loo. - 6 Feb 2017 14:55

• .

December 7, 1999

Practical Environmental Solutions

I .'

Ms. Karen Harmon ', North Carolina Department of Environment and Natural Resources Division of Waste Management, UST Section 3800 Barrett Drive, Suite 101 Raleigh, NC 27609

Re: Quarterly Site Status Monitoring Report Second and Third Quarter 1999 Exxon Party Pickup Route US 1 South Franklinton, North Carolina DWQ Incident # 6897

Dear Mr. Boyles:

•

...

On behalf of the Warren Oil Company, Handex of the Carolinas, Inc. (Handex) has prepared the attached second and third quarter 1999 site status monitoring report of remediation for the referenced site. This report summarizes system operation, groundwater quality monitoring, and field activities completed from April 1 through September 31, 1999.

Should you have any questions or comments concerning the attached report, please feel free to contact our office at (704) 598- 7900.

Sincerely,

H nde< "'['\[;;}'"· loo.

achary . Hall, L.G. enior H drogeologist

NC License #1630

Attachment

cc: Mark Warren - Warren Oil Company Vicki Garcia - Hand ex of Florida

{t Chr~. Ward, L. Senior Project Manager NC License #1600

3600-G Woodpark Blvd., Charlotte, NC 28206 • (704) 598-7900 • Fax: (704) 598-2248

i ;I

I I I I I I I I I I I I I I I I I I

Practical Environmental Solutions

QUARTERLY SITE STATUS MONITORING REPORT SECOND AND THIRD QUARTER 1999

CITGO (FORMERLY EXXON) PARTY PICKUP ROUTE US 1 SOUTH

FRANKLINTON, NORTH CAROLINA DWQ INCIDENT# 6897

Report Prepared For:

WARREN OIL COMPANY SOUTH BICKETT BOULEVARD

P.O. BOX 270 LOUISBURG, NORTH CAROLINA 27549

Report Prepared By:

HANDEX OF THE CAROLINAS, INC. 3600-G WOODPARK BOULEVARD

CHARLOTTE, NORTH CAROLINA 28206

,;1•

J.: .. ··, . . . ~ ... · .. -

Christ er J. Ward, L.G. NC Li nse Geologist #1600

3600-G Woodpark Blvd., Charlotte, NC 28206 • (704) 598-7900 • Fax: (704) 598-2248

I I I I I I I I I I I I I I I I I I I

TABLE OF CONTENTS ITEM PAGE

1.0 INTRODUCTION ................................................................................................. 1

2.0 OPERATIONAL STATUS ........................................... ......................................... 1 2. 1 Remediation System Configuration ............................................................ 1 2.2 Recovery and Treatment Systems Performance ........................................ 2 2.3 Remediation System Maintenance ............................................................. 2

3.0 LIQUID-LEVEL GAUGING ..................................................... .......................... 2

4.0 GROUNDWATER SAMPLING ............................................................................. 3 4.1 Monitoring and Recovery Well Sampling ................................................... 3 4.2 Potable Well and Surface Water Sampling .............................................. .4

5.0 TREATMENT SYSTEM MONITORING ............................................... ........... 5

6.0 CONCLUSIONS AND RECOMMENDATIONS ................................................ ... 6 6.1 Summary .................................................................................................... 6 6.2 Action Items and Recommendations .......................................................... 6

FIGURES

FIGURE 1: Topographic Location Map FIGURE 2: Site Plan FIGURE 3: Water Table Contour Map (Data Date: 6/17/99) FIGURE 3A: Water Table Contour Map (Data Date: 9/23/99) FIGURE 4: Groundwater Benzene Concentration Map (Data Date: 6/17/99) FIGURE 4A: Groundwater Benzene Concentration Map (Data Date: 9/23/99) FIGURE 5: Groundwater Total BTEX Concentration Map (Data Date: 6/17/99) FIGURE SA: Groundwater Total BTEX Concentration Map (Data Date: 9/23/99) FIGURE 6: Groundwater MTBE Concentration Map (Data Date: 6/17/99) FIGURE 6A: Groundwater MTBE Concentration Map (Data Date: 9/23/99)

TABLE 1: TABLE 2: TABLE 3: TABLE 4:

TABLES

Effluent Flow Readings Groundwater Analytical Data Summary Groundwater Treatment System Analytical Summaries Groundwater Treatment System Efficiency

-------------------

MONITORING REPORT- DATES

REPORT /Jh jq<) ·~:::::-17"· ~-MONITORING EVENT q/.::3/55 r '

~ RECEIPT o/8/00 ' -"- DATABASE ENTRY' . /))toJ1?j

r ' REVIEW--------REVIEWER---------

MONITORING REPORT INFORMATION

INCIDENTNAME &on ]ar-b ~duf?

INCIDENT# ~X-'-9_,_7 __ -,-,-----,--RANK 'Z"f\_±__ RISK l-f11Df= COUNTY E!LA-d!/Ci-IN MANAGER QL)-/

I I APPENDIX A:

APPENDICES

Observation Well Gauge Report

I APPENDIX 8: APPENDIX C:

Groundwater Quality Laboratory Analytical Report Groundwater Treatment System Analytical Reports (4/99- 9/99)

I I I I I I I I I I I I I I I I


1.0 INTRODUCTION

In accordance with the authorization of Warren Oil Company, Handex of the Carolinas,

Inc. (Handex) has prepared this second and third quarter 1999 site status monitoring

report for the Citgo (formerly Exxon) Party Pickup, located on Route US 1 South,

approximately 500 feet south of its intersection with State Route 56, in Franklinton,

North Carolina. A topographic location map showing the location of the site in relation

to nearby potable water sources and local surface features is presented as Figure 1.

The site is situated approximately 450 feet upgradient and at an elevation 70 feet

higher than the Sally Kearney Creek, a tributary to the Franklinton Reservoir. A site

plan showing the locations of monitoring wells, recovery wells, the creek and pond, and

the treatment system relative to other pertinent site features is presented as Figure 2.

This report summarizes groundwater recovery and treatment system operations,

treatment system efficiency monitoring, groundwater quality monitoring, and field

activities completed from April 1 through September 30, 1999.

2.0 OPERATIONAL STATUS

2.1 Remediation System Configuration

The remediation system at the site includes four active groundwater recovery wells

(RW-3, RW-4, RW-5, and MW-34}, each employing pneumatic pumps. Total fluids

from the recovery wells are first routed to an oil/water separator (OWS), where an iron

sequestering agent (Uitratreat C738S - tetrasodium salt of ethylenediaminetetraacetic

acid) is added to the process stream to minimize iron fouling of the remediation

equipment. Water from the OWS flows to a mixing tank, and is then pumped through a

particulate filter to a packed tower air stripper. From the air stripper, water is passed

through a 2,000-pound granular activated carbon adsorption vessel for final polishing.

Discharge of the treated water is to Sally Kearney Creek under National Pollutant

Discharge Elimination System (NPDES) General Permit Number NCG510046. Any

recovered liquid-phase petroleum hydrocarbons (LPH) are directed from the OWS by

gravity feed to a grounded 275-gallon vented steel aboveground tank for later

recycling.


Because the Sally Kearney Creek is a source for the Franklinton Reservoir, two

aerators are employed in the downgradient pond to further decrease the potential for

hydrocarbon migration from the site into the potable surface water supply. The

groundwater recovery and treatment systems were activated in their current

configuration in early 1993.

2.2 Recovery and Treatment Systems Performance

The recovery and treatment systems are inspected weekly by Handex personnel,

during which flow meter readings are checked and recorded, per NPDES Permit

requirements. The flow meter readings, total gallons recovered, and the average flow

rate from the remediation system are summarized in Table 1. From April 1, 1999

through September 30, 1999, a total of 769,354 gallons of groundwater was

remediated. The average flow rate for all four recovery wells for the period was 2.91

gallons per minute (gpm) (approximately 0.72 gpm per well). Since system activation in

early 1993, a total of 9,062,530 gallons of groundwater has been remediated.

With the exception of a few power outages, the remediation system was operative for

the remainder of the reporting period.

2.3 Remediation System Maintenance

Weekly O&M was conducted throughout the two quarter monitoring period. On June,

23, 1999, the check valve at MW-34 was replaced.

3.0 LIQUID-LEVEL GAUGING

Recovery wells are gauged for depth to water on a weekly basis to confirm system

operation and wellhead drawdown. All site monitoring and recovery wells are gauged

monthly for depth to water and presence of LPH using an electronic oil/water interface

probe. On July 21, 1999, depth to groundwater ranged from 1.26 to 49.14 feet below

land surface (BLS). On September 22, depth to groundwater ranged from 1.94 to 48.16

feet below land surface (BLS). These data were used to prepare the water table

contour maps shown on Figure 3 and Figure 3A. Groundwater depth and elevation

data are summarized in the well gauge monitoring report, included in Appendix A.

2


The water table elevations were calculated and plotted on a map of the site. Referring

to Figures 3 and 3A, groundwater flow is generally to the north-northwest. The water

table contours and elevations presented in Figures 3 and 3A indicate that the

groundwater recovery system is operating as expected, producing an apparent

drawdown of five to ten feet in the four active recovery wells. LPH were not

encountered during this monitoring event.

4.0 GROUNDWATER SAMPLING

4.1 Monitoring and Recovery Well Sampling

On June 17, 1999, groundwater samples were collected from twelve of the thirty site

monitoring wells (MW-2, -3, -12, -14, -16, -26, -27, -29, -30, -31, -32, and -33), and the

six recovery wells (RW-1 through RW-5, and MW-34). With the exception of MW-2,

the same wells were sampled during the September 23, 1999 sampling event.

Groundwater samples were retrieved from the monitoring wells and inactive recovery

wells using dedicated disposable bailers, and from the active recovery wells at the

system influent ports. A different bailer was used for each monitoring well sampled to

minimize the potential for cross-contamination. Prior to sampling, each well was

purged by hand-bailing or pumping (as appropriate) three to five well volumes of water

from the well to ensure a representative groundwater sample was obtained from the

aquifer. The water samples were shipped to Specialized Assays Environmental, Inc.

(Specialized Assays) in Nashville, Tennessee, where they were analyzed for purgeable

halocarbons and aromatics by EPA Method 8021 B (extended to include isopropylether

(IPE) and metyl-tertiary-butyl-ether (MTBE)) and for total lead by EPA Method 3030C.

When the results of the June sampling event are compared to the March 1999

sampling event, benzene concentrations decreased or remained below laboratory

detection limits in ten of the twelve monitoring wells sampled. MTBE concentrations

decreased or remained below the Title 15A, Subchapter 2L of the North Carolina

Administrative Code [15A NCAC 2L] standard of 200 J.lg/L in seven of the twelve

sampled monitoring wells. Naphthalene concentrations decreased or remained below

the 15A NCAC 2L standard of 21 J.lQ/L in six of the twelve monitoring wells sampled.

3


Chloroform and 1 ,2-dichloroethane concentrations decreased or remained below 15A

NCAC 2L standards in eleven of the twelve wells sampled. Lead concentrations were

below the 15A NCAC 2L standard of 0.015 mg/L in eleven of the twelve wells sampled.

Comparing the September 1999 sampling results to the June 1999 sampling results,

benzene concentrations decreased or remained below laboratory detection limits in ten

of the eleven monitoring wells sampled. MTBE concentrations decreased or remained

below the Title 15A, Subchapter 2L of the North Carolina Administrative Code [15A

NCAC 2L] standard of 200 Jlg/L in nine of the eleven sampled monitoring wells.

Naphthalene, chloroform and 1 ,2-dichloroethane were not analyzed during the

September sampling event. Lead concentrations were below the 15A NCAC 2L

standard of 0.015 mg/L in all of the samples collected.

4-Chlorotoluene and 1 ,2,3- trichlorobenzene were detected for the first time during the

March sampling event, however were not detected during the June sampling event.

The wells sampled and analytical results are summarized in Table 2. Dissolved

benzene, total BTEX, and MTBE concentration maps are shown on Figures 4, 5, and 6

for the June 1999 sampling event and Figures 4A, 5A and SA for the September 1999

sampling event, respectively. The laboratory analytical reports from Specialized

Assays are included in Appendix B.

4.2 Potable Well and Surface Water Sampling

Four potable water supply wells in the vicinity of the site (W-1, W-2, W-27, and W-30

(also known as the Claude C. Hayes Well [CCHW])}, and the downgradient pond

discharge point were sampled on June 17, 1999 and September 23, 1999. The water

supply well locations are shown on the Topographic Location Map, presented as

Figure 1. The water supply wells were purged for several minutes prior to sampling to

ensure a representative groundwater sample was obtained from the aquifer. The pond

discharge sample was collected directly from the water stream at the base of the

impoundment. The water samples were shipped to Specialized Assays for the above

listed parameters.

4


As shown by the June 1999 sampling event, W-1 had detectable concentrations of

naphthalene (4 ug/L), toluene (1 ug/L), and xylenes (2 ug/L). W-27 revealed

detectable (0.005 mg/L) concentrations of lead. With this exception, none of the other

tested organic analytes was encountered in the potable water supply wells or the pond

discharge.

According to the September 1999 analytical report, none of the sampled potable wells

had detectable concentrations of any of the analyzed constituents. However, the pond

revealed detectable concentrations (1.8 ug/L) of MTBE. The analytical results are

summarized in Table 2. The laboratory analytical report from Specialized Assays is

included in Appendix B.

5.0 TREATMENT SYSTEM MONITORING

The treatment system is checked twice weekly by Warren Oil Company personnel, and

weekly by Handex personnel to verify that it is functioning normally, and to perform

various items of system maintenance. The treatment system has functioned as

designed and was successful in treating approximately 769,354 gallons of groundwater

during the period from April 1, 1999 through September 30, 1999.

System effluent samples are collected monthly to monitor treatment system efficiency

and compliance with NPDES permit discharge requirements. Monthly system

discharge samples are analyzed for 1 ,2-dichloroethane by EPA Method 601, purgeable

aromatic compounds (BTEX, MTBE, and IPE) by EPA Method 602, oil & grease by EPA

Method 9071, total iron and manganese by ICP, and total suspended solids.

System influent and pre-carbon polish samples are collected and analyzed for

purgeable aromatic compounds (BTEX, MTBE, and IPE) by EPA Method 602 to help

track system performance. Monthly groundwater treatment system analytical results for

April through September 1999 are summarized in Table 3. All results indicated

concentrations lower than those specified in the NPDES General Permit. Laboratory

analytical data sheets are presented in Appendix C.

5

I I I

The efficiency of the groundwater treatment system is tracked as a function of benzene,

total BTEX, and MTBE reduction following the stripper tower and the carbon polishing

unit. System efficiency calculation results are presented in Table 4. The average

I efficiency of the tower for this reporting period was 96.49%, and of the carbon, 100%.

I I I I I I I I I I I I I I I

6.0 CONCLUSIONS AND RECOMMENDATIONS

6.1 Summary

During the second and third quarter 1999 reporting period, the recovery and treatment

systems at the Citgo (formerly Exxon) Party Pickup operated as designed, and

successfully recovered and treated approximately 769,354 gallons of groundwater.

During the next quarterly period, Handex and Warren Oil personnel will continue to

monitor and maintain the recovery and treatment systems. The next quarterly sampling

event will be conducted in January 2000 utilizing the same wells and for the same

analyses.

6.2 Action Items and Recommendations

Based on operational and analytical data collected during past quarters of operation,

the following observations and recommendations are made:

• Groundwater dissolved hydrocarbons observed in the site monitoring and recovery wells do not appear to have impacted any of the surrounding potable water supply wells. There was a slight impact of naphthalene, toluene, and xylenes in W-1.

• During the June sampling event concentrations of BTEX compounds at or above their respective 15A NCAC 2L standards were detected in twelve of the twentythree sample points. Chloroform and 1 ,2-dichloroethane was detected in one sample point at a concentration above its respective 15A NCAC 2L standards. Naphthalene was detected in eight sampling points at concentrations above its 15A NCAC 2L standard. During the September sampling event BTEX compounds at or above their respective 15A NCAC 2L standards were detected in eight of the eleven monitoring wells sampled.

6


• The areal extent of hydrocarbon compounds appears to be localized to the vicinity of the recovery wells and their respective upgradient capture zones. Past studies have indicated that soil vapor extraction in conjunction with air sparging would be effective in increasing the remedial capacity of the system.

• Due to the existence of an extensive groundwater analytical database which includes quarterly data since 1997, and to reduce site spending, Handex recommends a semi-annual sampling program for the site. Groundwater samples would be collected in January and July and analyzed by EPA methods 80218 including IPE and MTBE. Sampled wells should include MW-2,-3,-12,-14,-16,-26,-27,-29,-30,-31,-32,-33, RW-1 through RW-5 and MW-34.

7

I I

I I I I I I I I I I FIGURES

I I I I I I I I I ~·HANDEX®

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QUADRANGLE LOCATION

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lr ARREN OIL COMPANY, PAKI'Y PICKUP U~. HICHir AY I

FRANKLINTON. NOKTH CAROLINA

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I I I I I g

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DATA DATE: 06-17-99

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S~.iW-30 BDL

WARREN OIL COMPANY, PARTY PICKUP U.S. H ICHW AY 1

FRANKLINTON. NORTH CAROLINA

- - - - - - -I LEGE><>

S WI-X

~0 M::NTCRN:::; W'ELL: ~ MW-X

RECOVERY lf.IElL ~ RW-X

.AR SPARe£ WELL: 0 ASP-X

MTE£ ~RATCN (,ug/1): 196

MTE£ r50CCMQR ( l-'-9fl) ~100 _____./ l'ff~D 'M-EN DASl-£0:

E£LOW DETECTia-.1 LIMIT: BDL

NOTE: ACTIVE RECOVERY WELLS AND BEDROCK WELLS NOT USED IN CONSTRUCTING CONTOURS.

o20•o eo i""""'\MJ I

SC"LE 1 W

FIGURE 6A GROUNDWATER MTBE CONCENTRATION MAP

DATA DATEo 09-23-99

SC/11£ r · ao· PROJ. NO. 109155

O.O.TE: 11-23-99 ''"" X DfM aY: D.B. C915535H

i

'I I I I I I I I I I I I I I I I I I I

TABLES

4_, 'HANDEX® -


Table 1

Effluent Flow Readings

Citgo Party Pickup Route US 1 South Franklinton, North Carolina

As of: Wednesday June 30, 1999

Effluent Flowmeter

D a t e Reading (gallons)

Wednesday, 31-Mar-99 8,703,243 Wednesday, 07 -Apr-99 8,743,465 Wednesday, 14-Apr-99 8,752,570 Wednesday, 21-Apr-99 8,795,405 Wednesday, 28-Apr-99 8,828,310 Wednesday, 05-May-99 8,868,630 Wednesday, 12-May-99 8,907,810 Wednesday, 26-May-99 8,956,701 Wednesday, 02-Jun-99 9,008,296 Wednesday, 09-Jun-99 9,012,851 Wednesday, 16-Jun-99 9,056,321 Wednesday, 23-Jun-99 9,086,910 Wednesday, 30-Jun-99 9,113,310

Amount Processed Since Last

Date (gallons) •••

40,222 9,105

42,835 32,905 40,320 39,180 48,891 51,595 4,555

43,470 30,589 26,400

Total gallons treated this quarter= 410,067 Average flow rate this quarter= 3.39

Average Flow Rate

(gpm)

****

4.0 0.9 4.2 3.3 4.0 3.9 4.9 5.1 0.5 4.3 3.0 2.6


Table 1

Effluent Flow Readings


As of: Wednesday September 29, 1999

Effluent Flowmeter

D a t e Reading (gallons)

Wednesday, 07 -Jul-99 9,146,490 Wednesday, 14-Jul-99 9,179,950 Wednesday, 21-Jul-99 9,211,541 Wednesday, 28-Jul-99 9,239,043 Wednesday, 04-Aug-99 9,268,831 Wednesday, 11-Aug-99 9,292,071 Wednesday, 18-Aug-99 9,317,317 Wednesday, 25-Aug-99 9,344,394 Wednesday, 01-Sep-99 9,377,683 Wednesday, 08-Sep-99 9,401,941 Wednesday, 15-Sep-99 9,449,492 Wednesday, 22-Sep-99 9,486,150 Wednesday, 29-Sep-99 9,505,777

Amount Processed Since Last

Date (gallons) •••

33,460 31,591 27,502 29,788 23,240 25,246 27,077 33,289 24,258 47,551 36,658 19,627

Total gallons treated this quarter= 359,287 Average flow rate this quarter= 2.71

h:l ... hol/i_jlwarrenlwrrnflow.xls

Average Flow Rate

(gpm)

**** 3.3 3.1 2.7 3.0 2.3 2.5 2.7 3.3 2.4 4.7 3.6 1.9

,. JO ~ .e..:.

- - - - - - - - - - - - - - -

Sj)fz:IW8-IJI()

RUUOJr.III!ION 'UOIUU~UIJ~ lllftOS I Sn "'J10ll

dn>pld All•d o8!r.>

.<IIIWWIIS 11110 IROA-<illliV -nOJ!)

z •lq•!

- - - -

.,,.n G) ~ I ;oil a !!: il:!to " • -c:-a I ~

ij- .. •

'~ ,_q

"'i:!! I ~ o n 1: j ~ •

II ... i: &' !!. ! i ~ I .,

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i I N

a .

I /

- - - -Table 2

Groundwater Analyllcalllato Sununary

Clt;o Party Pickup Routa US 1 South Franklinton, North Corollna

Gol_lll'IBI2.»s

- - - - - - - - - - - - - - -

Page 3 oU

- - - -Table 2

Groundwater Analytical Data Summary

Clt;o Party Pickup Route US 1 South Franklinton, North Corollna

M~,.-..,EPA-102tii(Jo01..).

_.,t~.llyi!PA-lOJOC~.

~ .. - .......... W-2t. ~ .... ,..,...... IC)•Noi~IIIL--,~.

NS•NIII~

~_anel2.lds

- - - - - - - - - - - - - - -

Page4of4


Table 3

Groundwater Treatment System Analytical Summaries


B¢i1iene· T.ollJehe .... Ethylb.eniei\e · Xylen1es TotaiBTEX MethYl ieri'butyrEttier .

ug/LF ... ··•···•· Beniene··· ···.·······. ···· i:61uerie. • ..•. S!~Y~~~n~ene ., Xylerl~s T.61aiBT.EX M~ilhlti~it~bul'/1 Ether

ND - Non Detect NS- Analyte not sampled

h:J ... hoiiiJiwarrenlsys_anal.xls

May 12, 1999 Influent Midpoint Effluent

87.8 ND ND 2760 3.8 ND 58.4 ND ND 257 5.9 ND

3163.2 9.7 ND .. 1450 201.0 113.0

June 17, 1999 Influent . Midpoint Effluent

597 5.0 ND 2780 8.7 ND

385 1 . 1 ND 3160 12.9 ND 6922 27.7 ND 1780 142.0 NS

Analytical Summary


Table 3

Groundwater Treatment System Analytical Summaries


ug/L~

Benzene r6iU~ne ... E:thYI\Jenzene . · ..• ····•··· Xvleries i · •.•••..•. · • .••... ·.·.· . To)~ I BTE~ i. · .. · · · .. MethYI.tert,butYI Ether.·.·

August 25, 1999 Influent

600 . 2150 550

2800 6100 1300

September 23, 1999 IJg/L Benzene Toluene E;t~yii:Jehzellei Xylenes · .•. Jotalf3TEX i .•.. ··••·.·

Me!Hyl\eiiiiJulvrE:tiler ·· / . ·

ND - Non Detect NS - Analyte not sampled

Influent 655

2460 330 870

4315 3020

Midpoint ND 1.0 ND 3.0 4.0

111.0

Midpoint 1.4 4.1 ND 8.6

14.1 219.0

Effluent ND ND ND ND ND NS

Effluent ND ND ND ND ND NS


Table 4

Groundwater Treatment System Efficiency


h:l. •• ho/1/Jiwarren/sys_anal.xls System Efflclancy


Table 4

Groundwater Treatment System Efficiency


August 26, 1999

~~Qtl'lQ!l (llgfL)) ·.• · · . /. . ·.····... 600 0.0 E:tficiency .. < .... /.. .·.· ... · .... •·· / > 1 oo.oo%

T9!~!~T~~ \~~~L~\ · ·. . . ···· ····•··.··· 61 oo 4.o Effic1encv! ......... · ......... i ........• ·.·.... . .... · .. · . . ) 99.93% M~thylt!;lit\IJYtyl Ether (ugtt:) . ··.· • ·•···· ·•·· ···.·. 13oo 111.0 Eifii::ieiicyi · · ·· · · . · 91.46%

Post Carbon 0.0

100.00% 0.0

100.00% 0.0

100.00%

i I I I I I I I I I I I I I I I I I I I

APPENDIX A

OBSERVATION WELL GAUGE REPORT

I OBSERVATION WELL GAUGE REPORTS

I CLIENT: WARREN OIL CLIENT CODE: LOCATION: PARTY PICKUP/US 1, FRANKLINTON HAND EX CODE: 109155

I STATE: NC

Print date: 11/18/99 Page 1

I MONITORING WELL c PRODUCT WATER PRODUCT PRODUCT GW CORR GW DATE TYPE-# DEPTH DEPTH THICK. ELEV. ELEV. ELEV.

(feet) (feet) (feet) (feet) (feet) (feet)

I 20-Jan-99 MW-1

I 20-Jan-99 MW-2 1.13 378.34 378.34 20-Jan-99 MW-3 3.52 374.48 374.48 20-Jan-99 MW-4 3.26 374.19 374.19 20-Jan-99 MW-5 3.66 374.11 374.11

I 20-Jan-99 MW-6 5.19 374.08 374.08 20-Jan-99 MW-7 4.83 373.99 373.99 20-Jan-99 MW-8

I 20-Jan-99 MW-9 6.47 371.18 371. 18 20-Jan-99 MW-10 6.32 371.17 371.17 20-Jan-99 MW-11 36.50 370.68 370.68 20-Jan-99 MW-12 49.38 384.38 384.38

I 20-Jan-99 MW-13 45.62 384.90 384.90 20-Jan-99 MW-14 43.40 387.40 387.40 20-Jan-99 MW-16 38.33 392.46 392.46

I 20-Jan-99 MW-17 20-Jan-99 MW-18 20-Jan-99 MW-19 20-Jan-99 MW-20 36.30 398.37 398.37

I 20-Jan-99 MW-21 7.04 371.79 371.79 20-Jan-99 MW-22 6.12 372.15 372 0 15 20-Jan-99 MW-23 1. 91 376.87 376.87


I 20-Jan-99 MW-27 6.52 374.67 374.67 20-Jan-99 MW-28 8.40 374.98 374.98 20-Jan-99 MW-29 32.34 386.14 386.14 20-Jan-99 MW-30 16.08 379.45 379.45


I 20-Jan-99 MW-34 48.22 369.43 369.43 20-Jan-99 AW-l 11.91 375.52 375.52 20-Jan-99 RW-1 47.14 376.87 376.87 20-Jan-99 RW-2 17.71 375.82 375.82

I 20-Jan-99 RW-3 20.08 373.11 373.11 20-Jan-99 RW-4 21.50 372.01 372.01

I "C"omments: [P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment]

I [I = Well Inaccessible; # = nth Monitoring Event of Day] [D = Dry Well; F = Film or Trace of Product] 109155

I

I I I I I I I I I I D I I I I I I I I

I Print date: 11/18/99 Page 2


I (feet) (feet) (feet) (feet) (feet) (feet)

20-Jan-99 RW-5 19.91

I 20-Jan-99 PW-1 44.08 375.09 375.09

17-Feb-99 MW-1

I 17-Feb-99 MW-2 1.16 378.31 378.31 17-Feb-99 MW-3 3.71 374.29 374.29 17-Feb-99 MW-4 3.33 374.12 374.12 17-Feb-99 MW-5 3.69 374.08 374.08

I 17-Feb-99 MW-6 5.19 374.08 374.08 17-Feb-99 MW-7 4.84 373.98 373.98 17-Feb-99 MW-8

I 17-Feb-99 MW-9 6.58 371.07 371. 07 17-Feb-99 MW-10 6.40 371.09 371. 09 17-Feb-99 MW-11 35.75 371.43 371.43


I 17-Feb-99 MW-17 17-Feb-99 MW-18 17-Feb-99 MW-19

I 17-Feb-99 MW-20 35.63 399.04 399.04 17-Feb-99 MW-21 7.31 371.52 371. 52 17-Feb-99 MW-22 6.20 372.07 372.07 17-Feb-99 MW-23 3.48 375.30 375.30

I 17-Feb-99 MW-24 9.24 373.94 373.94 17-Feb-99 MW-25 9.97 374.07 374.07 17-Feb-99 MW-26 6.29 374.37 374.37

I 17-Feb-99 MW-27 6.60 374.59 374.59 17-Feb-99 MW-28 8.73 374.65 374.65 17-Feb-99 MW-29 31.94 386.54 386.54


I 17-Feb-99 MW-34 45.27 372.38 372.38 17-Feb-99 AW-l 12.06 375.37 375.37 17-Feb-99 RW-1 47.28 376.73 376.73

I 17-Feb-99 RW-2 17.95 375.58 375.58 17-Feb-99 RW-3 20.05 373.14 373.14 17-Feb-99 RW-4 21.58 371.93 371.93 17-Feb-99 RW-5 19.98

I 17-Feb-99 PW-1 42.96 376.21 376.21



I




24-Feb-99 MW-1

I 24-Feb-99 MW-2 24-Feb-99 MW-3 12.36 365.64 365.64 24-Feb-99 MW-4 23.82 353.63 353.63

I 24-Feb-99 MW-5 20.73 357.04 357.04 24-Feb-99 MW-6 24-Feb-99 MW-7 24-Feb-99 MW-8



I 24-Feb-99 MW-16 24-Feb-99 MW-17 24-Feb-99 MW-18 24-Feb-99 MW-19


I 24-Feb-99 MW-23 24-Feb-99 MW-24 24-Feb-99 MW-25 24-Feb-99 MW-26



I 24-Feb-99 MW-33 24-Feb-99 MW-34 50.85 366.80 366.80 24-Feb-99 AW-l 24-Feb-99 RW-1

I 24-Feb-99 RW-2 24-Feb-99 RW-3 24-Feb-99 RW-4

I 24-Feb-99 RW-5 24-Feb-99 PW-1

10-Mar-99 MW-1

I 10-Mar-99 MW-2 1. 36 378.11 378.11 10-Mar-99 MW-3 3.56 374.44 374.44

I "C"omments: Pumping; N = Non-Pumping; B/A = Before/After Adjustment] [P =


I




13-Mar-99 MW-7

I 13-Mar-99 MW-8 13-Mar-99 MW-9 13-Mar-99 MW-10

I 13-Mar-99 MW-11 13-Mar-99 MW-12 13-Mar-99 MW-13 13-Mar-99 MW-14






I 13-Mar-99 MW-33 13-Mar-99 MW-34 13-Mar-99 AW-l

I 13-Mar-99 RW-1 46.68 377.33 377.33 13-Mar-99 RW-2 13-Mar-99 RW-3 19.53 373.66 373.66

I 13-Mar-99 RW-4 22.64 370.87 370.87 13-Mar-99 RW-5 18.71 13-Mar-99 PW-1

I 14-Apr-99 MW-1 14-Apr-99 MW-2 1.16 378.31 378.31 14-Apr-99 MW-3 3.54 374.46 374.46

I 14-Apr-99 MW-4 3.25 374.20 374.20 14-Apr-99 MW-5 3.55 374.22 374.22 14-Apr-99 MW-6 5.13 374.14 374.14 14-Apr-99 MW-7 4.76 374.06 374.06

I 14-Apr-99 MW-8 14-Apr-99 MW-9 6.16 371.49 371.49

I "C"omments: (P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment]

I (I = Well Inaccessible; # = nth Monitoring Event of Day] (D = Dry Well; F = Film or Trace of Product] 109155

I




14-Apr-99 MW-10 6.34 371.15 371.15

I 14-Apr-99 MW-11 34.89 372.29 372.29 14-Apr-99 MW-12 46.66 387.10 387.10 14-Apr-99 MW-13 44.38 386.14 386.14

I 14-Apr-99 MW-14 43.01 387.79 387.79 14-Apr-99 MW-16 37.92 392.87 392.87 14-Apr-99 MW-17

I 14-Apr-99 MW-18 14-Apr-99 MW-19 14-Apr-99 MW-20 35.35 399.32 399.32 14-Apr-99 MW-21 6.80 372.03 372.03


I 14-Apr-99 MW-25 9.91 374.13 374.13 14-Apr-99 MW-26 6.05 374.61 374.61 14-Apr-99 MW-27 6.43 374.76 374.76 14-Apr-99 MW-28 8.28 375.10 375.10


I 14-Apr-99 MW-32 12.97 376.33 376.33 14-Apr-99 MW-33 10.86 375.93 375.93 14-Apr-99 MW-34 46.45 371.20 3 71.20 14-Apr-99 AW-l 11.34 376.09 376.09

I 14-Apr-99 RW-1 46.48 377.53 377.53 14-Apr-99 RW-2 17.38 376.15 376.15 14-Apr-99 RW-3 20.15 373.04 373.04

I 14-Apr-99 RW-4 23.49 370.02 370.02 14-Apr-99 RW-5 19.45 14-Apr-99 PW-1 41.08 378.09 378.09

I 28-Apr-99 MW-1 28-Apr-99 MW-2 28-Apr-99 MW-3


I 28-Apr-99 MW-7 28-Apr-99 MW-8 28-Apr-99 MW-9 28-Apr-99 MW-10

I 28-Apr-99 MW-11 28-Apr-99 MW-12

I N = Non-Pumping; "C"omments: [P = Pumping; B/A = Before/After Adjustment]

I [I = Well Inaccessible; # = nth Monitoring Event of Day) [D = Dry Well; F = Film or Trace of Product] 109155

I




28-Apr-99 MW-13






I 28-Apr-99 MW-32 28-Apr-99 MW-33 28-Apr-99 MW-34 37.39 380.26 380.26

I 28-Apr-99 AW-l 28-Apr-99 RW-1 46.96 377.05 377.05 28-Apr-99 RW-2 28-Apr-99 RW-3 20.07 373.12 373.12

I 28-Apr-99 RW-4 21.92 371.59 371.59 28-Apr-99 RW-5 17.54 28-Apr-99 PW-1

I 12-May-99 MW-1 12-May-99 MW-2 1. 27 378.20 378.20

I 12-May-99 MW-3 3.83 374.17 374.17 12-May-99 MW-4 3.39 374.06 374.06 12-May-99 MW-5 3.65 374.12 374.12 12-May-99 MW-6 5.15 374.12 374.12

I 12-May-99 MW-7 4.81 374.01 374.01 12-May-99 MW-8 12-May-99 MW-9 6. 32 371.33 371.33

I 12-May-99 MW-10 6.50 370.99 370.99 12-May-99 MW-11 34.48 372.70 372.70 12-May-99 MW-12 46.95 386.81 386.81 12-May-99 MW-13 44.46 386.06 386.06

I 12-May-99 MW-14 43.04 387.76 387.76 12-May-99 MW-16 37.73 393.06 393.06


I [I = Well Inaccessible; # = nth Monitoring Event of Day) [D = Dry Well; F = Film or Trace of Product) 109155

I


Print date: 11/18/99 Page

MONITORING WELL c PRODUCT WATER PRODUCT PRODUCT GW CORR GW DATE TYPE-# DEPTH DEPTH THICK. ELEV. ELEV. ELEV.

(feet) (feet) (feet) (feet) (feet) (feet)

12-May-99 MW-17 12-May-99 MW-18 12-May-99 MW-19 12-May-99 MW-20 35.42 399.25 399.25 12-May-99 MW-21 7.06 371.77 371.77 12-May-99 MW-22 5.94 372.33 372.33 12-May-99 MW-23 4.76 374.02 374.02 12-May-99 MW-24 9.17 374.01 374.01 12-May-99 MW-25 9.99 374.05 374.05 12-May-99 MW-26 6. 30 374.36 374.36 12-May-99 MW-27 6.79 374.40 374.40 12-May-99 MW-28 8.79 374.59 374.59 12-May-99 MW-29 31.38 387.10 387.10 12-May-99 MW-30 15.77 379.76 379.76 12-May-99 MW-31 13.83 375.49 375.49 12-May-99 MW-32 13.50 375.80 375.80 12-May-99 MW-33 11.39 375.40 375.40 12-May-99 MW-34 47.35 370.30 370.30 12-May-99 AW-l 11.88 375.55 375.55 12-May-99 RW-1 47.10 376.91 376.91 12-May-99 RW-2 17.90 375.63 375.63 12-May-99 RW-3 20.62 372.57 3 72.57 12-May-99 RW-4 23.17 370.34 370.34 12-May-99 RW-5 19.53 12-May-99 PW-1

19-May-99 MW-1 19-May-99 MW-2 19-May-99 MW-3 19-May-99 MW-4 19-May-99 MW-5 19-May-99 MW-6 19-May-99 MW-7 19-May-99 MW-8 19-May-99 MW-9 19-May-99 MW-10 19-May-99 MW-11 19-May-99 MW-12 19-May-99 MW-13 19-May-99 MW-14 19-May-99 MW-16 19-May-99 MW-17 19-May-99 MW-18 19-May-99 MW-19

"C"omments: [P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment] (I = Well Inaccessible; # = nth Monitoring Event of Day] [D = Dry Well; F = Film or Trace of Product) 109155

8




19-May-99 MW-20

I 19-May-99 MW-21 19-May-99 MW-22 19-May-99 MW-23


I 19-May-99 MW-27 19-May-99 MW-28 19-May-99 MW-29 19-May-99 MW-30


I 19-May-99 MW-34 40.39 377.26 377.26 19-May-99 AW-l 19-May-99 RW-1 46.23 377.78 377.78 19-May-99 RW-2

I 19-May-99 RW-3 16.24 376.95 376.95 19-May-99 RW-4 17.18 376.33 376.33 19-May-99 RW-5 16.52

I 19-May-99 PW-1

9-Jun-99 MW-1 9-Jun-99 MW-2

I 9-Jun-99 MW-3 9-Jun-99 MW-4 9-Jun-99 MW-5


I 9-Jun-99 MW-9 9-Jun-99 MW-10 9-Jun-99 MW-11 9-Jun-99 MW-12



I 9-Jun-99 MW-21 9-Jun-99 MW-22

I "C"omments: Pumping; N = Non-Pumping; B/A = Before/After Adjustment] [P =


I




9-Jun-99 MW-23




I 9-Jun-99 MW-34 45.12 3 72.53 372.53 9-Jun-99 AW-l 9-Jun-99 RW-1 46.25 377.76 377.76

I 9-Jun-99 RW-2 9-Jun-99 RW-3 19.64 373.55 373.55 9-Jun-99 RW-4 23.18 370.33 370.33 9-Jun-99 RW-5 18.43

I 9-Jun-99 PW-1

16-Jun-99 MW-1

I 16-Jun-99 MW-2 1. 29 378.18 378.18 16-Jun-99 MW-3 3.61 374.39 374.39 16-Jun-99 MW-4 3.21 374.24 374.24 16-Jun-99 MW-5 3.54 374.23 374.23

I 16-Jun-99 MW-6 5.04 374.23 374.23 16-Jun-99 MW-7 4.73 374.09 374.09 16-Jun-99 MW-8

I 16-Jun-99 MW-9 6.30 371.35 371.35 16-Jun-99 MW-10 6.18 371.31 371.31 16-Jun-99 MW-11 34.59 372.59 372.59

I 16-Jun-99 MW-12 48.07 385.69 385.69 16-Jun-99 MW-13 44.95 385.57 385.57 16-Jun-99 MW-14 42.99 387.81 387.81 16-Jun-99 MW-16 37.62 393.17 393.17


I 16-Jun-99 MW-20 35.55 399.12 399.12 16-Jun-99 MW-21 7.07 371.76 371.76 16-Jun-99 MW-22 5.36 372.91 372.91 16-Jun-99 MW-23 5.18 373.60 373.60

I 16-Jun-99 MW-24 9.16 374.02 374.02 16-Jun-99 MW-25 9.87 374.17 374.17



I


MONITORING DATE

16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99 16-Jun-99

23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99

WELL TYPE-#

MW-26 MW-27 MW-28 MW-29 MW-30 MW-31 MW-32 MW-33 MW-34 AW-l RW-1 RW-2 RW-3 RW-4 RW-5 PW-1

MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 MW-24 MW-25 MW-26 MW-27 MW-28

C PRODUCT DEPTH (feet)

WATER DEPTH (feet)

6.22 6.80 8.73

31.44 15.81 13.82 13.57 11.20 45.19 11.81 47.00 17.80 21.64 23.00 19.62 41.14


PRODUCT THICK. (feet)

PRODUCT ELEV.

(feet)

GW ELEV.

(feet)

374.44 374.39 374.65 387.04 379.72 375.50 375.73 375.59 372.46 375.62 377.01 375.73 371.55 370.51

378.03

CORR GW ELEV.

(feet)

374.44 374.39 374.65 387.04 379.72 375.50 375.73 375.59 372.46 375.62 377.01 375.73 371. 55 370.51

378.03

"C"omments: [P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment) [I = Well Inaccessible; # = nth Monitoring Event of Day] [D = Dry Well; F = Film or Trace of Product] 109155


MONITORING DATE

23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99 23-Jun-99

30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99 30-Jun-99

WELL TYPE-#

MW-29 MW-30 MW-31 MW-32 MW-33 MW-34 AW-l RW-1 RW-2 RW-3 RW-4 RW-5 PW-1

MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-16 MW-17 MW-18 MW-19 MW-20 MW-21 MW-22 MW-23 MW-24 MW-25 MW-26 MW-27 MW-28 MW-29 MW-30 MW-31

C PRODUCT WATER DEPTH DEPTH (feet) (feet)

41.32

46.85

19.95 23.24 17.76


PRODUCT THICK. (feet)

PRODUCT ELEV.

(feet)

GW ELEV.

(feet)

376.33

377.16

373.24 370.27

CORR GW ELEV.

(feet)

376.33

377.16

373.24 370.27

"C"omments: [P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment] [I = Well Inaccessible; # = nth Monitoring Event of Day] [D = Dry Well; F = Film or Trace of Product] 109i55




30-Jun-99 MW-32

I 30-Jun-99 MW-33 30-Jun-99 MW-34 49.62 368.03 368.03 30-Jun-99 AW-l

I 30-Jun-99 RW-1 30-Jun-99 RW-2 30-Jun-99 RW-3 20.97 372.22 372.22

I 30-Jun-99 RW-4 22.84 370.67 370.67 30-Jun-99 RW-5 19.65 30-Jun-99 PW-1

I 7-Jul-99 MW-1 7-Jul-99 MW-2 7-Jul-99 MW-3

I 7-Jul-99 MW-4 7-Jul-99 MW-5 7-Jul-99 MW-6 7-Jul-99 MW-7








I 7-Jul-99 MW-33 7-Jul-99 MW-34 41.74 375.91 375.91


I [I = Well Inaccessible; # = nth Monitoring Event of Day] [D = Dry Well; F = Film or Trace of Product) 109155

I


•




7-Jul-99 AW-l

I 7-Jul-99 RW-1 46.78 377.23 377.23 7-Jul-99 RW-2 7-Jul-99 RW-3 20.15 373.04 373.04

I 7-Jul-99 RW-4 23.75 369.76 369.76 7-Jul-99 RW-5 17.91 7-Jul-99 PW-1

I 21-Jul-99 MW-1 21-Jul-99 MW-2 1. 26 378.21 378.21 21-Jul-99 MW-3 3.73 374.27 374.27

I 21-Jul-99 MW-4 3.42 374.03 374.03 21-Jul-99 MW-5 3.76 374.01 374.01 21-Jul-99 MW-6 5.33 373.94 373.94

I 21-Jul-99 MW-7 5.00 373.82 373.82 21-Jul-99 MW-8 21-Jul-99 MW-9 6.73 370.92 370.92 21-Jul-99 MW-10 6.55 370.94 370.94


I 21-Jul-99 MW-14 43.08 387.72 387.72 21-Jul-99 MW-16 37.70 393.09 393.09 21-Jul-99 MW-17 21-Jul-99 MW-18

I 21-Jul-99 MW-19 21-Jul-99 MW-20 21-Jul-99 MW-21 35.80 343.03 343.03


I 21-Jul-99 MW-25 10.22 373.82 373.82 21-Jul-99 MW-26 6.63 374.03 374.03 21-Jul-99 MW-27 6.90 374.29 374.29 21-Jul-99 MW-28 8.94 374.44 374.44


I 21-Jul-99 MW-32 13.56 375.74 375.74 21-Jul-99 MW-33 11.51 375.28 375.28 21-Jul-99 MW-34 45.26 372.39 372.39 21-Jul-99 AW-l 12.13 375.30 375.30

I 21-Jul-99 RW-1 47.09 376.92 376.92 21-Jul-99 RW-2 18.14 375.39 375.39



I

I I I I I I I I

• I I I I I I I I u I




21-Jul-99 RW-3 21.57 371.62 371.62

I 21-Jul-99 RW-4 22.93 370.58 370.58 21-Jul-99 RW-5 19.60 21-Jul-99 PW-1 41.20 377.97 377.97

I 11-Aug-99 MW-1 11-Aug-99 MW-2 11-Aug-99 MW-3



I 11-Aug-99 MW-10 11-Aug-99 MW-11 11-Aug-99 MW-12 11-Aug-99 MW-13






I 11-Aug-99 MW-32 11-Aug-99 MW-33 11-Aug-99 MW-34 41.73 375.92 375.92

I 11-Aug-99 AW-l 11-Aug-99 RW-1 47.54 376.47 376.47 11-Aug-99 RW-2 11-Aug-99 RW-3 20.05 373.14 373.14

I 11-Aug-99 RW-4 22.94 370.57 370.57 11-Aug-99 RW-5 18.06

I "C"omments: [P Pumping; N = Non-Pumping; B/A = Before/After Adjustment] = [I = Well Inaccessible; # = nth Monitoring Event of Day]

I [D = Dry Well; F = Film or Trace of Product] 109155

I

I I I I I I I

• I I I I I I I I u I I




11-Aug-99 PW-1

I 18-Aug-99 MW-1 18-Aug-99 MW-2









I 18-Aug-99 MW-31 18-Aug-99 MW-32 18-Aug-99 MW-33 18-Aug-99 MW-.34 41.04 376.61 376.61

I 18-Aug-99 AW-l 18-Aug-99 RW-1 46.06 377.95 377.95 18-Aug-99 RW-2

I 18-Aug-99 RW-3 17.12 376.07 376.07 18-Aug-99 RW-4 17.33 376.18 376.18 18-Aug-99 RW-5 16.60 18-Aug-99 PW-1

I 25-Aug-99 MW-1

I "C"omments: [P Pumping; N = Non-Pumping; B/A = Before/After Adjustment] = [I = Well Inaccessible; # = nth Monitoring Event of Day]

I [D = Dry Well; F = Film or Trace of Product] 109155

I




25-Aug-99 MW-2 1. 26 378.21 378.21

I 25-Aug-99 MW-3 4.06 373.94 373.94 25-Aug-99 MW-4 3.65 373.80 373.80 25-Aug-99 MW-5 4.05 373.72 373.72

I 25-Aug-99 MW-6 5.56 373.71 373.71 25-Aug-99 MW-7 5.34 373.48 373.48 25-Aug-99 MW-8 25-Aug-99 MW-9 7.23 370.42 370.42



I 25-Aug-99 MW-17 25-Aug-99 MW-18 25-Aug-99 MW-19 25-Aug-99 MW-20 36.22 398.45 398.45


I 25-Aug-99 MW-24 9.80 373.38 373.38 25-Aug-99 MW-25 10.50 373.54 373.54 25-Aug-99 MW-26 6.85 373.81 373.81 25-Aug-99 MW-27 7.21 373.98 373.98

I 25-Aug-99 MW-28 9.34 374.04 374.04 25-Aug-99 MW-29 25-Aug-99 MW-30 16.03 379.50 379.50


I 25-Aug-99 MW-34 35.76 381.89 381.89 25-Aug-99 AW-l 12.50 374.93 374.93 25-Aug-99 RW-1 47.48 376.53 376.53 25-Aug-99 RW-2 18.36 375.17 375.17

I 25-Aug-99 RW-3 19.37 373.82 373.82 25-Aug-99 RW-4 21.84 3 71.67 371.67 25-Aug-99 RW-5 19.36

I 25-Aug-99 PW-1 42.96 376.21 376.21

15-Sep-99 MW-1 15-Sep-99 MW-2

I 15-Sep-99 MW-3 15-Sep-99 MW-4

I "C"omments: [P Pumping; N = Non-Pumping; B/A = Before/After Adjustment] =


I




15-Sep-99 MW-5

I 15-Sep-99 MW-6 15-Sep-99 MW-7 15-Sep-99 MW-8

I 15-Sep-99 MW-9 15-Sep-99 MW-10 15-Sep-99 MW-11 15-Sep-99 MW-12







I 15-Sep-99 MW-34 40.32 377.33 377.33 15-Sep-99 AW-l 15-Sep-99 RW-1

I 15-Sep-99 RW-2 15-Sep-99 RW-3 16.13 3 77.06 377.06 15-Sep-99 RW-4 17.06 376.45 376.45 15-Sep-99 RW-5 19.88

I 15-Sep-99 PW-1

22-Sep-99 MW-1

I 22-Sep-99 MW-2 22-Sep-99 MW-3 3.25 374.75 374.75 22-Sep-99 MW-4 2.85 374.60 374.60 22-Sep-99 MW-5 3.33 374.44 374.44

I 22-Sep-99 MW-6 4.80 374.47 374.47 22-Sep-99 MW-7 4.50 374.32 374.32

I "C"omments: (P Pumping; N = Non-Pumping; B/A = Before/After Adjustment] = [I = Well Inaccessible; # = nth Monitoring Event of Day]

I [D = Dry Well; F = Film or Trace of Product) 109155

I




22-Sep-99 MW-8

I 22-Sep-99 MW-9 5.81 371.84 371.84 22-Sep-99 MW-10 6.41 371.08 371. 08 22-Sep-99 MW-11 34.42 372.76 372.76

I 22-Sep-99 MW-12 44.90 388.86 388.86 22-Sep-99 MW-13 43.18 387.34 387.34 22-Sep-99 MW-14 42.60 388.20 388.20 22-Sep-99 MW-16 37.74 393.05 393.05


I 22-Sep-99 MW-20 35.80 398.87 398.87 22-Sep-99 MW-21 6.49 372.34 372.34 22-Sep-99 MW-22 5.47 372.80 372.80 22-Sep-99 MW-23 1. 94 376.84 376.84

I 22-Sep-99 MW-24 8.72 374.46 374.46 22-Sep-99 MW-25 9.55 374.49 374.49 22-Sep-99 MW-26 5.55 375.11 375.11

I 22-Sep-99 MW-27 6.00 375.19 375.19 22-Sep-99 MW-28 7.78 375.60 375.60 22-Sep-99 MW-29 42.25 376.23 376.23

I 22-Sep-99 MW-30 15.54 379.99 379.99 22-Sep-99 MW-31 12.12 377.20 377.20 22-Sep-99 MW-32 12.07 377.23 377.23 22-Sep-99 MW-33 9.69 377.10 377.10

I 22-Sep-99 MW-34 48.16 369.49 369.49 22-Sep-99 AW-l 10.20 377.23 377.23 22-Sep-99 RW-1 45.33 378.68 378.68

I 22-Sep-99 RW-2 16.68 376.85 376.85 22-Sep-99 RW-3 14.72 378.47 378.47 22-Sep-99 RW.,-4 20.34 373.17 373.17 22-Sep-99 RW-5 21.62

I 22-Sep-99 PW-1 39.23 379.94 379.94

I I I I "C"omments: [P = Pumping; N = Non-Pumping; B/A = Before/After Adjustment)

[I = Well Inaccessible; # = nth Monitoring Event of Day)

I [D = Dry Well; F = Film or Trace of Product) 109155

I

~~

I I I I I I I J I I I I I I I I I I

APPENDIX 8

GROUNDWATER QUALITY LABORATORY ANALYTICAL REPORT

I

I I I I I I I I I I I

SP,ECIAVIZED_A&SAYS, INC.

2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

THE

A~LVTICAL REPORT

CEIViD JUN 0 2 1999

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I I I I I I I I I I I I I I I I I

SPECIAMZED ASSAYS, INC. ' -

2960, Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

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ANALYTICAL REPORT

Labo1·atory Number: 99-A90604 S3tnplE· 1D: i"lt.J-2

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SPECIALIZED ASSAYS, INC. ' '

2960'Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT

Laboratot·y Number: 99-A90604 Sample I 0: r~!W-·2

Report '-''PP1'0ved B•-1: +-ft!~~-------· f•:eport !)ate:

Theodo~e ~~- OtJello, Ph.D. Lab Director Michael H. Dunn, M.S. , Technical Director Johnny A. Mitchell.· Dir. lechn:ical Services Eric Smith, Assistant Tech11ical Director Russell Morgan, Technical Services

COPY2

-·

SPECIAlJIZED A•SSAYS, INC. ' .


OF THE c;~F(OL INt=~-5

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lr.~rnject.: Pr·ojer~'t

pamp 1 eT:

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Name: t;J~o\RREN DIL

ERIC DONNELLY

ANALYTICAL REPORT

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SPECIALIZED ASSAYS, INC. ' . .


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Theodore J. Duello, Ph.D., Lab Director Michdel H. Dunn, M.S., Technical Director .Johnny A. Mitchell, Dir. Technical Be1·vices Eric Smith, Assistant Technical t:Hrector Russell Morg~n, l'echnical Services

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2960 Foster Creighton Dr. P. 0. Bo• 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT

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Theodore .J. Duellc, Ph.D., L.atl O.i.!'ecto~

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Laboratory Certification Nuinb~t: 387

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I I I I I I I I I I

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SPECIALIZED ASSAYS, INC. ' '

2960 Foster Creighton Dr. ~ 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

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IIIII S~ECIAL'IZED ~SSAYS, INC.


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2960 Foster Creighton Dr. E 0. Box 40566 Nashville, TN 37204-0566

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L~borator~ Number: 99-A90608 5amp1t- ID: MW-.16

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SPECIALIZED ASSAYS, INC. . . .

2960 Foster Creighton Dr. P. 0. Box 40566 Nashville. TN 37204-0566 Phone 1-615-726-0177

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Laboratc~ry Number: 99-A90609 Sam~le ID: f'!W--26

Raport Date: 71 1/99

Theod0re J. Duello~ Ph.D. Lab DirectGr Michtiel H. Dur,n) M.s .. • Tec:tnlical Directc•rJohnnu A. Mit-chelL OiL Technical Ser-vices Eric Smith. Assistant Technical Director Rus:=:,ell Mor·ganJ Technical Ser·vtces

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S~ECIALlZED A:SSAYS, INC. . '


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S~ECIA';-IZED ~SSAYS, INC.

2960 Foster Creighron Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT

Laboratory Number: 99-A90610 Sample ID: MW-27

Page 3

Report Data: 7/ 1/99

Theodo~e J. 01Je!lo~ ?h. D., Lab Oirec·tor Micna~l H. Dunn, M.S. , Technical Oirect&r ...Johnny A. ~'litctH?lL Dir·. Technical Services Eric Sillith} Assi~tant Technical Director Russell Morgan~ ·recnni~al Services

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SPECIALIZED ASSAYS, INC. ' ' '

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SPECIALIZED ASSAYS, INC. ' . .

2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

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S~ECIALIZED ASSAYS, INC. . . 2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

Report App~oved B~.

ANALYTICAL REPORT

Laboratory Nu!nber: 99-A90611 samp 1 e I D: r·n •. r-:z~;

Theodore J. Oueilo, Ph.D., Lab Dire~tot·

Michdel H. Dunn, M.S., Technical Oiractor -Johnny l~. MitchelL Dtr. Technical Services Eric Smittl, Assist.Jnt Technical Director Russell Morgan, Tect1nic~l Services

Lat<o·r·atnry Cert.i fie at ion Number: 387

COPY2 --- -·--·- . - --· .. · -·

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SP,ECIALlZED ASSAYS, INC. . '


I HN·.n:.c:;c DF THE CAf1:l.JLINAS

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Lab Number: 99-A90612 S~mple IO: MW-30 Sa!np 1(~ Tl.Jpe: G'f'ound water S.t t;e ID:

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2960 Foster Creighton Dr. ~ 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL.

L-:ab ora tory sample ID:

Page 2

Numb et·: !"'!t.J-30

REPORT

99-A90612

I ---···-·------ ____ .. ______________________________ _

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SPECIALIZED ASSAYS, INC. ' . '


Laboratory Number: 99-A90612 Sample I D: 111~-30

Report Data: 71 1/99

Theodore J. DtJello, Ph.D.~ Lab Director Michael H. Dunn, M.S., ·rechnical DirEctor JO~'H'!ny A. Mi·tchell~ Dir·. Tec!"tnical Ser-vices Erit Sm1thJ Assistant Technical Director Russell MorganJ Technical Services

laborator4 Certificdtion Number: 387

COPY2




10-Mar-99 MW-4 3.25 374.20 374.20

I 10-Mar-99 MW-5 3.64 374.13 374.13 10-Mar-99 MW-6 5.16 374.11 374.11 10-Mar-99 MW-7 4.80 374.02 374.02

I 10-Mar-99 MW-8 10-Mar-99 MW-9 6.55 371.10 3 71. 10 10-Mar-99 MW-10 6.29 371.20 371.20

I 10-Mar-99 MW-11 35.46 371.72 371.72 10-Mar-99 MW-12 48.44 385.32 385.32 10-Mar-99 MW-13 45.04 385.48 385.48 10-Mar-99 MW-14 43.08 387.72 387.72

I lO-Mar-99 MW-16 38.10 392.69 392.69 10-Mar-99 MW-17 10-Mar-99 MW-18

I 10-Mar-99 MW-19 10-Mar-99 MW-20 35.65 399.02 399.02 10-Mar-99 MW-21 7.16 371.67 371.67 10-Mar-99 MW-22 6.15 372.12 372.12


I 10-Mar-99 MW-26 6.19 374.47 374.47 10-Mar-99 MW-27 6.53 374.66 374.66 10-Mar-99 MW-28 8.44 374.94 374.94 10-Mar-99 MW-29 31.82 386.66 386.66


I 10-Mar-99 MW-33 11.26 375.53 375.53 10-Mar-99 MW-34 45.22 372.43 372.43 10-Mar-99 AW-l 11.80 375.63 375.63

I 10-Mar-99 RW-1 46.91 377.10 377.10 10-Mar-99 RW-2 17.61 375.92 375.92 10-Mar-99 RW-3 21.67 371.52 371.52 10-Mar-99 RW-4 21.55 371.96 371.96

I 10-Mar-99 RW-5 20.12 10-Mar-99 PW-1 42.97 376.20 376.20


I 13-Mar-99 MW-5 13-Mar-99 MW-6

I "C"omments: Pumping; N = Non-Pumping; [P = B/A = Before/After Adjustment]

I [I = Well Inaccessible; # = nth Monitoring Event of Day) [D = Dry Well; F = Film or Trace of Product) 109155

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2960 Foster Creighton Dr. P. 0. Box 40566

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Nashville, TN 37204-0566 Phone 1-615-726-0177

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Proje•.:t: lGt:/5-lJ·-Ol

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S~ECIALIZED ASSAYS, INC. ' .


Lclboratory Number: 99-A90613 Sample 10: MW-31

I Repo~t Approved Bu· )'/ 1/99


Theodore .J. Duella, Ph.D., Lab Dire.r:tor Mich.3el H. Dunn, M.S., Technicdl Uirecto1' JohtHHJ !c £1itche-1L Dir·. Technical Servic~s Eric Smith, Assistdnt Technicdl Director t\ty.;-seli Mor·q-:Hh r~chnic.al S1?rvices

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I t-lt-\NDE;~ OF THE CAROLINAS

WDODPAR!I.. BLVD. NG 282fJ6

I Pr·c·jec·t: 1095.11-0.1 P~ejert Name: WARREN OIL Sampler: F.:RIC DONNELLY


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St t>? ID:

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204~0566 Phone 1-615-726-0177

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2960 Foster Creighton Dr. ~ 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT

L~boratory Number: 99-A90614 Sample ID: MW-32

Page 3

F:eport ;ippr·o·.;e•i P.'4: ~~/-____ RepoPt L'ate: /.•' lf'i''·'

~-~- Duello. Ph.D., Lab Director Michael H. Dunn) n. S. , T~chnical Director Johnny A. Mitchell) Dir. Technical Services Eric Smith, Assistant Technical Director Russell Morgan) Technical Services

labor-atory: Certifl.f>Jtion t-4umber: 387

COPY2


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Laborator~ Certification Number: 387

COPY2

SJ;'ECIALIZED ~SSAYS, INC.


1095.11-0l I Project: Project. Name: WARREN 01L


ERIC DONNELLY

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3;1W;:c::ll Phone 1-615-726-0177 ANALYTICAL REPORT

Laboratory Number: 99-A90616 SamplC! .!D: Mt.-J-34

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Laboratory Numbe~: 99-A90617 -5-a.mple ID: RW-;?

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SPECIALiZED ~SSAYS, INC.


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Labordtory Certification Number: 387

COPY2

I I

SPECIALiZED ASSAYS, INC. . . 2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

G:. THE Ci~ROL. I NAS

3S{~0-·S WOODPAR~ B~VD.

I p,o_1 e-cct: Proje(t N3ft!e: WARREN OIL 53mplar: ERIC DONNELLY


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Lab Number: 99--119·D61 9 Sarr:p l 0 1 D: RW-·-3 Sc:ur~plf-1 Tl:lpt?: Grou-:-1d wate-·r· :3ite "fD:

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' ' I I I I I I I I I I I I I I I I I I I


SP.ECIAJ,IZED J\,SSAYS, INC.


Laboratory Number: 99-A90619 5afnp l e I D: RI,.J--3

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' . I I I I I I I I I I I I I I I I I I I



2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL

Lab or .a t:>:J rt.J Sample ID:

Number: Rl-1-3

Hepor-t Date:

fhe•_JdOf'l': d. Ou>?lhJ; f'h. 0., Ldb Director i1tcn.ael H. !)JJnn, M.S. I rechnic.al Director .Johnny A. Mitch.eJ.l, Dir. Te•:hni.c.al Ser'•lices

Eri'= Smitht Ass:istaot Te•.:hnic.al Director Russell Morqan, Technical Services

Laboratory Certification Nu•ber· 387

COPY2

REPORT

99-A90619

7/ 1/9)1'

S~ECIA~IZED f\SSAYS, INC.

2960 Foster Creighton Dr. P. 0. Bo< 40566 Nashville, TN 37204-0566 Phone l-615-726-0 177

109511.-C!l. I ;::.·r·o.je-:t;: Project Name: WARREN OIL !33mpl~r: ERIC DONNELLY


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I I I I I I I I m

I I I I I I I I I I


SP,ECIA~IZED ~SSAYS, INC.

2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone l-615-726-0177

Repo~t ApprDved By:

AI'IAL VT I CAL REPORT

Labor2tcr~ ~itJm~el~: 99-A~0620

Samp.le ID: gt.-J-4

~;zz ~ ... ):::? & .-dL""-'--- :_ ____ ---------

"fhe0dD~2 J. Duello, Ph.D.~ Lab Di~~ctor Mic~ael H. Dunn. M. S • Technical Oirector l.ic<irr:·r~~i f;_ r:itcti-211. Dir. ·r-~·chn:ical St~r-vii:(·::.

Er-:~c Sfln.·t.tJ., Assistnn·t- T=:chrficai Dir·r.-cto;' RL·~-,E-~11 J'lorg:H1. Tl?Cil!iic:al Se1·:..'i.ces

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL

La!JoT'.ator~J

Sample ID: Number·: Rl-J--5

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REPORT

99-A90621

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1..()15-72~0177 ANALYTICAL

Labor·atoT'y Samp 1 e ID:

Number: RW-:J

Theodor~ J. Ouello~ Ph.D., Lab Director Michael H. Dunn~ M.S., Technical Director Johnn~ A. Mitchell, Dir. Technical Services E~ic Smitn~ Assistant Technical DirectoJ· Russell Morgan, Technical Services

t_abot·atory CertificdtiDn Nuffiber: 387

REPORT

99-A90621

I I I I I I I I I I

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I



I 3600-G WDODPARK B~_VD.

28206

I Pr·o_ject:

EH!C DONNELLY

·------- --.-- --- -~- ----~----

ANALYTICAL REPORT

Lab Numter: 99-A90622 Sampl•:.:: IO: i..J-·l Sample T!Jpe: Groun•j water ~~:tte~ ID:

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Reporl: App1·oveJ Sy:

ANALYTICAL REPORT

Laboratory Nun1ber: 99-A90622 5aiflt:·1E ID: t.-J--1

(22;21~------ Report l)ate:

Tt:eGdors J. Du~llo. Ph.D., Michael H. ... :~

! L ;:;_ '

.. 'ohnn~} A. MitchelL Dil'. T2ct-:nical Service~

Erir Smith~ Assistaitt Technical Director· Russell Morgan. Tecl1nical Services

7/ 1/97'


I


H.'·:~f..!DEX OF THE CARDLlN/15

>-.>OODPARK BLVD. I 3c'>C0--3 ·:HARLDTTE, NC 28206


109:511-0l N-3-fi!.e:

ERIC WAR:F\EN OIL r:ONNELLY

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Laboratory Number: 99-A90623 5ample ID: l.J-2

Theodore J. C<u~llo .. Ph. C<. ntchdel H. Dunn. M.S. 1 Technical Director .Johnny: ~~- MitchE.1 lL Dir. Technical Services Eric St.nith, Assi·5t-3r.t Techni>:.:':l:l Director· Russell Morgdn, T~chnical 5er·vice~

Labo~atcry CertificatjoJ) NumbPJ': 367

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1·615-726.0177

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•::HARLGTTE.. NC 28206

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Name: lt.l1:::.RREN DIL EF I C OONNEL.L \~

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Lab Number: 99-A90624 samp 12 ID: ~1-27

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TheDdor~ J. D!Jel}o, Ph.D., Lot• Director t1ict~ae1 H. Dunn. 1'1. S. ~ Tect1nir.:al Oi'i't:ctc<r· Jol·H~n~i A. M::itche-11.· Dir·. ·recfHlical Se-rvir.es Er·ic Sir1ith) As-sis-tant TeciHJical Dir-ector Russell Morgan~ Technical Ser-vices

:•'/ 1/99


•·.:·.·


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone l-615-726-0 177

36CQ-G WODDPARK BLVD. CHARL8TTE. NC 28206

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Theodor·e d. Dv,=llof Ph. D., Lab Director fiich.ael H. Dur1n, N.S., Technic:-:il Director .Johnny A. f1ii.;chell, Dit,. Technical Service--;; Eric Smith, Assistant Technical Director Russell Morgan, Technical Services

Labor2tory Certjfl~ation NumbPr: 387

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Laboratory Number: 99-A90630 Sample ID: TRIP BLANK

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• SPECIALIZED ASSAYS, INC.

2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone l-615-726-0 177 ANAL y,- I CAL REPORT

Labo1·ato1·y Number: 99-A90630 S~3mp i.e ID: TRIP 3LAN~.

--1-fZd~------------Theodore~'- Duello. Pt1.0., Lab Oirect0:· Mi•::h,hli H. Dunn~ f'!. S. 1 Techni.cal Director Johnny A. flitchell1 Ccir·. Technic.:tl Sec\1 iCe5 Eric Sinith1 As·5is'i;d:nt TechnL:aJ. Uire,:::t.-::r Rus-sell Morq-Hlr Te>::hnic-31 !Services

7/ 1 /'19


I H~i-HJEX OF THE Ct~RDLlNi~S 61{:;~:;

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C~·Y'•,RLCTTE, NC :;~82-06

Samp 1.P. TL_!Fe: :rJc..1·ter· Site !D:

I P1'0_ject: 1091-55-(;ti. D.a te T i. 1ilt>

Date Time

CotlectEC:: Project Name: WARREN OIL 1-\;}ce ~vttd: ::o~mp .•>r: ~.. , I - l E'L'_ T C r •. ',f".J",JN!:".LL'{ R-ecei..,led:


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Thes~ r~~ult~ r~late an14 to t!te 1t8MS tested. l'hls r2p0~t sh~ll not be r~produced ex~~pt in ·ftlll and w!th permission of the labcr~tary.

l"heodare J. Duella1 Ph.D., Lab Director nt.ch.;tel H. Dunn~ i1. S. 1 Tecl'rntc.:.l Direc"tur' ,Johnny t\. MitchelL, lli r. Techo iL.a I SEH'Vi·::es r.1~i-•: Smith. A-~-sist.ant 'h!chnicdl Director Gail A ldge~ ·rechnic~l Servicas

Laborator4 :ertification Nurnbe7': 387

COPY3

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I Hf.ti·~DF-1; OF THE CPJ-.'!UL.INAS 6163

I :3600·-G ~IOODP .'IR!'. BLVD. CHARL.OTTE. NC 28206

I F1'G .i ec 1;: 10915,·-Ql Nam\>: I~ARREN OIL. I Sampler: ERIC DONNELLY

L.ab Number: 99-A146895 SB111p l e 1 D: M~l·-·1 t.=.~

5i-3mplf~ Typ!..~: ~-Ji:it-?T·

Date Collected: Ttme Gollecte·.ct: Date Recetvecl: Time Received :

r.;.·l~23t'9..:.;

to: ;::o 9/i.'~·~f/9'f?

9:00

---------------- ·----------·------------------- -··------.. ···~--~-----


Re~ort QU"fl D!l ~n•I9te ~£-E.Ult \Jrdt<E- Uiilt UKlt r ~~<;tor Date--~-.- --- ... -----·-----. ----·------. ·-··---- ·-------- --.. ------

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Tt1ese r0sults relate onl~ to the it~~s testetl. ·r·his report ~h~ll no~ be t·epr0duced e~cept ili full dGd ~itt1

p~1·miss!on af thr! laborator~.

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. L:- --~::20.~~-' ---~L:__ ___ _ RepOI't Date· 10/ 4/9~

Theodore J_ DuBllo, Ph.D. i Ldb Director Michael H. Dunn, M.S., Tech11ical Director Johnn1_4 A. MitchelL D'ir. Tee hr. ir:~ l Servi.cer:; Eric S~ith, Assistant Technical Director· Gail A La9e, Technical Services

Laborat .. rsr~ Certj_fica·tion N!Jtnber: 387

COPY3

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NC 2820·b

Lab N0mber: 99-Al46896 Samp 1 e l D: I'H·I-·- 1·1 Sample Type: Hater Site 1D:

I Project: 10915::!-01 Date Collect·~~d:

T.i.me CollectHd: 9 /~23/Cl~':f

10:10 Pro.j,~c-t; I i3arnpler:

Name: WARREN OIL ERIC DONNELLY

D.ate Received: Time- Received:

I I I I I I I I I

F.oport Ru:r:. Dll t:r1i•l!:tt:' Result l!nlts llN!t liNlt FiJCtH DiltE<

·-----~----· ··- -··· ---- --·-·-----·-- --- ··- --- ------··-_,. _________

~!:;f;£Alf1C FflRMEitRS.> f:e-r~2t~iie '17. ~ ugll l.V '1. i,l 1 .lfl/ '1./19 rolue~Jf.' 2.2 ugt1 1.0 1.0 ltll '2i9fJ !.::"th~.]J ~I:'{I:Z.i!l'lf !fL\ ug/1 1.0 1.0 1(1( ~u:n

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JIJU. ~ll ... 150.

fh~se i'E~ults r8ld·te anl~ to ths items te;ted. Tl·,.i·:; !'>~·~·-Jri.: ·;.;ha1.1 net l..!e \t~Pf'•::!ill..iC\?d 1£:~.·.:-.::yi; in ·fuJ.i <HHI :1HU!

parmissio11 of t!1e laticJratory.

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I Report Date: 101 4/~9

I I I

Ttteodore J. Ouello. Ph.D., lab Directol' nicl"!ael H. 0lH)I1, i1. S. I Ter.:tln'i.C.:Jl. Dii"(:!CtOl'

,Johnn\~ A. Mitc:ht:lL Dir. Technic41 St?l'Vice·;; ErJc Smith, {issist.lnt Tecf:nJ.cal Oil~ectar Gall A Lage, Technical Services

COPY3

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 Af'.IALVT I C:AL- REPORT

I ~1A~UEX 0~ THE CAf~OLll~AS 616:~

I ~],~·;_:::.~) ·-·:~ ~.JC'DD::l.~Rjli, .BLVD.

c:-iJ .. ;~L.llTTEI NC ;~~8::"!06

I P1··ojG·•.c'c: 1091.~5-~0l

Nama: WARREN OIL ERIC DONNELLY

La~l Number: 99---;:11'16::397 ;;_iample ID: l"~~l-L~.)

Sample Type: Wate~

S.i te ID:

f:c-3te ·-r j_ in eo

Col lee tert: Collect..;~;j:

D-~te Recet\··ed: Time Recei\ted:

9/23/99 10: :t j

9/2:.4/ f'j'9

··-----··-----------------------------------------------:-:-:--------------------------------------~£l'J'i)f't N~•i!!'J" DH


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f:i.•i(t:0nf: HD <JI:/1 :t.O .1. 0 1 !.0/ 2199 ·: {;}1.1[-(.'f' 1m u_~: 1 -'-· [; 1.[1 1 lrJ/ 219'! ~.tiu,.;. illliii\!·<\~ NV ~!{_:/ 1 I.!J l. !J l 10! 2rn :{g!~:;i.')_. bt~l li~ 1}~/l .1. tl ' D 1 10/ 'l./'l? .. l~E-tt:·~-~ -::-ht ~lt-t hs-~· ;W ~i!1/1 l.O .t. (l 1 )(ll 21'79 ~s.c~roy~~l , .. t~l€";' H!} l)~{l 1. 0 l.U 1 Wl 2191

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1h~s~ results r2la~:e only tQ the items t~st~d. ·!:'\';.~; r,_;.~~·~urt; sh,~ll. 110t lh::o ~·.-::·p~-,~>::!u,:~::·.--.1 J::.>:.:cf~pt in full -:1n1..1 '.!lith

~e1·mi~ston of ttte laborJtory.

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Report Approved By: ( . .AJ~ b _____ .<__! _ _L_ ______ ---------- Report Date: !0/ 4/99

The-or.lore d. Duel!.o, Ph. D., L~-1-b Director ~icti.Jel H. D,_mn, M.S .• f~·.:hni.cul Director Johnny A. Mitchell, l)ir•. r~chnical Sc~rv:!.ces

E1·ic Smith, A-ssi~tant T2ctmi'.:al Oir•e-ctor

Laboratory Certification Number: 387

COPY3

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT.

I :3bc;;~;--G :,..;ooDFJ~Hr.:. HL \?D_

Gi--1.•~\RLCTTTE, NC 28~~06

Lab Number: 99--Al46898 3an•ple 10: MW-26 Sanlple ·rype: Water Site ItJ:


l 09155--01 Name: WAHREN OIL

ERIC DONNELLY

Da t.~ Co 11 ec t'e-d · Tiu"n? Collt:,:t~d:

Date RS:.'t.:eived: Time Received:

"-7,/23/~79

11: 10 9/:;,'4-/99 r.r: •JO

-----·-·••·-~----~-----------H------------··•- -----------·--------·-·--------------~- ... ,,_,~,-------·-••-·-· RP~ort QuDrs Oil

A-l•J llite ""''"lt U11it:; llNit lirtlt f ~Cblf' cat:~ T ir1e - ... --------- ... _________ .... _ .... ------------- ··-·--·----

____ , ____

<i[;~f.B~IC ;'h~~Ftl~f: TUiS:--t r<t:·r:U·;~i< HD uq/1 '1. 0 t.G 1 lU/ 2n9 10:11 ~-.'}·_tiJi}(;t~ N~ >i~V'i. ' " ..__,/ i .. n '· 1!1/ ?PJ~ 10:11. ~: !:t, ~J \}t:?- are- i1e- :~o ~~~/l 1.3 1. J} l 10/ 7/~'~ 10:11 :>:;_;1.~1\il·~-. ~)}t.:);l m; ;jj/l 1.0 l.ll 1 10/ 2/9~ 10: ll r~et ~~~1-t -ltt1 t.~lt.-tMT 60.:i \J:;/1 1. !1 l.U 1 l!J/ 2/?7 10:.\.l L3•)j)fil~:4l Etil~l'' J.2.Q il•1ll l.O l.U I 10/ 7./'-rl 1\1:11

;>;:1~-.TI'.i .. ::> L,'!:!•! NG ;q/1 G.i!O~ n.>XH .,

If/ 2.$/'1~' t': N '·

100. ~0. - l~IJ.

T!J25E r-~::.~.uJ.t;;:. re.1at..::o on19 tu ttle tt.Gms t-E5t&rL 1~1\s ~epo~t sh~ll no·t be l'e~~od;Jted etcept jn Full a~d 1&1th per~issioll of tne laborAtor~.

i{tl-liy~t

-------·--------

r.t:undl F.G'undi f. :Ji..iil.~i f. GuaJJ. f. Gt111Ji ~-- Gun:E

f:. r\~u~~i

Report Date: lD! ~!99

l'hecdore J. Duello, Ph.D.} Lab Director Mit:i"!iH?-J. H. Dunn~ M.S.~ Techn1ca1. Dir-ectorJohnntj A. Mitchell, Dir. Technical Services Erit Sffiith. Assistant ·recllnical Director GdlJ. ,'; U.!ge.- Techn:i.r..:11 SPrvict:os


COPY3

tlltlhld U<tcb ---·--·---·--·-

80'lll{ 3~UO

SG2l3: 3JOV Blrl13 :150/l 81)2113 3~:-ao

au:tJr: :r..:uo 80~'18 ~~IJP.

:xH\h: :::'·16


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726.0177 ANALYTICAL REPORT

I WODDPi-\RK BL.\'D. I :!6(.}>.'}--t;.,

CHARLDTTEf NC

I Pro.j,ct: 1091:5:5-0l Project Name: WARREN OIL I Sampler: ERIC DONNELLY

Lab Nu!nber: 99-A146B99 Sample J:O: MW-27 SamplP T'Jpt?: ~o>;ateT'

Site !D:

Date C-ollG!~tect: 9/23/97 Tim1~.!' Collecte.~: 1.1: 10 Dat:e Recc~ivet:: 1Y/"C:4199

Time P:ecetved: c;·: 00

-··---------------------·-------··-------------------------


Revor-t Hui.Lr: on ~B~lytf:' P.esult Units l.l"!t UNit f•ctor Date TINt' -·-··--·------·--·-·-------·----- ·---·-------·- -------·--·

;.:JJR~mur r~mnnt:H:r~s);

Ptol::zer>t- l.b llq/1 .l. 0: 1. 0 .l 10/ u~·J 10:42

"!"•Jh..'e.<1e ~t., iJ•j/1 1.0 l.fl 1. lU! 2/99 10:-'12 t:t~l'JUI~nz\:;ae ~~ u~/1 l.U l.U 1. Ul/ 2/'1t; 10:~2

:<:~l~n~s .. tut:-11 ;~I) !.!'!'j/1 1.0 l.O 1. 10! 2/99 lO:.:lZ ti<?t hy1·~t··h1Jt~l~till'f 2~l6. •c.~/l l. t.l l.ll . 101 Jtn 10:42 ·' I~-tlj)T 1.<f.l_1}l ~thi-1' J8.U ug/1 1.0 1. 0 .1 10( 7./99 Jo:qz

'-I !"if. fA'!. 3:~ Lt-ild i-!!f )1;/l !}_{)(B 0. O~lJ ·' '1/L?l-1:1 7: }1

i-ie: = ;-~.ut >:1t~t~d~·}4 ,, U1'! re~m,i..: li.nil.:.

5G. ·· 150.

,-~ese ~esults rela~e Dltly to the items tested. This report shall ro~ be r~produced ex1:ept in full ~nd with permissiGn oF the labor2tnrij.

( / . _,.,

Al1i1ly!:.t ·--·--------··-

;: . ~;;nVJ

f.GUii•H r.Gun~!

r. tJJIICi F. Gmdi F. oun4i

H. i(e11ey

/ :tL; _2,._.,_:. ___ £_. ~--- Report Date: 10/ 4/97

Th~cdore J. Duello, Ph.D .. Lab Direc1;or Micllael H. Dunn. M.S. I r~cnnical Director Johnny A. rlit;ch~1 1l, Dtr. Technic.Jl Services Erit Smith, Assistant Technical Director Gail A Laye. Technical S8rvices

Laboratory Cet•tj ficatio·n Number: 387

COPY3

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2960 Foster Creighton Dr. P: 0. Box 40566 • Nashville, TN 37204-0566 Phone 1-615-726-0177 ANAL VT I CAL- r-.!EPCJRT

I Hf\l'JDEX 'JF THE CAi-lOLIN,:\5 bl6.'3

I 3600-G ~.JGODPARf.', BL\·'D. CHA!~LOTTE, NC 28206

I Pr·oj;o-c t: 1091!)5-01

Lab Nu,nber: 99-A146a93 Sa;np 1 e I D: r·1h!---.;t7 S:::rir:pl2 Ty:Je: ~~latf:)' ·

Site ID·

D3tE' Collected: Ttme-· Gollec·ti:•d: 12: l j

PT'Oj?Ci-1 Sampler: Name: l-IARREN OJL

ERIC DONNELLY Date Rec:e1\lt:?d: Tlme Recttivect·

9 I ;;!-4 .I '?''7

9:00

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R2porl; Date: 10/ ~!99

Tt1eorlo~e J. D~elto~ Ph.D., Lab Director ntchael H. Dunn~ M.S. I Technical Dir~ctor ,Johnn~t A. M:it.chelL Dir. ·rec~\nical Ser- 1.Jices E·l""i-c Smttf1• ,;sslstant. Tet:hrd.cal Dlrectm' G~ll '"~ Lagt.~ .. Tect",n1cal ~3crr-·~·h:es

L~boratory Certification Number: 387

COPY3

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2960 Foster Creighton Dr. P. 0. Box 40566 " ~ .•.

lh;\·~~ .,."1 .. -,,.,,.,'!~' . "c\:0 I '!o.:·~~-~!!~'

Nashville, TN 37204-0566 Phone I -615-726-0177 Af'iAL_ VT' I CAL HEPOHT

I H.C,ND.E '~. OF THE CPlf-~DL '1 NI~S ttl 63

I 360()-G WODDPARI\ .OL.VD. CHARL.OTTEJ NC 28206

Lab Nl.tmber: '.T9·-.$."':j146S'CO Samp 1 t:; 1 D. l~iw- :3c Eamr.; l e T~i r: 2: L.J6ter E:i t.e ID:

I F•·oj2•ci:: 1091.:35-01 Project Name: WARREN OTL I Sam:j 1 <>r: EH IC DONNELL'•{

Date Collect·::~a·.

Time. Collected: Date Heceived:

9 /~:..~3/1:/9 11 : !j.Q

C.,~/24/f"/9


Time Rec..=:: ive,j:

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T~iiS re~cJrt sh~ll not be re~~0ctuced ~~cept in full and with pe~mission of the labo~atory.

9:00

f. GiHidl f. ;;~n~! f. ~U!\~~ r .~l!t~H L!;UI\rli

F .. t;ua,~(

f\. ~tHey

Report Date: 10! 4!99

Ttle·odor-e \J. Dut?llC.· Ph. D., Lab Di"f'E'Ctor· Michael tt. Dunn, M.S. , l"ec~nical Direct~r

.Johnnu ''· MitchelL Oir. 1echn:\cal Servicr~;; Eric Smith. Assistant Technical Director Gail f1 L;3cg~·· TecnTtical Sc-rv:~c?s


COPY3

8;)1"1.£:

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I 2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 Ai"IAL VT I CAL REPORT

I I 3600--i; WOlJDPARK BLVD.

•:HJ~P.L.OTTE, 28206

109!.55-0l Project Nam~: WARREN O[L I Sample-r: ERIC DONNELLY

I I I I I

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Sample ID: J"IW-·31 Sample 'T!Jpe: ;,.;,;;;ter 51 te ID:

Date Collected: 9!23/99 TirY:e Col lee te~~: i. 1.: 32 Da!;e Receive-d: 9/24/~.Tt;'

Time Received. 9:00

r~tofC.:•t ilUi!ii iJH LiHlt Ll~it Fact9!' Dati' 1 iii~

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I I I I I I I I

~\0. - 130.

'iLes...::- ~·~E·SiJlt,s r·elate m:.l:.t to the :!.t£-m-:=. t.r:sted. 'lhis !'~p8rt shall not b~ reproduced except iP Full and with pE!'mission of the laboratoPy.

Repur1; Approved By:

fhe-m.1ori? 1J. Ou£-.tlo.' Ph. D. , Lab Direr.tor· nichael .,. Dunn, n. S. I Tecnn1t~l Director Johnnlj A. ititchelL Otr. Technic~l Servic-es Eric Smith. Asststdnt Technical Director Gail A Lage. Technical Ser't1ces

LaboratorH Cm•t.ification t-h.mbe-Y·: 33~'

COPY3


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANAL-YTICAL- REPORT

I

I P·•c-ject.: J0"'/155-01 PT·o .. iect. !\lame: t.-JARREN OIL I Sampler: ERIC DONNELLY

LaU Numb t~ r: 9'?-A 1. .!1·69C?2 S..=tmp le ID: r'H.J-<32

Sain;:rle T~Jpe: t.Jatf.H' ~:3it:e ID:

Date Cr..dl ect·rHJ: 9/23/?'-"l

TimE• Co1le:ctt:d: 1 1 : -~ ~-1 ..J

Date Received: 9/2Jt/9":;

Time Rece:i.vetl: Cf: 00

---------------------··-------··-·---·----·--


~•port YUill Dll fHFIJ.~\:~ Re\;ult Ur.its UNit Lift. it f:!Ctol• IJ-lte Htt~

----- ..... ---·- --------·------·- ·--- ·-----~-- "··----·--·-

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Til~~~ i'e~uits relJte an14 tr} the items test~J.

Thts re~ort shall nat be \'ept·adrJ~ed exce~t in ~ull dnd with p21'missio11 Df th~ laborJtory.

At\:fl!j':it

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f' .J);ndi

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RepG~t Approved By: Repor-t Date: J \)/ '-1/?9

Theodore J. Duello, Ph.D., Ldb Director Mich~el -H. Dunn, fi. !3. r 'fi:i(:t\nic.ai DirectoP Juhnnr~ (~. r!itchell, Oir. Technic,-il SePvice·5 Erl.':: Smttn, Assi.·i"jt.ant Technical DiP,:ctor G.ail A L-3.qe. T~chnical Sei'>/l.c.es

Labor·ator·y Cer-tification t-!wl\be--r: 387

COPY3

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPDR'T

I

NC 28206

Lab Number: 99-A146903 S<"Jfflp l:e ID: Mt-.f-.34 Sample Type: Water Sit,., ID:

Date Collected: 9/23/7? !. ()91 ~5-\).l Time Collectea:

Nama: WARREN OJL I Samp12r: ERIC DONNELLY Date TimE

Received: RE?CE'iVi?d:

I I I I I I I I I

t\t~(WI't I)U4il iHl Utdt Ut1tt facti}r

:...tWt;M-ltG F~f~Ji'1f.JO\.Si>!

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!'t1ese reslJlts re·lat~ 011.~ tG the items tested. ~-~fs rep0f't shall not be rep~oduced etcDpt iP f~ll afid wittl p~~~ission of the laboratOl'Y·

10:40 9/24/9'7 r:;: GO

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t .£\.i)ldi fJO'llU f. ttliliH OG2i.rt f. Gt.li\~3 !Jnl:.i{l,

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I Report Date: 10/ 4/9?

I I I

Theodo~P J. Duello, Ph.D .• Lab Oirec·tor Michael ti. Uunu. M.S., Technical Director Johnny A. Mitchell. Dir. Technical Services Eric Smith~ Assistant. Technical Director Ga:tl ,~ LBfll:~~ TeciHdcal Ser·vit:e-s

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CHf.\RL.OTTE, NC 2.B:;;.:06

10915~-01

Project rJame: WARREN OIL I Sampler: ERIC DONNELLY

!-:S:b Nun1lJ8Y': "?r7·-£\:!.·!!·6~;:o.q.

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Date CoJlt~ct·ed·

·rime Coll~cteu: Dat& R2C£.1 i'>leti: Tiu1e Hecejved:

9 !";:;3!'1? 11: 02 9/ C-'24 / ri9

9:00

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L:.:: 'H1 )J(•

··' :~~!/) G.DG3 D. GD3 1 'i/'FY'i'-1 /: 3'-l

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,.~QSP Pesu!ts i'Elate only to ~h~ 1te~s testact. iht·s rept1t"t: ~,;11-.d.l n•Jt tJt:..! r·f~fJ!"'..:l>:1ttcsd e~\·:~pt i.r. full .-JnJ ~,i;i.Ui

p~r·mlsston of tile lJboratory.

fmalyst --·~-·---·--·····

F. ~;Hrll.!

f" llun•H r. GuuGi. f.Glln~i

F. ~;tHlJ.i f. {;UTI<!:i

f~. t<•-:.Llt:~

Report Date: 101 4/9Y

Theod~re Ll. Oue!loJ Ph.D. i LaD Director Mict\del H. O~Jnn, M.S. 1 fect~ni.cal Director ~Johnny A. Mitchell, Dir. Technic.-)1 Set'vices f.!'ic Smith~ Assistant T-echnica.l Dl.rec:t.or Sail A Lage, Techtlical SeT'Vice~

COPV3

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANAL v-r I CAL RE:P'OR"T

I 1--!~NDE:~: OF THE CARGL IN1~1S 6163

I 3600-~(.) t.-JOCJDP.~RJ.(, BLVD. CHARLOTTE.. NC 28206

t_ab Nutnber: 99--A146903 Sample I D: Rt.-J·-;;? ~Sample T':lpf:: t~Jater

51te ID:

I Date CtJllecte-t1: 9/23/99 Pr·o j e·:~ t;: 10915~·-01 Timt?. Colle•cted: l.1: 20 Project N~me: WARREN OIL I Sampler: ERIC DONNELLY

Date Received: 9/2.4/99


Time Received: 9: 00

··--·--- ------•+ ---------------------R~pr.rt ~h.li!il Dll

Anali!ti' llestil t UnJt!) Uiilt LL<it Fisctor Dat< TltH?

--------------------------- -------------- ·····----- ---- ·····-

1!ffil.1;Hf1E f~R~i1f.T£R:S1t

&~i17..eH~ 18.1 \)~~11 L.l] LU 1 10/ 21'17 Q: ;!J)

loluelw MD 1..19!1 .1.0 1.0 1 10/ 2f1Y :t 10 t:tiiylBcf!l(·ne l!J) ,;~11 1.0 • n .\.U 1 10/ .219~ 0:70

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These results J'Gl~te only tn th0 items tested.

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Thi~ 1'epC•l't. sh11JJ. not. bE- ;•t:pro(iuc:t?d t-~·XCE1 pt in Pu1.1 lind 'J.iith per~ission of the labo~ato~y.

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Report Oate: 10/ 4/99

Theodore J. Duell-:'} f'tL D. , Lab Dir-ect.crr Mlcha~?l H. Dunn, M.S., Technical. D:tr·ector Johnny A. rtitct\ell} Dir. Technical Services Eric Smith, Assistant Technical Director o~::-:tl ~~ L~~ge. Tec.hrd.t:.i:'1l 5i?f'V1ces

Labordtory Certific~tion Number: 387

COPY3

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Nashville, TN 37204-0566 Phone 1-615-726-0177 AN.P>L. VI I CAL REPOF'1T

··--···-----·

I HAI'•l.DE.'X OF 'fHE (:P,HOLINI~S blo:·J

I 3600-G WODDPARK BLVD. CHAHLDTTE~ NC ;28206

L.ab Nuntbel': 99-Al46906 :SBJlip 1 £· 1:0: RW-<J Satr.plf! TJ;re: ..... ld·~:t?r


5.1 te !D:

109155-·01 T.t,ne CoJ.l,:?cto?f~:

Nam<!: WAHREN OIL ERIC DONNELL\'

Date Heceived: Tim~~ Receivefl:

Re;•ort Qu;;rj Dil iir;iiJ~'te Result U!tlts. llolt Lhut factor v~t~:> ·~ j iff:!

-···············-· -···-··----··---- ····-----·~··-- ---·-···-- -··--··-----

:•IDIXAH.lt P~P.I\NEfERS•

(H!IIi!F:fi~ 32). Hg/1 10.0 1.0 .VJ 10/ U?9 U::'<O Tolt~t-n-1:! 2:Kl0 og/l 100. 1. (I j_(fl) WI 2i99 o: ~~n ft~l!}} )H!I!Zf'N? m. e<rj/1 10.0 1. I) HJ iG/ Z/')'-) U: ~·U ~4le-nr.::. :- tot;J 121U ug/1 lO.U .1.(1 10 10/ 'l./';p; D: ~.i.!

i'tf:'tltyJ.··t--~utyl~Uet· Jl:m Uj/1 100. LD 1110 Wi 1/9V :.s: -:m :t ~-uvrop\Jl ~:th£oi" TN_.. 09/l 10.0 10.0 lfJ HV un f]; ~;~

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T!1ese r·estJlt~ relate ant~ ~a tn~ Ite~s tested. I11i··:i :·~~p·J~·t ·;h.:tlJ. i'!_-:r:.; he ~·epf'~~duo:ed E~t-.:cept 1.1 ·f~j1l .. ~r":J 1.u1~:;ti

p~rillj.nsion tlf tt1e labordtary.

Seport App~oved Py:

Tt1eodor0 d. Oul..~lJ.o~ Ph. P., L-.'!'.b Director Mich<H:c~l H. Dunn, M.S., Tt--~chnicdJ. Otn~ctc-r

Johnn'J A. l"iitchelll O.ir. Te-,:hnical Se:"'vic:,.--;s Er i.e Stn.t. th, t'i-ss:Uit.ailt Techni<::dl D.ti"'-ECttJf' Gail A Lag8, Technical Se~vic~~

Labor~tory CertiFicdtion Number: 387

COPV3

t.l/::::~3/'=19

10:20 9/24/97' 7':00

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------·-··· -- ------·------

r. G!Jfl<l.i t!Ol;.il f. ~tiTJIJi 31~i.'H!

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Nashville, TN 37204-0566 Phone 1-615-726-0177 RF.:::PORT

I HAN1.n::;( OF T!~E Ct-"-\fU.:JLlblt'~tS 616~3

I :3600·-c;· '.,)CJfJDPNFfl. BL'v'D. 282C6

I PT·t<j2tt;: 1091'::·5--0.i Project; Name: WARREN OIL I Sampla~ ERIC DONNEL.LY

LaD Number: 99-:~146907

S.3mp 1 e I D: PP-~4-

Sample Type: ~~~ter

Site TD:

Di:Jte Collected: Tlfl"IE· Col1PcterJ: Dr.r1t:e r~eceived:

Timt? Received:

·::;; 1 c.:J .1 tt~=;

10:30 9/ ;? .... 1 I 9'·;•

9:GO

--------------~-----·------·----------------------------·--


E t 1·~~:1 ~~t.~ r;U·ne ·r-:tl~n':~·;, tot:}:l M::: t ~:Jl·- f:-P:.:ty l~ th~rIJc~I\;?:Jl ~tl\l"!r

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u.na3 \1/2,1//'t'r

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fl1ese resEJlts rel~tB 0n14 to th0 it~Ms tested.

HM

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l: .7.0 li': 18 UQ

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r·~is report shalt \iOt be reproduced except in full and ~tth c2rmis5ion of the ldbordtOl'~.

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f. biH!li

f. ~Ur.lii F. :;,Jndi f. :;unl.!t F . bhn4!.

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Report Approved By: Report Date: 10/ 4/99

Theodor~ J. Duallc~ Ph.D. J Lab Director Michael H. Dunn. M.S. , Technical Director ,Johnny P1. Mitchell~ D1J'. Technical SeJ'Y:tce-s E~ic Smith, Assistant Technic~l DirectGr Odll H 1-3L~e. Tet:tn)1cal 5er·v:ices

Laborator~ Certific~tion Number: 387

COPY3

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I I 3bOC<·"·C; l<IODDPiiRV. !ll.\/D.

Lab Number. 99-Al46908 3..:tmp 1..: ID: Rlr-l·-~

S<...:Hnple TlJ~i,2: l.Jater· CH.~\P.LIJTTEI NC 28;;-;Q6 Si t;e ID:

I c0 7'C•jEct: 109155·-0.t Project Nama: WARREN OIL I Sampler·: ERIC DOl·lNEL.l_Y

Dcd;e· C.::11ec t·ed: Time Cr.d lee ted: DatE Rece-ived: Tlme Received·


•URGR!HC P~RAMHE£S• [tt? N":U·iH~

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U36, 226n. 340. ~~1.

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Report 0-dt!?·

Theodore J. Duello, Ph.D.; Lab Director rlichael H. Dunn~ M.S .. • Technici:1l Director JohnmJ A. MitchelL llir. Technical S.:,·vi<:es Erit Smith.· Assistant. Jec!·H1ic:a1 Di)~ectr.H'

Gail A Lagt:.•1 Technical Ber·v:icE~i

L.abor~ltnry Certificati...wn Nutnbep: 387

COPY3

9/t23/'-:79 1 o· 3~, 9/24/99 9:00

F. ~;~!J"J·Jl sam• f. ~IJIItJi 602ll3 F. i;vnd.i S02H< f. ~l.lT11H 3-((lli.l

r. J;u1HI -~0:?1t1

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f{ 1:~··Llt<i~ 3fEUc.

:<:<Ill ~~Hl

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'!;'t}t;


I t·~~NDEX OF THE CAROLINAS 6163

I ~3b:)r)··G ;.JOOC<?ARf\ Bl. VD. \:HI\RL.DTTE, N(: :;?.8206

Lab Number: 99--Al46909 St:Hnp 1 (~ 1 D: ~·J-1

S.:unple Typ0: t·l.~:tter>

~~1 te ID:

I Date Collected: (r / .2:..' / f:J'9


F-'TC jP.Ct: 109155-·01 Time Collectf:':J: Prc•,ject Name: WARREN OIL. Date Received:

ERIC DONNELLY Time R.,ce1veo:

R,;port Pti.ln ~!l

P!1.nlytl~ ~eSIJlt IJHit·'i Llt!lt U"lt f4.Cbl1' D>t~ HH\l

.. -·- -·-·····---~- ---····----·---- ---·-------- ---·----··

l,fi.f.:~~~E PARqn£ rn~s~ l~.::-1>7..~[1-~ i'U) ligli l.U "!.0 .. 1!)/ ':.'/91 3:19 "T·.:i.t•>?l}l:! ~l:• 'J9:'1. l.C J.O 1 l'i/ 21¥1 ·J:U ~= t i;~ll li"l1-r.re ae liD U~J/.l 1.tl 1.0 1 1\.i/ 2!~~ 3: 1'1 :~;_tL~r··~~-;, t(it~l HI' li?/1 LQ l.Q l 10/ ?./9"9 >:11 ;·!r:<t.h:~I .. t·-hut~ieth-er Hli \.)"j/1 1.n 1.0 1 !i)/ 'l./?9 ~:11

!:::.nvr-.:.,pyl 1'..!-th~r M~ >.:~!1 1.0 :!..~ l 10/ 2/9"J 3:1?

."':iu·~~L ~:;:;:

f~ .::1 :·\!) Uj/.i e.mH ,., .,.,.,, ' :-'ti.'~~/?9 '· H u.•.Ju'.) '·

!+f) ·- E\1~: \li'ti•C:tl:~.'j irt. tt.r: l't:·:·m·t l!itlt.

13. ~.iO. - 150.

11••::s~ n~·;;: .. : l. "\~s r ~?'lh'b~ ur1.lq t>) t1h;~ i t-eni·~ te·:;;ted. rh.~.5 !'~fJO:"'t -~:;h;J.ll iHJt tl:£~ 'i'~~pf">itiUCEtJ i,!-!-;(Ci?-pt :i.r. i~fJll .;:nd mJ.t.!1

pe!·misslon of the ldboratory.

.t2: 40 9/;.".:I.J/99

9: 00

r.wa~st n~ti\c~a.

-----·····-··-··- -·-·--·-··-··-

f'. G!..ii\<H 3H'll~

r. Gur .. u ~UllB

f. ~IJ!tdi £02lB

f. GVI\!.ii SC:!l!}

r. Gila~ i lj021.l~

f .li:Jn.ji 80ZW

R. Ki'l!~~ .,,, .... , .. JUJ~~,;

?:&port O.ate: lO/ 4/'J'j'

Tht:!-odor·~' .J. Ou>-;!llo; Ph. 0.,. Lab Diri:!Ctor Michael H. Dunn, M.S., Technicdl Director Johnny A. MitcllBll, Dir. Technical Services Eric Sm!th, Assistant ·rectt~ical Director Gail ~ Lage. Technical Serv1ces

Laboratory Certifica·tion Number: 397

COPY3

Hate It

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3~i01

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35C1 ;:~m

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2960 Foster Creighton Dr. r 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 A"JAL VT I CAL_ REPORT

I ~-it:·~f-,!~;f.:.:;< C.IF THE CP,ROt.INAS 611.::.:3

I '3bGO···G ~.JOODPAH~<. Bt_VD. Ct~ARl.OTTE, N(' 28206

Samp1.e Typp: Water -~7a tl'!! ID:

I r•·,-o ,i2C c: 1091:55--01 Project Na~e: WARREN OIL I :-'i-3mp .l er·: EFIIC DONNELLY

I ftll<\1~'::2 Re~11lt

····- --- ······-·· ------·--- ---·---~- -----------·--··-

I ~~GR!;P\W: pf,i;!'llft IERS:• u~~~u:~n:: Ht> fill~IE-:1>3 W*

I cu·::;l :~r.•n;r.r.!'ti' «D :-;!J~--~1,~-; ·. t\1t-;,.t IW !1d: h ~ l·- ~ '"i•Ut q.~{1 t'h€-"f P.fl

I 2:·;e~ny~'i. ~t~~\~ i~jj

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fi(.lpm•t Unit; Unit

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r• .! I"~~ .• v .. •

Date TilftP.

Date Tl.me

IHl

fl~tor

1

-~.

1 1 l

I -r:·,f:o·:~e :·~:·sult~ ·\·~~1.-:~t:? onl4 to 'tile iteit\S te-·sted.

r~.:ol1 et: ted: Collecte-d: Received: F?eceived:

D>te Ti.ti~

---·--·· ·---

iO/ i:N"' ):-=!~

10/ 2/9? 3: ~t~ 1.U/ Z/19 ~:4'1

l\11 2!'11 3: 49 !G/ :un ?.:49

!U/ Z/9';] -3:ti5'

9/2'-1/'/'J /: J4

I !~•ts reuort ~h~ll n~t he reproduced E!rcep~ In full ~nd ~i~h ~ermission of the l~boratory.

9/23/99 12: ;:•o 9 I 2-41 O:.J''l 9:00

ru~alyst ~tl\t.hJ

-··------·-·-··· ~---·---·-----~

f. ~ur:di 8021!) F. Gun11 i 60211J f. Gun.H UOZUi f . ~Vi18i oonu f_ ~!Jff•Ji lJIJlU! r. ;;,iihH BU21G

~~ v.,..L1f:~ J{J::t\Jt;

I /A_~ s --- '""'-·""" .'/ , .. ----- Repot•t Date: 10/ 4/99

I I I

Theodore- lJ. DL,e11o> Ph. D. J Lab Director Micl~del H. Dunr,, M. 5. ~ Tar.hnit:al Direct-or· clohnny A. Mitr.lielL Dir. Tethnital Servi•~es E-ric Sm1th, As.::.1st.c.n,"t ·re-chni~a:t OiT'ectnrGail A Laue, Techn1cal S~r-vices

COPV3

U>tclt

)501 :;501

:.~~1)1

NiH J":il\1

15a1

~rt•K\


I HANDEX OF THE CAROLINAS 6163

I :?. .. ':,c~o·-<~ WDIJDPARJ.~;. BLVD. CHri..RLiJTTE.t NC 28206

L.ab N!Jinbt?l': 9c1'·-Al4t.'.:.tS~l1

s.~mp J.e !D: ~.J--27'

C3.amp 1 e TIJ p e: ~.Jatel"'

Sit~? ID:

I Fr-c,je.:t:: 109155·-01 Date Collr~cted: i::; / 23/9':? ·r 1 me Collected:

?1' ,, j i?{: t Name: WARREN 01 L I Samr>l ;;r: ERIC DONNELLY

Dat;e Time

Rec<•1\li?d: Received:

I I I I I I I I I

Rep•J7t Gu•u Pil Re-:iult UHlt Uttlt ra~tm· octe

EF.Q~£.111-:lC Pil>:M£ rms.~ t!Na:t-r.t? »P l;g/l .t.O 1. tl 1 101 2/99 T1Jl1Y?i<~ 11~ U9/1 lJJ 1.3 1 10/ '1/99 Ett!~lt•~»Zf?i~ ~w u~/l 1.0 1.0 .1. 10/ 2191 :~.~~t~ng·;, ttt:ll i'lD 1J9/l 1.~ UJ ! 10/ 2!91 r~~th~ll·-t·· iwt~l!!ther Hi) 1]~/l J.n 1.1.) - lO/ 2/?~ :r~.opr::<?Jl tthrz.r liD <'911 1. 0 l.G 1 lll/ 2199

:-~\'tl r:::_\oi L-::;;.i ~~c, ~:}It LU]fH U.tWi :t ~tl.9!91

Xtl .. ~0t d~tect€·d dt tb!! ;pprwt lin\1:.

~i~l - l!iO.

Thes~ results I'e!dte only to the iteas tested. Thjs report shall nat be r0pr0duced except in full ~nd with pet'ffiissio~ of the laboratc1rq.

Tl11e

4:19 4:19 4:1~

q:11 4:1\' ~:19

1: ';4

13:00 9/24/99 9: 00

f. Gl•r,Gi aonr< r.;;uudl sg2w F. t;ucdi ~li1lP

f t<JI\Ji S~JT'd~

f. SHnH !HlZW f. Gt•nd.i fW11U

f:. k'~H·!~ ~i)·~i).;

I Report Date: 10/ 4/99

I I I

Tneodore J. Ouel1.o, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johr.r.y A. Mitchell, Dir·. Tf~chni~al Set'vices Eric Smith~ Assistant Technical Director Gail A.Lage. Technical services

Laboratory CertiFication Number: 387

COPY3

.l:;ct 3501 'J:jfJl

7:·501 )~i01

)~;(11

•7-(4.~

····--·----··· ......... ,. -..... , 1••1 I II 1•1 •••• •••• lUI 1•11a•a •••• I II 1•1.---• •••• ,L_ • .••. .... ... ·-· :=' -~ ·~t :II


2960 Foster Creighton Dr. P. 0. Box 40566 " ~ It .•. · • r~;.~.~h. "'

=~;~·~·;~-~·~- - J , •. &.~::.<r';Jl: •IIi•~•

Nashville, TN 37204-0566 Phone 1·615-726-0177 ANALYTICAL REPORT ·---.. ···----·

I HAf'.\DEf~ UF THE CAHOl.. [ f'.l!''\5 616~:?

I 3600--G 1-JOODPAf':V, BLVD. CHARl.OTTE, NC 28206

I PToject: 1091:}!:•-01 Project Name: WARREN OIL I Sampl<=r: ERIC DONNELLY

L~b Number: 99-A146912 Ela;TJP 1 e I D: W-3G Samp 1~:: ·rype: \.JatJ:?f' Site ID:

Date Collect·ecJ: Time Collected: Date RecP.:i.Ved: T:ime Hec~:liVt?d:

'?/23/0:.?CJ 10: 50 9/24/99 9:00

-------------····---------------------------------------- ·-------·-------


r.e~ort nu:w 1HI tlniil~t~ Re<ult Unit; L!Hit lilllt F.;c.tdl' 9<te ---- -··-· ... ---- ---------····-··- --··-----·-··- --···--- ----------

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Xyli·M!S. ~ tot-al M~ o~/1 LO J. 0 1 10/ 2/V, ~ethjl·t .. t·ut~leth••r 1-:f; u~/1 J. 0 l.G 1 lG/ 7fJ9

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~5. ~U. - t'JO.

r~0se resul.ts relate only t0 tt12 tteQs tested. 1his report ~hall not be ~'eproducad ~xc&~t in ~ull dnd witt~

pe1·misslan of tt1e ldboratory.

Till< Rni11!jSt ----·-··-----

1:-W f. Gtiih1t '1:~1 (. blHHU

~:~\' F. !;t.n12l 4:q1 F. Gtmdi 4: q9 f. Stu1~l .q:49 f.fundi

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The•jrf.:>re .J Due.t.lo, Fh. D., L·Jb Oif'i~ctor

r!lchael H. OlJnnl M.S. I Techn1c~l Dir~ctar

Johnny ,'=\_ MitchelL Ui~:·. Technical Ser•viu:~s t:r.it: Smi·th, Assistant Tt:!C:11nical Director· G-ail A L;-tq.-:.~, Tec~io.ie-31. Service·5

Laboratory Certiflcdtlan Number: 387

COPY3

n~tt.od [latct;

-------··-

w.nu 3501 SUlU< J:iOl 13021£ :r..:rn. a.:JZUI '!~01

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HA~·~C~E:X Df" THE CAROL .. !NAS 6J.63

I :>boo-G W'JIJDP,~RK eum. C~·lf~RLOTTEt NC 2El206

ANALYTICAL

S,;;.mpl.<::! In: POND S.:1mple 'T!Jpe: t,~L:iter·

Site rD:

I Date Collected: q/23/99 P r· o j !? r.: t : ! 091 ~ ~·--0 1 Time Collected: 11: !.~i

P~0ject Name: WARF~EN OIL I Sampler: ERIC DONNELLY .Da·ter R~~c e 1 ved: 9/;:1.4/<:j'-=.l


Time Heceived: 9:00

g,,~rt Q~l4!\ D!l. ftMlytP. f:e'S•Jlt Uu!to; UMlt U•tt factm .. O•t~

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lhese results relate onlij to ·~tiE iterns tested. T~ri'±- r-c-o.pcr·t. :::.hi-111 r .. ot. t'1E rr·proouced t~:~cept :in Pu11 an1:1 l!Jith p;ermission of the labor-crt-on;.

Htte A!illj~t

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:;·: -~-~ r\·. i>'(•::).e~r

Report Date: 10! 4/9~

Theodor-e- .J. 0ue-llO.· f'h. 0 ... Lab Dirt·c"tor-11ichael :1. Punn.• M.S. J Te-chnic~l Dir~r.to~·

\JotHH"ilJ A. rlitt:hell, Di:r. Tet:hnical Services. Erit Smith~ Assist~nt Techn:lcal Director Oaj_l A i.r:tge) Techrdca.l Services

Llboratory Certi~icatian Hu~ber: 387

COPY3

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYT:rCAL REPOR'T

I HANDEX OF THE CAROLINAS 616~

13600·-:.; WODDPARK BLVD. CHARLOTTE, NC 2B206

I Pro.ject: 1091':)5-01 Project Name: WARREN OIL

ISamplar: ERIC DONNELLY

Cab f';Jurnt.'2r: 99'-.. f~-146917 ::5amp] e 1 D: l"'JW-::-~:.1

S:3mple Type: l_...;att?T' ~-5it~:".' Jn·

Uatt: Col lee t·ed: Tim.t! Gollect;~?,j:

Date R e c e .t ve d : Tin1e Received:

l2: ::iO 9 f2f:l·/9"i' 9:00

··---·----------·-


RepOI't fh.iiJI) Dl:t Anol~t• Rto~-Ult lh:dts Li~it lirtlt far;tor Date ---··--------·-----·----~--·- ---·--------· ---------

>ORi;AAIC P~RMHERS• [lf'ra~nl:l' ~.].;_ llg/1 10.0 1.0 .·~o .WI 2199 loluen• .:Na. ug/1 1.0. 0 1.0 20 10/ U?9 EtbyHenzenP 144. ugll 20.0 l.O 20 10/ un ~:y1£rnes. > totdl ~tq_ ~ u~/1 10.l1 1.0 20 10/ 2/99 n.t ~yl· ·t-~vt yl•tber 311!1 vgll lU.D 1. a 10 10/ 2/'l'f

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;m - But ~etected at tt.e l'E'~OJ't .LiMit.

9~.

ThBse ?esutts r~late anl~ ta the lt~ms tested. This repo;·t ~ha!l nat be rep1'Uduced BXcept in ·fLsll dnct w1~h

permission of the laboratory.

nne MBa.tyst .... _,._, ______

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Report Appr·cved By: Report Date. 101 ~19?

Ttleodori-: (J. Ouelloj Ph. 0., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technicdl Service• Eric Smith, Assistant Technicdl Olrectol' Gail A L~ge, Techftical Services

Laoor·atol'tJ Certiflcat,ion l·lumo.-~: 3fJ/

COPY3

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PROJECT GIUALITV CONTROL

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12-X~l~~~~ i).l.iO.tG 1'!~1/1 '1J

J. .i>JH~:t!Ivrc.t'th·ilne- n. um (~ )~~/1 q3

.t _,.i·-;) i t:\iJ.Ortlet~".illff ' 0. OU10 !'?Fi 4.~

COPY3

DATA

rMI. ·"'·' .... : . ,,·: . . i '•''" ... '"'' ''l:j\''"-"" .. •

' .. :.; ,,::.. PECIA. IZED·.'rl:SSAYS, NC. · . liJ·~i~~S· .·>·:'··'·'.'1;!.t"'';;,··;:~~A.11,!i:>~~'f''•::~:l·. · · ...

~~ . . ,. .i•\.··~12960 ... FO..·ter.~.' .. · .~Drive. •.N .. u.hvllle,TN37204 RECEIVE OCT 121M\ 88-026780 ·~ X '•"":.l110CJ)7~.·.~ ~~77,· ~~ (615]726-3404. ~

/FacJSite 1.0. ----Fax Number 704-598"'2248

Method Preserved

Sampling

~ Q ~

SAl PROJECT or QUOTE NUMBER (to Insure coiT8Ct Analysis and Billing)

Received by:

Received by:

by: Laboratory

- -·-

Temperature Received _..J''-l''--

AJiblll Number ---'------

Date· llma

or;r 1 2 ~

/FacJSite 1.0. ___ _ FaxNumber-- · 704-598-2248

Matrix

,.

Method Preserved

-

Sampling

~ c w ~ F

g,;i rn.vv~v. v• ;;vv-.~ i..;vmu~n (to Insure correct Analysis and BliUng)

21[1"1: l~ ,-: Date lime

- - - - -

"·· ·j

1 · Te!"perature Received Alrbm Number

,-:- Time

- - - - -- - -

I I I I· I I I I I I I I I I I I I I I

»EECU~'to L:.

704-598-2248

Method Preserved

Sampling

~ c ~

88-026777

-TAT·

ri:t. ·: ·t f SPECIAL REPORTING REQUIREMENTS I ·- I I SAl PROJECT or QUOTE NUMBER (to Insure correct Analysis and Billing) ··-: Next Day a .

Other.....,..--..,. ,. · Temperature Received ----

Airblll Number ---'------

CUSTODY ··---,-,-·-"~7~ .J, 17/ -.-r;,.~ I lh -;.. Received by: . . . ·I.

;~_- ' CO · Relinquished by: · · · Dale llme Received by: Date · Time

Date· llme

~RE RD I . . I ••{ .C'"• • .•. 'k'.'· -::· Relinquished by: · · · Date llme Received by: Laboratory - ~-·· - -

·;· b

(\ i;o

-- ----- ... --- --· --- ------

/FacJSite I.D. ---Fax Number _:_'--'Z04-598•·2248 ·

_SPECIAL DETECTION UMITS

Method Preserved

Sampling

-~ ~

REMARKS

OCT 1 2 1999 88-026779

s:an:r:T :~~ ,: 3-Dav:: _ o 'I 1 1 \2·Day : · CJ . SPECIAL REPORTING REQUIREMENTS 1

:Next Day Cl Other. _ ___,...;., ,. SAl PROJECT or QUOTE NUMBER

(to Insure correct Anatya:ls and Billing) Temperature Received

Aliblll Number ----'-------'; ·-~~----------~------------~----------------L-----~------------~ Received by: Data·· Time

. RECORD. Rennqu1snea by: ·: ""' Datil I Time Received by: •. Date · I Tliilo 1

'';0.::~. Rollnqulshedby: Data Time Roceivedby:Laboratory AAn ,(Da!B Time I ' ·, .-' :~;. ' ---------


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL.. REP(.-:JR'T

I !.·JiJODPAii~i. HL.VD.

NC 28~;:06

L.ab Number: 9cr·-:>-~1 •t·b~t'.l4

2:\~~mplc ID: INF :3!:lt:"tple T~:pr:: ; .. Jater Site IU:

I Proje·cc<;: 109155-Gl. Date lime

Collect-ed: Collected:

9/23/99 1:.1: 20 9/24/q9

9:00 Pr·oje~r.:-t; I Gampl.er:

1\iame: WARHEN OIL ERIC DGf'.lf'.IELL.Y

I R~sul t Unit 5

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I 111ese 1·esults relate only_ to th~ items tested.

Received: Received:

Y!29191 !: 37 Yl2'i/99 1:37 51291~~ 1:37 '!J/2'!/9~ 1: ~7 ?!7S/~l'i l.: J7 '1/Z'i/1"1 1: cry

"

I 7his ~2port shall not be reproduced e~c~ut i1s Full an~ with pEt6ission of the l~bor~tury.

f. G!.HH1i

f. GunM f. f;ljtHii

f. r.:mJ1 f. t.::tm~!.i f. G:.H1~i

I R~part Date: 10/ 4!~~

I I I I

Theodore J. DuelloJ PM. D. 1 Lab Director Michael H. D~nn, M.S.~ Technic~l Directc)l' JohnntJ A. Mit.thell.· Dir. Technical Se1·vices Ei~ic !::\.roit.h .. ?'JSsistarrt Tr:chnicul Dir-ector Gr:-til A La~tt?' Te~:hnica1 Services

COPY3

C·O:l ,j:}2

602 fj\"") ..,,,,_ {.[Jf

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===~ ,.~ :iii::: .. , ..... . .. .. .. . lr } ·••



:trli~ _{v-.. ;i .. ~~ ... ~, Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYTICAL REPORT

----·-------·

I 1 360::.-<;,

G!--~t\RLCTTE.

I FTGj;ec:t: 1091:'\:'\-()J

Proj~~t Name: WARREN OIL I Sample~: ERIC DONNELLY

Lab Number: 99-Al46915 Sample I D: ~·!I !J

Sample Type: Water Site ID:

D21te tullec:·t~d:

Time Cnllec·t;ed. Date f~t~cl?.tVed:

Time Receivet1:

'-:1 / ~-."!3/ ~-rr:;

13: ~2~ 9/24/9'-? 9:00

----·--·----·-·-·-----·-·-·---·--·--·-·-----


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'f.JJ

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l.il u l l.U l.G 1 l..O 1.0 l J..D 1.0 1 1. u 1.0 J 1.9 1.0 J.

Jill<.

Th~sa l'eStllts t·~lat9 only to the items ~ested.

oat~

",'l211Y'9

1/2919? ~12.1r"t;..,l

if/2~'/9'1

·:/ /:t; /''11 ~: •. '29/'J.'9

·r;·,is r~port ;h~ll ~ot be rept·cdu~~d e~cept in ~11ll and with ~2rmi~si0n of thP l.atar~tur~.

2: !17 L t·Ui\J i l:Ol F.Sondi 2:U7 f. G\!!Hi~

2:07 f. G•Jti:Ji

:L 01 f _ t:un:E l:fU , . . G:Jt;,L

Report Date: JO' ~199

n-~eodO\'>~ d. Du2i.lol f'h. t> .• L.ab Dif',?Ct•JI'

nich~el H. Dunn. n.s. I Tecl1nical Dlrector Jo~nny A. Mitch~ll~ Dir. Technical Services f.ri~: Smtt.l''ll 1':f.S'SlStJnt T.s-·:hni·:al O.irector 13.a i.l A L-:l·~e. Techn L(.al Services

Labor·at,DT'IJ Ce:-rtificat.).on Number: 387

COPY3

MJZ <1!1~

61J.Z '1'13 6U1 493

~!)2 493

W.i -'-!'f3 602 ,m


. I

I I


-SPECIALIZED ASSAYS, INC.

2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone lo6l5o726°0177

Prc;j(~~~- 109155-(}1 Pr·Qji:!Ct N:Jrne: L~AR~{EN OIL. Sar:t~1l·~'i'' ERIC DONNELLY

(lr, :~} !:i:'2 R•sult ,.,._

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!1. Hlsi~"iic~: 602 M. Hi>.-llc-k 602 n. !Hw~Uc:k ·:'.ti.~.Z

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n. mt;~iit-:k •r•·• "'.IL

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone J-615-726-0177 Af'-iAL ·y,- I CAL REPORT

Laboratory Number: 99-Al46916 :;.")EHI1:p L P. I~. EFT

P::·iQ(-;: .2

These results relate only to the items ·tes·ted. Th:\s repor·t. S!"H311 1~ot tle repr·IJcS..:c£·tl e:-:·.:ept. :ir1 -Full c:H1d ·~1 ith

p·e-r-m1ssion fJf t.he laJ)orator·y.

fi>~pol't Appt'0VtH1 Bs.j: Repa1·t Da~:e: 10/ 4/99

Theodore J. Cuello, Ptl.D. ~ Lab Oir~:tor l1icthiel H. DWHII n. S.' Tentrdr.:al ~}ij'j;.<CCiff'

dohrlltl;) f:L fiit.t:ht:.'}}~ Di~'. Technic.:d SETV:i.1:i::s

Eric Sillith. Assistan·t l'ethnic~l D1r~cto:·

Gail ::t L~gr:-, "Tcr:hr,:\.c2l S.E"T'vices

COPY3

. -I

. ~

··.~. ·-.~ .. .;.~;-:} .. -'" ... !-!.l"i'".or."tt.-!. ': I I I I I I I I I I I I I I I

·I I I


APPENDIX C

GROUNDWATER TREATMENT SYSTEM ANALYTICAL REPORTS (07/99- 09/99)

~ HANDEX®


2960 Foster Creighton Dr. P .0. Box 40566


ANALYTICAL REPORT

I I HANDEX OF THE CAROLINAS

3600-G WOODPARK BLVD. CHARLOTTE, NC 28206

I

6163 Lab Number: 99-A53487 Sample ID: SYSTEM INFLUENT Sample Type: Water 51 te ID:

Project: 109155-01

I Project Name: WARREN OIL Sampler: LRRY PHILLIPS

Date Collected: 4/14/99 Time Co 11 ec ted: 10: 50 Date Received: 4/15/99 Time Received: 8:30


Report Au an Dil Analgte Result Units liHlt liHlt Factor Date T!He Analyst lletllod

------------------------ ----------- ------- ------- ----------- ---------MORGANIC PARAHETERSM Benzene '180. ug/1 100. 1.0 100 4/18199 17:31 r.Gundi Toluene 4140 ug/1 100. 1.0 100 4118/99 17:31 F.Gundi Etbglbenzene 340. ug/1 100. 1.0 100 4118/99 17:31 F.Gundi Xylenes, total 5500 ug/1 100. 1.0 100 4118/99 17:31 r.Gundi nethyl-t-butylether 880. ug/1 100. 1.0 100 4118/99 17:31 r. Gundi

ND = Hot detected at the report liHlt.

Surrogate Z Recovery hrget Range

DTEX/GRD Surr. , a,a,a-trifluorotoluene 97. 50. - 150.

Report Approved By: Report Date: 4/22/99

Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Russell Morgan, Technical Services


602 602 602 602 602

Batch

9Bl 9131 9131 9131 9131

I SPECIALIZED ASSAYS, INC.

2960 Foster Creighton Dr. P.O. Box 40566


ANALYTICAL REPORT

I HANDEX OF THE CAROLINAS


6163 Lab Number: 99-A~3488

Sample ID: SYSTEM MIDFLUENT Sample Type: Water Site ID:

I Project: 10915~-01


Date Collected: 4/14/99 Time Collected: 10: 4~ Date Received: 4/15/99 Time Received: 8:30


Report Quan Oil Aulgte Result Units Llnit Lin it ractor Date Tine ARilyst Method ------------------------ ----------- ------- ------- ----------- ---------

MDRGAHIC PARAMETERSM Denzene 3. 3 ug/1 1.0 1.0 1 4118/99 18:04 r.Gundi Toluene 15.8 ug/1 1.0 1.0 1 4118/99 18:04 r.Gundi Ethylbenzene 1.8 ug/1 1.0 1.0 1 4/18199 18:04 r. Gundl Xylene•, total 27.3 ug/1 1.0 1.0 1 4/18/99 18:04 r.Gundi netbyl-t-butylether :i4.3 ug/1 1.0 1.0 1 4118199 18:04 r.Gundi

NO = Not detected at the report linit.

Surrogate X Recovery Target Range

BTEXIGRD Surr., a,a,•-trifluorotoluene 102. so. - 150.

Report Approved By: Report Date: 4/22/99

Theodore J. Duello. Ph.D., Lab Director Michael H. Dunn. M.S .• Technical Director Johnny A. Mitchell. Dir. Technical Services Eric Smith. Assistant Technical Director Russell Morgan. Technical Services

Laboratory Certification Humber: 387

r.nPY 1

602 602 602 602 602

Batch

9131 9131 9131 9131 9131

I I I






I Project: 10915:5-01


I AD>lyto Result

6163

Report Units Unit

------------------------ ----------- -------

I MUDLATIL£ DRGAIIICS bg GCM Benzene HO ug/1 1.0

I Ethyl benzene NO ug/1 1.0 Toluene ND ug/1 1.0 n,p-Xylenes MD ug/1 1.0 o-Xylene HD ug/1 1.0

I 1,2-Dichloroethane MD ug/1 1.0 nTDE 114. ug/1 1.0

I MnETALSl< Iron, Tohl 27.60 ng/1 0.0500 nang•nese, Total 116.0 ng/1 0.1500

I MniSCELLAHEDUS CHEftlSTRYM Total Suspended Solids lOA ng/1 1.0 Oil ' Grease 3.2 ng/1 1.0

I MD = Mot detected at the report linit.

I Surrog•t• r. Recovery

------------ ----------

I PID Surr., a,a,a-trifluorotoluene 97. Hall Surr., 2-chloropropane 86. Hall Surr. , cbloroprene 94.

I Hall Surr. , 1-cbloro-3-fluorobenzene 81.

I I I

ANALVTXCAL REPORT

Quan llnlt

1.0 1.0 1.0 1.0 1.0 1.0 1.0

0.0500 0.0150

1.0 1.0

Lab Number: 99-A53489 Sample ID: SYSTEM EFFLUENT Sample Type: Water 51 te ID:

Date Collected: 4/14/99 Time Collected: 10:40 Date Received: 4/1:5/99 Time Received: 8:30

Dil F>Ctor D>te Tlne An>lyst net hod

----- ----------- ---------

1 ~/17/99 23:21 T ncCollun 602 1 4/17/99 23:21 T ftcCollun 602 1 4/17/99 23:21 T ncCollun 602 1 4/17/99 23:21 T nctollun 602 1 4117199 23:21 T nctollun 602 1 4/17/99 23:21 T ftcCollun 601 1 4/17/99 23:21 T ncCollun 602

1 4/21199 6:59 C.Holnes 60100 10 4121199 6:59 C.Holnes 60100

1 4117199 12:00 L. fisher 160.2 1 4120199 10:30 L. Philpott 9070

hrget Range

------------

50. - 150. 49. - 123. 63. - 122. 59. - 117.

r.nPv'

Patch

2~76

2~76

2476 2476 2476 2476 2476

8764 8764

9271 1~00





PRO~ECT GUALITV CONTROL DATA

natrix Spike Recovery

ffnolyte units Orig. U•l. ns Ual Spike Cone Recovery Target Range Q.C. Batch

Benzene Benzene Toluene Toluene Etbglbenzene Ethylbenzene Xglenes, tohl Xylenes, total netbyl-t-butyletber nethyl-t-butylether Benzene Ethglbenzene Toluene n,p-Xylenes o-Xylene nroE Iron, Total nanganese, Total

Analyte

Iron, Total nanganese, Total

Ana1yte

Benzene Toluene Ethy1benzene Xylenes, total nethyl-t-butylether Oil & Grease Benzene Ethylbenzene Toluene n, p-Xylenes o-Xg1ene 1,2-Dicbloroetbane nTDE Iron, Total nanganese, Total

ng/1 < 0. 0010 ng/1 < o. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < D. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < o. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < 0. 0010 ng/1 < o. 0010 ng/1 0.6220 ng/1 < 0. 0150

natrix Spike Duplicate

0.018~

0.0222 0.0189 0.0228 0.0192 0.0212 0.0378 0.0~27

0.0199 0.0171 0.0207 0.0203 0.0206 0.0~7

0.0216 0.0209 1.610 0.5150

units Orig. Ual. Duplicate

ng/1 ng/1

Laboratory Control Data

1.610 0.5150

1.730 0.5200

units Knoun Ual. Analyzed Ua1

ny/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1 ng/1

0.0200 0.0200 0.0200 0.0400 0.0200

20.0 0.0200 0.0200 0.0200 0.0400 0.0200 0.0200 0.0200 0.8500 0.2440

0.0216 0.0221 0.0207 0.0411 0.0193

18.9 0.0209 0.0206 0.0208 0.0428 0.0222 0.0207 0.0202 0.8880 0.2540

0.0200 0.0200 0.0200 0.0200 0.0200 0.0200 0.0~

0.0400 0.0200 0.0200 0.0200 0.0200 0.0200 0.0~00

0.0200 0.0200 1.000 0.5000

92 111 94

1H 96

106 9~

107 100

86 104 102 103 107 108 104

99 103

59. - 138. 59. - 138. 59. - 135. 59. - 135. ~7. - 1~~

~- - 14~. 58. - 136. 58. - B6. 62. - 133. 62. - 133. 76. - 122. 76. - 125. 7~. - 127. 75. - 133. 7~. - 126. 67. - 130. 80 - 120 80 - 120

RPll Unit Q. C. Oatch

7.19 0.97

20 20

8764 87M

r. Recovery Target Range Q.C. Oatch

108 110 104 103 96 94

104 103 104 107 1l1 104 101 104 104

70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70- 130 70 - 130 80 - 120 80 - 120

9131 9131 9131 nl1 9131 1400 2476 2476 2~6

2476 2476 2476 2476 8764 8764

9131 9131 9Bl 9131 9B1 9131 9131 9131 9131 9131 2476 2~76

2476 2476 2476 2476 87M 876~




Nashville, TN 37204-0566 Phone t-615-726-0177


Duplicates

Analyte units Drig. Ual. Duplicate RPD Lin it Q.C. Batch -------------- -------- ------- -------- -------Total Suspended Solids ng/1 10.4 10.4 0.00 15. 9271 Total Suspended Solids ng/1 8700 8560 1.62 1S. 9271

Ohnk Data

Analyte Olank Ualue Units Q. C. Oatch -------------- ------------ -------- ---------Denzene ( 0.0010 ngll 9131 Toluene ( 0.0010 ng/1 9131 Ethyl benzene ( 0.0010 ng/1 9B1 Xylenes, total < 0.0010 ng/1 9131 nethgl-t-butglether ( 0.0010 ng/1 9B1 Iron, Total ( 0. 0500 ng/1 8764 nanganese, Total ( 0.0150 ngll 87M Total Suspended Solids ( 1.0 ng/1 9271 Total Suspended Solids ( 1.0 ng/1 9271 Oenzene ( 0.0010 ng/1 2476 Ethylbenzene ( 0.0010 ng/1 2476 Toluene ( 0.0010 ng/1 2476 n,p-Xylenes ( 0.0010 ng/1 2476 o-Xylene < 0. 0010 ng/1 2476 1,2-0ichloroethane < 0. 0010 ng/1 2476 ftTBE < 0. 0010 ng/1 2476

COPY1

" . ···- • SPECIAliZED ASSAYS pBVED APR 2 1 • 7A- 042718

I ENVIRONMENTAL \R['' ' ··-

REFERRING CLIENT 2960 Foster Creighton Drive

··--·--·- -- . ... . .

Nashville, TN 37204

Account: 6163 . .. 615-726-017.7, 8()0, 765-0980 .. ···-··· · .. Handex of the Carolinas FAX 6151726-3404

I Jeff Hollis 3600-G Woodpark Blvd. Charlotte, NC 28206 Ph: 704-598-7900 Fax: 704-598-2248 Specialized Assays: ( 800) 765-0980

lNG CONTROL NUMBER (FOR LAB USE ONLY) PROJECT • P.O. •

\_~z.~ /&<1/S'"'s--oJ ... !09J.')~-dJ

MPLz:naruh??' lorrv p},-//.{}J PROJECT NAME

~1.#1 (fl./ R LAB USE ONLY

v .. .. !\ ::E < ACC# SAMPLE DESCRIPTION DATE TIME 8 " • ANALYSIS REQUESTED

" • I -·--)~ _£, /L. 5'3qg-:}- lt-1~-7'1 Jo:qo -- a.. u;;.._ BT6)'_ /J1ri3r::.

ls-~·-U1'8 " v

f. cl:. n. /J/;r//AJ i-t-t4 ..q~ j(J:l{ij v 'J< k;;z J! r,s v /J?rlfL

15'1'-i~'t lj 6'11;... 15T&x/mri!£

);, j"-4,, 6_-1//. 4-t<t-19 Jo:'fo ~ ) ?rn I J.- 1?. Y:-fhrr; ..... -LL v TV

TSS' 67 r /I!' 0 -w<:J<- {' 6P tH,m); ~

lllm.. ('{'£/;. C.Z:cj,'J v

...

. .. .. ---

~·; fquiwdA{Ai Date I lime Received by: (Signature) tory by:

~~~q~~;~•D .J .. ~~ .~ l&~ telinquisfled bY: (SignatUre) Date 1 lime Received by: (Signature) "lterharb

~r I

inquishcd by: (Signature) Date I Tune Received by: (Signature) .. -··

.. . .. . . . I inquished by: (Signature) Date/nme Rec:eived by: (Signature) . .. ·.,;--.··· . ·-···-·

I SAl Project #:

I For further assistance in completing the chain of custody form please refer to the instructions found on the opposite sil

I I; <


I ·2960 Foster Cr~ighton Dr. P.O. Box 40566


I HAND EX OF THE CAROL I r.J.;;s

I 3600-G WOODPARf<. BL\lD. CHI',RLOTTE .• NC 2B206

I Pl'oject: 109155-01 Project Name: WARREN OIL I Sampler: LARRY PHILLIPS

Analyte Result

6163

Report Unit'3 LiHit I

I -----·------- -----------·· ----------- -------


>.VOLATILE ORGANICS oy GC>. r!N,zer:e HD Ug/1 1.0 Chlorob·~nre-IH~ rm !.!911 1.0 l:.tfiylb~::~zene Ni) IJ9/l 1.0 r o-l uent- ~D u.q/1 1.0

!1 1 p-Xi!l€'flt'S HD U9/l 1.0 I!· .. Xyl £-ill? I!D uq/1 1.0 1 ,2-P i'lftloroethane Nli ug!l 1.0 MTUE 113. IJ9/l 10.0

ii:METALS* Iron, Tot•l 6. 270 11911 0.0~00

11anganes~ 1 Total 5.760 Hg/] 0.0150

<MISCEU.AMEDUS CHEniSTRY> Tot:al SiJ"j~~nde4 "Solid·; 4.0 r.gll 1.1] Oil & Grease HO M9fl 0.9

HO = ~ot detected •t the report liHi t.

~----------·------------

Surrogate Z Recovery ------------- -··--------

PI() SJJrr. , ~,a,a-trifluorotolue-ne 9!. Hall :';orr.

1 2-(:l\lol'opropa:h~· ?8.

Hall Surr., ct.loroprene- 94.

Hall Surr. , 1-chloro-3-fluurobeiilf.fli' 73.

Quai, LiHit

1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0

0.0500 0.0150

1.0 0.9

REPORT

Lab Number: 99-A68100 Sample ID: SYSTEM EFFLUENT Sample Type: Water Site ID:

Date Collected: 5112/99 Time Collected: 17:30 Date Received: ':'J/13/99 Time f1eceived: 9:00

Dll f>ctor D>te TiH< An:;lgst nethod

-------- ----------- ---------

1 ~/1~/91 1~:40 n.H1He1lck 602 1 5/15/99 lq: 40 n. HiHelick 602/601 1 5/15/99 14:40 M.HiHelick 602 1 ~/l":J/99 14:40 n.HiHelick 602 1 ~/l!.i/99 14:40 M.HiHelick 602 1 o/1~199 1~:40 M. HiHelick 602 1 ol1ot99 1q:qo M. HiHeliok 601 10 ,,1,/99 1q: qo M. Hi.Heliok 602

1 5/14/99 16:21 M. !<arb 6010!< l 5/14/~9 16:21 n. Barb 601@

1 5/14/99 21:15 l. fi·;her 160.2 1 5/14n9 H42 l. Philpott 9070

Target Range -----··------

50. - 150. q9. - 12). 63. - 122. <n

"" - 117.

B>tch

7113 7113 i'lB 7113 7113 7113 7113 7113

5496 ~4%

6059 6093

("'f"\DV 1




Nashville, TN 37204-0566 Phone t-6t5-726-0177

ANALYTICAL REPORT

Report Approved By:

Laboratory Number: 99-A68100 Sample ID: SYSTEM EFFLUENT

Page 2

Report Date:

Theodore J. Duello. Ph.D., Lab Director Michael H. Dunn~ M.S. 1 Technical Director Johnny A. Mitcr.eJ.l, Dir. Tecr.nical Services Eric Smith. Assistant Technical Director Russell MorganJ Technical Services


:5!18/99

I SPECIALIZED ASSAYS, INC.

2960 Foster Creighton Dr. I P.O. Box 40566 ANALYTICAL REPORT Nashville, TN 37204-0566

Phone 1-615-726-0177

I I-JANDE X

I 3600-G

OF THE CAROLINAS

1-JOODPAR~. BL'v'D.

6163 Lab Number: 99-A68101 Sample ID: SYSTEM MIDFLUENT Sample Type: Hater

CH'"'RLOTTE.• NC 28206

I Pro.ject: 1091j:J-01 Project Name: WARREN OIL I Sampler: LARRY PHILLIPS

I ~nalgte Result Report

Uolts LlHJt -·----------------------- ----------- -------

I ~ORGANIC PARP.~ETER$•

[\i-itZH!£o HD ugll 1.0 T uluer1E- 3. 3 ll9/l 1.0 £Uylten:zt-i1£- MD ug/1 1. 0 X~1en.s, total :i.1 u~/l 1.0 I nethyl-t-butyletheJ ZOl. ll~/1 1.0

I ND = Hot detected 't th<· roport liHit.

--------·---

I :>urrogate I. f!ecovery

I tH(X/Gf:U Surr., a 1 :a,~-trifluorotoluene 111.

Site ID:

Date Collected: 5/12/99 Time Collected: 17:35 Date Received: 5/13/99 Time Received: 9:00

Ruar1 DH l!Hlt F<ctor Date TINe Analyst lfettflld

-------- ----------- ---------

1.0 1 ~11~199 4:14 D. RiiHey 602 1.0 .l ~/15/99 4:14 D. Ra<1ey 602 1.0 1 :i/15199 4:14 D. RaNey 602 1.0 1 ~11~199 4:14 D. RaNey 602 1.0 1 5/15/99 4:14 D.R,Heg 602

Target Range

50. - 150.

I Report Approved By: Report Da·te: 5/18/99

I I I I I I

Theodore J. Due11o, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director . .Johnny A. t"litchelL Dir. Technical Service~ Eric Smith. Assistant Technical Director Russell Morgan, Technical Services


r<atch

~7~1

5751 ':j751 ~7~1

5751

--·-----------···~ ... ,.. -..... . •••• I 1111•1 •••• •••• I 1111•1 •••• •••• I II 1•1. ••••

Ill' \i; I 1iii-::: •• • ......... ~ ,. 1 ••


2960 Foster Creighton Dr. ar ·••

•• , ·~-<":··~' ••• . ••

t~Y:.S:T~.: -~4f''_,;! P .0. Box 40566 Nashville, TN 37204·0566

Phone 1·615·726·0177

ANALYTICAL REPORT ,.L~.:.c;, ••• ;: ....... , ··--·--------

I Hl'INDEX OF THE CAROLINAS 6163

13600-G WODDPARK BLVD.

Lab Number: 99-A68102 sample ID: SYSTEM INFLUENT Sample Type: Water

CHARLOTTE.. NC 28206 Site ID:

I Pro.ject: 1091:5:5-01 Project Name: WARREN OIL

ISam~ler: LARRY PHILLIPS

Date Collected: 5/12/99 TimeCollected: 17:40 Date Received: :l/13/99 Time Received: 9:00


·--··----- Report 9Udfl Oil :;;,alytE- Result U;Jits LiHit llHJt F•ctor O<te TIHe Analyst net bod ··------------------· --· ---- ----------- ------- -------- ----------- ---------

:>:ORGANIC P~RAMETERS• 3enzene 87.8 U9/l 1.0 1.0 1 5/15/99 4:44 O.RaHeg foluenE- zno L!gil 100. 1.0 100 ~11~191 4:44 O.RaHeg Ethylt<enZ{'fli' :ta. 4 tlg/1 1.0 1.0 1 511'5119 4:44 O.RaHeg :<\~~len~s 1

tl}t:tl .!.·JI , iJj/l 1.0 l.U 1 :J/1~/VY ~:qq V.Raney ii~~til~l-~t- !wtyl>? ther l.~'i0 ugtl 100. 1. 0 100 :J/l:;tv1J 4:44 D. R•••Y

MD = P.ot detected at the r•port linit.

·---··---·------·-·--·-·------

?urrogate I. Recovery 1arget Rang<·

l1TEX/GRO surr. _, il ~ <~ J a-tr 1 Hu6rutoluE-I'!E" 10~. ":.iD. - l~iO.

Report Approved By: f(eport Date:

Theodore J. Duello. Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Russell Morq.an1 Technical Services


5!18/99

602 601 602 602 602

l<<tct,

5751 :i7:il ~{7~1

:Jj':Jl :11:11

I


···---------·-···~ •• lr" - •••••• •••• I II)..' 1.1 •••• •••• I II 1•1 •••• 18.1 I II t•IL•••• •••• L-. ·-----•••• .... \'!•• ·-· iF. ·~~{e .. ,;;:~~: !i! • prn;·,-:s ,, =~·~-~;~·,.:;): - L>,')~l ••:·-.• 1.;";..· ···~ •: ... . .... __ .......... ...





flH11:£ofl£'

f.enz~ne

folue-n~

l'ol•Je-m~

Eth9lbenz:en~

Ethylb~rllen•

Xglenes, tot>l Xylenes, tot~l

nett. gl-· t·- butylethor nethgl-t-but~lether

Benzene P.enzene Ethgl.benzen~

Etl'lyltt-nzel!f.o Tolue-r,e-Tulu£-nf.' H,p-~ylt-r.e-s

n .. p-X~Ie-r:e; n-Xylene o-·Xylene nmE MTF[ lffj(i' rotal Mangars!?'Sf' ~ Total

Iron~ lrkill Mnngan£•s.e} Tutal

A11alyt£o

Benzen~~

Toluene Ethylb:en~!?r1e

Xylent-:., total netttyl-t- biJt~l~tn~;-r

IHl & Gr~··~3:S~

!<H2'H1f'

nen:c:enft GhlorobeilzE-n'=' J::hlcrobJ;!rtz-en.:

units Orli. Val. ns va Splke cone Recovery Target Range Q. c. !<atch

lig/1

H~/1

t19ll Hg/1 "911 Hg/l rtg/l Hg/1

iig/1 Hj/l

t!~/l

t1g/l

H9ll. J·ig!l

li§ll

l1§il

ltg/1 ti~/1

I! gil Jig/1

t:g/1 Hg/1 rtg:'l

Hg/l

( 0.0010 < G.fJIJlQ { 0. 0010 { 0.0010 { 0. 0010 { 0.0010 ( 0.0010 { 0. 0010 { 0.0010 { 0. 0010 ( 0. 0010 { 0. 0010 ~ U.OOlO ( 0. 0010 ( 0. 0010 < G.tlfi!O ( 0. 0010 < U. 0010 < 0. 0010 < 0. 0010 { 0.0010 ( 0. 0010

0.1.810 ·: 0. 0150

o.ozoa O.OZ16 o.on3 0.0203 0.0214 0.0224 0.0392 0.0410 0.018V 0.0192 O.OlV~

0.0207 0.0190 0. 0103 0.0193 0.020~

o.oqoz 0.0423 0.0210 0.0216 0.0185 0.0209 1.070 o.qno

units Orlg. V~l. Puplicate

Hg/1 1. 070 1. 080 Hg/1 0. '1920 0.4860

Labontory ClJntrol [•:!ta

units Knuun Val. Analyzed Val

"9/1 0.0200 0.0214 H§/l 0. 0200 0. 0201 Hg/l r.g/1 ngll ngll ng/l ng/1 Hg/l

"911

0.0100 0.0400 0.0200

21J.O 00200 0.0200 o.ozoo 0.0200

0.0121

0.0404 0.0189

18.8 0.0204 0. 0117 0.01?6 0.0202

0.0200 0.0200 o.ozoo 0.0200 0.0200 0.0200 o.oqoo o.oqoo 0.0200 0.0200 o.ozoo 0.0200 0.0200 0.0100 0.0200 0.0200 o.oqoo 0.0400 0.0200 0.0200 0.0200 0.0200 1. 000 0.5000

104

lOS %

102

107 112 98

lOZ 94 n vs

10'1

95 102

96 102 100 106 .105 108 92

104 89

93

09. - 138. !i7jl ~9. - ll8. ~7::U.

59. - 13~. ~7~1

51. - 135. 5751 47. - 1qq_ ~7:i1

47. - 1'1'1. ~7~1

58. - 136. 57~1

~- - 136. 5751 62. - 133. 5751 62. - lB. 5751 76. - 1ZZ. 7113 1'6. - 1ZZ. 7113 76. - 125. 7113 76. - 12~. 7113

74. - 127. 7113

H - m. 7113 75. - 133. 7113 75. - 133. 7113 74. - 126. 7113 R - 126. 7113 67. - 130. 7113 6?. - 130. 7113 80 - 120 5496 80 - 120 ~496

RPD Unit g_ C. Batch

0.93 1. 23

20 20

~ Recovery Target Range A. C. !<atch

107 70 - 130 5751 100 7\1 - 130 5751 110

101 vq 94

102 98 98

101

70 - 130 70 - 130 70 - 130 70 - 130

70 - 130 70 - 130 70 - 130 70 - 130

~7~1

:i7:il

5751 6093 7113 7113 7113 7113


····--·----··-..... •• II"-•• laa• .... . ... ~·· .••. 1aa1 I II 1a1 1aa1 1aa1 I II lal.---·

===' ~.:_ :iii-::: II' ~& .. A~& ill " ~ ~ '"' I ,!':.?;·J'.~\1 ,. •Li:·c.:•i ,...., .. ·•' l .. ~'~':uZY •li•':.~l -----·-------·

SPECIALIZED .ASSAYS, INC.

2960 Foster Cre.ighton Dr. P.O. Box 40566

Nashville, TN 37204-0566 Phone 1·615·726-0177

PROJECT GUALITV CONTROL DATA

Arc;lyto

Etbylbenleoe £tliylbHIZE!li? Toluene

roJ.u~ne

!1,p-Xylenes H,p-Xylene<· (:~·Xylene

o-Xylene l. ,2-Dlchloroetbane

1,2-Dicbloroetbane

MH<E MH<E I1·on r TOt-ill 1'lan~:ane:'5e 1 lQt~l

flnalyte

:~malyt£-

-··---··---------·· HHJ:ZHI€'

Toluene £tt,ylb:£oilZ€'llf' Xyler,es 1 total netby1-t-butylether

Iron, Total l'!angilr1ese 1 ·rotill l'9hl Suspen~f~4 'Solid'S Benzene P.en2ene thlorobenzene Chlor·obenzl?n~

£thylbenzene EttoyHenzene Toluene ToluE-r,t-li ·' p-XylEr,es H) p-Y.yl£<r,es o-Xylene

v-XylHE-1 J2-Dlohlo.Nettsane 1 J 2-D i chlur<J['t t,ani'

L>bor•tory Control ~ata

vnlts V.noun Val. Analyzed U;l 'i. Recovery ---------- ------------ ----------

11gil 0.0200 0.0200 100 Hg/1 0.0200 0.0112 ,6 Hg/1 0.0200 0.0202 101

t<g/1 0.0200 0. OJS4 ,7

ng/1 0.0400 0. 0417 104 ng/1 0.0400 0.0404 101

ng/1 0.0200 0.0214 107

ngil 0.0200 0.0209 104 Hg/1 0.0200 0.0182 n ng/1 0.0200 0.0197 98 Hg/1 0.0200 U. 0171 % ttg/1 0.0200 0.0204 102 Hgll 0. 3350 U. ·1000 119 ng!l 0.2440 ll.Z>?O 97

t'IJplicate-·;;

units Orig. t13L Ouplicate RPO LiHit -----····-~~ ---------- ----------

119/l 11. u 11. D 0.00 l:i.

[llar1k Data

Blank Ualue lir:i ts. R. C. [<atct,

----------~- ----·----·· --~·------·-

{ 0.0010 Hg/1 ~751

( o. 0010 Hg!! :i7~1

·: 0. 0010 Hgll '57Jl ( 0.0010 Hgil ~7~1

( 0. 0010 Hg/1 ~l!il

( o. 0~00 Hgil '!it\96 ( 0.01~0 Ng/1 ~4%

\ 1.0 ng/1 6059 { 0. 0010 ng/1 7113

{ 0.0010 ng/l i'lB ( 0.0010 ngll i'lB < 0.0010 tlg/1 7113 < 0. OOlC H9.'l 7113 ( 0. 0010 Hg/l 7113 ( 0. 0010 ii9il 7113 { 0. 0010 H~/l 7113 ( 0.0010 Hgfl 7113 ( 0. 0010 ng/1 lll3 ( 0. 0010 Hyll 7113 ( 0. 0010 Hg/l 7113

( o. 0010 H9ll 7113 < 0. 0010 Hg/1 7113

,.._,...,, ..

Target Range Q. C. Batch

------------ ---------70- 130 7113 70 - 130 7113 70 - 130 7113 70- 130 7113 70 - 130 7113 70 - 130 7113

70 - 130 7113 70- BO ?lB 70 - 130 7113

70 - 130 7113 70 - 130 7113

70 - 130 7113 so - 120 5.!196 80 - 120 ~496

Q.C. oatch

----------6059




Nashville, TN 37204-0566 Phone 1-615-726·0177


6l>nk Dat~

Analyte Hl anN Villue Ulllts R. C. [fatch

--------------- ------------ --------- ----------MH<E ( 0.0010 H911 7113 nn<E ( 0.0010 •gli 7113

··-·-·.--.----··- .--··--:-·~-- .~ ·--.. ··--.-·~.--~ ·-· -· ·--.--- ------ ·-·- ---- ·- ·-- --~ ---.-- .


"""'NALVTICAL REPORT

I HANDE:< OF THE CP,ROLINAS 6163

wOODPARf~. BLVD. I 3600·-c; CHP..RLGl_··rr:::, NC C:820b

Lab Numtrer: 9~-A90627

S~mple ID: SYSTEM INF E;.::w.1p1.e Type: GPound water E;i te ID:

109511-01 Pr·o j ec t Nl::di1B: WP.FH~EN 0! L I Samp 1 er: ERIC DONNELLY

I I I I I I

0:1\1! :;.:·~(·~~\\~: ':!1~}.;!-r.-?·~' ~~·}t~l

net:h ~~, 1- ~ .. -l:>Jt~l-2\.:i~.;~~·

"5 ~.c,~rq,g3. i·t r~t-i~

n-=sult -----------

597. 2i'£ij

38~~.

nw li'BIJ 11il.

h~po!~t ~IJ.lll

JJni t:':i U"!t LhH.t

------·-

ug/1. lJJ.U 1. 1)

ugil :"if.LO ·;_ 0

Uy/1 lO.U 'i.!J l}y/1. :}1},1_1 .ll

1.!•1/J H!.!.! -· -']

Uf!IJ .,, .H.•. .L

100.

Datt.~ •:ollect:f:.~d: 6/.17/99 Tim2 Cu1lect.ed: 12: O~r Dat.P Ht·r.eived: Tiflli~' Rece1vej: 8: 3(")

t~a

f-lCt!Jr· Pate- li.riE- r,tialg·:;t n~tfhl,!

--·------· ------------ -----·----

10 6/lS/'911 21}:46 [• ~::n>:y 602 '5U ..... ~, ..... ~

.... ,:,, ( ? ~ ~:u: -~6 L' . r::t:ie~ £02

"10 (1/?5'/~r; *'FI· ""I .!.<.1."1.-. D. E:t:!'!-1 &U7 ?! ,. ···~'""f.'

~H ,: .• f? t 1.0: ·~6 ~- 1\<tr.>:-:~ 60? J..>j iJf.'i<:''Pi 2U::.\~ i:<. t~cttieiJ 602 _;;} {•/~7."//YY 20: 4[• i.l. ~Cl',f•y bf.l2

~!0. ·- 1~!!.

I Repor··t. Appr·o•ied By: #~ ___ _ Report Date: 71 1/9Y

I I I I I I

iheodor·e J. Duello, Ph. D. 1 Lab Director Mich-H~l H. l)unn~ ti. S., Te·:hnic::l OiPector .JahrHVJ ~~- tlitchelL Vir. Tecl\lilc.al. Services Er·ic 8mitr,~ Assistdilt- Tec;·,nical DJ.r·ectGr-

L~boratory Certificatiort Number: 387

P.JW<

:Hr.~-::

:m::. )JE~

~8::::;

:;:.~2.::

~ ~·.-··' -'\'1. ••

.-- .-·- ---·. ---- -;--· -- --.-.--.--- --- ---------~-.---.- ---.--.-~------ -- -----


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-72&-0177

ANALYTICAL REPORT

I t-!.'<NDE:<. GF THE CAROLINAS

WODDPAfi.:~~. BLVD. NG

hl63 Lab Number: 99-A90628 Sample ID: SYSTEM MID Samp l•?. Type: GT'uun(.l IJJat~r

~~~it•? ID:

I Pre j ec-::: .1 0'·?~.11-0.t Dat.e Coil ectecl: TitT•E Collect.ed:

6/17/99

12: 10 PT·Cjt-Ct I Saiiip 1 ~=·T·:

~-·laifd::•: t-Jt";f~REN DlL ERJC DONNELLY

I I .J. >j

L.(Hf€\\l:O B. 'l

I tt t:~] t,f.'~{Zf'1lt:· J. l p.:o ·,;~11n,:~-:;. ~~~1t:::l

:;;:.t ~;~}.-< <·•3t 1~.Li UH 142.

I :;_{)_

I I

!J1ll

IJ;l/1

vg/:J lJ~~/1

i..<~/1

,:~:,!/l

Date Rt-cei\.'£•0: T J. IT•E ReceiVE-d:

f:~pl}l't P.rnn vn U.ttH: lhlt r.a;;;ti}r (;1.1te

l.U .:...u -~- f./7.?/?? :n l.'S

l.IJ l.'J ~ £.l'Z'JI''t1 2J.:D 1. (l J..G J ~i/7'ffY'3 11:D l. il 1.n ,( ,......, 'f'Q

'-Jo' L.i-' ! r 21:10

' c• .. i,l. {./.('J/:~9 }1:}~_:

l .. ".t.. ' &/"'lS/:1? 21:1~

llo.

(_-_,_/ 18/9'7

D:30

f.'. F..:;i'i~ij. w:: r·. t~:n1·?~t Wl'

v. f:~iif. \.~ 6.i.i}

l:•.f.::c-!1.1?1! 6U2 ,, r: "i;i"ji··~~ 00:.:

i~. j::;:r;~¥ -6>32

I F:epor·t, ,;~pr·o•,-ed By: --7'/~------- Report Date: 7/ 1/99

I I I I I I

The,:Jdor;::- J. Duello1 Fh. D. 1 ldb Dtrector Michael H. Dunn~ M.S. s Teci\Hic.;l Direct.:::-r· Johnn~j A. Mitchell~ Oir. Technical Services E~ic Smith. Assistant lechnjcal Director Ru;;~.ell Mor-gan.' T£·chnica1 Ser·v:ir:e~~.

Laboratory Certific~tion Number: ~87

::;-;;:-_-;

-:::o~':i

::~r}:,

;;;·;---~

·~·:!'!'. .. _,,_ -·

:;J;·~'::

I



Hi~NDEX OF THE CAFrOLINAS 61C·3

I 3600-G "·'ODDPAR~'· BLVD. Cl~ARLOTTE, NC 282Qt,


P~oj2ct Name: WARREN ()fL ERIC DDNNEL.l.V

·-·---- ··- -------~------------·-···

•um;Hr.E PAF'!lM£T£R3'< ;.rn ~ ~:'"'~<~::+

::;:nzH·~

·. tJ::~J \}l::'ltL>!·::t

!C.ltltl/JP

•: , ~~--x ~:;, rfr!r.-!

•.: -x~~l·:n•: ~ .2.-D tl}iiYJr:;~t~.;orl~

1c:nnn.s~.

I NH! J 1-.:k.d :1ilfl~fiil!t·!'-t-, 1ct~l

,,

<itU::sr.t:LLH!itnlJ:S Gttf.11f:STRf:-i

630(!

tm w:· ;w !{\~

tl~·

ilii

' ?3ft '· T nu

)';.}td :s~;-;pJ?oo,1e•! ~t:>li~s ~~- 'l.

~lD S:U1'i'. il" ii .c-·hlflu:Jrc•tol:Jf'~it>

H~U :surr. , z--.;hlQrl);:r•Jp.:;r,e

~:;11 :~:urr. ! !}~l.t.f<'IIP"~lie-

1-J~H S;J':f"., 1"-,_-;i\l•}!':r ~-~'l,:orDfr,~il.Ie-rv:

;_;~/]

!J!/1 lj:;/1

~,_;~_!/}

\J~J/1

H:-~/l.

u~/1

ii!V1 li9/]

Ri·f~UT·t

Unit

no.

L

1. l l

l 1

0. U~tK~ 0. 01'50

l.U

GZ.

?&. 1}7.

ANALYTICAL REPORT

fH..i?-11

Ut!lt

91(!.

]

' • .!

l

0. U~{<O t!. til~!O

l.fJ

l_ab Number: 99-A90629 Sample ID: SYSTEM EFF Sample Typ2: GrDLllld uJatE!T· ~::itf.: :ED:

D-3te Coll2cte(!: b/17/99 Tune Collected: ~ .-.. . .. ""'

J. ~'!- .l·J

D:lt•? H•?Leivt?.:::: 6/18/9~'

TiiTH~- F~;;;o.:eiv•?•::::

Oil

l 6n~::'9'-l 1~: :.t, n. t:~;uttJPr. 9Dl'O

!"~l2f....-''-ltt ::: ,''J n.HI.i-i~l:;.:~: bG2 l 0.·"?.6,. '-:;-<~ -.. ~ . .; tj_ ;: il1~li...:;f.: 6lJ2 .,

fJ};-~/'"f'i 3: j~ 11. H!nt:1ld: i;r:;: ' -6/J;:JT·i 3: :-·~· n. :~u~ellcY. 6!!1 f./t~6/?';1 :~. ~;I) n. Hin~lh':k 602

f:.n6!'i'?-V ,. )/_. n. fhn~li·* &ul

1 6-nt./'J'J !0: 10 !'·· V.t·Ilt.-~ 6(:1f)t;

1 t./7.6/'l'i 10: Hl f:. Kellf·~ 6010[1

1 6/J.-::/~'f) 1},:15 l.. fishllr 160.2

::~;.1:<

(.•'1:.:1,

,_, .... ·-,,_

.-:~1•n

f,!-}il}

'''''i (>'1"1 ••

l.'"'';l.

K.i~;[,

;~:m~

BlBB

-------·---------------------

0. 122.


2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204·0566 Phone 1-615-726-0177 ANALYTICAL REPORT

i

' Laboratory Number: 99-A90629 Samp 1 I? !D: SYSTE~l EFF

Page 2

t\eport D.ate:

Theoctor-? J. Duellc.=.· Ph. 0 ... La:t• Dir·ect.nr Michael H. DU:"IHL• n. S .. • TEchnical Dil'ect.or dohTiil~l A. Mitche-!lL Dir·. Techn~tc:al Set·vic£-s. Eric Sffiith~ Assis~ant Technjcal Director Russell Morgan~ Technical Services

Laborator~! C~rtifi~~tion Number: 387

7/ lf91'

---_,- .~


1. I Nashville, TN 37204.0566

Phone 1-615-726-0177 ANALVTXCAL REPORT

I I HANDEX OF THE CAROLINAS

3600-G WOODPARK BLVD.

6163 Lab Number: 99-A108653 Sample ID: SYSTEM MIDFLUENT Sample Type: Water

I CHARLOTTE, NC 28206

Project: 109155-01

I Project Name: WARREN OIL Sampler: LARRY PHILLIPS

I Analyte Rtsult Units

--------------- ------- -----I •DRQl!!IC PARAIIETERS ..

[IPOZtM' HP Ug/l Toluent HP ugll Etbglbtnmnt HD Ug/1

hport lluan Llnlt Llnlt

1.0 1.0 1.0 1.0 1.0 1.0

51 te ID:

Date Collected: Time Collected: Date Received: Time Received:

Dll FilCtor Datt Tine

------

1 7/TJ/'19 7:39 1 71T51'1'J 7:39 1 7m/'17 7:~7

7/21199

7/22/99 9:00

Analyst netllod

--------- ----

D. Rantg 602 D. Raney 602 D.Ri11e¥ 602 I

I I I

X,tenes, tohl MD ugtl 1.0 1.0 1 7m/'17 7:~ O.Raneg 602

I I I I I I I

nttbgl-t-butylttbtr 164 .. ug/1 1.0 1.0 1 712'5199 7:39 D. Rantg

HD = Hot detecte4 at the report l!n!t.

hrget Ruga

OTEXIGR!l Surr., a,a,a-trifluorotoluene Ul. 50. - 150.

Report Approved Fy: Report Da·te:

Theodot'e J. Duello, Ph.D., Lab Dit'ectot' Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Set'vices Eric Smith, Assistan·t Technical Director Gail A Lage, Technical Services

Laboratory Cet'Uf'ication Number: 387

7/29/99

602

~.tea

r.iB r.iB r.iB 75B 9513


HAND EX OF


THE CAROLINAS


Project: 109155-01 Project Name: WARREN OIL Sampler: LARRY PHILLIPS

Aul9b! Re~ult

6163

Report Unl~ l!nlt

---------------- ----------- -------

l\llltAlllE llRGAHICS bg GC• l<t.>oze!ll> liD ug/1 1.0 Cblorobenzene MD ug/1 1.0 1,2-Dichlorobenzene MD ug/1 1.0 1,3-Dicblorobenz•r* liD ug/1 1.0 1, 4-Di cblorobeozene MD ug/1 1.0 Etb!Jlbenzellt liD ug/1 1.0 lolue~~t MD ug/1 1.0 ", p-X!Jlene• liD ug/1 1.0 o-X!Jlene liD ug/1 1.0 1,2-0ichloroeth~ne liD ug/1 1.0

Mlll:lALS• Iron 8.220 ng/1 0.0"..00 nangaM'3e 11.30 ng/1 0.0150

I!IIISCEllAMEOUS CII£IIISTKY• Total Suspended Solids ~.0 ng/1 1.0 Oil l GreHe 1.~ ng/1 0.9

liD = Hot detected 3t t!IP report llnlt.

SUrrog-ate r. Reco\terg ----------- ---------

PID Surr., a,-a;;rtrlfluorotoluene 96. Hill SUrr. , 2-etsloropropane 97.

Hall Surr. , cbloroprene 93. Hill Surr. , 1-ebloro-3-fluorobeozeoe 7:i.

ANALYTICAL REPORT

Lab Number: 99-A108654 Sample 10: SYSTEM EFFLUENT Sample Type: Water Site ID:

Date Collected: 7/21/99 Time Collected: Date Received: 7/22/99 Time Received: 9:00

Qu~n Oil Lin it r~ctar Dab! Tine Aaalr.;t ftetllod Batcb

-------- ------ --------

1.0 1 7124/'1'/ 3:11 n.Hinelick 602 77 1.0 1 71241'1'1 3:19 n. Hlnellck 602/601 77 1.0 1 71241'1'1 3:19 n.Hinellck 602/601 77 1.0 1 71241'1'1 3:19 n. Hlnellck 602/601 77 1.0 1 7124199 3:19 n.Hinellck 602/601 77 1.0 1 7124199 3:19 n. Hlnellck 602 77 1.0 1 7124199 3:19 n. Hlnellck 602 77 1.0 1 71241'1'1 3:19 n.Hinelick 602 77 1.0 1 712~1'1'1 3:19 n.Hinellck 602 77 1.0 1 71231'1'1 16:30 T ftoCollun 80216 2~6

0. 0"..00 1 71261'1'1 10:23 G. Robinson 60101! 7:i73 0.0150 1 71261'1'1 10:23 G.Rvb!MOn 60106 9:i73

1.0 1 71231'1'1 15:20 G. &aun 160.2 96<18 0.9 1 71261'1'1 12:~4 l.Pbllpott 9070 327

hrget Range -----------

50. - 150. 4'1. - 123. 63. - 122. S9. - 117.



2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1·615-726-0 177

Report Approved Sy:

ANALVTXCAL REPORT

Laboratory Number: 99-Al086~4

Sample ID: SYSTEM EFFLUENT

Page 2

Report Da'te:

Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services


7/29/99

~~-~~ SPECIALIZED ASSAYS, INC.

2960 Foster Creighton Dr. I··.·. ·r}l..} ... . .. •• ',.1 •• " ~ .•. I• .. ~:.r?.· .,. =~ 5.*f~ . ~= ····'·~···~""· . ____ .. _______ _

P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177

I PRO~ECT GUALITV CONTROL DATA


Aaalyb

!<e02eDt l~02ene

Toluene TolueAe Etbglbe02ene Etbglbennne XylentS, total XglentS, total llttbgl-t-bt.ltgletbe~

llttbgl-t-butglotbt~

!<enze&e Ethylbtnzene Toluooe H ,p-Xy1ene-; o-Xylene

A .. Igto

I roo nangall!'so

Aoalyto

[~OZtM'

TolUODt Etbglbt02one Xg1elll!', tot~1 netby1-t-butyletber Oil & Gre~se l<ennne Cblorobenzeoe 1,2-Dicblorobtnzeae 1,~0lcblorobtnzene

1,4-Dicblorobenzeoe Etbglbenzene Toluene n,p-Xglenes o-Xglene 1,2-0icbloroetb~ne

I roo nangall!'se

ft~trix Spike Recovery

units D~ I g. Val.

ngll < 0. 0010 ngll < 0. 0010 ngll < 0. 0010 ngll < 0. 0010 ngll < 0. 0010 Hg/1 ( 0. 0010 Hg/1 ( 0. 0010 Hg/1 ( 0. 0010 ngll < 0. 0010 ngll < 0. 0010 Hg/1 ( 0.0010 Hg/1 ( 0.0010 Hg/1 ( 0. 0010 Hg/1 ( 0. 0010 Hg/1 ( 0.0010

natrlx Spike Duplicate

ns Val

0.0171 0.0179 0.0170 0.0181 0.0184 0.01?4 0.0343 0.0362 0.0173 0.0182 0.0202 o.om 0.0200 0.0404 0.0202

ualts Uri g. Val. Duplicate

Hf/1 Hg/1

7.080 7.170 U.60 U.70

Spike Cone

0.0200 0.0200 0.0200 0.0200 0.0200 0.0200 0. 0400 0. 0400 0. 0200 0.0200 0.0200 0.0200 0.0200 0.0400 0.0200

KtCOYtry hrgtt Rangt a. C. llatcb

U 51. - 138. r.iB 70 ~7. - 138. r.iB ~ ~7. - 13~. 7~3

70 ~7. - 1~. r.iB 72 47. - 144. r-.. 13 77 47. - 144. 7~13

u ~. - 136. 7""..13 70 ~. - 136. r.iB u 62. - m. 7""..13 71 62. - 133. r.i13

101 76. - 122. 77 78 76. - 125. 77

100 74. - 127. 77 101 75. - 133. 77 101 74. - 126. 77

RPD Llnit u. c. htch

1.20 20 9573 o.u 20 r.i73

uolts KBOIID Val. Aoalgzod Val 1. RtcOUl!ry hrgot Rugo a. C. Oatcb

ngll Hf/1 Hg/1 Hg/1 Hg/1 Hg/1 ngll ngll Hg/1 Hg/1 Hg/1 Hg/1 Hg/1 Hg/1 Hg/1 Hg/1 Hg/1 ngll

0.0200 0.0200 0.0200 0.0400 0.0200

20.0 0.0200 0.0200 0.0200 0.0200 0.0200 0. 0200 0.0200 0.0400 0.0200 0.0200 0.4330 0. 2440

0.0178 0.0180 0.01?2 0.036:1 0.0182

17.4 0.0176 0.0217 0.0177 0.0178 0.0201 0.0171 0.0174 0.0373 0. 0173 0.0177 0.4640 0.2540

89 70 76 n n 77 78

108 100

" 100 96 77 78 76

100 107 104

70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70- 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 80 - 120 80 - 120

r.iB r.i13 vm r.;u 7m

327 77 77 77 77 77 77 77 77 77

2646 7573 r.i73



PROJECT GUALXTV CONTROL DATA

~pllcatei

Rolllgte unlh Drlg. Ual. ~plicate 1!1'1) Llnit &.C. Sitch

---------- ------- ------ ---- ------Total SuspeDded Solid~ ng/1 1.6 9.2 4.26 1~. 7648 Total Suspended iOlld~ ngll 7.6 6.8 11.11 15. 7648

Blink Dati

Rnal9te BhRk Value Unit<; Q.C. ht:ch

-------- --------- ------ ------nnu~~e ( 0.0010 ng/1 9'".113 Tolue~~e < D. 0010 ng/1 ~13

Etbglbeozene ( 0. 0010 ng/1 ~13

Xgle~, total ( 0.0010 ng/1 ~13

l!etbgl-t-butyletber ( 0. 0010 Hg/1 ~13

Iron < o. o:roo "'11 ~B

nangaaeu < 0.01:50 "fll 7:\B Total ~U'ipen4ed ~olld~ < 1.0 "fll 7648 Total Su<ipended Solidi { 1.0 "fll 7648 llenzeae < 0.0010 "fll 77 Cblorobean~~e ( 0.0010 ng/1 77 1,2~icblorobeDZeae ( 0.0010 ng/1 77 1,3~lcblorobeDZeae ( 0. 0010 ng/1 77 1,~icblorobenzeae ( 0.0010 ngll 77 EtbylbeDZeM ( 0. 0010 ng/1 77 Tolue~~e ( 0.0010 ngll 77 n,p-Xgltnes ( 0.0010 ng/1 77 o-Xyltne ( 0. 0010 n~/1 77 1,2~lcbloroetbane ( 0. 0010 H9/l 2646

1 ..

... I

. . ~

I

I I

SPECIAUZED ASSAYS ENVIRONMENTAL

Account:_6163 Handex of.the Carolinas Jeff Holl ' 3600-G Charl·

.................. i.;:'

. 7A· 042}26

2960 Foster Creighton Drive Nashville, TN 37204 615·72~177, 8~765~80

FAX 615/726-3404

"765:-0980

ANALYSIS REQUESTED

to JJT~ .I?IT/J/5 ; ~ ~--JJ/c)Jarle+J,.j_

I·

SAl Project #:

I For further assistance in completing the chain of custody form please refer to the instructions found on the opposite si1




6163 Lab Number: 99-Al086~2

Sample ID: SYSTEM INFLUENT Sample Type: Water 51 te ID:

I Project: 109155-01

Date Collected: 7/21/99 Time Collected:

I Project Name: WARREN OIL Sampler: LARRY PHILLIPS

Date Received: 7/22/99 Time Received: 9:00

I Report Quu Dll Aaalgte Re~ult Unit~ Llnlt Llnlt factor Date TlHe Rnll~t netood ------------ ----------- ------- ------- -------- -------

I I I I

IEIIRGIIHlC PARIIIIElERS• [teazene 527. Toluene 1986 £thylll0ozene '!<l8. Xylene', total 1580 ftetbgl-t-butylether 1926

MD= Hot 6etected at the report llHit.

ugll 10.0 ug/1 10.0 ug/1 . 10.0 ugll 10.0 ug/1 10.0

i( Recovery

1.0 10 712"'-m 7:11 D. Ra11ey 1.0 10 7125/99 7:11 D.Raney 1.0 10 712:!1'19 7:11 D.Raney 1.0 10 1/'J."'.s/99 7:11 D. Raney 1.0 10 7125199 7:11 D.Raney

hrget Ruge

I t«TEX/01!11 Surr., •,a,a-trlfluorotoluene 85. 50. - 150.

I Report Approved I«y: , f21o / R. Cl.L71'cw , Report Date: 712'11'1'1

I I I I I I

Theodore J. Duello. Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell. Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services


602 602 602 602 602

Batch

9513 9513 9513 r .. .u 9513




I Hf">r-lDEX OF THE GAf~CJL I NAS

I :360-::J--G WODDFARK 1ll.VD. CHARLOTTE, NC 28206

I Pf'o.ject: 109155-01 ProJect Name: WARREN OIL

1 Sampler: LARRY PHILLIPS

6!63

ANALYTICAL REPORT

Lab Number: 99-Al30967 Sample ID: SYSTEM EFFLUENT Sample Type: Water Site ID:

Date C a 11 e c ted : Time C•Jllected: Date Received: Time Received:

8/26/99

9:00

------------------------------------------------Report Duan Oil AnalytE- Result Ur.Jts lJHlt Unit factor D•te TlHe Analyst net hod £tatch ------------------------ ----------- ------- --·------ ----------- ---------I >.IJOLATILE OR&AMICS by &C~ i:tHZE"f:E' MD ug/1 1.0 1.0 1 11 1179 7.i:q6 n. Hlnellck 601 ~67.i0

Ethyl~enzene MD 09/1 1.0 1.0 1 11 1191 S:46 n. Hinelick 602 S6!j0 I TolUflf1E' MD ug/1 1.0 1.0 1 11 1119 ~:46 n.Hinelick 602 56.!j[i !'I, p-Xylenes. MD ug/1 1.0 1.0 1 9/ 1/91 '5:46 n.H!ne1!ck 602 5650 •J-Xylen~ !!0 ug/1 1.0 1.0 1 91 l/99 ~:~6 n.HiHdick 602 5650 I 1,2-D i-:;lllnroetn~ne i!D lJ~/1 1.0 1.0 1 9! 1199 5:-16 M.HiHeliCi( 601 5650

I ;;nETALS>. tf'ilfl 6. :.il'G Hjll 0.0~00 0.0~00 1 S/ll/99 7:08 R. Kelle~ 6010£1 ! 33~~

L'2dli D.OO> ng/l 0.003 0.003 1 91 2/99 8:~8 R. Kelley 3030c ~978

li'HtQilrJ~Sf?' 4. 3BO Hg/l 0.0150 0.0150 1 8131/9'1 7:08 R. Kelley 6010!1 3355 I •MISC[lLAM<DUS CHEMISTRY> fot~l SSJsjien~ied Solid'S 2.0 Nq/1 1.0 1.0 1 8/27/99 19:~5 A. Gr~e-r 160.2 4070 Dil f.: Grease HD Hgil 0.8 o.n 1 8/30/99 7:03 L. Philpott 9070 4677 I MD = Hot detected at He report liHit.

·-~·-------I I

:;:urro9ate Z Recovery Target Range -------·-----~- ---------- ----··--·--·---

I'ID Surr. , a, • .• •-tr i fluorotoluer,e 99. ~0. - 1~0.

Hi!ll ~urr., 2-cbloropropilrst- 77. 49. -123. ;;,n :::urr. } ctduru~•l'tHiE- 83. ~3. - 111. I Hall Sun•., 1-ctlloro-3-flllO'robHll?i!i' 3~. J9. - 117.

I I I I COPY 1

I


···---··------•• ~~ .. ·• •r -: .. •••• 1111 I :11 ill 1111 •••1 I 1111•1.---• .... .._. ·------::,· ·~•::~~'!=r ·;j .. ···:·;....,., , .. . , ) .•. r~~ ::~~ ~·;~1 .I r~·~ ·)~j .•.. ...:~' •••.:·":..' .... __ ... _______ _




ANALYTICAL REPORT

Laboratory Number: 99-A130967 Sample ID: SYSTEM EFFLUENT

Page 2

Report Approved By:~·-~- Report Da·te: 9i 2i99

Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director .Johnny A. Mitchell. Dir. Technical Services Eric s,nith, Assistant Technical Director Gail A L•ge, Technical Services


COPY 1




ANALYTICAL REPORT

I ~iANDEX OF THE CAROLINAS

I 3600-•:;; WOODPARK I:JL'•/D.

CHARLOTTE, NC 28206

6163 Lab Number: 99-Al30968 Sample ID: SYSTEM INFLUENT Sample Type: Water Site ID:

I Pr-oje•:t: 109155-01 Pr-oJect Name: WARREN OIL


Date Time Date Time

Collected: Collected: Received: Received:


R~pnrt Ouan Oil An ill ytf' R~sult Unit; lJHit lJHit Factor Date TiNe

.. , ----------------------··- ----··------ ------- --------•DRSAHIC P~RAnETERS• h He-nzer,i' 600. ugfl !10 91 1111 10:42 TtJlUHIE.- Zl~O ugll ~0. 0 1. 0 ~0 91 1111 10:42 Ethylbenzent> sso. ugll ~0.0 1.0 ~0 91 1199 10:42 >:ylenes. > total zaoo ugfl ~0.0 1.0 ~0 91 1/19 10:42 n•tt.yl-t-~utylether 1300 ugll ~0.0 1.0 ~0 91 2/99 10:42

tm ~ ~ot deb:tJt~d i!t tb~? ~·eport Htd.t.

hrgot Range

11J7. 50. - 150.

F:epor·t Date:

Theodore J. Duello. Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director .Johnn•J A. !Htchell. Dir. Technic<ll Services Ertc Smith, Assistant Technical Director· Gail A Lage, Technical Services

Labora·tory Certification Number: 387

COPY1

8/26/99 9:00

Analy;t net hod

----------- ---------

Dur,can 1 J. 602 Duncan~ J. 602 Duncan~ J. 602 Duncan_, J. 602 Duncan) J. 601

'II 2/99

l<atch

662~

661~

0625 661~

662~



Nashville, TN 37204-0566 Phone 1·615-726·0177

ANALYTICAL REPORT

OF THE CAF.:OLINAS

I 3600-G WOODPARK ll!-VD. CHARLOTTE, NC 28206

I Project: 109155-01 Project Name: WARREN OIL


Lab Number: 99-Al30969 Sample ID: SYSTEM MIDFLVENT Sample Type: Water Site ID:

Date Collected: Time CollectE>d: Date Rec., 1 VE>d: Time Received:

8/26/99 9:00

-----------------R.-p-o-rt---Q-u-an-----D-!1-------------------------------------


ilnalyl:e Result Units LiHit Llnit factor Date Title Analyst

[~il'nz:ene-

1'oVJ~lll?

£thgl he!IZ:ene x~.jl€!fi~J I tot~l !'1ethyl-t-b1Jt~lether

~D ug/1 1.0 •Jg/1

"'' IJ~J/l

J.il ug/1 111. U~j/1

1.0 1.0 l u 2/99 11:09 Dunc~n, J. 1.0 1.0 1 9/ Z/99 11:09 Duncan, J. 1.0 1.0 :l 91 2/V9 11:09 Vuncan, J. 1.0 1.0 1 9/ 2/99 11:09 Puncu, J. 1.0 1.0 1 9/ 2/99 11:09 Puncan, J.

:10 ~ Hot dett·cted at thr report linit.

;~ Recovery

LfrEX/b"RiJ surr., dJnf~·tl•jflLtorotoluene 111. '50. - 1~0.

Report Approved By: ~--~-- Report Date:

Theodore J. Duello, Ph.D.~ Lab Director Michael H. Dunn, M.S., Technical Director ,Johnny A. MitchelL Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services


COPY1

9/ 2/99

net hod Catch

602 6625 602 6625 602 6625 602 6625 602 6625


Aifi!lyt£-





n:~trix :Spike ReJ;;QI,'l?f'l

units Uri g. Ual. ns Val Spik~ Cone Recovery Target Range A. C. [latch

--------------- -----·----- --------- ---------- --------- ------------ ----------llHZ£-nf' lty/1 ( 0.0010 0.0180 0.0200 10 :!9. " 138. MT.i 1oluene llg/1 ( 0. 0010 0.0180 0.0200 90 ~9. " 13:i. 662~

Ethylbenzene Hg/1 ( 0. 0010 0.0180 0.07.00 90 '17. " 1q4, 662~

Xyler.es., total Hg/1 ( 0.0010 0.0180 0.0200 90 '!i8. " 136. 662~

n.t hyl·-t-but y1et her Hg/1 ( 0. 0010 0.0200 0.0200 100 62. " 133. 662:i

Henzene 11911 ( 0. 0010 0.0219 0.0200 110 76. "122. ~6~0

Ethylbenzene 11911 ( 0. 0010 0.0213 0.0200 109 76. - ll:i. 56~0

To-lU£<1ie Hg/1 ( 0.0010 0.0211 0.0200 110 74. " 127. :,i6!i0

", p-Xyleroes. ugll ( 0. 0010 0.0413 0.0400 104 n. " 133. ~o:;o

o .. Xylene ligil < D. 0010 0.0224 0.0200 112 7q, " 126. ~6'50

Irur, 11911 0.1~00 1.040 l. 000 39 80 " 120 33~!i

i'tilfiQ'ilfl£-5f' Hgll 0.0.130 0.4720 0. ~.000 n 30 " 120 33'55

!'!1tril Spike V'JPli~::~te

t"!i!dl~t€' units. !Jrig. IJdl. Duplicate RPP liHi t R. C. [latch ··-------------- -•H---~·--·-- ---------- ---------- ----------Jr<Hl "9/1 1. 040 1. 070 1.84 20 3.3!i5 rlilngane-se ug/1 0.4720 0.4~70 3.23 20 33~!i

L4!>ontor~~ Control Dilta

An>l!tte unlts. Knoun Va:l. Anal~zed Ual l. Recovery Target Range Q.C. [latch ·~-------------- ---------- ------------ ~--------- ------------ ---------[lt>illt'DE' 119/l 0.0200 0.0180 ~0 70 " 130 662~

Toluene rtg/1 0.0200 0.0180 90 70 "130 6625 Ethyl benzene rtg/1 0.0200 0.0180 90 70 " 130 6625 X9lene;, total Hg/1 0. O:!OO 0.0180 90 70- BO 6625 Mett.yl-t-butylether rtgil 0.0200 0. 0170 9~ 70" 130 662~

!Jil t Gr()as.e "9/1 20.0 13.8 94 70" 130 4677 [ie-nzene ng/1 0.0200 0.02H 107 70 " 130 ~6!i0

f.thylbenzefl.e rtg/1 0.0200 O.OZB lOb 70 " 130 56~0

ToliJene rtg/1 0.0200 0.021q 107 70- BO S65U n ,p-:<ylenes ng/1 0.0400 0.0410 102 70 " 130 5650 o-X~len£- rtg/1 0.0100 0.0122 111 70 "130 5650 1 i 2·~(} ichloroett.urre rtg/1 0.0200 0.0203 .101 70 " 130 56!i0 Iron Hg/1 o.mo 0. 3180 95 80 " .120 3355 nangunes.e llg/1 0.2440 0.2370 97 00 " 120 33'5'5

Duplic1te;

~HI<1!9tt:: 'Jni.ts Uri9. V•l. Duplicat• R!'D Unit G. C. B•tcb

----·----------- -·--------- ---------- ---------- ---------Total :lu;peoded Solid; Hg/1 ':15.0 no 2.13 l!i. 4070 Total Su;pended Solids. llg/1 !i3Z. '534. 0.38 15. 4070

COPY1




Nashville, TN 37204·0566 Phone 1-615-726·0177


tHank D~t~

Analyt~ [{1 anJ.: !Jalu~:~ llnlts Q. C. [<atch ··-------------·· ------------ --------- ----------Iie-nzenf' ·: 0. 0010 ng/1 662"5 Toluene < 0. 0010 ngtl 661~

Ethylbenzene < 0. 0010 t19/l 662~

Xylene., total < 0.0010 Hg/1 662~

Methyl-t-butylether ( 0. 0010 rtgfl 061~

I run ( 0.0~00 ng/1 33!i~

Manganese ( 0.01~0 ng/l 3355 Tot•l Susvended Sollds ( 1.0 J1gl1 4070 Total Suspended Solids ( 1. 0 119/l 4070 ller,zenf' ( 0.0010 rtg/1 !i~SO

Ethylbenzene ( 0. 0010 Hg/l ":J6!i0

Toluene ( 0. 0010 rtgil 5650 rt, p-Xylenes ( 0. 0010 rtg/1 5650 o-Xylene ( 0.0010 11g/l 5650 1 )-DictJlon~ethrme- ( 0. 0010 ngll 5650

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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANAL "•r'T I CAL REPORT

HAf·JDE!< OF THE: CAEUL IN/~~; Lab Numoer·: ~9-A1469l4

s.-.-~mple ID: :U·-JF t3ar:rple "f~~pf:: H·-~t:er

SitE: JU:

.to·;:-; 155--.. (;: 1

Name: WARREr~ OIL EH l C Di.Jf•.iNELL. Y

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'i6. .on. ·· 150.

lttese 1·esults relate only to the items tested. 1his repo~t shall 1~ot be reprodu~ed e~ce?t i11 full and with permission of ·the lciboratory.

Report App1·ov~d By:

T:-H?odor·E· ,.J_ G-t:€-.tlo .. Ph. D., Lr.t-. Directo)' Mit:hi1t:1 H. fJur:.n .. n. S' .. · 'Tec;f,nic,:~.l Dirf~r.::tcr:·

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Lab Numbe~: 99-Al46915 Sample ID: MID Se.mf.Jl ~:: Type: t,.J.at.:~·'f'

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2:i17 r. r.-::.1:•.1!. 607. 4"~3

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These results ~·~late only to the items tested. Thi~11 report -st":.c~ll r1:ot be r·e-pr·cduced except in full t"Hid with permissi.on of the l.abarator4.

Report Date: JOr 4199

f~eodiJfe ~1. [)t;ello, Ph.D. • Lab Directa~·

Micll~el tt. Dunn, M.S. 1 l·ecll!liCJl Director ~Johnf~t.; ;-:!. rlitch·~lL· !Ji.r•. T~chni~~.al ServU>::·~

El~i~: Sm:i..f',h, A:asist.·lnt Te-chri.i·:,ll Oirectol' Gail A L~ge, Technicdl Se~·vlcas




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2960 Foster Creighton Dr. P. 0. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 Af'-IAI_ VT I CAL REPORT

Laboratory Numter: 79-A146916 Sample; ID: EFT

Page:.· 2

These J'~sult~ ~ala1:e o~l:~ t.o the it.ems ·tested. T!'d.s r-epor·t. s~ .. :-dl Hnt. ht~ r·epr-oQ;.jcf.·i.l ex·.:.ept :t·r~ Pull e<r;tl l.i•J th pe-rmission of ·UtE :.-~!)!f:0·~.cn·tJ.

R8port App~'iJved By:

Tftf:·r.,dort~ J. DuE.O:ilD.· P'tl. D .. • lab Cir~·-:t.oi'

!"!iCf!dE:·l H. DUi'i'il.· n. S. I Technical D:i.T'I~Ct.c:r

doT;f!ltY f.':. Mit.chEJ}) Oi'5'. Techr~ic:cd Sr:l'"Vi.c•~s

F..:ri~: ;_i:ldt.t;. A~·!:.~s.t;nl't Tettn1i(fjJ. D~r·i::·C"t.-.::·:·

,...nov.,

loo. - 6 Feb 2017 14:55

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