Appendix D Data Validation - King County

LowerDuwamishWaterwaySourceControl:BrandonCombinedSewerBasinStudy

KingCountyScienceandTechnicalSupportSection May 2016

Appendix D

Data Validation

D-1: Validation of Data Generated by King County Environmental Laboratory

D-2: Validation of Data Generated by AXYS Analytical Laboratory



Appendix D-1: Validation of Data Generated by King

County Environmental Laboratory

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Technical Memorandum

Date: August 10, 2012; Revised - February 10, 2015

To: Dean Wilson, King County Toxicology and Contaminant Assessment Group Debra Williston, King County Toxicology and Contaminant Assessment Group

From: Scott Mickelson, King County Marine and Sediment Assessment Group Carly Greyell, King County Toxicology and Contaminant Assessment Group

Subject: Data Validation Report Brandon CSO Study Dry Weather Baseflow Samples - Fall 2011

This technical memorandum summarizes the data validation review performed on 18 dry weather baseflow samples collected from within the Brandon combined sewer overflow (CSO) basin between September 13 and November 1, 2011. The sampling and analysis of these samples are specified in the project sampling and analysis plan (SAP) Lower Duwamish Waterway Source Control, Brandon Combined Sewer Basin Study, Sampling and Analysis Plan (King County 2011). The 18 samples were submitted for analysis of polycyclic aromatic hydrocarbons (PAHs), phthalates, total and dissolved organic carbon (TOC and DOC), total suspended solids (TSS), and total and dissolved metals. The data validation for PAHs and phthalates was revised based on re-analysis of detection limits for these compounds by the King County Environmental Laboratory. The specifics of the re-analysis are described in laboratory data anomaly forms (DAFs).

1.0 INTRODUCTION

This data validation review has been based, in part, on guidance found in USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review (EPA 2014) and USEPA Contract Laboratory Program National Functional Guidelines for Inorganic Superfund Data Review (EPA 2010), as well as the project SAP (King County 2011). Materials reviewed included Batch Reports and Analytical Quality Control (QC) Reports downloaded from the King County Laboratory Information Management System (LIMS) database, which are attached to this memorandum. Also reviewed were DAFs, which are available upon request. The QC parameters reviewed during this data validation include holding time, method blanks, spike blanks, spike blank duplicates, matrix spikes, matrix spike duplicates, laboratory control samples, laboratory duplicates, and surrogates, which are described below.

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1.1 Holding Time The analytical holding time is a method-specific timeframe, during which sample preparation and analysis should occur to provide valid data. All samples should be analyzed within this prescribed holding time. 1.2 Method Blank A method blank is an aliquot of clean reference matrix that is generally processed through the entire analytical procedure. Analysis of the method blank is used to evaluate the levels of contamination that might be associated with the processing and analysis of samples. Method blanks were used during all analyses. All method blank results should be less than the method detection limit (MDL). 1.3 Spike Blanks and Spike Blank Duplicates A spike blank is an aliquot of the clean reference matrix used for the method blank, to which a known concentration of target analyte(s) has been added. The spiked aliquot is processed through the entire analytical procedure. Analysis of the spike blank is used as an indicator of method accuracy. Spike blanks were used during PAH/phthalate, metals, and TOC/DOC analyses. Spike blanks are not addressed in the National Functional Guidelines; however, King County has empirically-derived control limits for spike blank analytes, which are shown on the attached QC reports. Spike blank results should be within these control limits. Spike blanks were run in duplicate for most organic analyses, due to a lack of other QC samples that could assess method precision. The RPD between spike blank duplicate results for organic analyses should be less than the 40% QC limit. 1.4 Matrix Spike A matrix spike is a sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Analysis of the matrix spike is used as an indicator of sample matrix effect on the recovery of target analyte(s). Matrix spikes were used during metals and TOC/DOC analyses. Control limits for organic carbon are not addressed in the National Functional Guidelines; however, King County has empirically-derived control limits for percent recoveries of these matrix spike analytes, which are shown on the attached QC reports. Matrix spike recoveries should be within these control limits. Control limits for metals matrix spike recoveries are addressed in the National Functional Guidelines. All trace metal matrix spike recoveries should be within the 75 to 125% control limits for all analytes (EPA 2010). 1.5 Matrix Spike Duplicate A matrix spike duplicate is a second sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Analysis of the matrix spike duplicate is used as an additional indicator of sample matrix effect on the recovery of target analyte(s) as well as an indicator of method precision. Matrix spike duplicates were used during mercury analysis. The relative percent difference (RPD) between matrix spike and matrix spike duplicate results should be less than 20% (EPA 2010).

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1.6 Laboratory Control Sample A laboratory control sample is a sample of known analyte concentration(s) that is prepared in the lab from a separate source of analyte(s) relative to the calibration standards. Since the laboratory control sample analysis should follow the entire analytical process, it should be stored and prepared following the same procedures as a field sample. Analysis of a laboratory control sample is used as an indicator of method accuracy and long-term analytical precision. Laboratory control samples were used during TOC/DOC and TSS analyses. King County used percent recovery control limits of 85 to 115% for TOC/DOC analysis and 80 to 120% for TSS analysis on this project. Percent recoveries for laboratory control sample results should be within these control limits. 1.7 Laboratory Duplicate A laboratory duplicate is a second aliquot of a sample, processed concurrently and in an identical manner with the original sample. Analysis of the laboratory duplicate is used as an indicator of method precision and laboratory subsampling procedures. The laboratory duplicate can also be used to provide information regarding the homogeneity of the sample matrix. Laboratory duplicates were used during TOC/DOC, TSS, ICPMS metals, and organic analyses. QC results are reported as an RPD between the sample and laboratory duplicate results. Control limits for conventional analyses are also not addressed under the National Functional Guidelines. King County used RPD control limits of 20% for TOC/DOC analysis and 25% for TSS analysis. The RPD for laboratory duplicate results should be below these control limits. Control limits for ICPMS laboratory duplicates are addressed in the National Function Guidelines. The RPD between all trace metal laboratory duplicate results should be below 20% (EPA 2010). King County used an RPD of 40% for this project as the RPD QC limit between laboratory duplicate results during organic analyses. Laboratory duplicate RPD results for samples in which the concentration is less than the reporting detection limit (RDL) will not be qualified based solely on whether the RPD is greater than the QC limit. This is based on the inherent analytical variability between the MDL and RDL, which is the limit of practical quantitation. 1.8 Surrogates A surrogate is a known concentration of non-target analyte which is added to each sample (both analytical and QC samples) prior to extraction and analysis for all trace organic analyses. Surrogate recovery is used as a sample-specific indication of method or matrix bias for target analytes. The surrogate is selected to behave in a similar manner to the target analytes.

The King County Environmental Laboratory used two surrogate compounds during analysis of trace organic compounds, 2-fluorobiphenyl and d14-terphenyl. King County has empirically-derived laboratory QC control limits for surrogate recoveries, which are 40 – 160%. Surrogate recoveries for all analytical and QC samples should be within these control limits. These two surrogate compounds are not addressed in National Functional Guidelines.

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2.0 CONVENTIONALS

Conventional analytes included total suspended solids and total and dissolved organic carbon. LIMS batch and analytical QC reports for conventional analyses are included as an attachment to this memorandum.

2.1 Total Suspended Solids Eighteen water samples were submitted for TSS analysis by gravimetric determination following Standard Method SM2540-D (APHA 1998). The samples were batched into the nine workgroups shown in Table 2-1. Each workgroup included analysis of a minimum of three QC samples; method blanks, laboratory control samples, and laboratory duplicates.

Table 2-1 TSS Workgroups and QC Samples

Workgroup Samples MB LCS LD WG117427 L54126-1, L54126-3, L54154-2, L54154-3 WG117585 L54174-2 WG117708 L54307-1, L54307-2, L54307-3 WG118100 L54454-1, L54454-2, L54454-3 WG118101 L54455-2, L54455-3 WG118160 L54488-2, L54488-3 WG118247 L54531-1 WG118281 L54532-1 WG118384 L54591-1

2.1.1 Holding Time All 18 TSS samples were analyzed within the prescribed 7-day holding time.

2.1.2 Method Blank Results TSS results in the method blanks associated with all nine workgroups were less than the MDL.

2.1.3 Laboratory Control Sample Results TSS recoveries in the laboratory control samples associated with all nine workgroups were within the 80 to 120% QC limits.

2.1.4 Laboratory Duplicate Results The RPDs between TSS laboratory duplicate results in all nine workgroups were less than the 25% QC limit.

2.2 Total and Dissolved Organic Carbon Eighteen water samples were submitted for TOC/DOC analysis by Standard Method SM5310-B (APHA 1998), which is a high-temperature combustion/infrared detection method. The samples were batched into the five workgroups shown in Table 2-2. Each workgroup included analysis of a minimum of five QC samples; method blanks, spike blanks, laboratory control samples, matrix spikes, and laboratory duplicates. Note that some samples appear twice in Table 2-2, when TOC and DOC analyses for the samples were split into two workgroups.

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Table 2-2 Total and Dissolved Organic Carbon Workgroups and QC Samples

Workgroup Samples MB SB LCS MS LD WG117545 L54126-1, L54126-3, L54154-2, L54154-3 WG117810 L54174-2, L54307-1, L54307-2, L54307-3

WG118166 L54454-1, L54454-2, L54454-3, L54455-2, L54455-3, L54488-2, L54488-3,

WG118427 L54531-1, L54532-1, L54591-1 WG117769 L54174-2, L54307-1, L54307-2, L54307-3

2.2.1 Holding Time All 18 TOC/DOC samples were analyzed within the prescribed 28-day holding time.

2.2.2 Method Blank Results TOC and DOC results in the method blanks associated with all five workgroups were less than the MDL. 2.2.3 Spike Blank Results The spike blank recoveries for TOC and DOC in each of the five workgroups were all within the laboratory QC limits of 80 to 120%. 2.2.4 Laboratory Control Sample Results TOC and DOC recoveries in the laboratory control samples associated with each of the five workgroups were all within the 85 to 115% QC limits. 2.2.5 Matrix Spike Results TOC and DOC matrix spike recoveries in each of the five workgroups were all within the 75 to 125% QC limits. 2.2.6 Laboratory Duplicate Results The RPD between TOC and DOC laboratory duplicate results in each of the five workgroups were all less than the 20% QC limit. 2.2.7 Sample Contamination Issue Acetone was originally employed to rinse the Teflon tubing associated with the autosamplers used to collect these samples, as part of the pre-sampling equipment decontamination procedure. This procedure; however, was shown to affect TOC/DOC results by returning false positives in field and equipment blanks (King County 2013). This procedure was discontinued subsequent to the collection of the first eight dry-weather baseflow samples. All TOC and DOC results for samples L54126-1, L54126-3, L54154-2, L54154-3, L54174-2, L54307-1, L54307-2, and L54307-3 should be qualified with a “J” flag and considered estimated with a high bias.

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3.0 TRACE METALS

Eighteen water samples were submitted for analysis of total metals and 16 samples were submitted for analysis of dissolved metals, which included mercury and other trace metals. LIMS batch and analytical QC reports for metals analyses are included as an attachment to this memorandum.

3.1 Total and Dissolved Mercury Total and dissolved mercury analysis was performed using cold vapor atomic absorption spectroscopy (CVAA) according to EPA Method 245.1 (EPA1994). The 18 samples for total mercury and 16 samples for dissolved mercury were batched into the three workgroups shown in Table 3-1. Each workgroup included analysis of a minimum of five QC samples; method blanks (for both total and dissolved mercury), spike blanks, matrix spikes, and matrix spike duplicates.

Table 3-1 Total and Dissolved Mercury Workgroups and QC Samples

Workgroup Samples MB SB MS MSD

WG117735 L54126-1, L54126-3, L54154-2, L54154-3, L54174-2, L54307-1, L54307-2, L54303-3

WG118289 L54454-1, L54454-2, L54454-3, L5455-2, L5455-3, L5488-2, L54488-3, L54531-1, L54532-1

WG118686 L54591-1

3.1.1 Holding Time All 18 total mercury samples and 16 dissolved mercury samples were analyzed within the prescribed 28-day holding time.

3.1.2 Method Blank Results Both total and dissolved mercury results in the method blanks associated with each workgroup were all less than the MDL.

3.1.3 Spike Blank Results Mercury spike blank recoveries in all three workgroups were within the laboratory QC limits of 85 to 115%.

3.1.4 Matrix Spike Results Mercury matrix spike recoveries in all three workgroups were within the 75 to 125% QC limits.

3.1.5 Matrix Spike Duplicate Results Mercury matrix spike duplicate recoveries in all three workgroups were within the 75 to 125% QC limits. The RPDs between matrix spike and matrix spike duplicate recoveries in all three workgroups were below the 20% QC limit.

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3.1.6 Sample Handling Issue All dissolved mercury samples were filtered outside of the method-specified 15-minute holding time. As a result, all dissolved mercury results should be qualified with a “J” flag and considered estimated with an unknown bias.

3.2 Total ICP-MS Metals Total metals, including arsenic, cadmium, chromium, copper, lead, nickel, silver, vanadium, and zinc, were analyzed by inductively coupled plasma mass spectroscopy (ICP-MS) following EPA Methods 200.8/6020A SW846 (EPA 1995). The samples were batched into the five workgroups shown in Table 3-2. Routine QC included analysis of method blanks, spike blanks, matrix spikes, and laboratory duplicates.

Table 3-2 Total ICP-MS Metals Workgroups and QC Samples

Workgroup Samples MB SB MS LD WG117467 L54126-1, L54126-3, L54154-2, L54154-3 WG117595 L54174-2 WG117692 L54307-1, L54307-2, L54307-3 WG118112 L54454-2, L54454-2, L54454-3, L54455-2, L54455-3 WG119368 L54488-2, L54488-3, L54531-1, L54532-1, L54591-1

3.2.1 Holding Time All 18 total metal samples were analyzed within the prescribed 6-month holding time.

3.2.2 Method Blank Results Results for each total metal in the method blank associated with each workgroup were all less than the MDL.

3.2.3 Spike Blank Results All total metal spike blank recoveries in each of the five workgroups were within the 85 to 115% QC limits.

3.2.4 Matrix Spike Results All total metal matrix spike recoveries in each of the five workgroups were within the 75 to 125% QC limits.

3.2.5 Laboratory Duplicate Results RPDs total metal laboratory duplicate results in all five workgroups were below the 20% QC limit.

3.2 Dissolved ICP-MS Metals Dissolved metals, including arsenic, cadmium, chromium, copper, lead, nickel, silver, vanadium, and zinc, were analyzed by inductively coupled plasma mass spectroscopy (ICP-MS) following EPA Methods 200.8/6020A SW846 (EPA 1995). The samples were batched into the four workgroups shown in Table 3-3. Routine QC included analysis of method blanks, spike blanks, matrix spikes, and laboratory duplicates.

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Table 3-3 Dissolved ICP-MS Metals Workgroups and QC Samples

Workgroup Samples MB SB MS LD WG117646 L54174-2 WG118036 L54126-3, L54154-3, L54307-1, L54307-2, L54307-3

WG118171 L54454-1, L54454-2, L54454-3, L5455-2, L5455-3, L5488-2, L5488-3

WG119371 L54531-1, L54532-1, L54591-1 3.3.1 Holding Time All 16 dissolved metal samples were analyzed within the prescribed 6-month holding time. 3.3.2 Method Blank Results Results for each dissolved metal in the method blank associated with each workgroup were all less than the MDL. 3.3.3 Spike Blank Results All dissolved metal spike blank recoveries in each of the five workgroups were within the 85 to 115% QC limits. 3.3.4 Matrix Spike Results All dissolved metal matrix spike recoveries in each of the five workgroups were within the 75 to 125% QC limits. 3.3.5 Laboratory Duplicate Results The RPD of 31% between laboratory duplicate results for nickel in workgroup WG118036 exceeded the QC limit of 20%. Both the sample and laboratory duplicate results were less than the RDL; however, so data will not be qualified based solely on this QC failure. RPDs for all other dissolved metal laboratory duplicate results were below the 20% QC limit. 3.3.6 Sampling Handling Issue All dissolved ICP-MS metals samples were filtered outside of the method-specified 15-minute holding time. As a result, all detected dissolved ICP-MS metals results should be qualified with a “J” flag and considered estimated with an unknown bias

4.0 TRACE ORGANICS

Eighteen water samples were submitted for analysis of PAH compounds and phthalates by gas chromatography mass spectroscopy (GC-MS) following EPA Methods 3520C/8270D – SW846 (EPA 1995). The instrument method was modified by the use of a large volume injector (LVI) and analysis using selected ion monitoring (SIM). The samples were batched into the six workgroups shown in Table 4-1. Routine QC included analysis of method blanks, spike blanks, spike blank duplicates, laboratory duplicates and surrogates. Due to insufficient sample volume, laboratory duplicates were not analyzed in association with workgroups WG117625, WG118307, and WG118436. Spike blank duplicates were not analyzed in association with workgroups WG117625 or WG118307. The project sampling and analysis plan (King County

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2011) prescribed the analysis of a matrix spike with each QC batch; however, due to insufficient sample volume, spike blanks were run instead. LIMS batch and analytical QC reports for PAH/phthalate analysis are included as an attachment to this memorandum.

Table 4-1 PAH/Phthalate Workgroups and QC Samples

Workgroup Samples MB SB SBD LD Surr. WG117498 L54126-1, L54126-3, L54154-2, L5415403 WG117625 L54174-2 WG117764 L54307-1, L54307-2, L54307-3

WG118172 L54454-1, L54454-2, L54454-3, L54455-2, L54455-3, L54488-2, L54488-3

WG118307 L54531-1, L54532-1 WG118436 L54591-1

4.1 Holding Time All 18 samples were extracted within the 7-day holding time and analyzed within the subsequent 40-day holding time. 4.2 Method Blank Results Between six and nine PAH and phthalate compounds were detected in every method blank associated with this data set. More than half the positive PAH and phthalate method blank results were detected at concentrations greater than the reporting detection limit (RDL), which is the limit of practical quantitation. Based on the recommendations in National Function Guidelines (EPA 2014), the following data qualification regime should be employed as a result of method blank contamination:

• When the compound is detected in the method blank and the sample concentration is less than the RDL, the sample value should be reported as the numeric RDL value and the result should be qualified with a “U” flag and considered undetected.

• When the method blank concentration is greater than the MDL and the sample concentration is greater than the RDL but less than five times the method blank concentration, the sample value should be used as reported but the result should be qualified with a “U” flag and considered undetected.

• When the method blank concentration is greater than the MDL and the sample concentration is greater than the RDL and greater than five times the method blank concentration, the sample result may be used as reported, without qualification.

4.3 Spike Blank and Spike Blank Duplicate Results The bis(2-ethylhexyl) phthalate recovery of 197% in the spike blank duplicate associated with workgroup WG117498 exceeded the upper QC limit of 160%. The bis(2-ethylhexyl) phthalate recovery of 110% in the spike blank associated with the same workgroup; however, was within the 40 to 160% QC limits and the RPD of 36% between spike blank and spike duplicate results was below the QC limit of 40%. Since the average between the primary and duplicate results

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was also within the QC limits, bis(2-ethylhexyl) phthalate sample data associated with workgroup WG117498 will not be qualified based on spike blank results.

The bis(2-ethylhexyl) phthalate recoveries of 9% and 28%, respectively, in the spike blank and spike blank duplicate associated with workgroup WG118172 were both below the lower QC limit of 40%, and the RPD between spike blank and spike duplicate results was within the QC limit of 40%. The detected bis(2-ethylhexyl) phthalate results in associated samples should be qualified with a “J” flag, with a low bias.

Spike blank recoveries of 384% for di-N-butyl phthalate, 176% for benzyl butyl phthalate, and 264% for bis(2-ethylhexyl) phthalate in workgroup WG118307 all exceeded the upper QC limit of 160%. Detected results of di-N-butyl phthalate, benzyl butyl phthalate, and bis(2-ethylhexyl) phthalate in the associated samples (L54531-1 and L54532-1) should be qualified with a “J” flag, with a high bias due to spike blank results; however, the lack of precision data for this workgroup results in an unknown bias for all results (See Section 4.6).

Bis(2-ethylhexyl) phthalate spike blank and spike blank duplicate recoveries of -171 and -140%, respectively, were reported for workgroup WG118436. These negative recoveries are an artifact of the spike blank recovery calculation and an elevated concentration of bis(2-ethylhexyl) phthalate in the method blank, relative to the spiking concentration. The bis(2-ethylhexyl) phthalate result in sample L54591-1 should be qualified with a “J” flag, with a low bias, as corroborated by the surrogate results for this sample.

All other spike blank and spike blank duplicate recoveries were within the QC limits of 40 to 160% and the RPDs between recoveries were all below the 40% QC limit. 4.4 Laboratory Duplicates A total of three laboratory duplicates were analyzed in association with the 18 samples in this dataset. The RPD of 51% between laboratory duplicate results for phenanthrene in the laboratory duplicate analyzed with workgroup WG118172, exceeded the QC limit of 40%. The phenanthrene result in sample L54454-1 should be qualified with a “J” flag, with an unknown bias. All other laboratory duplicate RPD results were less than the 40% laboratory QC limit. 4.5 Surrogates Recoveries of the surrogate 2-fluorobiphenyl in all analytical and QC samples in all seven workgroups were within the 40 to 160% QC limits. Recoveries of the other surrogate, d4-terphenyl, were below the lower QC limit of 40% in 15 of 18 samples. In three of those samples, a recovery of 0% was reported for d4-terphenyl. Non-matrix-specific QC samples (i.e., method blanks and spike blanks) returned d4-terphenyl recoveries that were within the 40 to 160% QC limits, indicating that there was some matrix suppression on the d4-terphenyl recovery. This surrogate is associated with the following target analytes; benzo(a)anthracene, chrysene, pyrene, benzyl butyl phthalate, bis(2-ethylhexyl) phthalate, di-n-butyl phthalate and fluoranthene. Based on all surrogate recoveries, sample results for these five compounds should be qualified with the following flags:

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• For samples L54126-3, L54307-1, L54307-3, L54454-1, L54454-2, L54454-3, L54455-2, L54455-3, L54488-3, L54531-1, L54532-1, and L54591-1: qualify detected sample results with a “J” flag and consider the results as estimated with a low bias; qualify undetected sample results with a “UJ” flag.

• For samples L54126-1, L54154-2, and L54154-3: qualify detected sample results with a “J” flag and consider the results as estimated with a very low bias; qualify undetected sample results with a “R” flag and consider the data rejected.

4.6 Lack of Precision Quality Control Information Two workgroups, WG117625 and WG118307, included no precision QC samples. As a result, samples L54174-2, L54531-1, and L54532-1 should be flagged as follows: all detected values should be qualified with a “J” flag and considered estimated with an unknown bias and all undetected results should be qualified with a “UJ” flag.

5.0 DATA USABILITY

As a general data reporting format, conventional parameters, total and dissolved metals, and organics sample results that are reported as “<MDL” should be assigned a “U” flag in all cases and considered undetected; any results also flagged with a “J” should be assigned a “UJ” flag. Conventional, total and dissolved metals, and organics sample results that are reported as “<RDL” should be assigned a “J” flag in all cases and considered estimated with an unknown bias. Table 1 at the end of this narrative provides any additional data qualifier flags, if required, for every sample/analyte in this data set. These flags are based on the data quality issues summarized in Sections 2.0, 3.0, and 4.0. LIMS Batch and QC reports are included as Attachment A.

6.0 REFERENCES

APHA 1998. Standard Methods for the Examination of Water and Wastewater, 20th Edition. American Public Health Association. Washington, D.C.

EPA 1994. Determination of Mercury in Water by Cold Vapor Atomic Absorption Spectrometry. EPA Method 245.1, Revision 3.0. U.S. Environmental Protection Agency, Office of Research and Development. Cincinnati, Ohio.

EPA 1995. Determination of Trace Elements in Waters and Wastes by Inductively Coupled Plasma – Mass Spectrometry. Method 200.8, Revision 5.4. United States Environmental Protection Agency, Office of Research and Development. Cincinnati, Ohio.

EPA 2007. Test Methods for Evaluating Solid Waste. Laboratory Manual – Physical/Chemical Methods, SW-846, 3rd Edition, Update IVB. United State Environmental Protection Agency, Office of Solid Waste and Emergency Response. Washington, D.C.

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EPA 2010. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Inorganic Data Review. OSWER 9240.1-51, USEPA-540-R-10-011. United States Environmental Protection Agency. Washington, D.C. January 2010. EPA 2014. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review. OSWER 9355.0-132, EPA-540-R-014-002. USEPA. Washington, D.C. August 2014.

King County 2011. Lower Duwamish Waterway Source Control, Brandon Combined Sewer Basin Study, Sampling and Analysis Plan. King County Department of Natural Resources and Parks. Seattle, Washington.

King County 2013. Personal communication from Colin Elliott, QA Officer, King County Environmental Laboratory, September 16, 2013. Seattle, Washington.

Table 1. Brandon CSO Dry Baseflow Samples - Data Validation Flags and Bias Notation

May 2016 1 of 9 Appendix D: Brandon Combined Sewer Basin Study

WORKGROUP LOCATOR COLLECTDATE SAMPLE ID PARMNAME NUMVALUE UNITS Lab QualDV

ValueDV

QualBias MDL RDL

WG117545 A01007 9/13/2011 L54126-1 Dissolved Organic Carbon 157 mg/L TA 157 J high 5 10WG117545 BRANDUTAH 9/13/2011 L54126-3 Dissolved Organic Carbon 75.5 mg/L TA 75.5 J high 5 10WG117545 BRANDREG 9/14/2011 L54154-2 Dissolved Organic Carbon 322 mg/L TA 322 J high 5 10WG117545 BRANDUTAH 9/14/2011 L54154-3 Dissolved Organic Carbon 93.8 mg/L TA 93.8 J high 5 10WG117810 BRANDREG 9/21/2011 L54174-2 Dissolved Organic Carbon 226 mg/L TA 226 J high 5 10WG117810 A01007 9/28/2011 L54307-1 Dissolved Organic Carbon 868 mg/L TA 868 J high 18 35WG117810 BRANDREG 9/28/2011 L54307-2 Dissolved Organic Carbon 193 mg/L TA 193 J high 5 10WG117810 BRANDUTAH 9/28/2011 L54307-3 Dissolved Organic Carbon 102 mg/L TA 102 J high 5 10WG117545 A01007 9/13/2011 L54126-1 Total Organic Carbon 513 mg/L TA 513 J high 50 100WG117545 BRANDUTAH 9/13/2011 L54126-3 Total Organic Carbon 138 mg/L TA 138 J high 50 100WG117545 BRANDREG 9/14/2011 L54154-2 Total Organic Carbon 463 mg/L TA 463 J high 50 100WG117545 BRANDUTAH 9/14/2011 L54154-3 Total Organic Carbon 159 mg/L TA 159 J high 50 100WG117769 BRANDREG 9/21/2011 L54174-2 Total Organic Carbon 259 mg/L TA 259 J high 18 35WG117769 A01007 9/28/2011 L54307-1 Total Organic Carbon 972 mg/L TA 972 J high 50 100WG117769 BRANDREG 9/28/2011 L54307-2 Total Organic Carbon 251 mg/L TA 251 J high 18 35WG117769 BRANDUTAH 9/28/2011 L54307-3 Total Organic Carbon 154 mg/L TA 154 J high 18 35WG117735 BRANDUTAH 9/13/2011 L54126-3 Mercury, Dissolved, CVAA 0.0077 ug/L <RDL,H 0.0077 J unknown 0.005 0.015WG117735 BRANDUTAH 9/14/2011 L54154-3 Mercury, Dissolved, CVAA 0.008 ug/L <RDL,H 0.008 J unknown 0.005 0.015WG117735 BRANDREG 9/21/2011 L54174-2 Mercury, Dissolved, CVAA 0.0061 ug/L <RDL,H 0.0061 J unknown 0.005 0.015WG117735 A01007 9/28/2011 L54307-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG117735 BRANDREG 9/28/2011 L54307-2 Mercury, Dissolved, CVAA 0.0059 ug/L <RDL,H 0.0059 J unknown 0.005 0.015WG117735 BRANDUTAH 9/28/2011 L54307-3 Mercury, Dissolved, CVAA 0.012 ug/L <RDL,H 0.012 J unknown 0.005 0.015WG118289 A01007 10/17/2011 L54454-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG118289 BRANDREG 10/17/2011 L54454-2 Mercury, Dissolved, CVAA 0.0051 ug/L <RDL,H 0.0051 J unknown 0.005 0.015WG118289 BRANDUTAH 10/17/2011 L54454-3 Mercury, Dissolved, CVAA 0.011 ug/L <RDL,H 0.011 J unknown 0.005 0.015WG118289 BRANDREG 10/18/2011 L54455-2 Mercury, Dissolved, CVAA 0.0057 ug/L <RDL,H 0.0057 J unknown 0.005 0.015WG118289 BRANDUTAH 10/18/2011 L54455-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG118289 BRANDREG 10/19/2011 L54488-2 Mercury, Dissolved, CVAA 0.01 ug/L <RDL,H 0.01 J unknown 0.005 0.015WG118289 BRANDUTAH 10/19/2011 L54488-3 Mercury, Dissolved, CVAA 0.0081 ug/L <RDL,H 0.0081 J unknown 0.005 0.015WG118289 A01007 10/25/2011 L54531-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG118289 A01007 10/26/2011 L54532-1 Mercury, Dissolved, CVAA 0.0065 ug/L <RDL,H 0.0065 J unknown 0.005 0.015WG118686 A01007 11/1/2011 L54591-1 Mercury, Dissolved, CVAA 0.0165 ug/L H 0.0165 J unknown 0.005 0.015WG117646 BRANDREG 9/21/2011 L54174-2 Arsenic, Dissolved, ICP-MS 0.951 ug/L H 0.951 J unknown 0.1 0.5WG117646 BRANDREG 9/21/2011 L54174-2 Cadmium, Dissolved, ICP-MS 0.25 ug/L <RDL,H 0.25 J unknown 0.05 0.25WG117646 BRANDREG 9/21/2011 L54174-2 Chromium, Dissolved, ICP-MS 2.62 ug/L H 2.62 J unknown 0.2 1WG117646 BRANDREG 9/21/2011 L54174-2 Copper, Dissolved, ICP-MS 20 ug/L H 20 J unknown 0.4 2WG117646 BRANDREG 9/21/2011 L54174-2 Lead, Dissolved, ICP-MS 0.616 ug/L H 0.616 J unknown 0.1 0.5WG117646 BRANDREG 9/21/2011 L54174-2 Nickel, Dissolved, ICP-MS 17.3 ug/L H 17.3 J unknown 0.1 0.5WG117646 BRANDREG 9/21/2011 L54174-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2




ValueDV

QualBias MDL RDL

WG117646 BRANDREG 9/21/2011 L54174-2 Vanadium, Dissolved, ICP-MS 0.645 ug/L H 0.645 J unknown 0.075 0.375WG117646 BRANDREG 9/21/2011 L54174-2 Zinc, Dissolved, ICP-MS 36.2 ug/L H 36.2 J unknown 0.5 2.5WG118036 BRANDUTAH 9/13/2011 L54126-3 Arsenic, Dissolved, ICP-MS 0.846 ug/L H 0.846 J unknown 0.1 0.5WG118036 BRANDUTAH 9/13/2011 L54126-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118036 BRANDUTAH 9/13/2011 L54126-3 Chromium, Dissolved, ICP-MS 0.48 ug/L <RDL,H 0.48 J unknown 0.2 1WG118036 BRANDUTAH 9/13/2011 L54126-3 Copper, Dissolved, ICP-MS 20.7 ug/L H 20.7 J unknown 0.4 2WG118036 BRANDUTAH 9/13/2011 L54126-3 Lead, Dissolved, ICP-MS 1.31 ug/L H 1.31 J unknown 0.1 0.5WG118036 BRANDUTAH 9/13/2011 L54126-3 Nickel, Dissolved, ICP-MS 3.16 ug/L H 3.16 J unknown 0.1 0.5WG118036 BRANDUTAH 9/13/2011 L54126-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118036 BRANDUTAH 9/13/2011 L54126-3 Vanadium, Dissolved, ICP-MS 1.04 ug/L H 1.04 J unknown 0.075 0.375WG118036 BRANDUTAH 9/13/2011 L54126-3 Zinc, Dissolved, ICP-MS 33.7 ug/L H 33.7 J unknown 0.5 2.5WG118036 BRANDUTAH 9/14/2011 L54154-3 Arsenic, Dissolved, ICP-MS 0.86 ug/L H 0.86 J unknown 0.1 0.5WG118036 BRANDUTAH 9/14/2011 L54154-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118036 BRANDUTAH 9/14/2011 L54154-3 Chromium, Dissolved, ICP-MS 0.46 ug/L <RDL,H 0.46 J unknown 0.2 1WG118036 BRANDUTAH 9/14/2011 L54154-3 Copper, Dissolved, ICP-MS 18.9 ug/L H 18.9 J unknown 0.4 2WG118036 BRANDUTAH 9/14/2011 L54154-3 Lead, Dissolved, ICP-MS 1.56 ug/L H 1.56 J unknown 0.1 0.5WG118036 BRANDUTAH 9/14/2011 L54154-3 Nickel, Dissolved, ICP-MS 3.3 ug/L H 3.3 J unknown 0.1 0.5WG118036 BRANDUTAH 9/14/2011 L54154-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118036 BRANDUTAH 9/14/2011 L54154-3 Vanadium, Dissolved, ICP-MS 1.03 ug/L H 1.03 J unknown 0.075 0.375WG118036 BRANDUTAH 9/14/2011 L54154-3 Zinc, Dissolved, ICP-MS 25.2 ug/L H 25.2 J unknown 0.5 2.5WG118036 A01007 9/28/2011 L54307-1 Arsenic, Dissolved, ICP-MS 1.04 ug/L H 1.04 J unknown 0.1 0.5WG118036 A01007 9/28/2011 L54307-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118036 A01007 9/28/2011 L54307-1 Chromium, Dissolved, ICP-MS 0.74 ug/L <RDL,H 0.74 J unknown 0.2 1WG118036 A01007 9/28/2011 L54307-1 Copper, Dissolved, ICP-MS 10.7 ug/L H 10.7 J unknown 0.4 2WG118036 A01007 9/28/2011 L54307-1 Lead, Dissolved, ICP-MS 0.734 ug/L H 0.734 J unknown 0.1 0.5WG118036 A01007 9/28/2011 L54307-1 Nickel, Dissolved, ICP-MS 3.5 ug/L H 3.5 J unknown 0.1 0.5WG118036 A01007 9/28/2011 L54307-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118036 A01007 9/28/2011 L54307-1 Vanadium, Dissolved, ICP-MS 0.98 ug/L H 0.98 J unknown 0.075 0.375WG118036 A01007 9/28/2011 L54307-1 Zinc, Dissolved, ICP-MS 52.6 ug/L H 52.6 J unknown 0.5 2.5WG118036 BRANDREG 9/28/2011 L54307-2 Arsenic, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.1 0.5WG118036 BRANDREG 9/28/2011 L54307-2 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118036 BRANDREG 9/28/2011 L54307-2 Chromium, Dissolved, ICP-MS 1.1 ug/L H 1.1 J unknown 0.2 1WG118036 BRANDREG 9/28/2011 L54307-2 Copper, Dissolved, ICP-MS 10.6 ug/L H 10.6 J unknown 0.4 2WG118036 BRANDREG 9/28/2011 L54307-2 Lead, Dissolved, ICP-MS 0.46 ug/L <RDL,H 0.46 J unknown 0.1 0.5WG118036 BRANDREG 9/28/2011 L54307-2 Nickel, Dissolved, ICP-MS 12.9 ug/L H 12.9 J unknown 0.1 0.5WG118036 BRANDREG 9/28/2011 L54307-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118036 BRANDREG 9/28/2011 L54307-2 Vanadium, Dissolved, ICP-MS 1.39 ug/L H 1.39 J unknown 0.075 0.375WG118036 BRANDREG 9/28/2011 L54307-2 Zinc, Dissolved, ICP-MS 46.6 ug/L H 46.6 J unknown 0.5 2.5WG118036 BRANDUTAH 9/28/2011 L54307-3 Arsenic, Dissolved, ICP-MS 1.12 ug/L H 1.12 J unknown 0.1 0.5




ValueDV

QualBias MDL RDL

WG118036 BRANDUTAH 9/28/2011 L54307-3 Cadmium, Dissolved, ICP-MS 0.068 ug/L <RDL,H 0.068 J unknown 0.05 0.25WG118036 BRANDUTAH 9/28/2011 L54307-3 Chromium, Dissolved, ICP-MS 0.57 ug/L <RDL,H 0.57 J unknown 0.2 1WG118036 BRANDUTAH 9/28/2011 L54307-3 Copper, Dissolved, ICP-MS 18.1 ug/L H 18.1 J unknown 0.4 2WG118036 BRANDUTAH 9/28/2011 L54307-3 Lead, Dissolved, ICP-MS 1.49 ug/L H 1.49 J unknown 0.1 0.5WG118036 BRANDUTAH 9/28/2011 L54307-3 Nickel, Dissolved, ICP-MS 3.01 ug/L H 3.01 J unknown 0.1 0.5WG118036 BRANDUTAH 9/28/2011 L54307-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118036 BRANDUTAH 9/28/2011 L54307-3 Vanadium, Dissolved, ICP-MS 0.807 ug/L H 0.807 J unknown 0.075 0.375WG118036 BRANDUTAH 9/28/2011 L54307-3 Zinc, Dissolved, ICP-MS 38.1 ug/L H 38.1 J unknown 0.5 2.5WG118171 A01007 10/17/2011 L54454-1 Arsenic, Dissolved, ICP-MS 1.38 ug/L H 1.38 J unknown 0.1 0.5WG118171 A01007 10/17/2011 L54454-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118171 A01007 10/17/2011 L54454-1 Chromium, Dissolved, ICP-MS 0.91 ug/L <RDL,H 0.91 J unknown 0.2 1WG118171 A01007 10/17/2011 L54454-1 Copper, Dissolved, ICP-MS 11.3 ug/L H 11.3 J unknown 0.4 2WG118171 A01007 10/17/2011 L54454-1 Lead, Dissolved, ICP-MS 1.23 ug/L H 1.23 J unknown 0.1 0.5WG118171 A01007 10/17/2011 L54454-1 Nickel, Dissolved, ICP-MS 5.24 ug/L H 5.24 J unknown 0.1 0.5WG118171 A01007 10/17/2011 L54454-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118171 A01007 10/17/2011 L54454-1 Vanadium, Dissolved, ICP-MS 2.22 ug/L H 2.22 J unknown 0.075 0.375WG118171 A01007 10/17/2011 L54454-1 Zinc, Dissolved, ICP-MS 36.5 ug/L H 36.5 J unknown 0.5 2.5WG118171 BRANDREG 10/17/2011 L54454-2 Arsenic, Dissolved, ICP-MS 1.42 ug/L H 1.42 J unknown 0.1 0.5WG118171 BRANDREG 10/17/2011 L54454-2 Cadmium, Dissolved, ICP-MS 0.084 ug/L <RDL,H 0.084 J unknown 0.05 0.25WG118171 BRANDREG 10/17/2011 L54454-2 Chromium, Dissolved, ICP-MS 2.61 ug/L H 2.61 J unknown 0.2 1WG118171 BRANDREG 10/17/2011 L54454-2 Copper, Dissolved, ICP-MS 23.3 ug/L H 23.3 J unknown 0.4 2WG118171 BRANDREG 10/17/2011 L54454-2 Lead, Dissolved, ICP-MS 1.52 ug/L H 1.52 J unknown 0.1 0.5WG118171 BRANDREG 10/17/2011 L54454-2 Nickel, Dissolved, ICP-MS 27.9 ug/L H 27.9 J unknown 0.1 0.5WG118171 BRANDREG 10/17/2011 L54454-2 Silver, Dissolved, ICP-MS 0.081 ug/L <RDL,H 0.081 J unknown 0.04 0.2WG118171 BRANDREG 10/17/2011 L54454-2 Vanadium, Dissolved, ICP-MS 2.88 ug/L H 2.88 J unknown 0.075 0.375WG118171 BRANDREG 10/17/2011 L54454-2 Zinc, Dissolved, ICP-MS 31.9 ug/L H 31.9 J unknown 0.5 2.5WG118171 BRANDUTAH 10/17/2011 L54454-3 Arsenic, Dissolved, ICP-MS 1.05 ug/L H 1.05 J unknown 0.1 0.5WG118171 BRANDUTAH 10/17/2011 L54454-3 Cadmium, Dissolved, ICP-MS 0.08 ug/L <RDL,H 0.08 J unknown 0.05 0.25WG118171 BRANDUTAH 10/17/2011 L54454-3 Chromium, Dissolved, ICP-MS 0.45 ug/L <RDL,H 0.45 J unknown 0.2 1WG118171 BRANDUTAH 10/17/2011 L54454-3 Copper, Dissolved, ICP-MS 13.4 ug/L H 13.4 J unknown 0.4 2WG118171 BRANDUTAH 10/17/2011 L54454-3 Lead, Dissolved, ICP-MS 1.81 ug/L H 1.81 J unknown 0.1 0.5WG118171 BRANDUTAH 10/17/2011 L54454-3 Nickel, Dissolved, ICP-MS 2.93 ug/L H 2.93 J unknown 0.1 0.5WG118171 BRANDUTAH 10/17/2011 L54454-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118171 BRANDUTAH 10/17/2011 L54454-3 Vanadium, Dissolved, ICP-MS 1.81 ug/L H 1.81 J unknown 0.075 0.375WG118171 BRANDUTAH 10/17/2011 L54454-3 Zinc, Dissolved, ICP-MS 26.1 ug/L H 26.1 J unknown 0.5 2.5WG118171 BRANDREG 10/18/2011 L54455-2 Arsenic, Dissolved, ICP-MS 1.58 ug/L H 1.58 J unknown 0.1 0.5WG118171 BRANDREG 10/18/2011 L54455-2 Cadmium, Dissolved, ICP-MS 0.095 ug/L <RDL,H 0.095 J unknown 0.05 0.25WG118171 BRANDREG 10/18/2011 L54455-2 Chromium, Dissolved, ICP-MS 2.32 ug/L H 2.32 J unknown 0.2 1WG118171 BRANDREG 10/18/2011 L54455-2 Copper, Dissolved, ICP-MS 18 ug/L H 18 J unknown 0.4 2




ValueDV

QualBias MDL RDL

WG118171 BRANDREG 10/18/2011 L54455-2 Lead, Dissolved, ICP-MS 2.85 ug/L H 2.85 J unknown 0.1 0.5WG118171 BRANDREG 10/18/2011 L54455-2 Nickel, Dissolved, ICP-MS 24.5 ug/L H 24.5 J unknown 0.1 0.5WG118171 BRANDREG 10/18/2011 L54455-2 Silver, Dissolved, ICP-MS 0.075 ug/L <RDL,H 0.075 J unknown 0.04 0.2WG118171 BRANDREG 10/18/2011 L54455-2 Vanadium, Dissolved, ICP-MS 2.82 ug/L H 2.82 J unknown 0.075 0.375WG118171 BRANDREG 10/18/2011 L54455-2 Zinc, Dissolved, ICP-MS 53.7 ug/L H 53.7 J unknown 0.5 2.5WG118171 BRANDUTAH 10/18/2011 L54455-3 Arsenic, Dissolved, ICP-MS 0.936 ug/L H 0.936 J unknown 0.1 0.5WG118171 BRANDUTAH 10/18/2011 L54455-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG118171 BRANDUTAH 10/18/2011 L54455-3 Chromium, Dissolved, ICP-MS 0.47 ug/L <RDL,H 0.47 J unknown 0.2 1WG118171 BRANDUTAH 10/18/2011 L54455-3 Copper, Dissolved, ICP-MS 11.2 ug/L H 11.2 J unknown 0.4 2WG118171 BRANDUTAH 10/18/2011 L54455-3 Lead, Dissolved, ICP-MS 1.15 ug/L H 1.15 J unknown 0.1 0.5WG118171 BRANDUTAH 10/18/2011 L54455-3 Nickel, Dissolved, ICP-MS 2.99 ug/L H 2.99 J unknown 0.1 0.5WG118171 BRANDUTAH 10/18/2011 L54455-3 Silver, Dissolved, ICP-MS 0.398 ug/L H 0.398 J unknown 0.04 0.2WG118171 BRANDUTAH 10/18/2011 L54455-3 Vanadium, Dissolved, ICP-MS 1.76 ug/L H 1.76 J unknown 0.075 0.375WG118171 BRANDUTAH 10/18/2011 L54455-3 Zinc, Dissolved, ICP-MS 11.7 ug/L H 11.7 J unknown 0.5 2.5WG118171 BRANDREG 10/19/2011 L54488-2 Arsenic, Dissolved, ICP-MS 1.43 ug/L H 1.43 J unknown 0.1 0.5WG118171 BRANDREG 10/19/2011 L54488-2 Cadmium, Dissolved, ICP-MS 0.097 ug/L <RDL,H 0.097 J unknown 0.05 0.25WG118171 BRANDREG 10/19/2011 L54488-2 Chromium, Dissolved, ICP-MS 2.27 ug/L H 2.27 J unknown 0.2 1WG118171 BRANDREG 10/19/2011 L54488-2 Copper, Dissolved, ICP-MS 22.9 ug/L H 22.9 J unknown 0.4 2WG118171 BRANDREG 10/19/2011 L54488-2 Lead, Dissolved, ICP-MS 2.03 ug/L H 2.03 J unknown 0.1 0.5WG118171 BRANDREG 10/19/2011 L54488-2 Nickel, Dissolved, ICP-MS 19.2 ug/L H 19.2 J unknown 0.1 0.5WG118171 BRANDREG 10/19/2011 L54488-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118171 BRANDREG 10/19/2011 L54488-2 Vanadium, Dissolved, ICP-MS 3.08 ug/L H 3.08 J unknown 0.075 0.375WG118171 BRANDREG 10/19/2011 L54488-2 Zinc, Dissolved, ICP-MS 44.5 ug/L H 44.5 J unknown 0.5 2.5WG118171 BRANDUTAH 10/19/2011 L54488-3 Arsenic, Dissolved, ICP-MS 0.891 ug/L H 0.891 J unknown 0.1 0.5WG118171 BRANDUTAH 10/19/2011 L54488-3 Cadmium, Dissolved, ICP-MS 0.058 ug/L <RDL,H 0.058 J unknown 0.05 0.25WG118171 BRANDUTAH 10/19/2011 L54488-3 Chromium, Dissolved, ICP-MS 0.39 ug/L <RDL,H 0.39 J unknown 0.2 1WG118171 BRANDUTAH 10/19/2011 L54488-3 Copper, Dissolved, ICP-MS 12.6 ug/L H 12.6 J unknown 0.4 2WG118171 BRANDUTAH 10/19/2011 L54488-3 Lead, Dissolved, ICP-MS 0.839 ug/L H 0.839 J unknown 0.1 0.5WG118171 BRANDUTAH 10/19/2011 L54488-3 Nickel, Dissolved, ICP-MS 2.02 ug/L H 2.02 J unknown 0.1 0.5WG118171 BRANDUTAH 10/19/2011 L54488-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG118171 BRANDUTAH 10/19/2011 L54488-3 Vanadium, Dissolved, ICP-MS 1.51 ug/L H 1.51 J unknown 0.075 0.375WG118171 BRANDUTAH 10/19/2011 L54488-3 Zinc, Dissolved, ICP-MS 18 ug/L H 18 J unknown 0.5 2.5WG119371 A01007 10/25/2011 L54531-1 Arsenic, Dissolved, ICP-MS 1.2 ug/L H 1.2 J unknown 0.1 0.5WG119371 A01007 10/25/2011 L54531-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG119371 A01007 10/25/2011 L54531-1 Chromium, Dissolved, ICP-MS 0.94 ug/L <RDL,H 0.94 J unknown 0.2 1WG119371 A01007 10/25/2011 L54531-1 Copper, Dissolved, ICP-MS 12.7 ug/L H 12.7 J unknown 0.4 2WG119371 A01007 10/25/2011 L54531-1 Lead, Dissolved, ICP-MS 0.784 ug/L H 0.784 J unknown 0.1 0.5WG119371 A01007 10/25/2011 L54531-1 Nickel, Dissolved, ICP-MS 4.71 ug/L H 4.71 J unknown 0.1 0.5WG119371 A01007 10/25/2011 L54531-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2




ValueDV

QualBias MDL RDL

WG119371 A01007 10/25/2011 L54531-1 Vanadium, Dissolved, ICP-MS 1.72 ug/L H 1.72 J unknown 0.075 0.375WG119371 A01007 10/25/2011 L54531-1 Zinc, Dissolved, ICP-MS 40.7 ug/L H 40.7 J unknown 0.5 2.5WG119371 A01007 10/26/2011 L54532-1 Arsenic, Dissolved, ICP-MS 1.52 ug/L H 1.52 J unknown 0.1 0.5WG119371 A01007 10/26/2011 L54532-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG119371 A01007 10/26/2011 L54532-1 Chromium, Dissolved, ICP-MS 2.81 ug/L H 2.81 J unknown 0.2 1WG119371 A01007 10/26/2011 L54532-1 Copper, Dissolved, ICP-MS 6.68 ug/L H 6.68 J unknown 0.4 2WG119371 A01007 10/26/2011 L54532-1 Lead, Dissolved, ICP-MS 0.7 ug/L H 0.7 J unknown 0.1 0.5WG119371 A01007 10/26/2011 L54532-1 Nickel, Dissolved, ICP-MS 5.96 ug/L H 5.96 J unknown 0.1 0.5WG119371 A01007 10/26/2011 L54532-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG119371 A01007 10/26/2011 L54532-1 Vanadium, Dissolved, ICP-MS 2.05 ug/L H 2.05 J unknown 0.075 0.375WG119371 A01007 10/26/2011 L54532-1 Zinc, Dissolved, ICP-MS 87.9 ug/L H 87.9 J unknown 0.5 2.5WG119371 A01007 11/1/2011 L54591-1 Arsenic, Dissolved, ICP-MS 1.21 ug/L H 1.21 J unknown 0.1 0.5WG119371 A01007 11/1/2011 L54591-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG119371 A01007 11/1/2011 L54591-1 Chromium, Dissolved, ICP-MS 0.87 ug/L <RDL,H 0.87 J unknown 0.2 1WG119371 A01007 11/1/2011 L54591-1 Copper, Dissolved, ICP-MS 10.9 ug/L H 10.9 J unknown 0.4 2WG119371 A01007 11/1/2011 L54591-1 Lead, Dissolved, ICP-MS 1.42 ug/L H 1.42 J unknown 0.1 0.5WG119371 A01007 11/1/2011 L54591-1 Nickel, Dissolved, ICP-MS 3.68 ug/L H 3.68 J unknown 0.1 0.5WG119371 A01007 11/1/2011 L54591-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG119371 A01007 11/1/2011 L54591-1 Vanadium, Dissolved, ICP-MS 1.79 ug/L H 1.79 J unknown 0.075 0.375WG119371 A01007 11/1/2011 L54591-1 Zinc, Dissolved, ICP-MS 43.7 ug/L H 43.7 J unknown 0.5 2.5WG117498 A01007 9/13/2011 L54126-1 Benzo(a)anthracene ug/L <MDL 0.019 R very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Benzo(a)anthracene 0.024 ug/L <RDL 0.024 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Benzo(a)anthracene ug/L <MDL 0.019 R very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Benzo(a)anthracene ug/L <MDL 0.019 R very low 0.019 0.0377WG117498 A01007 9/13/2011 L54126-1 Benzyl Butyl Phthalate 0.675 ug/L 0.675 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Benzyl Butyl Phthalate 7.28 ug/L 7.28 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Benzyl Butyl Phthalate 1.31 ug/L 1.31 J very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Benzyl Butyl Phthalate 43 ug/L 43 J very low 0.12 0.236WG117498 A01007 9/13/2011 L54126-1 Bis(2-Ethylhexyl)Phthalate 5.46 ug/L 5.46 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Bis(2-Ethylhexyl)Phthalate 4.59 ug/L 4.59 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Bis(2-Ethylhexyl)Phthalate 2.99 ug/L 2.99 J very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Bis(2-Ethylhexyl)Phthalate 8.39 ug/L 8.39 J very low 0.019 0.0377WG117498 A01007 9/13/2011 L54126-1 Chrysene 0.037 ug/L <RDL 0.037 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Chrysene 0.0384 ug/L 0.0384 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Chrysene 0.034 ug/L <RDL 0.034 J very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Chrysene ug/L <MDL 0.019 R very low 0.019 0.0377WG117498 A01007 9/13/2011 L54126-1 Di-N-Butyl Phthalate 0.43 ug/L <RDL 0.472 R very low 0.019 0.472WG117498 BRANDUTAH 9/13/2011 L54126-3 Di-N-Butyl Phthalate 0.27 ug/L <RDL,B2 0.472 UJ low 0.019 0.472WG117498 BRANDREG 9/14/2011 L54154-2 Di-N-Butyl Phthalate 0.31 ug/L <RDL,B2 0.472 R very low 0.019 0.472




ValueDV

QualBias MDL RDL

WG117498 BRANDUTAH 9/14/2011 L54154-3 Di-N-Butyl Phthalate 0.563 ug/L 0.563 R very low 0.019 0.472WG117498 A01007 9/13/2011 L54126-1 Fluoranthene 0.0843 ug/L 0.0843 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Fluoranthene 0.0605 ug/L 0.0605 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Fluoranthene 0.0699 ug/L 0.0699 J very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Fluoranthene 0.0952 ug/L 0.0952 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Naphthalene 0.081 ug/L <RDL 0.0943 U unknown 0.047 0.0943WG117498 BRANDREG 9/14/2011 L54154-2 Naphthalene 0.088 ug/L <RDL 0.0943 U unknown 0.047 0.0943WG117498 A01007 9/13/2011 L54126-1 Pyrene 0.0473 ug/L 0.0473 J very low 0.019 0.0377WG117498 BRANDUTAH 9/13/2011 L54126-3 Pyrene 0.038 ug/L <RDL 0.038 J low 0.019 0.0377WG117498 BRANDREG 9/14/2011 L54154-2 Pyrene 0.0558 ug/L 0.0558 J very low 0.019 0.0377WG117498 BRANDUTAH 9/14/2011 L54154-3 Pyrene 0.0555 ug/L 0.0555 J very low 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 2-Methylnaphthalene 0.218 ug/L 0.218 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Acenaphthene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Acenaphthylene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Anthracene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Benzo(a)anthracene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Benzo(a)pyrene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Benzo(b,j,k)fluoranthene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Benzo(g,h,i)perylene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Benzyl Butyl Phthalate 3.59 ug/L 3.59 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Bis(2-Ethylhexyl)Phthalate 2.07 ug/L 2.07 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Chrysene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Dibenzo(a,h)anthracene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Diethyl Phthalate 1.69 ug/L 1.69 J unknown 0.019 0.0943WG117625 BRANDREG 9/21/2011 L54174-2 Dimethyl Phthalate 0.124 ug/L 0.124 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Di-N-Butyl Phthalate 0.18 ug/L <RDL,B2 0.472 UJ unknown 0.019 0.472WG117625 BRANDREG 9/21/2011 L54174-2 Di-N-Octyl Phthalate 0.138 ug/L 0.138 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Fluoranthene 0.028 ug/L <RDL 0.028 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Fluorene 0.024 ug/L <RDL 0.024 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Indeno(1,2,3-Cd)Pyrene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Naphthalene 0.239 ug/L 0.239 J unknown 0.047 0.0943WG117625 BRANDREG 9/21/2011 L54174-2 Phenanthrene 0.0499 ug/L 0.0499 J unknown 0.019 0.0377WG117625 BRANDREG 9/21/2011 L54174-2 Pyrene ug/L <MDL 0.019 UJ unknown 0.019 0.0377WG117764 A01007 9/28/2011 L54307-1 Benzo(a)anthracene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Benzo(a)anthracene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 A01007 9/28/2011 L54307-1 Benzyl Butyl Phthalate 0.231 ug/L 0.231 J low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Benzyl Butyl Phthalate 4.32 ug/L 4.32 J low 0.04 0.08WG117764 A01007 9/28/2011 L54307-1 Bis(2-Ethylhexyl)Phthalate 1.96 ug/L 1.96 J low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Bis(2-Ethylhexyl)Phthalate 5 ug/L 5 J low 0.04 0.08




ValueDV

QualBias MDL RDL

WG117764 A01007 9/28/2011 L54307-1 Chrysene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Chrysene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 A01007 9/28/2011 L54307-1 Di-N-Butyl Phthalate 0.35 ug/L <RDL,B2 1 UJ low 0.04 1WG117764 BRANDREG 9/28/2011 L54307-2 Di-N-Butyl Phthalate 0.25 ug/L <RDL,B 1 U 0.04 1WG117764 BRANDUTAH 9/28/2011 L54307-3 Di-N-Butyl Phthalate 0.35 ug/L <RDL,B2 1 UJ low 0.04 1WG117764 A01007 9/28/2011 L54307-1 Fluoranthene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Fluoranthene 0.058 ug/L <RDL 0.058 J low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Phenanthrene 0.054 ug/L <RDL 0.08 U 0.04 0.08WG117764 A01007 9/28/2011 L54307-1 Pyrene ug/L <MDL 0.04 UJ low 0.04 0.08WG117764 BRANDUTAH 9/28/2011 L54307-3 Pyrene ug/L <MDL 0.04 UJ low 0.04 0.08WG118172 BRANDREG 10/18/2011 L54455-2 2-Methylnaphthalene 0.034 ug/L <RDL,B3 0.064 U 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Benzo(a)anthracene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Benzyl Butyl Phthalate 0.499 ug/L 0.499 J low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Benzyl Butyl Phthalate 2.77 ug/L 2.77 J low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Benzyl Butyl Phthalate 12.3 ug/L 12.3 J low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Benzyl Butyl Phthalate 3.87 ug/L 3.87 J low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Benzyl Butyl Phthalate 6.46 ug/L 6.46 J low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Benzyl Butyl Phthalate 44.4 ug/L 44.4 J low 0.16 0.32WG118172 A01007 10/17/2011 L54454-1 Bis(2-Ethylhexyl)Phthalate 4.1 ug/L 4.1 J low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Bis(2-Ethylhexyl)Phthalate 3.98 ug/L 3.98 J low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Bis(2-Ethylhexyl)Phthalate 2.35 ug/L B2 2.35 J low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Bis(2-Ethylhexyl)Phthalate 4.5 ug/L 4.5 J low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Bis(2-Ethylhexyl)Phthalate 5.47 ug/L 5.47 J low 0.032 0.064WG118172 BRANDREG 10/19/2011 L54488-2 Bis(2-Ethylhexyl)Phthalate 7.79 ug/L 7.79 J low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Bis(2-Ethylhexyl)Phthalate 3.82 ug/L 3.82 J low 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Chrysene 0.037 ug/L <RDL 0.037 J low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Chrysene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Chrysene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Chrysene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Chrysene 0.0719 ug/L 0.0719 J low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Chrysene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Di-N-Butyl Phthalate 0.45 ug/L <RDL,B2 0.8 UJ low 0.032 0.8WG118172 BRANDREG 10/17/2011 L54454-2 Di-N-Butyl Phthalate 0.34 ug/L <RDL,B 0.8 UJ low 0.032 0.8WG118172 BRANDUTAH 10/17/2011 L54454-3 Di-N-Butyl Phthalate 0.28 ug/L <RDL,B 0.8 UJ low 0.032 0.8




ValueDV

QualBias MDL RDL

WG118172 BRANDREG 10/18/2011 L54455-2 Di-N-Butyl Phthalate 0.51 ug/L <RDL,B2 0.8 UJ low 0.032 0.8WG118172 BRANDUTAH 10/18/2011 L54455-3 Di-N-Butyl Phthalate ug/L <MDL 0.032 UJ low 0.032 0.8WG118172 BRANDREG 10/19/2011 L54488-2 Di-N-Butyl Phthalate 0.52 ug/L <RDL,B2 0.8 U 0.032 0.8WG118172 BRANDUTAH 10/19/2011 L54488-3 Di-N-Butyl Phthalate 0.49 ug/L <RDL,B2 0.8 UJ low 0.032 0.8WG118172 A01007 10/17/2011 L54454-1 Fluoranthene 0.0948 ug/L 0.0948 J low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Fluoranthene 0.056 ug/L <RDL 0.056 J low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Fluoranthene 0.041 ug/L <RDL 0.041 J low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Fluoranthene 0.0662 ug/L 0.0662 J low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Fluoranthene 0.148 ug/L 0.148 J low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Fluoranthene 0.038 ug/L <RDL 0.038 J low 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Phenanthrene 0.13 ug/L 0.13 J unknown 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Phenanthrene 0.062 ug/L <RDL 0.064 U 0.032 0.064WG118172 A01007 10/17/2011 L54454-1 Pyrene 0.053 ug/L <RDL 0.053 J low 0.032 0.064WG118172 BRANDREG 10/17/2011 L54454-2 Pyrene 0.04 ug/L <RDL 0.04 J low 0.032 0.064WG118172 BRANDUTAH 10/17/2011 L54454-3 Pyrene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDREG 10/18/2011 L54455-2 Pyrene 0.034 ug/L <RDL 0.034 J low 0.032 0.064WG118172 BRANDUTAH 10/18/2011 L54455-3 Pyrene ug/L <MDL 0.032 UJ low 0.032 0.064WG118172 BRANDUTAH 10/19/2011 L54488-3 Pyrene ug/L <MDL 0.032 UJ low 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 2-Methylnaphthalene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 2-Methylnaphthalene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Acenaphthene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Acenaphthene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Acenaphthylene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Acenaphthylene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Benzo(a)anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Benzo(a)anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Benzo(a)pyrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Benzo(a)pyrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Benzo(b,j,k)fluoranthene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Benzo(b,j,k)fluoranthene 0.033 ug/L <RDL 0.033 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Benzo(g,h,i)perylene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Benzo(g,h,i)perylene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Benzyl Butyl Phthalate 0.21 ug/L B2 0.21 J unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Benzyl Butyl Phthalate 0.372 ug/L 0.372 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Bis(2-Ethylhexyl)Phthalate 1.87 ug/L B2 1.87 J unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Bis(2-Ethylhexyl)Phthalate 5.83 ug/L 5.83 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Chrysene ug/L <MDL 0.032 UJ unknown 0.032 0.064




ValueDV

QualBias MDL RDL

WG118307 A01007 10/26/2011 L54532-1 Chrysene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Dibenzo(a,h)anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Dibenzo(a,h)anthracene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Diethyl Phthalate 2.56 ug/L 2.56 J unknown 0.032 0.16WG118307 A01007 10/26/2011 L54532-1 Diethyl Phthalate 2.81 ug/L 2.81 J unknown 0.032 0.16WG118307 A01007 10/25/2011 L54531-1 Dimethyl Phthalate ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Dimethyl Phthalate 0.287 ug/L 0.287 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Di-N-Butyl Phthalate 0.66 ug/L <RDL,B2 0.8 UJ unknown 0.032 0.8WG118307 A01007 10/26/2011 L54532-1 Di-N-Butyl Phthalate 0.867 ug/L B2 0.867 J unknown 0.032 0.8WG118307 A01007 10/25/2011 L54531-1 Di-N-Octyl Phthalate 0.033 ug/L <RDL 0.033 J unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Di-N-Octyl Phthalate 0.395 ug/L 0.395 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Fluoranthene 0.034 ug/L <RDL 0.034 J unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Fluoranthene 0.084 ug/L 0.084 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Fluorene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Fluorene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Indeno(1,2,3-Cd)Pyrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Indeno(1,2,3-Cd)Pyrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Naphthalene ug/L <MDL 0.08 UJ unknown 0.08 0.16WG118307 A01007 10/26/2011 L54532-1 Naphthalene ug/L <MDL 0.08 UJ unknown 0.08 0.16WG118307 A01007 10/25/2011 L54531-1 Phenanthrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Phenanthrene 0.093 ug/L 0.093 J unknown 0.032 0.064WG118307 A01007 10/25/2011 L54531-1 Pyrene ug/L <MDL 0.032 UJ unknown 0.032 0.064WG118307 A01007 10/26/2011 L54532-1 Pyrene 0.055 ug/L <RDL 0.055 J unknown 0.032 0.064WG118436 A01007 11/1/2011 L54591-1 Benzo(a)anthracene ug/L <MDL 0.008 UJ low 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Benzyl Butyl Phthalate 0.244 ug/L B2 0.244 J low 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Bis(2-Ethylhexyl)Phthalate 2.6 ug/L B,J 2.6 J low 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Chrysene 0.015 ug/L <RDL 0.015 J low 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Di-N-Butyl Phthalate 0.451 ug/L B 0.451 UJ low 0.008 0.2WG118436 A01007 11/1/2011 L54591-1 Fluoranthene 0.0266 ug/L 0.0266 J low 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Naphthalene 0.0786 ug/L B 0.0786 U 0.02 0.04WG118436 A01007 11/1/2011 L54591-1 Phenanthrene 0.0446 ug/L B 0.0446 U 0.008 0.016WG118436 A01007 11/1/2011 L54591-1 Pyrene ug/L <MDL 0.008 UJ low 0.008 0.016

1

ATTACHMENT A

LIMS BATCH AND QC REPORTS

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Work Group WG117545 - TOC/DOC

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54020-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 09/19/11 09/20/11 09/21/11L54020-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 09/19/11 09/20/11 09/20/11L54020-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 09/19/11 09/20/11 09/21/11L54020-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 09/19/11 09/20/11 09/20/11L54020-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 09/19/11 09/20/11 09/21/11L54020-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 09/19/11 09/20/11 09/20/11L54021-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 09/19/11 09/20/11 09/21/11L54021-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 09/19/11 09/20/11 09/20/11L54021-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 09/19/11 09/20/11 09/21/11L54021-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 09/19/11 09/20/11 09/20/11L54021-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 09/19/11 09/20/11 09/21/11L54021-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 09/19/11 09/20/11 09/20/11L54073-1 421422-HTGW SWD-HTGW CVTOC GRND WTR 09/15/11 09/19/11 09/19/11L54073-3 421422-HTGW SWD-HTGW CVTOC GRND WTR 09/15/11 09/19/11 09/19/11L54073-5 421422-HTGW SWD-HTGW CVTOC GRND WTR 09/19/11 09/19/11 09/19/11L54075-1 421422-HTGW SWD-HTGW CVTOC GRND WTR 09/14/11 09/19/11 09/19/11L54076-1 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 09/19/11 09/19/11 09/19/11L54126-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/13/11 09/15/11 09/21/11L54126-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/13/11 09/20/11 09/20/11L54126-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/13/11 09/15/11 09/21/11L54126-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/13/11 09/20/11 09/20/11L54147-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/13/11 09/15/11 09/21/11L54147-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/13/11 09/20/11 09/20/11L54147-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/13/11 09/15/11 09/21/11L54147-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/13/11 09/20/11 09/20/11L54147-3 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/13/11 09/15/11 09/21/11L54147-3 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/13/11 09/20/11 09/20/11L54147-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/13/11 09/15/11 09/21/11L54147-4 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/13/11 09/20/11 09/20/11L54148-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/14/11 09/16/11 09/20/11L54148-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/14/11 09/19/11 09/19/11L54148-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/14/11 09/16/11 09/20/11L54148-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/14/11 09/19/11 09/19/11L54149-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/15/11 09/16/11 09/21/11L54149-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/15/11 09/19/11 09/19/11L54149-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC FRESH WTR 09/15/11 09/16/11 09/21/11L54149-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC FRESH WTR 09/15/11 09/19/11 09/19/11L54154-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/14/11 09/16/11 09/21/11

LIMSView Batch Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Conventionals

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L54154-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/14/11 09/20/11 09/20/11L54154-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/14/11 09/16/11 09/21/11L54154-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/14/11 09/20/11 09/20/11WG117545-1 MB CVTOC BLANK WTR 09/19/11 09/19/11 MB1 09/19/11WG117545-2 LCS CVTOC BLANK WTR 09/19/11 09/19/11 LEVEL1WG117545-3 SB CVTOC BLANK WTR 09/19/11 09/19/11 WG117545-1WG117545-4 LD CVTOC GRND WTR 09/19/11 09/19/11 L54073-5WG117545-5 MS CVTOC GRND WTR 09/19/11 09/19/11 L54075-1WG117545-6 LD CVTOC FRESH WTR 09/19/11 09/19/11 L54076-1WG117545-7 LD CVTOC FRESH WTR 09/19/11 09/19/11 L54149-2WG117545-8 MS CVTOC FRESH WTR 09/20/11 09/20/11 L54147-1WG117545-9 MB CVTOC BLANK WTR 09/20/11 09/20/11 MB1 09/20/11WG117545-10 LCS CVTOC BLANK WTR 09/20/11 09/20/11 LEVEL1WG117545-11 MS CVTOC SEWER WTR 09/20/11 09/20/11 L54154-2WG117545-12 SB CVTOC BLANK WTR 09/20/11 09/20/11 WG117545-9WG117545-13 LD CVTOC FRESH WTR 09/20/11 09/20/11 L54020-1WG117545-14 MS CVTOC FRESH WTR 09/20/11 09/20/11 L54020-3WG117545-15 LD CVTOC SALT WTR 09/20/11 09/20/11 L54021-1WG117545-16 MS CVTOC SALT WTR 09/20/11 09/20/11 L54021-3WG117545-17 MB CVDOC BLANK WTR 09/16/11 09/20/11 MB1 09/16/11WG117545-18 LCS CVDOC BLANK WTR 09/20/11 09/20/11 LEVEL1WG117545-19 SB CVDOC BLANK WTR 09/16/11 09/20/11 WG117545-17WG117545-20 MB CVDOC BLANK WTR 09/16/11 09/21/11 MB2 09/16/11WG117545-21 LD CVDOC FRESH WTR 09/16/11 09/21/11 L54149-1WG117545-22 MS CVDOC FRESH WTR 09/16/11 09/21/11 L54149-2WG117545-23 MB CVDOC BLANK WTR 09/15/11 09/21/11 MB2 09/15/11WG117545-24 MB CVDOC BLANK WTR 09/20/11 09/21/11 MB1 09/20/11WG117545-25 LCS CVDOC BLANK WTR 09/21/11 09/21/11 LEVEL1WG117545-26 SB CVDOC BLANK WTR 09/20/11 09/21/11 WG117545-24WG117545-27 LD CVDOC FRESH WTR 09/20/11 09/21/11 L54020-1WG117545-28 MS CVDOC FRESH WTR 09/20/11 09/21/11 L54020-3WG117545-29 LD CVDOC SALT WTR 09/20/11 09/21/11 L54021-1WG117545-30 MS CVDOC SALT WTR 09/20/11 09/21/11 L54021-3WG117545-31 LD CVTOC SEWER WTR 09/20/11 09/20/11 L54154-2WG117545-32 LD CVDOC SEWER WTR 09/16/11 09/21/11 L54154-3WG117545-33 MS CVDOC SEWER WTR 09/16/11 09/21/11 L54154-3

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Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54174-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/21/11 09/23/11 10/04/11L54176-1 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 09/26/11 09/27/11 10/03/11L54176-2 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 09/26/11 09/27/11 10/03/11L54176-3 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 09/26/11 09/27/11 10/03/11L54190-1 422027 Lab Lake Wash PBT-EPA Grant CVDOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-1 422027 Lab Lake Wash PBT-EPA Grant CVTOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-2 422027 Lab Lake Wash PBT-EPA Grant CVDOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-2 422027 Lab Lake Wash PBT-EPA Grant CVTOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-3 422027 Lab Lake Wash PBT-EPA Grant CVDOC FRESH WTR 10/03/11 10/03/11 10/03/11L54190-3 422027 Lab Lake Wash PBT-EPA Grant CVTOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-4 422027 Lab Lake Wash PBT-EPA Grant CVDOC FRESH WTR 10/03/11 10/03/11 10/03/11L54190-4 422027 Lab Lake Wash PBT-EPA Grant CVTOC FRESH WTR 10/03/11 10/04/11 10/04/11L54190-5 422027 Lab Lake Wash PBT-EPA Grant CVDOC FRESH WTR 10/03/11 10/03/11 10/03/11L54190-5 422027 Lab Lake Wash PBT-EPA Grant CVTOC FRESH WTR 10/03/11 10/04/11 10/04/11L54307-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/28/11 09/30/11 10/04/11L54307-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/28/11 09/30/11 10/03/11L54307-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 09/28/11 09/30/11 10/03/11WG117810-1 MB CVDOC BLANK WTR 09/27/11 10/03/11 MB1 110927WG117810-2 LCS CVDOC BLANK WTR 10/03/11 10/03/11 LEVEL1WG117810-3 SB CVDOC BLANK WTR 09/27/11 10/03/11 WG117810-1WG117810-4 LD CVDOC STORM WTR 09/27/11 10/03/11 L54176-1WG117810-5 MS CVDOC STORM WTR 09/27/11 10/03/11 L54176-3WG117810-6 MB CVDOC BLANK WTR 10/03/11 10/03/11 MB1 111003WG117810-7 MB CVDOC BLANK WTR 09/30/11 10/03/11 MB1 110930WG117810-8 MS CVDOC SEWER WTR 09/30/11 10/03/11 L54307-3WG117810-9 MB CVDOC BLANK WTR 09/23/11 10/04/11 MB1 110923WG117810-10 LD CVDOC SEWER WTR 09/23/11 10/04/11 L54174-2WG117810-11 MB CVTOC BLANK WTR 10/04/11 10/04/11 MB1 111003WG117810-12 LCS CVTOC BLANK WTR 10/04/11 10/04/11 LEVEL1WG117810-13 SB CVTOC BLANK WTR 10/04/11 10/04/11 WG117810-11WG117810-14 LD CVTOC FRESH WTR 10/04/11 10/04/11 L54190-3WG117810-15 MS CVTOC FRESH WTR 10/04/11 10/04/11 L54190-5WG117810-16 MB CVDOC BLANK WTR 10/04/11 10/04/11 MB1 111004

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Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54271-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 10/17/11 10/18/11 10/19/11L54271-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 10/17/11 10/18/11 10/18/11L54271-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 10/17/11 10/18/11 10/19/11L54271-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 10/17/11 10/18/11 10/18/11L54271-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 10/17/11 10/18/11 10/19/11L54271-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 10/17/11 10/19/11 10/19/11L54272-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 10/17/11 10/18/11 10/19/11L54272-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 10/17/11 10/19/11 10/19/11L54272-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 10/17/11 10/18/11 10/19/11L54272-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 10/17/11 10/19/11 10/19/11L54272-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 10/17/11 10/18/11 10/20/11L54272-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 10/17/11 10/19/11 10/19/11L54349-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/17/11 10/18/11 10/18/11L54349-5 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/17/11 10/18/11 10/18/11L54349-6 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/17/11 10/18/11 10/18/11L54391-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/18/11 10/18/11 10/18/11L54391-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/18/11 10/18/11 10/18/11L54391-5 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/19/11 10/21/11 10/21/11L54391-6 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/19/11 10/21/11 10/21/11L54391-7 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/19/11 10/21/11 10/21/11L54395-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/20/11 10/21/11 10/21/11L54395-5 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/21/11 10/21/11 10/21/11L54395-6 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/21/11 10/21/11 10/21/11L54454-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/17/11 10/18/11 10/20/11L54454-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/17/11 10/19/11 10/19/11L54454-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/17/11 10/18/11 10/20/11L54454-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/17/11 10/19/11 10/19/11L54454-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/17/11 10/18/11 10/20/11L54454-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/17/11 10/19/11 10/19/11L54455-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/18/11 10/20/11 10/21/11L54455-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/18/11 10/21/11 10/21/11L54455-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/18/11 10/20/11 10/21/11L54455-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/18/11 10/21/11 10/21/11L54457-1 421195-470 Miller Creek DOC Study CVDOC FRESH WTR 10/18/11 10/18/11 10/19/11L54457-2 421195-470 Miller Creek DOC Study CVDOC FRESH WTR 10/18/11 10/18/11 10/20/11L54488-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/19/11 10/21/11 10/21/11L54488-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/19/11 10/21/11 10/21/11L54488-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/19/11 10/21/11 10/21/11

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L54488-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/19/11 10/21/11 10/21/11WG118166-1 MB CVTOC BLANK WTR 10/18/11 10/18/11 MB1 10/18/11WG118166-2 LCS CVTOC BLANK WTR 10/18/11 10/18/11 LEVEL1WG118166-3 SB CVTOC BLANK WTR 10/18/11 10/18/11 WG118166-1WG118166-4 LD CVTOC GRND WTR 10/18/11 10/18/11 L54391-2WG118166-5 MS CVTOC GRND WTR 10/18/11 10/18/11 L54349-6WG118166-6 LD CVTOC FRESH WTR 10/18/11 10/18/11 L54271-2WG118166-7 MS CVTOC SALT WTR 10/19/11 10/19/11 L54272-3WG118166-8 LD CVTOC SEWER WTR 10/19/11 10/19/11 L54454-3WG118166-9 MS CVTOC SEWER WTR 10/19/11 10/19/11 L54454-3WG118166-10 MB CVDOC BLANK WTR 10/18/11 10/19/11 MB1 10/18/11WG118166-11 LCS CVDOC BLANK WTR 10/19/11 10/19/11 LEVEL1WG118166-12 SB CVDOC BLANK WTR 10/18/11 10/19/11 WG118166-10WG118166-13 LD CVDOC FRESH WTR 10/18/11 10/19/11 L54271-2WG118166-14 MB CVDOC BLANK WTR 10/18/11 10/19/11 MB1 10/18/11WG118166-15 LD CVDOC FRESH WTR 10/18/11 10/19/11 L54457-1WG118166-16 LCS CVDOC BLANK WTR 10/20/11 10/20/11 LEVEL1WG118166-17 MS CVDOC SALT WTR 10/18/11 10/20/11 L54272-3WG118166-18 SB CVDOC BLANK WTR 10/18/11 10/20/11 WG118166-20WG118166-19 MS CVDOC FRESH WTR 10/18/11 10/20/11 L54457-2WG118166-20 MB CVDOC BLANK WTR 10/18/11 10/20/11 MB2 10/18/11WG118166-21 LD CVDOC SEWER WTR 10/18/11 10/20/11 L54454-3WG118166-22 MS CVDOC SEWER WTR 10/18/11 10/20/11 L54454-3WG118166-23 MB CVTOC BLANK WTR 10/21/11 10/21/11 MB1 111020WG118166-24 LCS CVTOC BLANK WTR 10/21/11 10/21/11 LEVEL1WG118166-25 MB CVTOC BLANK WTR 10/21/11 10/21/11 MB1 111021WG118166-26 LCS CVTOC BLANK WTR 10/21/11 10/21/11 LEVEL1WG118166-27 MB CVDOC BLANK WTR 10/20/11 10/21/11 MB1 10/20/11 9:30WG118166-28 LCS CVDOC BLANK WTR 10/21/11 10/21/11 LEVEL1WG118166-29 MB CVDOC BLANK WTR 10/21/11 10/21/11 MB1 10/21/11 8:30


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL53806-2 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/25/11 11/01/11 11/01/11L53806-3 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/25/11 11/01/11 11/01/11L53806-5 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/25/11 11/01/11 11/01/11L53806-6 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/25/11 11/01/11 11/01/11L53806-8 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/27/11 11/01/11 11/01/11L53806-9 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/26/11 11/01/11 11/01/11L53806-10 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/27/11 11/01/11 11/01/11

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L53806-11 421422-CHSW-Q SWD-CHSW CVTOC FRESH WTR 10/26/11 11/01/11 11/01/11L54322-1 421422-CHGW SWD-CHSW CVTOC GRND WTR 10/24/11 10/31/11 10/31/11L54349-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/25/11 10/31/11 10/31/11L54393-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/25/11 10/31/11 10/31/11L54393-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/24/11 10/31/11 10/31/11L54395-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/28/11 11/01/11 11/01/11L54398-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/25/11 11/01/11 11/01/11L54398-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/26/11 11/01/11 11/01/11L54398-5 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/26/11 11/01/11 11/01/11L54400-1 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/28/11 10/31/11 10/31/11L54400-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/24/11 10/31/11 10/31/11L54400-5 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/26/11 10/31/11 10/31/11L54429-2 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/28/11 10/31/11 10/31/11L54429-6 421422-CHGW SWD-CHGW CVTOC GRND WTR 10/28/11 10/31/11 10/31/11L54531-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/25/11 10/27/11 11/02/11L54531-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/25/11 11/02/11 11/02/11L54532-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 10/26/11 10/27/11 11/02/11L54532-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 10/26/11 11/02/11 11/02/11L54541-1 421422-VAGW SWD-VAGW CVTOC GRND WTR 11/01/11 11/02/11 11/02/11L54547-2 421422-VAGW SWD-VAGW CVTOC GRND WTR 11/03/11 11/03/11 11/03/11L54591-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 11/01/11 11/03/11 11/03/11L54591-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 11/01/11 11/03/11 11/03/11WG118427-1 MB CVTOC BLANK WTR 10/31/11 10/31/11 MB1 10/31/11WG118427-2 LCS CVTOC BLANK WTR 10/31/11 10/31/11 LEVEL1WG118427-3 SB CVTOC BLANK WTR 10/31/11 10/31/11 WG118427-1WG118427-4 LD CVTOC GRND WTR 10/31/11 10/31/11 L54349-1WG118427-5 MS CVTOC GRND WTR 10/31/11 10/31/11 L54393-1WG118427-6 MB CVTOC BLANK WTR 11/01/11 11/01/11 MB2 10/31/11WG118427-7 LCS CVTOC BLANK WTR 11/01/11 11/01/11 LEVEL1WG118427-8 LD CVTOC FRESH WTR 11/01/11 11/01/11 L53806-5WG118427-9 MS CVTOC FRESH WTR 11/01/11 11/01/11 L53806-8WG118427-10 MB CVTOC BLANK WTR 11/02/11 11/02/11 MB1 11/01/11WG118427-11 LCS CVTOC BLANK WTR 11/02/11 11/02/11 LEVEL1WG118427-12 SB CVTOC BLANK WTR 11/02/11 11/02/11 WG118427-10WG118427-13 LD CVTOC SEWER WTR 11/02/11 11/02/11 L54531-1WG118427-14 MS CVTOC SEWER WTR 11/02/11 11/02/11 L54531-1WG118427-15 MB CVDOC BLANK WTR 10/27/11 11/02/11 MB1 10/17/11WG118427-16 LCS CVDOC BLANK WTR 11/02/11 11/02/11 LEVEL1WG118427-17 SB CVDOC BLANK WTR 10/27/11 11/02/11 WG118427-15WG118427-18 LD CVDOC SEWER WTR 10/27/11 11/02/11 L54531-1WG118427-19 MS CVDOC SEWER WTR 10/27/11 11/02/11 L54531-1

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WG118427-20 MB CVDOC BLANK WTR 10/27/11 11/02/11 MB2 10/27/11WG118427-21 MB CVTOC BLANK WTR 11/03/11 11/03/11 MB1 11/03/11WG118427-22 LCS CVTOC BLANK WTR 11/03/11 11/03/11 LEVEL1WG118427-23 MB CVDOC BLANK WTR 11/03/11 11/03/11 MB1 11/03/11WG118427-24 LCS CVDOC BLANK WTR 11/03/11 11/03/11 LEVEL1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54076-2 421422-CHSW-M SWD-CHSW CVTOC FRESH WTR 09/26/11 09/30/11 09/30/11L54076-3 421422-CHSW-M SWD-CHSW CVTOC FRESH WTR 09/26/11 09/30/11 09/30/11L54081-1 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/23/11 09/30/11 09/30/11L54081-3 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/27/11 09/29/11 09/29/11L54084-1 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/26/11 09/29/11 09/29/11L54084-3 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/23/11 09/30/11 09/30/11L54086-1 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/27/11 09/29/11 09/29/11L54086-3 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/27/11 09/29/11 09/29/11L54087-1 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/28/11 09/29/11 09/29/11L54087-3 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/27/11 09/29/11 09/29/11L54174-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/21/11 09/30/11 09/30/11L54176-1 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 09/26/11 09/30/11 09/30/11L54176-2 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 09/26/11 09/30/11 09/30/11L54176-3 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 09/26/11 09/30/11 09/30/11L54286-1 421422-PUGW SWD-PUGW CVTOC GRND WTR 09/29/11 09/30/11 09/30/11L54307-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/28/11 09/30/11 09/30/11L54307-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/28/11 09/30/11 09/30/11L54307-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 09/28/11 09/30/11 09/30/11WG117769-1 MB CVTOC BLANK WTR 09/29/11 09/29/11 MB1 09/29/11WG117769-2 LCS CVTOC BLANK WTR 09/29/11 09/29/11 LEVEL1WG117769-3 SB CVTOC BLANK WTR 09/29/11 09/29/11 WG117769-1WG117769-5 MS CVTOC GRND WTR 09/29/11 09/29/11 L54086-3WG117769-6 LD CVTOC STORM WTR 09/30/11 09/30/11 L54176-2WG117769-7 LD CVTOC SEWER WTR 09/30/11 09/30/11 L54174-2WG117769-8 MS CVTOC SEWER WTR 09/30/11 09/30/11 L54174-2WG117769-9 MB CVTOC BLANK WTR 09/30/11 09/30/11 MB1 09/30/11WG117769-10 LCS CVTOC BLANK WTR 09/30/11 09/30/11 LEVEL1WG117769-11 SB CVTOC BLANK WTR 09/30/11 09/30/11 WG117769-9WG117769-12 LD CVTOC GRND WTR 09/30/11 09/30/11 L54081-1WG117769-13 MS CVTOC STORM WTR 09/30/11 09/30/11 L54176-3

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Work Group WG117427 - TSS

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54063-3 421422-DUGW SWD-DUGW CVTSS GRND WTR 09/13/11 09/16/11 09/19/11L54065-1 421422-DUGW SWD-DUGW CVTSS GRND WTR 09/12/11 09/16/11 09/19/11L54065-3 421422-DUGW SWD-DUGW CVTSS GRND WTR 09/12/11 09/16/11 09/19/11L54072-1 421422-DUGW SWD-DUGW CVTSS GRND WTR 09/12/11 09/16/11 09/19/11L54073-1 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/15/11 09/16/11 09/19/11L54073-3 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/15/11 09/16/11 09/19/11L54075-1 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/14/11 09/16/11 09/19/11L54125-1 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/12/11 09/16/11 09/19/11L54125-3 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/12/11 09/16/11 09/19/11L54125-4 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/12/11 09/16/11 09/19/11L54126-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/13/11 09/16/11 09/19/11L54126-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/13/11 09/16/11 09/19/11L54147-1 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/13/11 09/16/11 09/19/11L54147-2 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/13/11 09/16/11 09/19/11L54147-3 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/13/11 09/16/11 09/19/11L54147-4 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/13/11 09/16/11 09/19/11L54148-1 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/14/11 09/16/11 09/19/11L54148-2 423589-330-4 Green Rvr PCB/PAH Loading CVTSS FRESH WTR 09/14/11 09/16/11 09/19/11L54154-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/14/11 09/16/11 09/19/11L54154-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/14/11 09/16/11 09/19/11WG117427-1 MB CVTSS BLANK WTR 09/16/11 09/19/11 MB1 110916WG117427-2 LCS CVTSS BLANK WTR 09/16/11 09/19/11 LEVEL1WG117427-3 LD CVTSS GRND WTR 09/16/11 09/19/11 L54072-1WG117427-4 LD CVTSS FRESH WTR 09/16/11 09/19/11 L54125-3WG117427-5 LD CVTSS SEWER WTR 09/16/11 09/19/11 L54126-3


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL53871-3 421422-CFGW SWD-CFGW CVTSS GRND WTR 09/21/11 09/23/11 09/23/11L54020-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 09/19/11 09/23/11 09/23/11L54020-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 09/19/11 09/23/11 09/23/11L54020-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 09/19/11 09/23/11 09/23/11L54021-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 09/19/11 09/23/11 09/23/11L54021-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 09/19/11 09/23/11 09/23/11L54021-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 09/19/11 09/23/11 09/23/11L54073-4 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/21/11 09/23/11 09/23/11L54073-5 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/19/11 09/23/11 09/23/11

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L54075-3 421422-HTGW SWD-HTGW CVTSS GRND WTR 09/21/11 09/23/11 09/23/11L54076-1 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 09/19/11 09/23/11 09/23/11L54078-1 421422-ENLS SWD-ENLS CVTSS IW WTR 09/23/11 09/23/11 09/23/11L54079-1 421422-CFGW SWD-CFGW CVTSS GRND WTR 09/21/11 09/23/11 09/23/11L54081-1 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/23/11 09/23/11 09/23/11L54083-1 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/22/11 09/23/11 09/23/11L54083-3 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/22/11 09/23/11 09/23/11L54084-3 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/23/11 09/23/11 09/23/11L54144-3 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 09/21/11 09/23/11 09/23/11L54144-4 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 09/21/11 09/23/11 09/23/11L54144-5 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 09/21/11 09/23/11 09/23/11L54144-6 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 09/21/11 09/23/11 09/23/11L54144-8 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 09/21/11 09/23/11 09/23/11L54174-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/21/11 09/23/11 09/23/11WG117585-1 MB CVTSS BLANK WTR 09/23/11 09/23/11 MB1 110923WG117585-2 LCS CVTSS BLANK WTR 09/23/11 09/23/11 LEVEL1WG117585-3 LD CVTSS FRESH WTR 09/23/11 09/23/11 L54076-1WG117585-4 LD CVTSS GRND WTR 09/23/11 09/23/11 L54083-3WG117585-5 LD CVTSS IW WTR 09/23/11 09/23/11 L54078-1WG117585-6 LD CVTSS FRESH WTR 09/23/11 09/23/11 L54020-3WG117585-7 LD CVTSS SALT WTR 09/23/11 09/23/11 L54021-1WG117585-8 LD CVTSS SEWER WTR 09/23/11 09/23/11 L54174-2WG117585-9 MB CVTSS BLANK WTR 09/23/11 09/23/11 MB2 110923WG117585-10 LCS CVTSS BLANK WTR 09/23/11 09/23/11 LEVEL1WG117585-11 LD CVTSS SALT WTR 09/23/11 09/23/11 L54144-5


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL53350-1 421879-220 NPDES SW Sammamish CVTSS STORM WTR 09/26/11 09/30/11 10/03/11L53392-2 421879-220 NPDES SW Sammamish CVTSS STORM WTR 09/26/11 09/30/11 10/03/11L54087-1 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/28/11 09/30/11 10/03/11L54210-1 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-2 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-3 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-4 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-5 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-6 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-8 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-9 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-10 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11

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L54210-11 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-12 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-13 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-14 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-15 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-16 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-17 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-19 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-20 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-21 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-22 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-23 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-25 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-26 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-27 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-29 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-30 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-31 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-32 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-33 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-37 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-38 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-39 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-40 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-41 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-42 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-44 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-45 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-46 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-47 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-48 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54210-49 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 09/28/11 09/30/11 10/03/11L54286-1 421422-PUGW SWD-PUGW CVTSS GRND WTR 09/29/11 09/30/11 10/03/11L54307-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/28/11 09/30/11 10/03/11L54307-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/28/11 09/30/11 10/03/11L54307-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 09/28/11 09/30/11 10/03/11WG117708-1 MB CVTSS BLANK WTR 09/30/11 10/03/11 MB1 110930WG117708-2 LCS CVTSS BLANK WTR 09/30/11 10/03/11 LEVEL1WG117708-3 LD CVTSS FRESH WTR 09/30/11 10/03/11 L54210-6WG117708-4 MB CVTSS BLANK WTR 09/30/11 10/03/11 MB2 110930WG117708-5 LCS CVTSS BLANK WTR 09/30/11 10/03/11 LEVEL1

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WG117708-6 LD CVTSS FRESH WTR 09/30/11 10/03/11 L54210-44WG117708-7 MB CVTSS BLANK WTR 09/30/11 10/03/11 MB3 110930WG117708-8 LCS CVTSS BLANK WTR 09/30/11 10/03/11 LEVEL1WG117708-9 LD CVTSS SEWER WTR 09/30/11 10/03/11 L54307-1WG117708-10 LD CVTSS STORM WTR 09/30/11 10/03/11 L53350-1WG117708-11 LD CVTSS GRND WTR 09/30/11 10/03/11 L54087-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54271-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 10/17/11 10/19/11 10/21/11L54271-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 10/17/11 10/19/11 10/21/11L54271-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 10/17/11 10/19/11 10/21/11L54272-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 10/17/11 10/19/11 10/21/11L54272-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 10/17/11 10/19/11 10/21/11L54272-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 10/17/11 10/19/11 10/21/11L54349-2 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/17/11 10/19/11 10/21/11L54349-5 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/17/11 10/19/11 10/21/11L54349-6 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/17/11 10/19/11 10/21/11L54391-1 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/18/11 10/19/11 10/21/11L54391-2 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/18/11 10/19/11 10/21/11L54454-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/17/11 10/19/11 10/21/11L54454-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/17/11 10/19/11 10/21/11L54454-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/17/11 10/19/11 10/21/11WG118100-1 MB CVTSS BLANK WTR 10/19/11 10/21/11 MB1 111019WG118100-2 LCS CVTSS BLANK WTR 10/19/11 10/21/11 LEVEL1WG118100-3 LD CVTSS GRND WTR 10/19/11 10/21/11 L54391-2WG118100-4 LD CVTSS FRESH WTR 10/19/11 10/21/11 L54271-2WG118100-5 LD CVTSS SALT WTR 10/19/11 10/21/11 L54272-3WG118100-6 LD CVTSS SEWER WTR 10/19/11 10/21/11 L54454-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54391-5 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/19/11 10/19/11 10/21/11L54391-6 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/19/11 10/19/11 10/21/11L54391-7 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/19/11 10/19/11 10/21/11L54455-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/18/11 10/19/11 10/21/11L54455-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/18/11 10/19/11 10/21/11L54463-3 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 10/18/11 10/19/11 10/21/11L54463-4 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 10/18/11 10/19/11 10/21/11

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L54463-5 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 10/18/11 10/19/11 10/21/11L54463-6 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 10/18/11 10/19/11 10/21/11L54463-8 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 10/18/11 10/19/11 10/21/11WG118101-1 MB CVTSS BLANK WTR 10/19/11 10/21/11 MB1 111019WG118101-2 LCS CVTSS BLANK WTR 10/19/11 10/21/11 LEVEL1WG118101-3 LD CVTSS SALT WTR 10/19/11 10/21/11 L54463-3WG118101-4 LD CVTSS GRND WTR 10/19/11 10/21/11 L54391-7WG118101-5 LD CVTSS SEWER WTR 10/19/11 10/21/11 L54455-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54395-2 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/20/11 10/21/11 10/24/11L54395-5 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/21/11 10/21/11 10/24/11L54395-6 421422-CHGW SWD-CHGW CVTSS GRND WTR 10/21/11 10/21/11 10/24/11L54488-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/19/11 10/21/11 10/24/11L54488-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/19/11 10/21/11 10/24/11WG118160-1 MB CVTSS BLANK WTR 10/21/11 10/24/11 MB1 111021WG118160-2 LCS CVTSS BLANK WTR 10/21/11 10/24/11 LEVEL1WG118160-3 LD CVTSS GRND WTR 10/21/11 10/24/11 L54395-2WG118160-4 LD CVTSS SEWER WTR 10/21/11 10/24/11 L54488-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL53806-2 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/25/11 10/26/11 10/27/11L53806-3 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/25/11 10/26/11 10/27/11L53806-5 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/25/11 10/26/11 10/27/11L53806-6 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/25/11 10/26/11 10/27/11L53806-9 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/26/11 10/26/11 10/27/11L53806-11 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/26/11 10/26/11 10/27/11L54398-2 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/26/11 10/26/11 10/27/11L54398-5 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/26/11 10/26/11 10/27/11L54400-5 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/26/11 10/26/11 10/27/11L54531-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/25/11 10/26/11 10/27/11WG118247-1 MB CVTSS BLANK WTR 10/26/11 10/27/11 MB1 111026WG118247-2 LCS CVTSS BLANK WTR 10/26/11 10/27/11 LEVEL1WG118247-3 LD CVTSS FRESH WTR 10/26/11 10/27/11 L53806-2WG118247-4 LD CVTSS GRND WTR 10/26/11 10/27/11 L54398-2WG118247-5 LD CVTSS SEWER WTR 10/26/11 10/27/11 L54531-1

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Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL53806-8 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/27/11 10/28/11 10/31/11L53806-10 421422-CHSW-Q SWD-CHSW CVTSS FRESH WTR 10/27/11 10/28/11 10/31/11L54395-1 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/28/11 10/28/11 10/31/11L54400-1 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/28/11 10/28/11 10/31/11L54429-2 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/28/11 10/28/11 10/31/11L54429-6 421422-CHGW SWD-CHSW CVTSS GRND WTR 10/28/11 10/28/11 10/31/11L54493-1 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54494-1 421161 IW SURCHARGE CVTSS IW WTR 10/24/11 10/28/11 10/31/11L54494-2 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54495-1 421161 IW SURCHARGE CVTSS IW WTR 10/24/11 10/28/11 10/31/11L54495-2 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54496-1 421161 IW SURCHARGE CVTSS IW WTR 10/24/11 10/28/11 10/31/11L54496-2 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54503-1 421161 IW SURCHARGE CVTSS IW WTR 10/24/11 10/28/11 10/31/11L54503-2 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54504-1 421161 IW SURCHARGE CVTSS IW WTR 10/26/11 10/28/11 10/31/11L54504-2 421161 IW SURCHARGE CVTSS IW WTR 10/26/11 10/28/11 10/31/11L54505-1 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54505-2 421161 IW SURCHARGE CVTSS IW WTR 10/26/11 10/28/11 10/31/11L54506-1 421161 IW SURCHARGE CVTSS IW WTR 10/25/11 10/28/11 10/31/11L54506-2 421161 IW SURCHARGE CVTSS IW WTR 10/26/11 10/28/11 10/31/11L54513-1 421161 IW SURCHARGE CVTSS IW WTR 10/26/11 10/28/11 10/31/11L54532-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 10/26/11 10/28/11 10/31/11WG118281-1 MB CVTSS BLANK WTR 10/28/11 10/31/11 MB1 111028WG118281-2 LCS CVTSS BLANK WTR 10/28/11 10/31/11 LEVEL1WG118281-3 LD CVTSS FRESH WTR 10/28/11 10/31/11 L53806-10WG118281-4 LD CVTSS GRND WTR 10/28/11 10/31/11 L54429-6WG118281-5 LD CVTSS SEWER WTR 10/28/11 10/31/11 L54532-1WG118281-6 LD CVTSS IW WTR 10/28/11 10/31/11 L54495-1WG118281-7 MB CVTSS BLANK WTR 10/28/11 10/31/11 MB2 111028WG118281-8 LCS CVTSS BLANK WTR 10/28/11 10/31/11 LEVEL1WG118281-9 LD CVTSS GRND WTR 10/28/11 10/31/11 L54395-1

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Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54326-1 422027 Lab Lake Wash PBT-EPA Grant CVTSS STORM WTR 11/02/11 11/03/11 11/04/11L54326-11 422027 Lab Lake Wash PBT-EPA Grant CVTSS STORM WTR 11/02/11 11/03/11 11/04/11L54422-1 421879-210 NPDES SW Fall City CVTSS STORM WTR 10/28/11 11/03/11 11/04/11L54423-1 421879-210 NPDES SW Fall City CVTSS STORM WTR 10/28/11 11/03/11 11/04/11L54430-1 421422-CHSW-P2 SWD-CHSW CVTSS FRESH WTR 10/31/11 11/03/11 11/04/11L54430-2 421422-CHSW-P2 SWD-CHSW CVTSS FRESH WTR 10/31/11 11/03/11 11/04/11L54430-3 421422-CHSW-P2 SWD-CHSW CVTSS FRESH WTR 10/31/11 11/03/11 11/04/11L54541-1 421422-VAGW SWD-VAGW CVTSS GRND WTR 11/01/11 11/03/11 11/04/11L54547-2 421422-VAGW SWD-VAGW CVTSS GRND WTR 11/03/11 11/03/11 11/04/11L54591-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 11/01/11 11/03/11 11/04/11WG118384-1 MB CVTSS BLANK WTR 11/03/11 11/04/11 MB1 111103WG118384-2 LCS CVTSS BLANK WTR 11/03/11 11/04/11 LEVEL1WG118384-3 LD CVTSS FRESH WTR 11/03/11 11/04/11 L54430-3WG118384-4 LD CVTSS STORM WTR 11/03/11 11/04/11 L54422-1WG118384-5 LD CVTSS GRND WTR 11/03/11 11/04/11 L54541-1WG118384-6 LD CVTSS SEWER WTR 11/03/11 11/04/11 L54591-1WG118384-7 LD CVTSS STORM WTR 11/03/11 11/04/11 L54326-11

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Work Group WG117735 - Total and Dissolved Mercury

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54010-1 421184-100 OCS-City of Buckley MTHG-LOW EFFLUENT 09/12/11 10/03/11 10/03/11L54126-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/13/11 10/03/11 10/03/11L54126-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/13/11 10/03/11 10/03/11L54126-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/13/11 10/03/11 10/03/11L54145-1 423589-340-4 CSO Source Characterization MTHG-LOW BLANK WTR 09/14/11 10/03/11 10/03/11L54145-2 423589-340-4 CSO Source Characterization MTHG-LOW BLANK WTR 09/14/11 10/03/11 10/03/11L54154-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/14/11 10/03/11 10/03/11L54154-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/14/11 10/03/11 10/03/11L54154-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/14/11 10/03/11 10/03/11L54174-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/21/11 10/03/11 10/03/11L54174-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/21/11 10/03/11 10/03/11L54307-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/28/11 10/03/11 10/03/11L54307-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/28/11 10/03/11 10/03/11L54307-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/28/11 10/03/11 10/03/11L54307-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/28/11 10/03/11 10/03/11L54307-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 09/28/11 10/03/11 10/03/11L54307-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 09/28/11 10/03/11 10/03/11WG117735-1 MB MTHG-LOW BLANK WTR 10/03/11 10/03/11 METHOD BLANKWG117735-1 MB MTHG-LOW-DISS BLANK WTR 10/03/11 10/03/11 METHOD BLANKWG117735-2 SB MTHG-LOW BLANK WTR 10/03/11 10/03/11 WG117735-1 HG-LLOWWG117735-3 MS MTHG-LOW EFFLUENT 10/03/11 10/03/11 L54010-1 HG-LLOWWG117735-4 MSD MTHG-LOW EFFLUENT 10/03/11 10/03/11 WG117735-3 L54010-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54380-3 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTHG-LOW EFFLUENT 10/11/11 10/31/11 10/31/11L54454-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/17/11 10/31/11 10/31/11L54454-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/17/11 10/31/11 10/31/11L54454-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/17/11 10/31/11 10/31/11L54454-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/17/11 10/31/11 10/31/11L54454-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/17/11 10/31/11 10/31/11L54454-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/17/11 10/31/11 10/31/11L54455-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/18/11 10/31/11 10/31/11L54455-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/18/11 10/31/11 10/31/11L54455-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/18/11 10/31/11 10/31/11L54455-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/18/11 10/31/11 10/31/11L54488-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/19/11 10/31/11 10/31/11

LIMSView Batch Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Metals

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L54488-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/19/11 10/31/11 10/31/11L54488-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/19/11 10/31/11 10/31/11L54488-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/19/11 10/31/11 10/31/11L54531-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/25/11 10/31/11 10/31/11L54531-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/25/11 10/31/11 10/31/11L54532-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 10/26/11 10/31/11 10/31/11L54532-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 10/26/11 10/31/11 10/31/11WG118289-1 MB MTHG-LOW BLANK WTR 10/31/11 10/31/11 METHOD BLANKWG118289-1 MB MTHG-LOW-DISS BLANK WTR 10/31/11 10/31/11 METHOD BLANKWG118289-2 SB MTHG-LOW BLANK WTR 10/31/11 10/31/11 WG118289-1 HG-LLOWWG118289-3 MS MTHG-LOW-DISS SEWER WTR 10/31/11 10/31/11 L54488-3 HG-LLOWWG118289-4 MSD MTHG-LOW-DISS SEWER WTR 10/31/11 10/31/11 WG118289-3 L54488-3


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54591-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 11/01/11 11/28/11 11/28/11L54591-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 11/01/11 11/28/11 11/28/11WG118686-1 MB MTHG-LOW BLANK WTR 11/28/11 11/28/11 METHOD BLANKWG118686-1 MB MTHG-LOW-DISS BLANK WTR 11/28/11 11/28/11 METHOD BLANKWG118686-2 SB MTHG-LOW BLANK WTR 11/28/11 11/28/11 WG118686-1 HG-LLOWWG118686-3 MS MTHG-LOW-DISS SEWER WTR 11/28/11 11/28/11 L54591-1 HG-LLOWWG118686-4 MSD MTHG-LOW-DISS SEWER WTR 11/28/11 11/28/11 WG118686-3 L54591-1

Work Group WG117467 - Total ICPMS Metals

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL53996-1 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/16/11 09/20/11 09/26/11L53996-2 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/16/11 09/20/11 09/26/11L53996-3 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/16/11 09/20/11 09/26/11L54076-1 421422-CHSW-Q SWD-CHSW MTICPMS FRESH WTR 09/19/11 09/20/11 09/26/11L54106-1 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/11 09/20/11 09/26/11L54106-2 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/11 09/20/11 09/26/11L54106-3 421196-130 Roads Groundwater MTICPMS GRND WTR 09/19/11 09/20/11 09/26/11L54126-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/13/11 09/20/11 09/26/11L54126-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/13/11 09/20/11 09/26/11L54147-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/13/11 09/20/11 09/26/11L54147-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/13/11 09/20/11 09/26/11L54147-3 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/13/11 09/20/11 09/26/11L54147-4 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/13/11 09/20/11 09/26/11L54148-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/14/11 09/20/11 09/26/11

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L54148-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/14/11 09/20/11 09/26/11L54149-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/15/11 09/20/11 09/26/11L54149-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS FRESH WTR 09/15/11 09/20/11 09/26/11L54154-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/14/11 09/20/11 09/26/11L54154-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/14/11 09/20/11 09/26/11WG117467-1 MB MTICPMS BLANK WTR 09/20/11 09/26/11 METHOD BLANKWG117467-2 SB MTICPMS BLANK WTR 09/20/11 09/26/11 WG117467-1 MS-20WG117467-3 LD MTICPMS FRESH WTR 09/20/11 09/26/11 L54076-1 RPD-LIQWG117467-4 MS MTICPMS FRESH WTR 09/20/11 09/26/11 L54076-1 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL53556-1 421430-300 OCS-Lake Haven Utility District MTICPMS STORM WTR 09/19/11 09/26/11 09/28/11L53556-2 421430-300 OCS-Lake Haven Utility District MTICPMS STORM WTR 09/19/11 09/26/11 09/28/11L53899-1 421195-260 Ravensdale Monthly GW MTICPMS GRND WTR 09/21/11 09/26/11 09/28/11L54095-1 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/30/11 09/26/11 09/28/11L54095-2 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/30/11 09/26/11 09/28/11L54095-3 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 08/30/11 09/26/11 09/28/11L54106-5 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/11 09/26/11 09/28/11L54106-6 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/11 09/26/11 09/28/11L54106-7 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/11 09/26/11 09/28/11L54106-8 421196-130 Roads Groundwater MTICPMS GRND WTR 09/20/11 09/26/11 09/28/11L54106-9 421196-130 Roads Groundwater MTICPMS GRND WTR 09/21/11 09/26/11 09/28/11L54106-10 421196-130 Roads Groundwater MTICPMS GRND WTR 09/21/11 09/26/11 09/28/11L54106-11 421196-130 Roads Groundwater MTICPMS GRND WTR 09/21/11 09/26/11 09/28/11L54106-12 421196-130 Roads Groundwater MTICPMS GRND WTR 09/21/11 09/26/11 09/28/11L54106-13 421196-130 Roads Groundwater MTICPMS GRND WTR 09/22/11 09/26/11 09/28/11L54106-14 421196-130 Roads Groundwater MTICPMS GRND WTR 09/22/11 09/26/11 09/28/11L54106-15 421196-130 Roads Groundwater MTICPMS GRND WTR 09/22/11 09/26/11 09/28/11L54174-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/21/11 09/26/11 09/28/11L54247-1 421301A Georgetown Yard SW Monitoring MTICPMS STORM WTR 09/26/11 09/26/11 09/28/11WG117595-1 MB MTICPMS BLANK WTR 09/26/11 09/28/11 METHOD BLANKWG117595-2 SB MTICPMS BLANK WTR 09/26/11 09/28/11 WG117595-1 MS-20WG117595-3 LD MTICPMS BLANK WTR 09/26/11 09/28/11 L54095-2 RPD-LIQWG117595-4 MS MTICPMS BLANK WTR 09/26/11 09/28/11 L54095-2 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL53350-1 421879-220 NPDES SW Sammamish MTICPMS STORM WTR 09/26/11 09/30/11 10/10/11

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L53392-2 421879-220 NPDES SW Sammamish MTICPMS STORM WTR 09/26/11 09/30/11 10/03/11L54076-2 421422-CHSW-M SWD-CHSW MTICPMS FRESH WTR 09/26/11 09/30/11 10/03/11L54076-3 421422-CHSW-M SWD-CHSW MTICPMS FRESH WTR 09/26/11 09/30/11 10/03/11L54109-1 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-2 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-3 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-4 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-5 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-6 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/26/11 09/30/11 10/03/11L54109-7 423258-400 Reclaimed Water Soil Cove MTICPMS DRINK WTR 09/26/11 09/30/11 10/03/11L54109-8 423258-400 Reclaimed Water Soil Cove MTICPMS DRINK WTR 09/26/11 09/30/11 10/03/11L54109-9 423258-400 Reclaimed Water Soil Cove MTICPMS DRINK WTR 09/26/11 09/30/11 10/03/11L54126-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/13/11 09/30/11 10/10/11L54307-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/28/11 09/30/11 10/03/11L54307-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/28/11 09/30/11 10/03/11L54307-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 09/28/11 09/30/11 10/03/11WG117692-1 MB MTICPMS BLANK WTR 09/30/11 10/03/11 METHOD BLANKWG117692-2 SB MTICPMS BLANK WTR 09/30/11 10/03/11 WG117692-1 MS-20WG117692-3 LD MTICPMS FRESH WTR 09/30/11 10/03/11 L54076-2 RPD-LIQWG117692-4 MS MTICPMS FRESH WTR 09/30/11 10/03/11 L54076-2 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL53142-1 421879-210 NPDES SW Fall City MTICPMS STORM WTR 10/10/11 10/20/11 10/21/11L53142-2 421879-210 NPDES SW Fall City MTICPMS STORM WTR 10/10/11 10/20/11 10/21/11L53697-1 421879-210 NPDES SW Fall City MTICPMS STORM WTR 10/10/11 10/20/11 10/21/11L54096-1 421195-260 Ravensdale Monthly GW MTICPMS GRND WTR 10/18/11 10/20/11 10/21/11L54310-1 421301A Georgetown YardSW Monitoring MTICPMS STORM WTR 10/11/11 10/20/11 10/21/11L54375-1 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/27/11 10/20/11 10/21/11L54375-2 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/27/11 10/20/11 10/21/11L54375-3 423258-400 Reclaimed Water Soil Cove MTICPMS OTHR WTR 09/27/11 10/20/11 10/21/11L54380-1 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTICPMS INFLUENT 10/11/11 10/20/11 10/21/11L54380-3 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTICPMS EFFLUENT 10/11/11 10/20/11 10/21/11L54380-4 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTICPMS EFFLUENT 10/11/11 10/20/11 10/21/11L54454-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/17/11 10/20/11 10/21/11L54454-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/17/11 10/20/11 10/21/11L54454-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/17/11 10/20/11 10/21/11L54455-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/18/11 10/20/11 10/21/11L54455-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/18/11 10/20/11 10/21/11WG118112-1 MB MTICPMS BLANK WTR 10/20/11 10/21/11 METHOD BLANK

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WG118112-2 SB MTICPMS BLANK WTR 10/20/11 10/21/11 WG118112-1 MS-20WG118112-3 LD MTICPMS OTHR WTR 10/20/11 10/21/11 L54375-2 RPD-LIQWG118112-4 MS MTICPMS OTHR WTR 10/20/11 10/21/11 L54375-2 MS-20WG118112-5 LD MTICPMS EFFLUENT 10/20/11 10/21/11 L54380-4 RPD-LIQWG118112-6 MS MTICPMS EFFLUENT 10/20/11 10/21/11 L54380-4 MS-20WG118112-7 LD MTICPMS SEWER WTR 10/20/11 10/21/11 L54454-2 RPD-LIQWG118112-8 MS MTICPMS SEWER WTR 10/20/11 10/21/11 L54454-2 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54488-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/19/11 01/10/12 01/12/12L54488-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/19/11 01/10/12 01/12/12L54531-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/25/11 01/10/12 01/12/12L54532-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 10/26/11 01/10/12 01/12/12L54591-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 11/01/11 01/10/12 01/12/12WG119368-1 MB MTICPMS BLANK WTR 01/10/12 01/12/12 METHOD BLANKWG119368-2 SB MTICPMS BLANK WTR 01/10/12 01/12/12 WG119368-1 MS-20WG119368-3 LD MTICPMS SEWER WTR 01/10/12 01/12/12 L54488-2 RPD-LIQWG119368-4 MS MTICPMS SEWER WTR 01/10/12 01/12/12 L54488-2 MS-20

Work Group WG117646 - Dissolved ICPMS Metals

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL53871-3 421422-CFGW SWD-CFGW MTICPMS-DISS GRND WTR 09/21/11 09/27/11 09/27/11L54073-4 421422-HTGW SWD-HTGW MTICPMS-DISS GRND WTR 09/21/11 09/27/11 09/27/11L54073-5 421422-HTGW SWD-HTGW MTICPMS-DISS GRND WTR 09/19/11 09/27/11 09/27/11L54075-3 421422-HTGW SWD-HTGW MTICPMS-DISS GRND WTR 09/21/11 09/27/11 09/27/11L54076-1 421422-CHSW-Q SWD-CHSW MTICPMS-DISS FRESH WTR 09/19/11 09/27/11 09/27/11L54076-2 421422-CHSW-M SWD-CHSW MTICPMS-DISS FRESH WTR 09/26/11 09/27/11 09/27/11L54076-3 421422-CHSW-M SWD-CHSW MTICPMS-DISS FRESH WTR 09/26/11 09/27/11 09/27/11L54079-1 421422-CFGW SWD-CFGW MTICPMS-DISS GRND WTR 09/21/11 09/27/11 09/27/11L54081-1 421422-PUGW SWD-PUGW MTICPMS-DISS GRND WTR 09/23/11 09/27/11 09/27/11L54083-1 421422-PUGW SWD-PUGW MTICPMS-DISS GRND WTR 09/22/11 09/27/11 09/27/11L54083-3 421422-PUGW SWD-PUGW MTICPMS-DISS GRND WTR 09/22/11 09/27/11 09/27/11L54084-1 421422-PUGW SWD-PUGW MTICPMS-DISS GRND WTR 09/26/11 09/27/11 09/27/11L54084-3 421422-PUGW SWD-PUGW MTICPMS-DISS GRND WTR 09/23/11 09/27/11 09/27/11L54117-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS FRESH WTR 09/07/11 09/27/11 09/27/11L54117-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS FRESH WTR 09/07/11 09/27/11 09/27/11L54117-3 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS FRESH WTR 09/07/11 09/27/11 09/27/11L54117-4 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS FRESH WTR 09/07/11 09/27/11 09/27/11

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L54174-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/21/11 09/27/11 09/27/11WG117646-1 MB MTICPMS-DISS BLANK WTR 09/27/11 09/27/11 METHOD BLANKWG117646-2 SB MTICPMS-DISS BLANK WTR 09/27/11 09/27/11 WG117646-1 MS-20WG117646-3 LD MTICPMS-DISS FRESH WTR 09/27/11 09/27/11 L54076-2 RPD-LIQWG117646-4 MS MTICPMS-DISS FRESH WTR 09/27/11 09/27/11 L54076-2 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54126-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/13/11 10/17/11 10/18/11L54154-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/14/11 10/17/11 10/18/11L54307-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/28/11 10/17/11 10/18/11L54307-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/28/11 10/17/11 10/18/11L54307-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 09/28/11 10/17/11 10/18/11L54323-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/12/11 10/17/11 10/18/11L54324-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/14/11 10/17/11 10/18/11L54344-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/12/11 10/17/11 10/18/11L54345-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/12/11 10/17/11 10/18/11L54345-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/12/11 10/17/11 10/18/11L54346-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/13/11 10/17/11 10/18/11L54346-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/13/11 10/17/11 10/18/11L54346-5 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/13/11 10/17/11 10/18/11L54346-6 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/13/11 10/17/11 10/18/11L54348-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/14/11 10/17/11 10/18/11L54348-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/14/11 10/17/11 10/18/11L54348-5 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/14/11 10/17/11 10/18/11L54348-6 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/14/11 10/17/11 10/18/11WG118036-1 MB MTICPMS-DISS BLANK WTR 10/17/11 10/18/11 METHOD BLANKWG118036-2 SB MTICPMS-DISS BLANK WTR 10/17/11 10/18/11 WG118036-1 MS-20WG118036-3 LD MTICPMS-DISS GRND WTR 10/17/11 10/18/11 L54345-1 RPD-LIQWG118036-4 MS MTICPMS-DISS GRND WTR 10/17/11 10/18/11 L54345-1 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54309-1 421879-220 NPDES SW Sammamish MTICPMS-DISS STORM WTR 10/21/11 10/24/11 10/27/11L54309-4 421879-220 NPDES SW Sammamish MTICPMS-DISS STORM WTR 10/21/11 10/24/11 10/27/11L54349-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/17/11 10/24/11 10/27/11L54349-5 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/17/11 10/24/11 10/27/11L54349-6 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/17/11 10/24/11 10/27/11L54391-1 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/18/11 10/24/11 10/27/11

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L54391-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/18/11 10/24/11 10/27/11L54391-5 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/19/11 10/24/11 10/27/11L54391-6 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/19/11 10/24/11 10/27/11L54391-7 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/19/11 10/24/11 10/27/11L54395-2 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/20/11 10/24/11 10/27/11L54395-5 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/21/11 10/24/11 10/27/11L54395-6 421422-CHGW SWD-CHGW MTICPMS-DISS GRND WTR 10/21/11 10/24/11 10/27/11L54454-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/17/11 10/24/11 10/27/11L54454-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/17/11 10/24/11 10/27/11L54454-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/17/11 10/24/11 10/27/11L54455-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/18/11 10/24/11 10/27/11L54455-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/18/11 10/24/11 10/27/11L54488-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/19/11 10/24/11 10/27/11L54488-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/19/11 10/24/11 10/27/11WG118171-1 MB MTICPMS-DISS BLANK WTR 10/24/11 10/27/11 METHOD BLANKWG118171-2 SB MTICPMS-DISS BLANK WTR 10/24/11 10/27/11 WG118171-1 MS-20WG118171-3 LD MTICPMS-DISS GRND WTR 10/24/11 10/27/11 L54391-7 RPD-LIQWG118171-4 MS MTICPMS-DISS GRND WTR 10/24/11 10/27/11 L54391-7 MS-20


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Datge CommentsL54531-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/25/11 01/12/12 01/12/12L54532-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 10/26/11 01/12/12 01/12/12L54591-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 11/01/11 01/12/12 01/12/12WG119371-1 MB MTICPMS-DISS BLANK WTR 01/12/12 01/12/12 METHOD BLANKWG119371-2 SB MTICPMS-DISS BLANK WTR 01/12/12 01/12/12 WG119371-1 MS-20WG119371-3 LD MTICPMS-DISS SEWER WTR 01/12/12 01/12/12 L54531-1 RPD-LIQWG119371-4 MS MTICPMS-DISS SEWER WTR 01/12/12 01/12/12 L54531-1 MS-20

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Work Group WG117498 - PAHs/Phthalates

Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54126-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/13/11 09/20/11 10/10/11L54126-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/13/11 09/20/11 10/10/11L54154-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/14/11 09/20/11 10/10/11L54154-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/14/11 09/20/11 10/10/11WG117498-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/20/11 09/29/11 MB110920WG117498-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/20/11 09/29/11 WG117498-1WG117498-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/20/11 09/29/11 WG117498-2 WG117498-1WG117498-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/20/11 10/10/11 L54154-3


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54174-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/21/11 09/27/11 10/12/11WG117498-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/20/11 09/29/11 WG117498-1WG117498-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/20/11 09/29/11 WG117498-2 WG117498-1WG117498-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/20/11 10/10/11 L54154-3WG117625-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/27/11 10/12/11 MB110927WG117625-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 09/27/11 10/12/11 WG117625-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54307-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/28/11 10/04/11 10/12/11L54307-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/28/11 10/04/11 10/12/11L54307-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 09/28/11 10/04/11 10/12/11WG117764-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/04/11 10/12/11 MB111004WG117764-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/04/11 10/12/11 WG117764-1WG117764-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/04/11 10/12/11 WG117764-2 WG117764-1WG117764-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/04/11 10/12/11 L54307-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54454-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/17/11 10/24/11 11/08/11L54454-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/17/11 10/24/11 11/08/11L54454-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/17/11 10/24/11 11/08/11L54455-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/18/11 10/24/11 11/08/11L54455-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/18/11 10/24/11 11/08/11

LIMSView Batch Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Organics

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LIMSView Batch Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Organics

L54488-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/19/11 10/24/11 11/08/11L54488-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/19/11 10/24/11 11/08/11WG118172-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/24/11 11/08/11 MB111024WG118172-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/24/11 11/08/11 WG118172-1WG118172-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/24/11 11/08/11 WG118172-2 WG118172-1WG118172-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/24/11 11/08/11 L54454-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54531-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/25/11 10/31/11 11/08/11L54532-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 10/26/11 10/31/11 11/08/11WG118172-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/24/11 11/08/11 WG118172-1WG118172-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/24/11 11/08/11 WG118172-2 WG118172-1WG118307-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/31/11 11/08/11 MB111031WG118307-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 10/31/11 11/08/11 WG118307-1


Sample Project Project Description List Type Matrix Collect Date Prep Date Analysis Date CommentsL54591-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 11/01/11 11/08/11 12/13/11WG118436-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 11/08/11 12/13/11 MB111107WG118436-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 11/08/11 12/13/11 WG118436-1WG118436-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 11/08/11 12/13/11 WG118436-2 WG118436-1

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WG117545

MB:WG117545-1 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL

LCS:WG117545-2 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10.7 107 85--115

SB:WG117545-3 MB:WG117545-1 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L <MDL 20 20.7 103 80--120

LD:WG117545-4 L54073-5 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HTGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 16.4 15.7 5 0--20

MS:WG117545-5 L54075-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HTGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 15 10 24.5 95 75--125

LD:WG117545-6 L54076-1 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 11.4 11.5 1 0--20

LD:WG117545-7 L54149-2 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

LIMSView QC Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Conventionals

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Total Organic Carbon 0.5 1 mg/L 4.57 4.69 3 0--20

MS:WG117545-8 L54147-1 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.82 10 12.1 102 75--125MB:WG117545-9 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL


MS:WG117545-11 L54154-2 Matrix: SEWER WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 50 100 mg/L 463 10 1450 98 75--125


LD:WG117545-13 L54020-1 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.07 1.81 13 0--20

MS:WG117545-14 L54020-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.18 10 12.4 102 75--125

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LD:WG117545-15 L54021-1 Matrix: SALT WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.86 1.78 4 0--20

MS:WG117545-16 L54021-3 Matrix: SALT WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.02 10 11.9 98 75--125

MB:WG117545-17 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualDissolved Organic Carbon 0.5 1 mg/L <MDL

LCS:WG117545-18 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 10 10.4 104 85--115

SB:WG117545-19 MB:WG117545-17 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L <MDL 10 10.3 103 80--120


LD:WG117545-21 L54149-1 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

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Dissolved Organic Carbon 0.5 1 mg/L 2.09 2.43 15 0--20

MS:WG117545-22 L54149-2 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 3.72 10 14 102 75--125





LD:WG117545-27 L54020-1 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.93 1.91 1 0--20

MS:WG117545-28 L54020-3 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.95 10 12 101 75--125

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LD:WG117545-29 L54021-1 Matrix: SALT WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.91 1.73 10 0--20

MS:WG117545-30 L54021-3 Matrix: SALT WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.67 10 11.5 99 75--125

LD:WG117545-31 L54154-2 Matrix: SEWER WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 50 100 mg/L 463 481 4 0--20

LD:WG117545-32 L54154-3 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 5 10 mg/L 93.8 95.3 2 0--20

MS:WG117545-33 L54154-3 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 5 10 mg/L 93.8 10 198 104 75--125

WG117810



SB:WG117810-3 MB:WG117810-1 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit

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Dissolved Organic Carbon 0.5 1 mg/L <MDL 10 10.5 105 80--120

LD:WG117810-4 L54176-1 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 8.84 9.55 8 0--20

MS:WG117810-5 L54176-3 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:422027 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 11.9 10 22.6 107 75--125


MB:WG117810-7 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualDissolved Organic Carbon 0.5 1 mg/L <MDLMS:WG117810-8 L54307-3 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 5 10 mg/L 102 10 207 104 75--125


LD:WG117810-10 L54174-2 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 5 10 mg/L 226 225 0 0--20


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LD:WG117810-14 L54190-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.53 1.39 10 0--20

MS:WG117810-15 L54190-5 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.75 10 12.7 110 75--125


WG118166



SB:WG118166-3 MB:WG118166-1 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit

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Total Organic Carbon 0.5 1 mg/L <MDL 10 9.92 99 80--120

LD:WG118166-4 L54391-2 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.78 0.81 0--20

MS:WG118166-5 L54349-6 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.34 10 11.6 102 75--125


MS:WG118166-7 L54272-3 Matrix: SALT WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.92 10 11.8 99 75--125LD:WG118166-8 L54454-3 Matrix: SEWER WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 18 35 mg/L 141 157 11 0--20




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LD:WG118166-15 L54457-1 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:421195-470 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 3.5 3.74 7 0--20


MS:WG118166-17 L54272-3 Matrix: SALT WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 1 2 mg/L 2.26 10 22.7 102 75--125


MS:WG118166-19 L54457-2 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:421195-470 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 1 2 mg/L 3.75 10 25.8 110 75--125

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LD:WG118166-21 L54454-3 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 18 35 mg/L 85.4 86 1 0--20







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WG118427


LCS:WG118427-2 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10.6 106 85--115SB:WG118427-3 MB:WG118427-1 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L <MDL 10 9.98 100 80--120

LD:WG118427-4 L54349-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.23 1.12 9 0--20



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MS:WG118427-9 L53806-8 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHSW-Q Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 6.26 10 16.4 101 75--125






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MS:WG118427-19 L54531-1 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 18 35 mg/L 916 10 1350 123 75--125




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WG117769


LCS:WG117769-2 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10.2 102 85--115SB:WG117769-3 MB:WG117769-1 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L <MDL 10 9.94 99 80--120

MS:WG117769-5 L54086-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.65 10 12.7 101 75--125

LD:WG117769-6 L54176-2 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 9.08 10.1 11 0--20


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LD:WG117769-12 L54081-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.7 0.73 0--20

MS:WG117769-13 L54176-3 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 1 2 mg/L 13.2 10 31.9 93 75--125

WG117427

MB:WG117427-1 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualTotal Suspended Solids 0.5 1 mg/L <MDL

LCS:WG117427-2 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimit

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Total Suspended Solids 5 10 mg/L 100 112 112 80--120

LD:WG117427-3 L54072-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-DUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 23 23.6 3 0--25

LD:WG117427-4 L54125-3 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:423589-330-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 4.4 4.6 4 0--25

LD:WG117427-5 L54126-3 Matrix: SEWER WTR Listtype:CVTSS Method:SM2540-D Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 20 40 mg/L 260 296 13 0--25

WG117585


LCS:WG117585-2 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Suspended Solids 5 10 mg/L 100 89 89 80--120

LD:WG117585-3 L54076-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 4.8 4.8 0 0--25

LD:WG117585-4 L54083-3 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

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Total Suspended Solids 1 2 mg/L 33.8 35 3 0--25

LD:WG117585-5 L54078-1 Matrix: IW WTR Listtype:CVTSS Method:SM2540-D Project:421422-ENLS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 20 40 mg/L 444 428 4 0--25


LD:WG117585-7 L54021-1 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L 3 3.6 0--25

LD:WG117585-8 L54174-2 Matrix: SEWER WTR Listtype:CVTSS Method:SM2540-D Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 5 10 mg/L 152 152 0 0--25MB:WG117585-9 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualTotal Suspended Solids 0.5 1 mg/L <MDL


LD:WG117585-11 L54144-5 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:421250BS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1.1 22 mg/L 2.9 2.7 0--25

WG117708

MB:WG117708-1 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value Qual

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Total Suspended Solids 0.5 1 mg/L <MDL


LD:WG117708-3 L54210-6 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 4.4 4.8 9 0--25


LCS:WG117708-5 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Suspended Solids 5 10 mg/L 100 98 98 80--120LD:WG117708-6 L54210-44 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1 <MDL 0--25




of 23


LD:WG117708-10 L53350-1 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:421879-220 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 5 10 mg/L 50 51 2 0--25

LD:WG117708-11 L54087-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1 1.2 0--25

WG118100


LCS:WG118100-2 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Suspended Solids 5 10 mg/L 100 101 101 80--120LD:WG118100-3 L54391-2 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1 <MDL 0--25


LD:WG118100-5 L54272-3 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L 5.6 6.4 0--25


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WG118101



LD:WG118101-3 L54463-3 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:421250BS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L 3 2.6 0--25

LD:WG118101-4 L54391-7 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.4 1.8 0--25LD:WG118101-5 L54455-2 Matrix: SEWER WTR Listtype:CVTSS Method:SM2540-D Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 10 20 mg/L 306 320 4 0--25

WG118160



LD:WG118160-3 L54395-2 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

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Total Suspended Solids 1.1 2.2 mg/L <MDL <MDL 0--25


WG118247



LD:WG118247-3 L53806-2 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 3.6 3 18 0--25

LD:WG118247-4 L54398-2 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1 <MDL 0--25


WG118281


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LD:WG118281-3 L53806-10 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 5.4 4.6 16 0--25

LD:WG118281-4 L54429-6 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1 <MDL 0--25

LD:WG118281-5 L54532-1 Matrix: SEWER WTR Listtype:CVTSS Method:SM2540-D Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 50 100 mg/L 1110 1080 3 0--25LD:WG118281-6 L54495-1 Matrix: IW WTR Listtype:CVTSS Method:SM2540-D Project:421161 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 25 50 mg/L 245 225 9 0--25



LD:WG118281-9 L54395-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L <MDL <MDL 0--25

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WG118384



LD:WG118384-3 L54430-3 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-P2 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.2 1.2 0--25

LD:WG118384-4 L54422-1 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:421879-210 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 10 20 mg/L 232 226 3 0--25LD:WG118384-5 L54541-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-VAGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1.1 2.2 mg/L 1.1 <MDL 0--25


LD:WG118384-7 L54326-11 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 2.5 5 mg/L 127 135 7 0--25

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WG117735

MB:WG117735-1 Matrix: BLANK WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualMercury, Total, CVAA 0.005 0.015 ug/L <MDL

MB:WG117735-1 Matrix: BLANK WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualMercury, Dissolved, CVAA 0.005 0.015 ug/L <MDL

SB:WG117735-2 MB:WG117735-1 Matrix: BLANK WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L <MDL 0.2 0.193 96 85--115

MSD:WG117735-4 MS:WG117735-3 L54010-1 Matrix: EFFLUENT Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:421184-100 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L 0.009 0.2 0.2 95 75--125 0.2 0.206 98 3 0--20

WG118289




LIMSView QC Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Metals

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MSD:WG118289-4 MS:WG118289-3 L54488-3 Matrix: SEWER WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L 0.0081 0.2 0.19 91 75--125 0.2 0.19 91 0 0--20

WG118686




MSD:WG118686-4 MS:WG118686-3 L54591-1 Matrix: SEWER WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L 0.0165 0.05 0.0587 84 75--125 0.05 0.0598 87 2 0--20

WG117467

MB:WG117467-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDLSodium, Total, ICP-MS 100 100 ug/L <MDLMagnesium, Total, ICP-MS 50 50 ug/L <MDLAluminum, Total, ICP-MS 2 10 ug/L <MDLPotassium, Total, ICP-MS 100 500 ug/L <MDLCalcium, Total, ICP-MS 50 50 ug/L <MDLVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLIron, Total, ICP-MS 10 50 ug/L <MDL

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Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDLCobalt, Total, ICP-MS 0.05 0.25 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Total, ICP-MS 0.5 1 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLTin, Total, ICP-MS 0.3 1.5 ug/L <MDLAntimony, Total, ICP-MS 0.3 1 ug/L <MDLBarium, Total, ICP-MS 0.05 0.25 ug/L <MDLThallium, Total, ICP-MS 0.04 0.2 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG117467-2 MB:WG117467-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.6 103 85--115Sodium, Total, ICP-MS 100 100 ug/L <MDL 5000 5350 107 85--115Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5320 106 85--115Aluminum, Total, ICP-MS 2 10 ug/L <MDL 20 22.2 111 85--115Potassium, Total, ICP-MS 100 500 ug/L <MDL 5000 4960 99 85--115Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4960 99 85--115Vanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 20.3 102 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 19.1 96 85--115Iron, Total, ICP-MS 10 50 ug/L <MDL 5000 5110 102 85--115Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.8 104 85--115Cobalt, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.5 98 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.3 102 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 20.1 101 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 19.5 98 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 99 85--115Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20.3 102 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.9 105 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.6 98 85--115Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 20.3 102 85--115Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 20.2 101 85--115Barium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19 95 85--115Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 21 105 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.9 104 85--115

of 23


LD:WG117467-3 L54076-1 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Sodium, Total, ICP-MS 100 100 ug/L 6430 6230 3 0--20Magnesium, Total, ICP-MS 50 50 ug/L 3420 3380 1 0--20Aluminum, Total, ICP-MS 2 10 ug/L 269 267 1 0--20Potassium, Total, ICP-MS 100 500 ug/L 3320 3320 0 0--20Calcium, Total, ICP-MS 50 50 ug/L 10300 10000 2 0--20Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.26 1.23 3 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 0.74 0.72 0--20Iron, Total, ICP-MS 10 50 ug/L 370 370 0 0--20Manganese, Total, ICP-MS 0.1 0.5 ug/L 12.8 12.6 1 0--20Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.19 0.19 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 2.73 2.74 0 0--20Copper, Total, ICP-MS 0.4 2 ug/L 13 12.9 1 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 34.5 33.8 2 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.62 0.63 2 0--20Selenium, Total, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL <MDL 0--20Antimony, Total, ICP-MS 0.3 1 ug/L 1.58 1.54 3 0--20Barium, Total, ICP-MS 0.05 0.25 ug/L 13.6 13.2 2 0--20Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 0.912 0.914 0 0--20

MS:WG117467-4 L54076-1 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-Q Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 75--125Sodium, Total, ICP-MS 100 100 ug/L 6430 5000 12200 116 75--125Magnesium, Total, ICP-MS 50 50 ug/L 3420 5000 8740 106 75--125Aluminum, Total, ICP-MS 2 10 ug/L 269 20 283 4xRule 75--125Potassium, Total, ICP-MS 100 500 ug/L 3320 5000 8470 103 75--125Calcium, Total, ICP-MS 50 50 ug/L 10300 5000 15400 103 75--125Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.26 20 22.5 106 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 0.74 20 20.5 99 75--125Iron, Total, ICP-MS 10 50 ug/L 370 5000 5620 105 75--125Manganese, Total, ICP-MS 0.1 0.5 ug/L 12.8 20 34.2 107 75--125Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.19 20 19.9 98 75--125

of 23


Nickel, Total, ICP-MS 0.1 0.5 ug/L 2.73 20 24.5 109 75--125Copper, Total, ICP-MS 0.4 2 ug/L 13 20 35 110 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 34.5 20 54.4 99 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.62 20 21.4 104 75--125Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20.4 102 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 21.6 108 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 20.1 100 75--125Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 19.4 97 75--125Antimony, Total, ICP-MS 0.3 1 ug/L 1.58 20 21.8 101 75--125Barium, Total, ICP-MS 0.05 0.25 ug/L 13.6 20 32.6 95 75--125Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 21.3 107 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 0.912 20 22 106 75--125

WG117595

MB:WG117595-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualMagnesium, Total, ICP-MS 50 50 ug/L <MDLCalcium, Total, ICP-MS 50 50 ug/L <MDLVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLManganese, Total, ICP-MS 0.1 0.5 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Total, ICP-MS 0.5 1 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG117595-2 MB:WG117595-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitMagnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5090 102 85--115Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4860 97 85--115Vanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 19.7 98 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 19.8 99 85--115Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 100 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.1 101 85--115

of 23


Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 20.1 101 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 19.5 97 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.6 98 85--115Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20 100 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.6 98 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.7 99 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20 100 85--115

LD:WG117595-3 L54095-2 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423258-400 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitMagnesium, Total, ICP-MS 50 50 ug/L 6260 6170 1 0--20Calcium, Total, ICP-MS 50 50 ug/L 60800 61500 1 0--20Vanadium, Total, ICP-MS 0.075 0.375 ug/L 19.2 19.8 3 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 7.4 7.59 3 0--20Manganese, Total, ICP-MS 0.1 0.5 ug/L 44.2 45 2 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 7.68 8.03 4 0--20Copper, Total, ICP-MS 0.4 2 ug/L 13.7 14.3 4 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 30.1 31.5 5 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 5.98 6.08 2 0--20Selenium, Total, ICP-MS 0.5 1 ug/L 1.35 1.58 16 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.08 0.095 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.19 0.2 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 3.21 3.09 4 0--20

MS:WG117595-4 L54095-2 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423258-400 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitMagnesium, Total, ICP-MS 50 50 ug/L 6260 5000 12200 119 75--125Calcium, Total, ICP-MS 50 50 ug/L 60800 5000 69000 4xRule 75--125Vanadium, Total, ICP-MS 0.075 0.375 ug/L 19.2 20 38.5 97 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 7.4 20 26 93 75--125Manganese, Total, ICP-MS 0.1 0.5 ug/L 44.2 20 63.6 97 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 7.68 20 27.7 100 75--125Copper, Total, ICP-MS 0.4 2 ug/L 13.7 20 34.5 104 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 30.1 20 50 99 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 5.98 20 26.3 101 75--125Selenium, Total, ICP-MS 0.5 1 ug/L 1.35 20 21 98 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.08 20 17.8 88 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.19 20 19.8 98 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 3.21 20 22.8 98 75--125

of 23


WG117692

MB:WG117692-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDLSodium, Total, ICP-MS 100 100 ug/L <MDLMagnesium, Total, ICP-MS 50 50 ug/L <MDLAluminum, Total, ICP-MS 2 10 ug/L 2.7 BPotassium, Total, ICP-MS 100 500 ug/L <MDLCalcium, Total, ICP-MS 50 50 ug/L <MDLVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLIron, Total, ICP-MS 10 50 ug/L <MDLManganese, Total, ICP-MS 0.1 0.5 ug/L <MDLCobalt, Total, ICP-MS 0.05 0.25 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Total, ICP-MS 0.5 1 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLTin, Total, ICP-MS 0.3 1.5 ug/L <MDLAntimony, Total, ICP-MS 0.3 1 ug/L <MDLBarium, Total, ICP-MS 0.05 0.25 ug/L <MDLThallium, Total, ICP-MS 0.04 0.2 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG117692-2 MB:WG117692-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.5 102 85--115Sodium, Total, ICP-MS 100 100 ug/L <MDL 5000 5080 102 85--115Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 5060 101 85--115Aluminum, Total, ICP-MS 2 10 ug/L 2.7 20 25.6 115 85--115Potassium, Total, ICP-MS 100 500 ug/L <MDL 5000 4920 98 85--115Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4600 92 85--115Vanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 18.5 93 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 18.6 93 85--115Iron, Total, ICP-MS 10 50 ug/L <MDL 5000 4790 96 85--115

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Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 18.7 93 85--115Cobalt, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 18.6 93 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.4 97 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 19.3 96 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 21.1 105 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.6 98 85--115Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20.5 103 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.8 99 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.3 97 85--115Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 17.9 89 85--115Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 17.7 89 85--115Barium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.8 99 85--115Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 17.5 87 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 17.6 88 85--115

LD:WG117692-3 L54076-2 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Sodium, Total, ICP-MS 100 100 ug/L 5700 5630 1 0--20Magnesium, Total, ICP-MS 50 50 ug/L 6080 5950 2 0--20Aluminum, Total, ICP-MS 2 10 ug/L 474 469 1 0--20Potassium, Total, ICP-MS 100 500 ug/L 1630 1640 1 0--20Calcium, Total, ICP-MS 50 50 ug/L 14100 14100 0 0--20Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.55 1.55 0 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 0.77 0.76 0--20Iron, Total, ICP-MS 10 50 ug/L 646 643 1 0--20Manganese, Total, ICP-MS 0.1 0.5 ug/L 72.9 73 0 0--20Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.278 0.274 2 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 1.35 1.34 0 0--20Copper, Total, ICP-MS 0.4 2 ug/L 2 2 2 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 11.7 12.2 5 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.903 0.914 1 0--20Selenium, Total, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.069 0.071 0--20Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL <MDL 0--20Antimony, Total, ICP-MS 0.3 1 ug/L <MDL <MDL 0--20Barium, Total, ICP-MS 0.05 0.25 ug/L 8.01 8.09 1 0--20Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 0.39 0.38 0--20

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MS:WG117692-4 L54076-2 Matrix: FRESH WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 99 75--125Sodium, Total, ICP-MS 100 100 ug/L 5700 5000 10800 103 75--125Magnesium, Total, ICP-MS 50 50 ug/L 6080 5000 11200 102 75--125Aluminum, Total, ICP-MS 2 10 ug/L 474 20 492 4xRule 75--125Potassium, Total, ICP-MS 100 500 ug/L 1630 5000 6640 100 75--125Calcium, Total, ICP-MS 50 50 ug/L 14100 5000 18800 94 75--125Vanadium, Total, ICP-MS 0.075 0.375 ug/L 1.55 20 20.3 94 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 0.77 20 19.5 94 75--125Iron, Total, ICP-MS 10 50 ug/L 646 5000 5580 99 75--125Manganese, Total, ICP-MS 0.1 0.5 ug/L 72.9 20 89.9 4xRule 75--125Cobalt, Total, ICP-MS 0.05 0.25 ug/L 0.278 20 18.1 89 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 1.35 20 20.7 97 75--125Copper, Total, ICP-MS 0.4 2 ug/L 2 20 21.3 97 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 11.7 20 31.4 98 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 0.903 20 19.8 94 75--125Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 18.7 94 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.9 99 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.069 20 19.2 96 75--125Tin, Total, ICP-MS 0.3 1.5 ug/L <MDL 20 16 80 75--125Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 17.6 88 75--125Barium, Total, ICP-MS 0.05 0.25 ug/L 8.01 20 28.1 100 75--125Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 17.6 88 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 0.39 20 18.2 89 75--125

WG118112

MB:WG118112-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDLMagnesium, Total, ICP-MS 50 50 ug/L <MDLCalcium, Total, ICP-MS 50 50 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLManganese, Total, ICP-MS 0.1 0.5 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL

of 23


Selenium, Total, ICP-MS 0.5 1 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLAntimony, Total, ICP-MS 0.3 1 ug/L <MDLBarium, Total, ICP-MS 0.05 0.25 ug/L <MDLThallium, Total, ICP-MS 0.04 0.2 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG118112-2 MB:WG118112-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.4 97 85--115Magnesium, Total, ICP-MS 50 50 ug/L <MDL 5000 4960 99 85--115Calcium, Total, ICP-MS 50 50 ug/L <MDL 5000 4970 99 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 20.6 103 85--115Manganese, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.1 101 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 19.9 100 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 20.2 101 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.7 98 85--115Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20 100 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.8 104 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 20.5 102 85--115Antimony, Total, ICP-MS 0.3 1 ug/L <MDL 20 21.2 106 85--115Barium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 20.1 100 85--115Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.6 98 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.5 103 85--115

LD:WG118112-3 L54375-2 Matrix: OTHR WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423258-400 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitMagnesium, Total, ICP-MS 50 50 ug/L 5270 5200 1 0--20Calcium, Total, ICP-MS 50 50 ug/L 43700 44400 2 0--20Manganese, Total, ICP-MS 0.1 0.5 ug/L 38 38.6 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 11.8 12 2 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 28.5 29.2 2 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 4.82 4.95 3 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.063 0.073 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.15 0.16 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 2.48 2.52 1 0--20

of 23


MS:WG118112-4 L54375-2 Matrix: OTHR WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423258-400 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitMagnesium, Total, ICP-MS 50 50 ug/L 5270 5000 9590 86 75--125Calcium, Total, ICP-MS 50 50 ug/L 43700 5000 47200 4xRule 75--125Manganese, Total, ICP-MS 0.1 0.5 ug/L 38 20 57.9 100 75--125Copper, Total, ICP-MS 0.4 2 ug/L 11.8 20 30.3 93 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 28.5 20 47.6 95 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 4.82 20 23.6 94 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.063 20 18.8 94 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.15 20 20 99 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 2.48 20 22.1 98 75--125

LD:WG118112-5 L54380-4 Matrix: EFFLUENT Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421186B Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 0.97 0.98 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 3.53 3.53 0 0--20Copper, Total, ICP-MS 0.4 2 ug/L 7.74 7.72 0 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 32.4 31.8 2 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.72 1.73 0 0--20Selenium, Total, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.072 0.077 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Antimony, Total, ICP-MS 0.3 1 ug/L 0.61 0.62 0--20Barium, Total, ICP-MS 0.05 0.25 ug/L 4.43 4.45 1 0--20Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 0.37 0.32 0--20

MS:WG118112-6 L54380-4 Matrix: EFFLUENT Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:421186B Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.2 96 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 0.97 20 21.3 102 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 3.53 20 23.4 99 75--125Copper, Total, ICP-MS 0.4 2 ug/L 7.74 20 27.2 97 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 32.4 20 49.9 88 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.72 20 21.8 100 75--125Selenium, Total, ICP-MS 0.5 1 ug/L <MDL 20 20.3 102 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.072 20 21 105 75--125

of 23


Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 20.4 102 75--125Antimony, Total, ICP-MS 0.3 1 ug/L 0.61 20 22.5 109 75--125Barium, Total, ICP-MS 0.05 0.25 ug/L 4.43 20 25.1 104 75--125Thallium, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19.5 97 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 0.37 20 20.7 102 75--125

LD:WG118112-7 L54454-2 Matrix: SEWER WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 5.19 5.28 2 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 11.5 11.2 3 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 33.8 34.4 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 70.2 72.1 3 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 148 151 2 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 2.02 2.04 1 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.496 0.485 2 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.378 0.378 0 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 12.8 12.6 1 0--20

MS:WG118112-8 L54454-2 Matrix: SEWER WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 5.19 20 25 99 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 11.5 20 31.1 98 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 33.8 20 54.8 105 75--125Copper, Total, ICP-MS 0.4 2 ug/L 70.2 20 90.4 101 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 148 20 171 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 2.02 20 22 100 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.496 20 15.6 75 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.378 20 20.6 101 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 12.8 20 33.3 102 75--125

WG119368

MB:WG119368-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDL

of 23


Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG119368-2 MB:WG119368-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 20.4 102 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 20.6 103 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21.9 109 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 21.7 109 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 21.8 109 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 22.8 114 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 21.5 107 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 22.5 113 85--115

LD:WG119368-3 L54488-2 Matrix: SEWER WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 3.53 3.75 6 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 6.96 7.31 5 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 24.6 25.1 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 60 60.8 1 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 119 119 0 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.89 1.9 0 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.298 0.342 14 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.299 0.289 3 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 10.3 10.3 0 0--20

MS:WG119368-4 L54488-2 Matrix: SEWER WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 3.53 20 23.8 102 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 6.96 20 26.3 97 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 24.6 20 45.8 106 75--125Copper, Total, ICP-MS 0.4 2 ug/L 60 20 80.5 103 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 119 20 139 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.89 20 22.4 103 75--125

of 23


Silver, Total, ICP-MS 0.04 0.2 ug/L 0.298 20 18.9 93 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.299 20 21.2 104 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 10.3 20 32.1 109 75--125

WG117646

MB:WG117646-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSodium, Dissolved, ICP-MS 100 100 ug/L <MDLMagnesium, Dissolved, ICP-MS 50 50 ug/L <MDLAluminum, Dissolved, ICP-MS 2 10 ug/L <MDLPotassium, Dissolved, ICP-MS 100 500 ug/L <MDLCalcium, Dissolved, ICP-MS 50 50 ug/L <MDLVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDLChromium, Dissolved, ICP-MS 0.2 1 ug/L <MDLIron, Dissolved, ICP-MS 10 50 ug/L <MDLManganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLNickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCopper, Dissolved, ICP-MS 0.4 2 ug/L <MDLZinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Dissolved, ICP-MS 0.5 1 ug/L <MDLSilver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLTin, Dissolved, ICP-MS 0.3 1.5 ug/L <MDLAntimony, Dissolved, ICP-MS 0.3 1 ug/L <MDLBarium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLThallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLLead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG117646-2 MB:WG117646-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 85--115Sodium, Dissolved, ICP-MS 100 100 ug/L <MDL 5000 4840 97 85--115Magnesium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 5300 106 85--115Aluminum, Dissolved, ICP-MS 2 10 ug/L <MDL 20 21.9 110 85--115Potassium, Dissolved, ICP-MS 100 500 ug/L <MDL 5000 5090 102 85--115

of 23


Calcium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 4660 93 85--115Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 19.4 97 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.7 98 85--115Iron, Dissolved, ICP-MS 10 50 ug/L <MDL 5000 4870 97 85--115Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.2 96 85--115Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.2 101 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.1 101 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 20.4 102 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 21 105 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 100 85--115Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 21.6 108 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 19.4 97 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.2 101 85--115Tin, Dissolved, ICP-MS 0.3 1.5 ug/L <MDL 20 19.9 99 85--115Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 19.9 99 85--115Barium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.4 97 85--115Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 19.3 96 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.4 102 85--115

LD:WG117646-3 L54076-2 Matrix: FRESH WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Sodium, Dissolved, ICP-MS 100 100 ug/L 5240 5200 1 0--20Magnesium, Dissolved, ICP-MS 50 50 ug/L 6330 6270 1 0--20Aluminum, Dissolved, ICP-MS 2 10 ug/L 27.8 28.2 1 0--20Potassium, Dissolved, ICP-MS 100 500 ug/L 1890 1890 0 0--20Calcium, Dissolved, ICP-MS 50 50 ug/L 13900 13900 0 0--20Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.643 0.643 0 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.28 0.28 0--20Iron, Dissolved, ICP-MS 10 50 ug/L 182 181 1 0--20Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 13.2 12.9 2 0--20Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L 0.079 0.079 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 0.848 0.859 1 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 1.1 1.1 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 4.08 4 2 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.722 0.714 1 0--20Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Tin, Dissolved, ICP-MS 0.3 1.5 ug/L <MDL <MDL 0--20

of 23


Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL <MDL 0--20Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 4.79 4.81 1 0--20Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20

MS:WG117646-4 L54076-2 Matrix: FRESH WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHSW-M Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.9 105 75--125Sodium, Dissolved, ICP-MS 100 100 ug/L 5240 5000 9970 95 75--125Magnesium, Dissolved, ICP-MS 50 50 ug/L 6330 5000 12000 113 75--125Aluminum, Dissolved, ICP-MS 2 10 ug/L 27.8 20 49.1 106 75--125Potassium, Dissolved, ICP-MS 100 500 ug/L 1890 5000 7050 103 75--125Calcium, Dissolved, ICP-MS 50 50 ug/L 13900 5000 18400 90 75--125Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.643 20 20.2 98 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.28 20 20.1 99 75--125Iron, Dissolved, ICP-MS 10 50 ug/L 182 5000 5110 99 75--125Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 13.2 20 32 94 75--125Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L 0.079 20 19.4 96 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 0.848 20 21 101 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 1.1 20 21.8 104 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 4.08 20 24.8 103 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.722 20 21.3 103 75--125Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 21.9 110 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 18.4 92 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.3 101 75--125Tin, Dissolved, ICP-MS 0.3 1.5 ug/L <MDL 20 20 100 75--125Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 20.4 102 75--125Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 4.79 20 24.7 100 75--125Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 19.3 97 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.6 103 75--125

WG118036

MB:WG118036-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSodium, Dissolved, ICP-MS 100 100 ug/L <MDLMagnesium, Dissolved, ICP-MS 50 50 ug/L <MDLPotassium, Dissolved, ICP-MS 100 500 ug/L <MDL

of 23


Calcium, Dissolved, ICP-MS 50 50 ug/L <MDLVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDLChromium, Dissolved, ICP-MS 0.2 1 ug/L <MDLIron, Dissolved, ICP-MS 10 50 ug/L <MDLManganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLNickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCopper, Dissolved, ICP-MS 0.4 2 ug/L <MDLZinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Dissolved, ICP-MS 0.5 1 ug/L <MDLSilver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLAntimony, Dissolved, ICP-MS 0.3 1 ug/L <MDLBarium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLThallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLLead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG118036-2 MB:WG118036-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.5 102 85--115Sodium, Dissolved, ICP-MS 100 100 ug/L <MDL 5000 4880 98 85--115Magnesium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 4780 96 85--115Potassium, Dissolved, ICP-MS 100 500 ug/L <MDL 5000 4880 98 85--115Calcium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 4740 95 85--115Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 19.5 98 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.6 98 85--115Iron, Dissolved, ICP-MS 10 50 ug/L <MDL 5000 4930 99 85--115Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.8 99 85--115Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20 100 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 100 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 20.6 103 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 20.9 105 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.8 99 85--115Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 21.6 108 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 21.3 107 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.9 105 85--115Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 20 100 85--115

of 23


Barium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.8 99 85--115Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.2 101 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.7 103 85--115

LD:WG118036-3 L54345-1 Matrix: GRND WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Sodium, Dissolved, ICP-MS 100 100 ug/L 5590 5620 1 0--20Magnesium, Dissolved, ICP-MS 50 50 ug/L 6910 7020 2 0--20Potassium, Dissolved, ICP-MS 100 500 ug/L 993 1000 1 0--20Calcium, Dissolved, ICP-MS 50 50 ug/L 12100 12000 0 0--20Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL <MDL 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL <MDL 0--20Iron, Dissolved, ICP-MS 10 50 ug/L 4250 4280 1 0--20Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 194 195 0 0--20Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 0.15 0.11 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL <MDL 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL <MDL 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.555 0.554 0 0--20Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL <MDL 0--20Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 6.98 7 0 0--20Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20

MS:WG118036-4 L54345-1 Matrix: GRND WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 75--125Sodium, Dissolved, ICP-MS 100 100 ug/L 5590 5000 11000 109 75--125Magnesium, Dissolved, ICP-MS 50 50 ug/L 6910 5000 12100 104 75--125Potassium, Dissolved, ICP-MS 100 500 ug/L 993 5000 6200 104 75--125Calcium, Dissolved, ICP-MS 50 50 ug/L 12100 5000 17000 98 75--125Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 20.4 102 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 20.5 103 75--125Iron, Dissolved, ICP-MS 10 50 ug/L 4250 5000 9440 104 75--125Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 194 20 214 4xRule 75--125

of 23


Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.1 96 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 0.15 20 20.6 102 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 21.3 106 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 21.1 106 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.555 20 21 102 75--125Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 21.6 108 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 21.4 107 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 21.3 106 75--125Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 20.4 102 75--125Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 6.98 20 27.1 101 75--125Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.5 102 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.8 104 75--125

WG118171

MB:WG118171-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSodium, Dissolved, ICP-MS 100 100 ug/L <MDLMagnesium, Dissolved, ICP-MS 50 50 ug/L <MDLPotassium, Dissolved, ICP-MS 100 500 ug/L <MDLCalcium, Dissolved, ICP-MS 50 50 ug/L <MDLVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDLChromium, Dissolved, ICP-MS 0.2 1 ug/L <MDLIron, Dissolved, ICP-MS 10 50 ug/L <MDLManganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLNickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCopper, Dissolved, ICP-MS 0.4 2 ug/L <MDLZinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSelenium, Dissolved, ICP-MS 0.5 1 ug/L <MDLSilver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLAntimony, Dissolved, ICP-MS 0.3 1 ug/L <MDLBarium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLThallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLLead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL

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SB:WG118171-2 MB:WG118171-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.1 96 85--115Sodium, Dissolved, ICP-MS 100 100 ug/L <MDL 5000 4730 95 85--115Magnesium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 4790 96 85--115Potassium, Dissolved, ICP-MS 100 500 ug/L <MDL 5000 5050 101 85--115Calcium, Dissolved, ICP-MS 50 50 ug/L <MDL 5000 4830 97 85--115Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 20.1 100 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 20.2 101 85--115Iron, Dissolved, ICP-MS 10 50 ug/L <MDL 5000 5220 104 85--115Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.6 103 85--115Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.6 103 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.3 102 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 20.1 100 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 20.1 101 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 99 85--115Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 20.2 101 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 21.3 106 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.9 99 85--115Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 19.8 99 85--115Barium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.6 98 85--115Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.6 103 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.7 103 85--115

LD:WG118171-3 L54391-7 Matrix: GRND WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Sodium, Dissolved, ICP-MS 100 100 ug/L 8190 8020 2 0--20Magnesium, Dissolved, ICP-MS 50 50 ug/L 9350 9150 2 0--20Potassium, Dissolved, ICP-MS 100 500 ug/L 1550 1530 1 0--20Calcium, Dissolved, ICP-MS 50 50 ug/L 14400 14000 3 0--20Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.13 0.13 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL <MDL 0--20Iron, Dissolved, ICP-MS 10 50 ug/L 778 765 2 0--20Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 262 259 1 0--20Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL <MDL 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 2.62 2.52 4 0--20

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Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.31 1.33 2 0--20Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL <MDL 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL <MDL 0--20Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 6.18 6.23 1 0--20Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL <MDL 0--20

MS:WG118171-4 L54391-7 Matrix: GRND WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:421422-CHGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitBeryllium, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 18.9 94 75--125Sodium, Dissolved, ICP-MS 100 100 ug/L 8190 5000 12700 90 75--125Magnesium, Dissolved, ICP-MS 50 50 ug/L 9350 5000 13900 92 75--125Potassium, Dissolved, ICP-MS 100 500 ug/L 1550 5000 6400 97 75--125Calcium, Dissolved, ICP-MS 50 50 ug/L 14400 5000 19300 99 75--125Vanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.13 20 19.8 98 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.7 99 75--125Iron, Dissolved, ICP-MS 10 50 ug/L 778 5000 5950 103 75--125Manganese, Dissolved, ICP-MS 0.1 0.5 ug/L 262 20 283 4xRule 75--125Cobalt, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.4 102 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.3 102 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 19.9 100 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 2.62 20 22.8 101 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.31 20 21.4 100 75--125Selenium, Dissolved, ICP-MS 0.5 1 ug/L <MDL 20 20.3 101 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.7 103 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.7 99 75--125Antimony, Dissolved, ICP-MS 0.3 1 ug/L <MDL 20 20 100 75--125Barium, Dissolved, ICP-MS 0.05 0.25 ug/L 6.18 20 25.9 99 75--125Thallium, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.4 102 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.5 102 75--125

WG119371

MB:WG119371-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDLChromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL

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Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCopper, Dissolved, ICP-MS 0.4 2 ug/L <MDLZinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSilver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLLead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG119371-2 MB:WG119371-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 19.4 97 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.6 98 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.9 104 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 20.7 104 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 20.1 101 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.8 99 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 21.5 108 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.1 100 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21.5 107 85--115

LD:WG119371-3 L54531-1 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.72 1.74 1 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.94 0.92 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 4.71 4.6 2 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 12.7 12.4 3 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 40.7 41 1 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.2 1.23 2 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.784 0.795 1 0--20

MS:WG119371-4 L54531-1 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.72 20 20.2 93 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.94 20 18.9 90 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 4.71 20 25 101 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 12.7 20 32.1 97 75--125

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Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 40.7 20 60.3 98 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.2 20 23.6 112 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 19.3 96 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.9 100 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.784 20 21.4 103 75--125

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Workgroup: WG117498 (pahll#003 pahphth-sim-lvi) Run ID: R200673

MB:WG117498-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.0025 0.00504 ug/L 0.0044 B2-Methylnaphthalene 0.001 0.00202 ug/L 0.00229 BDimethyl Phthalate 0.001 0.00202 ug/L 0.0013 BAcenaphthylene 0.001 0.00202 ug/L <MDLAcenaphthene 0.001 0.00202 ug/L <MDLDiethyl Phthalate 0.001 0.00504 ug/L 0.00975 BFluorene 0.001 0.00202 ug/L <MDLPhenanthrene 0.001 0.00202 ug/L 0.00243 BAnthracene 0.001 0.00202 ug/L <MDLDi-N-Butyl Phthalate 0.001 0.0252 ug/L 0.0429 BFluoranthene 0.001 0.00202 ug/L <MDLPyrene 0.001 0.00202 ug/L <MDLBenzyl Butyl Phthalate 0.001 0.00202 ug/L 0.0116 BBenzo(a)anthracene 0.001 0.00202 ug/L <MDLChrysene 0.001 0.00202 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.001 0.00202 ug/L 0.0861 BDi-N-Octyl Phthalate 0.001 0.00202 ug/L 0.0011 BBenzo(b,j,k)fluoranthene 0.001 0.00202 ug/L <MDLBenzo(a)pyrene 0.001 0.00202 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.001 0.00202 ug/L <MDLDibenzo(a,h)anthracene 0.001 0.00202 ug/L <MDLBenzo(g,h,i)perylene 0.001 0.00202 ug/L <MDL

SBD:WG117498-3 SB:WG117498-2 MB:WG117498-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.0025 0.00504 ug/L 0.0044 0.101 0.0865 81 40--160 0.101 0.0904 85 4 0--402-Methylnaphthalene 0.001 0.00202 ug/L 0.00229 0.101 0.0848 82 40--160 0.101 0.0863 83 2 0--40Dimethyl Phthalate 0.001 0.00202 ug/L 0.0013 0.101 0.111 109 40--160 0.101 0.114 112 3 0--40Acenaphthylene 0.001 0.00202 ug/L <MDL 0.101 0.0928 92 40--160 0.101 0.101 100 8 0--40Acenaphthene 0.001 0.00202 ug/L <MDL 0.101 0.0871 86 40--160 0.101 0.0911 90 5 0--40Diethyl Phthalate 0.001 0.00504 ug/L 0.00975 0.101 0.118 108 40--160 0.101 0.12 110 2 0--40Fluorene 0.001 0.00202 ug/L <MDL 0.101 0.0939 93 40--160 0.101 0.0985 98 5 0--40Phenanthrene 0.001 0.00202 ug/L 0.00243 0.101 0.0894 86 40--160 0.101 0.0931 90 4 0--40Anthracene 0.001 0.00202 ug/L <MDL 0.101 0.0719 71 40--160 0.101 0.0838 83 15 0--40

LIMSView QC Report for Brandon CSO Dry Weather Baseflow Samples - Data Validation for Organics - REVISED

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Di-N-Butyl Phthalate 0.001 0.0252 ug/L 0.0429 0.101 0.169 125 40--160 0.101 0.16 116 5 0--40Fluoranthene 0.001 0.00202 ug/L <MDL 0.101 0.104 103 40--160 0.101 0.109 108 4 0--40Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.102 102 40--160 0.101 0.106 105 3 0--40Benzyl Butyl Phthalate 0.001 0.00202 ug/L 0.0116 0.101 0.154 141 40--160 0.101 0.154 141 0 0--40Benzo(a)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.106 105 40--160 0.101 0.113 112 7 0--40Chrysene 0.001 0.00202 ug/L <MDL 0.101 0.103 102 40--160 0.101 0.106 106 4 0--40Bis(2-Ethylhexyl)Phthalate 0.001 0.00202 ug/L 0.0861 0.101 0.197 110 40--160 0.101 0.284 197 * 36 0--40Di-N-Octyl Phthalate 0.001 0.00202 ug/L 0.0011 0.101 0.155 153 40--160 0.101 0.159 157 2 0--40Benzo(b,j,k)fluoranthene 0.001 0.00202 ug/L <MDL 0.202 0.218 108 40--160 0.202 0.23 114 5 0--40Benzo(a)pyrene 0.001 0.00202 ug/L <MDL 0.101 0.0761 76 40--160 0.101 0.0904 90 17 0--40Indeno(1,2,3-Cd)Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.102 101 40--160 0.101 0.113 112 10 0--40Dibenzo(a,h)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.103 103 40--160 0.101 0.115 115 11 0--40Benzo(g,h,i)perylene 0.001 0.00202 ug/L <MDL 0.101 0.1 99 40--160 0.101 0.109 109 9 0--40

LD:WG117498-4 L54154-3 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitNaphthalene 0.047 0.0943 ug/L 0.124 0.122 1 0--402-Methylnaphthalene 0.019 0.0377 ug/L <MDL <MDL 0--40Dimethyl Phthalate 0.019 0.0377 ug/L <MDL <MDL 0--40Acenaphthylene 0.019 0.0377 ug/L <MDL <MDL 0--40Acenaphthene 0.019 0.0377 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.019 0.0943 ug/L 1.85 1.7 8 0--40Fluorene 0.019 0.0377 ug/L 0.031 0.031 0--40Phenanthrene 0.019 0.0377 ug/L 0.113 0.104 9 0--40Anthracene 0.019 0.0377 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.019 0.472 ug/L 0.563 0.547 3 0--40Fluoranthene 0.019 0.0377 ug/L 0.0952 0.0879 8 0--40Pyrene 0.019 0.0377 ug/L 0.0555 0.0547 1 0--40Benzyl Butyl Phthalate 0.12 0.236 ug/L 43 43.7 2 0--40Benzo(a)anthracene 0.019 0.0377 ug/L <MDL <MDL 0--40Chrysene 0.019 0.0377 ug/L <MDL <MDL 0--40Bis(2-Ethylhexyl)Phthalate 0.019 0.0377 ug/L 8.39 8.48 1 0--40Di-N-Octyl Phthalate 0.019 0.0377 ug/L 1.2 1.26 5 0--40Benzo(b,j,k)fluoranthene 0.019 0.0377 ug/L 0.0834 0.0984 17 0--40Benzo(a)pyrene 0.019 0.0377 ug/L 0.0522 0.0506 3 0--40Indeno(1,2,3-Cd)Pyrene 0.019 0.0377 ug/L 0.023 0.027 0--40Dibenzo(a,h)anthracene 0.019 0.0377 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.019 0.0377 ug/L 0.035 0.027 0--40

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Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54126-1 62 0 *L54126-3 78 32 *L54154-2 52 0 *L54154-3 76 0 *WG117498-1 100 124WG117498-2 91 113WG117498-3 93 114WG117498-4 79 22 *

Workgroup: WG117625 (pahll#003) Run ID: R200678

MB:WG117625-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.0025 0.00504 ug/L 0.0027 B2-Methylnaphthalene 0.001 0.00202 ug/L 0.0015 BDimethyl Phthalate 0.001 0.00202 ug/L 0.0013 BAcenaphthylene 0.001 0.00202 ug/L <MDLAcenaphthene 0.001 0.00202 ug/L <MDLDiethyl Phthalate 0.001 0.00504 ug/L 0.00855 BFluorene 0.001 0.00202 ug/L <MDLPhenanthrene 0.001 0.00202 ug/L 0.00214 BAnthracene 0.001 0.00202 ug/L <MDLDi-N-Butyl Phthalate 0.001 0.0252 ug/L 0.0256 BFluoranthene 0.001 0.00202 ug/L <MDLPyrene 0.001 0.00202 ug/L <MDLBenzyl Butyl Phthalate 0.001 0.00202 ug/L 0.00826 BBenzo(a)anthracene 0.001 0.00202 ug/L <MDLChrysene 0.001 0.00202 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.001 0.00202 ug/L 0.0413 BDi-N-Octyl Phthalate 0.001 0.00202 ug/L <MDLBenzo(b,j,k)fluoranthene 0.001 0.00202 ug/L <MDLBenzo(a)pyrene 0.001 0.00202 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.001 0.00202 ug/L <MDLDibenzo(a,h)anthracene 0.001 0.00202 ug/L <MDLBenzo(g,h,i)perylene 0.001 0.00202 ug/L <MDL

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SB:WG117625-2 MB:WG117625-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitNaphthalene 0.0025 0.00504 ug/L 0.0027 0.101 0.083 80 40--1602-Methylnaphthalene 0.001 0.00202 ug/L 0.0015 0.101 0.0723 70 40--160Dimethyl Phthalate 0.001 0.00202 ug/L 0.0013 0.101 0.104 102 40--160Acenaphthylene 0.001 0.00202 ug/L <MDL 0.101 0.097 96 40--160Acenaphthene 0.001 0.00202 ug/L <MDL 0.101 0.0814 81 40--160Diethyl Phthalate 0.001 0.00504 ug/L 0.00855 0.101 0.115 106 40--160Fluorene 0.001 0.00202 ug/L <MDL 0.101 0.0907 90 40--160Phenanthrene 0.001 0.00202 ug/L 0.00214 0.101 0.0866 84 40--160Anthracene 0.001 0.00202 ug/L <MDL 0.101 0.0822 82 40--160Di-N-Butyl Phthalate 0.001 0.0252 ug/L 0.0256 0.101 0.151 125 40--160Fluoranthene 0.001 0.00202 ug/L <MDL 0.101 0.0994 99 40--160Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.0943 94 40--160Benzyl Butyl Phthalate 0.001 0.00202 ug/L 0.00826 0.101 0.143 134 40--160Benzo(a)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.103 102 40--160Chrysene 0.001 0.00202 ug/L <MDL 0.101 0.0981 97 40--160Bis(2-Ethylhexyl)Phthalate 0.001 0.00202 ug/L 0.0413 0.101 0.167 125 40--160Di-N-Octyl Phthalate 0.001 0.00202 ug/L <MDL 0.101 0.141 140 40--160Benzo(b,j,k)fluoranthene 0.001 0.00202 ug/L <MDL 0.202 0.213 105 40--160Benzo(a)pyrene 0.001 0.00202 ug/L <MDL 0.101 0.086 85 40--160Indeno(1,2,3-Cd)Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.0986 98 40--160Dibenzo(a,h)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.1 99 40--160Benzo(g,h,i)perylene 0.001 0.00202 ug/L <MDL 0.101 0.0982 97 40--160

SBD:WG117498-3 SB:WG117498-2 MB:WG117498-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.0025 0.00504 ug/L 0.0044 0.101 0.0865 81 40--160 0.101 0.0904 85 4 0--402-Methylnaphthalene 0.001 0.00202 ug/L 0.00229 0.101 0.0848 82 40--160 0.101 0.0863 83 2 0--40Dimethyl Phthalate 0.001 0.00202 ug/L 0.0013 0.101 0.111 109 40--160 0.101 0.114 112 3 0--40Acenaphthylene 0.001 0.00202 ug/L <MDL 0.101 0.0928 92 40--160 0.101 0.101 100 8 0--40Acenaphthene 0.001 0.00202 ug/L <MDL 0.101 0.0871 86 40--160 0.101 0.0911 90 5 0--40Diethyl Phthalate 0.001 0.00504 ug/L 0.00975 0.101 0.118 108 40--160 0.101 0.12 110 2 0--40Fluorene 0.001 0.00202 ug/L <MDL 0.101 0.0939 93 40--160 0.101 0.0985 98 5 0--40Phenanthrene 0.001 0.00202 ug/L 0.00243 0.101 0.0894 86 40--160 0.101 0.0931 90 4 0--40Anthracene 0.001 0.00202 ug/L <MDL 0.101 0.0719 71 40--160 0.101 0.0838 83 15 0--40Di-N-Butyl Phthalate 0.001 0.0252 ug/L 0.0429 0.101 0.169 125 40--160 0.101 0.16 116 5 0--40

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Fluoranthene 0.001 0.00202 ug/L <MDL 0.101 0.104 103 40--160 0.101 0.109 108 4 0--40Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.102 102 40--160 0.101 0.106 105 3 0--40Benzyl Butyl Phthalate 0.001 0.00202 ug/L 0.0116 0.101 0.154 141 40--160 0.101 0.154 141 0 0--40Benzo(a)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.106 105 40--160 0.101 0.113 112 7 0--40Chrysene 0.001 0.00202 ug/L <MDL 0.101 0.103 102 40--160 0.101 0.106 106 4 0--40Bis(2-Ethylhexyl)Phthalate 0.001 0.00202 ug/L 0.0861 0.101 0.197 110 40--160 0.101 0.284 197 * 36 0--40Di-N-Octyl Phthalate 0.001 0.00202 ug/L 0.0011 0.101 0.155 153 40--160 0.101 0.159 157 2 0--40Benzo(b,j,k)fluoranthene 0.001 0.00202 ug/L <MDL 0.202 0.218 108 40--160 0.202 0.23 114 5 0--40Benzo(a)pyrene 0.001 0.00202 ug/L <MDL 0.101 0.0761 76 40--160 0.101 0.0904 90 17 0--40Indeno(1,2,3-Cd)Pyrene 0.001 0.00202 ug/L <MDL 0.101 0.102 101 40--160 0.101 0.113 112 10 0--40Dibenzo(a,h)anthracene 0.001 0.00202 ug/L <MDL 0.101 0.103 103 40--160 0.101 0.115 115 11 0--40Benzo(g,h,i)perylene 0.001 0.00202 ug/L <MDL 0.101 0.1 99 40--160 0.101 0.109 109 9 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54174-2 80 64WG117625-1 84 109WG117625-2 87 110


MB:WG117764-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.005 0.0101 ug/L <MDL2-Methylnaphthalene 0.002 0.00403 ug/L <MDLDimethyl Phthalate 0.002 0.00403 ug/L 0.0025 BAcenaphthylene 0.002 0.00403 ug/L <MDLAcenaphthene 0.002 0.00403 ug/L <MDLDiethyl Phthalate 0.002 0.0101 ug/L 0.0166 BFluorene 0.002 0.00403 ug/L <MDLPhenanthrene 0.002 0.00403 ug/L 0.0032 BAnthracene 0.002 0.00403 ug/L <MDLDi-N-Butyl Phthalate 0.002 0.0504 ug/L 0.0621 BFluoranthene 0.002 0.00403 ug/L <MDLPyrene 0.002 0.00403 ug/L <MDLBenzyl Butyl Phthalate 0.002 0.00403 ug/L 0.0207 BBenzo(a)anthracene 0.002 0.00403 ug/L <MDL

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Chrysene 0.002 0.00403 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.002 0.00403 ug/L 0.195 BDi-N-Octyl Phthalate 0.002 0.00403 ug/L <MDLBenzo(b,j,k)fluoranthene 0.002 0.00403 ug/L <MDLBenzo(a)pyrene 0.002 0.00403 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.002 0.00403 ug/L <MDLDibenzo(a,h)anthracene 0.002 0.00403 ug/L <MDLBenzo(g,h,i)perylene 0.002 0.00403 ug/L <MDL

SBD:WG117764-3 SB:WG117764-2 MB:WG117764-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.005 0.0101 ug/L <MDL 0.202 0.166 82 40--160 0.202 0.157 78 5 0--402-Methylnaphthalene 0.002 0.00403 ug/L <MDL 0.202 0.138 68 40--160 0.202 0.132 65 5 0--40Dimethyl Phthalate 0.002 0.00403 ug/L 0.0025 0.202 0.202 99 40--160 0.202 0.2 98 1 0--40Acenaphthylene 0.002 0.00403 ug/L <MDL 0.202 0.19 94 40--160 0.202 0.183 91 4 0--40Acenaphthene 0.002 0.00403 ug/L <MDL 0.202 0.16 79 40--160 0.202 0.152 76 5 0--40Diethyl Phthalate 0.002 0.0101 ug/L 0.0166 0.202 0.219 100 40--160 0.202 0.215 98 2 0--40Fluorene 0.002 0.00403 ug/L <MDL 0.202 0.173 86 40--160 0.202 0.166 82 4 0--40Phenanthrene 0.002 0.00403 ug/L 0.0032 0.202 0.168 82 40--160 0.202 0.161 78 4 0--40Anthracene 0.002 0.00403 ug/L <MDL 0.202 0.157 78 40--160 0.202 0.157 78 0 0--40Di-N-Butyl Phthalate 0.002 0.0504 ug/L 0.0621 0.202 0.309 122 40--160 0.202 0.311 123 1 0--40Fluoranthene 0.002 0.00403 ug/L <MDL 0.202 0.194 96 40--160 0.202 0.19 94 2 0--40Pyrene 0.002 0.00403 ug/L <MDL 0.202 0.192 95 40--160 0.202 0.186 92 3 0--40Benzyl Butyl Phthalate 0.002 0.00403 ug/L 0.0207 0.202 0.287 132 40--160 0.202 0.279 128 3 0--40Benzo(a)anthracene 0.002 0.00403 ug/L <MDL 0.202 0.206 102 40--160 0.202 0.203 101 1 0--40Chrysene 0.002 0.00403 ug/L <MDL 0.202 0.198 98 40--160 0.202 0.194 96 2 0--40Bis(2-Ethylhexyl)Phthalate 0.002 0.00403 ug/L 0.195 0.202 0.357 80 40--160 0.202 0.385 94 7 0--40Di-N-Octyl Phthalate 0.002 0.00403 ug/L <MDL 0.202 0.284 141 40--160 0.202 0.277 137 2 0--40Benzo(b,j,k)fluoranthene 0.002 0.00403 ug/L <MDL 0.403 0.425 105 40--160 0.403 0.422 105 1 0--40Benzo(a)pyrene 0.002 0.00403 ug/L <MDL 0.202 0.168 83 40--160 0.202 0.173 86 3 0--40Indeno(1,2,3-Cd)Pyrene 0.002 0.00403 ug/L <MDL 0.202 0.196 97 40--160 0.202 0.193 96 2 0--40Dibenzo(a,h)anthracene 0.002 0.00403 ug/L <MDL 0.202 0.198 98 40--160 0.202 0.196 97 1 0--40Benzo(g,h,i)perylene 0.002 0.00403 ug/L <MDL 0.202 0.167 83 40--160 0.202 0.164 81 2 0--40

LD:WG117764-4 L54307-1 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.04 0.08 ug/L <MDL <MDL 0--40

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Dimethyl Phthalate 0.04 0.08 ug/L 0.519 0.565 9 0--40Acenaphthylene 0.04 0.08 ug/L <MDL <MDL 0--40Acenaphthene 0.04 0.08 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.04 0.2 ug/L 5.28 5.89 11 0--40Fluorene 0.04 0.08 ug/L <MDL <MDL 0--40Phenanthrene 0.04 0.08 ug/L <MDL 0.041 0--40Anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 0.35 0.31 0--40Fluoranthene 0.04 0.08 ug/L <MDL <MDL 0--40Pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 0.231 0.273 16 0--40Benzo(a)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Chrysene 0.04 0.08 ug/L <MDL <MDL 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 1.96 2.07 5 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 0.077 0.0857 11 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(a)pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L <MDL <MDL 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54307-1 77 31 *L54307-2 88 52L54307-3 92 38 *WG117764-1 86 113WG117764-2 93 113WG117764-3 85 110WG117764-4 78 32 *

Workgroup: WG118172 (pahll#005 pah) Run ID: R200694

MB:WG118172-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.008 0.016 ug/L 0.01 B2-Methylnaphthalene 0.0032 0.0064 ug/L 0.0041 B

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Dimethyl Phthalate 0.0032 0.0064 ug/L <MDLAcenaphthylene 0.0032 0.0064 ug/L <MDLAcenaphthene 0.0032 0.0064 ug/L <MDLDiethyl Phthalate 0.0032 0.016 ug/L 0.0184 BFluorene 0.0032 0.0064 ug/L <MDLPhenanthrene 0.0032 0.0064 ug/L 0.0046 BAnthracene 0.0032 0.0064 ug/L <MDLDi-N-Butyl Phthalate 0.0032 0.08 ug/L 0.079 BFluoranthene 0.0032 0.0064 ug/L <MDLPyrene 0.0032 0.0064 ug/L <MDLBenzyl Butyl Phthalate 0.0032 0.0064 ug/L 0.0167 BBenzo(a)anthracene 0.0032 0.0064 ug/L <MDLChrysene 0.0032 0.0064 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.0032 0.0064 ug/L 0.278 BDi-N-Octyl Phthalate 0.0032 0.0064 ug/L <MDLBenzo(b,j,k)fluoranthene 0.0032 0.0064 ug/L <MDLBenzo(a)pyrene 0.0032 0.0064 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.0032 0.0064 ug/L <MDLDibenzo(a,h)anthracene 0.0032 0.0064 ug/L <MDLBenzo(g,h,i)perylene 0.0032 0.0064 ug/L <MDL

SBD:WG118172-3 SB:WG118172-2 MB:WG118172-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.008 0.016 ug/L 0.01 0.2 0.155 73 40--160 0.2 0.145 67 7 0--402-Methylnaphthalene 0.0032 0.0064 ug/L 0.0041 0.2 0.148 72 40--160 0.2 0.135 65 9 0--40Dimethyl Phthalate 0.0032 0.0064 ug/L <MDL 0.2 0.192 96 40--160 0.2 0.18 90 7 0--40Acenaphthylene 0.0032 0.0064 ug/L <MDL 0.2 0.176 88 40--160 0.2 0.161 81 9 0--40Acenaphthene 0.0032 0.0064 ug/L <MDL 0.2 0.159 79 40--160 0.2 0.147 73 8 0--40Diethyl Phthalate 0.0032 0.016 ug/L 0.0184 0.2 0.21 96 40--160 0.2 0.201 91 5 0--40Fluorene 0.0032 0.0064 ug/L <MDL 0.2 0.174 87 40--160 0.2 0.162 81 7 0--40Phenanthrene 0.0032 0.0064 ug/L 0.0046 0.2 0.165 80 40--160 0.2 0.153 74 8 0--40Anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.153 76 40--160 0.2 0.144 72 6 0--40Di-N-Butyl Phthalate 0.0032 0.08 ug/L 0.079 0.2 0.289 105 40--160 0.2 0.273 97 6 0--40Fluoranthene 0.0032 0.0064 ug/L <MDL 0.2 0.179 90 40--160 0.2 0.169 85 6 0--40Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.175 87 40--160 0.2 0.161 81 8 0--40Benzyl Butyl Phthalate 0.0032 0.0064 ug/L 0.0167 0.2 0.229 106 40--160 0.2 0.215 99 6 0--40Benzo(a)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.168 84 40--160 0.2 0.159 80 5 0--40Chrysene 0.0032 0.0064 ug/L <MDL 0.2 0.178 89 40--160 0.2 0.168 84 6 0--40Bis(2-Ethylhexyl)Phthalate 0.0032 0.0064 ug/L 0.278 0.2 0.296 9 * 40--160 0.2 0.334 28 * 12 0--40

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Di-N-Octyl Phthalate 0.0032 0.0064 ug/L <MDL 0.2 0.216 108 40--160 0.2 0.213 107 2 0--40Benzo(b,j,k)fluoranthene 0.0032 0.0064 ug/L <MDL 0.4 0.375 94 40--160 0.4 0.352 88 6 0--40Benzo(a)pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.152 76 40--160 0.2 0.143 71 6 0--40Indeno(1,2,3-Cd)Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.165 82 40--160 0.2 0.158 79 4 0--40Dibenzo(a,h)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.167 83 40--160 0.2 0.163 82 2 0--40Benzo(g,h,i)perylene 0.0032 0.0064 ug/L <MDL 0.2 0.158 79 40--160 0.2 0.149 75 6 0--40

LD:WG118172-4 L54454-1 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitNaphthalene 0.08 0.16 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.032 0.064 ug/L <MDL <MDL 0--40Dimethyl Phthalate 0.032 0.064 ug/L 0.125 0.115 9 0--40Acenaphthylene 0.032 0.064 ug/L <MDL <MDL 0--40Acenaphthene 0.032 0.064 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.032 0.16 ug/L 2.68 2.63 2 0--40Fluorene 0.032 0.064 ug/L <MDL <MDL 0--40Phenanthrene 0.032 0.064 ug/L 0.13 0.077 51 * 0--40Anthracene 0.032 0.064 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.032 0.8 ug/L 0.45 0.38 0--40Fluoranthene 0.032 0.064 ug/L 0.0948 0.0914 4 0--40Pyrene 0.032 0.064 ug/L 0.053 0.041 0--40Benzyl Butyl Phthalate 0.032 0.064 ug/L 0.499 0.657 27 0--40Benzo(a)anthracene 0.032 0.064 ug/L <MDL <MDL 0--40Chrysene 0.032 0.064 ug/L 0.037 <MDL 0--40Bis(2-Ethylhexyl)Phthalate 0.032 0.064 ug/L 4.1 3.77 8 0--40Di-N-Octyl Phthalate 0.032 0.064 ug/L 0.188 0.157 18 0--40Benzo(b,j,k)fluoranthene 0.032 0.064 ug/L 0.042 0.034 0--40Benzo(a)pyrene 0.032 0.064 ug/L <MDL <MDL 0--40Indeno(1,2,3-Cd)Pyrene 0.032 0.064 ug/L <MDL <MDL 0--40Dibenzo(a,h)anthracene 0.032 0.064 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.032 0.064 ug/L <MDL <MDL 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54454-1 65 24 *L54454-2 69 31 *L54454-3 86 28 *

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L54455-2 93 35 *L54455-3 69 26 *L54488-2 81 58L54488-3 76 34 *WG118172-1 88 101WG118172-2 83 103WG118172-3 77 98WG118172-4 58 23 *

Workgroup: WG118307 (pahll#005 pah) Run ID: R200695

MB:WG118307-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.008 0.016 ug/L <MDL2-Methylnaphthalene 0.0032 0.0064 ug/L 0.0033 BDimethyl Phthalate 0.0032 0.0064 ug/L 0.00656 BAcenaphthylene 0.0032 0.0064 ug/L <MDLAcenaphthene 0.0032 0.0064 ug/L <MDLDiethyl Phthalate 0.0032 0.016 ug/L 0.0348 BFluorene 0.0032 0.0064 ug/L <MDLPhenanthrene 0.0032 0.0064 ug/L 0.0047 BAnthracene 0.0032 0.0064 ug/L <MDLDi-N-Butyl Phthalate 0.0032 0.08 ug/L 0.1 BFluoranthene 0.0032 0.0064 ug/L <MDLPyrene 0.0032 0.0064 ug/L <MDLBenzyl Butyl Phthalate 0.0032 0.0064 ug/L 0.0346 BBenzo(a)anthracene 0.0032 0.0064 ug/L <MDLChrysene 0.0032 0.0064 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.0032 0.0064 ug/L 0.202 BDi-N-Octyl Phthalate 0.0032 0.0064 ug/L <MDLBenzo(b,j,k)fluoranthene 0.0032 0.0064 ug/L <MDLBenzo(a)pyrene 0.0032 0.0064 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.0032 0.0064 ug/L <MDLDibenzo(a,h)anthracene 0.0032 0.0064 ug/L <MDLBenzo(g,h,i)perylene 0.0032 0.0064 ug/L <MDL

SB:WG118307-2 MB:WG118307-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit

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Naphthalene 0.008 0.016 ug/L <MDL 0.2 0.157 79 40--1602-Methylnaphthalene 0.0032 0.0064 ug/L 0.0033 0.2 0.156 77 40--160Dimethyl Phthalate 0.0032 0.0064 ug/L 0.00656 0.2 0.195 94 40--160Acenaphthylene 0.0032 0.0064 ug/L <MDL 0.2 0.173 86 40--160Acenaphthene 0.0032 0.0064 ug/L <MDL 0.2 0.157 78 40--160Diethyl Phthalate 0.0032 0.016 ug/L 0.0348 0.2 0.31 137 40--160Fluorene 0.0032 0.0064 ug/L <MDL 0.2 0.177 88 40--160Phenanthrene 0.0032 0.0064 ug/L 0.0047 0.2 0.166 80 40--160Anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.145 73 40--160Di-N-Butyl Phthalate 0.0032 0.08 ug/L 0.1 0.2 0.869 384 * 40--160Fluoranthene 0.0032 0.0064 ug/L <MDL 0.2 0.184 92 40--160Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.173 87 40--160Benzyl Butyl Phthalate 0.0032 0.0064 ug/L 0.0346 0.2 0.386 176 * 40--160Benzo(a)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.168 84 40--160Chrysene 0.0032 0.0064 ug/L <MDL 0.2 0.18 90 40--160Bis(2-Ethylhexyl)Phthalate 0.0032 0.0064 ug/L 0.202 0.2 0.729 264 * 40--160Di-N-Octyl Phthalate 0.0032 0.0064 ug/L <MDL 0.2 0.237 118 40--160Benzo(b,j,k)fluoranthene 0.0032 0.0064 ug/L <MDL 0.4 0.373 93 40--160Benzo(a)pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.142 71 40--160Indeno(1,2,3-Cd)Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.17 85 40--160Dibenzo(a,h)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.171 85 40--160Benzo(g,h,i)perylene 0.0032 0.0064 ug/L <MDL 0.2 0.167 83 40--160

SBD:WG118172-3 SB:WG118172-2 MB:WG118172-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.008 0.016 ug/L 0.01 0.2 0.155 73 40--160 0.2 0.145 67 7 0--402-Methylnaphthalene 0.0032 0.0064 ug/L 0.0041 0.2 0.148 72 40--160 0.2 0.135 65 9 0--40Dimethyl Phthalate 0.0032 0.0064 ug/L <MDL 0.2 0.192 96 40--160 0.2 0.18 90 7 0--40Acenaphthylene 0.0032 0.0064 ug/L <MDL 0.2 0.176 88 40--160 0.2 0.161 81 9 0--40Acenaphthene 0.0032 0.0064 ug/L <MDL 0.2 0.159 79 40--160 0.2 0.147 73 8 0--40Diethyl Phthalate 0.0032 0.016 ug/L 0.0184 0.2 0.21 96 40--160 0.2 0.201 91 5 0--40Fluorene 0.0032 0.0064 ug/L <MDL 0.2 0.174 87 40--160 0.2 0.162 81 7 0--40Phenanthrene 0.0032 0.0064 ug/L 0.0046 0.2 0.165 80 40--160 0.2 0.153 74 8 0--40Anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.153 76 40--160 0.2 0.144 72 6 0--40Di-N-Butyl Phthalate 0.0032 0.08 ug/L 0.079 0.2 0.289 105 40--160 0.2 0.273 97 6 0--40Fluoranthene 0.0032 0.0064 ug/L <MDL 0.2 0.179 90 40--160 0.2 0.169 85 6 0--40Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.175 87 40--160 0.2 0.161 81 8 0--40Benzyl Butyl Phthalate 0.0032 0.0064 ug/L 0.0167 0.2 0.229 106 40--160 0.2 0.215 99 6 0--40Benzo(a)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.168 84 40--160 0.2 0.159 80 5 0--40

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Chrysene 0.0032 0.0064 ug/L <MDL 0.2 0.178 89 40--160 0.2 0.168 84 6 0--40Bis(2-Ethylhexyl)Phthalate 0.0032 0.0064 ug/L 0.278 0.2 0.296 9 * 40--160 0.2 0.334 28 * 12 0--40Di-N-Octyl Phthalate 0.0032 0.0064 ug/L <MDL 0.2 0.216 108 40--160 0.2 0.213 107 2 0--40Benzo(b,j,k)fluoranthene 0.0032 0.0064 ug/L <MDL 0.4 0.375 94 40--160 0.4 0.352 88 6 0--40Benzo(a)pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.152 76 40--160 0.2 0.143 71 6 0--40Indeno(1,2,3-Cd)Pyrene 0.0032 0.0064 ug/L <MDL 0.2 0.165 82 40--160 0.2 0.158 79 4 0--40Dibenzo(a,h)anthracene 0.0032 0.0064 ug/L <MDL 0.2 0.167 83 40--160 0.2 0.163 82 2 0--40Benzo(g,h,i)perylene 0.0032 0.0064 ug/L <MDL 0.2 0.158 79 40--160 0.2 0.149 75 6 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54531-1 90 29 *L54532-1 79 23 *WG118307-1 81 98WG118307-2 80 105

Workgroup: WG118436 (pahll#006 pah-lvi) Run ID: R200698

MB:WG118436-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L 0.022 B2-Methylnaphthalene 0.008 0.016 ug/L 0.01 BDimethyl Phthalate 0.008 0.016 ug/L 0.0086 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.108 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.012 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.243 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0455 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 1.72 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDL

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Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG118436-3 SB:WG118436-2 MB:WG118436-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L 0.022 0.5 0.343 64 40--160 0.5 0.393 74 14 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.01 0.5 0.358 70 40--160 0.5 0.409 80 13 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.0086 0.5 0.506 99 40--160 0.5 0.486 96 4 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.421 84 40--160 0.5 0.422 84 0 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.374 75 40--160 0.5 0.393 79 5 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.108 0.5 0.587 96 40--160 0.5 0.574 93 2 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.453 91 40--160 0.5 0.463 93 2 0--40Phenanthrene 0.008 0.016 ug/L 0.012 0.5 0.414 80 40--160 0.5 0.41 80 1 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.375 75 40--160 0.5 0.359 72 4 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.243 0.5 0.733 98 40--160 0.5 0.749 101 2 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.486 97 40--160 0.5 0.465 93 5 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.387 77 40--160 0.5 0.382 76 1 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0455 0.5 0.551 101 40--160 0.5 0.554 102 0 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.444 89 40--160 0.5 0.433 87 2 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.467 93 40--160 0.5 0.46 92 2 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 1.72 0.5 0.866 -171 * 40--160 0.5 1.02 -140 * 16 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.492 98 40--160 0.5 0.495 99 1 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.958 96 40--160 1 0.932 93 3 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.387 77 40--160 0.5 0.351 70 10 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.512 102 40--160 0.5 0.483 97 6 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.531 106 40--160 0.5 0.495 99 7 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.49 98 40--160 0.5 0.461 92 6 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54591-1 85 37 *WG118436-1 70 102WG118436-2 76 105WG118436-3 85 103

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Technical Memorandum Date: August 21, 2013; Revised – February 11, 2015 To: Richard Jack, King County Toxicology and Contaminant Assessment Group Debra Williston, King County Toxicology and Contaminant Assessment Group From: Scott Mickelson, King County Marine and Sediment Assessment Group Carly Greyell, King County Toxicology and Contaminant Assessment Group Subject: Data Validation Report

Brandon CSO Study Wet-Weather Baseflow and Storm Samples, Winter/Spring 2012 This technical memorandum summarizes the data validation review performed on 60 wet-weather and storm samples collected from within the Brandon combined sewer overflow (CSO) basin between January 25 and June 21, 2012. The sampling and analysis of these samples are specific in the project sampling and analysis plan (SAP) Lower Duwamish Waterway Source Control, Brandon Combined Sewer Basin Study, Sampling and Analysis Plan (King County 2011). The 20 wet-weather baseflow and 40 storm samples were submitted for analysis of polycyclic aromatic hydrocarbons (PAHs), phthalates, total and dissolved organic carbon (TOC and DOC), total suspended solids (TSS), and total and dissolved metals. All 60 samples were analyzed for TSS, TOC, DOC, and total metals. Due to insufficient sample volume, only 59 of the 60 samples were analyzed for PAHs and phthalates and 56 were analyzed for dissolved metals. The data validation for PAHs and phthalates was revised based on re-analysis of detection limits for these compounds by the King County Environmental Laboratory. The specifics of the re-analysis are described in laboratory data anomaly forms (DAFs).

1.0 INTRODUCTION

This data validation review has been based, in part, on guidance found in USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review (EPA 2014) and USEPA Contract Laboratory Program National Functional Guidelines for Inorganic Superfund Data Review (EPA 2010), as well as the project SAP (King County 2011). Materials reviewed included Batch Reports and Analytical Quality Control (QC) Reports downloaded from the King County Laboratory Information Management System (LIMS) database, which are attached to this memorandum. Also reviewed were DAFs, which are available upon request. The QC parameters reviewed during this data validation include holding time, method blanks, spike blanks, spike blank duplicates, matrix spikes, matrix spike duplicates, laboratory control samples, laboratory duplicates, and surrogates, which are described below.

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1.1 Holding Time The analytical holding time is a method-specific timeframe, during which sample preparation and analysis should occur to provide valid data. All samples should be analyzed within this prescribed holding time. 1.2 Method Blank A method blank is an aliquot of clean reference matrix that is generally processed through the entire analytical procedure. Analysis of the method blank is used to evaluate the levels of contamination that might be associated with the processing and analysis of samples. Method blanks were used during all analyses. All method blank results should be less than the method detection limit (MDL). 1.3 Spike Blanks and Spike Blank Duplicates A spike blank is an aliquot of the clean reference matrix used for the method blank, to which a known concentration of target analyte(s) has been added. The spiked aliquot is processed through the entire analytical procedure. Analysis of the spike blank is used as an indicator of method accuracy. Spike blanks were used during organics, metals, and TOC/DOC analyses. Spike blanks are not addressed in the National Functional Guidelines, however, King County has empirically-derived control limits for spike blank analytes, which are shown on the attached QC reports. Spike blank results should be within these control limits. Spike blanks were run in duplicate for most organic analyses, due to a lack of other QC samples that could assess method precision. The RPD between spike blank duplicate results for organic analyses should be less than the 40% QC limit. 1.4 Matrix Spike A matrix spike is a sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Analysis of the matrix spike is used as an indicator of sample matrix effect on the recovery of target analyte(s). Matrix spikes were used during organics, metals, and TOC/DOC analyses. Control limits for individual organic analytes and organic carbon are not addressed in the National Functional Guidelines, however, King County has empirically-derived control limits for percent recoveries of these matrix spike analytes, which are shown on the attached QC reports. Matrix spike recoveries should be within these control limits. Control limits for arsenic matrix spike recoveries are addressed in the National Functional Guidelines. All trace metal matrix spike recoveries should be within the 75 to 125% control limits for all analytes (EPA 2010). 1.5 Matrix Spike Duplicate A matrix spike duplicate is a second sample aliquot fortified with a known concentration of a target analyte(s). The spiked sample is processed through the entire analytical procedure. Analysis of the matrix spike duplicate is used as an additional indicator of sample matrix effect on the recovery of target analyte(s) as well as an indicator of method precision. A matrix spike duplicate was used routinely during mercury analysis and on two QC batches during organic analysis. The relative percent difference (RPD) between matrix spike and matrix spike duplicate results for organic analytes are not addressed in the National Functional Guidelines, however,

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King County used an empirically-derived control limit of 40% for this project. The RPD control limit between mercury matrix spike duplicate results is 20% (EPA 2010). 1.6 Laboratory Control Sample A laboratory control sample is a sample of known analyte concentration(s) that is prepared in the lab from a separate source of analyte(s) relative to the calibration standards. Since the laboratory control sample analysis should follow the entire analytical process, it should be stored and prepared following the same procedures as a field sample. Analysis of a laboratory control sample is used as an indicator of method accuracy and long-term analytical precision. Laboratory control samples were used during TOC/DOC and TSS analyses. King County used percent recovery control limits of 85 to 115% for TOC/DOC analysis and 80 to 120% for TSS analysis on this project. Percent recoveries for laboratory control sample results should be within these control limits. 1.7 Laboratory Duplicate A laboratory duplicate is a second aliquot of a sample, processed concurrently and in an identical manner with the original sample. Analysis of the laboratory duplicate is used as an indicator of method precision and laboratory subsampling procedures. The laboratory duplicate can also be used to provide information regarding the homogeneity of the sample matrix. Laboratory duplicates were used during TOC/DOC, TSS, ICPMS metals, and organic analyses. QC results are reported as an RPD between the sample and laboratory duplicate results. Control limits for conventional analyses are also not addressed under the National Functional Guidelines. King County used RPD control limits of 20% for TOC/DOC analysis and 25% for TSS analysis. The RPD for laboratory duplicate results should be below these control limits. Control limits for ICPMS laboratory duplicates are addressed in the National Function Guidelines. The RPD between all trace metal laboratory duplicate results should be below 20% (EPA 2004). King County used an RPD of 40% for this project as the RPD QC limit between laboratory duplicate results during organic analyses. Laboratory duplicate RPD results for samples in which the concentration is less than the reporting detection limit (RDL) will not be qualified based solely on whether the RPD is greater than the QC limit. This is based on the inherent analytical variability between the MDL and RDL, which is the limit of practical quantitation. 1.8 Surrogates A surrogate is a known concentration of non-target analyte which is added to each sample (both analytical and QC samples) prior to extraction and analysis for all trace organic analyses. Surrogate recovery is used as a sample-specific indication of method or matrix bias for target analytes. The surrogate is selected to behave in a similar manner to the target analytes.

The King County Environmental Laboratory used two surrogate compounds during analysis of trace organic compounds, 2-fluorobiphenyl and d14-terphenyl. King County has empirically-derived laboratory QC control limits for surrogate recoveries, which are 40 – 160%. Surrogate recoveries for all analytical and QC samples should be within these control limits. These two surrogate compounds are not addressed in National Functional Guidelines.

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2.0 CONVENTIONALS

Conventional analytes included total suspended solids and total and dissolved organic carbon. LIMS batch and analytical QC reports for conventional analyses are included as Attachment A. 2.1 Total Suspended Solids Sixty water samples were submitted for TSS analysis by gravimetric determination following Standard Method SM2540-D (APHA 1998). The samples were batched into the 15 workgroups shown in Table 2-1. Each workgroup included analysis of a minimum of three QC samples; method blanks (MB), laboratory control samples (LCS), and laboratory duplicates (LD).

Table 2-1 TSS Workgroups and QC Samples

Workgroup Samples MB LCS LD WG119517 L54687-1, L54687-2, L54687-3 WG119808 L55012-1, L55012-3

WG119972 L55011-1, L55011-2, L55011-3, L55186-1, L55186-2, L55186-3

WG120350 L55154-1, L55154-2, L55154-3

WG120479 L55185-1, L55185-2, L55185-3, L55285-2, L55285-3

WG120569 L55183-1, L55183-2, L55183-3 WG120580 L55184-1, L55184-2, L55184-3 WG120684 L55433-1, L55433-2, L55433-3 WG120818 L55511-1, L55511-2, L55511-3

WG120873 L55512-1, L55512-2, L55512-3, L55584-1, L55584-2, L55584-3

WG121035 L55572-1, L55572-3, L55686-1, L55686-2, L55686-3

WG121219 L55638-1, L55638-2, L55638-3, L55763-1, L55763-2, L55763-3

WG121455 L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3, L55876-1, L55876-2, L55876-3

WG121636 L55936-2 WG121711 L55698-1

2.1.1 Holding Time All 60 TSS samples were analyzed within the prescribed 7-day holding time. 2.1.2 Method Blank Results TSS results in the method blanks associated with all 15 workgroups were less than the MDL. 2.1.3 Laboratory Control Sample Results TSS recoveries in the laboratory control samples associated with all 15 workgroups were within the 80 to 120% QC limits.

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2.1.4 Laboratory Duplicate Results The RPDs between TSS laboratory duplicate results in all 15 workgroups were less than the 25% QC limit. 2.2 Total and Dissolved Organic Carbon Sixty water samples were submitted for TOC/DOC analysis by Standard Method SM5310-B (APHA 1998), which is a high-temperature combustion/infrared detection method. The samples were batched into the 13 workgroups shown in Table 2-2. Each workgroup included analysis of a minimum of five QC samples; method blanks, spike blanks (SB), laboratory control samples, matrix spikes (MS), and laboratory duplicates.

Table 2-2 TOC/DOC Workgroups and QC Samples

Workgroup Samples MB SB LCS MS LD WG119562 L54687-1, L54687-2, L54687-3 WG119910 L55012-1, L55012-3 WG119964 L55011-1, L55011-2, L55011-3 WG120092 L55186-1, L55186-2, L55186-3 WG120382 L55154-1, L55154-2, L55154-3

WG120560 L55185-1, L55185-2, L55185-3, L55285-2, L55285-3

WG120836

L55183-1, L55183-2, L55183-3, L55184-1, L55184-2, L55184-3, L55433-1, L55433-2, L55433-3, L55511-1, L55511-2, L55511-3, L55512-1, L55512-2, L55512-3, L55584-1, L55584-2, L55584-3

WG121155 L55572-1, L55572-3, L55686-1, L55686-2, L55686-3

WG121213 L55638-1, L55638-2, L55638-3, L55763-1, L55763-2, L55763-3

WG121474 L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3

WG121560 L55876-1, L55876-2, L55876-3 WG121701 L55936-2 WG121752 L55698-1

2.2.1 Holding Time All 60 TOC/DOC samples were analyzed within the prescribed 28-day holding time. 2.2.2 Method Blank Results TOC and DOC results in the method blanks associated with all 13 workgroups were less than the MDL. 2.2.3 Spike Blank Results The spike blank recoveries for TOC and DOC in each of the 14 workgroups were all within the laboratory QC limits of 80 to 120%.

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2.2.4 Laboratory Control Sample Results TOC and DOC recoveries in the laboratory control samples associated with each of the 13 workgroups were all within the 85 to 115% QC limits. 2.2.5 Matrix Spike Results TOC and DOC matrix spike recoveries in each of the 13 workgroups were all within the 75 to 125% QC limits. 2.2.6 Laboratory Duplicate Results The RPD between TOC and DOC laboratory duplicate results in each of the 13 workgroups were all less than the 20% QC limit.

3.0 TRACE METALS

Sixty water samples were submitted for analysis of total metals and 56 samples were submitted for analysis of dissolved metals, both of which included mercury and other trace metals. LIMS batch and analytical QC reports for metals analyses are included as Attachment A. 3.1 Total and Dissolved Mercury Total and dissolved mercury analysis was performed using cold vapor atomic absorption spectroscopy (CVAA) according to EPA Method 245.1 (EPA1994). The 60 samples for total mercury and 56 samples for dissolved mercury were batched into the 10 workgroups shown in Table 3-1. Each workgroup included analysis of a minimum of five QC samples; method blanks (for both total and dissolved mercury), spike blanks, matrix spikes, and matrix spike duplicates.

Table 3-1 Total and Dissolved Mercury Workgroups and QC Samples

Workgroup Samples MB SB MS MSD WG119801 L54687-1, L54687-2, L54687-3

WG120040 L55011-2 (D), L55011-3, L55012-3, L55186-2, L55186-3

WG120057 L55011-1, L55011-2 (T), L55012-1, L55186-1

WG120641 L55154-1, L55154-2, L55154-3, L55185-2, L55185-2, L55185-3, L55285-2, L55285-3

WG120674 L55183-1, L55183-2, L55183-3, L55184-1, L55184-2, L55184-3, L55433-1, L55433-2, L55433-3

WG120894 L55511-1, L55511-2, L55511-3, L55512-1, L55512-2, L55512-3, L55584-1, L55584-2, L55584-3

WG121053 L55572-1, L55572-3, L55586-1, L55586-2, L55586-3

WG121351 L55638-1, L55638-2, L55638-3, L55763-1, L55763-2, L55763-3

WG121500 L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3, L55876-1, L55876-2, L55876-3

WG121764 L55698-1, L55936-2

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3.1.1 Holding Time All 60 total and 56 dissolved mercury samples were analyzed within the prescribed 28-day holding time. 3.1.2 Method Blank Results Both total and dissolved mercury results in the method blanks associated with each of the 10 works group were all less than the MDL. 3.1.3 Spike Blank Results Mercury spike blank recoveries in each of the 10 workgroups were all within the laboratory QC limits of 85 to 115%. 3.1.4 Matrix Spike and Matrix Spike Duplicate Results The total mercury recoveries in the matrix spike (204%) and matrix spike duplicate (189%) associated with workgroup WG120674 exceeded the upper QC limit of 125%. The total mercury result for sample L55433-2 should be qualified with a “J” flag and considered estimated with a high bias. The mercury matrix spike and matrix spike duplicate recoveries in the other nine workgroups were all within the 75 to 125% QC limits and the RPDs between matrix spike duplicate results were all less than the 20% QC limit. 3.1.5 Sample Handling Issue All dissolved mercury samples were filtered outside of the method-specified 15-minute holding time. As a result, all dissolved mercury results should be qualified with a “J” flag and considered estimated with an unknown bias. 3.2 Total ICP-MS Metals Total metals, including arsenic, cadmium, chromium, copper, lead, nickel, silver, vanadium, and zinc, were analyzed by inductively coupled plasma mass spectroscopy (ICP-MS) following EPA Methods 200.8/6020A SW846 (EPA 1995). The samples were batched into the four workgroups shown in Table 3-2. Each workgroup included a minimum of four QC samples; method blanks, spike blanks, matrix spikes, and laboratory duplicates.

Table 3-2 Total ICP-MS Metals Workgroups and QC Samples

Workgroup Samples MB SB MS LD

WG120032 L54687-1, L54687-2, L54687-3, L55011-1, L55011-2, L55011-3, L55012-1, L55012-3, L55186-1, L55186-2, L55186-3

WG120860

L55154-1, L55154-2, L55154-3, L55183-1, L55183-2, L55183-3, L55184-1, L55184-2, L55184-3, L55185-1, L55185-2, L55185-3, L55285-2, L55285-3, L55433-1, L55433-2, L55433-3, L55584-1, L55584-2, L55584-3

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WG121194

L55511-1, L55511-2, L55511-3, L55512-1, L55512-2, L55512-3, L55572-1, L55572-3, L55638-1, L55638-2, L55638-3, L55686-1, L55686-2, L55686-3, L55763-1, L55763-2, L55763-3

WG121947 L55698-1, L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3, L55876-1, L55876-2, L55876-3, L55936-2

3.2.1 Holding Time All 60 total metal samples were analyzed within the prescribed 6-month holding time. 3.2.2 Method Blank Results Results for each total metal in the method blank associated with of the four workgroups were all less than the MDL. 3.2.3 Spike Blank Results All total metal spike blank recoveries in each of the four workgroups were within the 85 to 115% QC limits. 3.2.4 Matrix Spike Results All total metal matrix spike recoveries in each of the four workgroups were within the 75 to 125% QC limits. 3.2.5 Laboratory Duplicate Results RPDs between total metal laboratory duplicate results in each of the four workgroups were all below the 20% QC limit. 3.3 Dissolved ICP-MS Metals Dissolved metals, including arsenic, cadmium, chromium, copper, lead, nickel, silver, vanadium, and zinc, were analyzed by inductively coupled plasma mass spectroscopy (ICP-MS) following EPA Methods 200.8/6020A SW846 (EPA 1995). The samples were batched into the four workgroups shown in Table 3-3. Each workgroup included a minimum of four QC samples; method blanks, spike blanks, matrix spikes, and laboratory duplicates.

Table 3-3 Dissolved ICP-MS Metals Workgroups and QC Samples


WG120037 L54687-1, L54687-2, L54687-3, L55011-1, L55011-2, L55011-3, L55012-1, L55012-3, L55186-1, L55186-2, L55186-3

WG120847

L55154-1, L55154-2, L55183-1, L55183-2, L55183-3, L55184-2, L55184-3, L55185-1, L55185-2, L55185-3, L55285-2, L55285-3, L55433-1, L55433-2, L55433-3, L55511-1, L55511-2, L55511-3, L55512-1, L55512-3,

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WG121302

L55512-2, L55572-1, L55572-3, L55584-1, L55584-2, L55584-3, L55638-1, L55638-2, L55638-3, L55686-1, L55686-2, L55686-3, L55763-1, L55763-2, L55763-3

WG121990 L55698-1, L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3, L55876-3, L55936-2

3.3.1 Holding Time All 56 dissolved metal samples were analyzed within the prescribed 6-month holding time. 3.3.2 Method Blank Results Results for each dissolved metal in the method blank associated with each of the four workgroups were all less than the MDL. 3.3.3 Spike Blank Results All dissolved metal spike blank recoveries in each of the four workgroups were within the 85 to 115% QC limits. 3.3.4 Matrix Spike Results All dissolved metal matrix spike recoveries in each of the four workgroups were within the 75 to 125% QC limits. 3.3.5 Laboratory Duplicate Results RPDs between dissolved metals laboratory duplicate results in each of the eight four groups were all below the 20% QC limit. 3.3.6 Sampling Handling Issue All dissolved ICP-MS metals samples were filtered outside of the method-specified 15-minute holding time. As a result, all detected dissolved ICP-MS metals results should be qualified with a “J” flag and considered estimated with an unknown bias.

4. 0 TRACE ORGANICS

Fifty-nine water samples were submitted for analysis of PAHs and phthalates by gas chromatography mass spectroscopy (GC-MS) following EPA Methods 3520C/8270D – SW846 (EPA 1995). The instrument method was modified by the use of a large volume injector (LVI) and analysis using selected ion monitoring (SIM). The samples were batched into the 12 workgroups shown in Table 4-1. With the exception of workgroup WG120555, each workgroup included a minimum of five QC samples; method blanks, spike blanks, spike blank duplicates (SBD), laboratory duplicates and surrogates. Only two workgroups had sufficient sample volume to include analysis of a matrix spike and matrix spike duplicate (MSD), as specified in the SAP. LIMS batch and analytical QC reports for PAH/phthalate analysis are included as Attachment A.

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Table 4-1 PAH/Phthalate Workgroups and QC Samples

Workgroup Samples MB SB SBD LD SUR WG119537 L54687-1, L54687-2, L54687-3

WG119973 L55011-1, L55011-2, L55011-3, L55186-1, L55186-2, L55186-3

WG119848 L55012-1, L55012-3

WG120438 L55154-1, L55154-2, L55154-3, L55185-1, L55185-2, L55185-3, L55285-2, L55285-3

WG120555 L55183-1, L55183-2, L55183-3

WG120654 L55184-2, L55184-3, L54333-1, L54333-2, L54333-3

WG120867 L55511-1, L55511-2, L55511-3, L55512-1, L55512-2, L55512-3, L55584-1, L55584-2, L55584-3

WG121052 L55572-1, L55572-3, L55686-1, L55686-2, L55686-3

WG121217 L55638-1, L55638-2, L55638-3, L55763-1, L55763-2, L55763-3

WG121458 L55764-1, L55764-2, L55764-3, L55859-2, L55859-3, L55875-2, L55875-3, L55876-1, L55876-2, L55876-3

WG121670 L55936-2 MS MSD WG121757 L55698-1 MS MSD

4.1 Holding Time All 59 samples were extracted within the 7-day holding time and analyzed within the subsequent 40-day holding time. 4.2 Method Blank Results Diethyl phthalate, di-n-butyl phthalate, benzyl butyl phthalate and bis(2-ethylhexyl) phthalate were detected in all 12 method blanks associated with this data set. Dimethyl phthalate and phenanthrene were detected in nine and eight method blanks, respectively. An additional six PAH compounds were detected in at least one method blank. More than half the positive PAH and phthalate method blank results were detected at concentrations greater than the reporting detection limit (RDL), which is the limit of practical quantitation. Based on the recommendations in National Function Guidelines (EPA 2014), the following data qualification regime should be employed as a result of method blank contamination:

• When the method blank concentration is greater than the MDL and the sample concentration is less than the RDL, the sample value should be reported as the numeric RDL value and the result should be qualified with a “U” flag and considered undetected.

• When the method blank concentration is less than the RDL and the sample concentration is greater than the RDL but less than five times the method blank concentration, the numeric sample value should be used as reported but the result should be qualified with a “U” flag and considered undetected.

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• When the method blank concentration is less than the RDL and the sample concentration is greater than the RDL and greater than five times the method blank concentration, the sample result may be used as reported, without qualification.

• When the method blank concentration is greater than the RDL and the sample concentration is less than five times the method blank concentration, the sample result may be used as reported but the result should be qualified with a “U” flag. The data validator may choose to reject the data in this case.

• When the method blank concentration is greater than the RDL and the sample concentration is greater than five times the method blank concentration, the sample result may be used as reported without qualification.

Overall, 63 PAH/phthalate results (four PAHs and three phthalates) were qualified as nondetects based on method blank results. Table 1 at the end of this memo presents the validated data with the final qualifiers after the consideration of all QC sample results. 4.3 Spike Blank and Spike Blank Duplicate Results Bis(2-ethylhexyl) phthalate recoveries in the spike blanks and spike blank duplicates associated with 11 of 12 workgroups were outside of the 40 to 160% QC limits. In four workgroups spike blank recoveries were greatly impacted by laboratory contamination issues for this compound, with method blank concentrations exceeding the spike concentration by a factor of four or greater. Because of this, accuracy could not be successfully assessed with the spike blank and spike blank duplicates samples in these workgroups. All detected bis(2-ethylhexyl) phthalate sample data in workgroups WG120654, WG120867, WG121052 and WG121458 should be qualified with a “J” flag and considered estimated with unknown bias, and all nondetect bis(2-ethylhexyl) phthalate sample data in these workgroups should be qualified with a “UJ” flag and considered estimated nondetects with unknown bias.

The bis(2-ethylhexyl) phthalate recoveries of 257% and 191% in the spike blank and spike blank duplicate associated with workgroup WG119848 exceeded the 160% upper QC limit. The RPD of 22% between spike blank and spike blank duplicate results was below the 40% QC limit. Detected results for bis(2-ethylhexyl) phthalate in this workgroup will be qualified with a “J” flag and considered estimated with a high bias based on these spike blank results.

The bis(2-ethylhexyl) phthalate recovery was 126% in the spike blank and was 224% in the spike blank duplicate associated with workgroup WG119973; both the spike blank duplicate and the average recovery (175%) of the two spike blanks exceeded the 160% upper QC limit. The 32% RPD between spike blank and spike blank duplicate results was below the 40% QC limit. Detected results for bis(2-ethylhexyl) phthalate in this workgroup should be qualified with a “J” flag and considered estimated with a high bias based on these spike blank recovery results.

In workgroup WG120438, the bis(2-ethylhexyl) phthalate recovery of 214% in the spike blank exceeded the upper QC limit of 160%; the recovery of the spike blank duplicate was 87%. The RPD was 49% between spike blank and spike blank duplicate results, which exceeded the 40% QC limit. Because of the high RPD and the high recovery limit for the spike blank, detected

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results for bis(2-ethylhexyl) phthalate in this workgroup will be qualified with a “J” flag and considered estimated with a unknown bias, while nondetect results will be qualified with a “UJ” flag based on these spike blank results.

The bis(2-ethylhexyl) phthalate recovery of 335% in the spike blank associated with workgroup WG120555 exceeded the 160% upper QC limit. There was no spike blank duplicate associated with this workgroup. Detected results for bis(2-ethylhexyl) phthalate in this workgroup should be qualified with a “J” flag and considered estimated with a high bias based on the spike blank result; however, the lack of precision QC samples in this workgroup results in unknown bias overall.

The bis(2-ethylhexyl) phthalate recovery of 6,646% in the spike blank duplicate associated with workgroup WG121217 exceeded the 160% upper QC limit. The spike blank duplicate recovery of 148% was within the 40 to 160% QC limits; however, the RPD of 186% between spike blank and spike blank duplicate results grossly exceeded the 40% QC limit. Detected results for bis(2-ethylhexyl) phthalate in this workgroup will be qualified with a “J” flag and considered estimated with a unknown bias, while nondetect results will be qualified with a “UJ” flag based on these spike blank results.

The bis(2-ethylhexyl) phthalate recovery of 17% in the spike blank associated with workgroup WG121670 was below the 40% lower QC limit. There was no spike blank duplicate associated with this workgroup, but a matrix spike and matrix spike duplicate were analyzed (discussed in Section 4.5 below). Detected results for bis(2-ethylhexyl) phthalate in this workgroup should be qualified with a “J” flag and considered estimated with a low bias based on the spike blank result.

The bis(2-ethylhexyl) phthalate recovery of 260% in the spike blank associated with workgroup WG121757 exceeded the 160% upper QC limit. There was no spike blank duplicate associated with this workgroup, but a matrix spike and matrix spike duplicate were analyzed (discussed in Section 4.5 below). Detected results for bis(2-ethylhexyl) phthalate in this workgroup should be qualified with a “J” flag and considered estimated with a high bias based on the spike blank result, but the matrix spike and matrix spike RPD indicates unknown bias (See Section 4.5).

The di-N-octyl phthalate recovery was 181% in the spike blank and was 135% in the spike blank duplicate associated with workgroup WG120867; the spike blank recovery exceeded the 160% upper QC limit, but the average recovery (158%) of the two spike blanks did not. The 29% RPD between spike blank and spike blank duplicate results was below the 40% QC limit. As a result, associated sample data for di-N-butyl phthalate will not be qualified based on these spike blank results.

The benzyl butyl phthalate recoveries of 170 and 166% in the spike blank and spike blank duplicate associated with workgroup WG121217 both exceeded the 160% upper QC limit. Benzyl butyl phthalate results in all associated samples should all be qualified with a “J” flag and considered estimated with a high bias.

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The di-N-octyl phthalate recoveries of 171 and 172% in the spike blank and spike blank duplicates associated with workgroup WG121217 both exceeded the 160% upper QC limit. Di-N-butyl phthalate results in all associated samples should be qualified with a “J” flag and considered estimated with a high bias. The benzo(a)pyrene recovery of 33% in the spike blank associated with workgroup WG121217 was below the 40% lower QC limit. The spike blank duplicate recovery of 58%, however, was within the 40 to 160% QC limits. The RPD of 55% between spike blank and spike blank duplicate results exceeded the 40% QC limit. Benzo(a)pyrene results in samples L55638-1 and -2 and L55763-3 should be qualified with a “J” flag and considered estimated with an unknown bias. Benzo(a)pyrene results in samples L55638-3 and L55763-1 and -2 were less than the MDL and should be qualified with a “UJ” flag with unknown bias. All other spike blank and spike blank duplicate recoveries were within QC limits, as were the RPDs between spike blank and spike blank duplicate results. 4.4 Laboratory Duplicates The 43% RPD between bis(2-ethylhexyl) phthalate results in the laboratory duplicate associated with workgroup WG119537 exceeded the 40% QC limit. The bis(2-ethylhexyl) phthalate result in sample L54687-1 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The 43% RPD between benzyl butyl phthalate results in the laboratory duplicate associated with workgroup WG119848 exceeded the 40% QC limit. The benzyl butyl phthalate result in sample L55012-3 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The 65% RPD between fluoranthene results in the laboratory duplicate associated with workgroup WG119973 exceeded the 40% QC limit. The fluoranthene result in sample L55186-3 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The 200% RPD between acenaphthylene results in the laboratory duplicate associated with workgroup WG121052 exceeded the 40% QC limit. The acenaphthylene result in sample L55572-3 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The 68% RPD between bis(2-ethylhexyl) phthalate results in the laboratory duplicate associated with workgroup WG121217 exceeded the 40% QC limit. The bis(2-ethylhexyl) phthalate result in sample L55638-1 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The 49% RPD between dimethyl phthalate results in the laboratory duplicate associated with workgroup WG121458 exceeded the 40% QC limit. The dimethyl phthalate result in sample L55764-2 should be qualified with a “J” flag and considered an estimate with an unknown bias.

The RPDs between all other laboratory duplicate results were below the 40% QC limit.

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4.5 Matrix Spikes/Matrix Spike Duplicates Two workgroups, WG121670 and WG121757, had sufficient volume for matrix spikes and matrix spike duplicates instead of spike blank duplicates and laboratory duplicates. In workgroup WG121670, benzyl butyl phthalate recovery of 175% in the matrix spike duplicate exceeded the upper 160% QC limit. In workgroup WG121757, the bis(2-ethylhexyl) phthalate recoveries of 10,183% and 391% in the matrix spike and matrix spike duplicate both grossly exceeded the upper QC limit of 160%. For both workgroups, the sample concentrations for these compounds were over four times those of the spiked concentration, meaning the matrix spike and matrix spike duplicate were unable to successfully assess matrix effects on accuracy. The associated sample results (L55936-2 for benzyl butyl phthalate and L55698-1 for bis(2-ethylhexyl) phthalate) should be qualified with “J” flags and considered estimates with unknown bias. Additionally, the RPD between the matrix spike and matrix spike duplicate for bis(2-ethylhexyl) phthalate in workgroup WG121757 was 160%, exceeding the QC limit of 40%. This indicates precision was outside acceptable limits for this compound, further supporting the flagging regime described above.

All other matrix spike and matrix duplicate recoveries were within the 40 to 160% QC limits and all other RPDs between results were below the 40% QC limit. 4.6 Surrogates Recoveries of the surrogate d4-terphenyl in all analytical and QC samples in each of the 12 workgroups were within the 40 to 160% QC limits. Recoveries of the other surrogate compound, 2-fluorobiphenyl, were below the lower QC limit of 40% in two analytical samples and three QC samples. Sample data will not be qualified based on the surrogate recoveries in the three QC samples. The recoveries of 2-fluorobiphenyl in samples L55763-1 and L55763-2 were 34% and 36%, respectively. This surrogate is associated with the following target analytes; 2-methylnaphthalene, acenaphthene, acenaphthylene, fluorene, naphthalene, diethyl phthalate and dimethyl phthalate. Results for these seven compounds in samples L55763-1 and -2 should be qualified with the following flags: qualify detected sample results with a “J” flag and consider the results as estimated with a low bias; qualify undetected sample results with a “UJ” flag. 4.7 Lack of Precision Quality Control Information One workgroup, WG120555, included no precision QC samples. As a result, all associated PAH and phthalate sample results (L55183-1, L55183-2 and L55183-3) should be flagged as follows: all detected values should be qualified with a “J” flag and considered estimated with an unknown bias and all undetected results should be qualified with a “UJ” flag. These flags should be applied in addition to but not in lieu of other flags referenced in the previous sections.

5.0 DATA USABILITY

As a general data reporting format, conventional parameters, total and dissolved metals, and organics sample results that are reported as “<MDL” should be assigned a “U” flag in all cases and considered undetected; any results also flagged with a “J” should be assigned a “UJ” flag. Conventional, total and dissolved metals, and organics sample results that are reported as

15

“<RDL” should be assigned a “J” flag in all cases and considered estimated with an unknown bias. Table 1 at the end of this narrative provides any additional data qualifier flags, if required, for every sample/analyte in this data set. These flags are based on the data quality issues summarized in Sections 2.0, 3.0, and 4.0. LIMS Batch and QC reports and data anomaly forms are provided as Attachment A.

6.0 REFERENCES

APHA 1998. Standard Methods for the Examination of Water and Wastewater, 20th Edition. American Public Health Association. Washington, D.C.

EPA 1994. Determination of Mercury in Water by Cold Vapor Atomic Absorption Spectrometry. EPA Method 245.1, Revision 3.0. U.S. Environmental Protection Agency, Office of Research and Development. Cincinnati, Ohio.

EPA 1995. Determination of Trace Elements in Waters and Wastes by Inductively Coupled Plasma – Mass Spectrometry. Method 200.8, Revision 5.4. United States Environmental Protection Agency, Office of Research and Development. Cincinnati, Ohio.

EPA 2007. Test Methods for Evaluating Solid Waste. Laboratory Manual – Physical/Chemical Methods, SW-846, 3rd Edition, Update IVB. United State Environmental Protection Agency, Office of Solid Waste and Emergency Response. Washington, D.C.

EPA 2010. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Inorganic Data Review. OSWER 9240.1-51, USEPA-540-R-10-011. United States Environmental Protection Agency. Washington, D.C. January 2010.

EPA 2014. USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review. OSWER 9355.0-132, EPA-540-R-014-002. USEPA. Washington, D.C. August 2014.

King County 2011. Lower Duwamish Waterway Source Control, Brandon Combined Sewer Basin Study, Sampling and Analysis Plan. King County Department of Natural Resources and Parks. Seattle, Washington.


Table 1. Brandon CSO Wet Baseflow and Storm Event Samples - Data Validation Flags and Bias Notation

WORKNUM LOCATORSAMPLE

TYPECOLLECTDATE SAMPLE ID PARMNAME NUMVALUE UNITS Lab Qual

DV Value

DV Flag

Bias MDL RDL

WG120674 BRANDREG Storm 4/11/2012 L55433-2 Mercury, Total, CVAA 0.162 ug/L J 0.162 J high 0.05 0.15WG119801 A01007 Storm 1/25/2012 L54687-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG119801 BRANDREG Storm 1/25/2012 L54687-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG119801 BRANDUTAHStorm 1/25/2012 L54687-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120040 BRANDREG Storm 2/28/2012 L55011-2 Mercury, Dissolved, CVAA 0.0068 ug/L <RDL,H 0.0068 J unknown 0.005 0.015WG120040 BRANDUTAHStorm 2/28/2012 L55011-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120040 BRANDREG Storm 2/29/2012 L55186-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120040 BRANDUTAHStorm 2/29/2012 L55186-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120040 BRANDUTAHWet Base 2/15/2012 L55012-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120057 A01007 Storm 2/28/2012 L55011-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.01 UJ unknown 0.01 0.03WG120057 A01007 Storm 2/29/2012 L55186-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.01 UJ unknown 0.01 0.03WG120057 A01007 Wet Base 2/15/2012 L55012-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.01 UJ unknown 0.01 0.03WG120641 A01007 Storm 3/27/2012 L55185-1 Mercury, Dissolved, CVAA 0.0089 ug/L <RDL,H 0.0089 J unknown 0.005 0.015WG120641 BRANDREG Storm 3/27/2012 L55185-2 Mercury, Dissolved, CVAA 0.0211 ug/L H 0.0211 J unknown 0.005 0.015WG120641 BRANDUTAHStorm 3/27/2012 L55185-3 Mercury, Dissolved, CVAA 0.0055 ug/L <RDL,H 0.0055 J unknown 0.005 0.015WG120641 BRANDREG Storm 3/28/2012 L55285-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120641 BRANDUTAHStorm 3/28/2012 L55285-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120641 A01007 Wet Base 3/26/2012 L55154-1 Mercury, Dissolved, CVAA 0.0055 ug/L <RDL,H 0.0055 J unknown 0.005 0.015WG120641 BRANDREG Wet Base 3/26/2012 L55154-2 Mercury, Dissolved, CVAA 0.014 ug/L <RDL,H 0.014 J unknown 0.005 0.015WG120674 A01007 Storm 4/11/2012 L55433-1 Mercury, Dissolved, CVAA 0.026 ug/L H 0.026 J unknown 0.005 0.015WG120674 BRANDREG Storm 4/11/2012 L55433-2 Mercury, Dissolved, CVAA 0.013 ug/L <RDL,H 0.013 J unknown 0.005 0.015WG120674 BRANDUTAHStorm 4/11/2012 L55433-3 Mercury, Dissolved, CVAA 0.013 ug/L <RDL,H 0.013 J unknown 0.005 0.015WG120674 A01007 Wet Base 4/9/2012 L55183-1 Mercury, Dissolved, CVAA 0.011 ug/L <RDL,H 0.011 J unknown 0.005 0.015WG120674 BRANDREG Wet Base 4/9/2012 L55183-2 Mercury, Dissolved, CVAA 0.0065 ug/L <RDL,H 0.0065 J unknown 0.005 0.015WG120674 BRANDUTAHWet Base 4/9/2012 L55183-3 Mercury, Dissolved, CVAA 0.0066 ug/L <RDL,H 0.0066 J unknown 0.005 0.015WG120674 BRANDREG Wet Base 4/10/2012 L55184-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120674 BRANDUTAHWet Base 4/10/2012 L55184-3 Mercury, Dissolved, CVAA 0.0051 ug/L <RDL,H 0.0051 J unknown 0.005 0.015WG120894 A01007 Storm 4/24/2012 L55512-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120894 BRANDREG Storm 4/24/2012 L55512-2 Mercury, Dissolved, CVAA 0.0065 ug/L <RDL,H 0.0065 J unknown 0.005 0.015WG120894 BRANDUTAHStorm 4/24/2012 L55512-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120894 A01007 Storm 4/25/2012 L55584-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120894 BRANDREG Storm 4/25/2012 L55584-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120894 BRANDUTAHStorm 4/25/2012 L55584-3 Mercury, Dissolved, CVAA 0.0077 ug/L <RDL,H 0.0077 J unknown 0.005 0.015WG120894 A01007 Wet Base 4/23/2012 L55511-1 Mercury, Dissolved, CVAA 0.0098 ug/L <RDL,H 0.0098 J unknown 0.005 0.015WG120894 BRANDREG Wet Base 4/23/2012 L55511-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG120894 BRANDUTAHWet Base 4/23/2012 L55511-3 Mercury, Dissolved, CVAA 0.0078 ug/L <RDL,H 0.0078 J unknown 0.005 0.015WG121053 A01007 Wet Base 5/7/2012 L55572-1 Mercury, Dissolved, CVAA 0.0267 ug/L H 0.0267 J unknown 0.005 0.015WG121053 BRANDUTAHWet Base 5/7/2012 L55572-3 Mercury, Dissolved, CVAA 0.0074 ug/L <RDL,H 0.0074 J unknown 0.005 0.015





DV Value

DV Flag

Bias MDL RDL

WG121053 A01007 Wet Base 5/8/2012 L55686-1 Mercury, Dissolved, CVAA 0.02 ug/L H 0.02 J unknown 0.005 0.015WG121053 BRANDREG Wet Base 5/8/2012 L55686-2 Mercury, Dissolved, CVAA 0.0074 ug/L <RDL,H 0.0074 J unknown 0.005 0.015WG121053 BRANDUTAHWet Base 5/8/2012 L55686-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121351 A01007 Storm 5/21/2012 L55638-1 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121351 BRANDREG Storm 5/21/2012 L55638-2 Mercury, Dissolved, CVAA 0.0054 ug/L <RDL,H 0.0054 J unknown 0.005 0.015WG121351 BRANDUTAHStorm 5/21/2012 L55638-3 Mercury, Dissolved, CVAA 0.0054 ug/L <RDL,H 0.0054 J unknown 0.005 0.015WG121351 A01007 Storm 5/22/2012 L55763-1 Mercury, Dissolved, CVAA 0.0091 ug/L <RDL,H 0.0091 J unknown 0.005 0.015WG121351 BRANDREG Storm 5/22/2012 L55763-2 Mercury, Dissolved, CVAA 0.0076 ug/L <RDL,H 0.0076 J unknown 0.005 0.015WG121351 BRANDUTAHStorm 5/22/2012 L55763-3 Mercury, Dissolved, CVAA 0.0064 ug/L <RDL,H 0.0064 J unknown 0.005 0.015WG121500 A01007 Storm 6/4/2012 L55764-1 Mercury, Dissolved, CVAA 0.0068 ug/L <RDL,H 0.0068 J unknown 0.005 0.015WG121500 BRANDREG Storm 6/4/2012 L55764-2 Mercury, Dissolved, CVAA 0.0056 ug/L <RDL,H 0.0056 J unknown 0.005 0.015WG121500 BRANDUTAHStorm 6/4/2012 L55764-3 Mercury, Dissolved, CVAA 0.0086 ug/L <RDL,H 0.0086 J unknown 0.005 0.015WG121500 BRANDREG Storm 6/5/2012 L55859-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121500 BRANDUTAHStorm 6/5/2012 L55859-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121500 BRANDREG Storm 6/6/2012 L55875-2 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121500 BRANDUTAHStorm 6/6/2012 L55875-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121500 BRANDUTAHStorm 6/7/2012 L55876-3 Mercury, Dissolved, CVAA ug/L <MDL,H 0.005 UJ unknown 0.005 0.015WG121764 BRANDREG Storm 6/18/2012 L55936-2 Mercury, Dissolved, CVAA 0.0069 ug/L <RDL,H 0.0069 J unknown 0.005 0.015WG121764 BRANDREG Wet Base 6/20/2012 L55698-1 Mercury, Dissolved, CVAA 0.014 ug/L <RDL,H 0.014 J unknown 0.005 0.015WG120037 A01007 Storm 1/25/2012 L54687-1 Arsenic, Dissolved, ICP-MS 0.659 ug/L H 0.659 J unknown 0.1 0.5WG120037 BRANDREG Storm 1/25/2012 L54687-2 Arsenic, Dissolved, ICP-MS 1.05 ug/L H 1.05 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Arsenic, Dissolved, ICP-MS 0.766 ug/L H 0.766 J unknown 0.1 0.5WG120037 A01007 Storm 2/28/2012 L55011-1 Arsenic, Dissolved, ICP-MS 1.15 ug/L H 1.15 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/28/2012 L55011-2 Arsenic, Dissolved, ICP-MS 1.06 ug/L H 1.06 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Arsenic, Dissolved, ICP-MS 0.825 ug/L H 0.825 J unknown 0.1 0.5WG120037 A01007 Storm 2/29/2012 L55186-1 Arsenic, Dissolved, ICP-MS 0.951 ug/L H 0.951 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/29/2012 L55186-2 Arsenic, Dissolved, ICP-MS 0.995 ug/L H 0.995 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Arsenic, Dissolved, ICP-MS 0.59 ug/L H 0.59 J unknown 0.1 0.5WG120037 A01007 Wet Base 2/15/2012 L55012-1 Arsenic, Dissolved, ICP-MS 1.07 ug/L H 1.07 J unknown 0.1 0.5WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Arsenic, Dissolved, ICP-MS 0.754 ug/L H 0.754 J unknown 0.1 0.5WG120037 A01007 Storm 1/25/2012 L54687-1 Cadmium, Dissolved, ICP-MS 0.426 ug/L H 0.426 J unknown 0.05 0.25WG120037 BRANDREG Storm 1/25/2012 L54687-2 Cadmium, Dissolved, ICP-MS 0.12 ug/L <RDL,H 0.12 J unknown 0.05 0.25WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Cadmium, Dissolved, ICP-MS 0.057 ug/L <RDL,H 0.057 J unknown 0.05 0.25WG120037 A01007 Storm 2/28/2012 L55011-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG120037 BRANDREG Storm 2/28/2012 L55011-2 Cadmium, Dissolved, ICP-MS 0.067 ug/L <RDL,H 0.067 J unknown 0.05 0.25WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Cadmium, Dissolved, ICP-MS 0.06 ug/L <RDL,H 0.06 J unknown 0.05 0.25WG120037 A01007 Storm 2/29/2012 L55186-1 Cadmium, Dissolved, ICP-MS 0.055 ug/L <RDL,H 0.055 J unknown 0.05 0.25WG120037 BRANDREG Storm 2/29/2012 L55186-2 Cadmium, Dissolved, ICP-MS 0.066 ug/L <RDL,H 0.066 J unknown 0.05 0.25





DV Value

DV Flag

Bias MDL RDL

WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Cadmium, Dissolved, ICP-MS 0.064 ug/L <RDL,H 0.064 J unknown 0.05 0.25WG120037 A01007 Wet Base 2/15/2012 L55012-1 Cadmium, Dissolved, ICP-MS 0.061 ug/L <RDL,H 0.061 J unknown 0.05 0.25WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Cadmium, Dissolved, ICP-MS 0.12 ug/L <RDL,H 0.12 J unknown 0.05 0.25WG120037 A01007 Storm 1/25/2012 L54687-1 Chromium, Dissolved, ICP-MS 0.72 ug/L <RDL,H 0.72 J unknown 0.2 1WG120037 BRANDREG Storm 1/25/2012 L54687-2 Chromium, Dissolved, ICP-MS 1.07 ug/L H 1.07 J unknown 0.2 1WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Chromium, Dissolved, ICP-MS 1.25 ug/L H 1.25 J unknown 0.2 1WG120037 A01007 Storm 2/28/2012 L55011-1 Chromium, Dissolved, ICP-MS 1.22 ug/L H 1.22 J unknown 0.2 1WG120037 BRANDREG Storm 2/28/2012 L55011-2 Chromium, Dissolved, ICP-MS 1.95 ug/L H 1.95 J unknown 0.2 1WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Chromium, Dissolved, ICP-MS 0.55 ug/L <RDL,H 0.55 J unknown 0.2 1WG120037 A01007 Storm 2/29/2012 L55186-1 Chromium, Dissolved, ICP-MS 1.18 ug/L H 1.18 J unknown 0.2 1WG120037 BRANDREG Storm 2/29/2012 L55186-2 Chromium, Dissolved, ICP-MS 1.79 ug/L H 1.79 J unknown 0.2 1WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Chromium, Dissolved, ICP-MS 0.86 ug/L <RDL,H 0.86 J unknown 0.2 1WG120037 A01007 Wet Base 2/15/2012 L55012-1 Chromium, Dissolved, ICP-MS 0.88 ug/L <RDL,H 0.88 J unknown 0.2 1WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Chromium, Dissolved, ICP-MS 0.58 ug/L <RDL,H 0.58 J unknown 0.2 1WG120037 A01007 Storm 1/25/2012 L54687-1 Copper, Dissolved, ICP-MS 12.3 ug/L H 12.3 J unknown 0.4 2WG120037 BRANDREG Storm 1/25/2012 L54687-2 Copper, Dissolved, ICP-MS 11 ug/L H 11 J unknown 0.4 2WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Copper, Dissolved, ICP-MS 6.28 ug/L H 6.28 J unknown 0.4 2WG120037 A01007 Storm 2/28/2012 L55011-1 Copper, Dissolved, ICP-MS 16.1 ug/L H 16.1 J unknown 0.4 2WG120037 BRANDREG Storm 2/28/2012 L55011-2 Copper, Dissolved, ICP-MS 22.8 ug/L H 22.8 J unknown 0.4 2WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Copper, Dissolved, ICP-MS 14 ug/L H 14 J unknown 0.4 2WG120037 A01007 Storm 2/29/2012 L55186-1 Copper, Dissolved, ICP-MS 17.1 ug/L H 17.1 J unknown 0.4 2WG120037 BRANDREG Storm 2/29/2012 L55186-2 Copper, Dissolved, ICP-MS 15.9 ug/L H 15.9 J unknown 0.4 2WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Copper, Dissolved, ICP-MS 8.8 ug/L H 8.8 J unknown 0.4 2WG120037 A01007 Wet Base 2/15/2012 L55012-1 Copper, Dissolved, ICP-MS 18.8 ug/L H 18.8 J unknown 0.4 2WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Copper, Dissolved, ICP-MS 12.1 ug/L H 12.1 J unknown 0.4 2WG120037 A01007 Storm 1/25/2012 L54687-1 Lead, Dissolved, ICP-MS 2.81 ug/L H 2.81 J unknown 0.1 0.5WG120037 BRANDREG Storm 1/25/2012 L54687-2 Lead, Dissolved, ICP-MS 0.96 ug/L H 0.96 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Lead, Dissolved, ICP-MS 0.48 ug/L <RDL,H 0.48 J unknown 0.1 0.5WG120037 A01007 Storm 2/28/2012 L55011-1 Lead, Dissolved, ICP-MS 1.34 ug/L H 1.34 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/28/2012 L55011-2 Lead, Dissolved, ICP-MS 1.08 ug/L H 1.08 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Lead, Dissolved, ICP-MS 0.947 ug/L H 0.947 J unknown 0.1 0.5WG120037 A01007 Storm 2/29/2012 L55186-1 Lead, Dissolved, ICP-MS 1.91 ug/L H 1.91 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/29/2012 L55186-2 Lead, Dissolved, ICP-MS 0.828 ug/L H 0.828 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Lead, Dissolved, ICP-MS 0.504 ug/L H 0.504 J unknown 0.1 0.5WG120037 A01007 Wet Base 2/15/2012 L55012-1 Lead, Dissolved, ICP-MS 2.53 ug/L H 2.53 J unknown 0.1 0.5WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Lead, Dissolved, ICP-MS 1.64 ug/L H 1.64 J unknown 0.1 0.5WG120037 A01007 Storm 1/25/2012 L54687-1 Nickel, Dissolved, ICP-MS 1.94 ug/L H 1.94 J unknown 0.1 0.5WG120037 BRANDREG Storm 1/25/2012 L54687-2 Nickel, Dissolved, ICP-MS 6.74 ug/L H 6.74 J unknown 0.1 0.5





DV Value

DV Flag

Bias MDL RDL

WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Nickel, Dissolved, ICP-MS 1.26 ug/L H 1.26 J unknown 0.1 0.5WG120037 A01007 Storm 2/28/2012 L55011-1 Nickel, Dissolved, ICP-MS 2.97 ug/L H 2.97 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/28/2012 L55011-2 Nickel, Dissolved, ICP-MS 22.4 ug/L H 22.4 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Nickel, Dissolved, ICP-MS 2.64 ug/L H 2.64 J unknown 0.1 0.5WG120037 A01007 Storm 2/29/2012 L55186-1 Nickel, Dissolved, ICP-MS 2.34 ug/L H 2.34 J unknown 0.1 0.5WG120037 BRANDREG Storm 2/29/2012 L55186-2 Nickel, Dissolved, ICP-MS 12.2 ug/L H 12.2 J unknown 0.1 0.5WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Nickel, Dissolved, ICP-MS 1.37 ug/L H 1.37 J unknown 0.1 0.5WG120037 A01007 Wet Base 2/15/2012 L55012-1 Nickel, Dissolved, ICP-MS 2.69 ug/L H 2.69 J unknown 0.1 0.5WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Nickel, Dissolved, ICP-MS 2.01 ug/L H 2.01 J unknown 0.1 0.5WG120037 A01007 Storm 1/25/2012 L54687-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDREG Storm 1/25/2012 L54687-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 A01007 Storm 2/28/2012 L55011-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDREG Storm 2/28/2012 L55011-2 Silver, Dissolved, ICP-MS 0.17 ug/L <RDL,H 0.17 J unknown 0.04 0.2WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 A01007 Storm 2/29/2012 L55186-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDREG Storm 2/29/2012 L55186-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 A01007 Wet Base 2/15/2012 L55012-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Silver, Dissolved, ICP-MS 0.245 ug/L H 0.245 J unknown 0.04 0.2WG120037 A01007 Storm 1/25/2012 L54687-1 Vanadium, Dissolved, ICP-MS 0.771 ug/L H 0.771 J unknown 0.075 0.375WG120037 BRANDREG Storm 1/25/2012 L54687-2 Vanadium, Dissolved, ICP-MS 1.58 ug/L H 1.58 J unknown 0.075 0.375WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Vanadium, Dissolved, ICP-MS 1.34 ug/L H 1.34 J unknown 0.075 0.375WG120037 A01007 Storm 2/28/2012 L55011-1 Vanadium, Dissolved, ICP-MS 0.904 ug/L H 0.904 J unknown 0.075 0.375WG120037 BRANDREG Storm 2/28/2012 L55011-2 Vanadium, Dissolved, ICP-MS 0.737 ug/L H 0.737 J unknown 0.075 0.375WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Vanadium, Dissolved, ICP-MS 0.743 ug/L H 0.743 J unknown 0.075 0.375WG120037 A01007 Storm 2/29/2012 L55186-1 Vanadium, Dissolved, ICP-MS 1.23 ug/L H 1.23 J unknown 0.075 0.375WG120037 BRANDREG Storm 2/29/2012 L55186-2 Vanadium, Dissolved, ICP-MS 0.808 ug/L H 0.808 J unknown 0.075 0.375WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Vanadium, Dissolved, ICP-MS 0.822 ug/L H 0.822 J unknown 0.075 0.375WG120037 A01007 Wet Base 2/15/2012 L55012-1 Vanadium, Dissolved, ICP-MS 1.05 ug/L H 1.05 J unknown 0.075 0.375WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Vanadium, Dissolved, ICP-MS 0.904 ug/L H 0.904 J unknown 0.075 0.375WG120037 A01007 Storm 1/25/2012 L54687-1 Zinc, Dissolved, ICP-MS 98.2 ug/L H 98.2 J unknown 0.5 2.5WG120037 BRANDREG Storm 1/25/2012 L54687-2 Zinc, Dissolved, ICP-MS 57.3 ug/L H 57.3 J unknown 0.5 2.5WG120037 BRANDUTAHStorm 1/25/2012 L54687-3 Zinc, Dissolved, ICP-MS 22.5 ug/L H 22.5 J unknown 0.5 2.5WG120037 A01007 Storm 2/28/2012 L55011-1 Zinc, Dissolved, ICP-MS 75.5 ug/L H 75.5 J unknown 0.5 2.5WG120037 BRANDREG Storm 2/28/2012 L55011-2 Zinc, Dissolved, ICP-MS 73.6 ug/L H 73.6 J unknown 0.5 2.5WG120037 BRANDUTAHStorm 2/28/2012 L55011-3 Zinc, Dissolved, ICP-MS 61.3 ug/L H 61.3 J unknown 0.5 2.5WG120037 A01007 Storm 2/29/2012 L55186-1 Zinc, Dissolved, ICP-MS 52.9 ug/L H 52.9 J unknown 0.5 2.5





DV Value

DV Flag

Bias MDL RDL

WG120037 BRANDREG Storm 2/29/2012 L55186-2 Zinc, Dissolved, ICP-MS 63.6 ug/L H 63.6 J unknown 0.5 2.5WG120037 BRANDUTAHStorm 2/29/2012 L55186-3 Zinc, Dissolved, ICP-MS 39.5 ug/L H 39.5 J unknown 0.5 2.5WG120037 A01007 Wet Base 2/15/2012 L55012-1 Zinc, Dissolved, ICP-MS 63.9 ug/L H 63.9 J unknown 0.5 2.5WG120037 BRANDUTAHWet Base 2/15/2012 L55012-3 Zinc, Dissolved, ICP-MS 50.9 ug/L H 50.9 J unknown 0.5 2.5WG120847 A01007 Storm 3/27/2012 L55185-1 Arsenic, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/27/2012 L55185-2 Arsenic, Dissolved, ICP-MS 3.19 ug/L H 3.19 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Arsenic, Dissolved, ICP-MS 0.888 ug/L H 0.888 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/28/2012 L55285-2 Arsenic, Dissolved, ICP-MS 1.36 ug/L H 1.36 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Arsenic, Dissolved, ICP-MS 0.724 ug/L H 0.724 J unknown 0.1 0.5WG120847 A01007 Storm 4/11/2012 L55433-1 Arsenic, Dissolved, ICP-MS 8.62 ug/L H 8.62 J unknown 0.1 0.5WG120847 BRANDREG Storm 4/11/2012 L55433-2 Arsenic, Dissolved, ICP-MS 3.35 ug/L H 3.35 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Arsenic, Dissolved, ICP-MS 1.19 ug/L H 1.19 J unknown 0.1 0.5WG120847 A01007 Storm 4/24/2012 L55512-1 Arsenic, Dissolved, ICP-MS 1.2 ug/L H 1.2 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Arsenic, Dissolved, ICP-MS 1.01 ug/L H 1.01 J unknown 0.1 0.5WG120847 A01007 Wet Base 3/26/2012 L55154-1 Arsenic, Dissolved, ICP-MS 1.07 ug/L H 1.07 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Arsenic, Dissolved, ICP-MS 125 ug/L H 125 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/9/2012 L55183-1 Arsenic, Dissolved, ICP-MS 1.21 ug/L H 1.21 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Arsenic, Dissolved, ICP-MS 2.43 ug/L H 2.43 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Arsenic, Dissolved, ICP-MS 1 ug/L H 1 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Arsenic, Dissolved, ICP-MS 2.55 ug/L H 2.55 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Arsenic, Dissolved, ICP-MS 0.848 ug/L H 0.848 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/23/2012 L55511-1 Arsenic, Dissolved, ICP-MS 1.07 ug/L H 1.07 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Arsenic, Dissolved, ICP-MS 1.47 ug/L H 1.47 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Arsenic, Dissolved, ICP-MS 0.896 ug/L H 0.896 J unknown 0.1 0.5WG120847 A01007 Storm 3/27/2012 L55185-1 Cadmium, Dissolved, ICP-MS 0.1 ug/L <RDL,H 0.1 J unknown 0.05 0.25WG120847 BRANDREG Storm 3/27/2012 L55185-2 Cadmium, Dissolved, ICP-MS 0.375 ug/L H 0.375 J unknown 0.05 0.25WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Cadmium, Dissolved, ICP-MS 0.1 ug/L <RDL,H 0.1 J unknown 0.05 0.25WG120847 BRANDREG Storm 3/28/2012 L55285-2 Cadmium, Dissolved, ICP-MS 0.1 ug/L <RDL,H 0.1 J unknown 0.05 0.25WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Cadmium, Dissolved, ICP-MS 0.086 ug/L <RDL,H 0.086 J unknown 0.05 0.25WG120847 A01007 Storm 4/11/2012 L55433-1 Cadmium, Dissolved, ICP-MS 0.082 ug/L <RDL,H 0.082 J unknown 0.05 0.25WG120847 BRANDREG Storm 4/11/2012 L55433-2 Cadmium, Dissolved, ICP-MS 0.15 ug/L <RDL,H 0.15 J unknown 0.05 0.25WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG120847 A01007 Storm 4/24/2012 L55512-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Cadmium, Dissolved, ICP-MS 0.066 ug/L <RDL,H 0.066 J unknown 0.05 0.25WG120847 A01007 Wet Base 3/26/2012 L55154-1 Cadmium, Dissolved, ICP-MS 0.448 ug/L H 0.448 J unknown 0.05 0.25WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Cadmium, Dissolved, ICP-MS 0.743 ug/L H 0.743 J unknown 0.05 0.25WG120847 A01007 Wet Base 4/9/2012 L55183-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Cadmium, Dissolved, ICP-MS 0.16 ug/L <RDL,H 0.16 J unknown 0.05 0.25





DV Value

DV Flag

Bias MDL RDL

WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Cadmium, Dissolved, ICP-MS 0.072 ug/L <RDL,H 0.072 J unknown 0.05 0.25WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Cadmium, Dissolved, ICP-MS 0.18 ug/L <RDL,H 0.18 J unknown 0.05 0.25WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Cadmium, Dissolved, ICP-MS 0.065 ug/L <RDL,H 0.065 J unknown 0.05 0.25WG120847 A01007 Wet Base 4/23/2012 L55511-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Cadmium, Dissolved, ICP-MS 0.11 ug/L <RDL,H 0.11 J unknown 0.05 0.25WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Cadmium, Dissolved, ICP-MS 0.08 ug/L <RDL,H 0.08 J unknown 0.05 0.25WG120847 A01007 Storm 3/27/2012 L55185-1 Chromium, Dissolved, ICP-MS 0.93 ug/L <RDL,H 0.93 J unknown 0.2 1WG120847 BRANDREG Storm 3/27/2012 L55185-2 Chromium, Dissolved, ICP-MS 2.26 ug/L H 2.26 J unknown 0.2 1WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Chromium, Dissolved, ICP-MS 0.69 ug/L <RDL,H 0.69 J unknown 0.2 1WG120847 BRANDREG Storm 3/28/2012 L55285-2 Chromium, Dissolved, ICP-MS 1.27 ug/L H 1.27 J unknown 0.2 1WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Chromium, Dissolved, ICP-MS 0.49 ug/L <RDL,H 0.49 J unknown 0.2 1WG120847 A01007 Storm 4/11/2012 L55433-1 Chromium, Dissolved, ICP-MS 1.35 ug/L H 1.35 J unknown 0.2 1WG120847 BRANDREG Storm 4/11/2012 L55433-2 Chromium, Dissolved, ICP-MS 1.87 ug/L H 1.87 J unknown 0.2 1WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Chromium, Dissolved, ICP-MS 0.51 ug/L <RDL,H 0.51 J unknown 0.2 1WG120847 A01007 Storm 4/24/2012 L55512-1 Chromium, Dissolved, ICP-MS 1.07 ug/L H 1.07 J unknown 0.2 1WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Chromium, Dissolved, ICP-MS 0.8 ug/L <RDL,H 0.8 J unknown 0.2 1WG120847 A01007 Wet Base 3/26/2012 L55154-1 Chromium, Dissolved, ICP-MS 0.95 ug/L <RDL,H 0.95 J unknown 0.2 1WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Chromium, Dissolved, ICP-MS 177 ug/L H 177 J unknown 0.2 1WG120847 A01007 Wet Base 4/9/2012 L55183-1 Chromium, Dissolved, ICP-MS 2.01 ug/L H 2.01 J unknown 0.2 1WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Chromium, Dissolved, ICP-MS 1.69 ug/L H 1.69 J unknown 0.2 1WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Chromium, Dissolved, ICP-MS 0.51 ug/L <RDL,H 0.51 J unknown 0.2 1WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Chromium, Dissolved, ICP-MS 1.74 ug/L H 1.74 J unknown 0.2 1WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Chromium, Dissolved, ICP-MS 0.35 ug/L <RDL,H 0.35 J unknown 0.2 1WG120847 A01007 Wet Base 4/23/2012 L55511-1 Chromium, Dissolved, ICP-MS 2.07 ug/L H 2.07 J unknown 0.2 1WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Chromium, Dissolved, ICP-MS 1.77 ug/L H 1.77 J unknown 0.2 1WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Chromium, Dissolved, ICP-MS 4.09 ug/L H 4.09 J unknown 0.2 1WG120847 A01007 Storm 3/27/2012 L55185-1 Copper, Dissolved, ICP-MS 14.9 ug/L H 14.9 J unknown 0.4 2WG120847 BRANDREG Storm 3/27/2012 L55185-2 Copper, Dissolved, ICP-MS 19.4 ug/L H 19.4 J unknown 0.4 2WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Copper, Dissolved, ICP-MS 11.8 ug/L H 11.8 J unknown 0.4 2WG120847 BRANDREG Storm 3/28/2012 L55285-2 Copper, Dissolved, ICP-MS 16.1 ug/L H 16.1 J unknown 0.4 2WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Copper, Dissolved, ICP-MS 14.3 ug/L H 14.3 J unknown 0.4 2WG120847 A01007 Storm 4/11/2012 L55433-1 Copper, Dissolved, ICP-MS 18.7 ug/L H 18.7 J unknown 0.4 2WG120847 BRANDREG Storm 4/11/2012 L55433-2 Copper, Dissolved, ICP-MS 29.1 ug/L H 29.1 J unknown 0.4 2WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Copper, Dissolved, ICP-MS 12.9 ug/L H 12.9 J unknown 0.4 2WG120847 A01007 Storm 4/24/2012 L55512-1 Copper, Dissolved, ICP-MS 13.6 ug/L H 13.6 J unknown 0.4 2WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Copper, Dissolved, ICP-MS 12.9 ug/L H 12.9 J unknown 0.4 2WG120847 A01007 Wet Base 3/26/2012 L55154-1 Copper, Dissolved, ICP-MS 16.3 ug/L H 16.3 J unknown 0.4 2WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Copper, Dissolved, ICP-MS 21.2 ug/L H 21.2 J unknown 0.4 2





DV Value

DV Flag

Bias MDL RDL

WG120847 A01007 Wet Base 4/9/2012 L55183-1 Copper, Dissolved, ICP-MS 14.3 ug/L H 14.3 J unknown 0.4 2WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Copper, Dissolved, ICP-MS 19.8 ug/L H 19.8 J unknown 0.4 2WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Copper, Dissolved, ICP-MS 17.5 ug/L H 17.5 J unknown 0.4 2WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Copper, Dissolved, ICP-MS 31.7 ug/L H 31.7 J unknown 0.4 2WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Copper, Dissolved, ICP-MS 13.9 ug/L H 13.9 J unknown 0.4 2WG120847 A01007 Wet Base 4/23/2012 L55511-1 Copper, Dissolved, ICP-MS 18.3 ug/L H 18.3 J unknown 0.4 2WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Copper, Dissolved, ICP-MS 31.6 ug/L H 31.6 J unknown 0.4 2WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Copper, Dissolved, ICP-MS 17.3 ug/L H 17.3 J unknown 0.4 2WG120847 A01007 Storm 3/27/2012 L55185-1 Lead, Dissolved, ICP-MS 1.87 ug/L H 1.87 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/27/2012 L55185-2 Lead, Dissolved, ICP-MS 3.48 ug/L H 3.48 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Lead, Dissolved, ICP-MS 0.957 ug/L H 0.957 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/28/2012 L55285-2 Lead, Dissolved, ICP-MS 1.65 ug/L H 1.65 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Lead, Dissolved, ICP-MS 1.14 ug/L H 1.14 J unknown 0.1 0.5WG120847 A01007 Storm 4/11/2012 L55433-1 Lead, Dissolved, ICP-MS 1.22 ug/L H 1.22 J unknown 0.1 0.5WG120847 BRANDREG Storm 4/11/2012 L55433-2 Lead, Dissolved, ICP-MS 3.32 ug/L H 3.32 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Lead, Dissolved, ICP-MS 1.04 ug/L H 1.04 J unknown 0.1 0.5WG120847 A01007 Storm 4/24/2012 L55512-1 Lead, Dissolved, ICP-MS 0.794 ug/L H 0.794 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Lead, Dissolved, ICP-MS 1.53 ug/L H 1.53 J unknown 0.1 0.5WG120847 A01007 Wet Base 3/26/2012 L55154-1 Lead, Dissolved, ICP-MS 3.5 ug/L H 3.5 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Lead, Dissolved, ICP-MS 2.98 ug/L H 2.98 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/9/2012 L55183-1 Lead, Dissolved, ICP-MS 1.24 ug/L H 1.24 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Lead, Dissolved, ICP-MS 4.38 ug/L H 4.38 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Lead, Dissolved, ICP-MS 1.57 ug/L H 1.57 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Lead, Dissolved, ICP-MS 4.81 ug/L H 4.81 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Lead, Dissolved, ICP-MS 1.48 ug/L H 1.48 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/23/2012 L55511-1 Lead, Dissolved, ICP-MS 1.33 ug/L H 1.33 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Lead, Dissolved, ICP-MS 1.34 ug/L H 1.34 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Lead, Dissolved, ICP-MS 2.03 ug/L H 2.03 J unknown 0.1 0.5WG120847 A01007 Storm 3/27/2012 L55185-1 Nickel, Dissolved, ICP-MS 3.01 ug/L H 3.01 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/27/2012 L55185-2 Nickel, Dissolved, ICP-MS 9.98 ug/L H 9.98 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Nickel, Dissolved, ICP-MS 3.18 ug/L H 3.18 J unknown 0.1 0.5WG120847 BRANDREG Storm 3/28/2012 L55285-2 Nickel, Dissolved, ICP-MS 553 ug/L H 553 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Nickel, Dissolved, ICP-MS 2.74 ug/L H 2.74 J unknown 0.1 0.5WG120847 A01007 Storm 4/11/2012 L55433-1 Nickel, Dissolved, ICP-MS 4.23 ug/L H 4.23 J unknown 0.1 0.5WG120847 BRANDREG Storm 4/11/2012 L55433-2 Nickel, Dissolved, ICP-MS 120 ug/L H 120 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Nickel, Dissolved, ICP-MS 3.49 ug/L H 3.49 J unknown 0.1 0.5WG120847 A01007 Storm 4/24/2012 L55512-1 Nickel, Dissolved, ICP-MS 4.94 ug/L H 4.94 J unknown 0.1 0.5WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Nickel, Dissolved, ICP-MS 3.31 ug/L H 3.31 J unknown 0.1 0.5





DV Value

DV Flag

Bias MDL RDL

WG120847 A01007 Wet Base 3/26/2012 L55154-1 Nickel, Dissolved, ICP-MS 4.32 ug/L H 4.32 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Nickel, Dissolved, ICP-MS 11.4 ug/L H 11.4 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/9/2012 L55183-1 Nickel, Dissolved, ICP-MS 3.88 ug/L H 3.88 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Nickel, Dissolved, ICP-MS 25.3 ug/L H 25.3 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Nickel, Dissolved, ICP-MS 2.11 ug/L H 2.11 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Nickel, Dissolved, ICP-MS 748 ug/L H 748 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Nickel, Dissolved, ICP-MS 1.81 ug/L H 1.81 J unknown 0.1 0.5WG120847 A01007 Wet Base 4/23/2012 L55511-1 Nickel, Dissolved, ICP-MS 3.17 ug/L H 3.17 J unknown 0.1 0.5WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Nickel, Dissolved, ICP-MS 27.6 ug/L H 27.6 J unknown 0.1 0.5WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Nickel, Dissolved, ICP-MS 2.57 ug/L H 2.57 J unknown 0.1 0.5WG120847 A01007 Storm 3/27/2012 L55185-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Storm 3/27/2012 L55185-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Silver, Dissolved, ICP-MS 0.19 ug/L <RDL,H 0.19 J unknown 0.04 0.2WG120847 BRANDREG Storm 3/28/2012 L55285-2 Silver, Dissolved, ICP-MS 0.212 ug/L H 0.212 J unknown 0.04 0.2WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 A01007 Storm 4/11/2012 L55433-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Storm 4/11/2012 L55433-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 A01007 Storm 4/24/2012 L55512-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Silver, Dissolved, ICP-MS 0.665 ug/L H 0.665 J unknown 0.04 0.2WG120847 A01007 Wet Base 3/26/2012 L55154-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 A01007 Wet Base 4/9/2012 L55183-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Silver, Dissolved, ICP-MS 0.065 ug/L <RDL,H 0.065 J unknown 0.04 0.2WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Silver, Dissolved, ICP-MS 0.16 ug/L <RDL,H 0.16 J unknown 0.04 0.2WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 A01007 Wet Base 4/23/2012 L55511-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Silver, Dissolved, ICP-MS 0.057 ug/L <RDL,H 0.057 J unknown 0.04 0.2WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Silver, Dissolved, ICP-MS 0.908 ug/L H 0.908 J unknown 0.04 0.2WG120847 A01007 Storm 3/27/2012 L55185-1 Vanadium, Dissolved, ICP-MS 1.25 ug/L H 1.25 J unknown 0.075 0.375WG120847 BRANDREG Storm 3/27/2012 L55185-2 Vanadium, Dissolved, ICP-MS 1.37 ug/L H 1.37 J unknown 0.075 0.375WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Vanadium, Dissolved, ICP-MS 1.22 ug/L H 1.22 J unknown 0.075 0.375WG120847 BRANDREG Storm 3/28/2012 L55285-2 Vanadium, Dissolved, ICP-MS 1.02 ug/L H 1.02 J unknown 0.075 0.375WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Vanadium, Dissolved, ICP-MS 0.957 ug/L H 0.957 J unknown 0.075 0.375WG120847 A01007 Storm 4/11/2012 L55433-1 Vanadium, Dissolved, ICP-MS 1.28 ug/L H 1.28 J unknown 0.075 0.375WG120847 BRANDREG Storm 4/11/2012 L55433-2 Vanadium, Dissolved, ICP-MS 1.4 ug/L H 1.4 J unknown 0.075 0.375WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Vanadium, Dissolved, ICP-MS 1.51 ug/L H 1.51 J unknown 0.075 0.375





DV Value

DV Flag

Bias MDL RDL

WG120847 A01007 Storm 4/24/2012 L55512-1 Vanadium, Dissolved, ICP-MS 1.1 ug/L H 1.1 J unknown 0.075 0.375WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Vanadium, Dissolved, ICP-MS 1.11 ug/L H 1.11 J unknown 0.075 0.375WG120847 A01007 Wet Base 3/26/2012 L55154-1 Vanadium, Dissolved, ICP-MS 0.977 ug/L H 0.977 J unknown 0.075 0.375WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Vanadium, Dissolved, ICP-MS 5.71 ug/L H 5.71 J unknown 0.075 0.375WG120847 A01007 Wet Base 4/9/2012 L55183-1 Vanadium, Dissolved, ICP-MS 1.24 ug/L H 1.24 J unknown 0.075 0.375WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Vanadium, Dissolved, ICP-MS 2.77 ug/L H 2.77 J unknown 0.075 0.375WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Vanadium, Dissolved, ICP-MS 1.04 ug/L H 1.04 J unknown 0.075 0.375WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Vanadium, Dissolved, ICP-MS 1.88 ug/L H 1.88 J unknown 0.075 0.375WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Vanadium, Dissolved, ICP-MS 0.854 ug/L H 0.854 J unknown 0.075 0.375WG120847 A01007 Wet Base 4/23/2012 L55511-1 Vanadium, Dissolved, ICP-MS 1.3 ug/L H 1.3 J unknown 0.075 0.375WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Vanadium, Dissolved, ICP-MS 1.27 ug/L H 1.27 J unknown 0.075 0.375WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Vanadium, Dissolved, ICP-MS 0.971 ug/L H 0.971 J unknown 0.075 0.375WG120847 A01007 Storm 3/27/2012 L55185-1 Zinc, Dissolved, ICP-MS 76.4 ug/L H 76.4 J unknown 0.5 2.5WG120847 BRANDREG Storm 3/27/2012 L55185-2 Zinc, Dissolved, ICP-MS 114 ug/L H 114 J unknown 0.5 2.5WG120847 BRANDUTAHStorm 3/27/2012 L55185-3 Zinc, Dissolved, ICP-MS 73.3 ug/L H 73.3 J unknown 0.5 2.5WG120847 BRANDREG Storm 3/28/2012 L55285-2 Zinc, Dissolved, ICP-MS 51.4 ug/L H 51.4 J unknown 0.5 2.5WG120847 BRANDUTAHStorm 3/28/2012 L55285-3 Zinc, Dissolved, ICP-MS 65.4 ug/L H 65.4 J unknown 0.5 2.5WG120847 A01007 Storm 4/11/2012 L55433-1 Zinc, Dissolved, ICP-MS 89.2 ug/L H 89.2 J unknown 0.5 2.5WG120847 BRANDREG Storm 4/11/2012 L55433-2 Zinc, Dissolved, ICP-MS 73.8 ug/L H 73.8 J unknown 0.5 2.5WG120847 BRANDUTAHStorm 4/11/2012 L55433-3 Zinc, Dissolved, ICP-MS 28 ug/L H 28 J unknown 0.5 2.5WG120847 A01007 Storm 4/24/2012 L55512-1 Zinc, Dissolved, ICP-MS 71 ug/L H 71 J unknown 0.5 2.5WG120847 BRANDUTAHStorm 4/24/2012 L55512-3 Zinc, Dissolved, ICP-MS 84.5 ug/L H 84.5 J unknown 0.5 2.5WG120847 A01007 Wet Base 3/26/2012 L55154-1 Zinc, Dissolved, ICP-MS 50.7 ug/L H 50.7 J unknown 0.5 2.5WG120847 BRANDREG Wet Base 3/26/2012 L55154-2 Zinc, Dissolved, ICP-MS 82.6 ug/L H 82.6 J unknown 0.5 2.5WG120847 A01007 Wet Base 4/9/2012 L55183-1 Zinc, Dissolved, ICP-MS 59.8 ug/L H 59.8 J unknown 0.5 2.5WG120847 BRANDREG Wet Base 4/9/2012 L55183-2 Zinc, Dissolved, ICP-MS 62.3 ug/L H 62.3 J unknown 0.5 2.5WG120847 BRANDUTAHWet Base 4/9/2012 L55183-3 Zinc, Dissolved, ICP-MS 27.6 ug/L H 27.6 J unknown 0.5 2.5WG120847 BRANDREG Wet Base 4/10/2012 L55184-2 Zinc, Dissolved, ICP-MS 78.6 ug/L H 78.6 J unknown 0.5 2.5WG120847 BRANDUTAHWet Base 4/10/2012 L55184-3 Zinc, Dissolved, ICP-MS 20.4 ug/L H 20.4 J unknown 0.5 2.5WG120847 A01007 Wet Base 4/23/2012 L55511-1 Zinc, Dissolved, ICP-MS 53.4 ug/L H 53.4 J unknown 0.5 2.5WG120847 BRANDREG Wet Base 4/23/2012 L55511-2 Zinc, Dissolved, ICP-MS 79.1 ug/L H 79.1 J unknown 0.5 2.5WG120847 BRANDUTAHWet Base 4/23/2012 L55511-3 Zinc, Dissolved, ICP-MS 40.5 ug/L H 40.5 J unknown 0.5 2.5WG121302 BRANDREG Storm 4/24/2012 L55512-2 Arsenic, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.1 0.5WG121302 A01007 Storm 4/25/2012 L55584-1 Arsenic, Dissolved, ICP-MS 1.03 ug/L H 1.03 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/25/2012 L55584-2 Arsenic, Dissolved, ICP-MS 0.987 ug/L H 0.987 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Arsenic, Dissolved, ICP-MS 0.827 ug/L H 0.827 J unknown 0.1 0.5WG121302 A01007 Storm 5/21/2012 L55638-1 Arsenic, Dissolved, ICP-MS 0.995 ug/L H 0.995 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/21/2012 L55638-2 Arsenic, Dissolved, ICP-MS 1.03 ug/L H 1.03 J unknown 0.1 0.5





DV Value

DV Flag

Bias MDL RDL

WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Arsenic, Dissolved, ICP-MS 0.771 ug/L H 0.771 J unknown 0.1 0.5WG121302 A01007 Storm 5/22/2012 L55763-1 Arsenic, Dissolved, ICP-MS 2.3 ug/L H 2.3 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/22/2012 L55763-2 Arsenic, Dissolved, ICP-MS 1.55 ug/L H 1.55 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Arsenic, Dissolved, ICP-MS 0.97 ug/L H 0.97 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/7/2012 L55572-1 Arsenic, Dissolved, ICP-MS 1.11 ug/L H 1.11 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Arsenic, Dissolved, ICP-MS 0.8 ug/L H 0.8 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/8/2012 L55686-1 Arsenic, Dissolved, ICP-MS 1.43 ug/L H 1.43 J unknown 0.1 0.5WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Arsenic, Dissolved, ICP-MS 1.43 ug/L H 1.43 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Arsenic, Dissolved, ICP-MS 0.916 ug/L H 0.916 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/24/2012 L55512-2 Cadmium, Dissolved, ICP-MS 0.082 ug/L <RDL,H 0.082 J unknown 0.05 0.25WG121302 A01007 Storm 4/25/2012 L55584-1 Cadmium, Dissolved, ICP-MS 0.051 ug/L <RDL,H 0.051 J unknown 0.05 0.25WG121302 BRANDREG Storm 4/25/2012 L55584-2 Cadmium, Dissolved, ICP-MS 0.097 ug/L <RDL,H 0.097 J unknown 0.05 0.25WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Cadmium, Dissolved, ICP-MS 0.1 ug/L <RDL,H 0.1 J unknown 0.05 0.25WG121302 A01007 Storm 5/21/2012 L55638-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121302 BRANDREG Storm 5/21/2012 L55638-2 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Cadmium, Dissolved, ICP-MS 0.1 ug/L <RDL,H 0.1 J unknown 0.05 0.25WG121302 A01007 Storm 5/22/2012 L55763-1 Cadmium, Dissolved, ICP-MS 0.072 ug/L <RDL,H 0.072 J unknown 0.05 0.25WG121302 BRANDREG Storm 5/22/2012 L55763-2 Cadmium, Dissolved, ICP-MS 0.11 ug/L <RDL,H 0.11 J unknown 0.05 0.25WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Cadmium, Dissolved, ICP-MS 0.096 ug/L <RDL,H 0.096 J unknown 0.05 0.25WG121302 A01007 Wet Base 5/7/2012 L55572-1 Cadmium, Dissolved, ICP-MS 0.067 ug/L <RDL,H 0.067 J unknown 0.05 0.25WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121302 A01007 Wet Base 5/8/2012 L55686-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Cadmium, Dissolved, ICP-MS 0.069 ug/L <RDL,H 0.069 J unknown 0.05 0.25WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Cadmium, Dissolved, ICP-MS 0.053 ug/L <RDL,H 0.053 J unknown 0.05 0.25WG121302 BRANDREG Storm 4/24/2012 L55512-2 Chromium, Dissolved, ICP-MS 1.35 ug/L H 1.35 J unknown 0.2 1WG121302 A01007 Storm 4/25/2012 L55584-1 Chromium, Dissolved, ICP-MS 0.64 ug/L <RDL,H 0.64 J unknown 0.2 1WG121302 BRANDREG Storm 4/25/2012 L55584-2 Chromium, Dissolved, ICP-MS 0.85 ug/L <RDL,H 0.85 J unknown 0.2 1WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Chromium, Dissolved, ICP-MS 0.53 ug/L <RDL,H 0.53 J unknown 0.2 1WG121302 A01007 Storm 5/21/2012 L55638-1 Chromium, Dissolved, ICP-MS 0.9 ug/L <RDL,H 0.9 J unknown 0.2 1WG121302 BRANDREG Storm 5/21/2012 L55638-2 Chromium, Dissolved, ICP-MS 0.96 ug/L <RDL,H 0.96 J unknown 0.2 1WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Chromium, Dissolved, ICP-MS 0.65 ug/L <RDL,H 0.65 J unknown 0.2 1WG121302 A01007 Storm 5/22/2012 L55763-1 Chromium, Dissolved, ICP-MS 1.39 ug/L H 1.39 J unknown 0.2 1WG121302 BRANDREG Storm 5/22/2012 L55763-2 Chromium, Dissolved, ICP-MS 1.36 ug/L H 1.36 J unknown 0.2 1WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Chromium, Dissolved, ICP-MS 0.89 ug/L <RDL,H 0.89 J unknown 0.2 1WG121302 A01007 Wet Base 5/7/2012 L55572-1 Chromium, Dissolved, ICP-MS 4.7 ug/L H 4.7 J unknown 0.2 1WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Chromium, Dissolved, ICP-MS 0.7 ug/L <RDL,H 0.7 J unknown 0.2 1WG121302 A01007 Wet Base 5/8/2012 L55686-1 Chromium, Dissolved, ICP-MS 3.04 ug/L H 3.04 J unknown 0.2 1WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Chromium, Dissolved, ICP-MS 2.08 ug/L H 2.08 J unknown 0.2 1





DV Value

DV Flag

Bias MDL RDL

WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Chromium, Dissolved, ICP-MS 0.48 ug/L <RDL,H 0.48 J unknown 0.2 1WG121302 BRANDREG Storm 4/24/2012 L55512-2 Copper, Dissolved, ICP-MS 20.9 ug/L H 20.9 J unknown 0.4 2WG121302 A01007 Storm 4/25/2012 L55584-1 Copper, Dissolved, ICP-MS 9.82 ug/L H 9.82 J unknown 0.4 2WG121302 BRANDREG Storm 4/25/2012 L55584-2 Copper, Dissolved, ICP-MS 12.8 ug/L H 12.8 J unknown 0.4 2WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Copper, Dissolved, ICP-MS 12.6 ug/L H 12.6 J unknown 0.4 2WG121302 A01007 Storm 5/21/2012 L55638-1 Copper, Dissolved, ICP-MS 7.17 ug/L H 7.17 J unknown 0.4 2WG121302 BRANDREG Storm 5/21/2012 L55638-2 Copper, Dissolved, ICP-MS 11.2 ug/L H 11.2 J unknown 0.4 2WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Copper, Dissolved, ICP-MS 11.2 ug/L H 11.2 J unknown 0.4 2WG121302 A01007 Storm 5/22/2012 L55763-1 Copper, Dissolved, ICP-MS 14.4 ug/L H 14.4 J unknown 0.4 2WG121302 BRANDREG Storm 5/22/2012 L55763-2 Copper, Dissolved, ICP-MS 27.1 ug/L H 27.1 J unknown 0.4 2WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Copper, Dissolved, ICP-MS 13.4 ug/L H 13.4 J unknown 0.4 2WG121302 A01007 Wet Base 5/7/2012 L55572-1 Copper, Dissolved, ICP-MS 23.5 ug/L H 23.5 J unknown 0.4 2WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Copper, Dissolved, ICP-MS 15.3 ug/L H 15.3 J unknown 0.4 2WG121302 A01007 Wet Base 5/8/2012 L55686-1 Copper, Dissolved, ICP-MS 9.77 ug/L H 9.77 J unknown 0.4 2WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Copper, Dissolved, ICP-MS 7.64 ug/L H 7.64 J unknown 0.4 2WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Copper, Dissolved, ICP-MS 7.87 ug/L H 7.87 J unknown 0.4 2WG121302 BRANDREG Storm 4/24/2012 L55512-2 Lead, Dissolved, ICP-MS 1.24 ug/L H 1.24 J unknown 0.1 0.5WG121302 A01007 Storm 4/25/2012 L55584-1 Lead, Dissolved, ICP-MS 1.22 ug/L H 1.22 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/25/2012 L55584-2 Lead, Dissolved, ICP-MS 1.1 ug/L H 1.1 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Lead, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.1 0.5WG121302 A01007 Storm 5/21/2012 L55638-1 Lead, Dissolved, ICP-MS 1.08 ug/L H 1.08 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/21/2012 L55638-2 Lead, Dissolved, ICP-MS 1.15 ug/L H 1.15 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Lead, Dissolved, ICP-MS 1.09 ug/L H 1.09 J unknown 0.1 0.5WG121302 A01007 Storm 5/22/2012 L55763-1 Lead, Dissolved, ICP-MS 6.31 ug/L H 6.31 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/22/2012 L55763-2 Lead, Dissolved, ICP-MS 3.53 ug/L H 3.53 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Lead, Dissolved, ICP-MS 2.53 ug/L H 2.53 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/7/2012 L55572-1 Lead, Dissolved, ICP-MS 1.74 ug/L H 1.74 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Lead, Dissolved, ICP-MS 1.59 ug/L H 1.59 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/8/2012 L55686-1 Lead, Dissolved, ICP-MS 1.89 ug/L H 1.89 J unknown 0.1 0.5WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Lead, Dissolved, ICP-MS 0.604 ug/L H 0.604 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Lead, Dissolved, ICP-MS 1.01 ug/L H 1.01 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/24/2012 L55512-2 Nickel, Dissolved, ICP-MS 21.8 ug/L H 21.8 J unknown 0.1 0.5WG121302 A01007 Storm 4/25/2012 L55584-1 Nickel, Dissolved, ICP-MS 1.86 ug/L H 1.86 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/25/2012 L55584-2 Nickel, Dissolved, ICP-MS 10.7 ug/L H 10.7 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Nickel, Dissolved, ICP-MS 2.63 ug/L H 2.63 J unknown 0.1 0.5WG121302 A01007 Storm 5/21/2012 L55638-1 Nickel, Dissolved, ICP-MS 1.33 ug/L H 1.33 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/21/2012 L55638-2 Nickel, Dissolved, ICP-MS 10.3 ug/L H 10.3 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Nickel, Dissolved, ICP-MS 1.72 ug/L H 1.72 J unknown 0.1 0.5





DV Value

DV Flag

Bias MDL RDL

WG121302 A01007 Storm 5/22/2012 L55763-1 Nickel, Dissolved, ICP-MS 3.76 ug/L H 3.76 J unknown 0.1 0.5WG121302 BRANDREG Storm 5/22/2012 L55763-2 Nickel, Dissolved, ICP-MS 13.1 ug/L H 13.1 J unknown 0.1 0.5WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Nickel, Dissolved, ICP-MS 2.75 ug/L H 2.75 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/7/2012 L55572-1 Nickel, Dissolved, ICP-MS 3.97 ug/L H 3.97 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Nickel, Dissolved, ICP-MS 2.99 ug/L H 2.99 J unknown 0.1 0.5WG121302 A01007 Wet Base 5/8/2012 L55686-1 Nickel, Dissolved, ICP-MS 4.81 ug/L H 4.81 J unknown 0.1 0.5WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Nickel, Dissolved, ICP-MS 32.7 ug/L H 32.7 J unknown 0.1 0.5WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Nickel, Dissolved, ICP-MS 2.24 ug/L H 2.24 J unknown 0.1 0.5WG121302 BRANDREG Storm 4/24/2012 L55512-2 Silver, Dissolved, ICP-MS 0.08 ug/L <RDL,H 0.08 J unknown 0.04 0.2WG121302 A01007 Storm 4/25/2012 L55584-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDREG Storm 4/25/2012 L55584-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Silver, Dissolved, ICP-MS 0.16 ug/L <RDL,H 0.16 J unknown 0.04 0.2WG121302 A01007 Storm 5/21/2012 L55638-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDREG Storm 5/21/2012 L55638-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Silver, Dissolved, ICP-MS 0.052 ug/L <RDL,H 0.052 J unknown 0.04 0.2WG121302 A01007 Storm 5/22/2012 L55763-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDREG Storm 5/22/2012 L55763-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 A01007 Wet Base 5/7/2012 L55572-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 A01007 Wet Base 5/8/2012 L55686-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121302 BRANDREG Storm 4/24/2012 L55512-2 Vanadium, Dissolved, ICP-MS 0.942 ug/L H 0.942 J unknown 0.075 0.375WG121302 A01007 Storm 4/25/2012 L55584-1 Vanadium, Dissolved, ICP-MS 1.31 ug/L H 1.31 J unknown 0.075 0.375WG121302 BRANDREG Storm 4/25/2012 L55584-2 Vanadium, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.075 0.375WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Vanadium, Dissolved, ICP-MS 1.53 ug/L H 1.53 J unknown 0.075 0.375WG121302 A01007 Storm 5/21/2012 L55638-1 Vanadium, Dissolved, ICP-MS 1.37 ug/L H 1.37 J unknown 0.075 0.375WG121302 BRANDREG Storm 5/21/2012 L55638-2 Vanadium, Dissolved, ICP-MS 1.22 ug/L H 1.22 J unknown 0.075 0.375WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Vanadium, Dissolved, ICP-MS 1.47 ug/L H 1.47 J unknown 0.075 0.375WG121302 A01007 Storm 5/22/2012 L55763-1 Vanadium, Dissolved, ICP-MS 1.76 ug/L H 1.76 J unknown 0.075 0.375WG121302 BRANDREG Storm 5/22/2012 L55763-2 Vanadium, Dissolved, ICP-MS 1.19 ug/L H 1.19 J unknown 0.075 0.375WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Vanadium, Dissolved, ICP-MS 1.54 ug/L H 1.54 J unknown 0.075 0.375WG121302 A01007 Wet Base 5/7/2012 L55572-1 Vanadium, Dissolved, ICP-MS 1.28 ug/L H 1.28 J unknown 0.075 0.375WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Vanadium, Dissolved, ICP-MS 0.8 ug/L H 0.8 J unknown 0.075 0.375WG121302 A01007 Wet Base 5/8/2012 L55686-1 Vanadium, Dissolved, ICP-MS 1.41 ug/L H 1.41 J unknown 0.075 0.375WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Vanadium, Dissolved, ICP-MS 1.63 ug/L H 1.63 J unknown 0.075 0.375WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Vanadium, Dissolved, ICP-MS 0.89 ug/L H 0.89 J unknown 0.075 0.375





DV Value

DV Flag

Bias MDL RDL

WG121302 BRANDREG Storm 4/24/2012 L55512-2 Zinc, Dissolved, ICP-MS 80.8 ug/L H 80.8 J unknown 0.5 2.5WG121302 A01007 Storm 4/25/2012 L55584-1 Zinc, Dissolved, ICP-MS 54.5 ug/L H 54.5 J unknown 0.5 2.5WG121302 BRANDREG Storm 4/25/2012 L55584-2 Zinc, Dissolved, ICP-MS 64.6 ug/L H 64.6 J unknown 0.5 2.5WG121302 BRANDUTAHStorm 4/25/2012 L55584-3 Zinc, Dissolved, ICP-MS 70.1 ug/L H 70.1 J unknown 0.5 2.5WG121302 A01007 Storm 5/21/2012 L55638-1 Zinc, Dissolved, ICP-MS 42.1 ug/L H 42.1 J unknown 0.5 2.5WG121302 BRANDREG Storm 5/21/2012 L55638-2 Zinc, Dissolved, ICP-MS 61.4 ug/L H 61.4 J unknown 0.5 2.5WG121302 BRANDUTAHStorm 5/21/2012 L55638-3 Zinc, Dissolved, ICP-MS 48.9 ug/L H 48.9 J unknown 0.5 2.5WG121302 A01007 Storm 5/22/2012 L55763-1 Zinc, Dissolved, ICP-MS 127 ug/L H 127 J unknown 0.5 2.5WG121302 BRANDREG Storm 5/22/2012 L55763-2 Zinc, Dissolved, ICP-MS 93.2 ug/L H 93.2 J unknown 0.5 2.5WG121302 BRANDUTAHStorm 5/22/2012 L55763-3 Zinc, Dissolved, ICP-MS 82.2 ug/L H 82.2 J unknown 0.5 2.5WG121302 A01007 Wet Base 5/7/2012 L55572-1 Zinc, Dissolved, ICP-MS 52.4 ug/L H 52.4 J unknown 0.5 2.5WG121302 BRANDUTAHWet Base 5/7/2012 L55572-3 Zinc, Dissolved, ICP-MS 33.4 ug/L H 33.4 J unknown 0.5 2.5WG121302 A01007 Wet Base 5/8/2012 L55686-1 Zinc, Dissolved, ICP-MS 85.4 ug/L H 85.4 J unknown 0.5 2.5WG121302 BRANDREG Wet Base 5/8/2012 L55686-2 Zinc, Dissolved, ICP-MS 98 ug/L H 98 J unknown 0.5 2.5WG121302 BRANDUTAHWet Base 5/8/2012 L55686-3 Zinc, Dissolved, ICP-MS 48.3 ug/L H 48.3 J unknown 0.5 2.5WG121990 A01007 Storm 6/4/2012 L55764-1 Arsenic, Dissolved, ICP-MS 1.28 ug/L H 1.28 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/4/2012 L55764-2 Arsenic, Dissolved, ICP-MS 1.03 ug/L H 1.03 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Arsenic, Dissolved, ICP-MS 0.87 ug/L H 0.87 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/5/2012 L55859-2 Arsenic, Dissolved, ICP-MS 1.23 ug/L H 1.23 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Arsenic, Dissolved, ICP-MS 0.729 ug/L H 0.729 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/6/2012 L55875-2 Arsenic, Dissolved, ICP-MS 0.879 ug/L H 0.879 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Arsenic, Dissolved, ICP-MS 0.624 ug/L H 0.624 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Arsenic, Dissolved, ICP-MS 0.775 ug/L H 0.775 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/18/2012 L55936-2 Arsenic, Dissolved, ICP-MS 1.47 ug/L H 1.47 J unknown 0.1 0.5WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Arsenic, Dissolved, ICP-MS 1.19 ug/L H 1.19 J unknown 0.1 0.5WG121990 A01007 Storm 6/4/2012 L55764-1 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDREG Storm 6/4/2012 L55764-2 Cadmium, Dissolved, ICP-MS 0.059 ug/L <RDL,H 0.059 J unknown 0.05 0.25WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Cadmium, Dissolved, ICP-MS 0.051 ug/L <RDL,H 0.051 J unknown 0.05 0.25WG121990 BRANDREG Storm 6/5/2012 L55859-2 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDREG Storm 6/6/2012 L55875-2 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDREG Storm 6/18/2012 L55936-2 Cadmium, Dissolved, ICP-MS ug/L <MDL,H 0.05 UJ unknown 0.05 0.25WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Cadmium, Dissolved, ICP-MS 0.074 ug/L <RDL,H 0.074 J unknown 0.05 0.25WG121990 A01007 Storm 6/4/2012 L55764-1 Chromium, Dissolved, ICP-MS 0.84 ug/L <RDL,H 0.84 J unknown 0.2 1WG121990 BRANDREG Storm 6/4/2012 L55764-2 Chromium, Dissolved, ICP-MS 1.17 ug/L H 1.17 J unknown 0.2 1WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Chromium, Dissolved, ICP-MS 0.53 ug/L <RDL,H 0.53 J unknown 0.2 1





DV Value

DV Flag

Bias MDL RDL

WG121990 BRANDREG Storm 6/5/2012 L55859-2 Chromium, Dissolved, ICP-MS 0.93 ug/L <RDL,H 0.93 J unknown 0.2 1WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Chromium, Dissolved, ICP-MS 0.63 ug/L <RDL,H 0.63 J unknown 0.2 1WG121990 BRANDREG Storm 6/6/2012 L55875-2 Chromium, Dissolved, ICP-MS 0.77 ug/L <RDL,H 0.77 J unknown 0.2 1WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Chromium, Dissolved, ICP-MS 0.42 ug/L <RDL,H 0.42 J unknown 0.2 1WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Chromium, Dissolved, ICP-MS 0.67 ug/L <RDL,H 0.67 J unknown 0.2 1WG121990 BRANDREG Storm 6/18/2012 L55936-2 Chromium, Dissolved, ICP-MS 1.32 ug/L H 1.32 J unknown 0.2 1WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Chromium, Dissolved, ICP-MS 1.63 ug/L H 1.63 J unknown 0.2 1WG121990 A01007 Storm 6/4/2012 L55764-1 Copper, Dissolved, ICP-MS 8.61 ug/L H 8.61 J unknown 0.4 2WG121990 BRANDREG Storm 6/4/2012 L55764-2 Copper, Dissolved, ICP-MS 13.9 ug/L H 13.9 J unknown 0.4 2WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Copper, Dissolved, ICP-MS 10.1 ug/L H 10.1 J unknown 0.4 2WG121990 BRANDREG Storm 6/5/2012 L55859-2 Copper, Dissolved, ICP-MS 9.08 ug/L H 9.08 J unknown 0.4 2WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Copper, Dissolved, ICP-MS 8.17 ug/L H 8.17 J unknown 0.4 2WG121990 BRANDREG Storm 6/6/2012 L55875-2 Copper, Dissolved, ICP-MS 8.85 ug/L H 8.85 J unknown 0.4 2WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Copper, Dissolved, ICP-MS 7.76 ug/L H 7.76 J unknown 0.4 2WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Copper, Dissolved, ICP-MS 8.08 ug/L H 8.08 J unknown 0.4 2WG121990 BRANDREG Storm 6/18/2012 L55936-2 Copper, Dissolved, ICP-MS 19.4 ug/L H 19.4 J unknown 0.4 2WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Copper, Dissolved, ICP-MS 18.7 ug/L H 18.7 J unknown 0.4 2WG121990 A01007 Storm 6/4/2012 L55764-1 Lead, Dissolved, ICP-MS 1.23 ug/L H 1.23 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/4/2012 L55764-2 Lead, Dissolved, ICP-MS 1.21 ug/L H 1.21 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Lead, Dissolved, ICP-MS 1.34 ug/L H 1.34 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/5/2012 L55859-2 Lead, Dissolved, ICP-MS 1.16 ug/L H 1.16 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Lead, Dissolved, ICP-MS 0.613 ug/L H 0.613 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/6/2012 L55875-2 Lead, Dissolved, ICP-MS 0.614 ug/L H 0.614 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Lead, Dissolved, ICP-MS 0.513 ug/L H 0.513 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Lead, Dissolved, ICP-MS 0.42 ug/L <RDL,H 0.42 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/18/2012 L55936-2 Lead, Dissolved, ICP-MS 1.17 ug/L H 1.17 J unknown 0.1 0.5WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Lead, Dissolved, ICP-MS 0.776 ug/L H 0.776 J unknown 0.1 0.5WG121990 A01007 Storm 6/4/2012 L55764-1 Nickel, Dissolved, ICP-MS 3.36 ug/L H 3.36 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/4/2012 L55764-2 Nickel, Dissolved, ICP-MS 14.6 ug/L H 14.6 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Nickel, Dissolved, ICP-MS 2.72 ug/L H 2.72 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/5/2012 L55859-2 Nickel, Dissolved, ICP-MS 13.3 ug/L H 13.3 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Nickel, Dissolved, ICP-MS 2.11 ug/L H 2.11 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/6/2012 L55875-2 Nickel, Dissolved, ICP-MS 14.1 ug/L H 14.1 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Nickel, Dissolved, ICP-MS 1.45 ug/L H 1.45 J unknown 0.1 0.5WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Nickel, Dissolved, ICP-MS 1.25 ug/L H 1.25 J unknown 0.1 0.5WG121990 BRANDREG Storm 6/18/2012 L55936-2 Nickel, Dissolved, ICP-MS 43.1 ug/L H 43.1 J unknown 0.1 0.5WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Nickel, Dissolved, ICP-MS 29.5 ug/L H 29.5 J unknown 0.1 0.5WG121990 A01007 Storm 6/4/2012 L55764-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2





DV Value

DV Flag

Bias MDL RDL

WG121990 BRANDREG Storm 6/4/2012 L55764-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Silver, Dissolved, ICP-MS 0.055 ug/L <RDL,H 0.055 J unknown 0.04 0.2WG121990 BRANDREG Storm 6/5/2012 L55859-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDREG Storm 6/6/2012 L55875-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDREG Storm 6/18/2012 L55936-2 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Silver, Dissolved, ICP-MS ug/L <MDL,H 0.04 UJ unknown 0.04 0.2WG121990 A01007 Storm 6/4/2012 L55764-1 Vanadium, Dissolved, ICP-MS 1.24 ug/L H 1.24 J unknown 0.075 0.375WG121990 BRANDREG Storm 6/4/2012 L55764-2 Vanadium, Dissolved, ICP-MS 1.29 ug/L H 1.29 J unknown 0.075 0.375WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Vanadium, Dissolved, ICP-MS 1.35 ug/L H 1.35 J unknown 0.075 0.375WG121990 BRANDREG Storm 6/5/2012 L55859-2 Vanadium, Dissolved, ICP-MS 1.29 ug/L H 1.29 J unknown 0.075 0.375WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Vanadium, Dissolved, ICP-MS 1.53 ug/L H 1.53 J unknown 0.075 0.375WG121990 BRANDREG Storm 6/6/2012 L55875-2 Vanadium, Dissolved, ICP-MS 1.13 ug/L H 1.13 J unknown 0.075 0.375WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Vanadium, Dissolved, ICP-MS 1.25 ug/L H 1.25 J unknown 0.075 0.375WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Vanadium, Dissolved, ICP-MS 1.43 ug/L H 1.43 J unknown 0.075 0.375WG121990 BRANDREG Storm 6/18/2012 L55936-2 Vanadium, Dissolved, ICP-MS 1.11 ug/L H 1.11 J unknown 0.075 0.375WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Vanadium, Dissolved, ICP-MS 0.886 ug/L H 0.886 J unknown 0.075 0.375WG121990 A01007 Storm 6/4/2012 L55764-1 Zinc, Dissolved, ICP-MS 164 ug/L H 164 J unknown 0.5 2.5WG121990 BRANDREG Storm 6/4/2012 L55764-2 Zinc, Dissolved, ICP-MS 58.7 ug/L H 58.7 J unknown 0.5 2.5WG121990 BRANDUTAHStorm 6/4/2012 L55764-3 Zinc, Dissolved, ICP-MS 38.9 ug/L H 38.9 J unknown 0.5 2.5WG121990 BRANDREG Storm 6/5/2012 L55859-2 Zinc, Dissolved, ICP-MS 40.2 ug/L H 40.2 J unknown 0.5 2.5WG121990 BRANDUTAHStorm 6/5/2012 L55859-3 Zinc, Dissolved, ICP-MS 67.3 ug/L H 67.3 J unknown 0.5 2.5WG121990 BRANDREG Storm 6/6/2012 L55875-2 Zinc, Dissolved, ICP-MS 51.4 ug/L H 51.4 J unknown 0.5 2.5WG121990 BRANDUTAHStorm 6/6/2012 L55875-3 Zinc, Dissolved, ICP-MS 37.5 ug/L H 37.5 J unknown 0.5 2.5WG121990 BRANDUTAHStorm 6/7/2012 L55876-3 Zinc, Dissolved, ICP-MS 23.4 ug/L H 23.4 J unknown 0.5 2.5WG121990 BRANDREG Storm 6/18/2012 L55936-2 Zinc, Dissolved, ICP-MS 54.3 ug/L H 54.3 J unknown 0.5 2.5WG121990 BRANDREG Wet Base 6/20/2012 L55698-1 Zinc, Dissolved, ICP-MS 60 ug/L H 60 J unknown 0.5 2.5WG119537 BRANDUTAHStorm 1/25/2012 L54687-3 2-Methylnaphthalene 0.0358 ug/L B 0.0358 U 0.008 0.016WG119537 A01007 Storm 1/25/2012 L54687-1 Bis(2-Ethylhexyl)Phthalate 5.5 ug/L J 5.5 J unknown 0.032 0.064WG119537 BRANDREG Storm 1/25/2012 L54687-2 Bis(2-Ethylhexyl)Phthalate 4 ug/L 4 J unknown 0.008 0.016WG119537 BRANDUTAHStorm 1/25/2012 L54687-3 Bis(2-Ethylhexyl)Phthalate 7.53 ug/L 7.53 J unknown 0.016 0.032WG119537 A01007 Storm 1/25/2012 L54687-1 Di-N-Butyl Phthalate 0.705 ug/L B 0.705 U 0.008 0.2WG119537 BRANDREG Storm 1/25/2012 L54687-2 Di-N-Butyl Phthalate 0.731 ug/L B 0.731 U 0.008 0.2WG119848 BRANDUTAHWet Base 2/15/2012 L55012-3 Benzyl Butyl Phthalate 3.9 ug/L J 3.9 J unknown 0.016 0.032WG119848 A01007 Wet Base 2/15/2012 L55012-1 Bis(2-Ethylhexyl)Phthalate 4.39 ug/L JL 4.39 J high 0.016 0.032WG119848 BRANDUTAHWet Base 2/15/2012 L55012-3 Bis(2-Ethylhexyl)Phthalate 3.06 ug/L B2,JL 3.06 J high 0.016 0.032





DV Value

DV Flag

Bias MDL RDL

WG119848 A01007 Wet Base 2/15/2012 L55012-1 Di-N-Butyl Phthalate 0.528 ug/L B 0.528 U 0.008 0.2WG119848 BRANDUTAHWet Base 2/15/2012 L55012-3 Di-N-Butyl Phthalate 0.475 ug/L B 0.475 U 0.008 0.2WG119973 A01007 Storm 2/28/2012 L55011-1 Bis(2-Ethylhexyl)Phthalate 4.23 ug/L B2 4.23 J high 0.008 0.016WG119973 BRANDREG Storm 2/28/2012 L55011-2 Bis(2-Ethylhexyl)Phthalate 4.78 ug/L B2 4.78 J high 0.04 0.08WG119973 BRANDUTAHStorm 2/28/2012 L55011-3 Bis(2-Ethylhexyl)Phthalate 3.72 ug/L B2 3.72 J high 0.008 0.016WG119973 A01007 Storm 2/29/2012 L55186-1 Bis(2-Ethylhexyl)Phthalate 6.25 ug/L B2 6.25 J high 0.016 0.032WG119973 BRANDREG Storm 2/29/2012 L55186-2 Bis(2-Ethylhexyl)Phthalate 1.45 ug/L B 1.45 U 0.008 0.016WG119973 BRANDUTAHStorm 2/29/2012 L55186-3 Bis(2-Ethylhexyl)Phthalate 3.7 ug/L B2 3.7 J high 0.008 0.016WG119973 A01007 Storm 2/28/2012 L55011-1 Di-N-Butyl Phthalate 0.634 ug/L B 0.634 U 0.008 0.2WG119973 BRANDREG Storm 2/28/2012 L55011-2 Di-N-Butyl Phthalate 0.382 ug/L B 0.382 U 0.008 0.2WG119973 A01007 Storm 2/29/2012 L55186-1 Di-N-Butyl Phthalate 0.638 ug/L B 0.638 U 0.008 0.2WG119973 BRANDREG Storm 2/29/2012 L55186-2 Di-N-Butyl Phthalate 0.655 ug/L B 0.655 U 0.008 0.2WG119973 BRANDUTAHStorm 2/29/2012 L55186-3 Fluoranthene 0.16 ug/L J 0.16 J unknown 0.008 0.016WG120438 A01007 Storm 3/27/2012 L55185-1 Bis(2-Ethylhexyl)Phthalate 4.65 ug/L B2,J 4.65 J unknown 0.04 0.08WG120438 BRANDREG Storm 3/27/2012 L55185-2 Bis(2-Ethylhexyl)Phthalate 4.51 ug/L B2,J 4.51 J unknown 0.04 0.08WG120438 BRANDUTAHStorm 3/27/2012 L55185-3 Bis(2-Ethylhexyl)Phthalate 6.14 ug/L J 6.14 J unknown 0.08 0.16WG120438 BRANDREG Storm 3/28/2012 L55285-2 Bis(2-Ethylhexyl)Phthalate 5.93 ug/L J 5.93 J unknown 0.04 0.08WG120438 BRANDUTAHStorm 3/28/2012 L55285-3 Bis(2-Ethylhexyl)Phthalate 3.4 ug/L B2,J 3.4 J unknown 0.008 0.016WG120438 A01007 Wet Base 3/26/2012 L55154-1 Bis(2-Ethylhexyl)Phthalate 8.58 ug/L J 8.58 J unknown 0.08 0.16WG120438 BRANDREG Wet Base 3/26/2012 L55154-2 Bis(2-Ethylhexyl)Phthalate 3.08 ug/L B2,J 3.08 J unknown 0.08 0.16WG120438 BRANDUTAHWet Base 3/26/2012 L55154-3 Bis(2-Ethylhexyl)Phthalate 6.78 ug/L J 6.78 J unknown 0.08 0.16WG120438 BRANDREG Wet Base 3/26/2012 L55154-2 Dimethyl Phthalate 0.082 ug/L <RDL,B3 0.16 U 0.08 0.16WG120438 BRANDUTAHWet Base 3/26/2012 L55154-3 Dimethyl Phthalate 0.11 ug/L <RDL,B3 0.16 U 0.08 0.16WG120438 A01007 Storm 3/27/2012 L55185-1 Di-N-Butyl Phthalate 0.95 ug/L <RDL,B2 1 U 0.04 1WG120438 BRANDUTAHStorm 3/27/2012 L55185-3 Di-N-Butyl Phthalate 1.4 ug/L <RDL 2 U 0.08 2WG120438 BRANDUTAHStorm 3/28/2012 L55285-3 Di-N-Butyl Phthalate 0.573 ug/L B 0.573 U 0.008 0.2WG120438 A01007 Wet Base 3/26/2012 L55154-1 Di-N-Butyl Phthalate 1.2 ug/L <RDL,B2 2 U 0.08 2WG120438 BRANDUTAHWet Base 3/26/2012 L55154-3 Di-N-Butyl Phthalate 1.2 ug/L <RDL 2 U 0.08 2WG120438 A01007 Wet Base 3/26/2012 L55154-1 Phenanthrene 0.12 ug/L <RDL 0.16 U 0.08 0.16WG120438 BRANDREG Wet Base 3/26/2012 L55154-2 Phenanthrene 0.13 ug/L <RDL 0.16 U 0.08 0.16WG120438 BRANDUTAHWet Base 3/26/2012 L55154-3 Phenanthrene 0.12 ug/L <RDL 0.16 U 0.08 0.16WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Acenaphthylene 0.419 ug/L 0.419 J unknown 0.04 0.08WG120555 A01007 Wet Base 4/9/2012 L55183-1 Benzyl Butyl Phthalate 0.733 ug/L 0.733 J unknown 0.08 0.16WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Benzyl Butyl Phthalate 6.39 ug/L 6.39 J unknown 0.08 0.16WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Benzyl Butyl Phthalate 40.4 ug/L 40.4 J unknown 0.8 1.6WG120555 A01007 Wet Base 4/9/2012 L55183-1 Bis(2-Ethylhexyl)Phthalate 6.79 ug/L B2,JL 6.79 J unknown 0.08 0.16WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Bis(2-Ethylhexyl)Phthalate 4.86 ug/L B2,JL 4.86 J unknown 0.08 0.16WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Bis(2-Ethylhexyl)Phthalate 13.9 ug/L JL 13.9 J unknown 0.04 0.08





DV Value

DV Flag

Bias MDL RDL

WG120555 A01007 Wet Base 4/9/2012 L55183-1 Diethyl Phthalate 1.47 ug/L 1.47 J unknown 0.08 0.4WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Diethyl Phthalate 2.22 ug/L 2.22 J unknown 0.08 0.4WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Diethyl Phthalate 6.54 ug/L 6.54 J unknown 0.04 0.2WG120555 A01007 Wet Base 4/9/2012 L55183-1 Dimethyl Phthalate 0.397 ug/L 0.397 J unknown 0.08 0.16WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Dimethyl Phthalate 0.175 ug/L 0.175 J unknown 0.08 0.16WG120555 A01007 Wet Base 4/9/2012 L55183-1 Di-N-Butyl Phthalate 1.3 ug/L <RDL,B2 2 UJ unknown 0.08 2WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Di-N-Butyl Phthalate 0.78 ug/L <RDL,B 2 UJ unknown 0.08 2WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Di-N-Butyl Phthalate 1.29 ug/L B2 1.29 J unknown 0.04 1WG120555 A01007 Wet Base 4/9/2012 L55183-1 Di-N-Octyl Phthalate 0.262 ug/L 0.262 J unknown 0.08 0.16WG120555 BRANDREG Wet Base 4/9/2012 L55183-2 Di-N-Octyl Phthalate 0.73 ug/L 0.73 J unknown 0.08 0.16WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Di-N-Octyl Phthalate 0.217 ug/L 0.217 J unknown 0.04 0.08WG120555 BRANDUTAHWet Base 4/9/2012 L55183-3 Phenanthrene 0.0911 ug/L 0.0911 J unknown 0.04 0.08WG120654 A01007 Storm 4/11/2012 L55433-1 Bis(2-Ethylhexyl)Phthalate 7.49 ug/L B,J 7.49 J unknown 0.04 0.08WG120654 BRANDREG Storm 4/11/2012 L55433-2 Bis(2-Ethylhexyl)Phthalate 5.39 ug/L B,J 5.39 J unknown 0.04 0.08WG120654 BRANDUTAHStorm 4/11/2012 L55433-3 Bis(2-Ethylhexyl)Phthalate 7.32 ug/L B,J 7.32 J unknown 0.04 0.08WG120654 BRANDREG Wet Base 4/10/2012 L55184-2 Bis(2-Ethylhexyl)Phthalate 5.43 ug/L B,J 5.43 J unknown 0.04 0.08WG120654 BRANDUTAHWet Base 4/10/2012 L55184-3 Bis(2-Ethylhexyl)Phthalate 10.2 ug/L B,J 10.2 J unknown 0.04 0.08WG120654 A01007 Storm 4/11/2012 L55433-1 Di-N-Butyl Phthalate 0.66 ug/L <RDL,B2 1 U 0.04 1WG120654 BRANDREG Storm 4/11/2012 L55433-2 Di-N-Butyl Phthalate 0.63 ug/L <RDL,B2 1 U 0.04 1WG120654 BRANDUTAHStorm 4/11/2012 L55433-3 Di-N-Butyl Phthalate 0.51 ug/L <RDL,B 1 U 0.04 1WG120654 BRANDREG Wet Base 4/10/2012 L55184-2 Di-N-Butyl Phthalate 0.4 ug/L <RDL,B 1 U 0.04 1WG120654 BRANDUTAHWet Base 4/10/2012 L55184-3 Di-N-Butyl Phthalate 0.75 ug/L <RDL,B2 1 U 0.04 1WG120867 A01007 Storm 4/24/2012 L55512-1 Bis(2-Ethylhexyl)Phthalate 5.8 ug/L J 5.8 J unknown 0.038 0.0755WG120867 BRANDREG Storm 4/24/2012 L55512-2 Bis(2-Ethylhexyl)Phthalate 7.76 ug/L J 7.76 J unknown 0.038 0.0755WG120867 BRANDUTAHStorm 4/24/2012 L55512-3 Bis(2-Ethylhexyl)Phthalate 5.33 ug/L J 5.33 J unknown 0.038 0.0755WG120867 A01007 Storm 4/25/2012 L55584-1 Bis(2-Ethylhexyl)Phthalate 2.71 ug/L B2,J 2.71 J unknown 0.038 0.0755WG120867 BRANDREG Storm 4/25/2012 L55584-2 Bis(2-Ethylhexyl)Phthalate 2.06 ug/L B2,J 2.06 J unknown 0.038 0.0755WG120867 BRANDUTAHStorm 4/25/2012 L55584-3 Bis(2-Ethylhexyl)Phthalate 4.17 ug/L J 4.17 J unknown 0.038 0.0755WG120867 A01007 Wet Base 4/23/2012 L55511-1 Bis(2-Ethylhexyl)Phthalate 2.58 ug/L B2,J 2.58 J unknown 0.038 0.0755WG120867 BRANDREG Wet Base 4/23/2012 L55511-2 Bis(2-Ethylhexyl)Phthalate 11.1 ug/L J 11.1 J unknown 0.038 0.0755WG120867 BRANDUTAHWet Base 4/23/2012 L55511-3 Bis(2-Ethylhexyl)Phthalate 9.18 ug/L J 9.18 J unknown 0.038 0.0755WG120867 BRANDREG Storm 4/24/2012 L55512-2 Di-N-Butyl Phthalate 0.31 ug/L <RDL 0.943 U 0.038 0.943WG120867 BRANDUTAHStorm 4/24/2012 L55512-3 Di-N-Butyl Phthalate 0.4 ug/L <RDL 0.943 U 0.038 0.943WG120867 A01007 Storm 4/25/2012 L55584-1 Di-N-Butyl Phthalate 0.32 ug/L <RDL 0.943 U 0.038 0.943WG120867 BRANDREG Storm 4/25/2012 L55584-2 Di-N-Butyl Phthalate 0.38 ug/L <RDL 0.943 U 0.038 0.943WG120867 BRANDUTAHStorm 4/25/2012 L55584-3 Di-N-Butyl Phthalate 0.41 ug/L <RDL 0.943 U 0.038 0.943WG120867 A01007 Wet Base 4/23/2012 L55511-1 Di-N-Butyl Phthalate 0.35 ug/L <RDL 0.943 U 0.038 0.943WG120867 BRANDREG Wet Base 4/23/2012 L55511-2 Di-N-Butyl Phthalate 0.38 ug/L <RDL 0.943 U 0.038 0.943





DV Value

DV Flag

Bias MDL RDL

WG121052 BRANDUTAHWet Base 5/7/2012 L55572-3 Acenaphthylene 0.326 ug/L J 0.326 J unknown 0.04 0.08WG121052 A01007 Wet Base 5/7/2012 L55572-1 Bis(2-Ethylhexyl)Phthalate 7.51 ug/L B,J 7.51 J unknown 0.04 0.08WG121052 BRANDUTAHWet Base 5/7/2012 L55572-3 Bis(2-Ethylhexyl)Phthalate 21.9 ug/L B,J 21.9 J unknown 0.16 0.32WG121052 A01007 Wet Base 5/8/2012 L55686-1 Bis(2-Ethylhexyl)Phthalate 7.62 ug/L B,J 7.62 J unknown 0.04 0.08WG121052 BRANDREG Wet Base 5/8/2012 L55686-2 Bis(2-Ethylhexyl)Phthalate 7.24 ug/L B,J 7.24 J unknown 0.04 0.08WG121052 BRANDUTAHWet Base 5/8/2012 L55686-3 Bis(2-Ethylhexyl)Phthalate 33.9 ug/L B,J 33.9 J unknown 0.4 0.8WG121052 BRANDUTAHWet Base 5/7/2012 L55572-3 Dimethyl Phthalate 0.077 ug/L <RDL,B 0.08 U 0.04 0.08WG121052 BRANDREG Wet Base 5/8/2012 L55686-2 Dimethyl Phthalate 0.124 ug/L B 0.124 U 0.04 0.08WG121052 A01007 Wet Base 5/7/2012 L55572-1 Di-N-Butyl Phthalate 0.58 ug/L <RDL,B 1 U 0.04 1WG121052 BRANDUTAHWet Base 5/7/2012 L55572-3 Di-N-Butyl Phthalate 0.49 ug/L <RDL,B 1 U 0.04 1WG121052 A01007 Wet Base 5/8/2012 L55686-1 Di-N-Butyl Phthalate 0.78 ug/L <RDL,B 1 U 0.04 1WG121052 BRANDREG Wet Base 5/8/2012 L55686-2 Di-N-Butyl Phthalate 0.7 ug/L <RDL,B 1 U 0.04 1WG121052 BRANDUTAHWet Base 5/8/2012 L55686-3 Di-N-Butyl Phthalate 1 ug/L <RDL,B2 1 U 0.04 1WG121052 A01007 Wet Base 5/7/2012 L55572-1 Phenanthrene 0.065 ug/L <RDL,B3 0.08 U 0.04 0.08WG121052 BRANDUTAHWet Base 5/7/2012 L55572-3 Phenanthrene 0.051 ug/L <RDL,B 0.08 U 0.04 0.08WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 2-Methylnaphthalene 0.079 ug/L <RDL,B3 0.08 U 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 2-Methylnaphthalene 0.55 ug/L <RDL,JG 0.64 UJ low 0.32 0.64WG121217 BRANDREG Storm 5/22/2012 L55763-2 2-Methylnaphthalene ug/L <MDL,JG 0.32 UJ low 0.32 0.64WG121217 A01007 Storm 5/22/2012 L55763-1 Acenaphthene ug/L <MDL,JG 0.04 UJ low 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Acenaphthene ug/L <MDL,JG 0.04 UJ low 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Acenaphthylene ug/L <MDL,JG 0.04 UJ low 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Acenaphthylene ug/L <MDL,JG 0.04 UJ low 0.04 0.08WG121217 A01007 Storm 5/21/2012 L55638-1 Benzo(a)pyrene 0.041 ug/L <RDL,J 0.041 J unknown 0.04 0.08WG121217 BRANDREG Storm 5/21/2012 L55638-2 Benzo(a)pyrene 0.064 ug/L <RDL,J 0.064 J unknown 0.04 0.08WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Benzo(a)pyrene ug/L <MDL,J 0.04 UJ unknown 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Benzo(a)pyrene ug/L <MDL,J 0.04 UJ unknown 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Benzo(a)pyrene ug/L <MDL,J 0.04 UJ unknown 0.04 0.08WG121217 BRANDUTAHStorm 5/22/2012 L55763-3 Benzo(a)pyrene 0.077 ug/L <RDL,J 0.077 J unknown 0.04 0.08WG121217 A01007 Storm 5/21/2012 L55638-1 Benzyl Butyl Phthalate 0.503 ug/L B2,JL 0.503 J high 0.04 0.08WG121217 BRANDREG Storm 5/21/2012 L55638-2 Benzyl Butyl Phthalate 1.13 ug/L JL 1.13 J high 0.04 0.08WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Benzyl Butyl Phthalate 1.72 ug/L JL 1.72 J high 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Benzyl Butyl Phthalate 1.31 ug/L JL 1.31 J high 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Benzyl Butyl Phthalate 1.56 ug/L JL 1.56 J high 0.04 0.08WG121217 BRANDUTAHStorm 5/22/2012 L55763-3 Benzyl Butyl Phthalate 2.75 ug/L JL 2.75 J high 0.04 0.08WG121217 A01007 Storm 5/21/2012 L55638-1 Bis(2-Ethylhexyl)Phthalate 7.65 ug/L J 7.65 J unknown 0.04 0.08WG121217 BRANDREG Storm 5/21/2012 L55638-2 Bis(2-Ethylhexyl)Phthalate 7.91 ug/L J 7.91 J unknown 0.04 0.08WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Bis(2-Ethylhexyl)Phthalate 6.09 ug/L J 6.09 J unknown 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Bis(2-Ethylhexyl)Phthalate 11.9 ug/L J 11.9 J unknown 0.04 0.08





DV Value

DV Flag

Bias MDL RDL

WG121217 BRANDREG Storm 5/22/2012 L55763-2 Bis(2-Ethylhexyl)Phthalate 7.03 ug/L J 7.03 J unknown 0.04 0.08WG121217 BRANDUTAHStorm 5/22/2012 L55763-3 Bis(2-Ethylhexyl)Phthalate 5.01 ug/L B2,J 5.01 J unknown 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Diethyl Phthalate 2.27 ug/L JG 2.27 J low 0.04 0.2WG121217 BRANDREG Storm 5/22/2012 L55763-2 Diethyl Phthalate 1.36 ug/L JG 1.36 J low 0.04 0.2WG121217 BRANDREG Storm 5/21/2012 L55638-2 Dimethyl Phthalate 0.15 ug/L <RDL 0.16 U 0.08 0.16WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Dimethyl Phthalate 0.13 ug/L <RDL,B3 0.16 U 0.08 0.16WG121217 A01007 Storm 5/22/2012 L55763-1 Dimethyl Phthalate 0.504 ug/L JG 0.504 J low 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Dimethyl Phthalate 0.23 ug/L JG 0.23 J low 0.04 0.08WG121217 A01007 Storm 5/21/2012 L55638-1 Di-N-Butyl Phthalate 0.61 ug/L <RDL,B 1 U 0.04 1WG121217 BRANDREG Storm 5/21/2012 L55638-2 Di-N-Butyl Phthalate 0.74 ug/L <RDL,B2 1 U 0.04 1WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Di-N-Butyl Phthalate 0.54 ug/L <RDL,B 1 U 0.04 1WG121217 BRANDUTAHStorm 5/22/2012 L55763-3 Di-N-Butyl Phthalate 0.53 ug/L <RDL,B 1 U 0.04 1WG121217 A01007 Storm 5/21/2012 L55638-1 Di-N-Octyl Phthalate 10.2 ug/L JL 10.2 J high 0.04 0.08WG121217 BRANDREG Storm 5/21/2012 L55638-2 Di-N-Octyl Phthalate 4.29 ug/L JL 4.29 J high 0.04 0.08WG121217 BRANDUTAHStorm 5/21/2012 L55638-3 Di-N-Octyl Phthalate 1.02 ug/L JL 1.02 J high 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Di-N-Octyl Phthalate 12.5 ug/L JL 12.5 J high 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Di-N-Octyl Phthalate 6.06 ug/L JL 6.06 J high 0.04 0.08WG121217 BRANDUTAHStorm 5/22/2012 L55763-3 Di-N-Octyl Phthalate 1.85 ug/L JL 1.85 J high 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Fluorene 0.175 ug/L JG 0.175 J low 0.04 0.08WG121217 BRANDREG Storm 5/22/2012 L55763-2 Fluorene 0.0851 ug/L JG 0.0851 J low 0.04 0.08WG121217 A01007 Storm 5/22/2012 L55763-1 Naphthalene 2.11 ug/L JG 2.11 J low 0.8 1.6WG121217 BRANDREG Storm 5/22/2012 L55763-2 Naphthalene 1.3 ug/L <RDL,JG 1.3 J low 0.8 1.6WG121458 A01007 Storm 6/4/2012 L55764-1 Bis(2-Ethylhexyl)Phthalate 16.8 ug/L B2,J 16.8 J unknown 0.08 0.16WG121458 BRANDREG Storm 6/4/2012 L55764-2 Bis(2-Ethylhexyl)Phthalate 8.32 ug/L B,J 8.32 UJ unknown 0.04 0.08WG121458 BRANDUTAHStorm 6/4/2012 L55764-3 Bis(2-Ethylhexyl)Phthalate 12.1 ug/L B2,J 12.1 J unknown 0.04 0.08WG121458 BRANDREG Storm 6/5/2012 L55859-2 Bis(2-Ethylhexyl)Phthalate 9.56 ug/L B,J 9.56 UJ unknown 0.04 0.08WG121458 BRANDUTAHStorm 6/5/2012 L55859-3 Bis(2-Ethylhexyl)Phthalate 5.88 ug/L B,J 5.88 UJ unknown 0.04 0.08WG121458 BRANDREG Storm 6/6/2012 L55875-2 Bis(2-Ethylhexyl)Phthalate 5.39 ug/L B,J 5.39 UJ unknown 0.04 0.08WG121458 BRANDUTAHStorm 6/6/2012 L55875-3 Bis(2-Ethylhexyl)Phthalate 3.66 ug/L B,J 3.66 UJ unknown 0.04 0.08WG121458 A01007 Storm 6/7/2012 L55876-1 Bis(2-Ethylhexyl)Phthalate 6.08 ug/L B,J 6.08 UJ unknown 0.04 0.08WG121458 BRANDREG Storm 6/7/2012 L55876-2 Bis(2-Ethylhexyl)Phthalate 8.57 ug/L B,J 8.57 UJ unknown 0.04 0.08WG121458 BRANDUTAHStorm 6/7/2012 L55876-3 Bis(2-Ethylhexyl)Phthalate 6.09 ug/L B,J 6.09 UJ unknown 0.04 0.08WG121458 BRANDREG Storm 6/4/2012 L55764-2 Dimethyl Phthalate 0.31 ug/L J 0.31 J unknown 0.04 0.08WG121458 A01007 Storm 6/4/2012 L55764-1 Phenanthrene 0.096 ug/L <RDL,B3 0.16 U 0.08 0.16WG121670 BRANDREG Storm 6/18/2012 L55936-2 Benzo(g,h,i)perylene 0.139 ug/L B 0.139 U 0.04 0.08WG121670 BRANDREG Storm 6/18/2012 L55936-2 Benzyl Butyl Phthalate 5.12 ug/L 5.12 J unknown 0.04 0.08WG121670 BRANDREG Storm 6/18/2012 L55936-2 Bis(2-Ethylhexyl)Phthalate 11.8 ug/L B2,J 11.8 J low 0.04 0.08WG121670 BRANDREG Storm 6/18/2012 L55936-2 Indeno(1,2,3-Cd)Pyrene 0.0875 ug/L B 0.0875 U 0.04 0.08





DV Value

DV Flag

Bias MDL RDL

WG121757 BRANDREG Wet Base 6/20/2012 L55698-1 Bis(2-Ethylhexyl)Phthalate 8.25 ug/L B2,J 8.25 J unknown 0.04 0.08WG121757 BRANDREG Wet Base 6/20/2012 L55698-1 Di-N-Butyl Phthalate 1.63 ug/L B 1.63 U 0.04 1

1

ATTACHMENT A

LIMS BATCH AND QC REPORTS

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WG119517 (TSS) Department: 3 - Conventionals Move Date: 02-FEB-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54687-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 1/25/2012 1/27/2012 1/30/2012L54687-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 1/25/2012 1/27/2012 1/30/2012L54687-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 1/25/2012 1/27/2012 1/30/2012L54843-1 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-2 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-3 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-4 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-5 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-6 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-7 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-8 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-9 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-10 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-11 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-12 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-13 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-14 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-15 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-16 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-17 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-18 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-19 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-21 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-22 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-23 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-24 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-25 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-26 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-27 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-28 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-29 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-30 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-31 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-32 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54843-33 421250OS Ambient Offshore Water Column-South CVTSS SALT WTR 1/26/2012 1/27/2012 1/30/2012L54904-1 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-2 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-3 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012

LIMSView Batch Report for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Conventionals

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L54904-4 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-5 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-6 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 2/2/2012L54904-7 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-8 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-9 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-10 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54904-11 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 1/24/2012 1/27/2012 1/30/2012L54924-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 1/26/2012 1/27/2012 1/30/2012L54928-2 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 1/26/2012 1/27/2012 1/30/2012L54928-4 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 1/26/2012 1/27/2012 1/30/2012L54959-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 1/27/2012 1/27/2012 1/30/2012L54959-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 1/27/2012 1/27/2012 1/30/2012L54960-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 1/26/2012 1/27/2012 1/30/2012L54960-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 1/26/2012 1/27/2012 1/30/2012L54961-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 1/27/2012 1/27/2012 1/30/2012L54961-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 1/27/2012 1/27/2012 1/30/2012L54961-5 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 1/27/2012 1/27/2012 1/30/2012WG119517-1 MB CVTSS BLANK WTR 1/27/2012 1/30/2012 MB1 1/27/12WG119517-2 LCS CVTSS BLANK WTR 1/27/2012 1/30/2012 LEVEL1WG119517-3 LD CVTSS SALT WTR 1/27/2012 1/30/2012 L54843-2WG119517-4 MB CVTSS BLANK WTR 1/27/2012 1/30/2012 MB2 1/27/12WG119517-5 LCS CVTSS BLANK WTR 1/27/2012 1/30/2012 LEVEL1WG119517-6 LD CVTSS SALT WTR 1/27/2012 1/30/2012 L54843-23WG119517-7 LD CVTSS GRND WTR 1/27/2012 1/30/2012 L54924-5WG119517-8 MB CVTSS BLANK WTR 1/27/2012 1/30/2012 MB3 1/27/12WG119517-9 LCS CVTSS BLANK WTR 1/27/2012 1/30/2012 LEVEL1WG119517-10 LD CVTSS FRESH WTR 1/27/2012 1/30/2012 L54928-4WG119517-11 LD CVTSS STORM WTR 1/27/2012 1/30/2012 L54687-2WG119517-12 LD CVTSS STORM WTR 1/27/2012 1/30/2012 L54904-3

WG119562 (toc/doc) Department: 3 - Conventionals Move Date: 09-FEB-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54686-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-3 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-3 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012

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L54686-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-4 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-5 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-5 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-6 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54686-6 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 1/31/2012 2/2/2012 2/2/2012L54687-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 1/25/2012 1/27/2012 2/2/2012L54687-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 1/25/2012 2/1/2012 2/1/2012L54687-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 1/25/2012 1/27/2012 2/1/2012L54687-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 1/25/2012 2/1/2012 2/1/2012L54687-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 1/25/2012 1/27/2012 2/1/2012L54687-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 1/25/2012 2/1/2012 2/1/2012L54924-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/26/2012 2/1/2012 2/1/2012L54924-6 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/2/2012 2/2/2012 2/2/2012L54928-2 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/26/2012 2/1/2012 2/1/2012L54928-4 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/26/2012 2/1/2012 2/1/2012L54928-6 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/31/2012 2/1/2012 2/1/2012L54928-7 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/31/2012 2/2/2012 2/2/2012L54928-8 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/31/2012 2/2/2012 2/2/2012L54928-9 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/31/2012 2/2/2012 2/2/2012L54928-10 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 1/31/2012 2/2/2012 2/2/2012L54956-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/31/2012 2/1/2012 2/1/2012L54958-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/30/2012 2/1/2012 2/1/2012L54958-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/30/2012 2/1/2012 2/1/2012L54958-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 2/1/2012 2/2/2012 2/2/2012L54959-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/27/2012 2/1/2012 2/1/2012L54959-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/27/2012 2/1/2012 2/1/2012L54959-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/30/2012 2/1/2012 2/1/2012L54960-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 1/26/2012 2/1/2012 2/1/2012L54960-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 1/26/2012 2/1/2012 2/1/2012L54961-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 1/27/2012 2/1/2012 2/1/2012L54961-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 1/27/2012 2/1/2012 2/1/2012L54961-5 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 1/27/2012 2/1/2012 2/1/2012L54961-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 1/30/2012 2/1/2012 2/1/2012L54963-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/1/2012 2/2/2012 2/2/2012L54963-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/1/2012 2/2/2012 2/2/2012L55020-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/2/2012 2/2/2012 2/2/2012L55020-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/2/2012 2/2/2012 2/2/2012L55020-5 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 2/2/2012 2/2/2012 2/2/2012WG119562-1 MB CVTOC BLANK WTR 2/1/2012 2/1/2012 MB1 120131WG119562-2 LCS CVTOC BLANK WTR 2/1/2012 2/1/2012 LEVEL1

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WG119562-3 SB CVTOC BLANK WTR 2/1/2012 2/1/2012 WG119562-1WG119562-4 MS CVTOC GRND WTR 2/1/2012 2/1/2012 L54956-6WG119562-5 LD CVTOC FRESH WTR 2/1/2012 2/1/2012 L54928-4WG119562-6 MS CVTOC FRESH WTR 2/1/2012 2/1/2012 L54928-6WG119562-7 LD CVTOC STORM WTR 2/1/2012 2/1/2012 L54687-1WG119562-8 MS CVTOC STORM WTR 2/1/2012 2/1/2012 L54687-3WG119562-9 LD CVTOC GRND WTR 2/1/2012 2/1/2012 L54959-5WG119562-10 MB CVDOC BLANK WTR 1/27/2012 2/1/2012 MB1 120127WG119562-11 LCS CVDOC BLANK WTR 2/1/2012 2/1/2012 LEVEL1WG119562-12 SB CVDOC BLANK WTR 1/27/2012 2/1/2012 WG119562-10WG119562-13 MS CVDOC STORM WTR 1/27/2012 2/1/2012 L54687-3WG119562-14 LCS CVDOC BLANK WTR 2/2/2012 2/2/2012 LEVEL1WG119562-15 LD CVDOC STORM WTR 1/27/2012 2/2/2012 L54687-1WG119562-16 MB CVDOC BLANK WTR 2/2/2012 2/2/2012 MB1 120202WG119562-17 MB CVTOC BLANK WTR 2/2/2012 2/2/2012 MB1 120202WG119562-18 LCS CVTOC BLANK WTR 2/2/2012 2/2/2012 LEVEL1WG119562-19 MB CVDOC BLANK WTR 2/2/2012 2/2/2012 MB2 120202

WG119808 (TSS) Department: 3 - Conventionals Move Date: 01-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55012-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 2/15/2012 2/17/2012 2/17/2012L55012-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 2/15/2012 2/17/2012 2/17/2012L55035-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 2/16/2012 2/17/2012 2/17/2012L55037-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-2 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-3 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-4 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-5 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-6 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-7 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-8 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/14/2012 2/17/2012 2/17/2012L55037-9 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55037-11 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55037-12 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55037-13 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55044-2 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55044-3 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012L55044-4 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 2/16/2012 2/17/2012 2/17/2012WG119808-1 MB CVTSS BLANK WTR 2/17/2012 2/17/2012 MB1 2/17/12

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WG119808-2 LCS CVTSS BLANK WTR 2/17/2012 2/17/2012 LEVEL1WG119808-3 LD CVTSS SEWER WTR 2/17/2012 2/17/2012 L55012-3WG119808-4 LD CVTSS GRND WTR 2/17/2012 2/17/2012 L55035-5WG119808-5 LD CVTSS FRESH WTR 2/17/2012 2/17/2012 L55037-12

WG119910 (toc/doc) Department: 3 - Conventionals Move Date: 01-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54898-4 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L54953-1 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L54953-2 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L54953-3 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55012-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 2/15/2012 2/17/2012 2/23/2012L55012-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 2/15/2012 2/23/2012 2/23/2012L55012-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 2/15/2012 2/17/2012 2/22/2012L55012-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 2/15/2012 2/23/2012 2/23/2012L55020-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 2/17/2012 2/23/2012 2/23/2012L55035-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 2/16/2012 2/23/2012 2/23/2012L55037-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-2 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-3 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-4 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-5 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-6 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-7 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-8 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/14/2012 2/23/2012 2/23/2012L55037-9 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/16/2012 2/23/2012 2/23/2012L55037-11 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/16/2012 2/23/2012 2/23/2012L55037-12 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/16/2012 2/23/2012 2/23/2012L55037-13 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 2/16/2012 2/23/2012 2/23/2012L55057-1 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 2/17/2012 2/23/2012 2/23/2012L55057-3 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 2/17/2012 2/23/2012 2/23/2012L55062-5 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 2/23/2012 2/24/2012 2/24/2012L55088-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 2/21/2012 2/22/2012 2/22/2012L55088-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 2/21/2012 2/23/2012 2/23/2012L55088-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 2/21/2012 2/22/2012 2/22/2012L55088-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 2/21/2012 2/24/2012 2/24/2012L55088-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 2/21/2012 2/22/2012 2/22/2012L55088-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 2/21/2012 2/24/2012 2/24/2012L55089-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 2/21/2012 2/22/2012 2/22/2012

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L55089-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 2/21/2012 2/24/2012 2/24/2012L55089-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 2/21/2012 2/22/2012 2/23/2012L55089-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 2/21/2012 2/24/2012 2/24/2012L55089-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 2/21/2012 2/22/2012 2/23/2012L55089-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 2/21/2012 2/24/2012 2/24/2012L55115-1 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/13/2012 2/17/2012 2/22/2012L55115-2 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/17/2012 2/18/2012 2/22/2012L55115-2 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/17/2012 2/24/2012 2/24/2012L55115-4 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/17/2012 2/18/2012 2/22/2012L55115-4 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/17/2012 2/24/2012 2/24/2012L55115-7 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/17/2012 2/18/2012 2/22/2012L55115-7 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/17/2012 2/24/2012 2/24/2012L55115-8 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/13/2012 2/17/2012 2/22/2012L55115-9 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/14/2012 2/18/2012 2/22/2012L55115-9 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/14/2012 2/24/2012 2/24/2012WG119910-1 MB CVDOC BLANK WTR 2/17/2012 2/22/2012 MB2 120217WG119910-2 LCS CVDOC BLANK WTR 2/22/2012 2/22/2012 LEVEL1WG119910-3 MB CVDOC BLANK WTR 2/17/2012 2/22/2012 MB1 120217WG119910-4 SB CVDOC BLANK WTR 2/17/2012 2/22/2012 WG119910-3WG119910-5 MS CVDOC SEWER WTR 2/17/2012 2/22/2012 L55012-3WG119910-6 MB CVDOC BLANK WTR 2/18/2012 2/22/2012 MB1 120218WG119910-7 LD CVDOC STORM WTR 2/18/2012 2/22/2012 L55115-4WG119910-8 MS CVDOC STORM WTR 2/18/2012 2/22/2012 L55115-9WG119910-9 MB CVDOC BLANK WTR 2/22/2012 2/22/2012 MB1 120222WG119910-10 MS CVDOC FRESH WTR 2/22/2012 2/22/2012 L55088-3WG119910-11 LD CVDOC SALT WTR 2/22/2012 2/23/2012 L55089-1WG119910-12 MB CVTOC BLANK WTR 2/23/2012 2/23/2012 MB1 120222WG119910-13 LCS CVTOC BLANK WTR 2/23/2012 2/23/2012 LEVEL1WG119910-14 LD CVTOC SEWER WTR 2/23/2012 2/23/2012 L55012-1WG119910-15 MS CVTOC SEWER WTR 2/23/2012 2/23/2012 L55012-3WG119910-16 LD CVTOC FRESH WTR 2/23/2012 2/23/2012 L54953-3WG119910-17 MS CVTOC FRESH WTR 2/23/2012 2/23/2012 L55037-7WG119910-18 LD CVDOC SEWER WTR 2/17/2012 2/23/2012 L55012-1WG119910-19 MB CVTOC BLANK WTR 2/23/2012 2/23/2012 MB1 120223WG119910-20 LCS CVTOC BLANK WTR 2/23/2012 2/23/2012 LEVEL1WG119910-21 SB CVTOC BLANK WTR 2/23/2012 2/23/2012 WG119910-19WG119910-22 LD CVTOC FRESH WTR 2/23/2012 2/23/2012 L55037-4WG119910-23 MS CVTOC FRESH WTR 2/23/2012 2/23/2012 L55037-13WG119910-24 LD CVTOC GRND WTR 2/23/2012 2/23/2012 L55057-3WG119910-25 MS CVTOC GRND WTR 2/23/2012 2/23/2012 L55020-4WG119910-26 MS CVTOC FRESH WTR 2/24/2012 2/24/2012 L55088-3

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WG119910-27 LD CVTOC SALT WTR 2/24/2012 2/24/2012 L55089-3WG119910-28 LD CVTOC STORM WTR 2/24/2012 2/24/2012 L55115-4WG119910-29 MB CVTOC BLANK WTR 2/24/2012 2/24/2012 MB2 120223WG119910-30 LCS CVTOC BLANK WTR 2/24/2012 2/24/2012 LEVEL1WG119910-31 MS CVTOC STORM WTR 2/24/2012 2/24/2012 L55115-9WG119910-32 SB CVTOC BLANK WTR 2/23/2012 2/23/2012 WG119910-12


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54864-3 421422-CHGW-OS SWD-CHGW-OS Cedar Hills Groundwater Off-Site CVTOC GRND WTR 2/29/2012 3/1/2012 3/1/2012L55011-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/28/2012 2/29/2012 3/1/2012L55011-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/28/2012 3/1/2012 3/1/2012L55011-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/28/2012 2/29/2012 3/1/2012L55011-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/28/2012 3/1/2012 3/1/2012L55011-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/28/2012 2/29/2012 3/1/2012L55011-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/28/2012 3/1/2012 3/1/2012L55034-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55035-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55035-3 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55055-1 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 2/28/2012 2/28/2012 2/28/2012L55057-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 2/29/2012 3/1/2012 3/1/2012L55061-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55062-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 2/24/2012 2/28/2012 2/28/2012L55062-3 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55062-4 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 2/27/2012 2/28/2012 2/28/2012L55077-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 2/24/2012 2/25/2012 2/29/2012L55077-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 2/24/2012 2/28/2012 2/28/2012L55077-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 2/24/2012 2/25/2012 2/29/2012L55077-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 2/24/2012 2/28/2012 2/28/2012L55077-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 2/24/2012 2/25/2012 2/29/2012L55077-4 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 2/24/2012 2/29/2012 2/29/2012L55077-6 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 2/24/2012 2/25/2012 2/29/2012L55077-6 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 2/24/2012 2/29/2012 2/29/2012L55175-2 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/24/2012 2/25/2012 2/28/2012L55175-2 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/24/2012 2/29/2012 2/29/2012L55175-3 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/24/2012 2/25/2012 2/28/2012L55175-3 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/24/2012 2/29/2012 2/29/2012L55175-6 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 2/24/2012 2/25/2012 2/28/2012L55175-6 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 2/24/2012 2/29/2012 2/29/2012

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WG119964-1 MB CVTOC BLANK WTR 2/28/2012 2/28/2012 MB1 120228WG119964-2 LCS CVTOC BLANK WTR 2/28/2012 2/28/2012 LEVEL1WG119964-3 SB CVTOC BLANK WTR 2/28/2012 2/28/2012 WG119964-1WG119964-4 LD CVTOC STORM WTR 2/28/2012 2/28/2012 L55077-1WG119964-5 MS CVTOC STORM WTR 2/28/2012 2/28/2012 L55077-2WG119964-6 LD CVTOC GRND WTR 2/28/2012 2/28/2012 L55035-1WG119964-7 MS CVTOC GRND WTR 2/28/2012 2/28/2012 L55062-3WG119964-8 MB CVDOC BLANK WTR 2/25/2012 2/28/2012 MB1 120225WG119964-9 LCS CVDOC BLANK WTR 2/28/2012 2/28/2012 LEVEL1WG119964-10 SB CVDOC BLANK WTR 2/25/2012 2/28/2012 WG119964-8WG119964-11 MB CVDOC BLANK WTR 2/25/2012 2/28/2012 MB2 120225WG119964-12 LD CVDOC STORM WTR 2/25/2012 2/29/2012 L55077-1WG119964-13 MS CVDOC STORM WTR 2/25/2012 2/29/2012 L55077-2WG119964-14 MB CVTOC BLANK WTR 2/29/2012 2/29/2012 MB1 120229WG119964-15 LCS CVTOC BLANK WTR 2/29/2012 2/29/2012 LEVEL1WG119964-16 MB CVTOC BLANK WTR 3/1/2012 3/1/2012 MB1 120301WG119964-17 LCS CVTOC BLANK WTR 3/1/2012 3/1/2012 LEVEL1WG119964-18 MB CVDOC BLANK WTR 2/29/2012 3/1/2012 MB1 120229WG119964-19 LCS CVDOC BLANK WTR 3/1/2012 3/1/2012 LEVEL1

WG119972 (TSS) Department: 3 - Conventionals Move Date: 08-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55011-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/28/2012 3/5/2012 3/5/2012L55011-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/28/2012 3/5/2012 3/5/2012L55011-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/28/2012 3/5/2012 3/5/2012L55035-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTSS GRND WTR 3/1/2012 3/5/2012 3/5/2012L55065-5 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTSS GRND WTR 3/2/2012 3/5/2012 3/5/2012L55112-8 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55139-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 3/2/2012 3/5/2012 3/5/2012L55139-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTSS GRND WTR 3/2/2012 3/5/2012 3/5/2012L55170-3 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55171-3 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55173-3 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55186-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/29/2012 3/5/2012 3/5/2012L55186-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/29/2012 3/5/2012 3/5/2012L55186-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 2/29/2012 3/5/2012 3/5/2012L55187-3 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55188-9 421161 IW SURCHARGE CVTSS IW WTR 2/29/2012 3/5/2012 3/5/2012L55205-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 3/1/2012 3/5/2012 3/5/2012

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L55205-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 3/1/2012 3/5/2012 3/5/2012L55205-4 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 3/1/2012 3/5/2012 3/5/2012L55214-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTSS GRND WTR 3/2/2012 3/5/2012 3/5/2012WG119972-1 MB CVTSS BLANK WTR 3/5/2012 3/5/2012 MB1 3/5/12WG119972-2 LCS CVTSS BLANK WTR 3/5/2012 3/5/2012 LEVEL1WG119972-3 LD CVTSS GRND WTR 3/5/2012 3/5/2012 L55139-1WG119972-4 LD CVTSS STORM WTR 3/5/2012 3/5/2012 L55011-1WG119972-5 LD CVTSS IW WTR 3/5/2012 3/5/2012 L55112-8


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55035-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 3/1/2012 3/7/2012 3/7/2012L55065-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 3/5/2012 3/7/2012 3/7/2012L55065-3 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 3/5/2012 3/7/2012 3/7/2012L55065-4 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 3/6/2012 3/7/2012 3/7/2012L55065-5 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 3/2/2012 3/7/2012 3/7/2012L55139-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 3/2/2012 3/7/2012 3/7/2012L55139-2 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 3/2/2012 3/7/2012 3/7/2012L55177-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/5/2012 3/7/2012 3/12/2012L55177-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/5/2012 3/7/2012 3/7/2012L55177-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/5/2012 3/7/2012 3/12/2012L55177-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/5/2012 3/7/2012 3/7/2012L55177-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/5/2012 3/7/2012 3/12/2012L55177-4 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/5/2012 3/13/2012 3/13/2012L55177-5 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/5/2012 3/7/2012 3/12/2012L55177-5 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-6 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/5/2012 3/7/2012 3/12/2012L55177-6 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/5/2012 3/8/2012 3/8/2012L55186-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/29/2012 3/2/2012 3/12/2012L55186-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/29/2012 3/13/2012 3/13/2012L55186-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/29/2012 3/2/2012 3/12/2012L55186-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/29/2012 3/13/2012 3/13/2012L55186-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 2/29/2012 3/2/2012 3/12/2012L55186-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 2/29/2012 3/7/2012 3/7/2012L55198-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 3/6/2012 3/7/2012 3/7/2012L55198-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 3/6/2012 3/7/2012 3/7/2012L55198-5 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 3/6/2012 3/7/2012 3/7/2012L55205-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/1/2012 3/7/2012 3/7/2012L55205-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/1/2012 3/7/2012 3/7/2012

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L55205-4 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/1/2012 3/7/2012 3/7/2012L55210-1 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 3/6/2012 3/6/2012 3/12/2012L55210-1 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 3/6/2012 3/8/2012 3/8/2012L55210-2 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 3/6/2012 3/6/2012 3/12/2012L55210-2 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 3/6/2012 3/8/2012 3/8/2012L55210-3 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 3/6/2012 3/6/2012 3/13/2012L55210-3 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 3/6/2012 3/8/2012 3/8/2012L55210-4 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 3/6/2012 3/6/2012 3/13/2012L55210-4 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 3/6/2012 3/8/2012 3/8/2012L55214-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 3/2/2012 3/7/2012 3/7/2012L55225-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 3/5/2012 3/7/2012 3/7/2012L55225-3 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 3/5/2012 3/7/2012 3/7/2012L55245-1 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 3/5/2012 3/7/2012 3/7/2012WG120092-1 MB CVTOC BLANK WTR 3/7/2012 3/7/2012 MB1 120307WG120092-2 LCS CVTOC BLANK WTR 3/7/2012 3/7/2012 LEVEL1WG120092-3 SB CVTOC BLANK WTR 3/7/2012 3/7/2012 WG120092-1WG120092-4 LD CVTOC GRND WTR 3/7/2012 3/7/2012 L55139-1WG120092-5 MS CVTOC GRND WTR 3/7/2012 3/7/2012 L55214-1WG120092-6 MS CVTOC STORM WTR 3/7/2012 3/7/2012 L55186-3WG120092-7 MB CVTOC BLANK WTR 3/7/2012 3/7/2012 MB2 120307WG120092-8 LCS CVTOC BLANK WTR 3/7/2012 3/7/2012 LEVEL1WG120092-9 LD CVTOC FRESH WTR 3/8/2012 3/8/2012 L55210-2WG120092-10 MS CVTOC FRESH WTR 3/8/2012 3/8/2012 L55210-4WG120092-11 MB CVDOC BLANK WTR 3/2/2012 3/12/2012 MB1 120302WG120092-12 LCS CVDOC BLANK WTR 3/12/2012 3/12/2012 LEVEL1WG120092-13 MB CVDOC BLANK WTR 3/7/2012 3/12/2012 MB1 120307WG120092-14 SB CVDOC BLANK WTR 3/7/2012 3/12/2012 WG120092-13WG120092-15 LD CVDOC STORM WTR 3/7/2012 3/12/2012 L55177-1WG120092-16 MS CVDOC STORM WTR 3/7/2012 3/12/2012 L55177-2WG120092-17 MB CVDOC BLANK WTR 3/6/2012 3/12/2012 MB1 120309WG120092-18 LD CVDOC FRESH WTR 3/6/2012 3/13/2012 L55210-2WG120092-19 MS CVDOC FRESH WTR 3/6/2012 3/13/2012 L55210-4WG120092-20 MB CVTOC BLANK WTR 3/13/2012 3/13/2012 MB1 120312WG120092-21 LCS CVTOC BLANK WTR 3/13/2012 3/13/2012 LEVEL1WG120092-22 LD CVTOC STORM WTR 3/13/2012 3/13/2012 L55186-1

WG120350 (TSS) Department: 3 - Conventionals Move Date: 03-APR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54930-1 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012

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L54930-2 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L54930-3 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L54930-4 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L54930-5 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L54930-6 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L54930-7 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L55043-1 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L55043-3 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTSS FRESH WTR 3/27/2012 3/28/2012 3/28/2012L55154-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55274-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 3/23/2012 3/28/2012 3/28/2012L55274-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 3/22/2012 3/28/2012 3/28/2012L55277-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 3/26/2012 3/28/2012 3/28/2012L55277-4 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 3/27/2012 3/28/2012 3/28/2012L55317-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTSS GRND WTR 3/22/2012 3/28/2012 3/28/2012L55358-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTSS GRND WTR 3/22/2012 3/28/2012 3/28/2012L55358-2 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTSS GRND WTR 3/22/2012 3/28/2012 3/28/2012L55362-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTSS GRND WTR 3/26/2012 3/28/2012 3/28/2012WG120350-1 MB CVTSS BLANK WTR 3/28/2012 3/28/2012 MB1 3/28/12WG120350-2 LCS CVTSS BLANK WTR 3/28/2012 3/28/2012 LEVEL1WG120350-3 LD CVTSS FRESH WTR 3/28/2012 3/28/2012 L54930-4WG120350-4 LD CVTSS SEWER WTR 3/28/2012 3/28/2012 L55154-2WG120350-5 LD CVTSS GRND WTR 3/28/2012 3/28/2012 L55358-2WG120350-6 LD CVTSS FRESH WTR 3/28/2012 3/28/2012 L55043-1

WG120382 (toc,doc) Department: 3 - Conventionals Move Date: 06-APR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55043-1 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTOC FRESH WTR 3/27/2012 3/28/2012 3/28/2012L55043-3 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTOC FRESH WTR 3/27/2012 3/28/2012 3/28/2012L55154-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55154-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 3/26/2012 3/28/2012 3/28/2012L55194-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 3/19/2012 3/20/2012 3/28/2012L55194-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 3/19/2012 3/20/2012 3/28/2012L55194-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 3/19/2012 3/20/2012 3/27/2012

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L55195-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 3/19/2012 3/20/2012 3/27/2012L55195-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 3/19/2012 3/20/2012 3/27/2012L55195-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 3/19/2012 3/20/2012 3/27/2012L55240-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/28/2012 3/29/2012 3/29/2012L55274-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/23/2012 3/28/2012 3/28/2012L55274-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/22/2012 3/28/2012 3/28/2012L55277-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/26/2012 3/28/2012 3/28/2012L55277-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/28/2012 3/29/2012 3/29/2012L55277-4 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 3/27/2012 3/28/2012 3/28/2012L55278-1 421422-DUSW SWD-DUSW Duvall Surface Water Quarterly CVTOC FRESH WTR 3/28/2012 3/29/2012 3/29/2012L55284-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/27/2012L55284-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/27/2012L55284-3 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/27/2012L55284-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/27/2012L55284-5 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/28/2012L55284-6 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/20/2012 3/22/2012 3/28/2012L55309-1 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 3/14/2012 3/15/2012 3/27/2012L55317-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 3/22/2012 3/28/2012 3/28/2012L55358-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 3/22/2012 3/28/2012 3/28/2012L55358-2 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 3/22/2012 3/28/2012 3/28/2012L55362-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 3/26/2012 3/28/2012 3/28/2012WG120382-1 MB CVDOC BLANK WTR 3/20/2012 3/27/2012 MB1 120320WG120382-2 LCS CVDOC BLANK WTR 3/27/2012 3/27/2012 LEVEL1WG120382-3 SB CVDOC BLANK WTR 3/20/2012 3/27/2012 WG120382-1WG120382-4 LD CVDOC SALT WTR 3/20/2012 3/27/2012 L55195-3WG120382-5 MB CVDOC BLANK WTR 3/15/2012 3/27/2012 MB1 120315WG120382-6 MB CVDOC BLANK WTR 3/22/2012 3/27/2012 MB1 120322WG120382-7 LD CVDOC STORM WTR 3/22/2012 3/27/2012 L55284-2WG120382-8 MS CVDOC STORM WTR 3/22/2012 3/28/2012 L55284-4WG120382-9 MB CVTOC BLANK WTR 3/28/2012 3/28/2012 MB1 120327WG120382-10 LCS CVTOC BLANK WTR 3/28/2012 3/28/2012 LEVEL1WG120382-11 SB CVTOC BLANK WTR 3/28/2012 3/28/2012 WG120382-9WG120382-12 MS CVTOC FRESH WTR 3/28/2012 3/28/2012 L55043-3WG120382-13 LD CVTOC GRND WTR 3/28/2012 3/28/2012 L55274-1WG120382-14 MS CVTOC GRND WTR 3/28/2012 3/28/2012 L55274-3WG120382-15 MB CVTOC BLANK WTR 3/28/2012 3/28/2012 MB1 120328WG120382-16 LCS CVTOC BLANK WTR 3/28/2012 3/28/2012 LEVEL1WG120382-17 SB CVTOC BLANK WTR 3/28/2012 3/28/2012 WG120382-15WG120382-18 LD CVTOC SEWER WTR 3/28/2012 3/28/2012 L55154-1WG120382-19 MS CVTOC SEWER WTR 3/28/2012 3/28/2012 L55154-3WG120382-20 MB CVDOC BLANK WTR 3/28/2012 3/28/2012 MB1 120328

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WG120382-21 LCS CVDOC BLANK WTR 3/28/2012 3/28/2012 LEVEL1WG120382-22 SB CVDOC BLANK WTR 3/28/2012 3/28/2012 WG120382-20WG120382-23 LD CVDOC SEWER WTR 3/28/2012 3/28/2012 L55154-1WG120382-24 MS CVDOC SEWER WTR 3/28/2012 3/28/2012 L55154-3WG120382-25 MS CVDOC FRESH WTR 3/20/2012 3/28/2012 L55194-1WG120382-26 LD CVTOC FRESH WTR 3/28/2012 3/28/2012 L55043-1WG120382-27 MB CVTOC BLANK WTR 3/29/2012 3/29/2012 MB1 120329WG120382-28 LCS CVTOC BLANK WTR 3/29/2012 3/29/2012 LEVEL1


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54893-1 421185 WP INPLANT 3 Day INTENSIVE STUDY CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-1 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-2 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-3 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-4 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-5 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-6 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-7 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-8 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-9 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-10 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55085-11 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55185-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 3/27/2012 4/4/2012 4/5/2012L55185-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 3/27/2012 4/4/2012 4/5/2012L55185-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 3/27/2012 4/4/2012 4/5/2012L55285-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 3/28/2012 4/4/2012 4/5/2012L55285-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 3/28/2012 4/4/2012 4/5/2012L55391-1 422027 Lab Lake Wash PBT-EPA Grant CVTSS STORM WTR 3/29/2012 4/4/2012 4/5/2012L55391-2 422027 Lab Lake Wash PBT-EPA Grant CVTSS STORM WTR 3/30/2012 4/4/2012 4/5/2012L55450-5 422027 Lab Lake Wash PBT-EPA Grant CVTSS STORM WTR 4/3/2012 4/4/2012 4/5/2012WG120479-1 MB CVTSS BLANK WTR 4/4/2012 4/5/2012 MB2 4/4/12WG120479-2 LCS CVTSS BLANK WTR 4/4/2012 4/5/2012 LEVEL1WG120479-3 LD CVTSS STORM WTR 4/4/2012 4/5/2012 L55285-3WG120479-4 LD CVTSS STORM WTR 4/4/2012 4/5/2012 L54893-1WG120479-5 LD CVTSS STORM WTR 4/4/2012 4/5/2012 L55085-9WG120479-6 LD CVTSS STORM WTR 4/4/2012 4/5/2012 L55391-1

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WG120560 (toc/doc) Department: 3 - Conventionals Move Date: 12-APR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55066-1 421422-VASW SWD-VASW Vashon Surface Water Quarterly CVTOC FRESH WTR 3/29/2012 4/3/2012 4/3/2012L55185-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 3/27/2012 3/28/2012 4/5/2012L55185-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 3/27/2012 4/4/2012 4/4/2012L55185-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 3/27/2012 3/28/2012 4/5/2012L55185-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 3/27/2012 4/4/2012 4/4/2012L55185-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 3/27/2012 3/28/2012 4/6/2012L55185-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 3/27/2012 4/4/2012 4/4/2012L55233-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/30/2012 4/3/2012 4/3/2012L55233-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/29/2012 4/3/2012 4/3/2012L55233-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/29/2012 4/3/2012 4/3/2012L55233-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 3/29/2012 4/3/2012 4/3/2012L55268-1 421422-CHGW-NP SWD-CHGW-NP Cedar Hills Groundwater Non-Potable CVTOC GRND WTR 3/30/2012 4/3/2012 4/3/2012L55270-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/3/2012 4/3/2012 4/3/2012L55270-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/3/2012 4/4/2012 4/4/2012L55285-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 3/28/2012 3/30/2012 4/5/2012L55285-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 3/28/2012 4/3/2012 4/3/2012L55285-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 3/28/2012 3/30/2012 4/5/2012L55285-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 3/28/2012 4/3/2012 4/3/2012L55356-3 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 3/29/2012 4/3/2012 4/3/2012L55356-6 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 3/29/2012 4/3/2012 4/3/2012L55356-7 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 3/29/2012 4/3/2012 4/3/2012L55381-1 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 4/3/2012 4/4/2012 4/5/2012L55381-1 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 4/3/2012 4/4/2012 4/4/2012L55381-2 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 4/3/2012 4/4/2012 4/5/2012L55381-2 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 4/3/2012 4/4/2012 4/4/2012L55381-3 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 4/3/2012 4/4/2012 4/5/2012L55381-3 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 4/3/2012 4/4/2012 4/4/2012L55381-4 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 4/3/2012 4/4/2012 4/5/2012L55381-4 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 4/3/2012 4/4/2012 4/4/2012L55384-1 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/29/2012 3/30/2012 4/5/2012L55384-1 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/29/2012 4/3/2012 4/3/2012L55384-2 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/29/2012 3/30/2012 4/5/2012L55384-2 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/29/2012 4/3/2012 4/3/2012L55384-3 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/29/2012 3/30/2012 4/5/2012L55384-3 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/29/2012 4/3/2012 4/3/2012L55384-4 423589-330-4 Green Rvr PCB/PAH Loading CVDOC STORM WTR 3/29/2012 3/30/2012 4/5/2012 FREP@L55384-3L55384-4 423589-330-4 Green Rvr PCB/PAH Loading CVTOC STORM WTR 3/29/2012 4/3/2012 4/3/2012 FREP@L55384-3L55391-1 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 3/29/2012 3/30/2012 4/5/2012

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L55391-1 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 3/29/2012 4/4/2012 4/4/2012L55391-2 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 3/30/2012 3/31/2012 4/5/2012L55391-2 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 3/30/2012 4/4/2012 4/4/2012L55397-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/3/2012 4/4/2012 4/4/2012L55397-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/3/2012 4/4/2012 4/4/2012L55399-1 421422-VALS-Q SWD-VALS-Q Vashon Leachate Quarterly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55399-3 421422-VALS-M SWD-VALS-M Vashon Leachate Monthly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55400-1 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55400-3 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55400-4 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55400-5 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 4/4/2012 4/6/2012 4/6/2012L55402-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/3/2012 4/3/2012 4/3/2012L55402-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/4/2012 4/6/2012 4/6/2012L55402-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55402-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55403-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55403-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/5/2012 4/6/2012 4/6/2012L55403-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/5/2012 4/6/2012 4/6/2012L55403-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55405-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55405-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/6/2012 4/6/2012 4/6/2012L55450-5 422027 Lab Lake Wash PBT-EPA Grant CVDOC STORM WTR 4/3/2012 4/4/2012 4/5/2012L55450-5 422027 Lab Lake Wash PBT-EPA Grant CVTOC STORM WTR 4/3/2012 4/4/2012 4/4/2012WG120560-1 MB CVTOC BLANK WTR 4/3/2012 4/3/2012 MB1 120403WG120560-2 LCS CVTOC BLANK WTR 4/3/2012 4/3/2012 LEVEL1WG120560-3 SB CVTOC BLANK WTR 4/3/2012 4/3/2012 WG120560-1WG120560-4 MS CVTOC GRND WTR 4/3/2012 4/3/2012 L55233-5WG120560-5 LD CVTOC FRESH WTR 4/3/2012 4/3/2012 L55356-3WG120560-6 LD CVTOC STORM WTR 4/3/2012 4/3/2012 L55384-2WG120560-7 MS CVTOC STORM WTR 4/3/2012 4/3/2012 L55384-4WG120560-8 MB CVTOC BLANK WTR 4/4/2012 4/4/2012 MB2 120403WG120560-9 LCS CVTOC BLANK WTR 4/4/2012 4/4/2012 LEVEL1WG120560-10 LD CVTOC FRESH WTR 4/4/2012 4/4/2012 L55381-1WG120560-11 MS CVTOC FRESH WTR 4/4/2012 4/4/2012 L55381-4WG120560-12 MB CVTOC BLANK WTR 4/4/2012 4/4/2012 MB1 120404WG120560-13 LCS CVTOC BLANK WTR 4/4/2012 4/4/2012 LEVEL1WG120560-14 SB CVTOC BLANK WTR 4/4/2012 4/4/2012 WG120560-12WG120560-15 LD CVTOC GRND WTR 4/4/2012 4/4/2012 L55270-2WG120560-16 MS CVTOC FRESH WTR 4/4/2012 4/4/2012 L55356-6WG120560-17 MB CVDOC BLANK WTR 4/4/2012 4/5/2012 MB1 120404WG120560-18 LCS CVDOC BLANK WTR 4/5/2012 4/5/2012 LEVEL1

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WG120560-19 SB CVDOC BLANK WTR 4/4/2012 4/5/2012 WG120560-17WG120560-20 LD CVDOC FRESH WTR 4/4/2012 4/5/2012 L55381-1WG120560-21 MS CVDOC FRESH WTR 4/4/2012 4/5/2012 L55381-3WG120560-22 MB CVDOC BLANK WTR 3/30/2012 4/5/2012 MB2 120330WG120560-23 LD CVDOC STORM WTR 3/30/2012 4/5/2012 L55384-1WG120560-24 MS CVDOC STORM WTR 3/30/2012 4/5/2012 L55384-3WG120560-25 MB CVDOC BLANK WTR 3/30/2012 4/5/2012 MB1 120330WG120560-26 MB CVDOC BLANK WTR 3/28/2012 4/5/2012 MB1 120328WG120560-27 LCS CVDOC BLANK WTR 4/5/2012 4/5/2012 LEVEL1WG120560-28 LD CVDOC STORM WTR 3/28/2012 4/5/2012 L55185-2WG120560-29 MS CVDOC STORM WTR 3/28/2012 4/6/2012 L55185-3WG120560-30 MB CVTOC BLANK WTR 4/6/2012 4/6/2012 MB1 120405WG120560-31 LCS CVTOC BLANK WTR 4/6/2012 4/6/2012 LEVEL1WG120560-32 SB CVTOC BLANK WTR 4/6/2012 4/6/2012 WG120560-30WG120560-33 LD CVTOC GRND WTR 4/6/2012 4/6/2012 L55402-2WG120560-34 MS CVTOC GRND WTR 4/6/2012 4/6/2012 L55403-5WG120560-35 MB CVDOC BLANK WTR 3/31/2012 4/6/2012 MB1 120331WG120560-36 MB CVTOC BLANK WTR 4/6/2012 4/6/2012 MB1 120406WG120560-37 LCS CVTOC BLANK WTR 4/6/2012 4/6/2012 LEVEL1WG120560-38 SB CVTOC BLANK WTR 4/6/2012 4/6/2012 WG120560-36WG120560-39 LD CVTOC LEACHATE 4/6/2012 4/6/2012 L55399-1WG120560-40 MS CVTOC LEACHATE 4/6/2012 4/6/2012 L55400-5


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54976-1 421195-140 Lake Sawyer CVTSS FRESH WTR 4/8/2012 4/11/2012 4/11/2012L54976-2 421195-140 Lake Sawyer CVTSS FRESH WTR 4/8/2012 4/11/2012 4/11/2012L54976-3 421195-140 Lake Sawyer CVTSS FRESH WTR 4/8/2012 4/11/2012 4/11/2012L55183-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/9/2012 4/11/2012 4/11/2012L55183-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/9/2012 4/11/2012 4/11/2012L55183-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/9/2012 4/11/2012 4/11/2012L55435-1 421422-ENLS SWD-ENLS Enumclaw Wastewater Permit CVTSS IW WTR 4/10/2012 4/11/2012 4/11/2012L55435-2 421422-ENLS SWD-ENLS Enumclaw Wastewater Permit CVTSS IW WTR 4/10/2012 4/11/2012 4/11/2012L55462-1 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-2 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-3 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-4 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-5 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-6 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012

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L55462-8 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-9 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-10 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-11 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-12 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-13 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-14 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-15 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-16 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-17 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-19 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-20 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-21 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-22 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-23 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-25 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-26 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-27 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-29 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-30 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-31 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-32 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-33 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/9/2012 4/11/2012 4/11/2012L55462-37 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-38 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-39 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-40 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-41 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-42 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-44 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-45 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-46 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-47 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-48 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012L55462-49 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/10/2012 4/11/2012 4/11/2012WG120569-1 MB CVTSS BLANK WTR 4/11/2012 4/11/2012 MB1 4/11/12WG120569-2 LCS CVTSS BLANK WTR 4/11/2012 4/11/2012 LEVEL1WG120569-3 LD CVTSS FRESH WTR 4/11/2012 4/11/2012 L55462-11WG120569-4 MB CVTSS BLANK WTR 4/11/2012 4/11/2012 MB2 4/11/12WG120569-5 LCS CVTSS BLANK WTR 4/11/2012 4/11/2012 LEVEL1WG120569-6 LD CVTSS FRESH WTR 4/11/2012 4/11/2012 L55462-30

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WG120569-7 MB CVTSS BLANK WTR 4/11/2012 4/11/2012 MB3 4/11/12WG120569-8 LCS CVTSS BLANK WTR 4/11/2012 4/11/2012 LEVEL1WG120569-9 LD CVTSS FRESH WTR 4/11/2012 4/11/2012 L55462-48WG120569-10 LD CVTSS FRESH WTR 4/11/2012 4/11/2012 L54976-1WG120569-11 LD CVTSS IW WTR 4/11/2012 4/11/2012 L55435-1WG120569-12 LD CVTSS SEWER WTR 4/11/2012 4/11/2012 L55183-3


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55184-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/10/2012 4/12/2012 4/12/2012L55184-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/10/2012 4/12/2012 4/12/2012L55184-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/10/2012 4/12/2012 4/12/2012L55402-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55402-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55403-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55403-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55405-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55405-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/6/2012 4/12/2012 4/12/2012L55405-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/9/2012 4/12/2012 4/12/2012L55405-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/9/2012 4/12/2012 4/12/2012L55436-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/9/2012 4/12/2012 4/12/2012L55436-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/9/2012 4/12/2012 4/12/2012L55436-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/10/2012 4/12/2012 4/12/2012L55444-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/10/2012 4/12/2012 4/12/2012L55444-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/10/2012 4/12/2012 4/12/2012WG120580-1 MB CVTSS BLANK WTR 4/12/2012 4/12/2012 MB1 4/12/12WG120580-2 LCS CVTSS BLANK WTR 4/12/2012 4/12/2012 LEVEL1WG120580-3 LD CVTSS GRND WTR 4/12/2012 4/12/2012 L55436-6WG120580-4 LD CVTSS SEWER WTR 4/12/2012 4/12/2012 L55184-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55382-1 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55382-2 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55382-3 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55382-4 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55382-5 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012

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L55382-6 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55382-7 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55382-8 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55382-9 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55382-10 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55382-11 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55382-12 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55406-1 421422-CHSW-P SWD-CHSW P Cedar Hills Surface Water Permit CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55406-2 421422-CHSW-P SWD-CHSW P Cedar Hills Surface Water Permit CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55406-3 421422-CHSW-P SWD-CHSW P Cedar Hills Surface Water Permit CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55433-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/11/2012 4/18/2012 4/18/2012L55433-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/11/2012 4/18/2012 4/18/2012L55433-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/11/2012 4/18/2012 4/18/2012L55440-1 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55440-2 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/16/2012 4/18/2012 4/18/2012L55440-3 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55440-4 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55440-5 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55440-6 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTSS FRESH WTR 4/17/2012 4/18/2012 4/18/2012L55444-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/12/2012 4/18/2012 4/18/2012L55446-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/16/2012 4/18/2012 4/18/2012L55446-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/16/2012 4/18/2012 4/18/2012L55446-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/16/2012 4/18/2012 4/18/2012L55471-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/17/2012 4/18/2012 4/18/2012L55471-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/17/2012 4/18/2012 4/18/2012L55471-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/17/2012 4/18/2012 4/18/2012WG120684-1 MB CVTSS BLANK WTR 4/18/2012 4/18/2012 MB1 4/18/12WG120684-2 LCS CVTSS BLANK WTR 4/18/2012 4/18/2012 LEVEL1WG120684-3 LD CVTSS GRND WTR 4/18/2012 4/18/2012 L55471-1WG120684-4 LD CVTSS FRESH WTR 4/18/2012 4/18/2012 L55440-1WG120684-5 MB CVTSS BLANK WTR 4/18/2012 4/18/2012 MB2 4/18/12WG120684-6 LCS CVTSS BLANK WTR 4/18/2012 4/18/2012 LEVEL1WG120684-7 LD CVTSS FRESH WTR 4/18/2012 4/18/2012 L55382-8WG120684-8 LD CVTSS STORM WTR 4/18/2012 4/18/2012 L55433-3

WG120818 (TSS) Department: 3 - Conventionals Move Date: 01-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55151-1 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55151-2 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012

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L55151-3 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55151-4 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55151-5 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55151-6 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55151-7 421874-100 City of Shoreline Monthly Water Quality Monitoring CVTSS FRESH WTR 4/24/2012 4/25/2012 4/26/2012L55511-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/23/2012 4/25/2012 4/26/2012L55511-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/23/2012 4/25/2012 4/26/2012L55511-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 4/23/2012 4/25/2012 4/26/2012L55526-1 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-2 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-3 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-4 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-5 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-6 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-8 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-9 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-10 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-11 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-12 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-13 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-14 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-15 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-16 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-17 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-19 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-20 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-21 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-22 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-23 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-25 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-26 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-27 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-29 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-30 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-31 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-32 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-33 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-37 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-38 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-39 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-40 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012

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L55526-41 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-42 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-44 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-45 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-46 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-47 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-48 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012L55526-49 421235 MAJOR LAKES (wtr col) CVTSS FRESH WTR 4/23/2012 4/25/2012 4/26/2012WG120818-1 MB CVTSS BLANK WTR 4/25/2012 4/26/2012 MB1 4/25/12WG120818-2 LCS CVTSS BLANK WTR 4/25/2012 4/26/2012 LEVEL1WG120818-3 LD CVTSS FRESH WTR 4/25/2012 4/26/2012 L55526-10WG120818-4 MB CVTSS BLANK WTR 4/25/2012 4/26/2012 MB2 4/25/12WG120818-5 LCS CVTSS BLANK WTR 4/25/2012 4/26/2012 LEVEL1WG120818-6 LD CVTSS FRESH WTR 4/25/2012 4/26/2012 L55526-26WG120818-7 MB CVTSS BLANK WTR 4/25/2012 4/26/2012 MB3 4/25/12WG120818-8 LCS CVTSS BLANK WTR 4/25/2012 4/26/2012 LEVEL1WG120818-9 LD CVTSS FRESH WTR 4/25/2012 4/26/2012 L55526-49WG120818-10 LD CVTSS FRESH WTR 4/25/2012 4/26/2012 L55151-5WG120818-11 LD CVTSS SEWER WTR 4/25/2012 4/26/2012 L55511-3

WG120836 (TOC,DOC) Department: 3 - Conventionals Move Date: 01-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55183-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/9/2012 4/10/2012 4/26/2012L55183-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/9/2012 4/25/2012 4/25/2012L55183-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/9/2012 4/10/2012 4/26/2012L55183-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/9/2012 4/25/2012 4/25/2012L55183-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/9/2012 4/10/2012 4/26/2012L55183-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/9/2012 4/25/2012 4/25/2012L55184-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/10/2012 4/12/2012 4/26/2012L55184-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/10/2012 4/25/2012 4/25/2012L55184-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/10/2012 4/12/2012 4/26/2012L55184-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/10/2012 4/25/2012 4/25/2012L55184-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/10/2012 4/12/2012 4/26/2012L55184-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/10/2012 4/25/2012 4/25/2012L55371-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 4/16/2012 4/17/2012 4/25/2012L55371-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 4/16/2012 4/17/2012 4/25/2012L55371-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 4/16/2012 4/17/2012 4/25/2012L55372-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 4/16/2012 4/17/2012 4/25/2012L55372-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 4/16/2012 4/17/2012 4/25/2012

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L55372-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 4/16/2012 4/17/2012 4/25/2012L55433-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/11/2012 4/12/2012 4/25/2012L55433-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/11/2012 4/25/2012 4/25/2012L55433-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/11/2012 4/12/2012 4/25/2012L55433-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/11/2012 4/25/2012 4/25/2012L55433-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/11/2012 4/12/2012 4/25/2012L55433-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/11/2012 4/25/2012 4/25/2012L55436-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/18/2012 4/24/2012 4/24/2012L55437-1 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/18/2012 4/24/2012 4/24/2012L55437-2 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/18/2012 4/24/2012 4/24/2012L55437-3 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/18/2012 4/24/2012 4/24/2012L55437-4 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/18/2012 4/25/2012 4/25/2012L55437-5 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/18/2012 4/24/2012 4/24/2012L55437-6 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/19/2012 4/24/2012 4/24/2012L55437-7 421422-CHSW-Q SWD-CHSW Q Cedar Hills Surface Water Quarterly CVTOC FRESH WTR 4/19/2012 4/24/2012 4/24/2012L55438-3 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 4/26/2012 4/26/2012 4/26/2012L55438-4 421422-CHSW-A5-TD SWD-CHSW - A5 TD Cedar Hills Surface Area 5 Top Deck CVTOC FRESH WTR 4/18/2012 4/24/2012 4/24/2012L55444-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/18/2012 4/24/2012 4/24/2012L55446-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/18/2012 4/24/2012 4/24/2012L55471-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/23/2012 4/24/2012 4/24/2012L55473-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55473-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55475-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55475-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/19/2012 4/24/2012 4/24/2012L55475-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/23/2012 4/24/2012 4/24/2012L55475-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55476-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55476-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/20/2012 4/24/2012 4/24/2012L55476-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/24/2012 4/25/2012 4/25/2012L55476-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/23/2012 4/24/2012 4/24/2012L55478-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/24/2012 4/24/2012 4/24/2012L55478-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/24/2012 4/24/2012 4/24/2012L55478-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/24/2012 4/24/2012 4/24/2012L55478-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/24/2012 4/24/2012 4/24/2012L55488-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/26/2012 4/26/2012 4/26/2012L55488-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/25/2012 4/25/2012 4/25/2012L55493-1 421422-CHGW-NP SWD-CHGW-NP Cedar Hills Groundwater Non-Potable CVTOC GRND WTR 4/27/2012 4/27/2012 4/27/2012L55496-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTOC GRND WTR 4/27/2012 4/27/2012 4/27/2012L55511-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/23/2012 4/25/2012 4/26/2012L55511-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/23/2012 4/25/2012 4/25/2012L55511-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/23/2012 4/25/2012 4/26/2012

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L55511-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/23/2012 4/25/2012 4/25/2012L55511-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 4/23/2012 4/25/2012 4/26/2012L55511-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 4/23/2012 4/25/2012 4/25/2012L55512-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/24/2012 4/25/2012 4/26/2012L55512-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/24/2012 4/25/2012 4/25/2012L55512-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/24/2012 4/25/2012 4/26/2012L55512-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/24/2012 4/25/2012 4/25/2012L55512-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/24/2012 4/25/2012 4/26/2012L55512-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/24/2012 4/25/2012 4/25/2012L55584-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/25/2012 4/26/2012 4/26/2012L55584-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/25/2012 4/26/2012 4/26/2012L55584-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/25/2012 4/26/2012 4/27/2012L55584-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/25/2012 4/26/2012 4/26/2012L55584-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 4/25/2012 4/26/2012 4/27/2012L55584-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 4/25/2012 4/26/2012 4/26/2012L55588-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 4/26/2012 4/26/2012 4/26/2012WG120836-1 MB CVTOC BLANK WTR 4/24/2012 4/24/2012 MB1 120424WG120836-2 LCS CVTOC BLANK WTR 4/24/2012 4/24/2012 LEVEL1WG120836-3 SB CVTOC BLANK WTR 4/24/2012 4/24/2012 WG120836-1WG120836-4 LD CVTOC GRND WTR 4/24/2012 4/24/2012 L55473-1WG120836-5 MS CVTOC GRND WTR 4/24/2012 4/24/2012 L55436-5WG120836-6 MS CVTOC FRESH WTR 4/24/2012 4/24/2012 L55437-5WG120836-7 MB CVTOC BLANK WTR 4/24/2012 4/24/2012 MB2 120424WG120836-8 LCS CVTOC BLANK WTR 4/24/2012 4/24/2012 LEVEL1WG120836-9 LD CVTOC SEWER WTR 4/25/2012 4/25/2012 L55184-1WG120836-10 MS CVTOC SEWER WTR 4/25/2012 4/25/2012 L55184-3WG120836-11 MB CVTOC BLANK WTR 4/25/2012 4/25/2012 MB1 120425WG120836-12 LCS CVTOC BLANK WTR 4/25/2012 4/25/2012 LEVEL1WG120836-13 SB CVTOC BLANK WTR 4/25/2012 4/25/2012 WG120836-11WG120836-14 LD CVTOC FRESH WTR 4/25/2012 4/25/2012 L55437-4WG120836-15 LD CVTOC STORM WTR 4/25/2012 4/25/2012 L55433-1WG120836-16 MS CVTOC STORM WTR 4/25/2012 4/25/2012 L55433-3WG120836-17 MB CVDOC BLANK WTR 4/17/2012 4/25/2012 MB1 120417WG120836-18 LCS CVDOC BLANK WTR 4/25/2012 4/25/2012 LEVEL1WG120836-19 SB CVDOC BLANK WTR 4/17/2012 4/25/2012 WG120836-17WG120836-20 MS CVDOC FRESH WTR 4/17/2012 4/25/2012 L55371-3WG120836-21 LD CVDOC SALT WTR 4/17/2012 4/25/2012 L55372-2WG120836-22 MB CVDOC BLANK WTR 4/12/2012 4/25/2012 MB2 120412WG120836-23 LD CVDOC STORM WTR 4/12/2012 4/25/2012 L55433-1WG120836-24 MS CVDOC STORM WTR 4/12/2012 4/25/2012 L55433-3WG120836-25 MB CVDOC BLANK WTR 4/10/2012 4/26/2012 MB1 120410

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WG120836-26 LD CVDOC SEWER WTR 4/10/2012 4/26/2012 L55183-1WG120836-27 MS CVDOC SEWER WTR 4/10/2012 4/26/2012 L55183-3WG120836-28 MB CVDOC BLANK WTR 4/12/2012 4/26/2012 MB1 120412WG120836-29 MB CVDOC BLANK WTR 4/25/2012 4/26/2012 MB1 120425WG120836-30 LCS CVDOC BLANK WTR 4/26/2012 4/26/2012 LEVEL1WG120836-31 MB CVTOC BLANK WTR 4/26/2012 4/26/2012 MB1 120426WG120836-32 LCS CVTOC BLANK WTR 4/26/2012 4/26/2012 LEVEL1WG120836-33 MB CVDOC BLANK WTR 4/26/2012 4/26/2012 MB1 120426WG120836-34 LCS CVDOC BLANK WTR 4/26/2012 4/26/2012 LEVEL1WG120836-35 MB CVTOC BLANK WTR 4/27/2012 4/27/2012 MB1 120427WG120836-36 LCS CVTOC BLANK WTR 4/27/2012 4/27/2012 LEVEL1WG120836-37 SB CVTOC BLANK WTR 4/27/2012 4/27/2012 WG120836-35WG120836-38 LD CVTOC GRND WTR 4/27/2012 4/27/2012 L55493-1WG120836-39 MS CVTOC GRND WTR 4/27/2012 4/27/2012 L55496-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55476-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/24/2012 4/30/2012 4/30/2012L55478-1 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/24/2012 4/30/2012 4/30/2012L55478-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/24/2012 4/30/2012 4/30/2012L55478-5 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/24/2012 4/30/2012 4/30/2012L55478-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/24/2012 4/30/2012 4/30/2012L55488-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/26/2012 4/30/2012 4/30/2012L55488-6 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/25/2012 4/30/2012 4/30/2012L55493-1 421422-CHGW-NP SWD-CHGW-NP Cedar Hills Groundwater Non-Potable CVTSS GRND WTR 4/27/2012 4/30/2012 4/30/2012L55496-2 421422-CHGW SWD-CHGW Cedar Hills Groundwater Quarterly CVTSS GRND WTR 4/27/2012 4/30/2012 4/30/2012L55512-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/24/2012 4/30/2012 4/30/2012L55512-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/24/2012 4/30/2012 4/30/2012L55512-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/24/2012 4/30/2012 4/30/2012L55584-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/25/2012 4/30/2012 4/30/2012L55584-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/25/2012 4/30/2012 4/30/2012L55584-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 4/25/2012 4/30/2012 4/30/2012L55588-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 4/26/2012 4/30/2012 4/30/2012WG120873-1 MB CVTSS BLANK WTR 4/30/2012 4/30/2012 MB1 4/30/12WG120873-2 LCS CVTSS BLANK WTR 4/30/2012 4/30/2012 LEVEL1WG120873-3 LD CVTSS GRND WTR 4/30/2012 4/30/2012 L55478-1WG120873-4 LD CVTSS FRESH WTR 4/30/2012 4/30/2012 L55588-1WG120873-5 LD CVTSS STORM WTR 4/30/2012 4/30/2012 L55512-1

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55572-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 5/7/2012 5/11/2012 5/11/2012L55572-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 5/7/2012 5/11/2012 5/11/2012L55639-1 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-2 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-3 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-4 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-5 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-6 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-7 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-8 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-9 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-10 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-11 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55639-12 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-1 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-2 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-3 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-4 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-5 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-6 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-7 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55640-8 421240A STREAMS MONITOR (surf wtr) CVTSS FRESH WTR 5/7/2012 5/11/2012 5/11/2012L55641-1 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 5/8/2012 5/11/2012 5/11/2012L55641-2 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 5/8/2012 5/11/2012 5/11/2012L55641-3 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 5/8/2012 5/11/2012 5/11/2012L55641-4 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 5/8/2012 5/11/2012 5/11/2012L55686-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 5/8/2012 5/11/2012 5/11/2012L55686-2 423589-320-4 CSO Basin Study CVTSS SEWER WTR 5/8/2012 5/11/2012 5/11/2012L55686-3 423589-320-4 CSO Basin Study CVTSS SEWER WTR 5/8/2012 5/11/2012 5/11/2012WG121035-1 MB CVTSS BLANK WTR 5/11/2012 5/11/2012 MB2 5/11/12WG121035-2 LCS CVTSS BLANK WTR 5/11/2012 5/11/2012 LEVEL1WG121035-3 LD CVTSS FRESH WTR 5/11/2012 5/11/2012 L55639-11WG121035-4 MB CVTSS BLANK WTR 5/11/2012 5/11/2012 MB3 5/11/12WG121035-5 LCS CVTSS BLANK WTR 5/11/2012 5/11/2012 LEVEL1WG121035-6 LD CVTSS FRESH WTR 5/11/2012 5/11/2012 L55641-3WG121035-7 LD CVTSS SEWER WTR 5/11/2012 5/11/2012 L55572-3

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WG121155 (toc/doc) Department: 3 - Conventionals Move Date: 25-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55572-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 5/7/2012 5/9/2012 5/15/2012L55572-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 5/7/2012 5/16/2012 5/16/2012L55572-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 5/7/2012 5/9/2012 5/15/2012L55572-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 5/7/2012 5/16/2012 5/16/2012L55605-1 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 5/2/2012 5/16/2012 5/16/2012L55605-3 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 5/3/2012 5/17/2012 5/17/2012L55605-4 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 5/3/2012 5/17/2012 5/17/2012L55605-5 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 5/3/2012 5/23/2012 5/23/2012L55606-1 421422-VALS-M SWD-VALS-M Vashon Leachate Monthly CVTOC LEACHATE 5/2/2012 5/15/2012 5/15/2012L55618-3 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/14/2012 5/17/2012 5/17/2012L55622-1 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/15/2012 5/17/2012 5/17/2012L55622-2 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/15/2012 5/17/2012 5/17/2012L55622-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/15/2012 5/17/2012 5/17/2012L55641-1 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 5/8/2012 5/9/2012 5/15/2012L55641-2 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 5/8/2012 5/9/2012 5/15/2012L55641-3 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 5/8/2012 5/9/2012 5/15/2012L55641-4 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 5/8/2012 5/9/2012 5/15/2012L55653-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/10/2012 5/15/2012 5/15/2012L55653-3 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/10/2012 5/15/2012 5/15/2012L55653-4 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/10/2012 5/15/2012 5/15/2012L55655-1 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/14/2012 5/17/2012 5/17/2012L55656-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/14/2012 5/17/2012 5/17/2012L55656-3 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/14/2012 5/17/2012 5/17/2012L55658-1 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/16/2012 5/17/2012 5/17/2012L55658-3 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/16/2012 5/17/2012 5/17/2012L55658-4 421422-ENGW SWD-ENGW Enumclaw Groundwater Quarterly CVTOC GRND WTR 5/16/2012 5/17/2012 5/17/2012L55660-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/16/2012 5/17/2012 5/17/2012L55686-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 5/8/2012 5/10/2012 5/15/2012L55686-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 5/8/2012 5/23/2012 5/23/2012L55686-2 423589-320-4 CSO Basin Study CVDOC SEWER WTR 5/8/2012 5/10/2012 5/15/2012L55686-2 423589-320-4 CSO Basin Study CVTOC SEWER WTR 5/8/2012 5/16/2012 5/16/2012L55686-3 423589-320-4 CSO Basin Study CVDOC SEWER WTR 5/8/2012 5/10/2012 5/15/2012L55686-3 423589-320-4 CSO Basin Study CVTOC SEWER WTR 5/8/2012 5/16/2012 5/16/2012L55699-1 421422-CFGW SWD-CFGW Cedar Falls Groundwater Quarterly CVTOC GRND WTR 5/11/2012 5/17/2012 5/17/2012WG121155-1 MB CVDOC BLANK WTR 5/9/2012 5/15/2012 MB1 120509WG121155-2 LCS CVDOC BLANK WTR 5/15/2012 5/15/2012 LEVEL1WG121155-3 SB CVDOC BLANK WTR 5/9/2012 5/15/2012 WG121155-1

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WG121155-4 LD CVDOC FRESH WTR 5/9/2012 5/15/2012 L55641-1WG121155-5 MS CVDOC FRESH WTR 5/9/2012 5/15/2012 L55641-4WG121155-6 LD CVDOC SEWER WTR 5/9/2012 5/15/2012 L55572-1WG121155-7 MS CVDOC SEWER WTR 5/9/2012 5/15/2012 L55572-3WG121155-8 MB CVDOC BLANK WTR 5/10/2012 5/15/2012 MB1 120510WG121155-9 MB CVTOC BLANK WTR 5/15/2012 5/15/2012 MB1 120510WG121155-10 LCS CVTOC BLANK WTR 5/15/2012 5/15/2012 LEVEL1WG121155-11 SB CVTOC BLANK WTR 5/15/2012 5/15/2012 WG121155-9WG121155-12 MB CVTOC BLANK WTR 5/16/2012 5/16/2012 MB1 120516WG121155-13 LCS CVTOC BLANK WTR 5/16/2012 5/16/2012 LEVEL1WG121155-14 SB CVTOC BLANK WTR 5/16/2012 5/16/2012 WG121155-12WG121155-15 LD CVTOC SEWER WTR 5/16/2012 5/16/2012 L55572-1WG121155-16 MS CVTOC SEWER WTR 5/16/2012 5/16/2012 L55572-3WG121155-17 LD CVTOC LEACHATE 5/17/2012 5/17/2012 L55605-1WG121155-18 MS CVTOC LEACHATE 5/23/2012 5/23/2012 L55605-3WG121155-19 LD CVTOC GRND WTR 5/17/2012 5/17/2012 L55618-3WG121155-20 MS CVTOC GRND WTR 5/17/2012 5/17/2012 L55622-1WG121155-21 MB CVTOC BLANK WTR 5/17/2012 5/17/2012 MB2 120516WG121155-22 LCS CVTOC BLANK WTR 5/17/2012 5/17/2012 LEVEL1WG121155-23 MB CVTOC BLANK WTR 5/23/2012 5/23/2012 MB1 120523WG121155-24 LCS CVTOC BLANK WTR 5/23/2012 5/23/2012 LEVEL1WG121155-25 SB CVTOC BLANK WTR 5/23/2012 5/23/2012 WG121155-23

WG121213 (toc/doc) Department: 3 - Conventionals Move Date: 30-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55536-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 5/21/2012 5/22/2012 5/24/2012L55536-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 5/21/2012 5/24/2012 5/24/2012L55536-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 5/21/2012 5/22/2012 5/24/2012L55536-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 5/21/2012 5/24/2012 5/24/2012L55536-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 5/21/2012 5/22/2012 5/24/2012L55536-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 5/21/2012 5/24/2012 5/24/2012L55537-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 5/21/2012 5/22/2012 5/24/2012L55537-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 5/21/2012 5/24/2012 5/24/2012L55537-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 5/21/2012 5/22/2012 5/24/2012L55537-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 5/21/2012 5/24/2012 5/24/2012L55537-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 5/21/2012 5/22/2012 5/24/2012L55537-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 5/21/2012 5/24/2012 5/24/2012L55638-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/21/2012 5/22/2012 5/25/2012L55638-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/21/2012 5/24/2012 5/24/2012

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L55638-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/21/2012 5/22/2012 5/25/2012L55638-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/21/2012 5/24/2012 5/24/2012L55638-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/21/2012 5/22/2012 5/25/2012L55638-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/21/2012 5/25/2012 5/25/2012L55671-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/17/2012 5/23/2012 5/23/2012L55671-3 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55671-4 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55671-5 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55671-6 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55671-7 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55672-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/22/2012 5/23/2012 5/23/2012L55672-2 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/22/2012 5/23/2012 5/23/2012L55672-3 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/22/2012 5/23/2012 5/23/2012L55672-4 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/22/2012 5/23/2012 5/23/2012L55672-5 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/22/2012 5/23/2012 5/23/2012L55672-6 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/23/2012 5/23/2012 5/23/2012L55672-7 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55672-8 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55672-9 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55672-10 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55672-11 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/24/2012 5/25/2012 5/25/2012L55672-12 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 5/24/2012 5/25/2012 5/25/2012L55674-1 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55674-2 421422-CFSW SWD-CFSW Cedar Falls Surface Water Quarterly CVTOC FRESH WTR 5/23/2012 5/24/2012 5/24/2012L55677-1 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/21/2012 5/23/2012 5/23/2012L55677-3 421422-HOGW SWD-HOGW Hobart Groundwater Quarterly CVTOC GRND WTR 5/22/2012 5/23/2012 5/23/2012L55763-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/22/2012 5/23/2012 5/24/2012L55763-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/22/2012 5/24/2012 5/24/2012L55763-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/22/2012 5/23/2012 5/25/2012L55763-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/22/2012 5/24/2012 5/24/2012L55763-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 5/22/2012 5/23/2012 5/25/2012L55763-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 5/22/2012 5/24/2012 5/24/2012WG121213-1 MB CVTOC BLANK WTR 5/23/2012 5/23/2012 MB2 120523WG121213-2 LCS CVTOC BLANK WTR 5/23/2012 5/23/2012 LEVEL1WG121213-3 SB CVTOC BLANK WTR 5/23/2012 5/23/2012 WG121213-1WG121213-4 LD CVTOC GRND WTR 5/23/2012 5/23/2012 L55671-3WG121213-5 MS CVTOC GRND WTR 5/23/2012 5/23/2012 L55671-5WG121213-6 LD CVTOC FRESH WTR 5/24/2012 5/24/2012 L55672-8WG121213-7 MS CVTOC FRESH WTR 5/24/2012 5/24/2012 L55672-9WG121213-8 MB CVTOC BLANK WTR 5/24/2012 5/24/2012 MB1 120524WG121213-9 LCS CVTOC BLANK WTR 5/24/2012 5/24/2012 LEVEL1

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WG121213-10 SB CVTOC BLANK WTR 5/24/2012 5/24/2012 WG121213-8WG121213-11 LD CVTOC FRESH WTR 5/24/2012 5/24/2012 L55536-3WG121213-12 MS CVTOC SALT WTR 5/24/2012 5/24/2012 L55537-2WG121213-13 LD CVTOC STORM WTR 5/24/2012 5/24/2012 L55638-2WG121213-14 MS CVTOC STORM WTR 5/24/2012 5/24/2012 L55763-1WG121213-15 MB CVDOC BLANK WTR 5/22/2012 5/24/2012 MB1 120522WG121213-16 LCS CVDOC BLANK WTR 5/24/2012 5/24/2012 LEVEL1WG121213-17 SB CVDOC BLANK WTR 5/22/2012 5/24/2012 WG121213-15WG121213-18 LD CVDOC FRESH WTR 5/22/2012 5/24/2012 L55536-3WG121213-19 MS CVDOC SALT WTR 5/22/2012 5/24/2012 L55537-2WG121213-20 MB CVDOC BLANK WTR 5/23/2012 5/24/2012 MB1 120523WG121213-21 MS CVDOC STORM WTR 5/23/2012 5/25/2012 L55763-1WG121213-22 MB CVDOC BLANK WTR 5/22/2012 5/25/2012 MB2 120522WG121213-23 LD CVDOC STORM WTR 5/22/2012 5/25/2012 L55638-2WG121213-24 MB CVTOC BLANK WTR 5/25/2012 5/25/2012 MB1 120525WG121213-25 LCS CVTOC BLANK WTR 5/25/2012 5/25/2012 LEVEL1WG121213-26 SB CVTOC BLANK WTR 5/25/2012 5/25/2012 WG121213-24WG121213-27 LCS CVDOC BLANK WTR 5/25/2012 5/25/2012 LEVEL1

WG121219 (TSS) Department: 3 - Conventionals Move Date: 21-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55638-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/21/2012 5/24/2012 5/24/2012L55638-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/21/2012 5/24/2012 5/24/2012L55638-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/21/2012 5/24/2012 5/24/2012L55738-3 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 5/23/2012 5/24/2012 5/24/2012L55738-4 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 5/23/2012 5/24/2012 5/24/2012L55738-5 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 5/23/2012 5/24/2012 5/24/2012L55738-6 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 5/23/2012 5/24/2012 5/24/2012L55738-8 421250BS Ambient Intertidal Beaches-South CVTSS SALT WTR 5/23/2012 5/24/2012 5/24/2012L55763-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/22/2012 5/24/2012 5/24/2012L55763-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/22/2012 5/24/2012 5/24/2012L55763-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 5/22/2012 5/24/2012 5/24/2012WG121219-1 MB CVTSS BLANK WTR 5/24/2012 5/24/2012 MB1 5/24/12WG121219-2 LCS CVTSS BLANK WTR 5/24/2012 5/24/2012 LEVEL1WG121219-3 LD CVTSS SALT WTR 5/24/2012 5/24/2012 L55738-5WG121219-4 LD CVTSS STORM WTR 5/24/2012 5/24/2012 L55763-1

WG121455 (TSS) Department: 3 - Conventionals Move Date: 03-JUL-12

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55463-1 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-2 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-3 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-4 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-5 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-6 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-7 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-8 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-9 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-10 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55463-11 421195-180 Mercer Island Stormwater Monitoring CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55756-1 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 6/5/2012 6/11/2012 6/12/2012L55756-2 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 6/5/2012 6/11/2012 6/12/2012L55756-3 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 6/5/2012 6/11/2012 6/12/2012L55756-4 421195-190 Vashon Island Surface Water CVTSS FRESH WTR 6/5/2012 6/11/2012 6/12/2012L55764-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/4/2012 6/11/2012 6/12/2012L55764-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/4/2012 6/11/2012 6/12/2012L55764-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/4/2012 6/11/2012 6/12/2012L55859-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/5/2012 6/11/2012 6/12/2012L55859-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/5/2012 6/11/2012 6/12/2012L55875-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/6/2012 6/11/2012 6/12/2012L55875-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/6/2012 6/11/2012 6/12/2012L55876-1 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55876-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012L55876-3 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/7/2012 6/11/2012 6/12/2012WG121455-1 MB CVTSS BLANK WTR 6/11/2012 6/12/2012 MB1 6/11/12WG121455-2 LCS CVTSS BLANK WTR 6/11/2012 6/12/2012 LEVEL1WG121455-3 LD CVTSS STORM WTR 6/11/2012 6/12/2012 L55875-3WG121455-4 LD CVTSS FRESH WTR 6/11/2012 6/12/2012 L55756-2WG121455-5 MB CVTSS BLANK WTR 6/11/2012 6/12/2012 MB2 6/11/12WG121455-6 LCS CVTSS BLANK WTR 6/11/2012 6/12/2012 LEVEL1WG121455-7 LD CVTSS STORM WTR 6/11/2012 6/12/2012 L55463-5

WG121474 (toc/doc) Department: 3 - Conventionals Move Date: 15-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55661-1 421422-VAGW SWD-VAGW Vashon Groundwater Quarterly CVTOC GRND WTR 6/5/2012 6/6/2012 6/6/2012L55661-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/7/2012 6/7/2012

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L55756-1 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 6/5/2012 6/5/2012 6/6/2012L55756-1 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 6/5/2012 6/6/2012 6/6/2012L55756-2 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 6/5/2012 6/5/2012 6/7/2012L55756-2 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 6/5/2012 6/7/2012 6/7/2012L55756-3 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 6/5/2012 6/5/2012 6/7/2012L55756-3 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 6/5/2012 6/7/2012 6/7/2012L55756-4 421195-190 Vashon Island Surface Water CVDOC FRESH WTR 6/5/2012 6/5/2012 6/7/2012L55756-4 421195-190 Vashon Island Surface Water CVTOC FRESH WTR 6/5/2012 6/6/2012 6/6/2012L55764-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/4/2012 6/5/2012 6/7/2012L55764-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/4/2012 6/7/2012 6/7/2012L55764-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/4/2012 6/5/2012 6/7/2012L55764-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/4/2012 6/6/2012 6/6/2012L55764-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/4/2012 6/5/2012 6/7/2012L55764-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/4/2012 6/6/2012 6/6/2012L55796-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/4/2012 6/6/2012 6/6/2012L55796-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/1/2012 6/6/2012 6/6/2012L55802-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/1/2012 6/6/2012 6/6/2012L55805-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/7/2012 6/7/2012 6/7/2012L55807-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/6/2012 6/6/2012L55807-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/6/2012 6/6/2012L55809-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/4/2012 6/6/2012 6/6/2012L55809-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/4/2012 6/6/2012 6/6/2012L55809-4 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/6/2012 6/6/2012L55811-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/7/2012 6/7/2012 6/7/2012L55811-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/7/2012 6/7/2012 6/7/2012L55812-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/7/2012 6/7/2012L55812-3 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/6/2012 6/7/2012 6/7/2012L55859-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/5/2012 6/7/2012 6/7/2012L55859-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/5/2012 6/7/2012 6/7/2012L55859-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/5/2012 6/7/2012 6/8/2012L55859-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/5/2012 6/8/2012 6/8/2012L55875-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/6/2012 6/7/2012 6/7/2012L55875-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/6/2012 6/7/2012 6/7/2012L55875-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/6/2012 6/7/2012 6/8/2012L55875-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/6/2012 6/8/2012 6/8/2012WG121474-1 MB CVTOC BLANK WTR 6/6/2012 6/6/2012 MB1 120606WG121474-2 LCS CVTOC BLANK WTR 6/6/2012 6/6/2012 LEVEL1WG121474-3 SB CVTOC BLANK WTR 6/6/2012 6/6/2012 WG121474-1WG121474-4 LD CVTOC GRND WTR 6/6/2012 6/6/2012 L55796-1WG121474-5 MS CVTOC GRND WTR 6/6/2012 6/6/2012 L55661-1WG121474-6 LD CVTOC FRESH WTR 6/6/2012 6/6/2012 L55756-1

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WG121474-7 MS CVTOC STORM WTR 6/6/2012 6/6/2012 L55764-2WG121474-8 MB CVDOC BLANK WTR 6/5/2012 6/6/2012 MB1 120605WG121474-9 LCS CVDOC BLANK WTR 6/6/2012 6/6/2012 LEVEL1WG121474-10 SB CVDOC BLANK WTR 6/5/2012 6/6/2012 WG121474-8WG121474-11 LD CVDOC FRESH WTR 6/5/2012 6/6/2012 L55756-1WG121474-12 MS CVDOC FRESH WTR 6/5/2012 6/7/2012 L55756-3WG121474-13 LD CVDOC STORM WTR 6/5/2012 6/7/2012 L55764-2WG121474-14 MS CVDOC STORM WTR 6/5/2012 6/7/2012 L55764-3WG121474-15 MB CVTOC BLANK WTR 6/7/2012 6/7/2012 MB1 120607WG121474-16 LCS CVTOC BLANK WTR 6/7/2012 6/7/2012 LEVEL1WG121474-17 SB CVTOC BLANK WTR 6/7/2012 6/7/2012 WG121474-15WG121474-18 MS CVTOC FRESH WTR 6/7/2012 6/7/2012 L55756-3WG121474-19 LD CVTOC STORM WTR 6/7/2012 6/7/2012 L55764-1WG121474-20 MB CVDOC BLANK WTR 6/5/2012 6/7/2012 MB1 120605WG121474-21 LCS CVDOC BLANK WTR 6/7/2012 6/7/2012 LEVEL1WG121474-22 SB CVDOC BLANK WTR 6/5/2012 6/7/2012 WG121474-20WG121474-23 MS CVDOC FRESH WTR 6/5/2012 6/7/2012 L55756-3WG121474-24 MB CVDOC BLANK WTR 6/7/2012 6/7/2012 MB1 120607WG121474-25 MB CVDOC BLANK WTR 6/7/2012 6/7/2012 MB2 120607WG121474-26 MB CVTOC BLANK WTR 6/8/2012 6/8/2012 MB1 120608WG121474-27 LCS CVTOC BLANK WTR 6/8/2012 6/8/2012 LEVEL1WG121474-28 LCS CVDOC BLANK WTR 6/8/2012 6/8/2012 LEVEL1


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55620-4 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/11/2012 6/13/2012 6/13/2012L55805-2 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/8/2012 6/13/2012 6/13/2012L55806-1 421422-DUGW SWD-DUGW Duvall Groundwater Quarterly CVTOC GRND WTR 6/8/2012 6/13/2012 6/13/2012L55806-2 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/15/2012 6/15/2012 6/15/2012L55818-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/15/2012 6/15/2012 6/15/2012L55820-1 421422-VALS-M SWD-VALS-M Vashon Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55820-3 421422-VALS-M SWD-VALS-M Vashon Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55821-1 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55821-3 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55821-4 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55821-5 421422-CHLS-M SWD-CHLS-M Cedar Hills Leachate Monthly CVTOC LEACHATE 6/13/2012 6/14/2012 6/14/2012L55824-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55824-3 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55824-4 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012

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L55824-5 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55825-1 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55825-3 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55825-4 421422-HTGW SWD-HTGW Houghton Groundwater Quarterly CVTOC GRND WTR 6/14/2012 6/14/2012 6/14/2012L55876-1 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/7/2012 6/8/2012 6/13/2012L55876-1 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/7/2012 6/13/2012 6/13/2012L55876-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/7/2012 6/8/2012 6/13/2012L55876-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/7/2012 6/13/2012 6/13/2012L55876-3 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/7/2012 6/8/2012 6/13/2012L55876-3 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/7/2012 6/13/2012 6/13/2012L55915-1 421168 Lander Street Storm Separation CVTOC BLANK WTR 6/14/2012 6/14/2012 6/14/2012WG121560-1 MB CVTOC BLANK WTR 6/13/2012 6/13/2012 MB1 120613WG121560-2 LCS CVTOC BLANK WTR 6/13/2012 6/13/2012 LEVEL1WG121560-3 SB CVTOC BLANK WTR 6/13/2012 6/13/2012 WG121560-1WG121560-4 LD CVTOC GRND WTR 6/13/2012 6/13/2012 L55805-2WG121560-5 MS CVTOC GRND WTR 6/13/2012 6/13/2012 L55620-4WG121560-6 LD CVTOC STORM WTR 6/13/2012 6/13/2012 L55876-2WG121560-7 MS CVTOC STORM WTR 6/13/2012 6/13/2012 L55876-3WG121560-8 MB CVDOC BLANK WTR 6/8/2012 6/13/2012 MB1 120608WG121560-9 LCS CVDOC BLANK WTR 6/13/2012 6/13/2012 LEVEL1WG121560-10 SB CVDOC BLANK WTR 6/8/2012 6/13/2012 WG121560-8WG121560-11 LD CVDOC STORM WTR 6/8/2012 6/13/2012 L55876-2WG121560-12 MS CVDOC STORM WTR 6/8/2012 6/13/2012 L55876-3WG121560-13 MB CVTOC BLANK WTR 6/14/2012 6/14/2012 MB1 120614WG121560-14 LCS CVTOC BLANK WTR 6/14/2012 6/14/2012 LEVEL1WG121560-15 SB CVTOC BLANK WTR 6/14/2012 6/14/2012 WG121560-13WG121560-16 LD CVTOC LEACHATE 6/14/2012 6/14/2012 L55821-3WG121560-17 MS CVTOC LEACHATE 6/14/2012 6/14/2012 L55821-5WG121560-18 MB CVTOC BLANK WTR 6/15/2012 6/15/2012 MB1 120615WG121560-19 LCS CVTOC BLANK WTR 6/15/2012 6/15/2012 LEVEL1WG121560-20 SB CVTOC BLANK WTR 6/15/2012 6/15/2012 WG121560-18WG121560-21 MS CVTOC GRND WTR 6/15/2012 6/15/2012 L55818-1WG121560-22 LD CVTOC GRND WTR 6/15/2012 6/15/2012 L55806-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55757-1 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-2 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-3 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012

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L55757-4 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-5 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-6 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-7 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-8 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-9 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-10 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-11 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55757-12 422019 WRIA 7 Streams Ambient Monitoring CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55789-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55789-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55789-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55790-1 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 6/18/2012 6/20/2012 6/21/2012L55790-2 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 6/18/2012 6/20/2012 6/21/2012L55790-3 423589-030-1 LDWG-Water Column PCB Analysis CVTSS SALT WTR 6/18/2012 6/20/2012 6/21/2012L55827-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-2 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-3 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-5 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-6 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-7 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-8 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-9 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-10 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-11 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/18/2012 6/20/2012 6/21/2012L55827-12 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTSS FRESH WTR 6/19/2012 6/20/2012 6/21/2012L55920-1 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 6/19/2012 6/20/2012 6/21/2012L55920-2 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 6/19/2012 6/20/2012 6/21/2012L55920-3 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 6/19/2012 6/20/2012 6/21/2012L55920-4 421422-CHSW-P2 SWD-CHSW P - 2 Cedar Hills Surface Water Permit 2 CVTSS FRESH WTR 6/19/2012 6/20/2012 6/21/2012L55936-2 423589-320-4 CSO Basin Study CVTSS STORM WTR 6/18/2012 6/20/2012 6/21/2012WG121636-1 MB CVTSS BLANK WTR 6/20/2012 6/21/2012 MB1 6/20/12WG121636-2 LCS CVTSS BLANK WTR 6/20/2012 6/21/2012 LEVEL1WG121636-3 LD CVTSS FRESH WTR 6/20/2012 6/21/2012 L55757-6WG121636-4 LD CVTSS FRESH WTR 6/20/2012 6/21/2012 L55789-3WG121636-5 LD CVTSS SALT WTR 6/20/2012 6/21/2012 L55790-3WG121636-6 MB CVTSS BLANK WTR 6/20/2012 6/21/2012 MB2 6/20/12WG121636-7 LCS CVTSS BLANK WTR 6/20/2012 6/21/2012 LEVEL1WG121636-8 LD CVTSS FRESH WTR 6/20/2012 6/21/2012 L55827-8WG121636-9 LD CVTSS STORM WTR 6/20/2012 6/21/2012 L55936-2

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55789-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 6/18/2012 6/19/2012 6/21/2012L55789-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55789-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 6/18/2012 6/19/2012 6/21/2012L55789-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55789-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC FRESH WTR 6/18/2012 6/19/2012 6/22/2012L55789-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC FRESH WTR 6/18/2012 6/21/2012 6/21/2012L55790-1 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 6/18/2012 6/19/2012 6/21/2012L55790-1 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 6/18/2012 6/21/2012 6/21/2012L55790-2 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 6/18/2012 6/19/2012 6/21/2012L55790-2 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 6/18/2012 6/21/2012 6/21/2012L55790-3 423589-030-1 LDWG-Water Column PCB Analysis CVDOC SALT WTR 6/18/2012 6/19/2012 6/21/2012L55790-3 423589-030-1 LDWG-Water Column PCB Analysis CVTOC SALT WTR 6/18/2012 6/21/2012 6/21/2012L55827-1 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-2 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-3 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-5 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-6 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-7 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-8 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-9 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-10 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-11 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/18/2012 6/20/2012 6/20/2012L55827-12 421422-CHSW-M SWD-CHSW M Cedar Hills Surface Water Monthly CVTOC FRESH WTR 6/19/2012 6/20/2012 6/20/2012L55828-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/19/2012 6/21/2012 6/21/2012L55828-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/19/2012 6/20/2012 6/20/2012L55829-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/21/2012 6/22/2012 6/22/2012L55830-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/21/2012 6/22/2012 6/22/2012L55830-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/21/2012 6/22/2012 6/22/2012L55927-1 421422-CHGW-OS SWD-CHGW-OS Cedar Hills Groundwater Off-Site CVTOC GRND WTR 6/20/2012 6/20/2012 6/20/2012L55936-2 423589-320-4 CSO Basin Study CVDOC STORM WTR 6/18/2012 6/19/2012 6/22/2012L55936-2 423589-320-4 CSO Basin Study CVTOC STORM WTR 6/18/2012 6/20/2012 6/20/2012WG121701-1 MB CVTOC BLANK WTR 6/20/2012 6/20/2012 MB1 120620WG121701-2 LCS CVTOC BLANK WTR 6/20/2012 6/20/2012 LEVEL1WG121701-3 SB CVTOC BLANK WTR 6/20/2012 6/20/2012 WG121701-1WG121701-4 LD CVTOC FRESH WTR 6/20/2012 6/20/2012 L55827-8WG121701-5 MS CVTOC FRESH WTR 6/20/2012 6/20/2012 L55827-10WG121701-6 MS CVTOC GRND WTR 6/20/2012 6/20/2012 L55828-3

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WG121701-7 LD CVTOC STORM WTR 6/20/2012 6/20/2012 L55936-2WG121701-8 MS CVTOC STORM WTR 6/20/2012 6/20/2012 L55936-2WG121701-9 MB CVTOC BLANK WTR 6/21/2012 6/21/2012 MB2 120620WG121701-10 LCS CVTOC BLANK WTR 6/21/2012 6/21/2012 LEVEL1WG121701-11 LD CVTOC SALT WTR 6/21/2012 6/21/2012 L55790-2WG121701-12 MB CVTOC BLANK WTR 6/21/2012 6/21/2012 MB1 120621WG121701-13 LCS CVTOC BLANK WTR 6/21/2012 6/21/2012 LEVEL1WG121701-14 SB CVTOC BLANK WTR 6/21/2012 6/21/2012 WG121701-12WG121701-15 LD CVTOC GRND WTR 6/21/2012 6/21/2012 L55828-1WG121701-16 MS CVTOC FRESH WTR 6/21/2012 6/21/2012 L55789-3WG121701-17 MB CVDOC BLANK WTR 6/19/2012 6/21/2012 MB1 120619WG121701-18 LCS CVDOC BLANK WTR 6/21/2012 6/21/2012 LEVEL1WG121701-19 SB CVDOC BLANK WTR 6/19/2012 6/21/2012 WG121701-17WG121701-20 LD CVDOC SALT WTR 6/19/2012 6/21/2012 L55790-2WG121701-21 MS CVDOC FRESH WTR 6/19/2012 6/22/2012 L55789-3WG121701-22 LD CVDOC STORM WTR 6/19/2012 6/22/2012 L55936-2WG121701-23 MS CVDOC STORM WTR 6/19/2012 6/22/2012 L55936-2


Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55698-1 423589-320-4 CSO Basin Study CVTSS SEWER WTR 6/20/2012 6/25/2012 6/25/2012L55828-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 6/19/2012 6/25/2012 6/25/2012L55828-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 6/19/2012 6/25/2012 6/25/2012L55829-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 6/21/2012 6/25/2012 6/25/2012L55830-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 6/21/2012 6/25/2012 6/25/2012L55830-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTSS GRND WTR 6/21/2012 6/25/2012 6/25/2012L55874-2 421879-210 NPDES SW Monitoring CVTSS STORM WTR 6/22/2012 6/25/2012 6/25/2012L55927-1 421422-CHGW-OS SWD-CHGW-OS Cedar Hills Groundwater Off-Site CVTSS GRND WTR 6/20/2012 6/25/2012 6/25/2012L55930-1 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTSS FRESH WTR 6/21/2012 6/25/2012 6/25/2012L55930-3 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTSS FRESH WTR 6/21/2012 6/25/2012 6/25/2012L55930-4 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTSS FRESH WTR 6/21/2012 6/25/2012 6/25/2012WG121711-1 MB CVTSS BLANK WTR 6/25/2012 6/25/2012 MB1 6/25/12WG121711-2 LCS CVTSS BLANK WTR 6/25/2012 6/25/2012 LEVEL1WG121711-3 LD CVTSS GRND WTR 6/25/2012 6/25/2012 L55830-1WG121711-4 LD CVTSS FRESH WTR 6/25/2012 6/25/2012 L55930-1WG121711-5 LD CVTSS SEWER WTR 6/25/2012 6/25/2012 L55698-1

WG121752 (toc,doc) Department: 3 - Conventionals Move Date: 02-JUL-12

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55698-1 423589-320-4 CSO Basin Study CVDOC SEWER WTR 6/20/2012 6/22/2012 6/27/2012L55698-1 423589-320-4 CSO Basin Study CVTOC SEWER WTR 6/20/2012 6/27/2012 6/27/2012L55811-4 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/26/2012 6/27/2012 6/27/2012L55829-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/26/2012 6/27/2012 6/27/2012L55834-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/25/2012 6/27/2012 6/27/2012L55834-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/25/2012 6/27/2012 6/27/2012L55918-1 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/26/2012 6/27/2012 6/27/2012L55918-3 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/26/2012 6/27/2012 6/27/2012L55918-4 421422-PUGW SWD-PUGW Puyallup Groundwater Quarterly CVTOC GRND WTR 6/27/2012 6/27/2012 6/27/2012L55923-2 421422-DUSW SWD-DUSW Duvall Surface Water Quarterly CVTOC FRESH WTR 6/28/2012 6/28/2012 6/28/2012L55930-1 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 6/21/2012 6/27/2012 6/27/2012L55930-3 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 6/21/2012 6/27/2012 6/27/2012L55930-4 421422-VASW-2 SWD-VASW-2 Vashon Surface Water Quarterly CVTOC FRESH WTR 6/21/2012 6/27/2012 6/27/2012WG121752-1 MB CVTOC BLANK WTR 6/27/2012 6/27/2012 MB1 120627WG121752-2 LCS CVTOC BLANK WTR 6/27/2012 6/27/2012 LEVEL1WG121752-3 SB CVTOC BLANK WTR 6/27/2012 6/27/2012 WG121752-1WG121752-4 LD CVTOC FRESH WTR 6/27/2012 6/27/2012 L55930-1WG121752-5 MS CVTOC FRESH WTR 6/27/2012 6/27/2012 L55930-4WG121752-6 LD CVTOC GRND WTR 6/27/2012 6/27/2012 L55918-1WG121752-7 MS CVTOC GRND WTR 6/27/2012 6/27/2012 L55918-4WG121752-8 LD CVTOC SEWER WTR 6/27/2012 6/27/2012 L55698-1WG121752-9 MS CVTOC SEWER WTR 6/27/2012 6/27/2012 L55698-1WG121752-10 MB CVDOC BLANK WTR 6/22/2012 6/27/2012 MB1 120622WG121752-11 LCS CVDOC BLANK WTR 6/27/2012 6/27/2012 LEVEL1WG121752-12 SB CVDOC BLANK WTR 6/22/2012 6/27/2012 WG121752-10WG121752-13 LD CVDOC SEWER WTR 6/22/2012 6/27/2012 L55698-1WG121752-14 MS CVDOC SEWER WTR 6/22/2012 6/27/2012 L55698-1WG121752-15 MB CVTOC BLANK WTR 6/28/2012 6/28/2012 MB1 120628WG121752-16 LCS CVTOC BLANK WTR 6/28/2012 6/28/2012 LEVEL1

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WG119801 (CSO basin, OCS-enum) Department: 6 - Metals Move Date: 21-FEB-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54687-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 1/25/2012 2/15/2012 2/17/2012L54687-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 1/25/2012 2/15/2012 2/17/2012L54687-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 1/25/2012 2/15/2012 2/17/2012L54687-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 1/25/2012 2/15/2012 2/17/2012L54687-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 1/25/2012 2/15/2012 2/17/2012L54687-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 1/25/2012 2/15/2012 2/17/2012L54967-1 421184-110 OCS-City of Enumclaw MTHG-LOW INFLUENT 2/5/2012 2/15/2012 2/17/2012L54967-2 421184-110 OCS-City of Enumclaw MTHG-LOW EFFLUENT 2/5/2012 2/15/2012 2/17/2012WG119801-1 MB MTHG-LOW BLANK WTR 2/15/2012 2/17/2012 METHOD BLANKWG119801-1 MB MTHG-LOW-DISS BLANK WTR 2/15/2012 2/17/2012 METHOD BLANKWG119801-2 SB MTHG-LOW BLANK WTR 2/15/2012 2/17/2012 WG119801-1 HG-LLOWWG119801-3 MS MTHG-LOW EFFLUENT 2/15/2012 2/17/2012 L54967-2 HG-LLOWWG119801-4 MSD MTHG-LOW EFFLUENT 2/15/2012 2/17/2012 WG119801-3 L54967-2 HG-LLOW-MSD

WG120032 (CSO Basin, Aqua Tox) Department: 6 - Metals Move Date: 12-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54687-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 1/25/2012 3/8/2012 3/8/2012L54687-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 1/25/2012 3/8/2012 3/8/2012L54687-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 1/25/2012 3/8/2012 3/8/2012L55011-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55011-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55011-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55012-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 2/15/2012 3/8/2012 3/8/2012L55012-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 2/15/2012 3/8/2012 3/8/2012L55157-1 421190 Accreditation MTICPMS FRESH WTR 2/21/2012 3/8/2012 3/8/2012L55177-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-4 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS STORM WTR 3/5/2012 3/8/2012 3/9/2012L55177-5 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-6 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55186-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/29/2012 3/8/2012 3/8/2012L55186-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/29/2012 3/8/2012 3/8/2012L55186-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 2/29/2012 3/8/2012 3/8/2012L55252-1 421155 Quality Assurance MTICPMS FRESH WTR 3/6/2012 3/8/2012 3/8/2012WG120032-1 MB MTICPMS BLANK WTR 3/8/2012 3/8/2012 METHOD BLANKWG120032-2 SB MTICPMS BLANK WTR 3/8/2012 3/8/2012 WG120032-1 MS-20

LIMSView Batch Report for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Metals

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WG120032-3 LD MTICPMS STORM WTR 3/8/2012 3/8/2012 L54687-3 RPD-LIQWG120032-4 MS MTICPMS STORM WTR 3/8/2012 3/8/2012 L54687-3 MS-20

WG120037 (CSO Basin) Department: 6 - Metals Move Date: 09-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54687-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 1/25/2012 3/8/2012 3/8/2012L54687-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 1/25/2012 3/8/2012 3/8/2012L54687-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 1/25/2012 3/8/2012 3/8/2012L55011-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55011-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55011-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/28/2012 3/8/2012 3/8/2012L55012-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 2/15/2012 3/8/2012 3/8/2012L55012-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 2/15/2012 3/8/2012 3/8/2012L55177-1 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-2 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-4 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-5 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55177-6 423589-330-4 Green Rvr PCB/PAH Loading MTICPMS-DISS STORM WTR 3/5/2012 3/8/2012 3/8/2012L55186-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/29/2012 3/8/2012 3/8/2012L55186-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/29/2012 3/8/2012 3/8/2012L55186-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 2/29/2012 3/8/2012 3/8/2012WG120037-1 MB MTICPMS-DISS BLANK WTR 3/8/2012 3/8/2012 METHOD BLANKWG120037-2 SB MTICPMS-DISS BLANK WTR 3/8/2012 3/8/2012 WG120037-1 MS-20WG120037-3 LD MTICPMS-DISS SEWER WTR 3/8/2012 3/8/2012 L54687-3 RPD-LIQWG120037-4 MS MTICPMS-DISS SEWER WTR 3/8/2012 3/8/2012 L54687-3 MS-20

WG120040 ( CSO Basin) Department: 6 - Metals Move Date: 15-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55011-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/28/2012 3/8/2012 3/9/2012L55011-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/28/2012 3/8/2012 3/9/2012L55011-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/28/2012 3/8/2012 3/9/2012L55012-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 2/15/2012 3/8/2012 3/9/2012L55012-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 2/15/2012 3/8/2012 3/9/2012L55186-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/29/2012 3/8/2012 3/9/2012L55186-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/29/2012 3/8/2012 3/9/2012L55186-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/29/2012 3/8/2012 3/9/2012L55186-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/29/2012 3/8/2012 3/9/2012

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WG120040-1 MB MTHG-LOW BLANK WTR 3/8/2012 3/9/2012 METHOD BLANKWG120040-1 MB MTHG-LOW-DISS BLANK WTR 3/8/2012 3/9/2012 METHOD BLANKWG120040-2 SB MTHG-LOW BLANK WTR 3/8/2012 3/9/2012 WG120040-1 HG-LLOWWG120040-3 MS MTHG-LOW STORM WTR 3/8/2012 3/9/2012 L55186-3 HG-LLOWWG120040-4 MSD MTHG-LOW STORM WTR 3/8/2012 3/9/2012 WG120040-3 L55186-3 HG-LLOW-MSD

WG120057 (CSO Basin) Department: 6 - Metals Move Date: 20-MAR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55011-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/28/2012 3/9/2012 3/12/2012L55011-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/28/2012 3/9/2012 3/12/2012L55011-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/28/2012 3/9/2012 3/12/2012L55012-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 2/15/2012 3/9/2012 3/12/2012L55012-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 2/15/2012 3/9/2012 3/12/2012L55186-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 2/29/2012 3/9/2012 3/12/2012L55186-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 2/29/2012 3/9/2012 3/12/2012WG120057-1 MB MTHG-LOW BLANK WTR 3/9/2012 3/12/2012 METHOD BLANKWG120057-1 MB MTHG-LOW-DISS BLANK WTR 3/9/2012 3/12/2012 METHOD BLANKWG120057-2 SB MTHG-LOW BLANK WTR 3/9/2012 3/12/2012 WG120057-1 HG-LLOWWG120057-3 MS MTHG-LOW STORM WTR 3/9/2012 3/12/2012 L55011-2 HG-LLOWWG120057-4 MSD MTHG-LOW STORM WTR 3/9/2012 3/12/2012 WG120057-3 L55011-2 HG-LLOW-MSD

WG120641 (CSO Basin study) Department: 6 - Metals Move Date: 24-APR-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55154-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 3/26/2012 4/16/2012 4/18/2012L55154-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 3/26/2012 4/16/2012 4/18/2012L55154-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 3/26/2012 4/16/2012 4/18/2012L55154-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 3/26/2012 4/16/2012 4/18/2012L55154-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 3/26/2012 4/16/2012 4/18/2012L55185-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 3/27/2012 4/16/2012 4/18/2012L55185-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 3/27/2012 4/16/2012 4/18/2012L55185-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 3/27/2012 4/16/2012 4/18/2012L55185-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 3/27/2012 4/16/2012 4/18/2012L55185-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 3/27/2012 4/16/2012 4/18/2012L55185-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 3/27/2012 4/16/2012 4/18/2012L55285-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 3/28/2012 4/16/2012 4/18/2012L55285-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 3/28/2012 4/16/2012 4/18/2012L55285-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 3/28/2012 4/16/2012 4/18/2012

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L55285-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 3/28/2012 4/16/2012 4/18/2012WG120641-1 MB MTHG-LOW BLANK WTR 4/16/2012 4/18/2012 METHOD BLANKWG120641-1 MB MTHG-LOW-DISS BLANK WTR 4/16/2012 4/19/2012 METHOD BLANKWG120641-2 SB MTHG-LOW BLANK WTR 4/16/2012 4/18/2012 WG120641-1 HG-LLOWWG120641-3 MS MTHG-LOW-DISS STORM WTR 4/16/2012 4/18/2012 L55285-2 HG-LLOWWG120641-4 MSD MTHG-LOW-DISS STORM WTR 4/16/2012 4/18/2012 WG120641-3 L55285-2 HG-LLOW-MSD

WG120674 (CSO Basin Study) Department: 6 - Metals Move Date: 25-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55183-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55183-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55183-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55183-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55183-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55183-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/9/2012 4/17/2012 4/19/2012L55184-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/10/2012 4/17/2012 4/19/2012L55184-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/10/2012 4/17/2012 4/19/2012L55184-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/10/2012 4/17/2012 4/19/2012L55184-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/10/2012 4/17/2012 4/19/2012L55184-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/10/2012 4/17/2012 4/19/2012L55433-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/11/2012 4/17/2012 4/19/2012L55433-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/11/2012 4/17/2012 4/19/2012L55433-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/11/2012 4/17/2012 4/19/2012L55433-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/11/2012 4/17/2012 4/19/2012L55433-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/11/2012 4/17/2012 4/19/2012L55433-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/11/2012 4/17/2012 4/19/2012WG120674-1 MB MTHG-LOW BLANK WTR 4/17/2012 4/19/2012 METHOD BLANKWG120674-1 MB MTHG-LOW-DISS BLANK WTR 4/17/2012 4/19/2012 METHOD BLANKWG120674-2 SB MTHG-LOW BLANK WTR 4/17/2012 4/19/2012 WG120674-1 HG-LLOWWG120674-3 MS MTHG-LOW STORM WTR 4/17/2012 4/19/2012 L55433-2 HG-LLOWWG120674-4 MSD MTHG-LOW STORM WTR 4/17/2012 4/19/2012 WG120674-3 L55433-2 HG-LLOW-MSD

WG120847 (CSO Basin Diss) Department: 6 - Metals Move Date: 11-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55154-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 3/26/2012 4/27/2012 4/27/2012L55154-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 3/26/2012 4/27/2012 4/27/2012L55183-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/9/2012 4/27/2012 4/27/2012

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L55183-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/9/2012 4/27/2012 4/27/2012L55183-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/9/2012 4/27/2012 4/27/2012L55184-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/10/2012 4/27/2012 4/27/2012L55184-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/10/2012 4/27/2012 4/27/2012L55185-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 3/27/2012 4/27/2012 4/27/2012L55185-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 3/27/2012 4/27/2012 4/27/2012L55185-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 3/27/2012 4/27/2012 4/27/2012L55285-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 3/28/2012 4/27/2012 4/27/2012L55285-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 3/28/2012 4/27/2012 4/27/2012L55433-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/11/2012 4/27/2012 4/27/2012L55433-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/11/2012 4/27/2012 4/27/2012L55433-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/11/2012 4/27/2012 4/27/2012L55511-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/23/2012 4/27/2012 4/27/2012L55511-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/23/2012 4/27/2012 4/27/2012L55511-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 4/23/2012 4/27/2012 4/27/2012L55512-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/24/2012 4/27/2012 4/27/2012L55512-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/24/2012 4/27/2012 4/27/2012WG120847-1 MB MTICPMS-DISS BLANK WTR 4/27/2012 4/27/2012 METHOD BLANKWG120847-2 SB MTICPMS-DISS BLANK WTR 4/27/2012 4/27/2012 WG120847-1 MS-20WG120847-3 LD MTICPMS-DISS STORM WTR 4/27/2012 4/27/2012 L55285-2 RPD-LIQWG120847-4 MS MTICPMS-DISS STORM WTR 4/27/2012 4/27/2012 L55285-2 MS-20

WG120860 (CSO Totals) Department: 6 - Metals Move Date: 11-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55154-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 3/26/2012 4/27/2012 4/30/2012L55154-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 3/26/2012 4/27/2012 4/30/2012L55154-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 3/26/2012 4/27/2012 4/30/2012L55183-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/9/2012 4/27/2012 4/30/2012L55183-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/9/2012 4/27/2012 4/30/2012L55183-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/9/2012 4/27/2012 4/30/2012L55184-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/10/2012 4/27/2012 4/30/2012L55184-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/10/2012 4/27/2012 4/30/2012L55184-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/10/2012 4/27/2012 4/30/2012L55185-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 3/27/2012 4/27/2012 4/30/2012L55185-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 3/27/2012 4/27/2012 4/30/2012L55185-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 3/27/2012 4/27/2012 4/30/2012L55285-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 3/28/2012 4/27/2012 4/30/2012L55285-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 3/28/2012 4/27/2012 4/30/2012L55433-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/11/2012 4/27/2012 4/30/2012

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L55433-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/11/2012 4/27/2012 4/30/2012L55433-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/11/2012 4/27/2012 4/30/2012L55584-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/25/2012 4/27/2012 4/30/2012L55584-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/25/2012 4/27/2012 4/30/2012L55584-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/25/2012 4/27/2012 4/30/2012WG120860-1 MB MTICPMS BLANK WTR 4/27/2012 4/30/2012 METHOD BLANKWG120860-2 SB MTICPMS BLANK WTR 4/27/2012 4/30/2012 WG120860-1 MS-20WG120860-3 LD MTICPMS STORM WTR 4/27/2012 4/30/2012 L55285-3 RPD-LIQWG120860-4 MS MTICPMS STORM WTR 4/27/2012 4/30/2012 L55285-3 MS-20

WG120894 (cso basin Sewer, strom wa) Department: 6 - Metals Move Date: 09-MAY-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55511-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55511-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55511-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55511-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55511-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55511-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 4/23/2012 5/3/2012 5/7/2012L55512-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/24/2012 5/3/2012 5/7/2012L55512-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/24/2012 5/3/2012 5/7/2012L55512-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/24/2012 5/3/2012 5/7/2012L55512-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/24/2012 5/3/2012 5/7/2012L55512-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/24/2012 5/3/2012 5/7/2012L55512-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/24/2012 5/3/2012 5/7/2012L55584-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/25/2012 5/3/2012 5/7/2012L55584-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/25/2012 5/3/2012 5/7/2012L55584-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/25/2012 5/3/2012 5/7/2012L55584-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/25/2012 5/3/2012 5/7/2012L55584-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 4/25/2012 5/3/2012 5/7/2012L55584-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 4/25/2012 5/3/2012 5/7/2012WG120894-1 MB MTHG-LOW BLANK WTR 5/3/2012 5/7/2012 METHOD BLANKWG120894-1 MB MTHG-LOW-DISS BLANK WTR 5/3/2012 5/7/2012 METHOD BLANKWG120894-2 SB MTHG-LOW BLANK WTR 5/3/2012 5/7/2012 WG120894-1 HG-LLOWWG120894-3 MS MTHG-LOW-DISS STORM WTR 5/3/2012 5/7/2012 L55584-3 HG-LLOWWG120894-4 MSD MTHG-LOW-DISS STORM WTR 5/3/2012 5/7/2012 WG120894-3 L55584-3 HG-LLOW-MSD

WG121053 (cso basin, RTP inplant) Department: 6 - Metals Move Date: 17-MAY-12

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55572-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 5/7/2012 5/14/2012 5/15/2012L55572-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 5/7/2012 5/14/2012 5/15/2012L55572-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 5/7/2012 5/14/2012 5/15/2012L55572-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 5/7/2012 5/14/2012 5/15/2012L55585-3 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTHG-LOW EFFLUENT 5/2/2012 5/14/2012 5/15/2012L55645-2 421186B RTP INPLNT 3 DAY INT (inf,eff,sl) MTHG-LOW EFFLUENT 5/3/2012 5/14/2012 5/15/2012L55686-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 5/8/2012 5/14/2012 5/15/2012L55686-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 5/8/2012 5/14/2012 5/15/2012L55686-2 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 5/8/2012 5/14/2012 5/15/2012L55686-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 5/8/2012 5/14/2012 5/15/2012L55686-3 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 5/8/2012 5/14/2012 5/15/2012L55686-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 5/8/2012 5/14/2012 5/15/2012WG121053-1 MB MTHG-LOW BLANK WTR 5/14/2012 5/15/2012 METHOD BLANKWG121053-1 MB MTHG-LOW-DISS BLANK WTR 5/14/2012 5/15/2012 METHOD BLANKWG121053-2 SB MTHG-LOW BLANK WTR 5/14/2012 5/15/2012 WG121053-1 HG-LLOWWG121053-3 MS MTHG-LOW EFFLUENT 5/14/2012 5/15/2012 L55645-2 HG-LLOWWG121053-4 MSD MTHG-LOW EFFLUENT 5/14/2012 5/15/2012 WG121053-3 L55645-2 HG-LLOW-MSD

WG121194 (5/23/12 CSO Basin Totals) Department: 6 - Metals Move Date: 06-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55511-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/23/2012 5/23/2012 5/24/2012L55511-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/23/2012 5/23/2012 5/24/2012L55511-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 4/23/2012 5/23/2012 5/24/2012L55512-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/24/2012 5/23/2012 5/24/2012L55512-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/24/2012 5/23/2012 5/24/2012L55512-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 4/24/2012 5/23/2012 5/24/2012L55572-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 5/7/2012 5/23/2012 5/24/2012L55572-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 5/7/2012 5/23/2012 5/24/2012L55638-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/21/2012 5/23/2012 5/24/2012L55638-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/21/2012 5/23/2012 5/24/2012L55638-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/21/2012 5/23/2012 5/24/2012L55686-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 5/8/2012 5/23/2012 5/24/2012L55686-2 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 5/8/2012 5/23/2012 5/24/2012L55686-3 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 5/8/2012 5/23/2012 5/24/2012L55763-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/22/2012 5/23/2012 5/24/2012L55763-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/22/2012 5/23/2012 5/24/2012L55763-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 5/22/2012 5/23/2012 5/24/2012WG121194-1 MB MTICPMS BLANK WTR 5/23/2012 5/24/2012 METHOD BLANK

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WG121194-2 SB MTICPMS BLANK WTR 5/23/2012 5/24/2012 WG121194-1 MS-20WG121194-3 LD MTICPMS STORM WTR 5/23/2012 5/24/2012 L55638-1 RPD-LIQWG121194-4 MS MTICPMS STORM WTR 5/23/2012 5/24/2012 L55638-1 MS-20

WG121302 (5/31/12 CSO Basin Dissolv) Department: 6 - Metals Move Date: 06-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55512-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/24/2012 5/31/2012 6/4/2012L55572-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 5/7/2012 5/31/2012 6/4/2012L55572-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 5/7/2012 5/31/2012 6/4/2012L55584-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/25/2012 5/31/2012 6/4/2012L55584-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/25/2012 5/31/2012 6/4/2012L55584-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 4/25/2012 5/31/2012 6/4/2012L55638-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/21/2012 5/31/2012 6/4/2012L55638-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/21/2012 5/31/2012 6/4/2012L55638-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/21/2012 5/31/2012 6/4/2012L55686-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 5/8/2012 5/31/2012 6/4/2012L55686-2 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 5/8/2012 5/31/2012 6/4/2012L55686-3 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 5/8/2012 5/31/2012 6/4/2012L55763-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/22/2012 5/31/2012 6/4/2012L55763-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/22/2012 5/31/2012 6/4/2012L55763-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 5/22/2012 5/31/2012 6/4/2012WG121302-1 MB MTICPMS-DISS BLANK WTR 5/31/2012 6/4/2012 METHOD BLANKWG121302-2 SB MTICPMS-DISS BLANK WTR 5/31/2012 6/4/2012 WG121302-1 MS-20WG121302-3 LD MTICPMS-DISS SEWER WTR 5/31/2012 6/4/2012 L55572-3 RPD-LIQWG121302-4 MS MTICPMS-DISS SEWER WTR 5/31/2012 6/4/2012 L55572-3 MS-20

WG121351 (CSO Basin study) Department: 6 - Metals Move Date: 18-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55638-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/21/2012 6/4/2012 6/5/2012L55638-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/21/2012 6/4/2012 6/5/2012L55638-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/21/2012 6/4/2012 6/5/2012L55638-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/21/2012 6/4/2012 6/5/2012L55638-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/21/2012 6/4/2012 6/5/2012L55638-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/21/2012 6/4/2012 6/5/2012L55763-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/22/2012 6/4/2012 6/5/2012L55763-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/22/2012 6/4/2012 6/5/2012L55763-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/22/2012 6/4/2012 6/5/2012

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L55763-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/22/2012 6/4/2012 6/5/2012L55763-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 5/22/2012 6/4/2012 6/5/2012L55763-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 5/22/2012 6/4/2012 6/5/2012WG121351-1 MB MTHG-LOW BLANK WTR 6/4/2012 6/5/2012 METHOD BLANKWG121351-1 MB MTHG-LOW-DISS BLANK WTR 6/4/2012 6/5/2012 METHOD BLANKWG121351-2 SB MTHG-LOW BLANK WTR 6/4/2012 6/5/2012 WG121351-1 HG-LLOWWG121351-3 MS MTHG-LOW-DISS STORM WTR 6/4/2012 6/5/2012 L55763-3 HG-LLOWWG121351-4 MSD MTHG-LOW-DISS STORM WTR 6/4/2012 6/5/2012 WG121351-3 L55763-3 HG-LLOW-MSD

WG121500 (CSO Basin Study) Department: 6 - Metals Move Date: 21-JUN-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55764-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/4/2012 6/13/2012 6/15/2012L55764-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/4/2012 6/13/2012 6/15/2012L55764-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/4/2012 6/13/2012 6/15/2012L55764-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/4/2012 6/13/2012 6/15/2012L55764-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/4/2012 6/13/2012 6/15/2012L55764-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/4/2012 6/13/2012 6/15/2012L55859-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/5/2012 6/13/2012 6/15/2012L55859-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/5/2012 6/13/2012 6/15/2012L55859-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/5/2012 6/13/2012 6/15/2012L55859-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/5/2012 6/13/2012 6/15/2012L55875-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/6/2012 6/13/2012 6/15/2012L55875-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/6/2012 6/13/2012 6/15/2012L55875-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/6/2012 6/13/2012 6/15/2012L55875-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/6/2012 6/13/2012 6/15/2012L55876-1 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/7/2012 6/13/2012 6/15/2012L55876-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/7/2012 6/13/2012 6/15/2012L55876-3 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/7/2012 6/13/2012 6/15/2012L55876-3 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/7/2012 6/13/2012 6/15/2012WG121500-1 MB MTHG-LOW BLANK WTR 6/13/2012 6/15/2012 METHOD BLANKWG121500-1 MB MTHG-LOW-DISS BLANK WTR 6/13/2012 6/15/2012 METHOD BLANKWG121500-2 SB MTHG-LOW BLANK WTR 6/13/2012 6/15/2012 WG121500-1 HG-LLOWWG121500-3 MS MTHG-LOW STORM WTR 6/13/2012 6/15/2012 L55859-3 HG-LLOWWG121500-4 MSD MTHG-LOW STORM WTR 6/13/2012 6/15/2012 WG121500-3 L55859-3 HG-LLOW-MSD

WG121764 (CSO Basin) Department: 6 - Metals Move Date: 03-JUL-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date Comments

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L55698-1 423589-320-4 CSO Basin Study MTHG-LOW SEWER WTR 6/20/2012 6/27/2012 6/28/2012L55698-1 423589-320-4 CSO Basin Study MTHG-LOW-DISS SEWER WTR 6/20/2012 6/27/2012 6/28/2012L55936-2 423589-320-4 CSO Basin Study MTHG-LOW STORM WTR 6/18/2012 6/27/2012 6/28/2012L55936-2 423589-320-4 CSO Basin Study MTHG-LOW-DISS STORM WTR 6/18/2012 6/27/2012 6/28/2012WG121764-1 MB MTHG-LOW BLANK WTR 6/27/2012 6/28/2012 METHOD BLANKWG121764-1 MB MTHG-LOW-DISS BLANK WTR 6/27/2012 6/28/2012 METHOD BLANKWG121764-2 SB MTHG-LOW BLANK WTR 6/27/2012 6/28/2012 WG121764-1 HG-LLOWWG121764-3 MS MTHG-LOW-DISS STORM WTR 6/27/2012 6/28/2012 L55936-2 HG-LLOWWG121764-4 MSD MTHG-LOW-DISS STORM WTR 6/27/2012 6/28/2012 WG121764-3 L55936-2 HG-LLOW-MSD

WG121947 (7/10/12 CSO Basin Study T) Department: 6 - Metals Move Date: 19-JUL-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55698-1 423589-320-4 CSO Basin Study MTICPMS SEWER WTR 6/20/2012 7/10/2012 7/11/2012L55764-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/4/2012 7/10/2012 7/11/2012L55764-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/4/2012 7/10/2012 7/11/2012L55764-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/4/2012 7/10/2012 7/11/2012L55859-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/5/2012 7/10/2012 7/11/2012L55859-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/5/2012 7/10/2012 7/11/2012L55875-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/6/2012 7/10/2012 7/11/2012L55875-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/6/2012 7/10/2012 7/11/2012L55876-1 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/7/2012 7/10/2012 7/11/2012L55876-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/7/2012 7/10/2012 7/11/2012L55876-3 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/7/2012 7/10/2012 7/11/2012L55936-2 423589-320-4 CSO Basin Study MTICPMS STORM WTR 6/18/2012 7/10/2012 7/11/2012WG121947-1 MB MTICPMS BLANK WTR 7/10/2012 7/11/2012 METHOD BLANKWG121947-2 SB MTICPMS BLANK WTR 7/10/2012 7/11/2012 WG121947-1 MS-20WG121947-3 LD MTICPMS STORM WTR 7/10/2012 7/11/2012 L55875-3 RPD-LIQWG121947-4 MS MTICPMS STORM WTR 7/10/2012 7/11/2012 L55875-3 MS-20

WG121990 (7/12/12 CSO Basin Diss) Department: 6 - Metals Move Date: 19-JUL-12

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55698-1 423589-320-4 CSO Basin Study MTICPMS-DISS SEWER WTR 6/20/2012 7/12/2012 7/12/2012L55764-1 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/4/2012 7/12/2012 7/12/2012L55764-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/4/2012 7/12/2012 7/12/2012L55764-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/4/2012 7/12/2012 7/12/2012L55859-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/5/2012 7/12/2012 7/12/2012L55859-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/5/2012 7/12/2012 7/12/2012

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L55875-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/6/2012 7/12/2012 7/12/2012L55875-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/6/2012 7/12/2012 7/12/2012L55876-3 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/7/2012 7/12/2012 7/12/2012L55936-2 423589-320-4 CSO Basin Study MTICPMS-DISS STORM WTR 6/18/2012 7/12/2012 7/12/2012WG121990-1 MB MTICPMS-DISS BLANK WTR 7/12/2012 7/12/2012 METHOD BLANKWG121990-2 SB MTICPMS-DISS BLANK WTR 7/12/2012 7/12/2012 WG121990-1 MS-20WG121990-3 LD MTICPMS-DISS STORM WTR 7/12/2012 7/12/2012 L55876-3 RPD-LIQWG121990-4 MS MTICPMS-DISS STORM WTR 7/12/2012 7/12/2012 L55876-3 MS-20

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WG119537 (pahll#008 pah-lvi) Department: 7 - Organics Move Date: 04-FEB-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL54687-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 1/25/2012 1/30/2012 3/7/2012L54687-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 1/25/2012 1/30/2012 3/7/2012L54687-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 1/25/2012 1/30/2012 3/7/2012WG119537-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 1/30/2012 3/7/2012 MB120130WG119537-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 1/30/2012 3/7/2012 WG119537-1WG119537-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 1/30/2012 3/7/2012 WG119537-2 WG119537-1WG119537-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 1/30/2012 3/7/2012 L54687-1

WG119848 (pahll#010 pahph-lvi) Department: 7 - Organics Move Date: 04-FEB-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55012-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 2/15/2012 2/22/2012 3/7/2012L55012-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 2/15/2012 2/22/2012 3/7/2012WG119848-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 2/22/2012 3/7/2012 MB120222WG119848-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 2/22/2012 3/7/2012 WG119848-1WG119848-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 2/22/2012 3/7/2012 WG119848-2 WG119848-1WG119848-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 2/22/2012 3/7/2012 L55012-3

WG119973 (pahll#012 PAH-LVI) Department: 7 - Organics Move Date: 29-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55011-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/28/2012 3/5/2012 3/9/2012L55011-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/28/2012 3/5/2012 3/9/2012L55011-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/28/2012 3/5/2012 3/9/2012L55186-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/29/2012 3/5/2012 3/9/2012L55186-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/29/2012 3/5/2012 3/9/2012L55186-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 2/29/2012 3/5/2012 3/9/2012WG119973-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 3/5/2012 3/9/2012 MB120305WG119973-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 3/5/2012 3/9/2012 WG119973-1WG119973-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 3/5/2012 3/9/2012 WG119973-2 WG119973-1WG119973-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 3/5/2012 3/9/2012 L55186-3

WG120438 (pahll#015 pah-lvi) Department: 7 - Organics Move Date: 29-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date Comments

LIMSView Batch Report for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Organics

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L55154-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 3/26/2012 4/2/2012 4/16/2012L55154-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 3/26/2012 4/2/2012 4/16/2012L55154-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 3/26/2012 4/2/2012 4/16/2012L55185-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 3/27/2012 4/2/2012 4/16/2012L55185-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 3/27/2012 4/2/2012 4/16/2012L55185-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 3/27/2012 4/2/2012 4/16/2012L55285-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 3/28/2012 4/2/2012 4/12/2012L55285-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 3/28/2012 4/2/2012 4/13/2012WG120438-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/2/2012 4/12/2012 MB120402WG120438-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/2/2012 4/12/2012 WG120438-1WG120438-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/2/2012 4/12/2012 WG120438-2 WG120438-1WG120438-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 4/2/2012 4/16/2012 L55185-2

WG120555 (pahll#015 pahphth-sim-lvi) Department: 7 - Organics Move Date: 29-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55183-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/9/2012 4/11/2012 4/17/2012L55183-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/9/2012 4/11/2012 4/17/2012L55183-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/9/2012 4/11/2012 4/17/2012WG120438-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/2/2012 4/12/2012 WG120438-1WG120438-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/2/2012 4/12/2012 WG120438-2 WG120438-1WG120555-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/11/2012 4/16/2012 MB120410WG120555-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/11/2012 4/16/2012 WG120555-1

WG120654 (pahll#017) Department: 7 - Organics Move Date: 29-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55184-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/10/2012 4/17/2012 4/25/2012L55184-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/10/2012 4/17/2012 4/25/2012L55433-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/11/2012 4/17/2012 4/25/2012L55433-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/11/2012 4/17/2012 4/25/2012L55433-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/11/2012 4/17/2012 4/25/2012WG120654-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/17/2012 4/25/2012 MB120417WG120654-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/17/2012 4/25/2012 WG120654-1WG120654-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/17/2012 4/25/2012 WG120654-2 WG120654-1WG120654-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 4/17/2012 4/25/2012 L55433-1

WG120867 (pahll#018) Department: 7 - Organics Move Date: 30-JAN-15

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Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55511-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/23/2012 4/30/2012 5/9/2012L55511-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/23/2012 4/30/2012 5/9/2012L55511-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/23/2012 4/30/2012 5/9/2012L55512-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/24/2012 4/30/2012 5/9/2012L55512-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/24/2012 4/30/2012 5/9/2012L55512-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/24/2012 4/30/2012 5/9/2012L55584-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/25/2012 4/30/2012 5/9/2012L55584-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/25/2012 4/30/2012 5/9/2012L55584-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 4/25/2012 4/30/2012 5/9/2012WG120867-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/30/2012 5/9/2012 MB120430WG120867-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/30/2012 5/9/2012 WG120867-1WG120867-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 4/30/2012 5/9/2012 WG120867-2 WG120867-1WG120867-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 4/30/2012 5/9/2012 L55511-3

WG121052 (pahll#019 pahphth-sim-lvi) Department: 7 - Organics Move Date: 30-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55572-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/7/2012 5/14/2012 6/1/2012L55572-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/7/2012 5/14/2012 6/1/2012L55686-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/8/2012 5/14/2012 6/1/2012L55686-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/8/2012 5/14/2012 6/1/2012L55686-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/8/2012 5/14/2012 6/1/2012WG121052-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/14/2012 6/1/2012 MB120514WG121052-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/14/2012 6/1/2012 WG121052-1WG121052-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/14/2012 6/1/2012 WG121052-2 WG121052-1WG121052-4 LD ORPAHPHTH-SIM-LVI-LL SEWER WTR 5/14/2012 6/1/2012 L55572-3

WG121217 (pahll#020 pahphth) Department: 7 - Organics Move Date: 30-JAN-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55638-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/21/2012 5/24/2012 6/22/2012L55638-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/21/2012 5/24/2012 6/22/2012L55638-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/21/2012 5/24/2012 6/22/2012L55763-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/22/2012 5/24/2012 6/22/2012L55763-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/22/2012 5/24/2012 6/22/2012L55763-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 5/22/2012 5/24/2012 6/22/2012WG121217-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/24/2012 6/22/2012 MB120524

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WG121217-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/24/2012 6/22/2012 WG121217-1WG121217-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 5/24/2012 6/22/2012 WG121217-2 WG121217-1WG121217-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 5/24/2012 6/22/2012 L55638-1

WG121458 (pahll#021 pah-lvi) Department: 7 - Organics Move Date: 03-FEB-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55764-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/4/2012 6/11/2012 7/21/2012L55764-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/4/2012 6/11/2012 7/21/2012L55764-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/4/2012 6/11/2012 7/21/2012L55859-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/5/2012 6/11/2012 7/21/2012L55859-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/5/2012 6/11/2012 7/21/2012L55875-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/6/2012 6/11/2012 7/21/2012L55875-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/6/2012 6/11/2012 7/21/2012L55876-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/7/2012 6/11/2012 7/21/2012L55876-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/7/2012 6/11/2012 7/21/2012L55876-3 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/7/2012 6/11/2012 7/21/2012WG121458-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/11/2012 7/21/2012 MB120611WG121458-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/11/2012 7/21/2012 WG121458-1WG121458-3 SBD ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/11/2012 7/21/2012 WG121458-2 WG121458-1WG121458-4 LD ORPAHPHTH-SIM-LVI-LL STORM WTR 6/11/2012 7/21/2012 L55764-2

WG121670 (pahll#022 pahphth-sim-lvi) Department: 7 - Organics Move Date: 04-FEB-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55936-2 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL STORM WTR 6/18/2012 6/21/2012 7/23/2012WG121670-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/21/2012 7/23/2012 MB120621WG121670-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/21/2012 7/23/2012 WG121670-1WG121670-3 MS ORPAHPHTH-SIM-LVI-LL STORM WTR 6/21/2012 7/23/2012 L55936-2WG121670-4 MSD ORPAHPHTH-SIM-LVI-LL STORM WTR 6/21/2012 7/23/2012 WG121670-3 L55936-2

WG121757 (pahll#023 pahphth-sim-lvi) Department: 7 - Organics Move Date: 04-FEB-15

Sample Project Project Description List Type Matrix Collect Date Prep Date Anal Date CommentsL55698-1 423589-320-4 CSO Basin Study ORPAHPHTH-SIM-LVI-LL SEWER WTR 6/20/2012 6/27/2012 7/23/2012WG121757-1 MB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/27/2012 7/23/2012 MB120627WG121757-2 SB ORPAHPHTH-SIM-LVI-LL BLANK WTR 6/27/2012 7/23/2012 WG121757-1WG121757-3 MS ORPAHPHTH-SIM-LVI-LL SEWER WTR 6/27/2012 7/23/2012 L55698-1WG121757-4 MSD ORPAHPHTH-SIM-LVI-LL SEWER WTR 6/27/2012 7/23/2012 WG121757-3 L55698-1

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Workgroup: WG119517 TSS Run ID: R171039



LD:WG119517-3 L54843-2 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:421250OS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L <MDL <MDL 0--25



LD:WG119517-6 L54843-23 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:421250OS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L 1.2 1.6 0--25

LD:WG119517-7 L54924-5 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L <MDL <MDL 0--25



LD:WG119517-10 L54928-4 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 6 5.8 3 0--25

LD:WG119517-11 L54687-2 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 5 10 mg/L 195 202 4 0--25

LIMSView QC Report for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Conventionals

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Workgroup: WG119562 toc/doc Run ID: R171085







LD:WG119562-7 L54687-1 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 2.5 5 mg/L 68.2 65.3 4 0--20

MS:WG119562-8 L54687-3 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 2.5 5 mg/L 17 10 78.3 123 75--125

LD:WG119562-9 L54959-5 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.22 1.01 19 0--20

MB:WG119562-10 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Method Blank)

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Parameter MDL RDL Units MB Value QualDissolved Organic Carbon 0.5 1 mg/L <MDL



MS:WG119562-13 L54687-3 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 7.05 10 16.8 97 75--125


LD:WG119562-15 L54687-1 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 1 2 mg/L 47.9 47.3 1 0--20







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LD:WG119808-4 L55035-5 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 2.8 2.4 15 0--25

LD:WG119808-5 L55037-12 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.2 1.2 0--25



LCS:WG119910-2 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 10 10 100 85--115



MS:WG119910-5 L55012-3 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 2.5 5 mg/L 27.9 10 79.5 103 75--125


LD:WG119910-7 L55115-4 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

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Dissolved Organic Carbon 0.5 1 mg/L 4.11 4.33 5 0--20

MS:WG119910-8 L55115-9 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:422027 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 7.78 10 18 103 75--125


MS:WG119910-10 L55088-3 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 2.37 10 12.1 97 75--125



LCS:WG119910-13 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10 100 85--115



LD:WG119910-16 L54953-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHSW-A5-TD Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 11.5 12.2 6 0--20

MS:WG119910-17 L55037-7 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHSW-M Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 3.46 10 13.9 105 75--125


6 of 42





LD:WG119910-22 L55037-4 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 4.44 4.34 2 0--20


LD:WG119910-24 L55057-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-ENGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.94 0.93 0--20

MS:WG119910-25 L55020-4 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-ENGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.22 10 11.8 106 75--125

MS:WG119910-26 L55088-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.7 10 12.7 100 75--125


LD:WG119910-28 L55115-4 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 2.5 5 mg/L 15.5 17 10 0--20


7 of 42



MS:WG119910-31 L55115-9 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:422027 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 2.5 5 mg/L 47.3 10 103 111 75--125







MS:WG119964-5 L55077-2 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 5.19 10 15.3 101 75--125

LD:WG119964-6 L55035-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CFGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.1 1 10 0--20

MS:WG119964-7 L55062-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HOGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.76 10 11.2 104 75--125

MB:WG119964-8 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value Qual

8 of 42


Dissolved Organic Carbon 0.5 1 mg/L <MDL




LD:WG119964-12 L55077-1 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-330-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 6.89 6.77 2 0--20








9 of 42





LD:WG119972-3 L55139-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-VAGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 12 11.8 2 0--25


LD:WG119972-5 L55112-8 Matrix: IW WTR Listtype:CVTSS Method:SM2540-D Project:421161 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 10 20 mg/L 378 386 2 0--25





LD:WG120092-4 L55139-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-VAGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.73 2.84 4 0--20

MS:WG120092-5 L55214-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CFGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.89 10 11.3 104 75--125

10 of 42


MS:WG120092-6 L55186-3 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 1 2 mg/L 28.3 10 52.6 122 75--125



LD:WG120092-9 L55210-2 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421195-190 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 5.56 5.82 5 0--20

MS:WG120092-10 L55210-4 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421195-190 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 6.77 10 14.8 81 75--125







11 of 42




MS:WG120092-19 L55210-4 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:421195-190 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 4.02 10 14.8 108 75--125



LD:WG120092-22 L55186-1 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 15 30 mg/L 503 539 7 0--20




LD:WG120350-3 L54930-4 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421874-100 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 9.4 9 4 0--25


LD:WG120350-5 L55358-2 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-HTGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

12 of 42


Total Suspended Solids 1 2 mg/L 1.4 1.6 0--25

LD:WG120350-6 L55043-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CFSW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 92.2 109 16 0--25

Workgroup: WG120382 toc,doc Run ID: R176013










LCS:WG120382-10 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD

13 of 42


(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 9.43 94 85--115


MS:WG120382-12 L55043-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CFSW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.85 10 11.8 109 75--125

LD:WG120382-13 L55274-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 3.68 3.99 8 0--20








LCS:WG120382-21 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)

14 of 42


Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 10 10.5 105 85--115





LD:WG120382-26 L55043-1 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-CFSW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.08 6.8 106 * 0--20







15 of 42


LD:WG120479-4 L54893-1 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:421185 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 101 109 7 0--25

LD:WG120479-5 L55085-9 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:421195-180 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 17 18.4 8 0--25

LD:WG120479-6 L55391-1 Matrix: STORM WTR Listtype:CVTSS Method:SM2540-D Project:422027 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 35.4 35 1 0--25






LD:WG120560-5 L55356-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-VASW-2 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 40.4 35 14 0--20



MB:WG120560-8 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value Qual

16 of 42


Total Organic Carbon 0.5 1 mg/L <MDL








MS:WG120560-16 L55356-6 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-VASW-2 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 21.5 10 61.7 80 75--125




17 of 42



MS:WG120560-21 L55381-3 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:421195-190 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 5.76 10 14.9 91 75--125







LD:WG120560-28 L55185-2 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 2.5 5 mg/L 91.3 90 1 0--20



18 of 42










LD:WG120560-39 L55399-1 Matrix: LEACHATE Listtype:CVTOC Method:SM5310-B Project:421422-VALS-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 7.31 6.83 7 0--20

MS:WG120560-40 L55400-5 Matrix: LEACHATE Listtype:CVTOC Method:SM5310-B Project:421422-CHLS-M Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 18 35 mg/L 439 10 747 88 75--125



19 of 42




LD:WG120569-3 L55462-11 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.4 1.6 0--25






LD:WG120569-9 L55462-48 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 6 6.2 3 0--25

LD:WG120569-10 L54976-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421195-140 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L <MDL <MDL 0--25

LD:WG120569-11 L55435-1 Matrix: IW WTR Listtype:CVTSS Method:SM2540-D Project:421422-ENLS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 10 20 mg/L 86 90 5 0--25


20 of 42





LD:WG120580-3 L55436-6 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 20 40 mg/L 308 304 1 0--25





LD:WG120684-3 L55471-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 6.4 6 6 0--25

LD:WG120684-4 L55440-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-Q Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 28 27.6 1 0--25



21 of 42







LD:WG120818-3 L55526-10 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.8 1.6 0--25



LD:WG120818-6 L55526-26 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L <MDL 1.2 0--25



LD:WG120818-9 L55526-49 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421235 Pkey:STD(Lab Duplicate)

22 of 42


Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 9.2 9.2 0 0--25

LD:WG120818-10 L55151-5 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421874-100 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2.1 mg/L 1.5 1.9 0--25


Workgroup: WG120836 TOC,DOC Run ID: R177335









23 of 42









MS:WG120836-16 L55433-3 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 18 35 mg/L 171 10 506 96 75--125




MS:WG120836-20 L55371-3 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD

24 of 42


(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.63 10 11.9 102 75--125



LD:WG120836-23 L55433-1 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 18 35 mg/L 228 226 1 0--20

MS:WG120836-24 L55433-3 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 18 35 mg/L 41.4 10 384 98 75--125







MB:WG120836-31 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Method Blank)

25 of 42


Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL







LD:WG120836-38 L55493-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CHGW-NP Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.74 2.31 17 0--20





26 of 42


LD:WG120873-3 L55478-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 5.6 5.4 4 0--25

LD:WG120873-4 L55588-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 2.4 3 22 0--25





LD:WG121035-3 L55639-11 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421240A Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 2.2 2 10 0--25



LD:WG121035-6 L55641-3 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421195-190 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 5 5 0 0--25



27 of 42






MS:WG121155-5 L55641-4 Matrix: FRESH WTR Listtype:CVDOC Method:SM5310-B Project:421195-190 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 4.46 10 15 105 75--125







MB:WG121155-12 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD

28 of 42


(Method Blank)Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL





LD:WG121155-17 L55605-1 Matrix: LEACHATE Listtype:CVTOC Method:SM5310-B Project:421422-CHLS-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 18 35 mg/L 152 141 7 0--20


LD:WG121155-19 L55618-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-CFGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.56 0.54 0--20

MS:WG121155-20 L55622-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-ENGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 4.64 10 15.5 109 75--125



MB:WG121155-23 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Method Blank)

29 of 42


Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL







LD:WG121213-4 L55671-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HOGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.83 0.73 0--20

MS:WG121213-5 L55671-5 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HOGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.87 10 10.9 100 75--125




30 of 42





MS:WG121213-12 L55537-2 Matrix: SALT WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 2.08 10 11.9 98 75--125

LD:WG121213-13 L55638-2 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 18 35 mg/L 47.9 45.1 6 0--20






MS:WG121213-19 L55537-2 Matrix: SALT WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.64 10 12.7 111 75--125

MB:WG121213-20 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD

31 of 42


(Method Blank)Parameter MDL RDL Units MB Value QualDissolved Organic Carbon 0.5 1 mg/L <MDL

MS:WG121213-21 L55763-1 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 18 35 mg/L 320 10 661 98 75--125










LD:WG121219-3 L55738-5 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:421250BS Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 20 mg/L 9 8.8 0--25

32 of 42







LD:WG121455-4 L55756-2 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421195-190 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 2 4 mg/L 110 111 1 0--25






LCS:WG121474-2 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10 100 85--115

33 of 42



LD:WG121474-4 L55796-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-DUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 16.6 17.3 4 0--20

MS:WG121474-5 L55661-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-VAGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 18.4 10 27.4 90 75--125









34 of 42


MS:WG121474-14 L55764-3 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 1 2 mg/L 45.7 10 64.3 93 75--125



SB:WG121474-17 MB:WG121474-15 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L <MDL 10 10 100 80--120








MB:WG121474-25 Matrix: BLANK WTR Listtype:CVDOC Method:SM5310-B Project: Pkey:STD

35 of 42


(Method Blank)Parameter MDL RDL Units MB Value QualDissolved Organic Carbon 0.5 1 mg/L <MDL








LD:WG121560-4 L55805-2 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-DUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 14.1 16.9 18 0--20

MS:WG121560-5 L55620-4 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-DUGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.87 10 10.8 99 75--125

LD:WG121560-6 L55876-2 Matrix: STORM WTR Listtype:CVTOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 18 35 mg/L 97.8 101 4 0--20


36 of 42





LD:WG121560-11 L55876-2 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 18 35 mg/L 61 59.7 2 0--20





LD:WG121560-16 L55821-3 Matrix: LEACHATE Listtype:CVTOC Method:SM5310-B Project:421422-CHLS-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 5 10 mg/L 121 121 0 0--20



37 of 42




MS:WG121560-21 L55818-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HTGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 11.4 10 21.4 100 75--125

LD:WG121560-22 L55806-2 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-HTGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.04 1.01 2 0--20






LD:WG121636-5 L55790-3 Matrix: SALT WTR Listtype:CVTSS Method:SM2540-D Project:423589-030-1 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 4.2 4.4 5 0--25


LCS:WG121636-7 Matrix: BLANK WTR Listtype:CVTSS Method:SM2540-D Project: Pkey:STD(Lab Control Sample)Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimit

38 of 42


Total Suspended Solids 5 10 mg/L 100 92 92 80--120

LD:WG121636-8 L55827-8 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-CHSW-M Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 1.4 <MDL 0--25








MS:WG121701-6 L55828-3 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.05 10 11 99 75--125



MB:WG121701-9 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD

39 of 42


(Method Blank)Parameter MDL RDL Units MB Value QualTotal Organic Carbon 0.5 1 mg/L <MDL






LD:WG121701-15 L55828-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 0.8 0.76 0--20

MS:WG121701-16 L55789-3 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 1 2 mg/L 2.45 10 22.6 101 75--125




LD:WG121701-20 L55790-2 Matrix: SALT WTR Listtype:CVDOC Method:SM5310-B Project:423589-030-1 Pkey:STD(Lab Duplicate)

40 of 42


Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 0.5 1 mg/L 1.86 1.6 15 0--20


LD:WG121701-22 L55936-2 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitDissolved Organic Carbon 5 10 mg/L 57.5 57 1 0--20

MS:WG121701-23 L55936-2 Matrix: STORM WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitDissolved Organic Carbon 5 10 mg/L 57.5 10 157 100 75--125




LD:WG121711-3 L55830-1 Matrix: GRND WTR Listtype:CVTSS Method:SM2540-D Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 9.8 9.6 2 0--25

LD:WG121711-4 L55930-1 Matrix: FRESH WTR Listtype:CVTSS Method:SM2540-D Project:421422-VASW-2 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Suspended Solids 1 2 mg/L 59.2 59.4 0 0--25


Workgroup: WG121752 toc,doc Run ID: R181967


LCS:WG121752-2 Matrix: BLANK WTR Listtype:CVTOC Method:SM5310-B Project: Pkey:STD(Lab Control Sample)

41 of 42


Parameter MDL RDL Units TrueValue LCS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 10 10 100 85--115


LD:WG121752-4 L55930-1 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-VASW-2 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 8.39 9.56 13 0--20

MS:WG121752-5 L55930-4 Matrix: FRESH WTR Listtype:CVTOC Method:SM5310-B Project:421422-VASW-2 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Value TrueValue MS Value % Rec. Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 8.06 10 16.7 87 75--125

LD:WG121752-6 L55918-1 Matrix: GRND WTR Listtype:CVTOC Method:SM5310-B Project:421422-PUGW Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimitTotal Organic Carbon 0.5 1 mg/L 1.08 0.99 9 0--20







LD:WG121752-13 L55698-1 Matrix: SEWER WTR Listtype:CVDOC Method:SM5310-B Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Value LD Value RPD Qual LabLimit

42 of 42


Dissolved Organic Carbon 5 10 mg/L 283 287 1 0--20




1 of 19

Workgroup: WG119801 CSO basin, OCS-enum Run ID: R172193



SB:WG119801-2 MB:WG119801-1 Matrix: BLANK WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L <MDL 0.05 0.0503 101 85--115

MSD:WG119801-4 MS:WG119801-3 L54967-2 Matrix: EFFLUENT Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:421184-110 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L <MDL 0.05 0.0522 104 75--125 0.05 0.0531 106 2 0--20

Workgroup: WG120032 CSO Basin, Aqua Tox Run ID: R173554

MB:WG120032-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDL

LIMSView QC Report for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Metals

2 of 19


Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG120032-2 MB:WG120032-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 20 100 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 20.6 103 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21.6 108 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 22 110 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 22.7 114 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21.3 107 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.7 103 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 21.3 107 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 21.3 107 85--115

LD:WG120032-3 L54687-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 9.73 9.73 0 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 8.59 8.7 1 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 9.03 8.97 1 0--20Copper, Total, ICP-MS 0.4 2 ug/L 34.5 34.7 1 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 170 169 1 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 2.06 2.08 1 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.19 0.18 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.363 0.368 1 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 29.7 30 1 0--20

MS:WG120032-4 L54687-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 9.73 20 28.7 95 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 8.59 20 28.4 99 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 9.03 20 29.6 103 75--125

3 of 19


Copper, Total, ICP-MS 0.4 2 ug/L 34.5 20 55.1 103 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 170 20 187 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 2.06 20 21.8 99 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.19 20 20.5 101 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.363 20 21.2 104 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 29.7 20 50.7 105 75--125

Workgroup: WG120037 CSO Basin Run ID: R173516

MB:WG120037-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDLChromium, Dissolved, ICP-MS 0.2 1 ug/L <MDLNickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLCopper, Dissolved, ICP-MS 0.4 2 ug/L <MDLZinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDLSilver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDLLead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG120037-2 MB:WG120037-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 21 105 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 21.1 106 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21.3 106 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 21.3 106 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 20.5 102 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.1 100 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 21.3 106 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 21 105 85--115

4 of 19


LD:WG120037-3 L54687-3 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.34 1.34 0 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 1.25 1.24 0 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 1.26 1.26 0 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 6.28 6.26 0 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 22.5 22.2 2 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.766 0.763 0 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.057 0.061 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.48 0.49 0--20

MS:WG120037-4 L54687-3 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.34 20 22.1 104 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 1.25 20 22 104 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 1.26 20 22.2 105 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 6.28 20 27.2 104 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 22.5 20 42.4 99 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.766 20 21.7 105 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20 100 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.057 20 20.8 104 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.48 20 21 103 75--125



5 of 19




MSD:WG120040-4 MS:WG120040-3 L55186-3 Matrix: STORM WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L 0.0391 0.2 0.218 89 75--125 0.2 0.214 87 2 0--20





MSD:WG120057-4 MS:WG120057-3 L55011-2 Matrix: STORM WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)

6 of 19


Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L 0.0331 0.2 0.21 88 75--125 0.2 0.209 88 0 0--20

Workgroup: WG120641 CSO Basin study Run ID: R177109




MSD:WG120641-4 MS:WG120641-3 L55285-2 Matrix: STORM WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L <MDL 0.05 0.0495 99 75--125 0.05 0.0502 100 1 0--20

Workgroup: WG120674 CSO Basin Study Run ID: R177112


MB:WG120674-1 Matrix: BLANK WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project: Pkey:STD

7 of 19


(Method Blank)Parameter MDL RDL Units MB Value QualMercury, Dissolved, CVAA 0.005 0.015 ug/L <MDL


MSD:WG120674-4 MS:WG120674-3 L55433-2 Matrix: STORM WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.05 0.15 ug/L 0.162 0.05 0.264 204 * 75--125 0.05 0.257 189 * 3 0--20

Workgroup: WG120847 CSO Basin Diss Run ID: R177412


SB:WG120847-2 MB:WG120847-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 18 90 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.1 96 85--115

8 of 19


Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.9 100 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 19.9 99 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 21.2 106 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.3 97 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 19.8 99 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.9 99 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.5 98 85--115

LD:WG120847-3 L55285-2 Matrix: STORM WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.02 1.05 3 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 1.27 1.26 0 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 553 548 1 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 16.1 16.1 0 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 51.4 51.2 0 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.36 1.38 2 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L 0.212 0.216 2 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.1 0.1 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 1.65 1.65 0 0--20

MS:WG120847-4 L55285-2 Matrix: STORM WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.02 20 20.3 97 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 1.27 20 20.4 96 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 553 20 578 4xRule 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 16.1 20 36.7 103 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 51.4 20 72.3 104 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 1.36 20 22.1 104 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L 0.212 20 20.2 100 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L 0.1 20 20.2 100 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 1.65 20 21.3 98 75--125

9 of 19


Workgroup: WG120860 CSO Totals Run ID: R177453

MB:WG120860-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG120860-2 MB:WG120860-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 19.5 98 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 19.6 98 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20 100 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 20.1 101 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 21.1 105 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.6 98 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 21 105 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 19.9 100 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.8 104 85--115

LD:WG120860-3 L55285-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 4.43 4.23 5 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 3.52 3.45 2 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.54 5.41 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 32.4 32 1 0--20

10 of 19


Zinc, Total, ICP-MS 0.5 2.5 ug/L 130 130 0 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.16 1.13 3 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.2 0.16 20 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.24 0.22 0--20Lead, Total, ICP-MS 0.1 0.5 ug/L 12.9 12.6 2 0--20

MS:WG120860-4 L55285-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 4.43 20 23.7 96 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 3.52 20 23.1 98 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.54 20 25.6 100 75--125Copper, Total, ICP-MS 0.4 2 ug/L 32.4 20 52.3 99 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 130 20 150 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.16 20 20.2 95 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.2 20 21 104 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.24 20 19.9 98 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 12.9 20 33.9 105 75--125

Workgroup: WG120894 cso basin Sewer, strom wa Run ID: R177557



SB:WG120894-2 MB:WG120894-1 Matrix: BLANK WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimit

11 of 19


Mercury, Total, CVAA 0.005 0.015 ug/L <MDL 0.05 0.0511 102 85--115

MSD:WG120894-4 MS:WG120894-3 L55584-3 Matrix: STORM WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L 0.0077 0.05 0.0578 100 75--125 0.05 0.0568 98 2 0--20

Workgroup: WG121053 cso basin, RTP inplant Run ID: R179273




MSD:WG121053-4 MS:WG121053-3 L55645-2 Matrix: EFFLUENT Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:421186B Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L 0.0307 0.05 0.0832 105 75--125 0.05 0.0795 98 5 0--20

Workgroup: WG121194 5/23/12 CSO Basin Totals Run ID: R180273

MB:WG121194-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)

12 of 19


Parameter MDL RDL Units MB Value QualVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG121194-2 MB:WG121194-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 19.6 98 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 18.6 93 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 18.9 94 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 18.6 93 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 19.5 97 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 18.3 91 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 19 95 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 18.6 93 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 19.1 95 85--115

LD:WG121194-3 L55638-1 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 6.69 6.66 1 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 6.61 6.62 0 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.15 5.23 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 33.8 33.7 0 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 157 156 1 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.92 1.92 0 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.089 0.095 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.307 0.321 4 0--20

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Lead, Total, ICP-MS 0.1 0.5 ug/L 19.8 20.2 2 0--20

MS:WG121194-4 L55638-1 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 6.69 20 26.7 100 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 6.61 20 25.6 95 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.15 20 24.6 97 75--125Copper, Total, ICP-MS 0.4 2 ug/L 33.8 20 54.4 103 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 157 20 176 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.92 20 20.1 91 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.089 20 18 90 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.307 20 19.3 95 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 19.8 20 40.4 103 75--125

Workgroup: WG121302 5/31/12 CSO Basin Dissolv Run ID: R180782


SB:WG121302-2 MB:WG121302-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 19.1 96 85--115

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Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 19.1 95 85--115Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.7 103 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 21 105 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 21.8 109 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 20.4 102 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.9 105 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 21 105 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 19.5 98 85--115

LD:WG121302-3 L55572-3 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.8 0.824 3 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.7 0.7 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 2.99 2.98 0 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 15.3 15.3 0 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 33.4 33 1 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.8 0.777 3 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 1.59 1.63 3 0--20

MS:WG121302-4 L55572-3 Matrix: SEWER WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 0.8 20 20.2 97 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.7 20 20.5 99 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 2.99 20 23.7 103 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 15.3 20 36.3 105 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 33.4 20 54.3 105 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.8 20 21.2 102 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 20.3 101 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 20.7 104 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 1.59 20 20.8 96 75--125

15 of 19


Workgroup: WG121351 CSO Basin study Run ID: R180915




MSD:WG121351-4 MS:WG121351-3 L55763-3 Matrix: STORM WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L 0.0064 0.05 0.0527 93 75--125 0.05 0.0519 91 2 0--20Workgroup: WG121500 CSO Basin Study Run ID: R181640



SB:WG121500-2 MB:WG121500-1 Matrix: BLANK WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project: Pkey:STD(Spike Blank, Method Blank)

16 of 19


Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L <MDL 0.05 0.046 92 85--115

MSD:WG121500-4 MS:WG121500-3 L55859-3 Matrix: STORM WTR Listtype:MTHG-LOW Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Total, CVAA 0.005 0.015 ug/L 0.0234 0.05 0.0677 89 75--125 0.05 0.0666 87 2 0--20





MSD:WG121764-4 MS:WG121764-3 L55936-2 Matrix: STORM WTR Listtype:MTHG-LOW-DISS Method:EPA 245.1*SW846 7470A Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitMercury, Dissolved, CVAA 0.005 0.015 ug/L 0.0069 0.05 0.0571 101 75--125 0.05 0.0588 104 3 0--20

Workgroup: WG121947 7/10/12 CSO Basin Study T Run ID: R182273

MB:WG121947-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Method Blank)

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Parameter MDL RDL Units MB Value QualVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDLChromium, Total, ICP-MS 0.2 1 ug/L <MDLNickel, Total, ICP-MS 0.1 0.5 ug/L <MDLCopper, Total, ICP-MS 0.4 2 ug/L <MDLZinc, Total, ICP-MS 0.5 2.5 ug/L <MDLArsenic, Total, ICP-MS 0.1 0.5 ug/L <MDLSilver, Total, ICP-MS 0.04 0.2 ug/L <MDLCadmium, Total, ICP-MS 0.05 0.25 ug/L <MDLLead, Total, ICP-MS 0.1 0.5 ug/L <MDL

SB:WG121947-2 MB:WG121947-1 Matrix: BLANK WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L <MDL 20 20.3 102 85--115Chromium, Total, ICP-MS 0.2 1 ug/L <MDL 20 20.7 104 85--115Nickel, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.7 104 85--115Copper, Total, ICP-MS 0.4 2 ug/L <MDL 20 21.5 108 85--115Zinc, Total, ICP-MS 0.5 2.5 ug/L <MDL 20 21.7 108 85--115Arsenic, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.1 101 85--115Silver, Total, ICP-MS 0.04 0.2 ug/L <MDL 20 20.2 101 85--115Cadmium, Total, ICP-MS 0.05 0.25 ug/L <MDL 20 20.4 102 85--115Lead, Total, ICP-MS 0.1 0.5 ug/L <MDL 20 20.8 104 85--115

LD:WG121947-3 L55875-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 5.3 5.29 0 0--20Chromium, Total, ICP-MS 0.2 1 ug/L 5.22 4.47 15 0--20Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.34 5.43 2 0--20Copper, Total, ICP-MS 0.4 2 ug/L 33.6 34.8 4 0--20Zinc, Total, ICP-MS 0.5 2.5 ug/L 146 149 2 0--20Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.2 1.22 2 0--20Silver, Total, ICP-MS 0.04 0.2 ug/L 0.14 0.13 0--20Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.272 0.269 1 0--20

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Lead, Total, ICP-MS 0.1 0.5 ug/L 17.8 18.4 3 0--20

MS:WG121947-4 L55875-3 Matrix: STORM WTR Listtype:MTICPMS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Total, ICP-MS 0.075 0.375 ug/L 5.3 20 25.2 100 75--125Chromium, Total, ICP-MS 0.2 1 ug/L 5.22 20 25.3 100 75--125Nickel, Total, ICP-MS 0.1 0.5 ug/L 5.34 20 25.5 101 75--125Copper, Total, ICP-MS 0.4 2 ug/L 33.6 20 54.8 106 75--125Zinc, Total, ICP-MS 0.5 2.5 ug/L 146 20 167 4xRule 75--125Arsenic, Total, ICP-MS 0.1 0.5 ug/L 1.2 20 20.2 95 75--125Silver, Total, ICP-MS 0.04 0.2 ug/L 0.14 20 20.9 104 75--125Cadmium, Total, ICP-MS 0.05 0.25 ug/L 0.272 20 20 99 75--125Lead, Total, ICP-MS 0.1 0.5 ug/L 17.8 20 39.6 109 75--125

Workgroup: WG121990 7/12/12 CSO Basin Diss Run ID: R182296


SB:WG121990-2 MB:WG121990-1 Matrix: BLANK WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValu SB Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L <MDL 20 17.1 85 85--115Chromium, Dissolved, ICP-MS 0.2 1 ug/L <MDL 20 17.9 89 85--115

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Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 18.8 94 85--115Copper, Dissolved, ICP-MS 0.4 2 ug/L <MDL 20 18.2 91 85--115Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L <MDL 20 19.4 97 85--115Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 18.2 91 85--115Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 17.9 89 85--115Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 18.4 92 85--115Lead, Dissolved, ICP-MS 0.1 0.5 ug/L <MDL 20 18 90 85--115

LD:WG121990-3 L55876-3 Matrix: STORM WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP Valu LD Value RPD Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.43 1.43 0 0--20Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.67 0.67 0--20Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 1.25 1.29 3 0--20Copper, Dissolved, ICP-MS 0.4 2 ug/L 8.08 8.06 0 0--20Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 23.4 23.1 1 0--20Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.775 0.791 2 0--20Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL <MDL 0--20Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL <MDL 0--20Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.42 0.43 0--20

MS:WG121990-4 L55876-3 Matrix: STORM WTR Listtype:MTICPMS-DISS Method:EPA 200.8*SW846 6020A Project:423589-320-4 Pkey:STD(Matrix Spike)Parameter MDL RDL Units SAMP Valu TrueValu MS Value % Rec. Qual LabLimitVanadium, Dissolved, ICP-MS 0.075 0.375 ug/L 1.43 20 19.3 89 75--125Chromium, Dissolved, ICP-MS 0.2 1 ug/L 0.67 20 19 92 75--125Nickel, Dissolved, ICP-MS 0.1 0.5 ug/L 1.25 20 20.7 97 75--125Copper, Dissolved, ICP-MS 0.4 2 ug/L 8.08 20 27 95 75--125Zinc, Dissolved, ICP-MS 0.5 2.5 ug/L 23.4 20 44 103 75--125Arsenic, Dissolved, ICP-MS 0.1 0.5 ug/L 0.775 20 20.3 98 75--125Silver, Dissolved, ICP-MS 0.04 0.2 ug/L <MDL 20 18.5 93 75--125Cadmium, Dissolved, ICP-MS 0.05 0.25 ug/L <MDL 20 19.5 97 75--125Lead, Dissolved, ICP-MS 0.1 0.5 ug/L 0.42 20 19 93 75--125======================================================================================4xRule indicates no MS/MSD recovery was calculated due to the 4x rule.

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SBD:WG119537-3 SB:WG119537-2 MB:WG119537-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.401 80 40--160 0.5 0.388 78 3 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.0083 0.5 0.383 75 40--160 0.5 0.371 72 3 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.012 0.5 0.774 152 40--160 0.5 0.778 153 1 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.419 84 40--160 0.5 0.415 83 1 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.398 80 40--160 0.5 0.396 79 0 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0714 0.5 0.844 155 40--160 0.5 0.812 148 4 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.511 102 40--160 0.5 0.514 103 1 0--40Phenanthrene 0.008 0.016 ug/L 0.0098 0.5 0.391 76 40--160 0.5 0.402 78 3 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.38 76 40--160 0.5 0.376 75 1 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.328 0.5 0.974 129 40--160 0.5 0.818 98 17 0--40

LIMSView Batch QC for Brandon CSO Wet Baseflow and Storm Samples - Data Validation for Organics - REVISED

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Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.504 101 40--160 0.5 0.5 100 1 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.571 114 40--160 0.5 0.565 113 1 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0346 0.5 0.798 153 40--160 0.5 0.825 158 3 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.484 97 40--160 0.5 0.494 99 2 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.453 91 40--160 0.5 0.472 94 4 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.296 0.5 0.701 81 40--160 0.5 1.02 145 37 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.541 108 40--160 0.5 0.571 114 5 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.935 94 40--160 1 0.976 98 4 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.383 77 40--160 0.5 0.374 75 2 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.387 77 40--160 0.5 0.36 72 7 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.384 77 40--160 0.5 0.348 70 10 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.37 74 40--160 0.5 0.353 71 5 0--40

LD:WG119537-4 L54687-1 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L 0.0942 0.0952 1 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.0666 0.0701 5 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.178 0.168 6 0--40Acenaphthylene 0.008 0.016 ug/L 0.014 0.016 0--40Acenaphthene 0.008 0.016 ug/L 0.0186 0.0204 9 0--40Diethyl Phthalate 0.008 0.04 ug/L 1.5 1.48 2 0--40Fluorene 0.008 0.016 ug/L 0.0347 0.034 2 0--40Phenanthrene 0.008 0.016 ug/L 0.111 0.11 1 0--40Anthracene 0.008 0.016 ug/L 0.0214 0.0228 6 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.705 0.795 12 0--40Fluoranthene 0.008 0.016 ug/L 0.148 0.138 7 0--40Pyrene 0.008 0.016 ug/L 0.139 0.139 0 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.445 0.461 4 0--40Benzo(a)anthracene 0.008 0.016 ug/L 0.0327 0.0298 9 0--40Chrysene 0.008 0.016 ug/L 0.0764 0.0723 5 0--40Bis(2-Ethylhexyl)Phthalate 0.032 0.064 ug/L 5.5 8.56 43 * 0--40Di-N-Octyl Phthalate 0.032 0.064 ug/L 8.86 8.76 1 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L 0.0773 0.0689 12 0--40Benzo(a)pyrene 0.008 0.016 ug/L 0.031 0.0303 2 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L 0.0247 0.0212 15 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L 0.01 0.01 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L 0.0492 0.0451 9 0--40

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Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L54687-1 93 140L54687-2 91 132L54687-3 93 157WG119537-1 89 122WG119537-2 89 133WG119537-3 89 136WG119537-4 91 137

Workgroup: WG119848 (pahll#010 pahph-lvi) Run ID: R200730

MB:WG119848-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L 0.0089 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.04 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.0085 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.12 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0327 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.382 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDLBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG119848-3 SB:WG119848-2 MB:WG119848-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD

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(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.357 71 40--160 0.5 0.373 74 4 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.348 70 40--160 0.5 0.36 72 3 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.0089 0.5 0.669 132 40--160 0.5 0.731 144 9 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.384 77 40--160 0.5 0.386 77 0 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.359 72 40--160 0.5 0.373 75 4 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.04 0.5 0.684 129 40--160 0.5 0.767 145 11 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.459 92 40--160 0.5 0.479 96 4 0--40Phenanthrene 0.008 0.016 ug/L 0.0085 0.5 0.373 73 40--160 0.5 0.372 73 0 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.372 74 40--160 0.5 0.38 76 2 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.12 0.5 0.677 111 40--160 0.5 0.761 128 12 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.449 90 40--160 0.5 0.47 94 5 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.537 107 40--160 0.5 0.498 100 8 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0327 0.5 0.717 137 40--160 0.5 0.76 145 6 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.441 88 40--160 0.5 0.452 90 2 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.428 86 40--160 0.5 0.428 85 0 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.382 0.5 1.66 257 * 40--160 0.5 1.34 191 * 22 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.498 100 40--160 0.5 0.537 107 8 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.872 87 40--160 1 0.88 88 1 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.366 73 40--160 0.5 0.375 75 2 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.365 73 40--160 0.5 0.356 71 3 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.365 73 40--160 0.5 0.353 71 3 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.362 72 40--160 0.5 0.353 71 3 0--40

LD:WG119848-4 L55012-3 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L 0.0692 0.0735 6 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.0619 0.0755 20 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.165 0.172 4 0--40Acenaphthylene 0.008 0.016 ug/L <MDL <MDL 0--40Acenaphthene 0.008 0.016 ug/L 0.0227 0.0189 18 0--40Diethyl Phthalate 0.008 0.04 ug/L 3.6 3.75 4 0--40Fluorene 0.008 0.016 ug/L 0.05 0.0522 4 0--40Phenanthrene 0.008 0.016 ug/L 0.205 0.195 5 0--40Anthracene 0.008 0.016 ug/L 0.0387 0.0408 5 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.475 0.56 16 0--40Fluoranthene 0.008 0.016 ug/L 0.283 0.266 6 0--40Pyrene 0.008 0.016 ug/L 0.231 0.2 15 0--40Benzyl Butyl Phthalate 0.016 0.032 ug/L 3.9 6.01 43 * 0--40

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Benzo(a)anthracene 0.008 0.016 ug/L 0.0746 0.0622 18 0--40Chrysene 0.008 0.016 ug/L 0.173 0.157 9 0--40Bis(2-Ethylhexyl)Phthalate 0.016 0.032 ug/L 3.06 4.18 31 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.867 1.05 19 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L 0.211 0.224 6 0--40Benzo(a)pyrene 0.008 0.016 ug/L 0.0882 0.0882 0 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L 0.0803 0.0947 17 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L 0.0274 0.0297 8 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L 0.126 0.137 8 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55012-1 83 73L55012-3 80 83WG119848-1 73 99WG119848-2 91 128WG119848-3 91 125WG119848-4 87 101

Workgroup: WG119973 (pahll#012 PAH-LVI) Run ID: R200799

MB:WG119973-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L 0.011 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0935 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L <MDLAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.17 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0782 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDL

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Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.654 BDi-N-Octyl Phthalate 0.008 0.016 ug/L 0.012 BBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG119973-3 SB:WG119973-2 MB:WG119973-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.322 64 40--160 0.5 0.276 55 15 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.278 56 40--160 0.5 0.231 46 19 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.011 0.5 0.646 127 40--160 0.5 0.563 110 14 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.326 65 40--160 0.5 0.291 58 12 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.339 68 40--160 0.5 0.294 59 14 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0935 0.5 0.466 74 40--160 0.5 0.588 99 23 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.239 48 40--160 0.5 0.287 57 18 0--40Phenanthrene 0.008 0.016 ug/L <MDL 0.5 0.361 72 40--160 0.5 0.33 66 9 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.313 63 40--160 0.5 0.253 51 21 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.17 0.5 0.696 105 40--160 0.5 0.617 89 12 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.523 105 40--160 0.5 0.473 95 10 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.289 58 40--160 0.5 0.312 62 8 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0782 0.5 0.811 146 40--160 0.5 0.55 94 38 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.432 86 40--160 0.5 0.407 81 6 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.431 86 40--160 0.5 0.419 84 3 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.654 0.5 1.29 126 40--160 0.5 1.77 224 * 32 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.012 0.5 0.49 96 40--160 0.5 0.5 98 2 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.822 82 40--160 1 0.827 83 1 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.334 67 40--160 0.5 0.307 61 8 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.39 78 40--160 0.5 0.279 56 33 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.392 78 40--160 0.5 0.278 56 34 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.388 78 40--160 0.5 0.279 56 33 0--40

LD:WG119973-4 L55186-3 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L 0.0695 0.081 15 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.0268 0.0296 10 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.15 0.165 10 0--40Acenaphthylene 0.008 0.016 ug/L 0.016 0.0203 25 0--40

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Acenaphthene 0.008 0.016 ug/L 0.012 0.014 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.722 0.78 8 0--40Fluorene 0.008 0.016 ug/L 0.0231 0.0278 19 0--40Phenanthrene 0.008 0.016 ug/L 0.113 0.137 19 0--40Anthracene 0.008 0.016 ug/L 0.0304 0.0358 17 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.956 1.1 14 0--40Fluoranthene 0.008 0.016 ug/L 0.16 0.315 65 * 0--40Pyrene 0.008 0.016 ug/L 0.222 0.251 12 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 3.61 4.16 14 0--40Benzo(a)anthracene 0.008 0.016 ug/L 0.0485 0.0609 23 0--40Chrysene 0.008 0.016 ug/L 0.152 0.181 18 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 3.7 4.19 12 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.431 0.358 18 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L 0.165 0.145 13 0--40Benzo(a)pyrene 0.008 0.016 ug/L 0.0573 0.0743 26 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L 0.0496 0.0605 20 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L 0.015 0.0211 34 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L 0.0906 0.125 32 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55011-1 72 47L55011-2 125 88L55011-3 103 58L55186-1 79 89L55186-2 81 133L55186-3 71 136WG119973-1 75 148WG119973-2 78 80WG119973-3 68 81WG119973-4 79 123


MB:WG120438-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDL

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Dimethyl Phthalate 0.008 0.016 ug/L 0.015 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0653 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.0088 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.12 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0374 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.55 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDLBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG120438-3 SB:WG120438-2 MB:WG120438-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.382 76 40--160 0.5 0.389 78 2 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.425 85 40--160 0.5 0.421 84 1 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.015 0.5 0.57 111 40--160 0.5 0.57 111 0 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.428 86 40--160 0.5 0.438 87 2 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.413 83 40--160 0.5 0.413 83 0 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0653 0.5 0.6 107 40--160 0.5 0.629 113 5 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.436 87 40--160 0.5 0.435 87 0 0--40Phenanthrene 0.008 0.016 ug/L 0.0088 0.5 0.451 88 40--160 0.5 0.451 88 0 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.378 76 40--160 0.5 0.376 75 0 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.12 0.5 0.611 99 40--160 0.5 0.654 107 7 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.476 95 40--160 0.5 0.461 92 3 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.451 90 40--160 0.5 0.452 90 0 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0374 0.5 0.636 120 40--160 0.5 0.628 118 1 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.471 94 40--160 0.5 0.459 92 3 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.488 98 40--160 0.5 0.475 95 3 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.55 0.5 1.62 214 * 40--160 0.5 0.983 87 49 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.592 118 40--160 0.5 0.614 123 4 0--40

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Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 1.01 101 40--160 1 0.994 99 2 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.382 76 40--160 0.5 0.357 71 7 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.503 101 40--160 0.5 0.486 97 3 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.524 105 40--160 0.5 0.504 101 4 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.5 100 40--160 0.5 0.481 96 4 0--40

LD:WG120438-4 L55185-2 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L 0.266 0.29 9 0--402-Methylnaphthalene 0.04 0.08 ug/L 0.545 0.516 5 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.208 0.205 1 0--40Acenaphthylene 0.04 0.08 ug/L <MDL 0.063 0--40Acenaphthene 0.04 0.08 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.04 0.2 ug/L 0.815 0.837 3 0--40Fluorene 0.04 0.08 ug/L <MDL <MDL 0--40Phenanthrene 0.04 0.08 ug/L 0.193 0.166 15 0--40Anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 2.1 2.11 0 0--40Fluoranthene 0.04 0.08 ug/L 0.258 0.199 26 0--40Pyrene 0.04 0.08 ug/L 0.289 0.234 21 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 1.88 1.86 1 0--40Benzo(a)anthracene 0.04 0.08 ug/L 0.1 0.0852 16 0--40Chrysene 0.04 0.08 ug/L 0.187 0.156 18 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 4.51 4.76 6 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 1.47 1.61 9 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.221 0.217 2 0--40Benzo(a)pyrene 0.04 0.08 ug/L 0.0979 0.0981 0 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L 0.075 0.079 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L 0.127 0.137 8 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55154-1 85 64L55154-2 84 87L55154-3 83 72L55185-1 75 67L55185-2 87 106

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L55185-3 83 86L55285-2 91 110L55285-3 103 110WG120438-1 99 106WG120438-2 99 107WG120438-3 101 108WG120438-4 83 98


MB:WG120555-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L <MDLAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0863 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L <MDLAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.19 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.058 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.826 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDLBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SB:WG120555-2 MB:WG120555-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.372 74 40--1602-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.455 91 40--160

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Dimethyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.584 117 40--160Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.398 80 40--160Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.378 76 40--160Diethyl Phthalate 0.008 0.04 ug/L 0.0863 0.5 0.598 102 40--160Fluorene 0.008 0.016 ug/L <MDL 0.5 0.438 87 40--160Phenanthrene 0.008 0.016 ug/L <MDL 0.5 0.41 82 40--160Anthracene 0.008 0.016 ug/L <MDL 0.5 0.346 69 40--160Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.19 0.5 0.711 103 40--160Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.405 81 40--160Pyrene 0.008 0.016 ug/L <MDL 0.5 0.471 94 40--160Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.058 0.5 0.691 127 40--160Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.45 90 40--160Chrysene 0.008 0.016 ug/L <MDL 0.5 0.489 98 40--160Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.826 0.5 2.5 335 * 40--160Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.62 124 40--160Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.973 97 40--160Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.376 75 40--160Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.431 86 40--160Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.436 87 40--160Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.428 86 40--160

SBD:WG120438-3 SB:WG120438-2 MB:WG120438-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.382 76 40--160 0.5 0.389 78 2 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.425 85 40--160 0.5 0.421 84 1 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.015 0.5 0.57 111 40--160 0.5 0.57 111 0 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.428 86 40--160 0.5 0.438 87 2 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.413 83 40--160 0.5 0.413 83 0 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0653 0.5 0.6 107 40--160 0.5 0.629 113 5 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.436 87 40--160 0.5 0.435 87 0 0--40Phenanthrene 0.008 0.016 ug/L 0.0088 0.5 0.451 88 40--160 0.5 0.451 88 0 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.378 76 40--160 0.5 0.376 75 0 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.12 0.5 0.611 99 40--160 0.5 0.654 107 7 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.476 95 40--160 0.5 0.461 92 3 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.451 90 40--160 0.5 0.452 90 0 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0374 0.5 0.636 120 40--160 0.5 0.628 118 1 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.471 94 40--160 0.5 0.459 92 3 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.488 98 40--160 0.5 0.475 95 3 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.55 0.5 1.62 214 * 40--160 0.5 0.983 87 49 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.592 118 40--160 0.5 0.614 123 4 0--40

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Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 1.01 101 40--160 1 0.994 99 2 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.382 76 40--160 0.5 0.357 71 7 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.503 101 40--160 0.5 0.486 97 3 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.524 105 40--160 0.5 0.504 101 4 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.5 100 40--160 0.5 0.481 96 4 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55183-1 81 55L55183-2 85 66L55183-3 104 104WG120555-1 93 108WG120555-2 92 108


MB:WG120654-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L 0.013 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0508 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L <MDLAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.1 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0649 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 2.12 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDLBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL

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Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG120654-3 SB:WG120654-2 MB:WG120654-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.499 0.36 72 40--160 0.5 0.395 79 9 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.499 0.42 84 40--160 0.5 0.459 92 9 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.013 0.499 0.652 128 40--160 0.5 0.63 123 3 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.499 0.387 78 40--160 0.5 0.428 86 10 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.499 0.367 74 40--160 0.5 0.398 80 8 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0508 0.499 0.731 136 40--160 0.5 0.689 128 6 0--40Fluorene 0.008 0.016 ug/L <MDL 0.499 0.451 90 40--160 0.5 0.456 91 1 0--40Phenanthrene 0.008 0.016 ug/L <MDL 0.499 0.415 83 40--160 0.5 0.438 88 5 0--40Anthracene 0.008 0.016 ug/L <MDL 0.499 0.302 61 40--160 0.5 0.35 70 15 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.1 0.499 0.774 134 40--160 0.5 0.612 102 23 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.499 0.477 96 40--160 0.5 0.484 97 1 0--40Pyrene 0.008 0.016 ug/L <MDL 0.499 0.475 95 40--160 0.5 0.488 98 3 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0649 0.499 0.688 125 40--160 0.5 0.673 122 2 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.499 0.454 91 40--160 0.5 0.463 93 2 0--40Chrysene 0.008 0.016 ug/L <MDL 0.499 0.483 97 40--160 0.5 0.49 98 1 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 2.12 0.5 7.97 1170 * 40--160 0.5 1.34 -156 * 142 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.499 0.549 110 40--160 0.5 0.556 111 1 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 0.998 0.972 97 40--160 1 0.986 99 1 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.499 0.337 68 40--160 0.5 0.359 72 6 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.499 0.429 86 40--160 0.5 0.425 85 1 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.499 0.433 87 40--160 0.5 0.429 86 1 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.499 0.43 86 40--160 0.5 0.425 85 1 0--40

LD:WG120654-4 L55433-1 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.04 0.08 ug/L 0.067 0.066 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.209 0.193 8 0--40Acenaphthylene 0.04 0.08 ug/L <MDL <MDL 0--40Acenaphthene 0.04 0.08 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.04 0.2 ug/L 1.5 1.33 12 0--40Fluorene 0.04 0.08 ug/L <MDL <MDL 0--40Phenanthrene 0.04 0.08 ug/L 0.13 0.127 2 0--40Anthracene 0.04 0.08 ug/L <MDL <MDL 0--40

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Di-N-Butyl Phthalate 0.04 1 ug/L 0.66 0.68 0--40Fluoranthene 0.04 0.08 ug/L 0.109 0.123 12 0--40Pyrene 0.04 0.08 ug/L 0.11 0.131 17 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 0.725 0.703 3 0--40Benzo(a)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Chrysene 0.04 0.08 ug/L 0.064 0.0872 30 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 7.49 5.66 28 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 3.12 3.01 4 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.062 0.0856 32 0--40Benzo(a)pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L <MDL <MDL 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55184-2 103 71L55184-3 134 77L55433-1 94 59L55433-2 109 75L55433-3 89 61WG120654-1 82 103WG120654-2 80 104WG120654-3 90 104WG120654-4 87 59


MB:WG120867-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L <MDLAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.011 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L <MDL

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Anthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.022 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0088 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.411 BDi-N-Octyl Phthalate 0.008 0.016 ug/L <MDLBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG120867-3 SB:WG120867-2 MB:WG120867-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.1 0.0731 73 40--160 0.1 0.0691 69 6 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.1 0.0957 96 40--160 0.1 0.0911 91 5 0--40Dimethyl Phthalate 0.008 0.016 ug/L <MDL 0.1 0.106 106 40--160 0.1 0.103 103 3 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.1 0.0745 74 40--160 0.1 0.0687 69 8 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.1 0.0805 80 40--160 0.1 0.0738 74 9 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.011 0.1 0.111 100 40--160 0.1 0.108 97 3 0--40Fluorene 0.008 0.016 ug/L <MDL 0.1 0.077 77 40--160 0.1 0.0669 67 14 0--40Phenanthrene 0.008 0.016 ug/L <MDL 0.1 0.0837 84 40--160 0.1 0.0748 75 11 0--40Anthracene 0.008 0.016 ug/L <MDL 0.1 0.0639 64 40--160 0.1 0.0584 58 9 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.022 0.1 0.12 102 40--160 0.1 0.13 110 6 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.1 0.0829 83 40--160 0.1 0.0803 80 3 0--40Pyrene 0.008 0.016 ug/L <MDL 0.1 0.0976 97 40--160 0.1 0.0968 97 1 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0088 0.1 0.113 104 40--160 0.1 0.104 95 8 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.1 0.0912 91 40--160 0.1 0.0887 89 3 0--40Chrysene 0.008 0.016 ug/L <MDL 0.1 0.102 102 40--160 0.1 0.0992 99 3 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.411 0.1 3.23 2814 * 40--160 0.1 0.263 -148 * 170 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 0.1 0.181 181 * 40--160 0.1 0.135 135 29 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 0.2 0.195 97 40--160 0.2 0.186 93 5 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.1 0.0664 66 40--160 0.1 0.0679 68 2 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.1 0.0926 92 40--160 0.1 0.0905 90 2 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.1 0.0956 95 40--160 0.1 0.0934 93 2 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.1 0.09 90 40--160 0.1 0.0872 87 3 0--40

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LD:WG120867-4 L55511-3 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.094 0.189 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.038 0.0755 ug/L <MDL <MDL 0--40Dimethyl Phthalate 0.038 0.0755 ug/L 0.101 0.106 5 0--40Acenaphthylene 0.038 0.0755 ug/L <MDL <MDL 0--40Acenaphthene 0.038 0.0755 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.038 0.189 ug/L 6.65 6.77 2 0--40Fluorene 0.038 0.0755 ug/L <MDL 0.05 0--40Phenanthrene 0.038 0.0755 ug/L 0.044 0.048 0--40Anthracene 0.038 0.0755 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.038 0.943 ug/L 3.7 3.96 7 0--40Fluoranthene 0.038 0.0755 ug/L <MDL 0.038 0--40Pyrene 0.038 0.0755 ug/L <MDL <MDL 0--40Benzyl Butyl Phthalate 0.38 0.755 ug/L 76.1 74 3 0--40Benzo(a)anthracene 0.038 0.0755 ug/L <MDL <MDL 0--40Chrysene 0.038 0.0755 ug/L <MDL <MDL 0--40Bis(2-Ethylhexyl)Phthalate 0.038 0.0755 ug/L 9.18 11.3 21 0--40Di-N-Octyl Phthalate 0.038 0.0755 ug/L <MDL <MDL 0--40Benzo(b,j,k)fluoranthene 0.038 0.0755 ug/L <MDL <MDL 0--40Benzo(a)pyrene 0.038 0.0755 ug/L <MDL <MDL 0--40Indeno(1,2,3-Cd)Pyrene 0.038 0.0755 ug/L <MDL <MDL 0--40Dibenzo(a,h)anthracene 0.038 0.0755 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.038 0.0755 ug/L <MDL <MDL 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55511-1 60 49L55511-2 68 52L55511-3 83 67L55512-1 117 51L55512-2 51 55L55512-3 96 65L55584-1 87 48L55584-2 91 68L55584-3 98 77WG120867-1 73 101WG120867-2 82 112

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WG120867-3 76 108WG120867-4 85 64


MB:WG121052-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L 0.0452 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.142 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.011 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.16 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.068 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.016 0.032 ug/L 6.84 BDi-N-Octyl Phthalate 0.008 0.016 ug/L 0.011 BBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG121052-3 SB:WG121052-2 MB:WG121052-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.292 58 40--160 0.5 0.3 60 3 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.308 62 40--160 0.5 0.325 65 5 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.0452 0.5 0.504 92 40--160 0.5 0.507 92 0 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.354 71 40--160 0.5 0.367 73 4 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.328 66 40--160 0.5 0.339 68 3 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.142 0.5 0.609 93 40--160 0.5 0.598 91 2 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.374 75 40--160 0.5 0.388 78 4 0--40

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Phenanthrene 0.008 0.016 ug/L 0.011 0.5 0.367 71 40--160 0.5 0.367 71 0 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.34 68 40--160 0.5 0.348 70 2 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.16 0.5 0.894 146 40--160 0.5 0.799 127 11 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.438 88 40--160 0.5 0.435 87 1 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.387 77 40--160 0.5 0.392 78 1 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.068 0.5 0.842 155 40--160 0.5 0.866 160 3 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.454 91 40--160 0.5 0.469 94 3 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.428 86 40--160 0.5 0.445 89 4 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 6.84 0.5 1.49 -1071 * 40--160 0.5 1.68 -1033 * 12 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.011 0.5 0.8 158 40--160 0.5 0.777 153 3 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 0.941 94 40--160 1 0.97 97 3 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.374 75 40--160 0.5 0.386 77 3 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.456 91 40--160 0.5 0.47 94 3 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.471 94 40--160 0.5 0.484 97 3 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.392 78 40--160 0.5 0.419 84 7 0--40

LD:WG121052-4 L55572-3 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.04 0.08 ug/L <MDL <MDL 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.077 0.108 33 0--40Acenaphthylene 0.04 0.08 ug/L 0.326 <MDL 200 * 0--40Acenaphthene 0.04 0.08 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.04 0.2 ug/L 4.97 4.92 1 0--40Fluorene 0.04 0.08 ug/L <MDL <MDL 0--40Phenanthrene 0.04 0.08 ug/L 0.051 0.053 0--40Anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 0.49 0.56 0--40Fluoranthene 0.04 0.08 ug/L <MDL 0.043 0--40Pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Benzyl Butyl Phthalate 0.16 0.32 ug/L 38.8 42.2 8 0--40Benzo(a)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Chrysene 0.04 0.08 ug/L <MDL <MDL 0--40Bis(2-Ethylhexyl)Phthalate 0.16 0.32 ug/L 21.9 27.2 22 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(a)pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L <MDL <MDL 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L <MDL <MDL 0--40

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Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55572-1 88 64L55572-3 108 63L55686-1 93 45L55686-2 102 67L55686-3 109 74WG121052-1 5 * 103WG121052-2 71 107WG121052-3 68 105WG121052-4 84 71

Workgroup: WG121217 (pahll#020 pahphth) Run ID: R200917

MB:WG121217-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L 0.0084 BDimethyl Phthalate 0.008 0.016 ug/L 0.014 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0887 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.0094 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.15 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.079 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.517 BDi-N-Octyl Phthalate 0.008 0.016 ug/L 0.0189 BBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL

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Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG121217-3 SB:WG121217-2 MB:WG121217-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.253 51 40--160 0.5 0.277 55 9 0--402-Methylnaphthalene 0.008 0.016 ug/L 0.0084 0.5 0.34 66 40--160 0.5 0.394 77 15 0--40Dimethyl Phthalate 0.008 0.016 ug/L 0.014 0.5 0.443 86 40--160 0.5 0.488 95 9 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.249 50 40--160 0.5 0.239 48 4 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.347 69 40--160 0.5 0.359 72 3 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0887 0.5 0.591 100 40--160 0.5 0.63 108 7 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.48 96 40--160 0.5 0.497 99 4 0--40Phenanthrene 0.008 0.016 ug/L 0.0094 0.5 0.392 76 40--160 0.5 0.387 76 1 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.408 82 40--160 0.5 0.419 84 3 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.15 0.5 0.923 156 40--160 0.5 0.877 146 5 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.542 108 40--160 0.5 0.512 102 6 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.496 99 40--160 0.5 0.498 100 0 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.079 0.5 0.929 170 * 40--160 0.5 0.909 166 * 2 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.582 116 40--160 0.5 0.574 115 1 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.481 96 40--160 0.5 0.469 94 3 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.517 0.5 1.26 148 40--160 0.5 33.7 6646 * 186 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.0189 0.5 0.873 171 * 40--160 0.5 0.881 172 * 1 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 1.11 111 40--160 1 1.08 108 2 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.165 33 * 40--160 0.5 0.292 58 55 * 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.494 99 40--160 0.5 0.475 95 4 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.479 96 40--160 0.5 0.458 92 5 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.419 84 40--160 0.5 0.405 81 3 0--40

LD:WG121217-4 L55638-1 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L 0.214 0.203 5 0--402-Methylnaphthalene 0.04 0.08 ug/L 0.128 0.115 11 0--40Dimethyl Phthalate 0.08 0.16 ug/L 0.225 0.217 4 0--40Acenaphthylene 0.08 0.16 ug/L <MDL <MDL 0--40Acenaphthene 0.08 0.16 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.08 0.4 ug/L 0.876 0.767 13 0--40Fluorene 0.08 0.16 ug/L 0.081 <MDL 0--40Phenanthrene 0.04 0.08 ug/L 0.151 0.15 0 0--40Anthracene 0.04 0.08 ug/L 0.061 0.064 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 0.61 0.58 0--40

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Fluoranthene 0.04 0.08 ug/L 0.163 0.165 1 0--40Pyrene 0.04 0.08 ug/L 0.168 0.168 0 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 0.503 0.653 26 0--40Benzo(a)anthracene 0.04 0.08 ug/L 0.053 0.052 0--40Chrysene 0.04 0.08 ug/L 0.137 0.135 2 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 7.65 15.6 68 * 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 10.2 10.4 1 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.123 0.126 2 0--40Benzo(a)pyrene 0.04 0.08 ug/L 0.041 0.041 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L 0.041 0.041 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L 0.07 0.071 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55638-1 70 141L55638-2 68 135L55638-3 63 144L55763-1 34 * 87L55763-2 36 * 121L55763-3 57 106WG121217-1 48 136WG121217-2 39 * 125WG121217-3 39 * 126WG121217-4 94 137


MB:WG121458-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L <MDLAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0945 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.014 B

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Anthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.249 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0524 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 2.2 BDi-N-Octyl Phthalate 0.008 0.016 ug/L 0.011 BBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDLBenzo(a)pyrene 0.008 0.016 ug/L <MDLIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDLDibenzo(a,h)anthracene 0.008 0.016 ug/L <MDLBenzo(g,h,i)perylene 0.008 0.016 ug/L <MDL

SBD:WG121458-3 SB:WG121458-2 MB:WG121458-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spiked Blank Duplicate, Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimit TrueValue SBD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 0.5 0.39 78 40--160 0.5 0.342 68 13 0--402-Methylnaphthalene 0.008 0.016 ug/L <MDL 0.5 0.383 77 40--160 0.5 0.337 67 13 0--40Dimethyl Phthalate 0.008 0.016 ug/L <MDL 0.5 0.502 100 40--160 0.5 0.476 95 5 0--40Acenaphthylene 0.008 0.016 ug/L <MDL 0.5 0.437 87 40--160 0.5 0.395 79 10 0--40Acenaphthene 0.008 0.016 ug/L <MDL 0.5 0.41 82 40--160 0.5 0.368 74 11 0--40Diethyl Phthalate 0.008 0.04 ug/L 0.0945 0.5 0.617 105 40--160 0.5 0.612 103 1 0--40Fluorene 0.008 0.016 ug/L <MDL 0.5 0.414 83 40--160 0.5 0.382 76 8 0--40Phenanthrene 0.008 0.016 ug/L 0.014 0.5 0.429 83 40--160 0.5 0.412 80 4 0--40Anthracene 0.008 0.016 ug/L <MDL 0.5 0.378 76 40--160 0.5 0.371 74 2 0--40Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.249 0.5 0.724 95 40--160 0.5 0.708 92 2 0--40Fluoranthene 0.008 0.016 ug/L <MDL 0.5 0.483 97 40--160 0.5 0.458 92 5 0--40Pyrene 0.008 0.016 ug/L <MDL 0.5 0.472 94 40--160 0.5 0.508 102 7 0--40Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0524 0.5 0.751 140 40--160 0.5 0.759 141 1 0--40Benzo(a)anthracene 0.008 0.016 ug/L <MDL 0.5 0.508 102 40--160 0.5 0.52 104 2 0--40Chrysene 0.008 0.016 ug/L <MDL 0.5 0.492 98 40--160 0.5 0.489 98 1 0--40Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 2.2 0.5 1.03 -232 * 40--160 0.5 3.24 209 * 103 * 0--40Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.011 0.5 0.629 124 40--160 0.5 0.63 124 0 0--40Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 1 1.1 110 40--160 1 1.07 107 3 0--40Benzo(a)pyrene 0.008 0.016 ug/L <MDL 0.5 0.41 82 40--160 0.5 0.441 88 7 0--40Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 0.5 0.557 111 40--160 0.5 0.54 108 3 0--40Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 0.5 0.566 113 40--160 0.5 0.549 110 3 0--40Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 0.5 0.507 101 40--160 0.5 0.497 99 2 0--40

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LD:WG121458-4 L55764-2 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Lab Duplicate)Parameter MDL RDL Units SAMP ValuLD Value RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L <MDL <MDL 0--402-Methylnaphthalene 0.04 0.08 ug/L 0.044 0.041 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.31 0.51 49 * 0--40Acenaphthylene 0.04 0.08 ug/L <MDL <MDL 0--40Acenaphthene 0.04 0.08 ug/L <MDL <MDL 0--40Diethyl Phthalate 0.04 0.2 ug/L 1.03 1.1 6 0--40Fluorene 0.04 0.08 ug/L <MDL <MDL 0--40Phenanthrene 0.04 0.08 ug/L 0.154 0.169 10 0--40Anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 2.09 2.51 18 0--40Fluoranthene 0.04 0.08 ug/L 0.213 0.24 12 0--40Pyrene 0.04 0.08 ug/L 0.162 0.177 9 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 21.2 21 1 0--40Benzo(a)anthracene 0.04 0.08 ug/L 0.076 0.0938 21 0--40Chrysene 0.04 0.08 ug/L 0.152 0.162 6 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 8.32 11 28 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 2.8 3.09 10 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.175 0.193 10 0--40Benzo(a)pyrene 0.04 0.08 ug/L 0.0817 0.0898 9 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L 0.068 0.078 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL <MDL 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L 0.0903 0.1 10 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55764-1 48 47L55764-2 47 85L55764-3 44 71L55859-2 56 97L55859-3 53 104L55875-2 55 91L55875-3 53 84L55876-1 60 72L55876-2 66 99L55876-3 48 92WG121458-1 67 96

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WG121458-2 74 98WG121458-3 64 102WG121458-4 50 89


MB:WG121670-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Method Blank)Parameter MDL RDL Units MB Value QualNaphthalene 0.02 0.04 ug/L <MDL2-Methylnaphthalene 0.008 0.016 ug/L <MDLDimethyl Phthalate 0.008 0.016 ug/L 0.0222 BAcenaphthylene 0.008 0.016 ug/L <MDLAcenaphthene 0.008 0.016 ug/L <MDLDiethyl Phthalate 0.008 0.04 ug/L 0.0679 BFluorene 0.008 0.016 ug/L <MDLPhenanthrene 0.008 0.016 ug/L 0.011 BAnthracene 0.008 0.016 ug/L <MDLDi-N-Butyl Phthalate 0.008 0.2 ug/L 0.284 BFluoranthene 0.008 0.016 ug/L <MDLPyrene 0.008 0.016 ug/L <MDLBenzyl Butyl Phthalate 0.008 0.016 ug/L 0.0412 BBenzo(a)anthracene 0.008 0.016 ug/L <MDLChrysene 0.008 0.016 ug/L <MDLBis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 2.14 BDi-N-Octyl Phthalate 0.008 0.016 ug/L 0.0191 BBenzo(b,j,k)fluoranthene 0.008 0.016 ug/L 0.0438 BBenzo(a)pyrene 0.008 0.016 ug/L 0.0173 BIndeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L 0.0324 BDibenzo(a,h)anthracene 0.008 0.016 ug/L 0.0285 BBenzo(g,h,i)perylene 0.008 0.016 ug/L 0.0378 B

SB:WG121670-2 MB:WG121670-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 1 0.76 76 40--1602-Methylnaphthalene 0.008 0.016 ug/L <MDL 1 0.701 70 40--160Dimethyl Phthalate 0.008 0.016 ug/L 0.0222 1 1.07 105 40--160Acenaphthylene 0.008 0.016 ug/L <MDL 1 0.804 80 40--160Acenaphthene 0.008 0.016 ug/L <MDL 1 0.825 83 40--160Diethyl Phthalate 0.008 0.04 ug/L 0.0679 1 1.25 118 40--160

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Fluorene 0.008 0.016 ug/L <MDL 1 0.677 68 40--160Phenanthrene 0.008 0.016 ug/L 0.011 1 0.868 86 40--160Anthracene 0.008 0.016 ug/L <MDL 1 0.902 90 40--160Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.284 1 1.7 142 40--160Fluoranthene 0.008 0.016 ug/L <MDL 1 1.13 113 40--160Pyrene 0.008 0.016 ug/L <MDL 1 0.953 95 40--160Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0412 1 1.55 151 40--160Benzo(a)anthracene 0.008 0.016 ug/L <MDL 1 1.05 105 40--160Chrysene 0.008 0.016 ug/L <MDL 1 0.968 97 40--160Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 2.14 1 2.31 17 * 40--160Di-N-Octyl Phthalate 0.008 0.016 ug/L 0.0191 1 1.33 131 40--160Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L 0.0438 2 2.19 107 40--160Benzo(a)pyrene 0.008 0.016 ug/L 0.0173 1 0.969 95 40--160Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L 0.0324 1 1.07 104 40--160Dibenzo(a,h)anthracene 0.008 0.016 ug/L 0.0285 1 1.07 104 40--160Benzo(g,h,i)perylene 0.008 0.016 ug/L 0.0378 1 0.93 89 40--160

MSD:WG121670-4 MS:WG121670-3 L55936-2 Matrix: STORM WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP ValuTrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L 0.695 1 1.43 74 40--160 1 1.48 79 4 0--402-Methylnaphthalene 0.04 0.08 ug/L 1.01 1 1.66 66 40--160 1 1.77 76 6 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.362 1 1.69 133 40--160 1 1.44 108 16 0--40Acenaphthylene 0.04 0.08 ug/L <MDL 1 0.894 89 40--160 1 1 100 11 0--40Acenaphthene 0.04 0.08 ug/L <MDL 1 0.863 86 40--160 1 0.969 97 12 0--40Diethyl Phthalate 0.04 0.2 ug/L 1.25 1 2.36 111 40--160 1 2.38 113 1 0--40Fluorene 0.04 0.08 ug/L 0.052 1 0.813 76 40--160 1 0.87 82 7 0--40Phenanthrene 0.04 0.08 ug/L 0.275 1 1.14 86 40--160 1 1.17 90 3 0--40Anthracene 0.04 0.08 ug/L 0.049 1 0.885 84 40--160 1 0.967 92 9 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 2.05 1 2.84 79 40--160 1 2.92 87 3 0--40Fluoranthene 0.04 0.08 ug/L 0.353 1 1.3 95 40--160 1 1.36 101 5 0--40Pyrene 0.04 0.08 ug/L 0.308 1 1.07 77 40--160 1 1.15 84 7 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 5.12 1 6.6 148 40--160 1 6.87 175 * 4 0--40Benzo(a)anthracene 0.04 0.08 ug/L 0.091 1 1.03 93 40--160 1 1.12 103 9 0--40Chrysene 0.04 0.08 ug/L 0.224 1 1.07 85 40--160 1 1.15 93 8 0--40Bis(2-Ethylhexyl)Phthalate 0.04 0.08 ug/L 11.8 1 13.1 134 40--160 1 12.5 77 4 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 4.99 1 5.57 59 40--160 1 5.5 51 1 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.277 2 2.05 89 40--160 2 2.11 92 3 0--40Benzo(a)pyrene 0.04 0.08 ug/L 0.102 1 0.965 86 40--160 1 0.99 89 3 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L 0.0875 1 1.04 96 40--160 1 1.09 100 4 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL 1 1.02 102 40--160 1 1.05 105 3 0--40

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Benzo(g,h,i)perylene 0.04 0.08 ug/L 0.139 1 0.966 83 40--160 1 0.981 84 2 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55936-2 67 70WG121670-1 65 88WG121670-2 74 100WG121670-3 67 73WG121670-4 59 72

Workgroup: WG121757 (pahll#023 pahphth-sim-lvi-ll) Run ID: R201081


SB:WG121757-2 MB:WG121757-1 Matrix: BLANK WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project: Pkey:STD

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(Spike Blank, Method Blank)Parameter MDL RDL Units MB Value TrueValue SB Value % Rec. Qual LabLimitNaphthalene 0.02 0.04 ug/L <MDL 1 0.799 80 40--1602-Methylnaphthalene 0.008 0.016 ug/L 0.0082 1 0.74 73 40--160Dimethyl Phthalate 0.008 0.016 ug/L 0.015 1 1.08 106 40--160Acenaphthylene 0.008 0.016 ug/L <MDL 1 0.848 85 40--160Acenaphthene 0.008 0.016 ug/L <MDL 1 0.848 85 40--160Diethyl Phthalate 0.008 0.04 ug/L 0.074 1 1.24 117 40--160Fluorene 0.008 0.016 ug/L <MDL 1 0.694 69 40--160Phenanthrene 0.008 0.016 ug/L 0.01 1 0.901 89 40--160Anthracene 0.008 0.016 ug/L <MDL 1 0.906 91 40--160Di-N-Butyl Phthalate 0.008 0.2 ug/L 0.341 1 1.58 124 40--160Fluoranthene 0.008 0.016 ug/L <MDL 1 1.13 113 40--160Pyrene 0.008 0.016 ug/L <MDL 1 0.932 93 40--160Benzyl Butyl Phthalate 0.008 0.016 ug/L 0.0476 1 1.57 152 40--160Benzo(a)anthracene 0.008 0.016 ug/L <MDL 1 1.07 107 40--160Chrysene 0.008 0.016 ug/L <MDL 1 0.99 99 40--160Bis(2-Ethylhexyl)Phthalate 0.008 0.016 ug/L 0.933 1 3.54 260 * 40--160Di-N-Octyl Phthalate 0.008 0.016 ug/L <MDL 1 1.32 132 40--160Benzo(b,j,k)fluoranthene 0.008 0.016 ug/L <MDL 2 2.18 109 40--160Benzo(a)pyrene 0.008 0.016 ug/L <MDL 1 0.928 93 40--160Indeno(1,2,3-Cd)Pyrene 0.008 0.016 ug/L <MDL 1 1.13 113 40--160Dibenzo(a,h)anthracene 0.008 0.016 ug/L <MDL 1 1.15 115 40--160Benzo(g,h,i)perylene 0.008 0.016 ug/L <MDL 1 0.994 99 40--160

MSD:WG121757-4 MS:WG121757-3 L55698-1 Matrix: SEWER WTR Listtype:ORPAHPHTH-SIM-LVI-LL Method:SW846 3520C*8270D SIM Project:423589-320-4 Pkey:STD(Matrix Spike Duplicate, Matrix Spike)Parameter MDL RDL Units SAMP ValuTrueValue MS Value % Rec. Qual LabLimit TrueValue MSD Value % Rec. Qual RPD Qual LabLimitNaphthalene 0.1 0.2 ug/L <MDL 1 0.778 78 40--160 1 0.763 76 2 0--402-Methylnaphthalene 0.04 0.08 ug/L <MDL 1 0.879 88 40--160 1 0.866 87 1 0--40Dimethyl Phthalate 0.04 0.08 ug/L 0.331 1 1.34 101 40--160 1 1.31 98 3 0--40Acenaphthylene 0.04 0.08 ug/L <MDL 1 0.944 94 40--160 1 0.917 92 3 0--40Acenaphthene 0.04 0.08 ug/L <MDL 1 0.893 89 40--160 1 0.804 80 10 0--40Diethyl Phthalate 0.04 0.2 ug/L 2.87 1 4.11 124 40--160 1 4.06 118 1 0--40Fluorene 0.04 0.08 ug/L <MDL 1 0.794 79 40--160 1 0.773 77 3 0--40Phenanthrene 0.04 0.08 ug/L 0.14 1 0.906 77 40--160 1 0.907 77 0 0--40Anthracene 0.04 0.08 ug/L <MDL 1 0.853 85 40--160 1 0.848 85 1 0--40Di-N-Butyl Phthalate 0.04 1 ug/L 1.63 1 2.67 104 40--160 1 2.88 125 8 0--40Fluoranthene 0.04 0.08 ug/L 0.159 1 0.876 72 40--160 1 0.901 74 3 0--40Pyrene 0.04 0.08 ug/L 0.135 1 0.706 57 40--160 1 0.742 61 5 0--40Benzyl Butyl Phthalate 0.04 0.08 ug/L 12.2 1 12.7 51 40--160 1 13.2 98 4 0--40

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Benzo(a)anthracene 0.04 0.08 ug/L 0.058 1 0.713 65 40--160 1 0.708 65 1 0--40Chrysene 0.04 0.08 ug/L 0.075 1 0.706 63 40--160 1 0.657 58 7 0--40Bis(2-Ethylhexyl)Phthalate 0.4 0.8 ug/L 8.25 1.01 111 10183 * 40--160 1 12.2 391 * 160 * 0--40Di-N-Octyl Phthalate 0.04 0.08 ug/L 1.01 1 1.52 51 40--160 1 1.71 70 12 0--40Benzo(b,j,k)fluoranthene 0.04 0.08 ug/L 0.117 2 1.23 56 40--160 2 1.33 60 7 0--40Benzo(a)pyrene 0.04 0.08 ug/L <MDL 1 0.576 58 40--160 1 0.623 62 8 0--40Indeno(1,2,3-Cd)Pyrene 0.04 0.08 ug/L <MDL 1 0.56 56 40--160 1 0.569 57 2 0--40Dibenzo(a,h)anthracene 0.04 0.08 ug/L <MDL 1 0.587 59 40--160 1 0.568 57 3 0--40Benzo(g,h,i)perylene 0.04 0.08 ug/L 0.045 1 0.529 48 40--160 1 0.56 51 6 0--40

Surrogate:

2-Fluorobiphenyl

d14-Terphenyl

(Lab Limits) 40--160 40--160L55698-1 68 68WG121757-1 71 94WG121757-2 69 95WG121757-3 73 67WG121757-4 69 64



Appendix D-2: Validation of Data Generated by AXYS

Analytical Laboratory

Appendix D Data Validation - King County

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