

-4 510

-4 510

-4 510

-4 510

-4 510

-4 310

-5

Max stress (MPa) 1144 978 1087 1160 1070 1087 72

Young modulus (GPa) 61 58 72 66 79 67 8

DC

Strain-rate (s-1) 1342 947 1055 923 1282 1109 192

Max stress (MPa) 1326 1126 1251 1081 1109 1179 105

Young modulus (GPa) 63 69 51 50 54 58 8

When analysing experimental data both the static and the dynamic standard deviation of the

maximum stress and longitudinal elastic modulus are calculated and found to be quite small

considering the rather large scattering of data usually encountered in brittle materials In addition

since the maximum stress increase under high strain-rate testing is comparable to the standard

Applied Mechanics and Materials Vol 82 65

deviation it can be stated that the analysed glass does not present noticeable strain-rate sensitivity

To conclude the analysis of compression tests it is interesting to observe the image sequence of a

dynamic experiment recorded with the high-speed camera (50000 fps) The specimen was elastically

loaded (for the small size of the specimen the dynamic equilibrium is verified) and some radial

cracks appear in the third image

Fig 4 High speed sequence of compression test (50000 fps)

At this point the specimen loaded in compression collapses and a tensile wave starts to propagate

in the glass Due to the extremely low tensile strength of glass (compared to its compression one)

the whole specimen blows up becoming a fine glass dust as shown in the last picture At this point

the glass is no more able to transmit any compressive load and the transmitted signal vanishes

Splitting tensile test (Brazilian test)

Splitting tensile test or Brazilian test is nowadays a conventional mechanical test for the

investigation of the tensile strength of brittle materials This test is standardized only for concrete

specimens [5] but it is also adopted for other brittle materials such as rocks ceramics or glass [6]

The setup of splitting tensile test is rather simple a cylindrical specimen is loaded in compression

along two opposite generatrices as shown in Fig 5a This compression load generates a particular

stress-strain field with two peaks of compression at the cylinder surface and an interior zone of

almost constant tension (Fig 5a) For the higher compression strength of brittle material the

specimen breaks under tension and the maximum tensile stress can be easily deduced with the well

known analytical expression

Db

P

sdotsdot

sdot=π

σ2

(1)

where σ is the tensile strength P the maximum compression force during the test and b and D are

the specimen height and diameter respectively

compression

tension

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Stress (MPa)

S5

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Displacement (mm)

S5P

Fig 5 a) Brazilian test setup and typical stressstrain field b) static experimental data

For the reduction of local compression peaks small pieces of compliant materials (bearing strips

usually made of plywood for concrete specimens) are used to better distribute compression loading

and to avoid the propagation of initial cracks For the current tests the effectiveness of bearing strips

66 Performance Protection and Strengthening of Structures under ExtremeLoading

to loading the specimens has been evaluated in a preliminary phase For this reason two series of

tests have been performed splitting tests on specimen without (S5) and with paper bearing strips

(S5P)

Table 2 Experimental splitting tensile data

1 2 3 4 5 mean Standard

deviation

S5 Velocity (mms) 0009 0009 0009 0009 0009 0009 1410

-4

Max stress (MPa) 756 546 382 523 861 614 192

S5P

Velocity (mms) 0010 0010 0010 0009 0009 0010 7710-4

Max stress (MPa) 667 473 505 509 574 545 77

D5 Velocity (ms) 550 483 698 599 528 572 064

Max stress (MPa) 998 773 348 475 621 643 254

D5P

Velocity (ms) 767 673 84 742 81 772 067

Max stress (MPa) 871 917 7614 981 947 895 851

As presented in Fig 5b and in Table 2 the series without bearing strips shows a higher scatter of

data results probably due to the effect of damage induced by compression loading plates Using the

paper bearing strips the standard deviation is three times smaller and allows to evaluate more

effectively the mechanical properties of the glass tested

Dynamic tests have been performed directly by loading the specimen with the SHPB bars as in a

standard compression test In this kind of tests specimen-bar alignment is essential to correctly

transfer the compression pulse from the bars to the specimen Also in this case two series of

experiments have been carried out with and without bearing strips (made of papers)

0 01 02 03 040

20

40

60

80

100

120

Stress (MPa)

D5

0 01 02 03 040

20

40

60

80

100

120

Displacement (mm)

D5P

10-6

10-4

10-2

100

102

0

20

40

60

80

100

120

Test speed (ms)

Stress (MPa)

S5

S5P

D5

D5P

Fig 6 a) Dynamic tensile data b) maximum stress vs strain-rate in splitting tensile tests

Preliminary tests have been conducted to ensure dynamic equilibrium and this condition has

been verified for all specimens Fig 6a summarizes the data results obtained by the dynamic

splitting tensile tests Also in dynamic tests data obtained without the bearing strips present high

scattering and this fact prevents the correct evaluation of the glass tensile strength (standard

deviation of D5 is three times greater than standard deviation of D5P) Contrary to the compression

data the tensile strength seems to be substantially influenced by strain-rate with an increase of about

30 MPa when the strain-rate grows by six magnitude orders This phenomenon has also been

noticed in the high strain-rate behaviour of concrete where the tensile strength is more strain-rate

influenced than the compressive strength

Applied Mechanics and Materials Vol 82 67

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

particular their dimensions were for compression tests of 5 mm diameter and 6 mm length and for

splitting tensile tests of 9 mm diameter and 5 or 10 mm length (Figure 2) To obtain reliable

experimental data about 5 repetitions for each type of tests have been performed

Compression tests

Compression tests on glass specimens have been carried out at two strain-rates of about 510-4

s-1

(SC=static compression) and about 1103s

-1 (DC=dynamic compression) Due to the small specimen

sizes it has not been possible to precisely characterize the glass longitudinal elastic modulus using

strain-gages however as shown below reliable estimates of the global mechanical behaviour of the

material have been reached For the static tests deformation has been obtained through cross-head

displacement measurements which have been corrected from the errors introduced by the machine

compliance using a calibrated test In the high strain-rate tests dynamic equilibrium has been

carefully checked and as mentioned before state-of-the-art compensations have been applied to

acquire signals and to improve their accuracy Fig 3a summarizes all compression tests at both

strain-rates and includes also additional dynamic compression test curves where specimens did not

break These latter allow to evaluate the longitudinal elastic modulus with good accuracy by using

both the loading and unloading test phases (DCNF= dynamic compression no fracture)

0 002 0040

500

1000

1500

Stress (MPa)

SC

0 002 0040

500

1000

1500

Strain

DC

0 002 0040

500

1000

1500

DCNF

10-4

10-2

100

102

104

0

500

1000

1500

Strainrate (1s)

Stress (MPa)

SC

DC

DCNF

Fig 3 a) Compression stress-strain curves b) Maximum stress vs strain-rate in compression tests

As easily noted glass maintains a brittle-pure elastic behaviour at both strain-rates and the elastic

longitudinal modulus seems not to be appreciably influenced by the test speed Compression

maximum stresses show also small strain-rate sensitivity (Fig 3b) Table 1 summarizes the

experimental results in terms of maximum stress and longitudinal elastic modulus

Table 1 Experimental compression data

1 2 3 4 5 mean

Standard

deviation

SC

Strain-rate (s-1) 510

-4 510

-4 510

-4 510

-4 510

-4 510

-4 310

-5

Max stress (MPa) 1144 978 1087 1160 1070 1087 72

Young modulus (GPa) 61 58 72 66 79 67 8

DC

Strain-rate (s-1) 1342 947 1055 923 1282 1109 192

Max stress (MPa) 1326 1126 1251 1081 1109 1179 105

Young modulus (GPa) 63 69 51 50 54 58 8

When analysing experimental data both the static and the dynamic standard deviation of the

maximum stress and longitudinal elastic modulus are calculated and found to be quite small

considering the rather large scattering of data usually encountered in brittle materials In addition

since the maximum stress increase under high strain-rate testing is comparable to the standard

Applied Mechanics and Materials Vol 82 65

deviation it can be stated that the analysed glass does not present noticeable strain-rate sensitivity

To conclude the analysis of compression tests it is interesting to observe the image sequence of a

dynamic experiment recorded with the high-speed camera (50000 fps) The specimen was elastically

loaded (for the small size of the specimen the dynamic equilibrium is verified) and some radial

cracks appear in the third image

Fig 4 High speed sequence of compression test (50000 fps)

At this point the specimen loaded in compression collapses and a tensile wave starts to propagate

in the glass Due to the extremely low tensile strength of glass (compared to its compression one)

the whole specimen blows up becoming a fine glass dust as shown in the last picture At this point

the glass is no more able to transmit any compressive load and the transmitted signal vanishes

Splitting tensile test (Brazilian test)

Splitting tensile test or Brazilian test is nowadays a conventional mechanical test for the

investigation of the tensile strength of brittle materials This test is standardized only for concrete

specimens [5] but it is also adopted for other brittle materials such as rocks ceramics or glass [6]

The setup of splitting tensile test is rather simple a cylindrical specimen is loaded in compression

along two opposite generatrices as shown in Fig 5a This compression load generates a particular

stress-strain field with two peaks of compression at the cylinder surface and an interior zone of

almost constant tension (Fig 5a) For the higher compression strength of brittle material the

specimen breaks under tension and the maximum tensile stress can be easily deduced with the well

known analytical expression

Db

P

sdotsdot

sdot=π

σ2

(1)

where σ is the tensile strength P the maximum compression force during the test and b and D are

the specimen height and diameter respectively

compression

tension

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Stress (MPa)

S5

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Displacement (mm)

S5P

Fig 5 a) Brazilian test setup and typical stressstrain field b) static experimental data

For the reduction of local compression peaks small pieces of compliant materials (bearing strips

usually made of plywood for concrete specimens) are used to better distribute compression loading

and to avoid the propagation of initial cracks For the current tests the effectiveness of bearing strips

66 Performance Protection and Strengthening of Structures under ExtremeLoading

to loading the specimens has been evaluated in a preliminary phase For this reason two series of

tests have been performed splitting tests on specimen without (S5) and with paper bearing strips

(S5P)

Table 2 Experimental splitting tensile data

1 2 3 4 5 mean Standard

deviation

S5 Velocity (mms) 0009 0009 0009 0009 0009 0009 1410

-4

Max stress (MPa) 756 546 382 523 861 614 192

S5P

Velocity (mms) 0010 0010 0010 0009 0009 0010 7710-4

Max stress (MPa) 667 473 505 509 574 545 77

D5 Velocity (ms) 550 483 698 599 528 572 064

Max stress (MPa) 998 773 348 475 621 643 254

D5P

Velocity (ms) 767 673 84 742 81 772 067

Max stress (MPa) 871 917 7614 981 947 895 851

As presented in Fig 5b and in Table 2 the series without bearing strips shows a higher scatter of

data results probably due to the effect of damage induced by compression loading plates Using the

paper bearing strips the standard deviation is three times smaller and allows to evaluate more

effectively the mechanical properties of the glass tested

Dynamic tests have been performed directly by loading the specimen with the SHPB bars as in a

standard compression test In this kind of tests specimen-bar alignment is essential to correctly

transfer the compression pulse from the bars to the specimen Also in this case two series of

experiments have been carried out with and without bearing strips (made of papers)

0 01 02 03 040

20

40

60

80

100

120

Stress (MPa)

D5

0 01 02 03 040

20

40

60

80

100

120

Displacement (mm)

D5P

10-6

10-4

10-2

100

102

0

20

40

60

80

100

120

Test speed (ms)

Stress (MPa)

S5

S5P

D5

D5P

Fig 6 a) Dynamic tensile data b) maximum stress vs strain-rate in splitting tensile tests

Preliminary tests have been conducted to ensure dynamic equilibrium and this condition has

been verified for all specimens Fig 6a summarizes the data results obtained by the dynamic

splitting tensile tests Also in dynamic tests data obtained without the bearing strips present high

scattering and this fact prevents the correct evaluation of the glass tensile strength (standard

deviation of D5 is three times greater than standard deviation of D5P) Contrary to the compression

data the tensile strength seems to be substantially influenced by strain-rate with an increase of about

30 MPa when the strain-rate grows by six magnitude orders This phenomenon has also been

noticed in the high strain-rate behaviour of concrete where the tensile strength is more strain-rate

influenced than the compressive strength

Applied Mechanics and Materials Vol 82 67

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

deviation it can be stated that the analysed glass does not present noticeable strain-rate sensitivity

To conclude the analysis of compression tests it is interesting to observe the image sequence of a

dynamic experiment recorded with the high-speed camera (50000 fps) The specimen was elastically

loaded (for the small size of the specimen the dynamic equilibrium is verified) and some radial

cracks appear in the third image

Fig 4 High speed sequence of compression test (50000 fps)

At this point the specimen loaded in compression collapses and a tensile wave starts to propagate

in the glass Due to the extremely low tensile strength of glass (compared to its compression one)

the whole specimen blows up becoming a fine glass dust as shown in the last picture At this point

the glass is no more able to transmit any compressive load and the transmitted signal vanishes

Splitting tensile test (Brazilian test)

Splitting tensile test or Brazilian test is nowadays a conventional mechanical test for the

investigation of the tensile strength of brittle materials This test is standardized only for concrete

specimens [5] but it is also adopted for other brittle materials such as rocks ceramics or glass [6]

The setup of splitting tensile test is rather simple a cylindrical specimen is loaded in compression

along two opposite generatrices as shown in Fig 5a This compression load generates a particular

stress-strain field with two peaks of compression at the cylinder surface and an interior zone of

almost constant tension (Fig 5a) For the higher compression strength of brittle material the

specimen breaks under tension and the maximum tensile stress can be easily deduced with the well

known analytical expression

Db

P

sdotsdot

sdot=π

σ2

(1)

where σ is the tensile strength P the maximum compression force during the test and b and D are

the specimen height and diameter respectively

compression

tension

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Stress (MPa)

S5

0 01 02 03 040

10

20

30

40

50

60

70

80

90

100

Displacement (mm)

S5P

Fig 5 a) Brazilian test setup and typical stressstrain field b) static experimental data

For the reduction of local compression peaks small pieces of compliant materials (bearing strips

usually made of plywood for concrete specimens) are used to better distribute compression loading

and to avoid the propagation of initial cracks For the current tests the effectiveness of bearing strips

66 Performance Protection and Strengthening of Structures under ExtremeLoading

to loading the specimens has been evaluated in a preliminary phase For this reason two series of

tests have been performed splitting tests on specimen without (S5) and with paper bearing strips

(S5P)

Table 2 Experimental splitting tensile data

1 2 3 4 5 mean Standard

deviation

S5 Velocity (mms) 0009 0009 0009 0009 0009 0009 1410

-4

Max stress (MPa) 756 546 382 523 861 614 192

S5P

Velocity (mms) 0010 0010 0010 0009 0009 0010 7710-4

Max stress (MPa) 667 473 505 509 574 545 77

D5 Velocity (ms) 550 483 698 599 528 572 064

Max stress (MPa) 998 773 348 475 621 643 254

D5P

Velocity (ms) 767 673 84 742 81 772 067

Max stress (MPa) 871 917 7614 981 947 895 851

As presented in Fig 5b and in Table 2 the series without bearing strips shows a higher scatter of

data results probably due to the effect of damage induced by compression loading plates Using the

paper bearing strips the standard deviation is three times smaller and allows to evaluate more

effectively the mechanical properties of the glass tested

Dynamic tests have been performed directly by loading the specimen with the SHPB bars as in a

standard compression test In this kind of tests specimen-bar alignment is essential to correctly

transfer the compression pulse from the bars to the specimen Also in this case two series of

experiments have been carried out with and without bearing strips (made of papers)

0 01 02 03 040

20

40

60

80

100

120

Stress (MPa)

D5

0 01 02 03 040

20

40

60

80

100

120

Displacement (mm)

D5P

10-6

10-4

10-2

100

102

0

20

40

60

80

100

120

Test speed (ms)

Stress (MPa)

S5

S5P

D5

D5P

Fig 6 a) Dynamic tensile data b) maximum stress vs strain-rate in splitting tensile tests

Preliminary tests have been conducted to ensure dynamic equilibrium and this condition has

been verified for all specimens Fig 6a summarizes the data results obtained by the dynamic

splitting tensile tests Also in dynamic tests data obtained without the bearing strips present high

scattering and this fact prevents the correct evaluation of the glass tensile strength (standard

deviation of D5 is three times greater than standard deviation of D5P) Contrary to the compression

data the tensile strength seems to be substantially influenced by strain-rate with an increase of about

30 MPa when the strain-rate grows by six magnitude orders This phenomenon has also been

noticed in the high strain-rate behaviour of concrete where the tensile strength is more strain-rate

influenced than the compressive strength

Applied Mechanics and Materials Vol 82 67

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

to loading the specimens has been evaluated in a preliminary phase For this reason two series of

tests have been performed splitting tests on specimen without (S5) and with paper bearing strips

(S5P)

Table 2 Experimental splitting tensile data

1 2 3 4 5 mean Standard

deviation

S5 Velocity (mms) 0009 0009 0009 0009 0009 0009 1410

-4

Max stress (MPa) 756 546 382 523 861 614 192

S5P

Velocity (mms) 0010 0010 0010 0009 0009 0010 7710-4

Max stress (MPa) 667 473 505 509 574 545 77

D5 Velocity (ms) 550 483 698 599 528 572 064

Max stress (MPa) 998 773 348 475 621 643 254

D5P

Velocity (ms) 767 673 84 742 81 772 067

Max stress (MPa) 871 917 7614 981 947 895 851

As presented in Fig 5b and in Table 2 the series without bearing strips shows a higher scatter of

data results probably due to the effect of damage induced by compression loading plates Using the

paper bearing strips the standard deviation is three times smaller and allows to evaluate more

effectively the mechanical properties of the glass tested

Dynamic tests have been performed directly by loading the specimen with the SHPB bars as in a

standard compression test In this kind of tests specimen-bar alignment is essential to correctly

transfer the compression pulse from the bars to the specimen Also in this case two series of

experiments have been carried out with and without bearing strips (made of papers)

0 01 02 03 040

20

40

60

80

100

120

Stress (MPa)

D5

0 01 02 03 040

20

40

60

80

100

120

Displacement (mm)

D5P

10-6

10-4

10-2

100

102

0

20

40

60

80

100

120

Test speed (ms)

Stress (MPa)

S5

S5P

D5

D5P

Fig 6 a) Dynamic tensile data b) maximum stress vs strain-rate in splitting tensile tests

Preliminary tests have been conducted to ensure dynamic equilibrium and this condition has

been verified for all specimens Fig 6a summarizes the data results obtained by the dynamic

splitting tensile tests Also in dynamic tests data obtained without the bearing strips present high

scattering and this fact prevents the correct evaluation of the glass tensile strength (standard

deviation of D5 is three times greater than standard deviation of D5P) Contrary to the compression

data the tensile strength seems to be substantially influenced by strain-rate with an increase of about

30 MPa when the strain-rate grows by six magnitude orders This phenomenon has also been

noticed in the high strain-rate behaviour of concrete where the tensile strength is more strain-rate

influenced than the compressive strength

Applied Mechanics and Materials Vol 82 67

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

Fig 7 presents a sequence of images of a dynamic splitting test without bearing strips recorded at

50000 fps It is interesting to observe the initial cracks due to compression loading (picture two) and

the tensile damage zone next to the barloading axis (picture three to five) This sequence confirms

that the specimenrsquos failure is due to tensile stresses generated along the diameter of the loading axis

as depicted in Fig5a

Fig 7 High speed sequence of splitting tensile test (50000 fps)

Further numerical and experimental investigations would be required to verify the actual stress-

strain field in the specimen during static and dynamic tests and to evaluate the accuracy of Eq 1

Summary

A study of the strain-rate influence on the compressive and tensile behaviour of commercial glass

has been conducted The experimental results try to cover the gap in literature concerning

mechanical behaviour of glassy materials at medium-high strain-rate To obtain reliable data state-

of-the-art compensations for SHPB tests have been adopted and concerning splitting tensile test

different testing setups have been evaluated Compression test results indicate that this glass does

not present any substantial sensitivity to the strain-rate concerning ultimate strength and Young

modulus With reference to tensile data glass tensile mechanical behaviour seems to be influenced

by strain rate and tensile strength increases by about 30 MPa when the strain-rate grows by six

magnitude orders Further numerical and experimental investigations will be suitable to verify the

accuracy of tensile properties deduced by splitting tensile tests on brittle materials like glass

especially under dynamic loading conditions Further it will be interesting to evaluate sizescale

effects also in dynamic tests using the high loading capability of the SHPB or simply to achieve

more representative specimen volumes

References

[1] HS Norville EJ Conrath Journal of Architectural Engineering Vol 7 (2001) p 80

[2] M Larcher N Gebbeken M Teich G Solomos Simulation of laminated glass loaded by air

blast waves Proc4th

ISAAG Munich (2010)

[3] E Cadoni G Solomos C Albertini Mag Concrete Res Vol 60 (2008) p221

[4] H Zhao G Gary J Mech Phys Solids Vol 45 (1997) p 1185

[5] A Tyas AJ Watson Int J Impact Eng Vol 25 (2001) p 87

[6] G Gary K Safa Accounting for the effect of local punching at the barspecimen interface in

SHPB experiments Proc DYMAT 2009 Bruxelles (2009)

[7] ASTM C496-96 Standard test method for splitting tensile strength of cylindrical concrete

specimens ASTM standard

[8] CS Chen E Pan B Amadei Int J Rock Mech Sci Vol 35 (1998) p 43

[9] C Rocco GV Guinea J Planas M Elices Cement Concrete Res Vol 31 (2001) p73

[10] C Johnstone C Ruiz Int J Solids Structures Vol 32 (1995) p2647

[11] T Holmquist G Johnson D Grady C Lopatin E Hertel High strain rate properties and

constitutive modelling of glass Proc 15th

International Symposium on Ballistics Israel (1995)

68 Performance Protection and Strengthening of Structures under ExtremeLoading

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263

Performance Protection and Strengthening of Structures under Extreme Loading doi104028wwwscientificnetAMM82 Experimental Investigation of High Strain-Rate Behaviour of Glass doi104028wwwscientificnetAMM8263