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Combined treatments of blanching and dehydration: study on potato cubes
Transcript of Combined treatments of blanching and dehydration: study on potato cubes
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Journal of Food Engineering 68 (2005) 289–296
Combined treatments of blanching and dehydration:study on potato cubes
Carla Severini, Antonietta Baiano *, Teresa De Pilli, Barbara F. Carbone, A. Derossi
Faculty of Agriculture, Department of Food Science, University of Foggia, Via Napoli 25, 71100 Foggia, Italy
Received 23 January 2004; accepted 31 May 2004
Abstract
Samples of Solanum tuberosum var. Primura were submitted to combined treatments of blanching and dehydration. Blanching
was alternatively performed in hot distilled water, hot sugary-saline solution, by microwaves in distilled water or by microwaves in
saline solution. Drying was alternatively carried out in an air cabinet, a microwave oven or a belt drier. In terms of process speed,
colour retention and water absorption capacity, the best results were obtained combining microwave blanching with dehydration on
the belt drier. In particular, dehydration on the belt drier levelled eventual negative effects determined by the blanching treatments.
� 2004 Elsevier Ltd. All rights reserved.
Keywords: Blanching; Colour; Dehydration; Potato; Rehydration
1. Introduction
In the production of canned, frozen and dehydrated
vegetables, the main purpose of a blanching treatment
is the inactivation of enzymes such as polyphenoloxid-ases, responsible for browning (Mapson, Swain, &
Tomalin, 1963; Collins & McCarty, 1969), peroxidase,
catalase and phenolase which leads to the development
of off-flavours (Pinsent, 1962; Bizzarri, Andreotti, &
Massini, 1981). In particular, thanks to their heat resis-
tance or regeneration capacity, peroxidase, catalase and
phenolase are considered as indices of the heat treatment
efficacy. Among them, peroxidase is the most heat resis-tant. Smith (1977) found that it is necessary to per-
formed a blanching treatment at 100 �C for 3 min, to
obtain its complete inactivation in cubed potatoes des-
tined for dehydration. Bizzarri et al. (1981) obtained
the complete and irreversible inactivation of peroxidase
by blanching potatoes for 4 min at 97 �C.
0260-8774/$ - see front matter � 2004 Elsevier Ltd. All rights reserved.
doi:10.1016/j.jfoodeng.2004.05.045
* Corresponding author. Tel.: +39 881 589242; fax: +39 881 740211.
E-mail address: [email protected] (A. Baiano).
Blanching can be performed by exposing vegetables
to hot water (the most common method), hot and boil-
ing solutions containing acids and/or salts, by steam
(Kidmose & Martens, 1999) or by microwaving product
dipped in water or solutions (Chen, Collins, McCarty, &Johnston, 1971; Ramaswamy & Van de Voort, 1990;
Ponne, Van Remmen, & Bartels, 1991; Severini, De Pilli,
Baiano, Mastrocola, & Massini, 2001) for several sec-
onds or minutes.
The effectiveness of a drying process depends on dif-
ferent factors: method of heat transfer, continuity or dis-
continuity of the process, direction of the heating fluids
with respect to the product, pressure (atmospheric, low,deep vacuum).
Dehydration can be performed by using different
kinds of equipment: air cabinet, belt drier, tunnel drier,
fluidized bed, spray drier, drum drier, foam drier,
freeze-drier, microwave oven. An interesting drying
method is represented by osmotic dehydration. Krokida,
Maroulis, and Saravacos (2001) investigated the effects of
different drying methods on the colour of the obtainedproducts. They found that colour characteristics are sig-
nificantly affected by the drying methods and that the
290 C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296
changes in redness (a*) and yellowness (b*) follow a first
order kinetic model. In particular, air-, vacuum and
microwave drying caused extensive browning in fruit
and vegetables with a decrease inL* value and an increase
in a* and b* values whereas freeze-drying improved col-
our characteristics. Osmotically pre-treated samples werepreserved from browning to a certain measure.
Drying methods also affect the behaviour of dehy-
drated product during rehydration. Krokida, Kiranou-
dis, and Maroulis (1999) and Krokida and Maroulis
(2000, 2001) studied the viscoelastic behaviour of
dehydrated products during rehydration. They found
that dehydrated foods do not keep their viscoelastic
behaviour after rehydration due to structural damagesthat occur during drying. Freeze-dried products
showed the highest hysteresis after rehydration, losing
their elasticity and becoming more viscous. Osmotic
pre-treatment helped freeze-dried materials to keep
their elastic nature probably thanks to the solid gain.
Air and vacuum dried foods showed the smallest hys-
teresis tendency, keeping their viscoelastic characteris-
tics during rehydration close to those of driedmaterials.
The purpose of this work was to study the effects of
different combined systems of blanching and dehydra-
tion on dehydration speed, colour characteristics and
the behaviour during rehydration of cubed potatoes.
2. Materials and methods
2.1. Raw material
Trials were performed on potato tubers (Solanum
tuberosum var. Primura) purchased at a local market.
This Italian variety, characterized by an early ripening
time, is the most commonly used in food industry
thanks to the regular shape and the good resistance tocooking of its big tubers.
2.2. Sample preparation
After grading, tubers were washed under running
water, wiped with blotting paper, hand-peeled and cut
into cubes (1 cm side).
2.3. Blanching
Blanching treatments were performed in four differ-
ent ways found as the optimal blanching conditions (in
terms of texture retention and enzyme inactivation) in
a previous screening:
� By immersion in a sodium-chloride solution (3%, w/w) at 98 �C for 5 min.
� By immersion in a corn syrup solution diluted to 70�Brix with distilled water and containing sodium-chlo-
ride (3%, w/w) at 100 �C for 5 min. The undiluted
corn syrup (commercial name ‘‘Glicosa’’, supplied
by Roquette Italia, Cassano Spinola, Italy) had the
following characteristics and chemical composition:refractometer grade 80.6� Brix, pH value 5.1 at 20
�C, 30% dextrose, 46% maltose, 10% trysaccharides,
14% polysaccharides.
� By microwaves in a domestic oven (De Longhi,
Milan, Italy) upon immersion in distilled water at
850 W for 5 min.
� By microwaves in a domestic oven (De Longhi,
Milan, Italy) upon immersion in a sodium-chloridesolution (3%, w/w) at 850 W for 5 min.
The product–solution ratio was always 1:5 (w/w).
After blanching, the samples were cooled in tap
water, drained and wiped with blotting paper.
Unblanched potato cubes were kept as controls.
2.4. Dehydration
Blanched and unblanched potato samples were sub-
mitted to three different methods of dehydration:
� in an air cabinet (I.S.C.O., Milan, Italy) at 100 �C;� in a microwave oven (De Longhi, Milan, Italy) at 85
W;
� in a monolayer on a concurrent belt drier (pilot plant,Sandvik Process Systems, Milan, Italy) at 100 �C.
During dehydration, samples were withdrawn at reg-
ular intervals (15 min) until the samples showed con-
stant weights.
2.5. Rehydration
The liquids used for rehydration trials were distilled
water and a vegetable stock obtained by dissolving
22 g of stock cubes in distilled water. Exactly weighed
potato cubes were dipped in the hot (initial tempera-
ture 80 �C) rehydration liquids (1:5 w/v ratio) for
0.5, 1, 2.5, 5, 7 and 10 min, recovered, drained and
weighed. Rehydration tests were also performed at room
temperature in water for 120 min with regular with-drawing.
2.6. Analyses
� Colour analysis: a tristimulus colorimeter (Chrom-
ameter-2 Reflectance, Minolta, Osaka, Japan)
equipped with a CR 300 measuring head was used.
Colour was expressed as L*, a* and b* (luminosity,red value and yellow value, respectively, on the Hun-
0
1
2
3
4
5
6
7
0 15 30 45 60 75 90 105120135150165180195 210225240255270285300315330345360375390405420Time (min)
W (g
H2O
/g d
ry m
atte
r) Air cabinet Microwave oven Belt drier
Fig. 1. Decrease in absolute moisture (g H2O/g dry matter) in
unblanced samples under different drying conditions as a function of
the dehydration time.
0.14
0.16Air cabinetMicrowave ovenBelt drier.
C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296 291
ter scale). The colorimeter was calibrated on a stand-
ard white tile (L*=93.5, a*=�1.0, b*=0.8) before
each series of measurements. For each samples, at
least five determinations were performed (coefficient
of variation less than 3% for L*, less than 45% for
a* and less than 48% for b*). Measurements were reg-ularly performed on samples withdrawn during dehy-
dration. The observer angle during colour analysis
was 90�.� Sample weight were measured using a balance Giber-
tini (mod. Europe 500, Milan, Italy). Determinations
were carried out in triplicate.
Kinetic constants (k) and correlation coefficients (r)were calculated from the linear regression on linear por-
tions of the curves using Excel 2002 software (Microsoft
Corporation, USA).
0
0.02
0.04
0.06
0.08
0.1
0.12
0 0.5 1 1.5 2 2.5 3 3.5 4
dW/d
t (g
H2O
/g d
ry m
atte
r*m
in)
W (g H2O/g dry matter)
Fig. 2. Dehydration speed of unblanced samples under different drying
conditions as a function of the absolute moisture.
3. Results and discussion
3.1. Drying speed
The kinetic constants reported in Table 1 show that
drying speeds were in the order: belt drier>microwave
oven>air cabinet, for all the considered samples.In particular, the time necessary to obtain complete
dehydration (absolute moisture <0.11 g H2O/g dry mat-
ter) of the unblanched cubed potatoes (Fig. 1) amounted
to 195 min for the belt drier, 210 min for the microwave
oven and 330 min for the air cabinet. For the un-
blanched samples, Fig. 2 reports the dehydration speed
as a function of the absolute moisture. The initial abso-
lute moisture amounted to about 3.95 g H2O/g drymatter corresponding to 78.5% of water content. The
graphical representation allows visualization of the
Table 1
Drying speed (k), expressed as g H2O/(g dry matter·min), correlation coeffic
systems (p) for the combined blanching–drying treatments
Drying methods Unblanched cubed
potatoes
Potatoes traditionally
blanched in the
NaCl solution
Po
bla
Gli
Air cabinet
k 0.019 0.021 0
r 0.998 0.998 0
p <0.001 <0.001 <0
Microwave oven
k 0.043 0.064 0
r 0.998 0.937 0
p <0.001 <0.01 <0
Belt drier
k 0.117 0.151 0
r 0.974 0.940 0
p <0.001 <0.01 <0
drying speed independently by the time of treatment.
During the first phase of drying (characterized by high
moisture level), remarkable differences in dehydration
ient (r) and significance as a function of the degrees of freedom of the
tatoes traditionally
nched in the
cosa–NaCl solution
Potatoes blanched
by microwaves in
distilled water
Potatoes blanched
by microwaves in
the NaCl solution
.012 0.021 0.016
.998 0.999 0.998
.001 <0.001 <0.001
.021 0.070 0.045
.993 0.952 0.988
.001 <0.001 <0.001
.078 0.228 0.185
.962 0.993 0.999
.05 <0.001 <0.001
292 C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296
speeds among the three drying methods were seen. At
the end of process, drying speeds, expressed as g H2O/
(g dry matter·min), were similar for the belt drier and
the microwave oven (about 0.02 g H2O/g of dry matter)
whereas the process performed in the air cabinet was
slower. From Fig. 2, it is well evident that drying speedin the air cabinet was constant over a large range of
absolute moisture.
For cubed potatoes blanched in sodium-chloride
solution, all the kinetic constants were higher than the
corresponding ones for to the unblanched samples
(Table 1). This behaviour was probably due to softening
by the blanching treatment which facilitated the water
removal. In the case of the belt drier, the time necessaryfor complete dehydration was equivalent to those for the
unblanched samples. However, dehydration in the air
cabinet and in the microwave oven was longer (405
and 210 min, respectively, Table 2). Considering drying
speed as a function of the absolute moisture (data not
shown), the trends were similar to those illustrated for
the unblanched potatoes.
For samples blanched in the Glicosa–NaCl solution,kinetic constants (Table 1) were lower than the corre-
sponding k for the unblanched samples and potatoes
blanched in NaCl solution. This behaviour was proba-
bly due to the blanching in the hypertonic solution
which caused enrichment in soluble solids and conse-
quent reduction in water activity.
Kinetic constants for drying of samples blanched by
microwaves were generally higher than the correspond-ing k values for the unblanched potatoes and the cubes
submitted to blanching by immersion in hot solutions.
In particular, kinetic constants for the dehydration of
samples blanched by microwaves in distilled water were
higher than the k values calculated for dehydration of
cubed potatoes blanched by microwaves in a hypertonic
(Glicosa–sodium-chloride) solution. Also in this case,
these differences were due to the enrichment in solublesolids that increased the bound water.
All the correlation coefficient values demonstrate the
goodness of fit.
3.2. Drying time
Table 2 reports the drying time required to reduce the
absolute moisture value below 0.25 g H2O/g dry matter
Table 2
Dehydration times for the combined blanching–drying treatments: dehydra
content equal to 0.25 g H2O/g dry matter
Drying time (min) Unblanched
cubed potatoes
Potatoes traditionally
blanched in the
NaCl solution
Pot
blan
Glic
Air cabinet 255 >405 255
Microwave oven 145 210 180
Belt drier 105 105 180
(i.e., an uncomplete dehydration). A good correlation is
evident among the kinetic constants (Table 1) and dry-
ing times is evident for drying performed on the belt
drier. Furthermore, dehydration performed by the belt
drier on samples previously blanched by microwaves
showed the greatest efficiency. However, dehydrationperformed by the air cabinet on the same types of sam-
ples was among the worst. This demonstrates that the
efficiency of the dehydration systems in terms of water
removal can compensate for the unfavourable effects
deriving from the presence of moistening substances in
the blanching solution.
3.3. Colour
Quality of potato cubes was evaluated during drying
through colour measurements. The average results of
the colour measurements performed on the raw potatoes
were the following: L* 52.55, a* �1.87, b* 15.84. Table 3
is a summary of the speeds of colour changes and re-
ports the kinetic constants calculated from the trends
in L*, a* and b* values during dehydration for all theconsidered samples. For unblanched potatoes, those
dried by microwave oven browned faster than the oth-
ers. The slowest browned cubes were those dried on
the belt drier. In fact, as is evident from data reported
in Table 3, L* kinetic constants were negative, indicating
a decrease in luminosity whereas a* and b* increased to
indicate an increase in the red and yellow value, respec-
tively. The increase in a* and b* values are indicesof Maillard reaction (Morales & van Boekel, 1998;
Carabasa-Giribet & Ibarz-Ribas, 2000). The better re-
sults obtained by the belt drier can be explained in the
following way: the potato cubes were brought faster
than the others to temperatures unfavourable to the ac-
tivity of enzyme responsible for browning; furthermore,
these temperatures were not high enough to induce non-
enzymatic browning (Maillard reaction).The colour of cubes blanched in the sodium-chloride
solution did not undergo great changes during drying
process (Table 3) with the exception of the b* value
which increased (higher yellow value) probably due to
the loss of water and the consequent colour concentra-
tion. It could be taken as an index of the start of
the Maillard reaction (Morales & van Boekel, 1998;
Carabasa-Giribet & Ibarz-Ribas, 2000).
tation was prolonged until the samples reached an absolute moisture
atoes traditionally
ched in the
osa–NaCl solution
Potatoes blanched
by microwaves in
distilled water
Potatoes blanched
by microwaves in
the NaCl solution
>360 325
240 240
85 75
Table 3
Speed of colour changes (k), expressed as colour parameter per min and correlation coefficient (r) for the combined blanching–drying treatments
Drying methods Unblanched cubed
potatoes
Potatoes traditionally
blanched in the NaCl
solution
Potatoes traditionally
blanched in the
Glicosa–NaCl
solution
Potatoes blanched by
microwaves in distilled
water
Potatoes blanched by
microwaves in the
NaCl solution
L* a* b* L* a* b* L* a* b* L* a* b* L* a* b*
Air cabinet
k �0.032 0.015 1·10�5 �0.010 0.005 0.052 �0.021 0.008 0.046 �0.010 0.005 0.052 �0.021 0.004 0.046
r 0.489 0.844 2·10�7 0.286 0.619 0.887 0.334 0.711 0.585 0.286 0.619 0.876 0.311 0.400 0.698
Microwave oven
k �0.118 0.024 0.030 �0.032 0.023 0.043 �0.053 0.025 0.006 �0.032 0.023 0.043 �0.040 0.011 0.054
r 0.777 0.828 0.612 0.371 0.868 0.588 0.542 0.886 0.065 0.371 0.868 0.588 0.212 0.707 0.737
Belt drier
k �0.002 0.011 0.009 �0.031 0.023 0.069 �0.027 0.022 0.018 �0.031 0.023 0.069 �0.071 0.030 0.093
r 0.028 0.767 0.272 0.467 0.887 0.721 0.472 0.852 0.248 0.467 0.887 0.721 0.560 0.977 0.714
Fig. 3. Increase in weight (g/100 g dry matter) in unblanched samples
as a function of the rehydration time in hot liquids.
C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296 293
In the case of samples blanched in the Glicosa–NaCl
solution, those dried by microwave oven browned faster
than the others (greater loss of luminosity and higher
red value, Table 3) probably due to the effects of micro-
waves on a higher solute concentration.
In samples blanched by microwaves (independently
by the kind of blanching solution), kinetic constants
for the b* index showed the greatest values and indicatea beginning of the Maillard reaction.
For all the considered samples, low correlation coef-
ficients were low. These low values could be explained in
terms of a very little dependence of the colour parame-
ters from the dehydration time.
3.4. Rehydration
After dehydration, samples were submitted to rehy-
dration trials to check their capability to rehydrate in
liquids of different nature. Rehydration in hot liquids
was carried out for only 10 min to avoid cooking the po-
tato. For the same reason, the temperature of the liquids
was not kept at 80 �C for all the time but decreased as a
result of both the addition of potato cubes and the lack
of heating. From Figs. 3–7, which report the rehydra-tion curves of all the samples, it is evident that potato
cubes absorbed more liquid if rehydrated in distilled
water rather than in vegetable stock. This behaviour
was probably due to the slower diffusion in the inner po-
tato cubes of liquid containing soluble solids and a fat
fraction. Furthermore, the behaviour of samples during
reconstitution was different depending on the drying
method to which they where submitted.Fig. 3 shows the increase in weight of unblanched
samples during rehydration. Potato cubes dehydrated
in the air cabinet and by microwaves had a slower rehy-
dration than samples dehydrated on the belt drier. The
latter absorbed a quantity of liquid amounting to about
100% of their weight during the first minute of immer-
sion and, by the end of the rehydration, they had ab-
sorbed the highest quantity of liquid compared to the
other samples.
These differences were amplified in the case of sam-
ples blanched in the sodium-chloride solution (Fig. 4).
Potato cubes dehydrated on the belt drier acquired after10 min a quantity of liquid (water or vegetable stock)
amounting to about 200% of their dry matter whereas
samples dehydrated in the air cabinet and by micro-
waves absorbed liquid amounting 50% and 100% of
their dry matter, respectively.
Fig. 6. Increase in weight (g/100 g dry matter) in samples blanched by
microwaves in distilled water as a function of the rehydration time in
hot liquids.
Fig. 5. Increase in weight (g/100 g dry matter) in samples traditionally
blanched in the glicosa–Nacl solution as a function of the rehydration
time in hot liquids.Fig. 7. Increase in weight (g/100 g dry matter) in samples blanched by
microwaves in the NaCl solution as a function of the rehydration time
in hot liquids.
Fig. 4. Increase in weight (g/100 g dry matter) in samples traditionally
blanched in the NaCl solution as a function of the rehydration time in
hot liquids.
294 C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296
Samples blanched in the Glicosa–sodium-chloride
solution showed slower rehydration kinetics and ac-
quired the smallest quantity of liquid (Fig. 5). This
behaviour was probably due to the acquisition of
soluble solids during the blanching, which resulted in a
decrease in porosity. The effect of the blanching treat-
ment minimized the differences due to the drying
methods.
Table 4
Rehydration time in distilled water at room temperature for the combined blanching–drying treatments
Rehydration time (min) Unblanched
cubed potatoes
Potatoes traditionally
blanched in the
NaCl solution
Potatoes traditionally
blanched in the
Glicosa–NaCl solution
Potatoes blanched by
microwaves in distilled
water
Potatoes blanched by
microwaves in the
NaCl solution
Air cabinet 70 >120 95 >120 >120
Microwave oven >120 >120 >120 >120 >120
Belt drier >120 >120 85 90 38
C. Severini et al. / Journal of Food Engineering 68 (2005) 289–296 295
Fig. 6 shows the rehydration curves of samples
blanched by microwaves in distilled water. In this
case, microwaves induced a modification of the starch
granules whose capacity to absorb liquid during rehy-
dration was increased, according to the results repor-
ted by Sikora, Tomasik, and Pielichowski (1997). Thiseffect was particularly evident in samples dehydrated
on the belt drier which absorbed liquids amounting to
about 300% of their dry matter. Among samples
blanched by microwaves in distilled water, those show-
ing the worse behaviour during rehydration were those
dehydrated by microwaves. This can be explained
considering that these samples were treated (blanched
and de-hydrated) exclusively by microwaves whichdetermined the complete starch gelatinization and, con-
sequently, the minor water holding capacity during re-
hydration.
Potato cubes blanched by microwaves in the sodium-
chloride solution showed a behaviour similar to those
blanched by microwaves in distilled water during rehy-
dration (Fig. 7) even if the effects of microwaves were re-
duced by the presence of salt.Table 4 reports the time of rehydration in distilled
water at room temperature necessary to bring samples
to their natural water content. From this point of view,
samples showing the best results were those blanched by
microwaves in the sodium-chloride solution and succes-
sively dehydrated on the belt drier. The other samples
needed double or triple rehydration times.
4. Conclusions
Dehydration performed by the air cabinet was the
slowest and did not yield, within the first phase of rehy-
dration at least, a satisfying water holding capacity.
Dehydration by microwaves gave a good drying
speed coupled to a good water holding capacity and col-our retention. Nevertheless, a blanching-drying process
totally carried out by microwaves would be too expen-
sive.
Dehydration performed on the belt drier was the
most effective both for speed and water absorption dur-
ing rehydration, independently of the kind of blanching.
In terms of process speed and quality (colour and re-
hydration capability) of the obtained samples, the best
combinations were by the blanching by microwaves cou-
pled to dehydration on the belt drier.
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