()JG7084

STL ST. LOUIS

STLSLLooks

13715 Rider TmVl North,Earthi ClIty, MO 63045

Tu:314 298 8566 F&X: 314 296 8157wwwjim.com

ANALYTICAL REPORT

PROJECT AD. 200-LU-1/LW-2

F03-D25

Lot #;FSL05BDG #.Q W 3SB

Steve Trent

Fluor Ran ord TncNB3M AO-21

P0O BOX 1000Richland, Wk 99352

110T2 7 2005

summ ~ ~ Ma -OA~~s m EDMC

PxOject Manager I

April1 19, 2005

Wavm TodS Laboubrim Inc.

LOT ffY3lbz W04380B 1 of 13

STL ST. LOUIS

Case NarotveLOT NUMBER: F5060257

SbG W043809

This report contains the analytcal results for the sample received at 5Th-St. Louis on 3/15/O5.This sample is associated with your P03-025 SAP.

The analytical results included in this report meet oil applicable quality control procedurerequirements except as noted belo.

The test results in this report meet all NELAP requirements for parameters in whichaccreditations are held by 5TL St. Louis. Any exceptions to NELAP requirements are noted inthe case narrative. The case narrative is on integral port of this report.

All chemical analysis results are based upon sample as received, wet weight, unless notedotherwise.

Ref erence the chain of custody and condition upon receipt report for any variations on receipt

conditions and temperature of samples on receipt.

TCLP non-volatiles preparation requires 100 grams of sample. There was insuff icient sampleprovided to perf orm analysis at the method specified amount. A reduced sample amount wasused.

The samples hod to be re-prepped. The MS/MSD vw created after sample preservation.

LOT # F5C160257 W04380B 2 of 13

STL ST. LOUIS

SAMPLE SUAMMY

VSCIG0257

SAMPLED SAMPNO.. # AMPLE# CLIENT SA14PLE ID DATE TIME

G6CPV 001 B191r1 08/18/04 08;58

- '1W X"ylc regilSo Of ft~6 hMIM d *0ow ue pnwoWe on 8w 1010wkt4 pqs.- AN =wiwhadoes we perfoand bosr, rouito a vold mod-off won In cak.w noub.

* Paw) midn.ND - mawdd damealors *m de uad lai

*f ThMuoni n- -o be nprod*. aoMp in ul.wkbool die we~i apreid In i labomry.

- Uniis for die fbDow4q porwinrs ars ovo apren a dry weiW buic calam, couvft. dw*y. fradtmoh. lgrztwkfy. layu odor.

-ao fibw on. pH. pocelty pmwae. tescdvky. miMx pctb. idll guvky, qow -H sie asbfy. mV-etf. vio-ky. ad ug

LOT # F5C160257 W04380B 3 of 13

STL ST. LOUTS

MODS SUMMAR"Y

FSC160257

ANALYTICAL PREPARATIONPARMETER METHOD METHOD

Mercury in Liquid Waste (Manual Cold-Vapor) SW846 747QA SW846 1311/7470

References:

sNw46 "Test Methodse for Evaluating solid waste, Physical/ChemicalMethods", Third Edition, November 1986 and its update.

LOT # FSC160257 W04380B 4. of 13

STL ST. LOUISI I

M5160267 CLIENT ANALYSIS SUMMARY Storausloc: 6127

Project Manager MAW Quote #: 58392 SOG: W04380BDaeRc d: 20-31

Prjet 00LW1/W- F3-=Analytcal Due Dale: 2005-04-14

Pot. MRC-SB6B-A-1 9981 Report to: Steve TrentReotDeae; 20040

Clent: 108302 FLUOR HAFR IC Report Type: 8 Standardi Report#SMPS in LOT: 1 EOD Code: FEADI

IJISAIMPLESAR9 HIGH WD-take proper pruuuilonaill Batch Hantordasmpes by thelnah oeanvresult ormebtur.

Anin: CCVIOGU flils 41-1014 Ardomftisat CROL sandard required +1-25% pH needs to he dons within 24 wtos ofrbmeipt

INA-tibutyl phosphate and phenol are tniytargot WTPH nodstololude Keo asedlesealrevueRepsstw1lOZ all raw data to reporting group

SAMPLE# CLIENT SAMPLE [D0it IDgf C1knLMWk DATE/TME SAMPLED WQBKORQER AI B1GIFI 2004-08-18/1858 GSCPV SOLIDSAMPLE COMMENTS:

MGl 08' 8w8461 7470A Mane) (7470A Col VAp*r)- ON TCLPI1 311) -uMETALS,TOTAL. 01 STANDAtD TESTSET PROT:A WRK 08Liquid (Method amdutee) LOG

L) HG 08 Sw~ 7470A Faruiy (740 Cold Vapo)- OMd TCLP(1 311) - METALS, TOTAL. 01 STANDARD)TEST SET PROT: A WVRK 06Liquid (Method e9odudu) LOG

S HG 08 SW646 7470A Mercury (7470A. Cold Vapor) - CM TCLP(13l I) -' METALS. TOTAL 01 STANDARD TEST SET PROT: A WRK 06Liquid (Method excluive) LOG

STL -SL Louls Logged In by: CLARKEJ 200"43-16 13:19:18 pintodon: Wednesay,Mact1B,200CZI9 PageoIof I

LOT # F5C160257 W043BOB S of 13

STL ST. LOUIS

.4'- ON

Eli

vp0

_ _ W.__ _

__d M._ 0____ ___

iI Y

We w oLu~

11V. 0.-o ..

0.0 z g

: A

?5 z z I

cca

LOT # FSC160257 W04380B 6 of 13

~STL ST. LOUIS -

IFi

41

iE

zz

-1

E a.IJ .I IL l~6

LOT T51602i W4i80 7jf 1

STL ST. LOUIS

S TL Lot No: F~(o'

Condition Upon Receipt FqrmSt. Lois Laboratory

Client: F/''Date 4~ rrun- 1e:_ _ _ _ _ _

Quote No: Initiated by:

Shipper/No. COCIRPA Numbers:F 3 -ocq

Con dition/ Variance (Cirde "Y- for yes," N" for no and "N/A" for not applicable):

1. 1 N Sample received in undamaged condition? 7. K Sampl- received with Chain or Custoy?

I.Y Sample received within 4-C * 2-Cb 8 S. N Chain fCut d atc m pl, n~ on otainers?

Record 9. Y N N/A Custody seal received intact on cooljer.?

3. Y W) Sample received with proper pH'? 10IYC ,-I Custody seal tamtper y-Weot ocooler.?

4. Y N If N/A - Was pH1 ces by original STL lab? .11. Y Nf~k Custody ala on bottles received intaWt

5. N Samiple received In proper containers? 12... Custody .1a tamper evident on bottles?

6.YN Sample volume sufficieni for analysis? 13. Y N Was CUR (equivalent) rec* d fromn original STL lab?

*Temiperature Variance Does Not Affect tW Following Analyses:___________________

tFor DOE-AL (PAts, LAM!, Sandi) Ates, verlfy pH all containers received, cteept for VOA, TOX, and %Wb.

Notes:

Corrective Action:

D3 Client's Name: lnfbrmzd by: ____________ By.,___________

o Sample(s) processed "as is".____________________________________

o Sample(s) on hold until: If released, notify; _______________

Project Masnagement Review: / (.4 Date: ~THIS FORM MUST BE COMPLMI AT THE TIME TifE ITEMS ARE BE3NG CaIECKED

IF ANY ITEM IS COMPLET1ED BY SOMSEONE OTHER THAN THE INITIATOR, THEN THAT PERSON IS REQUIRED TO APPLY THEIRINMTALS AND THE DATE NEXT TO THAT ITEM

5512 ADMfIN-0004, Revisedi2111104~\IsvrQ1\QA PORM3MT-LOUSADMNAdrniafl04 sv7.doc

LOT # F5C160257 W04380B B of 13

METALS

L4 1;

STL ST. LOUIS

MOOR WUORD 1C

client Bawple ID: B19171l

TCLP Metaim

Lot-BaM1I. #.. PSFC160257-001 Matrx .... SOLIDDate Bw1ed. . ... 06/2.8/04 Date Received..; 03/16/05Leach Date ... 03/17/05 Leach Batch #1..za P507612

REPORTING PREPARATION- WORKPARAMETER RESULT LIMIT UNITS UMOD ANALYSIS DATE ORDR #

PrOP Batch 0.;5079040mercury 1.9 B 10.0 ug/L 51846 7470A 03/20-03/22/05 "PCPVIA

DilUtion FaCtOr: 5 HM L.............I 0.23

Afhiypa wbezhu Is umo~im vAM USEPA To~iry~ Ca'wliic Lcacb4 Procawm Md 1311

R Enlumkd miL Rewk is km 11mn RL

LOT # F5C160257 W04380B 10 of 13

STL ST. LOUIS

fULTRfl SPIKE SAMPLE DA6TA REPORT

TCP Mettle

Client Lot t...; F5C160257 atriX ........... BSOLIDDate Sampled... : 08/18/04 Date Received.., 03/16/OS

SAMPLE SPIKE MEASUD PHRCNT PREPARATION- WORKPARAMETE AMUNT AwE AMOUNT WITS RECVRY RPD METHOD ANALYSIS DATE 2RP!L#

NO Lot-Sample #z 75C160257-OO1 Prep Batch #...:. 5079040Leach Date ....... 03/17/OS Leach Batch 8..: PS07612Mercury

1.9 25.0 24.9 ug/L 92 914846 7470A 03/20-03/22/05 Q6CPV1AC1.9 25.0 24.2 ugiL 89 3.0 514846 7470A 03/20-03/22/05 GECPV1AD

Dilution Factor: S

NOTE (8)Calojaiom an prefwoi bMove rmASq to DOW r0006-off eIMn Wn calu Lad2L

LOT 4 F5C160257 W04380B 11 of 13

STL ST. LOUIS

Nm RLAW wJPK

TCLP Netals

Client Wt t... F5C2.60257 Matrx r....... SOLID

REPORTING PREPARATION- WORK

PARAMETER _RESULT LIMIT UNIlTS METHOD ANALYSIS DATE ORDER

MB Lt-Saeple *: F5C170000-333 Prep Batch #... ; 5079040Leach Date ....... 03/17/05 Leach Batch #..: P507612mercury NO 10.0 ug/L SN8S46 7470A 03/20-03/22/05 G6F621AK

DAiution ractorn s

Ca"Mmaax ye pfflormed bdoui modnS m avoid roum~ff mITmT in calcidd rma .

LOT # F5C160257 W04380B 12 of 13

STL ST. LOUIS

LABORTORY (XWETROL SMPLE DATA REPORT

TCLP Metals

ClicUt Lot #. PS7C160257 Nati ..... SOLID

SPIKE MEASURED PERCNT PREPARATION- WORKPAR~AMEE AMOUNT AMOUNT UNITS RECVRY METHOD ANALYSIS DATE ORDER

ICS Lot-Sample#: F5C200000-040 PzW Batch # ... t 5079040Mercury 2S.0 25.9 ug/L 104 SW846 7470A 03/20-03/22/05 06L621AA

DilUtiOn FaCtOri 5

NOTE(8) :Ccarciamwu performed befoe rotin lo avoid Tound-offerrom incalciedI rewire.

LOT 1* F5C160257 W04380B 13 of 13