231SERBSF10,614 - 6 Feb 2017 14:55

*231SERBSF10,614*

*231SERBSF10,614 *

Site Name (Subject): S & S METALS RECYCLING COMPANY

Site ID (Document ID): NCD093334969

Document Name (DocType): Correspondence (C)

Report Segment:

Description: General Correspondence, 1972- 1995

Date of Document: 8/22/1995 ---~ -~------~~-------~~

Date Received:

Box: Enter SF and# with na spaces

Access Level:

Division:

Section:

Program (Document Group):

Document Category:

Print Report for Record

Go to New Blank Record

SF10,614

PUBLIC

WASTE MANAGEMENT

SUPERFUND

SERB (SERB)

FACILITY

Go to New Record -(default to last record values)

-----··~-

• DATE: August 22, 1.995

SUBJECT: . REMOVAL FROM EPA'S CERCLIS INVENTORY

FROM:

TO:

Matthew J. Robbins, Brownfields Coordinat Waste Management Division, Region IV

S & S METALS RECYCLING SHORTCUT RD # 2455 GOLD HILL NC 28071.

EPA has identified the Brownfields Initiative as one of the Agency's top priorities. The term "brownfields" refers to previously used properties that may lie vacant because potential contamination makes them unmarketable to the private sector. EPA has recently announced a comprehensive Brownfields · strategy, including Pilot grants to municipalities, to stimulate economic revitalization.

One part of the strategy has been for EPA to review its complete inventory of Superfund sites. These sites have been screened and determined to require no remedial action under the Federal Superfund Program b~sed on information available as well as on conditions and policies th~t currently exist. This is to notify you that EPA has removed your facility from EPA's computer inventory known as CERCLIS. THIS DOES NOT INDICATE THAT THE STATE HAS MADE A SIMILAR DETERMINATION. .

If you have any questions, please call me at 404/347-5059 ext. 621.4.

cc: State Agency

:...: ......

To: From: Date: Re:

•• MEMORANDUM

File Stuart F. Parker, Jr., Hydrogeologist August 1, 1995 S & S Metals Recycling site Cabarrus County, NC NCD 093 334 969

••

Telecommunication with Frank DeLoache, Salisbury Post.

SFP received a telephone call from Frank DeLoache of the newspaper "The Salisbury Post", inquiring about the S & S Metals Site. He had been referred to this office by Joe Parker of the Mooresville Regional Office. Apparently, the recent developments at the site, i.e., Delmer Cauble Sr's intentions to clean up metal debris and use the site as pastureland, had drawn the attention of neighbors concerned about the site. Mr. DeLoache was calling for further information about the site.

SFP summarized the site's status, including the history of allegations concerning chemical disposal, unsuccessful oil recycling and spillage, incineration of transformers, and the fact that the former site operator had left the state. SFP explained that off-site sampling had not indicated the spread of any likely site contaminants. SFP also referred him to Dr. Gerald Houghton, the local resident who had sworn out a deposition regarding suspicious site activity and relating other people's allegations of on-site disposal. DeLoache asked if this is a Superfund Site. SFP replied that the site had been investigated under CERCLA, but had been recommended for no further federal action. Deloache asked about groundwater sampling at the site. SFP explained that 3 wells close to the site had been tested in 1992 and found to be within drinking water standards, and that Houghton's well and another neighborhood well had tested safe within the past year.

To: From: Date: Re:

• • MEMORANDUM

File AJC.t t1f Stuart F. Parker, Jr., Hydrogeologist fY · July 26, 1995 S & S Metals Recycling site Cabarrus County, NC NCD 093 334 969 Telecommunication with Joe Parker, Hazardous Waste Section, Morrisville.

SFP returned a telephone call from Joe Parker, Morrisville Regional Office (704-663-1699). JP had received a call from Mrs. Sandra Wagoner, a local resident. Mrs. Wagoner had complained about the fact that material was being trucked away from the site, and that the trucks were passing close to her property. She was apparently concerned about PCBs from the site.

SFP and Grover Nicholson had spoken with Mrs. Wagoner in Gold Hill, Rowan County on 11/23/93. She is one of several local residents who have had longstanding concerns about the S & S Metals site, based on allegations by former employees regarding historical management and waste dispdsal practices at the formerS & S Metals facility. Joe Parker was not familiar with the site or its history.

SFP described the results and conclusions of the June 1994 Site Inspection Prioritization of the site, explaining that the site had not been recommended for further action under CERCLA, but that significant disposal of organic and inorganic contaminants was suspected to have occurred there. SFP also related the details of a telecommunication with Delmer Cauble, Sr., the current site owner, on July 25, 1995. Mr. Cauble planned to remove scrap metal piles from the ground surface at the site, and to use the land for pasture. SFP had advised Mr. Cauble (who knew of the site's alleged disposal history) to contact the State if he encountered any sludges or buried containers at the site, and not to attempt to clean up or disturb any such wastes because of safety and legal reprocussions.

Joe Parker reported that he had dropped by the site today in response to the call from Mrs. Wagoner, but had not entered the property. SFP described the location of the metal scrap piles onsite. JP said he had seen muddy truck tracks leading onto Short Cut Road from the site entrance, but that he had seen no other activity there.

To: From: Date: Re:

• • MEMORANDUM

File ,u. 9y Stuart F. Parker, Jr., Hydrogeologist y·· July 25, 1995 S & S Metals Recycling site Cabarrus County, NC NCD 093 334 969 Post SIP Site Development

On 7/11/95, SFP received a telephone call from Dr. Gerafd Houghton, a local resident who lives opposite the site on Gold Hill Road. Dr. Houghton had monitored the former S & S Metals Recycling Company operations during the late 1970s, and completed a deposition regarding alleged chemical disposal at the site. Dr. Houghton called to notify SFP that the property had apparently been purchased by persons unknown, and that bulldozers and cranes were removing the scrap metal and lathe turnings which had accumulated on the eastern side of the site.

SFP telephoned Mr. Charles Sehorn (704-786-6414), who was the site owner at the time that SFP completed the S & S Metals Site Inspection Prioritization (SIP) report. Mr. Sehorn reported that Delmer Cauble, Sr. had bought the property several months before and apparently planned to grow trees there. Sehorn reported that Mr. Cauble was aware that the site is considered a likely hazardous waste site. Mr. Cauble also owns the adjacent land tract to the east of the site. Delmer Cauble Jr. lives on the property. The NC Superfund Section sampled his well and 2 other local domestic wells in 1992 and found no contaminants attributable to the site.

SFP telephoned Mr. Cauble, Sr. (704-636-0517) on 7/11, but received no response. Following a week's absence from the Superfund Section office, SFP telephoned again on 7/25 and spoke with Mr. Cauble. He reported that he was removing the accumulated scrap metal from the ground surface at the site, and that he planned to convert the area to cattle pasture.

SFP advised Mr. Cauble that the site was no longer under Superfund investigation, but that hazardous materials may have been buried or dumped there by the S & S Metals company. He replied that his adjacent property had received some oil spillage from S & S Metals' unsuccessful oil reclamation attempts. The company had folded before he could initiate legal action, but the damage appeared limited to 1 dead tree and some other stressed vegetation (A sediment sample was collected from the property during the 1993-1994 SIP, but contaminants were limited to low ug/1 concentrations of ethylbenzene, xylenes, and MTBE).

SFP advised Mr. Cauble that ifhe encountered any containers or sludges, 1) he should stop work and immediately notify the local State DEM office or the NC Hazardous Waste Section, and 2) he should not attempt to remove, disturb or containerize any such material, because this would give him direct legal responsibility for its disposal. Mr. Cauble replied that he understood, but that he was skeptical about the allegations of chemical disposal

State of Nort~arlna Department of Environment, Health and Natural Resources Division of Solid Waste Management

James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary William L. Meyer, Director

Dr. Gerald Houghton Route 2, Box 238-A Gold Hill, NC 28071

May 16, 1995

SUBJECT: Well Sampling Results S&S Metals Recycling Gold Hill, Cabarrus County, NC

Dear Dr. Houghton:

•

As you are aware, the NC Superfund Section collected samples from your drinking water well on November 8, 1994 and January 18, 1995 as part of an environmental assessment of the subject site. Samples were analyzed by the state Laboratory of Public Health for the chemicals listed on the attached sheets. The contaminant listed below was detected in your water sample. Concentration is expressed in parts per billion (PPB).

Contaminant

Barium

Concentration (PPB)

30

NC Groundwater Standard (PPB)

2000

MCL (PPB)

2000

This contaminant was measured at a concentration which is below applicable NC groundwater standards and below Maximum Contaminant Levels (MCLs) considered acceptable for public water supplies. These results were reviewed by the state Environmental Epidemiology Section and they have concluded that your water is safe for continued usage. A copy of their evaluation is attached for your information.

P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/1 0% post-consumer paper

Dr. Houghton 5-16-95 Page 2

·- ·-If you have any questions regarding health concerns, please

contact Dr. Ken Rudo, Environmental Epidemiology Section at (919) 733-3410. If you have any other questions, please contact Stuart Parker, Superfund Section at (919) 733-2801, extension 277.

attachments

cc: Dr. Ken Rudo, letter only File Donna Keith Stuart Parker

Sincerely,

Pat DeRosa, Head CERCLA Branch Superfund Section

State of Nortlarlna Department of Environment, Health and Natural Resources Division of Solid Waste Management


Mr. Robert Burton 1.501.8 Short cut Road Gold Hill, NC 28071.

May 1.6, 1.995

SUBJECT: Well Sampling Results S&S Metals Recycling Gold Hill, NC

Dear Mr. Burton:

•

As you are aware, the NC Superfund Section collected samples from your drinking water well on November 8, 1.994 as part of an environmental assessment of the subject site. Samples were analyzed by the State Laboratory of Public Health for the chemicals listed on the attached sheets. The contaminants listed below were detected in your water sample. Concentrations are expressed in parts per billion (PPB).

Contaminant

Barium Chromium

Concentration (PPB)

20 l.O

NC Groundwater Standard (PPB)

2000 50

MCL (PPB)

2000 1.00

These contaminants were measured at concentrations which are below applicable NC groundwater standards and below Maximum Contaminant Levels (MCLs) considered acceptable for public water supplies. These results were reviewed by the State Environmental Epidemiology Section and they have concluded that your water is safe for continued usage. A copy of their evaluation is attached for your information.

P.O. Box27687. Raleigh. North Carolina 27611-7687 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/1 0% post-consumer paper

-Mr. Burton 5-16-95 Page 2

·- ·-If you have any questions regarding health concerns, please

contact Dr. Ken Rude, Environmental Epidemiology Section at (919) 733-3410. If you have any other questions, please contact Stuart Parker, Superfund Section at (919) 733-2801, extension 277.

attachments

cc: Dr. Ken Rude, letter only File Donna Keith Stuart Parker

Sincerely,


State of North cAna Department of Environment, Health and Natural Resources Division of Solid Waste Management


February 21, 1995

MEMORANDUM

TO: John Freeman, D.V.M., M.P.H., Chief Environmental Epidemiology Section

THROUGH: Bill Meyer, Directo~ Division of Solid ~~~e ~anagement

FROM: Pat DeRosa, CERCLA Branch HeaA ~A~ ~ · Superfund Section ~ ~

SUBJECT: Health Risk Evaluation Request s & S Metals Recycling, NCD093334969 Cabarrus County, NC

Please find attached a copy of the laboratory analyses for well samples collected by the Superfund Section around the subject site. Since these samples were collected from drinking water wells, the Superfund Section requests a health risk evaluation and a recommendation on the continued use of these wells. This information will be provided to the affected well users. If you have any questions regarding this matter, please contact stuart Parker or me at 733-2801.

attachments

cc: File Donna Keith Stuart Parker

PD/EPil

P.O. Box 27687, Raleigh. North Carolina 27611-7687 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/1 0% post-consumer paper

I

-------------- ---- --------

N.' ..... :) cn~ t-.t ,~H: n t of E nvi ronment, "" ' . I IC;! It l-:, & ; ·~ :ura l Resources Sol id Was1c ;,!anJgcmcn t D ivisio n

SA. LE ANALYSIS REQ1JEST

S'i tc Number tJ c.p ()~ l 3 :{ Lf ~ b ~r

Name of Site J" J... S Y\A.~fv:-,1 (

Coll ected By.S F f.., .. 'pN-/ f-1 -t : "" "' ID # Dale Collected f I/~~ q c/ ----- ---------~-~---------

{'>-gency: H azardous W aste Solid W as te x___ Superfund TCLP Comp oun ds -- -----

Sample Type In organ ic Com pounds Rl!s ults (mg/1) Environm enta l Concentrate Comments A rse nic --

(Lo~ ·a ... r~o,.. Barium X Ground wa ter (1)

--Solid (5) Cadru ium - -

--Liquid (6) J2- t.~ ; ~4- .. ·'h· ~I ~l( Chromium

_ _ Surface water (2) - -

Lead - -

D"''~'''r~ ""'It r;r ,._ -- M ercury _ Soil (3) _ Sludge (7) Selenium --

Silver --_Other (4) O ther (8) - -

- -

--Orga nic Chemistry Inorganic Chemistry --

Parameter Results (mg/1) Pa r ameter Resul ts (mg/1) (mg/kg) Organic Co mpounds Resu lts(mg/ 1) 2{_P&T:GC/MS Arsenic benzene -- -- -

Acid :B/N Ext. Barium carbon te trachloride - - -- - -MTBE Cadmium chlo rdane -- -- --

Chloride chlorobenzene -- -- - -Chromium chl oroform -- - - --

-- __ Copper o-cresol --F luoride m-creso l - - -- --

-- Iron p-cresol - - --Lead cresol -- -- --

-- __ M anganese -- 1,4-dichlorobenzene

-- _ _ M ercury 1,2-dichlo roe th ane - --- Nitrate 1,1-dichlo roethylen e -- - -

Selenium 2,4-dini trotoluene _ -- --Silver heptachlor - - --

Radioch emistry Sulfates hexachlo robenzene -- --·---- Z inc hexachlorobutad iene

-- --Res ults (PCi/1) Para meter pH hexach loroe th ane - - --

__ G ross A lpha _ _ Conduct ivi ty -- meth yl ethyl ketone G ross Beta T DS nitrobenzene -- - - --

T OC pentachlorophenol . ' - - - --- __ pyridine

Microbiology - - - - tetrach loroethylene

tri chloroethylene -- --Para meter Res ults (Col/ l OOm!) 2, 4,5- tri chlorophcn ol

-- - --- --

2, 4,6- trichl oro phenol --- - - - - - vinyl chlo ri de

endrin - -

1!- q__qy W& Repo rted~~~ l---->- lind ane D ate Received r:.- _ _ me thoxych lor

D a te Re~rted //-J.--K- ?rJ? _ _ toxaph e ne

D <J te Extr <J ct e tl _ 2,4-D

l/-!'l-9L/ -nw- 944394 _ _ 2,4 ,5-TP (Sil·1ex)

D ale An a lyzed Lab Number DIIS 3l'J I ( l (cviscd~/<Jl) 'fuC- 11 [~]14' ~ ;::1- c; V v·5 9 }L-

---c./)'- C77" 9V J

· ·· KC. Oepartmc.nt of Environ~ent, . ' llpli/.h, & Natural Resources

·• -Solid Waste Management Division

SAMPLE ANALYSIS REQUEST e State Laboratory of Public Health

A P.O. Be·~ 2&}17, 306 N. Wilmington Street W Raleigh, Nar'.h Car:Jlina 27611

s'itt·Number tJ t.p C~.:S, 3:5 lf. Ctf::/J

Name of Site .S A-S ~~~I/

Field Sample Number 0/SG't "2-,

· Coll~cted By.SF p.., ... ~j~ =e : ..... "" ID# __ _ Date Collected /r/ ~~ qu Time /0: 'I 0 ·--~~~~~~-----

Agency: Hazardous Waste Solid Waste X-_ Superfund TCLP Compounds ! I --

Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --

_· _Solid (5) · ft.o~rl- . (J c..rfo"" Barium

X Ground water (1) --

Cadmium ---Liquid (6) {Lt.~ ; ;~~1",· A I (/'Jvt( Chromium

__ Surface water (2) --

Lead --Sludge (7) 1?~•~1~1~~ I#IIVE't- -- Mercury

_Soil (3) Selenium --Silver --

_Other (4) _Other (8) ------

Organic Chemistry Inorganic Chemistry --Parameter Results (mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene -- --~ Acid:B/N Ext. Barium carbon tetrachloride -- --"MTBE Cadmium chlordane X ~';lc1PCJ/~~ --

Chloride --

chlorobenzene

=Edd.i!iil -- --<t?. ~ell?/ Chromium chloroform -- --

Lhi~Ne <o. en:~o .::Z.. __ Copper a-cresol .2!f~e/dtU. <:p. di'J/ Fluoride

--m-cresol -- = p-cresol _"70.X1fHet/£ ~<?~ dP~ Iron --

~"" <oooo<>.;z. Lead cresol -- ---- Manganese 1,4-dichlorobenzene _ ~-<<2· ooo/ __ Mercury --

1,2-dichloroethane Jl@ . ~~11'· e/Pt?/ _ P~s <o. ot?i?/ Nitrate

-- 1,1-dichloroethylene -- --Selenium 2,4-dinitrotoluene . --- = heptachlor Silver --

Radiochemistry Sulfates hexachlorobenzene -- --Zinc hexachlorobutadiene -- --

Results (PCi/1) Parameter _pH hexachloroethane __ Gross Alpha __ Conductivity -- methyl ethyl ketone

Gross Bela TDS -- nitrobenzene -- -- = pentachlorophenol TOC ' I ---- __ pyridine

Microbiology -- -- tetrachloroethylene

-- __ trichloroethylene Parameter Results (Col/100m!) __ 2,4,5-trichlorophenol ---- -- 2,4,6-trichlorophenol

-- -- = vinyl chloride endrin --

II- q --Cf if VIV lindane

Date Received Reported by ---- methoxychlor

Dale Extracted ~tif'hfli-«fg,'&£r£rcGReported -- toxaphene 2,4-D

~1)1# f'e;:r'1-A:;B~ ---- 2,4,5-TP (Sil'lex)

Dale An<~lyzed Jl-lif -~'{ U-17-7'/ypLab Number 944395 DIIS 31'Jl (Itcviscd 2/'Jl)&IJ

----

I

. ~:.c. Dep~hment of Environment, lleallh, & Natural Resources

Solid Waste Management Division

WPLE ANALYSIS REQUEST State Laboratory of Public Health

P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611

Site Number tJt(;) DtO.S 3:! lf. Cf{,~

Name of Site .S ~ S Yille,./TJt II'

Collected By.SF P ... ~~/r' ~ :""""

Field Sample Number 0 •rcte,3 I --------------------------------

Site ~cation (A. ~Gror!Jr Cd '-~"+7 rJC.....

ID# - Date Collected {I./~/ <:ft.( Time ll' :I 0

Agency: Hazardous Waste Solid Waste X-_ Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results (mg/1)

Environmental Concentrate Comments Arsenic --Gerc.rJ. J...lou~L,-f-p..._

Barium X Ground water (1) _Solid (5)

--Cadmium --

- Liquid (6) ~ t' J <-f"\Tl c I W<..ll Chromium

__ Surface water (2) --

Lead --P~•rl tG•~t WATE/\-

__ Mercury _Soil (3) _Sludge (7) Selenium --

Silver --_Other (4) _Other (8) --

----

Organic Chemistry Inorganic Chemistry --Parameter Results(mgfl) Parameter Results(mg/1) (mg/kg) Organlc Compounds Results (mg/1) ')( P&T:GC/MS Arsenic benzene -- --

Acid:B/N Ext. Barium carbon tetrachloride -- --MTBE ,· Cadmium chlordane -- -- --

Chloride chlorobenzene -- -- --Chromium chloroform -- -- --

-- __ Copper o-cresol --Fluoride m-cresol -- -- --

-- Iron p-cresol -- Lead cresol -- -- ---- __ Manganese -- 1,4-dichlorobenzene

-- __ Mercury __ 1,2-dichloroethane

-- Nitrate __ 1,1-dichloroethylene --Selenium __ 2,4-dinitrotoluene . ---

-- Silver __ heptachlor Radiochemistry Sulfates hexachlorobenzene -- --

Zinc hexachlorobutadiene -- --Results (PCi/1) Parameter _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- = pentachlorophenol TOC : i ---- __ pyridine

Microbiology -- __ tetrachloroethylene

-- __ trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ---- -- __ 2,4,6-trichlorophenol

-- -- __ vinyl chloride endrin --

lf- q -4lf VG--' lindane

Date Received Reported by = methoxychlor __ toxaphene

Dale Extracted Dale Reported __ 2,4-D /;

Dale AnalyLed 1/--J1--9tf-f/UT ~b Number 944396 _ 2,4,5-TP (SiJ·,ex)

DIIS 3191 (Revised 2/91) V~~~-~~..-94'£t 11\. . --

Purpose: Enforcement and co.nce with the N.C. Solid and Hazardous \. Management Rules. .: . "

Preparation: A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water) a sample label must be affiXed to one of the containers. The collector must then write the site and sample number on the duplicate container.

Do not submit an analysis request form without any parameters indicated.

Equivalent measurements: ppm = J.lg/ml = mg/1 = J.lg/g = mgjkg ppb = J.lg/1 = J.lg/lOOOg = J.lg/kg

DEFINITIONS/INSTRUCTIONS

Site Number- A unique twelve-digit site/location identifier (i.e., the EPA identification number).

Field Sample Number -A unique six-digit sample identifier which is pre-printed on the sample label.

Name of Site - Name of facility, landfill, etc.

Site Location - City and county.

Collected By - Name and staff identification number of collector.

Date and Time Collected - Self-explanatory.

Environmental - A sample of a naturally occurring substance such as ground water, surface water, or soils which may be contaminated.

Concentrate - A sample of a waste, including bu~ not limited to, sludges, resins, treatment effluents, or drummed wastes.

Comments - Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, and/or odors. · .. -

Inorganic Chemistry - Check ( ./ ) the desired parameters to be analyzed. If not ~sled, enter the · element/compound in the space provided.

Organic Chemistry - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided.

TCLP Compounds - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provid~d. TCLP can only be performed on solid or semisolid samples. For totals of the inorganic parameters, check ( ./ ) the corresponding parameter under Inorganic Chemistry.

Microbiology and Radiochemistry - Contact the Raleigh office prior to sampling either of these.

Distribution:

Disposition:

1. Send or deliver the original to the State Laboratory of Public Health. 2. The Lab then sends a copy (with results) to the Solid Waste Management Division. 3. The Solid Waste Management Division sends a copy to the field person or collector.

This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History

Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 27~p

N.C. Dcprm!:.H:nt of Environment, _.. . 'l!callh, & Natural Resources


S.PLE ANALYSIS REQUEST State Laboratory of Public Health P.O. Box 23047, 306 N. Wilmington Street

Raleigh, North Carolina 27611

s\te Number tJ Cp D~ 1 3:? lf . ct b c;

Name of Site .S J..- S Y\.4 ~.,.., I~

Collected By.SF p.., ... r-.--jrf :e :""""'

Field Sample ,Number __ D_LS_ct_q_'1 _________ _

Site L>cation (A. i tl,. ~ v.r Cd ..., ,., -f'7 -----------~·~------------

ID# Date Collected ( t/ f' / qy Time I C' : I 0 ----~~ ~--~~~~---~------

Agency: Hazardous Waste Solid Waste X-_ Superfund TCLP Compounds I -- --


Ger~,.J. J1ou.j"'~" Barium

X Ground water (1) --

_Solid (5) Cadmium --~,'(..{-c,"''Tr'c/ W<..ll

Chromium . Surface water (2) · _Liquid (6)

--Lead --

D (l.,uJ tG• ~ {, WAT'€/L Mercury

_Soil (3). _Sludge (7) --Selenium --Silver --

_Other (4) _Other (8) ------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene -- --')(. Acid:B/N Ext. Barium carbon tetrachloride -- --'MTBE Cadmium chlordane ')l fJ6m~tf1E:!/Pe-B.i -- --

Chloride chlorobenzene -- --6./d~i/ <:1!1. 61?17/ Chromium chloroform --- -- --_ L./A!dAIIE . <'o. 01717~ __ Copper a-cresol

~L <e:J. Od/ ---

Fluoride m-cresol -- = p-cresol ~ ~d.PI7~ Iron c.IJ.7&<tMHC. c::o. 01:?17~

-- Lead cresol ~ <:d. &'P~/ --- --__ Manganese -- 1,4-dichlorobenzene

i'/EXAfAI"""tkiv.rzye;: <17. P~~ I __ Mercury __ 1,2-dichloroethane ___ PM:f <o. poet I Nitrate __ 1,1-dichloroethylene --

Selenium 2,4-dinitrotoluene . - . -- --Silver __ heptachlor --

Radiochemistry Sulfates hexachlorobenzene -- ---Zinc hexachlorobutadiene -- --Parameter Results (PCi/1) _pH hexachloroethane --___ Gross Alpha ___ Conductivity ___ methyl ethyl ketone

Gross Beta TDS nitrobenzene --- -- --TOC __ pentachlorophenol .. --

-- __ pyridine Microbiology -- __ tetrachloroethylene

-- __ trichloroethylene Parameter Results (Col/100ml) -- __ 2,4,5-trichlorophenol

--- -- __ 2,4,6-trichlorophenol

--- -- __ vinyl chloride endrin r-..

--[l-q .£/<f U/G---Reported by

lindane Date Received = methoxychlor

Pur~~~ {£tf-?t/-YP,tJJ6 __ toxaphene Dale Extracted BI\J lf-1 SA£ Dale Reported 2,4-D

8JJA fJe:sTY"",P~ . 944397

= 2,4,5-TP (Sil·;ex) Dale AnalyLed//,JcJ-~//-/7-~Lab Number ---Dl IS 311JI (Revised 2/91) ~

, J/.C. D~pa'rtment of Environment, Health, & Natural Resources


.PLE ANALYSIS REQUEST. State Laboratory of Public Health

P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolina 27611

Site Number ,_l( 17 rfi:! 33'-1. G!?t:t

Name of Site ..f-4-.{ f'-le-f'p. !r Field Sample .Number __ .:...O_I_s-_Da_OJ_r ________ _

S. Lo. . ..... ~ b• ,., .. , (A,., .. 1t.. ,J c tte catton, __ c....-'"4 ___ _:"':_--~L!..---------

Collected By Sf P•rr...,.-j 1-f ~:,.... ID# - Date Collected. __ t _' /_t_:_/_~'1..:.__ ___ Time Tt-• ,.,

Agency: Hazardous Waste -- Solid Waste X Superfund TCLP Compounds

Sample Type Inorganic Compounds Results (mg/1) Environmental Concentrate Comments Arsenic -- Barium

__ Ground water (1) _Solid (5) Trt-•P --Cadmium --Chromium

c3c...~r ,.,I'(. Surface water (2) _Liquid (6)

--Lead --Mercury

_Soil (3) _Sludge (7) --Selenium -- Silver ~ Other (4) Other (8)

--------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) X P&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- --.MTBE Cadmium chlordane -- -- --


-- __ Copper a-cresol --Fluoride m-cresol -- --= p-cresol -- Iron --

Lead cresol --=Manganese

-- 1,4-dichlorobenzene -- ---- __ Mercury -- 1,2-dichloroethane

Nitrate 1,1-dichloroethylene -- -- --Selenium __ 2,4-dinitrotoluene _ --· --Silver __ heptachlor --

Radiochemistry Sulfates hexachlorobenzene -- --Zinc hexachlorobutadiene -- --Results (PCi/1) Parameter _pH hexachloroethane

__ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene -- --

= pentachlorophenol TOC :i ---- __ pyridine




/f- tf- fi Cf-(//~ Reported by lindane

Date Received --__ methoxychlor __ toxaphene

Date Extracted Date Reported 2,4-D

1/-r1-9'f"''lul Lab Number 944:398 = 2,4,5-TP (Sii·1ex)

Date AnalyLed DIIS 3191 (Revised 2/91) '\'OC..II/lZ}'ilf~ --

,•

/

Purpose: Enforcement and co-ance with the N.C. Solid and Hazardous etc Management Rules. ' . '

Preparation: A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate container.

. '

Do not submit an analysis request form without any parameters indicated. . '

Equivalent measurements: ppm = pgjmi = mg/1 = pg/g = mg/kg ppb = pg/1 = pg/lOOOg = pg/kg

DEFINITIONS/INSTRUCfiONS


Field Sample Number - A unique six-digit sample identifier which is pre-printed on the sample label.

Name of Site - Name of facility, landfill, etc . ./;

Site Location - City and county. ,•



Environ~ental - A sample of a naturally occurring substance such as ground water, surface water, or soils which may · be contaminated.

Concentrate - A sample of a waste, including bu~ not limited to, sludges, resins, treatment effluents, or drummed wastes.

Comments - Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, and/or odors. · ---

Inorganic Chemistry - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided.

Organic Chemistry - Check ( ../ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided.

TCLP Compounds - Check ( ./ ) the desired parameters to ~e analyzed. If not listed, enter the element/compound in the space provided. TCLP can only be performed on solid or semisolid samples. For totals of the inorganic parameters, check ( ./ ) the corresponding parameter under Inorganic Chemistry.


Distribution:

Disposition:



Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 2761~ ..... · , ~

• •t

STATE LABORATORY OF PUBLIC HEALTH

P.O. BOX 28047-306 N. ;WILMINGTON, ST., RALEIGH, N.C. 27611

ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID

EXTRACT ABLES COMPOUND

N-nitrosodimethvlamine bis(2-chloroethvllether 2 -ch 1 orooheno 1 phenol 1 3-dichlorobenzene 1,4-dichlorobenzene 1 2-dichlorobenzene bis(2-chloroi l)ether hexachloroethane N-nitroso-di-n-oroovlamine nitrobenzene isoohorone 2-ni troohenol 2 4-dimethvlohenol bis(2-chloroethoxv)methane 2 4-dichloroohenol 1 2,4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro~resol

hexachlorocvclopentadiene 2 4 6-trichloroohenol 2-chloronaphthalene acenaohthvlene dimethvl ohthalate 2 6-dinitrotoluene acenaohthene 2,4-dinitroohenol 5 4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlohenvlether diethvl phthalate 4,6-dinitro-o-cresol diohenvlanine azobenzene 4-braroohenvlohenvlether hexachlorobenzene oentachloroohenol phenanthrene anthracene dibutvl phthalate fl uoranthene

LAB NO FIELD # TYPE UNITS /(J/~3D

'V SO//t,So l!tJ/330 SO/iwSO to/~o

I

/()/330

/tJ/330

J - Estimated value.

m"DL Hz.O/.S0/1-

1. I > J..J >

I ,. \

K - Actual value is known to be less than value given.

( ) ( ) ( ) ( ) ug/1 ).Jg/~g ug/1 lJQ/~ _p_g/1 lJQ/kQ uQ/1 uQ/kQ

L - Actual value is known to be greater than value given. U - Material was analyzed for but not detected. The number is the Hinimum Detection Limit. fr)2)L. NA- Not analyzed. - - - _ 1/ - Tentative identification. ~I- On NROC List of Priority Pollutants.

...

STATE LABORATORY OF PUBLIC HEALTH

P.O. BOX 28047- 306 N. WILHINGTON, ST., RALEIGH, N.C. 27611

ORGANIC CHEHICAL NIALYSIS

BASE/NEUTRAL NID ACID LAB NO 1'1VV3CfS' 19</l/_3q 7 EXTRACT ABLES FIELD II JS'/9.).... Js-99'1 COMPOOND TYPE .1/) 1 I> ( . ) ( )

UNITS ~_}Jg/t)=&qc _}.lg/l~g }Jgll }Jg/kQ uQ!l uq/kq pyrene 1/0/.330 ""-- Vl-benzidine lsnl!hSO butyl benzyl phthalate 10/.330 benz(a)anthracene chrvsene J, 3 3-dichlorobenzidine 'lhStJ .SfJJ bis(2-ethvlhexyl)phthalate ~/tJ/330 di-n-octyl phthalate 1 /0/.S3o benzo(b)fluoranthene .S0/11£0 benzo1kJfluoranthene benzo(a)pyrene indeno(t 2 3-<:d}pyrene dibenzo(a h)anthracene / / benzo(qh i)oervlene \l.f "'' ... If

aniline S"tJ/JhS'O .VL-_ (.;1-benzoic acid benzvl alcohol 4-chloroaniline ~ , dibenzofuran /(J. '.330 2-roethylnaphthalene 2-roethylphenol 4-methvlphenol

··"' 2-nitroaniline s-o!JhSo 3-nitroani line 4-ni troani 1i ne f_ r_

2 4 5-trichloroohenol "" '" ' "

m'Dt-J - Estimated value. Ha-0/ $'(')/i-K - Actual value is known to be less than value given. L - Actual value is known to be greater than value given. U- Haterial was analyzed for but not detected. The number is the Hinimum Detection Limit. NA - Not analyzed. 1/ - Tentative identification. fl -On NROC List of Priority Pollutants.

( ) ( )

}JQ/1 \JQ/kQ uQ/1 uQ/kg

. . -= _; __ ~ . ..:-......... . -· .. ··----· --· ...... -. . .. -· ·--·-····-·-·-·:---·-------;...;.:-·:=::;.: .:;;.;_---

Sl:A:r.E I.ABORA:IORY OF PUBLIC 'HEALTH PO BOX 28047 - 306 N. WILlOl'iGTON ST- R.AI.EIGR. NC 2761.1

ORGANIC CHEMTCAL ANALYSIS

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:PO BOX 28047 - 306 l'l. 'WII.MINGTON ST_ RAIZTGR. NC 2761.!.

II POR~ CO.l!!POOlYDS I LAl3 NO I 9Jt.tt394- I9J/ q.3q {p I <f'f.i/.398 I I I i

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C-DCH~\/R

Divis ion of Solid Waste Management

0 Superfu nd Sec tio n

0 Hazardo us Was te Secti on

0 Solid Waste Section

Organics Lab: "?' lnorganics Lab: - -

CHAI N OF CUSTODY RECORD

Project Name: J -1-.S r"c-f~ { 1 Sampled by: .f p c ,.[:;..t..,r I H :e,."'" Site ID # (NCD#) oc;a :r~ "' c;-' :t Sampler ID -Location: c,~ ... ,..~ C()ln''M rJC Telephone:_(<J1<7) Ill l~l Address: s "'•ll"f- c ... -t rto( D ate Sampled: II I f/CJy

Time Sampled: -Sample Types: Soil Water '/- Waste Other

Remarks: f/r:.-.fci"_S w ... +-.,., WeA.f..t.

Field Sample o trc;q t 0 I ,r<j~'l.. o~rc;,~ 0 t.rc;~l( oi.I-c;~r

Tumbers -

Relinquished by: )J:Q »;!j/ Date: U/'1/CUf Time: il '-(_ 0 (S ignature)

~-~~~;~~d--~~---~~"~!f=Cf---------- --- ----- --------- ----r;~;~:uzps;v -- ~;;;;~: -E~~- -----------

II

II

I I

Relinquished by: Date: Time: =-1 (S ignature)

I ------------- -------------------- ---------------------------- ------ --- -------- -------------- -------------- ----- ------ ------ -- --- ------- ---------Received by: Date: Time:

(Signature)

Relinqu ished by: Date: Time: (Signature)

------------------------------------------------------------- ---------------------------- -------------------------------------------------- -----Received by: Date: Time:

(Sig_9,ature)

Results Reported: L ~ / ,/Lect__ D a te: l/-2cf-9.)CTime: I ~ignature) :# cr /XI y v - c/5L>69,f

l

------ -~ -- --------------

~.C. Department of Environment,

. · l lcal th, 6:. Nat ural Reso u rces

·, -Sol id Waste Manageme nt Division

SAMPLE ANALYSIS REQlJEST e S;atc Laboratory of Public Hc>lth

P.O . l3cx 2&).17, 306 N. W il .nington Stree t

Raleigh, North Carolina 276 i 1

Field Sample .Numbcr ___ _ t)_/_b_g_t._f _ _ --------

Name of Site S J.- S 'f"vv c..f-t:./1

Collected By.SF p., ... ~jH :t: : ...-""

Agency: Hazardous Waste ~ I

- - -

Sample Type Environmenta l Concentrate

X Ground water (1) _ Solid (5)

__ Surface water (2) _ Liquid (6)

Site ~cation _ _ ~ __ G_<l_,._~_ .... _.r __ Co _ _ '-~_"~_-f_,;--Lz __ rJ_c ___ _ _

ID# Date Collected /I / 2' / qy Time /0 : lf 0 --- - ------~~--L--------

Solid Waste ~Superfund TCLP Compounds

Inorganic Compounds Results (mg/ 1) Comments Arsenic --

rto&ert . 0 w.rfoV\ Barium --Cadmium --

{2-~-' ; ~~ ... 1-,· J..f ~l( Chromium --Lead - -

- - Mercury D "''~t~:..,r~ ,., " r;e 1'-. _ Soil (3) _ Sludge (7) Selenium --

Silva --Other (4) -- Other (8) - -

----

Organic Chemistry Inorganic Chemistry --Parameter Results (mg/1) Parameter Resu lts (mg/1) Gs m'l t9 Organic Compounds Results (mg/1)

P&T:GC/MS ~ Arsenic .L.O .. ol benzene -- --Acid :B/N Ext. ~ Barium o. oa carbon leLrachloride -- -- --MTBE 'J.. · Cadmium L.. o ... ooO... chlordane -- -- --

Chloride chlorobenzene -- - - ---- 1_ Chromium c::> ... ol chloroform ---- _ _ Copper a-cresol --

Fluoride m-cresol -- - - - - - --~

Iron _ _ p-cresol r --~ Lead ...L..o - oo5 cresol

Q --

i i _ _ Manganese - - 1,4-dichlorobenzene

u, _1:_ Mercury L_ 0 , OQ::)S -- 1,2-dich loroethane

> Nitra te 1, 1-dichloroet h ylene -- ---w lr.) 0 ".)(.. Seleni um -<.o ... oo:S 2,4-dinitrotoluene . 0 z - - -- -

l-

~~ :::l )(. Silver ...::.. o-o5 __ heptachlor

c..:> ~ --

L1J stry Sulfates hexachloroben~ene 9 UJ - - --- ~ Qi. Zinc hexachlorobutadiene

-~~ -- - -

..:..I Results (PCi/1) __ pH hexachloroethane - -

I __ Cond uctivity -- meth yl eth yl keton e

:> TDS nitrobenzene > -- --

T OC pc;-~ t ach !oro phenol --A,) AJ

. ' -- - -1-- pyridine

-?- -- --. ---- ;y tetrachloroethylene - - ---

\../) trichloroethylene -- --

ts (Col/lOOm !) 2,4 ,5-trichlorophenol -- --

I -- --2, 4,6-tri chJ oro phenol

-- -- -- vinyl chloride endrin --lindane

- -Date Received Reported by metho;>..-ychlor - -

toxaphene - -Dale Extracted Date Reported 2,4-0

019522 NOV 994 --2,4,5-TP (Si l·;cx) --

Dal e A nalyzed Lab N umbe r --1) 11:; 3! '1! (l(c·,iscd 2/'Jl)

- ------ ----r•- -- --- ------

NC-DEHNR A Division of Solid Waste .ManagementW

0 Superfund Section

0 Hazardous Waste Section


Organics Lab: -:-----:-

Inorganics Lab: z(

CHAIN OF CUSTODY RECORD

Project Name: S -1 ~ f\1e~ l..t Site ID # (NCD#) OC13 33'1 ct6CV Location: Cab~ ,.,. • ..r Cf) "':!7 rJ c... Address: Sl,or1- c.~

r-·

Sampled by: .f p~, ~/11 :t= "'~ Sampler ID~~----,~-.,--------Telephone: (<JrCJ )-,:?:r 'liD/ Date Sampiea:-,-, /-:-e-/_fi_'f _______ _

Time Sampled: -

Waste Other Sample Types: Soil Water ----- ----- ------

Field Sample Numbers

Relinquished by: Date: Time: II

F{;;~;;;~;;d--t:;;;---------;::~~~-~:::~~---------------------------------------------r;;;;~;------------------;:;;;;~;------------------------ I,

Relinquished by: _______________ _ Date: __ _ Time: ------(Signature)

Received by: Date: Time: (Signature)

Results Reported: ~~e~~ Date: rD~cf~ Time: I (Signature)'

- I

(A:\ COCR.FR.!'J)

• NG. i)£HNR A

•· Div isi on of Solid Waste l\'lanagemen t •

ilf Superfu nd Secti on

0 Hazardous Was te Section


FEB 1 71995


Project Name: S' -(-J M dr.-/J ,[JJ', Sampled by: S' rf>.. ... .,. r- /e !"iu-r ( 1-'tc.~'z Site ID # (NCD#) rJb() oc,'] 33'1 '7(;'1 Sampler ID -Location: G u l ,( r-': VI C.. c. 6.,. .r.t-1 Co t-'c . Telephone:_(lJ ?;) 1:!3 'Lt!tJ I Address: ..r t.. ,T · c~T ~-J.._ Date Sampled:

Time Sampled: 1~30

Sample Types: Soil W ater --< Waste Other

Remarks: (),. : ... ~ :, ~~

-

-Field Sample ,, ' ~ ~.;:__ Numbers ~

-

Relinquished by: JM cr~ (Signature) '

Date: t/t7/7.J Time: I Ll:tt 'f

~- .. --

·-

--------------------------------·---------------------------------------------------------------------------------------------------------------Received by: s:r~"-1 ~~ Date: \ l l<>t h .s Time: 1"'-l '. "-l:l

( 1gnature)

I

I

II

~-

II

I I

1

I

Relinquished by: Date: Time: ~ (Signature)

I

--------------------------------------------------- ------- --------- -- -- --------- --------------------------------- -- --------- --------------------Received by: D ate : Time :

(Signature)

Relinquished by: D ate : Time: (Signature)

-------------------------------------------------------------------- --------- -------------------------------------------------------------------Received by: D a te : Time:

(Signature) L "

Results Reported: $£~~ D a te : l'f/?i9rTime: (S!gnature)

(t\ :\COC R.FR.:\1 )

_.)

'

I

- ,_ ,. ·N.C. Department of Environment,

I lca lth, & Natu ra l Resources Solid Waste Management D ivision

ernPLE ANALYSIS REQUEST e State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street


Site Number -------------------------------- Field Sample Number ___ O_I_b_6_'-f.....:'( _________ _

Name of Site S -+ f f' oi--. lj fk~c-l: "). --------------------------~----

Site Location C tJ. {; .. ..~- .. ~J ~ , -----~----------------------

Collected By .S F fo .ti.U.- ( 11 ~;)..._ ... ----------~---------

ID# D ate Collected 1 / · 18/ 'i.j,..__ · T ime ----- --------------------- ------------

Agency: Hazardous Waste Solid Waste .:f::..._s uperfund TCLP Compounds -- --

Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic ---

G0re.r-/ f1 0 ~j l..:fr; 'i Barium

Y:. G round water (1) --

___ Solid (5) Cadmium --'f'c- / :- ) e- •• rfl ' c.{ We.-« Chromium --

__ Surface water (2) Liquid (6) Lead --1/{1--c ,J )~c ~ vJk11? ,A--" -- Mercury

_ Soil (3) ___ Sludge (7) Selenium --

Other (8) ( Y'-<-f 1• ' V O/ (,p .. 1 .. .) Silver

Other (4) ---------

Organic Chemist ry Inorganic Chemistry --Parameter Results (mgjl) Parameter Results (mgjl) WI n • Organic Compounds Results (mgjl)

P&T:GC/MS y. Arsenic L-0, 0 \ benzene --- -- --_ Acid:B/N Ext. >'- Barium o . os -- carbon tetrachloride

MTBE )(. Cadmium .C::..o . a o ?> chlordane -- -- --Chloride chlorobenzene -- -- --

-- X Chromium L..O • 0! chloroform ---- __ Copper o-cresol --

Fluoride m-cresol -- -- --- - Iron p-cresol --

>'- Lead L-O.oo5 cresol -- -- ---- ___ Manganese 1,4-dichlorobenzene ---- _2:_ Mercury ..:::.c. ooo.S -- 1,2-dichloroethane

-- Nitrate __ 1,1-dichloroethylene --'f. Selenium "'-.. 0 • D o.!) 2,4-dinitrotoluene --

7'- Silver .L 0, os __ heptachlor ---Radiochemistry Sulfates hexachlorobenzene -- --

······-··- Zinc hexachlorobutadiene -- --Results (PCi/1) Parameter ___ pH hexachloroethane --

__ G ross Alpha -- Conductivity -- methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- --

TOC __ pentachlorophenol ---- __ pyridine


--- -- trichloroethylene Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol ---- -- __ 2,4,6-trichlorophenol

-- -- -- vinyl chloride endrin --lindane --

Date R eceived Reported by -- methoxychlor __ toxaphene

D~ l c Extracted Date Re0orted 2,4-D

00 857 JAN 20 95' --___ 2,4,5-TP (Silvex)

Da le Analyzed Lab Number DIIS 31'11 (l ~c viscd 2/ Yl)

-----·

l_~ ---·- --- --- -

KC [.l<:panmut ol &vi.roouncat, llult~ •. 1.. ,..;aa .. ral R.aourcu

~.a Wwc MaM,cmcnt D~

SAMPLE ANALi SlS R£Q lit..ST ~'"' ~t:>orawr, o. h10uc hc.a llt>

P.O. Bo• 280ol7, 306 N. Wllm•nron Strut e Ralc•Jh. Nonh Carolina 27611

Fi ld S I N be /S I o "{ ?; P ae amp e um r _______________ _ Sile Number 1J CO 0~ 3 :l~ '1 Cf'-;

Site Location -----------------------------------Collected By.!" fC' ,.,. ,_,~IV ( 11 'b~ ,J ID# ___ Date CoUected ___ 4 __ /_'-l-'-/--~_'7 _____ Time t.l '2-0

Agency: --Hazardous Waste Solid Waste ~Superfund TCLP Compounds --Sample Type Inorganic Compounds . Results(mg/1)

Environmental Con~ntrau Comments Arsenic ---.ss- ~

Barium ---Ground water (1) Solid (5) ..S vJ - 0 Cadmium -=------

Chromium I )( Surface water (2) 8 1\-£:-t.C::. 6 /\.{) .. ""0 ---

-Liquid (6) Lead \. ---..c ... ,..~~ v./e.,..~,._.-

___ Mercury U.Y _Soil (3) _Sludge (7) Selenium --

Silver I -- JPERF '"'-' _Other (4) _Other (8) -- ~

----

Organic Chemistry Inorganic Chemistry ---Parameter Results(mg/J) Parameter R.esults(mg/1) (m&/kg) Orpnlc Compounds Results(m&/1) ~P&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- ---MTBE Cadmium chlordane -- -- --

Chloride chlorobenzene -- --- --Chromium chloroform -- -- --__ Copper o-crcsol -- --F1uoride m-cresol -- --- --

-- Iron p-cresol --Lead cresol -- -- --

-- __ Manganese -- 1,4-dichlorobenzene

-- __ Mercury --- 1,2-dichloroethane

-- Nitrate __ 1,1-dichloroethylene ---Selenium 2,4-dinitrotoluene --- --Silver __ heptachlor ---

Radiochemistry Sulfates hexachlorobenzene -- ---Zinc hexachlorobutadiene --- --

Pcu&tmtlt:r Results (PCI/1) _pH hexachloroethane ---__ Gross Alpha __ Conductivity __ methyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- --TOC __ pentachlorophenol --

--- __ pyridine

Microbiology --- __ telrachloroethylene

-- __ trichloroethylene Petramettr Results (Col/lOOm!) __ 2,4,5-trichlorophenol ---- --- __ 2,4,6-trichlorophenol

-- -- __ vinyl chloride endrin

Lf- 7 ~<ffii-Ropoctod bi/:1:_ L /U&L-1 ~ --lindane Date Received __ methoxychlor

__ toxaphene Date Extractr.:d · Date Repo ted ,)- Y - 9 Y __ 2,4-D .

__ 2,4 ,5-TP (Silvcx) Date AnalyL.r.:d 4 -;a -q L{ 7J..4j- Lab Number 94104.1 --Dl!S 31'11 (Revised 2/ 'll)

'--------

KC. I:k~nmcnt ol Eavirolamcat, J.lcalth; & •Natural Ruoum:s

:Solid Wutc Mana&cmcnt Division

SAMPLE ANALYSIS REQUEST

e State ubora&ol)' ol Public Health

P.O. Box 28047, 306 N. W&lminJton Strut RalciJb, North C:.rolina 27611

Site Number 1J CD 043 3.Z'1 '1'' IS' '10' Field Sample Number, ______________ _

Name of Site s -4-.! ""c'""'J M' ~"1~,.~ 6 Site Location Cit a A~l-"fJ I .ST4 ,lL7

Colleded By..C fC' r"lt ~·~,.., ( J1 't•,., ,.J · ID# ___ Date Colleded. __ 'I_/_Lf--:,/_,_'1 ___ Tune. __ f3_1.o __ _

Agency: _Hazardous Waste _Solid Waste ~Superfund

Sample Type Environmental Concentrate Comments

_ Ground water {1)

)( Surface water (2)

Soil (3)

_Other (4)

Solid <sfJ -.S 'U-.1 - 0 r""

=Liquid (6) LB ~{, ~ v.,J D)

_Sludge (7) ----------

-Other (8) ----------

TCLP Compounds

Inorganic Compounds Arsenic -- Barium - Cadmium - Chromium - Lead Mercury

-Selenium -- Silver

Results(mg/1)

---------------------------~---------------------~------------------------~ - _...;___;_· ----------

Organic Chemistry Inorganic Chemistry

Parameter _Arsenic

Barium --_Cadmium

Results(mg/l)(mK/kg)

_Chloride _Chromium _Copper __ Fluoride _Iron

Lead __ Manganese _Mercury

Nitrate Selenium -t--------------1 Silver

Radiochemistry

Parameter Results (PCI/1) __ Gross Alpha ------

Gross Beta

Microbiology

Parameter Results (Col/100ml)

--Sulfates Zinc -- pH

=Conductivity ------TDS --TOC

---------------

Date Received lf:='f-:et" ~Reported by. _______ _ fesr~ltVA if -H-9f"J't.8D ·

Dale ExtraclcdBNA 4-12-945-'.WG Date Reported. _______ _

I'~~~~ /3,1JA 9 Dale AnalyLcdty~ c./-t.J.-fit.j Lab Number 41042 DIIS 3191 (Revised 2j91)11f> 8& _____ ,..;..;.;.,;;;,..__--:....

--------------Organic Compounds

benzene -Results (mK/1)

_ carbon tetrachloride chlordane ------- chlorobenzene - chloroform - o-crcsol m-cresol = p-crcsol cresol

- 1,4-dichlorobenzene - 1,2-dichloroethane -------- 1,1-dichloroethylene - 2,4-dinitrotoluene ------= heptachlor

hexachlorobenzene _ hexachlorobutadiene

hexachloroethane ------= methyl ethyl ketone -------nitrobenzene = pentachlorophenol

___ pyridine _ tetrachloroethylene

trichloroethylene 2,4,5-trichlorophenol -----

__ 2,4,6-trichlorophenol -----vinyl chloride

--endrin -- lindane = methoxychlor __ toxaphene _ 2,4-D __ 2,4,5-TP (Silvex)

~----------------------------~

- ~ --·--·-- ----~

--

-----~--- ·-~---~------- -·------.._ --... ~---4-

r-.:.C: Dcpanmcnt ol E-iroarncat. I lc~lth, & Natu~l Raou~

Solid W~c Maru1cmcnt Div\Uon

.4.MPLE ANALYSIS REQUEST e Sate l.aboraa.ory ol Pvblic Health P.O. Box 28047, 306 N. Wilmin~ton Stn:ct

RalciP~, Nonh Carolina 27611

Site Number 1-J GD 0~ 3 :1~ '1 Cf'' Field Sample Number __ l_~_,_fa_y _________ _

Name of Site .f -#o..{ "'-~~~1..-.f Site Location c /'1 a A (L ~ .... j I ST., ,J ~....,

Collected By....r fC" r-tt ~,q:_,...., ( 11 't' ,.J ,.J IDl¥ ___ Date Collected __ 4_/_4_/_1_'i ___ Tune I 3 1o

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results (mg/1)

Environmental Concentrate Comments Arsenic --Barium

_Solid (5) __(( ---._( \l..J -or- --__ Ground water (1) Cadmium --(o ~~ur--o .,~v Chromium

X Surface water (2) --

-Liquid (6) Lead --__ Mercury _Soil (3) _Sludge (7) Selenium --

" Silver --_Other (4) _Other (8) ---- .. --

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter IWults(mg/1)" z'lill) Organic Compounds Results(mg/1) _P&T:GC/MS X Arsenic L__o.=\ benzene --_ Acid:B/N Ext. ~Barium 0-03 carbon telrachloride --MTBE ...JLCadmium .L_o . Q o ..;;l,. chlordane -- --

Chloride . chlorobenzene -- --Y- Chromium -- .L...o-O\ chloroform --__ Copper o-cresol -- --

Fluoride m-cresol -- -- ---- Iron __ p-cresol --

1_Lead Lo .co5 cresol -- ---- __ Manganese 1,4-dichlorobenzene ---- 1::._Mercury .L. 0 - 0 Q;;;2 s 1,2-dichloroethane ---- Nitrate __ 1,1-dichloroethylene --

~ Selenium .L..,a_oo5 2,4-dinitrotoluene --_L Silver .L...o.os __ heptachlor

Radiochemistry Sulfates hexachlorobenzene -- --1:._ Zinc .L.o.oS hexachlorobutadiene --

Pardmeltr Results (PCI/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- --




-- -- __ vinyl chloride endrin --lindane --

Date Received Reported by __ methoxychlor __ toxaphene

D:.~tc Extracted Date Reported a_~~ v "f( 2,4-D --005710 APR 8 9 _ 2,4,5-TP (Silvex) Dale AnalyLcd Lab Number DIIS 31~1 (Revised 2/Yl) --

--------~~~~-- - - ------- ---~------

N.C. tie.panmcnt ol ~meet, llcalth: 1.:. .Natural Resources

:~id Wwe Manascment Division


e S«atc Laboratory of Public Health

P.O. Box 28047, 306 N. WilminJton Str.:tl Raleich, North Carolina 27611

Site Number 1J CD 04 3 ~~ '1 ~'' · Field Sample Number. __ IS __ -,_0_7.;.._ _______ _

Name of Site S -4-.! l'ooi:T4 L.-J fL€ e,"f~,,,.J 6 . Site Location Cit a /tfl-~"fJ /..ST4 ,l'-7

Collected By..r fC' rtr ~·<.£tv I"" ft:,,J ,.J ID# Date Collected Lf/Lf/,'1 TUDe

. Agency: _Hazardous Waste _Solid Waste ~Superfund TCLP Compounds

Sample Type Inorganic: Compounds Results(mg/1) Environmental ton~ntrate Comments Arsenic - Barium ~ Ground water {1) _solid (S)Y-..rE'D- os- - Cadmium -

(B ~vv-£,~k.Jt;>l Chromium -~ Surface water (2) _Liquid (6) Lead

_Mercury _Soil (3) Sludge (7) Selenium - Silver X Other (4)Stt>lf'\E..,I -Other (8) ---Organic Chemistry

' Inorganic Chemistry -

Parameter Results(mg/1) Parameter llesults(mg/l)(ml/k&) Orpnlc Compounds Results(mg/1) X P&T:GC/MS Anenic benzene - -_ Acid:B/N Ext. Barium carbon tetrachloride - -MTBE Cadmium chlordane - - -Chloride chlorobenzcne - - -Chromium chloroform -

=Copper -- o-cresol -F1uoride m-c:resol - -- - p-cresol -- Iron - Lead cresol --- =Manganese = 1,4-dichlorobenzene

- _Mercwy _ 1,2-dichloroethane

- Nitrate _ 1,1-dichloroethylene - Selenium _ 2,4-dinitrotoluene - Silver _ heptachlor -Radiochemistry Sulfates hexachlorobenzcne - -Zinc hexachlorobutadiene -Parameter Results (PCI/1) hexachloroethane _pH _ Gross Alpha __ Conductivity = methyl ethyl ketone

Gross Beta TDS nitrobenzene - - = pentachlorophenol TOC -- pyridine

Microbiology - _ tetrachloroethylene

-- · trichloroethylene Parameter Results (Col/100ml) _ 2,4,5-trichlorophenol - 2,4,6-trichlorophenol - - - vinyl chloride -- - endrin -

Lf-7-9c,r llhReported by lindane

Date Received = methoxr,chlor __ toxaphene

Date Extracted Date Reported 2,4-D

Date AnalyLCd 4-J.;;}-9l-/Tll1rLab Number 941043 = 2,4,5-TP (Silvex)

DIIS 31!.11 (Revised 2/91) --

N.C. pc.-nmcftl ol ~ llcaltt-., ~ Natural ~rca

$.)lid Wau:: ManaJCIIICIU DMaiOII

SAMPLE ANALYSIS REQlJE.ST Stat.c Laboratory o! twbbc Hcallb

P.O. Boa: 210C7. 306 N. WilminJlon Strut e Rakip. North Carolina 27611

Field Sample NumbCr __ ,...c __ ,_o_? ________ _ Site Number 1J CD 0~ 3 .l.l '1 ~ ''

Name of Site .f ~.! ,...;-7"~h ... .f . Site Location cIt a A~~--.. J /.ST ~ ,l L'f

Collected By..!" fC' ,.,. ,...<,£,., / ~ ~·"' ,J JD# Date Collected 'I / L( / 1 '1 Tune ----- ·~=====·====~~======~ . Agency: _Hazardous Waste _Solid Waste ~SuperfuDd

Sample 'I)'pe Envlrnnmrntal Concentrate Comments

_ Ground water (1}

~ Surface water (2)

_Soil (3)

_ Solid (S)S! - ..f E1) - 0 !:.-

_Liquid (6) ~ 1'\~G~"t;t>J Sludge (7) _________ _

X Other (4).SE.t>ti"'E"'I_ Other (8) -----------

TCLP Compounds

lnorpnlc Compounds _Arsenic

Barium~ - Cadmium - Chromium - Lead =Mercury

Selenium - Silver

Results(ml/1)

-------------r------------------~------------------------~ ----------------------------Inorganic Chemistry · Organic Chemistry -------------~-----------------------~------------------------~

Radiochemistry _Sulfates --------------------1 Zinc

Parameter Results (PCI/1)

_Gross Alpha ------Gross Beta

_pH

--Conductivity -----TDS TOC

r-------------------------~--------Microbiology

Parameter Results (Col/lOOm!)

---- -----

Date Received Lf ~7-9ft t,hReported by _________ _

PCB1<!-Ibr '1-11/-91/1/1?-Date Exlractcilt;NA 4-14-q4 5\ Date Reported. _______ _

. $M /-'e-sr.r,~-/'M/ Date Analy~d1t..f-?iW ~-15=-W Lab Number 9~ 1044 I>IIS 31~1 (Revised 2/91 "Y/' __ __;_....;;;;...;~::......='----

Orpnlc Compounds benzene -

Results(ma/1)

_ carbon tetrachloride chlordane -------_ chlorobcnzene chloroform - o-cresol m-crcsol

- p-crcsol cresol

- 1,4-dichlorobenzenc - 1,2-dichloroethanc ------= 1,1-dichloroethylene

2.,4-dinitrotoluene ---------- heptachlor _ hcxachlorobcnzene _ hexachlorobutadiene

hexachloroethane ------- methyl ethyl ketone

nitrobenzene ------- pentachlorophenol __ p)Tidine

tetrachloroethylene _ trichloroethylene __ 2.,4,5-trichlorophenol -----__ 2.,4,6-trithlorophenol ------

--vinyl chloride endrin lindane = methoxychlor toxaphene 2,4-D = 2,4,5-TP (Silvex)

~----------------------------~

.

--- ---------· ·- - --- -·

.r-:.c Dcpanmc.ac o1 ~ llcahh, I;. Natural Raourna

SQiid Wu&C Mana~ 0i¥i1ioa

. . --- ---- ... ---- - -·

SAMPLE ANALYSlS REQUEST

e . S&&&& Ubor.&Oiy ol !"uoi.tc HC&IUI

A . P.O. Boz 1mC7. 306 N. W"llmiftJ!OII Slrcct • Rakip. Notth CaiOIUM 27611

Fadd~p~Num~ __ ~/_,_,_b_s-______________ __

Name of Site S ~.! ~t:T~L-.f rz.E" P-te."•"' 6 . Sitel.oc:atio~ C/IO/t~J.."fJ /.ST~,l'-7

Collected BY....CWC' ,..,~,(£~'>' /11 '=•~ ,J ID# Date Collected '1/Lf/''1 .. Agency: _Hazardous Waste _Solid Waste ~Superfund TCLP Compounds .. .. . .

Sample '.J)'pe . .. Jnorpnlc Compounch Results(m&/1) Envirnnmental ~on~ntrate Comments Arsenic - Barium

_ Ground water (1) _Solid (~-scp -OJ - Cadmium -l@ ~ '-1<=-&~vo,JD} Chromium -___:_ Surface water (2) Liquid (6) Lead '· -Mercury

_Soil (3) Sludge (7) -Selenium - Silver X"Other (4)SEb11"'E..,I_ Other (8) ----·Organic Chemistry Inorganic Chemistry -

Parameter Results(ml/l) Parameter Results~(m&/k&) Orpnlc Compounch .Results(me/1) _P&T:GC/MS ~Arsenic .5<J benzene -~ Acid:BfN Ext. :K Barium r.j- - carbon tetrachloride

MTBE "1( Cadmium ;a chlordane - - -Chloride chlorobenzenc - X.. Chromium 1/o - chloroform - -- _Copper o-cresol -Fluoride m·cresol - - =~cresol - Iron

- xLead ~0 cresol

- _Manganese = 1,4.dichlorobenzeue

- ~Mercwy ~o.:;;;.;~ _1,2.dicbloroethane

- Nitrate _ l,l·dichloroethylcnc X Selenium L..\ _ 2,4.dinitrotoluene

>< Silver < IO _ heptachlor -Radiochemistry Sulfates hcxachlorobenzcne - -X Zinc .C::t hcxachlorobutadicne

=pH -Parameter Results (PCI/1) hexachloroethane

__ Gross Alpha _ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene - - - pentachlorophenol TOC -

- pyridine Microbiology - _ tetrachloroethylene

trichloroethylene -Pnameter Results (Col/lOOml) 2,4,5-trichlorophenol ~ - __ 2,4,6-trichlorophenol -- - _ vinyl chloride

cndrin - lindane Date Received Reported by = methoxychlor

__ toxaphene D:1le Extracted Date Regrted 2,4.0

00 712 APR 8 Y4 - 2,4,5-TP (Silvex) Dale Analy.tcd Lab Number I>IIS 3191 (Revised 2tH) -

t".C.Ocpanmcat ol &Mroamcac. llcalCII. I. Natunl RaourtU

· • Solid Wwc ManaJC_mcat_r:>M&ioa

SAMPLE A.:"ALYSlS REQU£ST ~Le I.Abora&Ol)' ol tuouc hullh

P.O. Box 21047,306 N. W"almiaJ1on Strut e Ralcip, Nonh Carolau %7611 ''

Fi d 1 N be iS" I o '1 c 5 t I IS ael Samp e um r. ______________ _ Site Number 1J CD Oe; 3 ~.I '1 ~''

Site Location Cit a lt,..l-t~tJ /.JT~ ,lL'/

Colleded By..!'~ ,. .. ,_,~,.., /11 '=•"' ,.J IO# Date Collected. Lf /Lf_/ ''-1 Tame

Agency: _Hazardous Waste _Solid Waste )(. Superfund - TCLP Compounds

Sample 'I)pe Jnorpnlc Compounds Results(mg/1) Environmental ~on centrale Comments Arsenic - Barium

_:___ Solid (S).SJ - ..S ..U - Db . _ Ground water (1) - Cadmium --Liquid (6) ( j3JC. i3tl'rf- C.~ I'-)

Chromium )( Surface water (2) - Lead

-Mercury _Soil (3) _Sludge (7) -Selenium - Silver -_Other (4) Other (8) -- --Organic Chemistry Inorganic Chemistry -Parameter Results(mg/1) Parameter Results(mg/l)(ma/k&) Orpnlc Compounds Results{ma/1) X P&T:GC/MS Arsenic benzene - -_ Acid:BfN Ext. - Barium - carbon tetrachloride

MTBE Cadmium chlordane - - -Chloride chlorobenzcne - - -Chromium chloroform - - -- _Copper o-cresol -Fluoride m-crcsol - - - p-crcsol - - Iron Lead cresol - - = 1,4-dichlorobenzcne - _Manganese

- _Mercury _ 1,2-dichloroethane

- - Nitrate _ 1,1-dichloroethylene Selenium _ 2,4-dinitrotoluene -- Silver _ heptachlor

Radiochemistry - Sulfates hexachlorobenzcne -Zinc hexachlorobutadiene - -Patrameler Results (PCI/1) _pH hexachloroethane __ Gross Alpha _ Conductivity - methyl ethyl ketone

Gross Beta TDS -- nitrobenzene -- - = pentachlorophenol TOC -- pyridine Microbiology - _ tetrachloroethylene

_ trichloroethylene -P~rameter Results {Col/lOOml) _ 2,4,5-trichlorophenol -- - _ 2,4,6-tricblorophenol

-- - _ vinyl chloride endrin --

L.f-74cr ltb lindane

Date Received Reported by _ methoxychlor toxaphene

Date Extracted Date Reporled _2,4-D

D~tc Analy-'t:d lf-;J,;J _q L/ nw- Lab Number 9L11Q£\5 __ 2,4,5-TP (Silvcx)

J>IJS 3191 (Revised 2/91) --

t.:.C. [)epanmcJtl ol r:-uo.JDCat., llcaltti. 1.: 1\:atural RaourtU

· .Solid \l.:.uu'ManascllftCat DM&ioft

SAMPLE ANALYSiS REQUEST ~IC l.aboralOI)' ol l-uDuc hc.&ILh

P.O. Box ZBOC7, 306 N. W"alminJlon Slrut e Rakip. NotUI Carolau 27611

Site: Number 1J CD 0t;3 3Z'1 Cf ' ' Is 1 I\ ·. · Field Sample Number. __ ;..... ___________ _

Name of Site S ~.! "'i"T~a....r Site l..o?tioD Cit a lt~l-"fJ /.ST~ tl'-7 . ~c. co,,-

Collected By~~ ,.,. ~·~"" ( ., '=•"" ,J · IDtl' ___ Date CoUectcd. __ Lf_.;./_4_:../_,_'1 ___ T'amc:_1_~_.r:_s-__ . Agency: _Hazardous Waste _solid Waste ~Superfund TCLP Compounds

Sample 'I)'pe Inorganic Compounds . Results(ml/1) Envirnnmental Concentrate Comments Arsenic -

Solid (S) ..s.r- S "'-'- 0 6 Barium -_ Ground water (1) Cadmium - - Chromium )( Surface water (2) _Liquid (6) (81{, BE~,._. c.~c<) - Lead

-Mercury _Soil {3) _Sludge (1) -Selenium - Silver -_Other (4) _Other (8) -- -

·organic Chemistry -Inorganic Chemistry -Parameter Results(ma/1) Parameter Raults(m&/1) (ml/ka) Orpnle Compounds Results(ma/1) ~P&T:GC/MS Arsenic benzene - -_2L Acid:BfN Ext. Barium carbon tetrachloride:

MTBE - Cadmium - chlordane )( p~qtctllf./t~B - -Chloride chlorobenzcnc:

~AI - - chloroform <t?.O~i?/ Chromium - -

<'O.t:~dt?/ _Copper o-cresol

- ~~bW~ --<d • Oe?~ .:Z... Fluoride m-cresol - = p-cresol ~~A~,,~/y~~O~d#/ - Iron

_ 70KA~HO/IE' 4f:t?.I!IP..2.. Lead cresol - = 1,4-dichlorobcnzcnc: l'!li/~ .. ~uc: <:o,/?1?#~ _Manganese -y,_ .,.A,,.f,/._.. <t?.t717'/ _Mercury _ 1,2-dichloroethanc:

~ ~ ~<17~1?017/ - Nitrate: _ 1,1-dichlorocthylene

- Selenium _ 2,4-dinitrotoluenc: Silver _ heptachlor -Radiochemistry - Sulfates hcxachlorobcnzene -Zinc hexachlorobutadic:nc:

Parameter Results (PCI/1) - --_pH hexachloroethane _ Gross Alpha Conductivity = methyl ethyl ketone

Gross Beta TDS nitrobenzene: - - -- pentachlorophenol - TOC

-- _pyridine: Microbiology - _ tetrachloroethylene

- trichloroethylene: Parameter Results (ColflOOml) __ 2,4,5-trichlorophenol - 2,4,6-trichlorophenol - -- - - vinyl chloride

endrin -Date Received :t-7-<ffe"(- Reported by

lindane = methoxychlor {!~;.sr•l't!IJI ~-1. -~l."t/e-JJ _toxaphene

D:stc ExtractcdfNA4-I2.C14S'A.W(., Date Reported 2,4-D

~~ 8}/11 9L}~1046

= 2,4,5-TP (Silvex) Dale Analya:d't-U-?# 1.-1.3-9'1 Lab Number I>IIS 3191 (Revised 2/Yl)P/) 84 --

... ,

~ . -------------------- -· -------·····- . -·. ·- ··-··---- _________ ..,. ___ ---------- ------- ' . • ~.t Ocpen-.t ol ~ llcalth. £: Natural Raooucu ~ Wu&.c M&nascii'ICat Divilioa

SAMPLE ANALYSIS REQUEST e e Sl.&~ l.abora&ary ol hoolac Hc.&UII

1'.0. So& 230C7, 306 N. W"almin"on Strcct . RakiJtl, Nonll Caroliaa 27611

Site Number . 1J CO 04 3 ~Z '1 ~' ' Field Sample Number __ J_b_,_6_l> ________ _ . . .

Name of Site S -~>.! "'i1"""J . M' ~~,,,1 6 Site J..ocation cIt a A f- ,_ ... J I ..ST If ,l L'!

:.: Colleded By..!'~ ,. .. ~,GC;~ (Jot~·"" ,J ID# Date Colleded. 1./ /Lf/_ ''i Tune I:? S ..r

Agency: _Hazardous Waste _Solid Waste ~Superfwsd TCLP Co~pounds .. . .. ·:\·, .. : .; .. Sample 'I)'pe laorpnlc Compounds Results (mg/1)

.. Environmental Conqntrate Comments Arsenic -

_solid.(5) s..r-.SvJ -o& Barium -_Ground water (1) Cadmium - Chromium. --X Surface water {2) _Liquid (6) {31 b (]£ ....... ~ 1'-K.. Lead

-Mercury _Soil (3) _Sludge (7) --Selenium -.. Silver -_Other (4) _Other (8) -- --Organic Chemistry Inorganic Chemistry --Parameter R.esults(mi/1) Parameter Raults(m&/I)Cal'ill' Orpalc Compounds Results(ma/1} _ P&.T:GC/MS )( Arsctlic ~o .. ol benzene -_ Acid:B/N Ext. ~Barium o.o~ carbon tetrachloride -MTBE ...JL Cadmium L. 0. 0 Q.:l.. chlordane - -- Chloride. chlorobcnzcne ->'-- Chromium - .L...0-01 chloroform -- _Copper a-cresol -- Fluoride m-crcsol - - p-cresol - Iron

- .:i:._ Lead Lo-goS cresol -- _Manganese _ 1,4-dichlorobcnz.cnc

- LMerauy ""-o.oaaS _ 1,2-dichloroctha.ne

- Nitrate _ 1,1-dichloroetbylene ~ Selenium L..O- coS _ 2,4-dinitrotoluene

LSilver L..o.o~ heptachlor Radiochemistry Sulfates hexachlorobenzcae -LZinc """'-o-oS hexachlorobutadienc -Parameter Results (PCI/1) _pH hexachloroethane

_ GrosS Alpha • __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene - - - pentachlorophenol TOC -

- pyridine Microbiology - tetrachJoroethylene

- _ trichloroethylene Parameter Results (ColjlOOml) __ 2,4,5-trichloropheaol - 2,4,6-tric:hlorophenol - -- - _ vinyl chloride

endrin -- lindane Date Received Reported by =methoxychlor

_toxaphene D:~te Extracted Date Reported _2,4-D

005711 APR 8 94 _ 2,4,5-TP (Silvex) Date AnalylCd Lab Number J>IIS 3l'Jl (Revised 2/Yl) --

I I

1\:.C..Ocpanmcat ol ~t. llcalth, ,.. Natural Raourcu

~JI;cs Was&~ NanaJCme•t Diwilion

SAMPLE ANALYSlS KEQ UE.ST

Site Number 1J CD 0~ 3 3.I '1 ~''

~LC Latlora~1 ol twb tC U.llll

P.O. Be¥ :$)47. 306 N. WdminJton Street e Ralcip. North Caroliaa 27611

Field Sample Number __ .... t_.s-___ -, __ 1 '1.----------Name of Site S -~'.! "-~T~L.-J . Site l..oation C/1 a A~~"tJ /.ST~ ,lL'7

Collected By..r re' ,.,. 1-•Ci.tv (., ~·,J ,.J ID# ___ Date CoUected. __ LI_/_Lf_/;,_...,_'1 ___ Tame I:] S'S'

. Agency: _Hazardous Waste _Solid Waste ~SuperfuDd TCLP Compounds ... ..

Sample 1)pe Jnorpnlc Compounds Results (m&/1) Envlrnnmrntal ~oncentrate Comments Arsenic - Barium

_Solid (S) ..('J -.5 fV- 0 b -_.._ Ground water {1) - Cadmium

{g,~:, c3 C' .4\ /l.. c.,c-('(.) - Chromium __:_ Surface water {2) _Liquid (6) Lead

=Mercury _Soil (3) Sludge (7) Selenium -X Other (4)S£t>lf'\E..,tl_ Other (8)

Silver -----Organic Chemistry

' Inorganic Chemistry -

Parameter Results(m&/1) Parameter Raults(m&/1) (ma/k&) Orpnlc Compounds Results(me/1) X P&T:GC/MS Arsenic benzene = Acid:B/N Ext. - -Barium carbon tetrachloride - -MTBE Cadmium chlordane - - -- Chloride chlorobenzene -- -Chromium thloroform - -- _Copper o-aesol -F1uoride m-cresol - - =p-aesol - Iron - Lead aesol --- _Manganese = 1,4-dichlorobenzcne


- Nitrate _ 1,1-dichloroethylene - Selenium _ 2,4-dinitrotoluene - Silver _ heptachlor --Radiochemistry Sulfates bexachlorobenzene - -Zinc hexachlorobutadiene -Parameter Results (PCI/1) pH hexachloroethane Gross Alpha __ Conductivity - methyl ethyl ketone = Gross Bt'ta TDS - nitrobenzene. .. --TOC _ pentachlorophenol -- _pyridine

Microbiology - _ tetrachloroethylene · _ trichloroethylene - -

Parameter Results (Co1/100m1) _ 2,4,5-trichlorophenol -- - _ 2,4,6-tricblorophenol

- - _ vinyl chloride endrin -

·'4-- 7-4v AhReported by lindane

Date Received - methoxychlor - . _toxaphene

Dale Extracted Dale Reported _2,4-D

Dale Analy.a:d I..J- il:J-91-J 77ltr"'l.ab Number 9lJ104? _ 2,4,5-TP (Silvex)

--I>IJS 31'JI (llc:viscd 2/91)

f'.C. Dcpanmcnt or Enviroemcat, .llcaltl'., &.. Natunl Raourcu

. ·Soiid Wutc Manascment DMsion


e Slate Labontory oC Public Health

P.O. Box 28047, 306 N. Wilminrton Street Raleia;h, Nonh Carolina 27611

Site Number 1J CD 0~ 3 .l.I '1 ct'., Field Sample Number __ ,.r-_·_7_1_3 ________ _

Name of Site S -~'.! ""E"T"a....t M" e-t-f~,,~ 6

Collected By..!' P: ,.., ,.,~,.., ( ~ '=•,., ,.J ID#

. Site Location C/1 a /tfLI-,_,J /.ST4 ,JL7

Date Collected '1/Lf/,'f Tune

. Agency: _Hazardous Waste _Solid Waste ~Su~rfund TCLP Compounds

Sample Type Inorganic Compounds Results (mg/1) Environmental Concentrate Comments Arsenic -

_Solid (5) .SS-.S ~ -Db Barium -_Ground water (1) Cadmium -

e• t:. Ge"f~ c:::HL) Chromium -___:_ Surface water (2) _Liquid (6) Lead

-Mercury _Soil (3) _Sludge (7) -Selenium - Silver X Other (4)SEt>I,.,EtJI _Other (8) -

---Organic Chemistry Inorganic Chemistry -

Parameter Results(mg/1) Parameter Results(mg/J)(ma/kl) Orpnlc Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene - -X Acid:B/N Ext. Barium carbon tetrachloride - -MTBE Cadmium chlordane X t'G~flc.IPE: I Pe'€ - - chlorobenzene Chloride

-Chromium -_JOaB_:t < p ./ p I)!!./1'L chloroform _eocd&iJ <"'_g.u'/v,AI\. =Copper - o-cresol -bNt:IAA!E <t::J,.:J.b ,!JP.h'o. Fluoride m-cresol _LJrl.ft:>xycA/LR-<" /. ~e.e.M..... -Iron _ p-cresol

-~#eye -c,:J....,t71¥""'- -Lead cresol

-~~~~ <d·~J-- --Manganese = 1,4-dichlorobenzene ' ch'.., -:-p. / ;;r:, _ _..... -Mercury __ 1,2-dichloroethane

~ACA/~tretP~e-:b.·l, ..!NJ/1 -Nitrate _ 1,1-dichloroethylene ,, r-- Selenium _ 2,4-dinitrotoluene - Silver _ heptachlor -Radiochemistry Sulfates hexachlorobenzene - -Zinc hexachlorobutadiene =pH

- hexachloroethane Parameter Results (PCI/1) _ Gross Alpha _ Conductivity - methyl ethyl ketone '

Gross Beta TDS nitrobenzene - -- -- pentachlorophenol TOC -- pyridine

Microbiology - _ tetrachloroethylene __ trichloroethylene ' -Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol - 2,4,6-trichlorophenol - - - vinyl chloride - - endrin --

lf-7-11{ Ub lindane

Date Received Reported by = methoxychlor

~/hr ~-1~-9{/"J(P __ toxaphene Date Extractcii RN~=-C.t:H ~- - Date Reported 2,4-D

8/JII p.:-.;n-~ee; 9~1048 = 2,4,5-TP (Silvex)

Date Analyu:d1'tS: # '1-l.s-'lt/ Lab Number DIIS 3191 (Revised 2/91VJ() if}' -

·- - ··-- -~---------------~·--···---··----··-·-· ·-

"r-:.t:. Ocpartmc.al ol Ea¥iroameat. llcalth.ll. Natunl R.l:aourt"CS

Suli4 Wuu Mana&emciU OMsion


e. -· S&atc LabonCOiy oC Public Health P.O. Boz 280C7, 306 N. W"dmin&'loc Street

· · Rakip. Nortb Carolina 27611

Site Number 1J CD 0413 ~:!'1 q"' Field Sample Number _____ ._· _f_{,_~ _6 _7 ____ _

Name of Site S --~'.! ""i:T~L-J M e,'-fec,a,J 6

. Collected By...C~ ,..,,..,~"' ( 11 !:•,_~ ,J ID#

. Site Locatio~ cIt a It~,_ ... J /.ST ~ ,l L'!

Date Collected Lf/Lf/''1 Tunc /3S"".J

. Agency:. Hazardous Waste Solid Waste Lsu~rfund TCLP Compounds ..

Sample Type . Inorganic Compounds Results(mg/1) Environmental ~on centrale Comments Arsenic - Barium -_ Ground water (1) Cadmium _Solid (S) -

_ Uquid (6)S,.r-.rEi)- ()' Chromium -__:_ Surface water (2) Lead

lf'l:> SE~<tt- o-t<} -Mercury

_Soil (3) Sludge (7) -Sdenium - Silver X Other (4)SE.1>ti"\E""I_ Other (8) --

--Organic Chemistry Inorganic Chemistry -

Parameter Results(mi/1) Parameter R.esults~(mi/ka) Orpnlc Compounds Raults(mg/1) _P&T:GC/MS ){ Arsenic .3-2 :t benzene

7 -~ Ac:id:BfN Ext. Barium carbon tetrachloride T -MTBE Cadmium < /0 chlordane - -Chloride chlorobenzene - """5C:"" Chromium z~ - chloroform -=Copper

- o-acsol -- --Fluoride m-acsol - - =p-acsol - Iron xLcad ¢.o cresol -- -Manganese -- _ 1,4-dichlorobcnzene

- ~Mercury -'-o .... c:::J _ 1,2-dichlorocthane

- Nitrate 1,1-dichloroethylene ~ Selenium ..Z\ 2,4-dinitrotoluene X Silver <Zo - heptachlor --Radiochemistry Sulfates hcxachlorobenzene

X Zinc -2-Cf hcxachlorobutadiene -pH - hexachloroethane Parameter Results (PCI/1)

__ Gross Alpha _ Conductivity --methyl ethyl ketone Gross Beta TDS - nitrobenzene -- -- - pentachlorophenol TOC -- pyridine

Microbiology - _ tetrachloroethylene

- trichloroethylene Parameter Results (Col/lOOmJ) _ 2,4,5-trichlorophenol -- - _ 2,4,6-trichlorophenol

-- - vinyl chloride endrin - lindane

Date Received Reported by = methoxychlor _toxaphene

Date Extracted Date Reported _2,4-D

005713 APR 8 94 2,4,5-TP (Silvex) Date Analya:d Lab Num er Ill IS 3191 (Revised 2/91) --

N.C.· Dcpanmcnt ol Envirollmcat,

I !~lih, & ~at ural Resources • ·Solid Wu&e Mana,emen& Divi5ion

SAMPLE ANALYSIS ·REQUEST

e State lAboratory ol Public H~hh

P.O. Box 28047, 306 N. WilminJtori Street !Uieip, North Carolina 27611

Field Sample Number __ I_S_'l_1_'1 ________ _

Name of Site S _,,s "'6"1"".f M" ~~~"',J 6 Site Location C/'1 a Afl.~"'fJ I S'T"-4 ,lL7 cu; ~c..

Collected By..r r::'" ,.,. ~·~"' ( 11 '!::•,., ,.J ID# ___ Date Collected __ 'l_/_4_;/;_,_'1 ___ TllDe -rl'-'cl ~ L4 ,J,L.

Agency: _Hazardous Waste _Solid Waste ~Superfund TCLP Compounds

Sample 'JYpe Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic --

Bt... .. rJ f<. Barium

·~l t' -__ Ground water (1) _Solid (5) Cadmium -- Chromium )( Surface water (2) -_Liquid (6) Lead

Mercury _Soil (3) _Sludge (7) -Selenium - Silver --_Other (4) _Other (8) --

-- .. --Organic Chemistry Inorganic Chemistry -Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) X P&T:GC/MS Arsenic benzene - -_ Acid:B/N Ext. Barium carbon tetrachloride -- -MTBE Cadmium chlordane - - -- Chloride chlorobenzcne - -- Chromium chloroform -- -- _Copper o-cresol -- Fluoride m-cresol -- -- p-cresol - -- Iron

- Lead cresol -- _Manganese __ 1,4-dichlorobenzene


- Nitrate 1, 1-dichloroethylene - Selenium 2,4-dinitrotoluene -- = heptachlor Silver --Radiochemistry Sulfates hexachlorobenzcne - -Zinc hexachlorobutadiene Parameter Results (PCI/1) =pH

- hexachloroethane __ Gross Alpha __ Conductivity -- methyl ethyl ketone - .

Gross Beta TDS nitrobenzene -- -- -- pentachlorophenol TOC ---- __ pyridine

Microbiology -- tetrachloroethylene

-- __ trichloroethylene Parameter Results (Colf100ml) __ 2,4,5-trichlorophenol -- 2,4,6-trichlorophenol - -- - vinyl chloride -- -- endrin --

/f- 7-7<{ /th Reported by lindane

Date Received _ methoxychlor _toxaphene


4-d;)..-9'/71urLab Number 9410l~9 _ 2,4,5-TP (Silvex)

Date Analylcd DIJS 3191 (Revised 2/91) --

•• : •• •• -··-·-..;..._ _____ :_- ._, + --"---- --·-----··-·~:._:~~;-.:..~~::::_~·=-'-·-~~~_:_r_~,:__:~~--~~":...'....;...• ...., .. · .......... ~'""'++;,;,....,; ...... -~~~-~-;.,~,.-,...a'""_"'" ..• ...,··~;~ .... -> ............ · ·...,;-• ·.~n"":(·;L;;J~r.s...s:·:..brb.Lil.iio~i.+,2,t.-.. · ··--·-.. ·------ -------.-, -------~_ .. :····-----·- . . -·---- ··-.. --- -·----;-:--- -··

H

STATE LABORATORY OF POBUC HEALTH PO BOX 28047- 306 N. WILMINGTON ST •• RALEIGH. NC 27611

ORGANIC CREMTCALANAL'YSIS

.PURGEABLE COMPOUNDS LAB NO qlf/O'l( FIELD NO 157o'-/

COMPOVlVD ''• TYPE ( .,2 )

UNITS @pgf"q

CBLOROimTHAI'(!; dDwb lJ.-.

VINYL CBLORIDE 10 BROIIOM!:THAll!: J.o CBLOROI!:'I'IIA!m 10 TRICBLOROJI'UI'ORO~ 10 ACZTOZO: 50 l,l•DJCBLORO!:THER !5 JODOJa:1'HAlfl: 10 JO!:TJITIZZO: CBLORJDE 5 CARBOI'r DJSULFIDE \ TRAlf9-1,2·DICBLOROII!:Tlml'l!: 1/ ACRYI.Oifi1'JUI.E d00 l,l•DICBLORO!:THANJ!: 5 2·Bt1T.AI'rOZO: !50 CJ9-1,2·DICHLOROII!:Tlml'l!: .!5 CHLOROFORM

l,l,l·TRICHLOROI!:'I'IIA!m ,lj

CARBO!f TETRACHLORIDE 10 BE:fZ!:ZO: 5 l,2·DICBLORO!:TJIAKE

TRICBLOROI!:'I'IIA!m

l,2·DICBLOROPROPAN!: ... /

BROIIODICHLOROMETHA%'1'!; 10 "v

fMDLf e- QaU:G-AcUr-lO P~E'IIIT IN t.A6 BI.J:It-1~ • J - Estimated value

q'{-J0'/3 1570?

( lf ) pg/1€iftj}

I)_.

,y

X - Actual value is known to be leaa than T&lue given. L - Actual value is known to be greater than T&lue given.

qi.JI0'-15 J57o Cj

( ~)

~/kg

LA-

... J

94/0if 7 q'f /OJ.fCJ t57J~ J5 7 JL/

( Lf) ( ;;.. )

pg/1~ I(Pi~Y pgf"q

t..L- {..1-

. .

... / ,v

U - Material was analynd for but not detected. 'rha number is the llinimum. Detection Limit. HA - Rot analyzed. 1/ - Tentative identification. "fil - 011 R'I\DC List of Priority Pollutants. fi - C:olllPouND REUABLY :bETECTABU: CNLY AT lfiG-H CDNc£1\lTf!ATIC~:S • c. - P~•Bl.E. LR& CoNT'~MI~A"t'lotJ,

DEBNR 3065-0 (10/93) ·

( )

pg/1 pg/"q

PURGCOH.ORG

,_ .... ,,:, .... ·: ·.

-·-·-·-·· . ··-··· ···---- --- --··-·-··--------_;_ ..

H .~ H ·.• ' -~

:j !

H H

. ! STATE lABORATORY OF PUBLIC HEALTH I !

PO BOX 28047- 306 N. WILMINGTON ST •• RALEIGH. NC 27611

I ORGANIC CHEMICAL ANALYSIS

PVRGEA.Bl.E COMPOUNDS LAB NO C}LJJCJ41 qL.JIOLf3 q'-{ JOLJ-5 q '-1-1 ott? qt.JJO'fq ... FIELD NO 1670~ 1!5 707 J570CJ J 57Jd. 157J'/-

COMPOUND TYPE ( ~) ( l-1 ) ( ,;2_ ) ( lJ,:.) ( ;2.)

UNITS ~/kg p.g/1~ ~kg pgfliift?; i~/kg DIBROMOII!:THANJ!: JSnnb LL LA- LL u_ V-

4-JBTHTL-2-PENT.ANONE .5o ClS-1,3·DICm.oROPROPENJC ~ TOLm:tu::

I

TRANS-1,3-DICm.oROPROPEtu:: \I/ . . 1,1,2.2-n:TRACm.oROJ!:THAIU: Jo

1,1.2-TRicm.oROJ!:THAIU: !5 2-JmXAKONE 5o TETRACm.oRO!:TB!:NE 5 DIBROMOCm.oROJa:THAlfE JD ETHTI.Ztu:: DmROMIDE 5 CHLOROBENZ!:I'fE J, 1,1,1,2·TETRACm.oROETHAl'f!: ID ETHYL BEn'z:r:NE !5 XYL!:NES 10 ~ 5 BROMOFORM 10 TRANS-1,4-DICm.oR0..2-BUTEtu:: '?0 1,2,3-TRICHLOROPROP.An ·:xo 1,4-Dicm.oROBENZEN!: /D 1,2·Dicm.oROBENZENE J, 1,2·DmROM0·3-Cm.oROPROPANE ;;lfX)

VIN1'L AC!:TAT!! .J; "\ v " / \ 7 "'\ / \ l/ 1-ludf'ocn ~ h.,..,n -c; (f)/f-') (-) F) (-) (-1-) (-)

i-MDLt -5 SACk6~1lND PRESENT IW LAB 6LAI.JKS.

J - Estimated value !1: - Actual value is known to be le11 than value given. L - Actual value is known to be greater than value given. U - Material was analyzed for but not detected. The number is the K~ Detection L~t. !D. - Hot analyzed. 1/ - ~entative identification. ~I - on HRDC List of Priority Pollutants. ii - CoMf'OLn-tb REUJ:\51-V bETecTASLE oNLY AT J-11&1-t ccNC.fNTI!Ffnorus, C • PCS51SLE LR[3 C.ONTAMtNATJON. DEBNR 3068-0 (10/93)

( )

p.g/1 pg/kg

PURGCOM.ORG

BASE/NEUTRAL AND ACID EXTRACT ABLES COf1POUND

~STATE LABORATORY OF PUBLIC HEALTH ~ DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES

P.O. BOX 28047-306 N. ,WILHINGTON, ST., RALEIGH, N.C. 27611

ORGANIC CHEHICAL ANALYSIS LAB NO ¥~L{)~~ q_CIIt>YY lqtJIO¢lo 9tfJ/) 'LX. FIELD # IS'70~ J57oK 1.5'?11 /57/._=! TYPE (~) <!.fl. ~) ( 1/.) ( )

UNITS lJQ/1~ ~g!kQ) lJQ/1~ ~q/kq~ _llg/1 uq/kq N-nitrosodimethylamine I0/~3D LA.- I.A .,. -:1&-· I.A--;;-

bis(2-chloroethyl)ether 2-chlorophenol phenol 1_._3-dichlorobenzene 1,4-dichlorobenzene 1 2-dichlorobenzene bis(2-chloroi l)ether hexachloroethane N-nitroso-di-n...propylamine nitrobenzene isophorone 2-nitrophenol 2,4-dimethylphenol bis(2-chloroethoxy)methane 2 4-dichlorophenol 1.2,4-trichlorobenzene naphthalene hexachlorobutadiene 4-ch loro~resol hexachlorocyclapentadiene 2 4 6-trichlorophenol 2-chloronaphthalene acenaphthylene dimethYl ohthalate 2,6-dinitrotoluene acenaphthene 'if' 2.4-dinitrophenol SO/It;,SO 2 4-dinitrotoluene /tJ/330 4-nitrophenol .SO/'J"-SO fluorene to/~o 4-chlorophenylphenylether , diethyl phthalate ~ ~6-dinitro-o-cresol so/Jt::JSo diphenylamine ltJL33o azobenzene 4-braooohenvlohenvlether hexachlorobenzene 'V ~ntachlorophenol .SO/IItl5"0 phenanthrene IIJ/.330 anthracene dibutyl phthalate , , , / fl uoranthene '\jf' '~ ' 1/ " I \ {

J - Estimated value. K - Actual value is known to be less than value given. L - Actual value is known to be greater than value given. u - Material was analyzed for but not detected. The nlltber is the fHninun Detection Limit. m1JL NA - Not analyzed. - - - _ 1/ -Tentative identification. ~/ - On NROC List of Priority Pollutants .

. . N.C. Viv.<Aion o6 HeaLth SeJLvic.u VHS 3068-0 (4/86 Labo~o~y)

( )

uq/1 lJg/kg

STATE LABORATORY OF PUBLIC HEALTH DIVISIOH OF HEALTH SERVICES, N.C. DEPARTMENT OF HUHAN RESOURCES

P.O. BOX 28047- 306 N. WILHINGTON, ST., RALEIGH, N.C. 27611

ORGANIC CHEMICAL ANALYSIS

BASE/NEUTRAL AND ACID LAB HO 9L//0V,). tl~J0</-<1 Q'IJO~ 9Y/D<f..R_ EXTRACT ABLES FIELD II JSlof., I.:Y-702 /.171/ JS7L =l rot1POUND TYPE (~} (~ )_ c...;}) ( l,l)

UNITS ~1JQ/1 Jmtaeg '~{i,q/kq 1JQ/1~ TJ:I:lii£ \1 Q/ k _g_ pyrene /0/.330 v<- ve:::- i.A- t_,C. benzidine S"a/JbSO butyl benzyl phthalate 10/$30 benz(a)anthracene ' chrysene "' 3 3-dichlorobenzidine 'lbSO SOl bis(2-ethvlhexvl)phthalate llo/33o di-n-octyl phthalate I/O/.S3_o benzo(b)fluoranthene SO/Ji£0 benzo(k)fluoranthene benzo(a)pyrene indeno(l 2 3-<:d}ovrene dibenzo(a h)anthracene -' / "- _, benzo ( q h i) oerv 1 ene \ '/ 'II '\V ' '/ \ v

aniline S"olihSQ ·~ -~ ""'--" v---benzoic acid benzvl alcohol 4-chloroaniline ~ / dibenzofuran /()/330 2-methy\naphthalene 2-methylphenol 4-methyl pheno 1 ~ 2-ni troani 1 ine so/Jit:J5o ( 3-nitroaniHne 4-nitroaniline /_ / , ~4~5-trichlorophenol "" ,I( ' "'

,,

m'lH-J - Estimated value. H2-0/ $()/1-K - Actual value is known to be less than value given. L - Actual value is known to be greater than value given. U- Haterial was analyzed for but not detected. The number is the Hinimum Detection Limit. NA - Not analyzed. 1/ -Tentative identification. ~I -On NRDC List of Priority Pollutants.

N.C. V-i.v.i.6-i.on o6 He.a..Uh SVtv-i.c.e.-6 VHS 3068-0 (4/86 Labo~o~yl

( ) ( )

uo/1 1Jo/kg_ lJQ/1 uq/ko

•.! .:..- 0

'·. ·-..;:

r--- _Lt __ ~---

: c.DEH NR ,. livision of Solid Waste Management

~uperfund Section



Organics Lab: :------::----

lnorganics Lab: 7'

APR 2 9 1994


Project Name: .S~J ("\ ~+ ... {_j (4_ c; c-f•' ·~ Sampled by: .i~t.rT- fc.r-/u..r -I'4cu--R----f ..{~ Si te ID # (NCD#) 0~3 32 L( qhC, Sampler ID -Location: (._A jJJI ~'--"""' s I ..('/4-rll-'7 Co Telephone:_(q 1'7 ) 13s uo I Address: r..J~T - D ate Sampled: L1 L '-( l c, '-~

Time Sampled:

Sample Types: Soil Water )"- Waste Other J'8)ii'-Zr'"l

Remarks:

Field Sampl( I (, 6 b vC I 6& bs) ~ ~1 tlf~ 4-66() r I t661:- =JCG'f/CJ ' Numbers @ -;J:tt- 21:. iH:;~~ -·H6 9 f/. + f, fg ~:l =tf; 671?- 41:t~ -:1 I (:!!!Ji 4-.FJ t::r I

Relinquished by: ~ 9f,~ t- Date: '-1 ;-, /qlf. Time: /t.ts-1 (Signature)

I

------------------------------------------------------------------------------------------------------------------------------------------------Received by: ~(~i;~a~:) ~ ~

Date: .i..fh/_ ~'-1 Time: d. . .sa

Relinquished by: Date: Time: (Signature)

------------------------------------------------------------------------------------------------------------------------------------------------Received by: D ate : Time:

(Signature)

Relinquished by: D ate: Time: (Signature)

------------------------------------------------------------------------------------------------------------------------------------------------Received by: Date: Time:

(Sigr:-~a~e_L / __,

Results Reported: ~(?/p~ D ate: '{){;_tfovq'f Time : (Signature)

(A: \ COCR.FR.!\1)

~ I

I

I

I

-- ~-~~- ---- ---- -- ___ j

--;·c-DEHNR. •

liVision of Solid Waste .Management

0 Superfund Section·



Organics Lab: /Z lnorganics Lab: --


Project Name: s '"(" ..{ ""~~ /.I (Le. c '1 (, {: ':) Sampled by: s +.-.~.r"t- rt~"J.-~ .( ~re.r~...,{ ..J'e-cT

Site ID # (NCD#) ()'13 35'-1 9~~ Sampler ID -Location: ctr~-'~ll-,._...-! 7 ..fT 11 ,..~.-'t C() flC... Telephone:_('1tCf) 7s:! 1.-g'b I

Address: r-JA Date Sampled: ':1.L'-'~/9tf Time Sampled: '-

Sample Types: Soil · Water ~ Waste Other ..S8/l ""'E.tll

Remarks:

: Field Sample IS ·ID'-/ IS lbfo JS 101 IS /0? IS IOt!j [...l I I) ,,.r ? I?-------..

.~e~w I Numbers

l IS !13 JS 7'lf ~· -

I

Relinquished by: ~~B~~~ Date: ""/I /q'i Time: I '-1 :!Lf (igllllture)

R~~~;~~d~T"~-~~-----------;;.-;.;sz::z-:q~r:r;-~;----i?::i-.z:-----(Signature)



(Signature)



(Signature)

Results Reported: /l- Lv? ~ /[.,e~ Date: s-v-1 v Time: (S~ature) #-f V f 0 o/ 1- f l(tOt/Cf

'

(A:\COCR.FR.l\f)

I

l I

---- ----- -----~ ---- - - -------,

·:-:.c.. OCJ"':".mcnt or Environment,

I lcalth, ~: !"at ural Rc.sou rccs Solie Waste MAnagement Division

SAMPLE At"'iALYSIS REQUEST e . Site N umber ---------------------

Collected By ~+ ... .,.rT Pc.. r l~o.r

Agency: H azard ous Was te Solid Was te 7--- Superfund --- ----

Sample Type Environm ental Concentrate Comments

__ Ground water (1) Solid (5) 5 AM PLE'" .Sta? - 01

_ _ S urfa ce water (2) _Liquid (6) L11 rr+ ....... ,..., (rJ~)

-- Soil (3) _ Sludge (7) ..(vJ. ~ ~ ..... + .s ... ~lll-7'- Other (4) : -&""Other (8)

Organ ic Chemistry Inorganic Chemistry

Parameter Res ul ts (mg/1) Parameter Results(mg/1) (mg/k.g) X P &T:GC/ MS Arsenic --

Acid:B/ N E:>-.1. Barium -- --' MTBE Cadmium - - --

Chl orid e -- --Chromium - - --

-- __ Copper Fluori de -- - -I ron -- --Lead -- --

-- __ M anganese

-- __ M ercu ry N itra te -- --Seleni um --Silve r - -

Rad iochemistry -- Su lfa tes Zin c --

Param eter Resu Its (PCi / I) -- pH

-- G ross Alpha -- Conductivi ty G ross Bela T DS - - --

TOC ----

Microbio logy ----

Para m eter Results (Col/ lOOm!) ---- --- - --

Rcpoelc~ /. A/'<--C D ate R eceived lL' J ~/ 'iJ dtl DateR ort ed 9-)7-,s-/f Y D<.~te E xt ra ct ed ,

Date Analyzed cJ -d.3 - 9_ 'I l1 &.r Lab Number 9 3[;-~2 DII S 31~ 1 (l ~ cviscd 2/Y1)

T ime 1"(0_5 ·------

TCLP Compounds

Inorganic Compounds Results(mg/1) A rsenic --B ari um -- - -Cadm ium --Chrom ium --Lead - -

-- Mercu ry Selenium - -Sil ve r --

--- -- ---

Organic Compounds Results (mg/1 ) benzene --carbon te tr achlorid e --chlordane --chlorobenz::ne --chlo ro form --a-creso l --m-cresol --

- - p-cresol cresol --1,4-d ichlorobenzene --1,2-dichlo roe thane - -

-- 1, 1-di ch loroethylene 2,4-d in it ro toluene --

-- heptachlor

hex.ach I orobenzene --hexach lo robu tad iene - -hexachl oroethane --

__ m eth yl ethyl ket one nitro be nze ne - -

-- pentac hlo roph e no l

- - pyr idine

-- tel rachlo roe t hylcnc

-- trichl oroe thylen e __ 2,4,5-trichl orophenol __ 2,4,6-t richJorophenol __ vi nyl chlo ride

end rin --lind an e --meth oxychl or

_ _ toxaph ene 2,4-D --

__ 2,4 ,5-TP (Silvex)

--

-- --- --- ----- ---------- J

r-:~c. Dcpa:-.mcnt of Environment, • Health, &. !"atunl Resources

Solid Waste 'Management Division

SA11PLE ANALYSIS REQUEST

e State Laboratory of Public Health

A. . P.O. Oox ~7. 306 K Wilmington Street .. Raleigh, North Carolina 27611

Site Number rJ C.i/ 0"1.3 -:?'1'-i '1 b '1

Name ofSitc S&! ~et .. IJ r--~c..;c:l.'r_j

0 •..l€. '1.' Field Sample Number _______________ _

.. Site Location G "I«{ H,·lf D:.& .. "r..-.f G.

Collected By ~t-..... .rT P.:.rV-w- Time l'-(03

Agency: Hazardous Waste Solid Waste -f-. Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results(mg/1)

Environmental Concentrate Comments Arsenic --S, ftMP\.f" .rGO- Ol

Barium Ground water (1) _Solid (5)

-- -· Cadmium --(,.>~)

Chromium Surface water (2) _· _Liquid (6) vtrrt~...., -- Lead -· --

..r t-J~,..,_, ..... + .r ... -rl(l...-Mercury

_Soil (3) Sludge (7) --Selenium ' --

~Other (8) Silver

7'- Other ( 4) --: ------

Organic Chemistry Inorganic Chemistry --Parameter Results (mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds · Results(mg/1) _P&T:GC/MS Arsenic benzene -- --)(_ Acid:B/N Ext. Barium carbon tetrachloride -- --'MTBE Cadmium chlordane

:><.. ~E'T I f'-8 -- --

Chloride chlorobeniene -'-r-'-"' & 'd . -- ~

1-- 11. ',(!,I/ < o, I o /!f?trt Chromium chloroform -- --=~-- k'NdAnt= < o. ~qm... __ Copper o-cresol ---r-~t:~O/{ <p 0 ~ Fluoride m-cresol -- --

Iron __ p-cresol -1-- It;, Llfl (; <:Z.,trptmt --..:.~-- ""(M!uul#t£ < o. 3../T~()L Lead cresol -- ---f- %EJfA/u( < 0,/0 /),Rm. __ Manganese .. 1,4-dichlorobenzene --~L <()./0 f¥M __ Mercury 1,2-dichloroethane

Nitrate = 1,1-dichloroethylene -- -- Selenium 2,4-dinitrotoluene -- --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --Zinc hexachlorobutadiene -- --Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity _. _ methyl ethyl ketone


-- __ pyridine


-- __ trichloroethylene Parameter Results (Col/lOOm!) __ 2,4,5-trichlorophenol -- - 2,4,6-trichlorophcnol -- -- -- vinyl chloride -- -- endrin --

lindane . Date Received 11' J.tf-,91 A&.

--Reported by __ mcthox)'chlor

FE:rr all\ __ toxaphene Date Extractcd/.f-..?9-~II-30·CJ35l\Datc Reported . -- 2,4-D

p~ $P~ 9~3863 __ 2,4,5-TP (Silvex) Date An"dlyzcdU-3fJ-~ P-~j;?i Lab Number · --DllS Jl'Jl (Revised 2/'.11) ~ 8

t'.C.. Depa~ment o( Environment,

lleahh, l: 1'-'atunl Rc:.wurc~ Solid Waste Management Di~ion


e Stale Lat>oratory o( Public Health

· P.O. 13ox ~7. 306 K Wilmin(;1on Street Ralei);h, North Carolina 27Gll

Site Number r-l c..v o<73 :?'1'1 '1 b '1 Field Sample Numbcr __ O_I l:,_{,_J_7 __________ _

NameofSitc S$! ~e.+-.IJ '(1-'c.'lcl.'t-_j .. Site Location G "lq H.·u Ce.& .. ,.f'w.t Co

C II t dB r.L .. .,.rT P"ri~D-.1" 0 cc e y.::. l --------------------- Time lt.t03

Agency: Hazardous Waste Solid Waste ~ Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Resulls(mg/1)

Environmental Concentrate Comments )f Arsenic ~o~o \ --SA.MPl.~ ..rGV-01

-;( Barium _0- ~~\ _ Ground water (1) _Solid (5) "'!. Cadmium .L... 0-0-:, --

(rJ~) "X Chromium .4. c.- o..S

lArrl..-.. ....., --_ Surface water {2) _Liquid (6) ,(. Lead ..£..c.\O

..(~.·-,.~+ s ......... r:1~ "f... Mercury <... 0 .,Q 1 _Soil {3) _Sludge (7) ..,( Selenium LO.Oo.5 --

"· :f:__ Silver -'-0~ c .5 Y- Other ( 4) : _..!::.... Other (8)

~ ':..-

------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results~) (mg/kg) Organic Compounds Results (mg/1) _P&T:GC/MS -1- Arsenic -;:;_ \ benzene

T --_·_ Acid:B/N Ext. Barium 5'] carbon tetrachloride

--:r --'MTBE Cadmium L..9.g chlordane -- -- --Chloride chlorobenzene -- -- --

- -1 Chromium ~\ chloroform ---- __ Coppe: a-cresol --

Fiuoridc m-cresol -- ---- Iron = p-crcsol --.. i- Lead ·~v cresol -- ---- -- Mar.ganese -- 1,4-dichlorobcnzene

-- _t_ Mc:cury ..L..... a <o!!o5 1,2-dichloroethane ---- Nitrate __ 1,1-dichloroethylene --

..f. Selenium ""--'

2,4-dinitrotoluenc -- --y.. Silver ~5.£ __ heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --

Zinc hexachlorobutadiene -- --Parameter Results (PCi/1) -- pH -- hexachloroethane __ Gross Alpha __ Conductivity __ . mc!hyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- --TOC · __ pentachlorophenol --

-- __ pyridine

Microbiology -- __ tetrachloroethylene i. __ trichloroethylene --Parameter Results (Col/100ml) __ 2,4,5-trichlorophenol --

-- -- __ 2,4,6-trichlorophenol

-- -- _. _ vinyl chloride endrin --lindane --

.Date Received Reported by -- mcthO>.)'Chlor __ toxaphene

Dille Extracted oatm~~1s uov· ~ o 9 3 __ 2,4-D __ 2,4,5-TP (Silvex)

Date AnalyLcd Lab Number DIIS Jl'JJ (Revised 2/YI) --

t-:.C. Department or Environment, Jiealth, &. Natural Re.s.ources

Solid Waste Hanagement Division


• State Laboratory or Public Health

-· P.O. Dox 2SO-l7, 306 K Wilmintton St~et W Raleigh, North Carolina 27611

Site Numbe.r rJ C..j/ 0<7.3 -:?'l'-1 '1 b ~

Name or'Sitc S${ ~e+ ... {J Yl--L~cl:t-.5

Field Sample Number __ 0_1.l_b_"l,..:_:"L... __________ _

Time I'-{~.)

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Resulls(mg/1)

Environmental Concentrate Comments Arsenic --_Solid (5). SltMPl.~ ~ €:t? - 0 '2.-

Barium _Ground water (1)

-- _ .. Cadmium --

_Liquid (6) IAet<+.-u~. {iJE) Chromium

_ Surface water (2) --

Lead --,.fc..J.;,.._c-,.IT" ..r~-r lc_

Mercury _Soil (3) Sludge (7) --Selenium --

$-other (8) Silver

"7- Other ( 4) ,. --

------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds · Results(mg/1) _1!::... P&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- --'MTBE Cadmium chlordane - -- --

Chloride chlorobenzene -- --chromium

~

chloroform - -- ---- __ Copper o-cresol --

fluoride m-cresol -- -- = p-cresol Iron -- --.. Lead cresol -- -- --__ Manganese .. -- 1,4-dichlorobenzene


-- Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene -- = heptachlor Silver --


Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone


-- __ pyridine


-- __ trichloroethylene Parameter Results (Col/lOOml) -- __ 2,4,5-trichlorophenol

-- -· __ 2,4,6-trichlorophenol ---- -- __ vinyl chloride

endrin --lindane

,,, ~1/-93 11A --.Date Received Reported by __ methOX)'chlor

__ toxaphene Dale Extracted Date Reported -- 2,4-D

Dale Analy.tcd c2,;(3-q L/ '71 W 983864 __ 2,4,5-TP (Silvcx) Lab Number --DliS 3191 (Revised 2/91)

t'.C Dcp-;nmcnt of Environment,

llca!th, & NHunl Resources Sc·~id Waste M~nagemcnt Division

SAMPLE AN.' ... a c ......a

· P.O. l3ox 2SO-l7, 306 N. Wilmington Street

e RAleigh, North Carolin1 27611

Site Number ('} L.i/ 0'13 -::?1'1 '1 b ~ Field Sample Numbcr ___ 0_1...Jb __ 1..-_~ ____ -:-------

SiteLocation G.,ld_ H.·u C.c.&#ot-f'-l.f Co ..

Collected By ~ t-- .. .rT Pc.. r V-w- 1D#0(783f'tODate Collected !t/'l-s /'13 Time 1'-l 'l.-.)

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- ·--

Sample Type Inorganic Compounds Resulls(mg/1)

Environmental Concentrate Comments Arsenic --_Solid (5). S AMPl.~ ~ t:::D - 0 '2,..-

Barium -- -· _ Ground water (1) Cadmium --

_ Liqu.id (6) lApt<+r-u~. (tlE) Chromium --

_ Surface water (2) Lead --.r L..Cl : ,....__.rr s" , 1 c.- -- Mercury

_Soil (3) · _ Sludge (7) Selenium --Silver

7- Other (4) ~lher (8) --

~:

------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds · Results(mg/1)

P&T:GC/MS Arsenic benzene -- --~ Acid:B /N Ex1:. Barium carbon tetrachloride -- --

'MTBE Cadmium chlordane 7 r t.sr (_ rd3 -- --

Chloride chlorobenzene -·....-- -- -_ r- Ellde.!t/ < o ,J 0 f?!!/I'L Chromium chloroform --__ J_.,ildAJVE <'t7•..7Pffli'L Copper o-cresol -- --1J1E(IJ~Xtlf1.h/A# </, 0 4{JM. Fluoride m-cresol -- = p-cresol -r-'?dXA~HENE <:.:z,d~ · Iron --

Lead cresol ..::r- t!JN~tbtNE <o~:fo -- --"7-frE$~ <t'J./o#m __ Manganese ... 1,4-dichlorobenz.ene --'I <0•/0 ,PP'i __ Mercury 1,2-dichloroethane

Nitrate = 1,1-dichloroethylcne -- --Selenium 2,4-dinitrotoluene -- = heptachlor Silver --

Radiochemistry Sulfates hexachlorobcnzene -- --Zinc hexachlorobutadiene -- --

Parameter Results (PCi/1) pH hexachloroethane -- --__ Gross Alpha __ Conductivity __ methyl ethyl ketone

Gross Bela TDS nitrobenzene -- - -- --TOC __ pentachlorophenol --

-- __ pyridine

Microbiology -- -- tetrachloroethylene . __ trichloroethylene --Parameter Results (Col/lOOml) __ 2,4,5-trichlorophcnol ---- .. __ 2,4,6-trichlorophenol ---- -- __ vinyl chloride

endrin --lindane

.Date Received II-:;.'{- '13 ,911 --

Reported by methoxychlor --~ f3NA __ toxaphene

Dale ExtractcdL/:;:19-~11-32439\ Dale Reported -- 2,4-p

Pc:sr ~A S338G5 __ 2,4,5-TP (Silvcx)

Date Ana1yLcdiJ-3D-~ b21fr'li Lab Number --DIIS 31~1 (ltcviscd 2/Y1)~ f1p

t'.C. Dcpanmcnt o( Environment,

llealth, 6:. l'~lunl Ruourres Solid Waste M•nagcmcnt Division

SAMPLE ANALYSiS R.l:.(._ UE~ State l:...at>ontory ot rubloc He> .

· P.O. 13ox ZS0.:7, 306 ?". Wilminpon St~ct e R.alcig.h, North Carolina 27611

Site Number rJ C.[) 0'13 :?'1'-1 4 b ~

Name or"Site S.€f;J{ ~e.+-.1; yt.-L-c/cl:t-.5

Field Sample Number Ot blt3g-----------------------------------

Collected By ~ t-.... ,.t" Pc. r V-c.,r Time IL{ ~.)

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds ·-- ----

Sample Type Inorganic Compounds Resulls(mg/1) EnvironmenL'll Concentrate Comments -1- Arsenic <o. a l

_ Soi..id (5) . 5 AMPt.r;- .Sta?- o·z- ....:f::.... Barium _Q .. .31(D __ Ground water (1) -1. Cadmium ""'-o.oS

lAet<tr-~1"'1. ( t-'El -f. Chromium 4o.o-5 __ Surface water (2) _Liquid (6) T Lead .L.o- \O

JJ;~._,...-r .ft.-riC-T Mercury L..D-o \

_Soil (3) --

Selenium (" rJc o. o.s.-_Sludge (7) -!..

_!_ Other (8) _t_ Silver ..(.a. c ~

"7-- Other ( 4) :· ------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Resulls~(mg/kg) Organic Compounds Results(mg/1)

-- P&T:GC/MS i- Arsenic 3_l -- benzene Acid:B /N Ext. i- Barium ~9 carbon Lclrachloridc

-.MTBE -- --_:t_ Cadmium ..z9.B chlordane -- --

Chlorid:: chlorobenzene -- -- ~-

-- _1_ Chromium \la chloroform ---- Copper o-cresol -- --

Fluoride m-cresol -- -- ---- Iron __ p-cresol --.. 4- Lead ( ·d, 0 cresol -- -- --

__ hi:!nganese .. 1,4-dichlorobenzene ---- ..:1:::_ Mercury L_c ... o5 1,2-dichlorocthane ---- Nitrate 1,1-dichloroethylene -- --

i- Selenium ~I 2,4-dinitrotoluene Tsilver

--4-9 ,.e, __ heptachlor --Radiochemistry Sulfates hexach lorobenz.enc -- --

Zinc hexach !oro butadiene -- --Parameter Results (PCi/1) pH hexachloroethane -- --__ Gross Alpha Conducti\;tv

-- J

__ methyl ethyl ketone Gross Bela TDS nitrobenzene -- -- --



-- __ trichloroethylene Parameter Results (Col/lOOml) -- __ '2,4,5-trichlorophc:nol

-- -- __ 2.,4,6-trichJorophenol

-- -- __ vinyl chloride endrin ---lindane --

. Date Received Rc ported by __ methoxychlor __ toxaphene

D<.~tc Extracted D.Jtc Rcoorted 2,4-D

01.9476 UL:V :W 93 ---- 2,4,5-TP (Silvcx)

Date AnalyLcd Lab Number --DIIS Jl'Jl (ltcvisc<.! 2/Yl)

t'.C. Department of Environment,

Jl~alth, &. ~alural Resources 'solid Waste Management Division


e State Laban tory of Public Health

A· P.O. Iklx ~7. 306 K Wilmington Street W Raleigh, North Carolina 27611

Site Number rJ '-0 o-?3 :?'1'1 ~ b '1 Field Sample Number ___ o_1S_b_,__t.f _________ _

Collected By ~ t--.. ,.t' Pc." l~w- Time I'--( J1,

Agency: .Hazardous Waste Solid Waste ~Superfund TCLP Compounds --Sample Type Inorganic Compounds Results(mg/1)

Environmental Concentrate Comments Arsenic --Solid (5) . 5 AMPLe;- ~t::t?- 03

Barium -- -· _Ground water (1) Cadmium --

Chromium Do.....,"" s-+ re. .... "r" Su1 ..... e-;.-r --

Surface water (2) _Liquid (6) Lead - . Mercury _Soil (3) · _ Sludge (7) .s~ ..... c'c..- . --Selenium --

Silver ti- Other ( 4) 1: ~Other (8)

--------

Organic Chemistry Inorganic Chemistry --Parameter Resu Its (mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds · Results(mg/1) .,L. P&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- --

'MTBE Cadmium chlordane - -- --Chloride chlorobenzene -- -- -Chromium chloroform - -- --

-- __ Copper -- o-cresol Fluoride m-cresol -- -- = p-cresol Iron -- --.. Lead cresol -- -- --__ Manganese .. 1,4-dichlorobenzeoe --

-- __ Mercury 1,2-dichloroethane

-- Nitrate ~ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene -- -- heptachlor Silver --


Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity methyl ethyl ketone

Gross Beta TDS -- nitrobenzene -- -- --TOC pentachlorophenol -- --

-- __ pyridine


-- __ trichloroethylene Parameter Results (Col/lOOm!) __ 2,4,5-trichlorophenol ---- .. 2,4,6-trichlorophcnol -- -- vinyl chloride -- --

endrin --lindane

II·; ¢-13 --.Date Received M Reported by methO>.)'chlor --__ toxaphene

D:.~te Extracted Date Reported __ 2,4-D

Dale Analyzed cJ. -;;2..3-94- tllff Lab Number 933866 __ 2,4,5-TP (Silvcx)

--DIIS 31~1-(Rcviscd 2/Yl)

~.C Dcp:..rtmcnt of Environment, I Jc:lth, /,:. !':Lura! Rc.wurccs

5<;.1id Waste 1--!anagcment Division

SA.M.P Lt. A.i'\ . ' . P.O. nox :ZS0.:7, 306 K Wi1ming~on Street

R..tleigh, North Carolina 27611

Site Number rJ C...i/ 0~3 :?1'1 '1 b '1 e

Field Sample Nurnbcr __ O_I_S'_fo_'),_) _________ _

Collecled By ~ t-...... .,.T Pt..r l~w-- Time It..{ _n, .,

Agency: .Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results(mg/1)

Environmental Concentrate Comments Arsenic --·_Solid (5). S I\MPL6" .St::t? .- 03

Barium _Ground water (1)

-- -· Cadmium --Chromium

__ Surface wat~r (2) D ov.,.,s-f r~~rr' Se.-J.t,..._,_ ... -r --_ Liqu.ld (6) Lead --

s~ .... rte-__ Mercury

_Soil (3) · _ Sludge (7) . Selenium --~er(8)

Silver 7- Other (4) ~ .. --

------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/1) (rng/kg) Organic Compounds · Resu1ts(mg/1) _P&T:GC/MS Arsenic benzene -- --_::i__ Acid:B/N Ext. Barium carbon tetrachloride -- --

'MTB;, Cadmium chl'ordane -- --')(.... P£!1 :_!~a Chloride chlorobenzene -'r- ~ # --

Chromium -f- c::;v, ~,;;y' -<.Q./0 1'/?AL chloroform -- --= ,____ L_.,AidANE <o . .:zq qz/K- __ Copper o-cresol --_ ,____ 'jifcr-AcxsKAb~<l. t::1 )JPM- Fluoride m-cresol -- . = p-cresol - f-~ <'42. d 40"""-= Iron

..:.:.,.---:4 <o .. :/PJJI?m.... Lead cresol ---.,. r:- ~dk;C!. <0,/1? #0\.- __ Manganese .. __ 1,4-dichlorobenzene

~l t:'B'f <o./t:JpdL __ Mercury __ 1,2-dichloroethane Nitrate · 1,1-dichloroethylcne -- --Selenium -- 2,4-dinitroto\uene -- --Silver __ heptachlor --

Radiochemistry Sulfates hexach lorobenz.ene -- --Zinc hexachlorobutadiene -- --

Parameter Results (PCi/1) pH' hexachloroethane __ Gross Alpha

-- --__ Conductivity __ methyl ethyl ketone

'Gross Bela TDS nitrobenzene -- -- --TOC __ pentachlorophenol --

-- __ pyridine


-- __ trichloroethylene Parameter Results (Col/100ml) -- __ 2,4,5-trichlorophenol

~ __ 2,4,6-trichlorophcno\ -- ---- -- __ v)nyl chloride

cndrin --lindane

.Date Received fl· :J..'f_~tj_l --tltl Reported by -- methoxychlor

(/b-:r BNI\ __ toxaphene Date Ex1rac!cd//':('?-~ U-3).('BS'\ Date Reported -- ?.,4-D

IZ:sr~;1 9338617 __ 2,<1,5-TP (Silvcx) Dale Analyzed//-3~~12'.;/~l'l Lab Number --DJIS 31\11 (ltcviscd 2/Y1)U /1.

t'.C. Department of Environment,

llc.al~h. l:. !"alural Ruourcc.s

_: . .-~ .. -- .. ...~ ... •; -. P.O. nox 250-!7, 306 K Wilming1on Stn:ct

. Solid Waste M>.nagcmcnt Division

~ \ {..j/ , 0~3 "?'>J. 0. I C, Site Number ,~ ..:. -" • •" 1 ---------------------------------Field Sam pie Number ____ ~ ___ l_b_&_3_1 ___ R.A __ Ic._igh_. ~-·o_rt_h_Ca __ ro_l_in_

1

_

2

_

7

_G

1

_

1

C II t dB ~.~-.... .rt" Pt.rlt:.w-o ec e y ~ ,- ID#Oj/8'3-f<tO~ate Collected J,/.,s/'1 3 Time I'-{ .fb ----------------------

Agency: Hazardous Waste Solid Waste ~Superfund

Sample Type Environment.·d Concentrate Comments

_Ground water (1) _· Solid (5). S rtMPLf"" .S£r?- 0.3

_ Surface wat~r (2) -- Liqwd (6) Do....v ..... _s-+re~o"i""' su..•..-e-,.-1

_Soil (3) _ Sludge (7) _.{_ .... _-+f-l_e-________ _

-r:. Other ( 4) ;· _!:_ Other (8)

Organic Chemistry

Parameter _P&T:GC/MS

Acid:B/N Ext. -.MTBE

Results(mg/1)

Inorganic Chemistry

Parameter --1- Arsenic

7Barium "'JI- Cadmium --

Chloride -1- Chromium

Copper -- F1uoride . --

Iron --_:!_Lead

Results~)(mg/kg)

dl G:t. \

__ Manganese -f... Mercury

--Nitrate

_L Scleniumf------------------~----11_ Silver

Radiochemistry

P<Jramelcr __ Gross Alpha

Gross Beta

Results (PCi/1)

. Microbiology

Parameter Results (Col/lOOm!)

--------

Sulfates Zinc --

_pH

__ Conductivity -----------TDS --TOC

Date Received Reported by ----------------- -------------------Dale Ext;-aclet! Date Rcport~d ----------------- -----------------

LQ12,"4.77 NOV .~0 93. Date Analyzed :N !) liS } l 'J 1 (Jtcvisc-:c:-=~-::/Y:-:-1:-) ----------- a 0 u m ocr ____________ _

TCLP Compounds

Inorganic Compounds '1- Arsenic

_25._ Barium

Resulls(mg/1)

<' o. a I -;< Cadmium

T Chromium .:t::_ Lead

L o .. o.S

-f.. Mercury +.. Selenium

..f:::_ Silver

...L-o.o \

Organic Compounds benzene --

Results(mg/1)

-- carbon tetrachloride ------------chfordane chlorobenzenc -- chloroform o-cresol --m-crcsol --p-crcsol

--cresol ---- 1,4-dichlorobenzenc -----------

1,2-dichloroethanc -- 1,1-dichlorocthylenc = 2,4-dinitrotoluene ------------

-- heptachlor hexachlorobenzene hexachlorobutadicne -- -----------hexachloroethane --

-- methyl ethyl ketone nitrobenzene --

-- pentachlorophenol __ pyridine

__ telrachlorocthylcoc __ trichloroethylene

2,4,5-lrichlorophcnol

_ 2,4,6-trichlorophcnol -----------vinvl chloride -- , c:1drin --lindane --

-- mcthm:ychlor __ toxaphene __ 2,4-D

2.·~ ,5-TP (Silvcx)

~--------------------------------~

t'.C. Department o( Environment, ll~llh, & t\atunl Resources

Solid Waste l-ob.nagement Division


e State Laboratory or Public Health

A· P.O. Dox :ZS0.:7, 306 K Wilmington Street • ~leigh, North Carolina 27611

Site Number rJ C..i/ 0"1.3 :?'1'1 ") I:J ~ Fie.ld Sample Number __ O_I~.f:._b.=-1..--.::.(, ________ _

Collected By ~+ ...... .rT Pc..ri./..W"" Time ------IS" I o

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results(mg/1)


_Solid (5) . S f1 MPl.~ .!~-oY. -- -·· _ Ground water (1) Cadmium --

(/Jut lA ... ,{ s ~ ··-e-.:il Chromium

Surface water (2) _Liqwd (6) --

Lead -· --Mercury

_Soil (3) · _ Sludge (7) Sc-../IA.e_le..-- --Selenium --Silver

-r-· Other (4) ,. ~Other (8) --------

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results (mg/1) (mg/kg) Organic Compounds Results(mg/1) --I- P&T:GC/MS Arsenic benzene -- --

_ Acid:B/N Ext. Barium carbon tetrachloride -- --'MTBE Cadmium chlordane -- -- --_ chlorobeniene Chloride -- --Chromium chloroform -- -- --

-- __ Copper a-cresol --Fluoride m-cresol -- -- = p-cresol -- Iron --.. Lead cresol -- -- --__ Manganese .. 1,4-dichlorobenzene --__ Mercury 1,2-dichloroethane ---- Nitrate = 1,1-dichloroethylene --

Selenium 2,4-dinilrotolucne -- = heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene -- --

Zinc hexachlorobutadiene -- --Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity -- methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- --



-- __ trichloroethylene Parameter Results (Col/lOOm!) __ 2,4,5-trichlorophenol ---- -- 2,4,6-trichJorophenol

-- -- = vinyl chloride endrin --lindane

//':llf-93 --

. Date Received 1111 Reported by methox)'chlor --_. _ toxaphene

Dale Extracted Date Reported 2,4-D

r:2 -;J.'f__ ~q If 77 lt]"Lab Number S338G8 = 2,4,5-TP (Silvcx)

Date Analyzed --))liS 3W1 (Revised 2/')1)

~.C. Dcp.anmcnt of Environment, .L • .J -· -

llcahh, &. !'atun.l RC$0urcc.s

S<;>lid • Waste. ~fanagement Di...Uion

Site Number rJ c..i) ------------~-----------------

· P.O. IJ,ox ~~. 306 ?'. Wilmin&~on Street

Ralci&}l, North C..rolina 27611

Field Sample Numbcr ___ I_,_S_~_v_1 _________ _

Collected By ~ t--.. .rT P.:. r ~~~ Time -------

Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds -- --

Sample Type Inorganic Compounds Resulls(mg/1) Environmental Concentrate Comments Arsenic --

_Solid (5). S /tMPL~ ~a?- oL-f. Barium -- -· _ Ground water (1) Cadmium --

lf.J tft , ....... .,{ S~··-e../1 Chromium --

__ Surface water (2) _LiqUid (6) Lead --Jc--/IA.('Ie....----

__ Mercury

_Soil (3) · _ Sludge (7) . Selenium --Silver

-r:-· Other ( 4) ,. ~ther (8) --------

Organic Chemistry Inorganic Chemistry --Parameter Results (mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) _P&T:GC/MS Arsenic benzene -- --

")( Acid:B/N Ext. Barium carbon tetrachloride -- --"MTBE Cadmium chlordane ~ rccr L r4~. -- --

Chloride chlorobeniene ...~.,_ENd; • -- c·hromium --

chloroform -I- ~"' <1!7./11? AA?\. -- --__ L..t#dAN€ <o6~~ __ Copper a-cresol --

=~~~c:: :::~~;;t Fluoride m-cresol -- --Iron p-cresol --_:_:_ _ CJ1ft#!.d4HE <o~;z.fJ P/1""- Lead cresol -- --

~~Cflk~ <t:J.tP/Pm- __ Manganese .. 1,4-dichlorobenzene --~ <::0./d#.I'X,.., __ Mercury -- 1,2-dichloroethane

Nitrate _-_ 1,1-dichloroethylene -- --Selenium ' 2,4-dinitrotoluene -- --Silver __ heptachlor --

Radiochemistry Sulfates hexachlorobenzene -- --Zinc hexachlorobutadiene -- --Parameter Results (PCi/1) _pH hexachloroethane --

__ Gross Alpha __ Conductivity methyl ethyl ketone Gross Bela TDS -- nitrobenzene -- -- --



-- __ trichloroethylene Parameter Results (ColflOOml) __ 2,4,5-trichlorophcnol --

- __ 2,4,6-trichlorophenol -- ---- -- __ vinyl chloride

endrin --lindane

.Date Received l/-)Lf-93 /II) --Reported by __ methox-ychlor

t/'e.:r:r BrJA __ toxaphene Date Exiractcc.l//-;.79~}\·l)-lO:A Date Reported -- 2,4-D

(/EJr l}tJIJ 933869 __ 2,4,5-TP (Silve>:)

D<~tc AnalyLcdU-30-~M-tt-91 Lab Number --DIIS 31~1 (ltcviscd 2/Yl) ~ .-1J.D

t'.C Dcpanmcnt o( Environment,

J)c.3ith, l:. l'atun.l Ruources Solid Waste. Manaccmcnl Division w .

S.:_

e ' P.O. 13ox ~~. 306 1". Wilminblon Street

R..tlci&}l, North Carolina 27611

rJ (.." . QG._3 "?"''-( 0. I C, Site Number v 1 ~ ~ t t:> 1 -------------------------------- Field Sample Numbcr ___ O_I_b_b_t.-t_D ________ _

Collected By £ +-... .rT Pc. r j/-W"""

Agency: Hazardous Waste Solid Waste __i:__:__ Superfund

Sample Type EnvirnnmcnL1l Concentrate Comments

-Ground water (1) -Solid (5) . sAMPLE" ~{3:(?- oC...l

_Surface water (2) _Liquid (6) (!Jut 1 ...... ~ .f,_J i.-.e.JI

_Soil (3) · Sludge (7) _..s_·"-""'_.(';..._.._1 ~!../------~~

"'T-- Other (4) :· -/.. Other (8)

Organic Chemistry

Parameter _P&T:GC/MS _ Acid:B/N Ext.

'MTBE

Resu I ts(mg/1)

Inorganic Chemistry

Parameter "'1- Arsenic -f. Barium

Results(~(rng/kg)

'1-'1

--:;:::- Cadmium --Chloride

'i- Chromium __ Copper

F1uoridc Iron --+ Lead

__ Manganese _L Mercury

Nitrate --)( Selenium

\~

!---------------------~ ~Silver 4..~-5 Radiochemistry

Pi:lramell!r Results (PCi/1)

__ Gross Alpha ------Gross Beta

Microbiology

Pi:lrameter Results (Col/lOOml)

Sulfates Zinc

_pH __ Conductivity--------

TDS --TOC

. Date Received _______________ R c ported by __________ ~---

Date Extracted Date R::ooned ------------- 019478t~i0~-~~,~-.Q--9_3 ____ __

D<~!e AnalyLed Lab Number · J)JIS 31')1 (Revised '2/'Jl)

Time lSI 0 -----------TCLP Compounds

Inorganic Compounds -f. Arsenic

.:t:;_ Barium f- Cadmium

T Chromium ~Lead

Resulls(mg/1)

<o.o f

-f.. Mercury --:;:- Selenium

..L-0-0)

f.. Silver

Orgnnic Compounds benzene --carbon tetrachloride

?'o.oo.S:

Resu Its (mg/1)

-- -----------chlordane chlorobcnzenc --chloroform a-cresol -- m-cresol p-crcsol

--cresol

__ 1.~-dichlorobenzeoe ---------1,2-dichlorocthane

-- 1,1-dichlorocthylene -- 2,4-dinitrotoluene -----------= heptachlor

hcxachlorobenzenc hexachlorobutadienc --- -------------hexachloroethane --

--- methyl ethyl ketone nitrobcnz.enc --

-- pentachlorophenol __ pyridine

__ tetrachloroethylene trichloroethylene

--~.4,5-trichlorophenol = 2,4,6-trichlorophenol __ vinyl chloride

cndrin --lindane --

-- methoxychlor __ toxaphene __ :2,4-D __ :2,4,5-TP (Silvc>:)

--I

H

STATE lABORATORY OF PUBUC HEALTH PO BOX 28047- 306 N. WILMJNGTON ST •• RAI.EIGH. NC 27611

ORGAN.lC CHEMICAL ANALYSIS

PURGEABI.E COMPOUNDS LAB NO Cl~3Beful Ci336l.otf o.338LPu Q33Bu€ FIELD NO J5l..o.J.O I 5 £» .;l:l. t5lP:l'f ~~~.J..{p

COMPOUND TYPE ( 3 ) ( 3 ) (.3 ) ( 3 ) ( )

UNITS pg/1~ pg/1~ pg/1~ pg/~ pg/1 pg/kg

cm.oROKETHAme ;)[) nnh L.L LA- l.A__ u__ . VINYL cm.oRIDI!: 10 BROIIOia:'t'HAlO!: ~0 cm.oROJ!:l'HAlfE 10 TRicm.oROI"UJOROIIIIl!';TIL\!OC 10 ¥ ,v .ACZTOR ao l<o:S>B 7J,B l.l·DlCHLOROETBElU: 5 LA- u._ lODOIIIEtliA!OC tO ~ 'llll!:TBn.Zl'l CHLORIDE 5 lq~ CARBOI'f DlSm.nDI!: LA._.

TRAKS-1..2·DlCHLOROIC'TBE:lfl!: -.J /

ACX!LOI'fiT1ULll: d.OO l.l·DlCHLOROICTHA!IE 5 ~B'OT.Al'IOR ;J..O CIS-1..2-DlCHLOROIC'TBE:lfl!: 5 cm.oROI"'RK

l.l.l·T1UCHLOROET2L\1'11: ,if

CAJUIOI'f nr:t'JlACBLORJDJ: 10 ............. z 5 '

1..2-DlCHLOROET2L\1'11:

TR1CHLOROE1'JI.Al'I1C

!'" 1..2-DICHLOROPROPA!f!l \J /' BROIIODICHLOROJOC't'HAR 10 '\ / ,lf \ / \ /

Me-flu.. I-{- bu-lul e+hf'r 5 LL u_ [A_ I :r, K I

J - Satimated ~ue tMDL1'

E - Actual ~ue ia known to be lea• than value given. L - Actual ~ue ia known to be greater than value given. U - Xate:i&l wa• &D&lped !o: but 110t detected. 'l'he number is the Minimum Detection Limit. D. • :zrot: anal.y:ed. - - -1/ - Tectativ. identification. ~I - ou mu:x: Liat of Priority Pollut:anta.

H - ~c~Pcu}Jf) ~&'-1116!-V D€Tcc.TA8LE ON'-Y Ar llleH ca~cNT £A/JoN~. DEmiR 3085-0 (10/93)

B-~ ~ ..&-lr~<AL4 ( .ln:t~o~) C!..- C0'7"?'t/nnon k..1r co-rd~

-

(r)

( )

pg/1 pg/kg

PDRGCOM.ORC

H H

STATE LABORATORY OF PUBLIC HEALTH PO BOX 28047- 306 N. WILMINGTON ST •• RALEIGH. NC 2'!611

ORG.ti.NIC Cl:lE.MlCAL ANALYSIS

PURGEABI.E COMPOUNDS LAB NO q33~(D~ q33Bt.o1 q336({Jl.c q:a3etoB FIELD NO 15(DcJ:0 t5U>~ 15CtJ.J't J5Ci>;Lto

COMPOUND TYPE ( .3 ) ( 3 ) ( 3 ) ( 3 ) ( )

UNITS pg/1~ pg/1~ pg/1@ pg/1~ pg/1-pg/kg

DIBROMOH!:'l'HAlfZ 5oob LL LL LL u_

4-Ja:Tln"L.:Z.PZKTA1'fO!fE

CIS-l.:S·DICBLOROPROP!:IfE \V TOLtll!:lfE 45 TRAlfS-l.,.:S.DICBLOROPROPZIB ~~ LA-1.1.:Z.:Z·T!:T1lACBLOROETBAIOC /Ornh 1.1.2-TRICBLOROr:nL\lR 511 :Z.BJ!:%Al{OifE 10 n:TRACBLORO!:THEl'nC 5 DIBROMOCHLOROJa:l'lJA!f!: iO !:'l"HTLZ!fE DmROIIIDE 5 CBLORO~ J 1.1.1.2-Tl!:TRACBLOROr:l'BAlf!: /0 ,v I!:THYL DDZEifE 5 I d... XYLZ%fES /0 qlf st'TREZ(E 5 u_ BROMOFORM 10 T1ZA!f8-1.4-DICBLORO.:Z.IItn%KZ ~0 1..2.,.:S.T1UCBLOROPROPAlfZ ~co 1.4-DICBLOROBEl'IZD!: 10 1.2-DICBLOROBEl'IZD!: t .z

1.2-DIBROMo-3-CBLOROPROPA1'f!: ~00

VINTLACrrATZ -1 \ 1/ 'v \I/ \I

J - Zatimated value JC - Actual value ia li::nawD to be 1eae than value given. L - Actual value b lclawn to be ;reatar than value given. 0' - Jlaterial -• anal.~ed 1!or but not detected. 'l'he number ia the Hinillzum Detection Limit. D. - IIJot analyzed. - - -1/ - ~entative identification. 2/ - On JlllUX: Liat of Priority Pollutanta.

H- l!oNPOUIJf> Rt:UR/31...Y oer~CTRBLE ONLY A-1 H/6-H c.oNC.&vT~TJol\h. DEmiR 3068-0 (10/93)

( )

pg/1 pg/kg

PORGCOH.ORG

BASE/NEUTRAL AND ACID EXTRACT ABLES COf1POOND

N-nitrosodimethvlamine bis(2-chloroethvl)ether 2-chloroohenol ohenol 1.3-dichlorobenzene 1 4-dichlorobenzene 1 2-dichlorobenzene bisC2-chloroi llether hexachloroethane N-ni troso-di -n-oroovl amine nitrobenzene isoohorone 2-ni troohenol 2,4-dimethvlohenol bisC2-chloroethoxy)methane 2,4-dichloroohenol 1.2 4-trichlorobenzene naohthalene hexachlorobutadiene 4-chloro~resol

hexachlorocvclooentadiene 2.4 6-trichloroohenol 2-chloronaohthalene acenaohthvlene dimethyl phthalate 2.6-dinitrotoluene acenaohthene 2.4-dinitroohenol 2 4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlohenvlether diethvl Phthalate 4,6-dinitro-o-cresol diohenvlamine azobenzene 4-braroohenylphenylether hexachlorobenzene pentachlorophenol phenanthrene anthracene dibutvl Phthalate fluoranthene

STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTI1ENT OF HUMAN RESOORCES

P.O. BOX 28047- 306 N •• WILMINGTON, ST., RALEIGH,. N.C. 27611

ORGANIC CHEHICAL ANALYSIS LAB NO FIELD II TYPE UNITS •rn:t1(uofkQ. ~~ lJQ/kg) ~llg/kg • ~llg/kg /0/~3/:J lA LA.- lA...:: .I A.-

v So//~50 I!D./330

to/~o

' so IJe,so /()/330

I

/tJ/~3D

/ , r

' ' \ \ m'])L

J - Estimated value. Hoz.O/SOI J-K - Actual value is known to be less than value given.

( ) ( )

llQ/1 uQ/kQ uq/1 uq/kq

l - Actual value is known to be greater than value given. U - Material was analyzed for but not detected. The nurber is the Hininun Detection Limit. m1JL NA - Not analyzed. - - - _ 1/ - Tentative identification. ~/ - On NRDC List of Priority Pollutants •

. . N.C. V.i.v.i-6-i.on o6 HeaLth SeJr..v.i.c.e.6 VHS 3068-0 {4/86 Labo~o~yl

STATE LABORATORY OF PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES

P.O. BOX 28047- 306 N. WILMINGTON, ST., RALEIGH, N.C. 27611

BASE/NEUTRAL AND ACID EXTRACT ABLES

LAB NO FIELD tl

ORGANIC CHEMICAL ANAL YS lS

COf1POUND TYPE ( lJ )_ ( i../) (I..J ) (~) UNITS

Pvrene l/0/~30 benzidine lso/JbSO butyl benzyl phthalate IJ0/.!!30 benz(a)anthracene chr-ysene 3 3-dichlorobenzidine so/JI:JStJ bis(2-ethylhexyl)phthalate lo/33o di-n-octyl phthalate I/O/.S3o benzo(b)fluoranthene benzo(lc)fluoranthene benzo(a)ovrene indeno(l 2 3-cd)pyrene dibenzo(a h)anthracene , , benzo(q h i)perylene ' I ' w \

aniline .s-oli~~ ,_,..__ benzoic acid benzvl alcohol 4-ch loroani 1i ne ~ , dibeniofuran lttJ ·r.33o 2-nethylnaphthalene 2-nethvlohenol 4-nethvlohenol "' 2-nitroani 1 ine S'o!J"So 3-nitroaniline 4-n i troan i 1i ne L , 2 4 5-trichloroohenol "' '\

m'DL. J- Estimated value. Ha.OI.Sf'Jit-K - Actual value is known to be less than value given. l - Actual value is known to be greater than value given. U - Haterial was analyzed for but not detected. The nlnber is the P1ininun Detection Limit. NA - Not analyzed. 1/- Tentative identification. fl -On NROC List of Priority Pollutants.

N.C. V.<.v.i.6.<.on o 6 HeaLth SVLv.<.ce..6 VHS 3068-0 (4/86 Labo~o~yl

( ) ( )

UQ/1 lJQ/Icq lJQ/ 1 lJQ/IcQ

SOLID WASTE MANAGEMENT DIVISION SUPERFUND SECTION

Chain of Custody Record

Hazardous Waste Materials

Location of sampling: Generator ___ Transporter :==Treatment Facility ___ Storage Facility

Disposal Facility Landfill --Z:::.,.0ther: ,,..,llC(I<I~ .s'IT"f'"" ---

Company's Name t-!L Suf'ffl-fw,.IO .St"v'fto~ Telephone: Cfl'l

'" 0 I ODe.r J,'.._ fi..P.... ~ .. lt !.5 L N C.. '2,..:7& 11 76&'7 Address ___ ---'------~-----------------------------------------------------Collector Is Name e '¢- .P'Y.

signature Telephone: c, ,<7 73'1 1..~1

Date s amp 1 e d _____ l.....:' /:...._J._'J_/_<?_3~----------------T im e s amp 1 e d 1 '1 o:? -I r 1 0

lA t.. +"' L!' (2.LC<, c (,' ..,(, Type of Process Generating Waste ___ , __ ~ __________ / __ ~J~---------------

F i e 1 d Info rma ti on: __ S._:.t_.rc-_.,_ ...... ____ S_e..J. __ : ~ __ .... _+ ___ S._ .. _""'_.f,_i~_..r....~.,:...._..f' __ -r_.{ __ "'_1_-P-__ 1_f __ f2-c __ '_7_e._'_,. ..,..:..:5 __ _

(tJc.v oc:,3 s:r"i •%«t) G..,t.A H:ll tJL

Field sample No. 01{,63? O•,t.38' 01~6~'7 Qt~c.?'o -----

Chain of Possession:

inclusive dates

=z/t 44 [I~ 7 inclGsiveates

signature title inclusive dates

title

Instructions: Complete all applicable information including signatures, and submit with analysis request forms.

SOLID WASTE MANAGEMENT DIVISION SUPERFUND SECTION

CERCLA Chain of Custody Record


Location of Sampling: Generator ___ Transporter ___ Treatment Facility ___ Storage Facility

· Disposal Facility Landfill -Z::.. 0 the r : ' , .. HlcT I"'~ .sIn:=- ---

Cof!tpany 1 s Name f'lC SufG.fL-fw,JO ..{t"V'fto~ Telephone: Cf 1 'l

lAo I one.rl•'"' fl.eJ}._ ~ .. lt i5L NC '2..-""Jbll 7t,G'7 Address ___ -~'------~------------------------------------------------------Collector 1 s Name ANt ¢ ..o:;y-

. · signature Telephone: c.,'~

Date s amp 1 e d _____ l _.:.1 / __ 1-_3_/_<?--'-3 ________________ T im e s amp 1 e d 1 Yo:? -I r 1 0

111 l. +.-. L!- (2.. LCC., c (,' "'<• Type of Process Generating Waste ___ ,_-__________ / __ ~J~----------------

Field Information: S-tJ""C-"~ .,[~: ......... + .s,:.,_,el~..r, ..{'-.<.{ ,f-.~-+~ 1f fl-o '7c.1

,. -:5

Lf'lC:V D«t3 s3'"{ Cj6"f) brJt-A H:ll tJC

Field sample No. 0 1% t..o oiJ"[,-z.t

0(Jb1.. '1


J-17 ..1N.jeolo.!J ~..f- ;::- 1•fu..,t_3 title inclusive dates

t:h,_ ~"~ tl: ;) ':fr -9 z s1.gnature title incl)..lsive dates


Results Reported:

~~A-eo/. -~ s1.gnature title

. ,F-737$62-...- f35~9 7 date

Instructions: Complete all applicable information including signatures~ and submit with analysis request forms.

State of Nort.arolina Department . environment I Health and Natural Resources Division of Solid Waste Management

James B. Hunt, Jr ., Governor Jonathan B. Howes, Secretary William L. Meyer, Director

Mr. Robert Farris Environmental Health Supervisor Cabarrus County Health Department Post Office Box 1149 Concord, North Carolina 28026-11 49

October 25, 1994

RE: Site Inspection Prioritization On-Site Reconnaissance Galvan Industries, NCD00344861 0 Follow-up Sampling S & Metals Recycling, NCD093334969

Dear Ms. Farris:

:«rA DEHNR

David Lilley of the NC Superfund Section spoke with Wendy Gainey of your office today to notify you that the NC Superfund Section will conduct site inspections of the subject sites located in Caldwell County, North Carolina. The inspections will be conducted on November 7, 1994 by Stuart Parker of the NC Superfund Section.

The purpose of the inspections is to determine if the sites pose a hazard to public health or the environment because of contaminant rel eases to soil, surface water, groundwater, or air. The inspection team will take samples around S & S Metals Recycling to determine if a hazardous condition exists. Additionally, they will locate all nearby water supplies (surface and groundwater, community and private) and any close sensitive environments, schools, and day care centers in the vicinity of both sites.

These inspections are not emergency situations but are a normal step in the evaluation of all uncontrolled and unregulated potential waste sites in North Carolina. You may want to have your representative meet the inspection team at the sites. If so, please contact Stuart Parker at (91 9) 733-2801 and he will coordinate a meeting. I am enclosing background data on the sites for your information.

If the inspections indicate the need for future study of the sites, we will contact your office to advise. If you have any questions, please don't hesitate to call David Lilley or me at (919) 733-2801.

cc: Phil Prete Doug Holyfield Pat Williamson Scott Ross David Lilley Donna Keith

s· c.ef ely, f l ;Jf-c~/J~·

~iR~~o~";;,~c~ad Superfund Section

P.O. Box 27687, Raleigh , North Carolina 27611-7687 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity A ffirmat ive Action Employer 50% recycled/ l 0% post-consumer paper

I

__ j

...... - ..... • Federal • Trip Notification & Authorization

Prepared by: s+ ... .cvl f.MUv Today's Date: ( 0/ UJ/'~ 'I •use Dlack Ink or Typewriter only-S1aff to fill out first 2 blocks only.

Site Trip

Date of Trip: t1 / 7/CJt..( ----~-------------------

If trip date changed or cancelled note below: Trip Date Changed To: Cancelled:

NCD#: o~ 3 33'1 o;'j City: Go U. J.Nh

Site Name: S _.S r'1d" .. lJ ~y ... I::J ----------------

County: C4C,&.n"'.s

Reason for Trip: r::C) II o U-' '1. r .S ... "'t I,·.,. J --~--------~----~.~--~---------------------------

Name of Hotel (Overnight Trip): @ Hotel Telephone Number: (-4-~---------------

Project Team Leader: S -1-4 ,..-r f~,.J;.er

Assistants: f-1e..,-,.7 ~ .," )

Attach To Notification Form: 1 copy each: Submit to the

Industrial Hygienist

Preliminary Assessment Form (First page only) Site Map PA Transmittal Letter

(!'lease Jist appropriate County Health Depanment contact person to call to advise of trip)/)')r. ~obt?.rf fO.rri.s ~/LI/. 1/etZ./</t.. Environmental Supervisor or Health Director to call: ff!s .:U,11 7 e 47-cCcl{- Title: 5ytrcvt.50c

(Note if Dr., M.l'., etc.) _./

Telephone Number: (7tt/fJfi- :t:::f:..kf:~<B' //

Notes: Health Department Official Contacted: f!'1.F_ HJe;, ly Ga v-..~ Back Up Letter Required: Yes ~ No ___ 7

A'Jtf~~_!-L( [l!A~c dJr, fa~~~~ C'h_

No«' Sl,od origl"'l <o D•" M'"'"''

• /' ?>34'1fo 1

d:::o . le_ REMEDIAL SITE ASSESSMENT DECISION- EPA REGION IV / V · fJ

Site Name: S & S Metals Recycling Site EPA ID#: NCD 98e-659-62& C T U J ~~j4

Alias Site Names: ----------

City: Gold Hill C01mty or Parish: _ _o:C""a=barrus=.:=o..--- State: -'N::..:....::::C __

Refer to Report Dated: June 28, 1994 Report type: ...;S=IP=---------

Report developed by: Stuart Parker, NCDEHNR

DECISION:

I x I 1. Further Remedial Site Assessment under CERCLA (Superfund) is not required because:

I x I la Site does not qualify for further remedial site assessment under CERCLA

(No Further Remedial Action Planned - NFRAP)

I lb. Site may qualify for further action, but is deferred to:

I RCRA I NRC

I 2. Further Assessment Needed Under CERCLA: 2a (optional) Priority: I I Higher I I Lower

2b. Activity Type:

PA SI

Other:

ESI HRS evaluation

DISCUSSION/RATIONALE: State and Federal investigations conducted at the site between 1980 and 1994 indicated that soil and/or sludge samples from the site contained chlorinated solvents and elevated levels of chromium. However due to the lack of actual and potential target values, a disposition of no further action was assigned.

Report Reviewed and Approved by: Cynthia K Gurley

Site Decision Made by: Cynthia K Gurley Signature:

EPA Form # 9100-3

·- ---- -- ____ ____)

• • UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

4WD-WPB

MS. Pat DeRosa, Head CERCLA Branch

REGION IV

345 COURTLAND STREET. N.E. · ATLANTA. GEORGIA 30365

September 29, 1994

North Carolina Department of Environment, Health and Natural Resources

Division of Solid Waste Management P.O. Box 27687 Raleigh, North Carolina 27611-7687

Dear MS. DeRosa:

OCT 0 3 1994

The following reports have recently been reviewed and accepted by EPA - Region IV Site Assessment Section:

Site Inspections

Forbes Road Well Site Spann Property

Site Inspection Prioritizations (SIPs)

Anilox Roll Asheboro Municipal Landfill Ashland Petroleum Company BP Oil Carochem Cone Mills Corporation Plant Croft Metals Dayco Corporation Eaton Corporation Fasco Industries, Inc. Gaston Co., Dyeing Machine Company Gaston Co., Dyeing Machine Company (Stanley) Greensboro City Landfill Harrisburg Park Landfill Henson Landfill Highway 8 01 Barber . Holding Pond for Scrubber Waste Honeywell Micro Switch Division Kelly-Springfield Tire Company Lee County Landfill Marantz Piano Company Old Western NC Fairgrounds

NFRAP NFRAP

NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP Further Action NFRAP NFRAP NFRAP

r- ··-i ' - •

Olin Corp . Ecusta Paper & Film Pantasote, Inc. REA Magnet Wire Company Rowe Corporation Property S&S Metals Recycling Site Scovill Inc. Stewart-Warner Site Superior Products Company Texaco, Inc. Torpedo Wire and Strip Union County Landfill Uniroyal, Inc.

EXPANDED SITE INSPECTION

Davis Park Road TCE Site

2

Group

• NFRAP NFRAP Further Action NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP NFRAP Further Action NFRAP

Further Action

Enclosed please find the Remedial Site Assessment Decision Forms for each report generated by the North Carolina Superfund program and a copy of the actual report generated by the EPA Contractor.

If you have any questions concerning these site decisions, please call me at (404) 347-5059, Extension 6150 .

Enclosures

Sincerely,

C~-\-\~, Cll\J{\ly Cynthia K. Gurley North Carolina, PO

I State of NorthA,rolina Department o~vironment, Health and Natural Resources Division of Solid Waste Management

James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary William L Meyer, Director

Mr. Robert Farris Environmental Health Supervisor Cabarrus County Health Department Post Office Box 1149 Concord, North Carolina 28026-1149

RE: Follow-Up Sampling S & S Metals NCO 093 334 969

Dear Mr. Farris:

March 11, 1994

:;.;rA DEHNR.

David Lilley of the North Carolina Superfund Section spoke with you today to notify you that the North Carolina Superfund Section will conduct a site inspection of the subject site located in Cabarrus County, North Carolina. The inspection will be conducted on March 31, 1994 by Stuart Parker of the NC Superfund Section.

The purpose of the inspection is to determine if the. site poses a hazard to public health or the environment because of releases of contaminants to soil, surface water, groundwater, or air.

This inspection is not an emergency situation but is a normal step in the evaluation of all uncontrolled and unregulated potential hazardous waste sites in North Carolina. You may want to have your representative meet the inspection team at the site. If so, please contact Stuart Parker at (919) 733-2801 and he will coordinate a meeting. I am enclosing background data on the site for your information.

If the inspection indicates the need for future study of the site, we will contact your office to advise. If you have any questions, please don't hesitate to call David Lilley or me at (919) 733-280L

Enclosures

cc: Dexter Matthews Doug Holyfield Pat Williamson Kim Clarke David Lilley Donna Keith

Sincerely,

Pat DeRosa, Head CERCI.A Branch NC Superfund Section

P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/1 0% post-consumer paper

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Note: Signed original to Data Manager

I •

State of North A olina Department u~vironment, Health and Natural Resources Division of Solid Waste Management

James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary

- -·----

DEHNR

November 4, 1993

Mr. Robert Farris Environmental Health Supervisor Cabarrus County Health Department Post Office Box 1149 Concord, NC 28026-1149

RE: Site Inspection Prioritization S & S Metals Recycling NCD 093 334 969

Dear Mr. Farris:

David Lilley of the NC Superfund Section spoke with David Troutman of your office today to notify you that the NC Superfund Section will conduct a site inspection of the subject site located in Cabarrus County, NC. The inspection will be conducted on November 23, 1993 by Stuart Parker of the NC Superfund Section.

The purpose of the inspection is to determine if the site poses a hazard to public health or the environment because of releases of contaminants to soil, surface water, groundwater, or air.

This inspection is not an emergency situation but is a normal step in the evaluation of all uncontrolled and unregulated potential hazardous waste sites in North Carolina. You may want to have your representative meet the inspection team at the site. If so, please contact Stuart Parker at (919) 733-2801 and he will coordinate a meeting. I am enclosing background data on the site for your information.

P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone 919-733-4996 FI\X. 919-733-4810 An Equal Opportunity Affirmative Acti on Employer 50% recycled/ 1 0% post-consumer paper

------ - - ---- --

_ ..

' ..

Mr. Farris 11-4-93 Page 2

• • If the inspection indicated the need for future study of the site, we will contact your

office to advise. If you have any questions, please don't hesitate to call David Lilley or me at (919) 733-2801.

Enclosures

cc: Dexter Matthews Doug Holyfield Debbie Crane Kim Clarke David Lilley File

Sincerely,


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• • State of North Carolina

Department of Environment, Health, and Natural Resources Division of Solid Waste Management

James G. Martin, Govemo~ William W. Cobey, Jr., Secretary

Ms. Mae R. Knight cfo Ms. Becky Cooke 3710 Gold Hill Road East Gold Hill, NC·28071

Dear Ms. Cooke:

5 November 1992 William L. Meyer

Director

On 23 September 1992 I took samples of water from your well and sent them to the State Laboratory For Public Health for analyses. On 29 October 1992, I received the final results of the analyses from the laboratory, and now I want to transmit those results to you.

1. There were no detectable levels of inorganic elements (metals) or PCB in the samples.

2. The only organic chemicals detected in the samples were chloroform, at a concentration of less than 1 microgram per liter, and traces of p-xylene and m-xylene. According to the NC Environmental Epidemiology Section, the concentration of chloroform is well below the Maximum Contaminant Level (MCL) of about 100 micrograms per liter and is not a health risk. The xylene concentrations are well below the MCL of 10000 milligrams per liter and are not a health risk. The MCL is the maximum permissible concentration of a substance in water that is delivered to any user of a public water supply.

Since several area residents reported a "rotten egg" taste and smell to the water, I suggest that the water be tested for iron and sulfur bacteria by the Cabarrus County Health Department, telephone 704 786-8121. If you have any questions about these results, please call me at (919) 733-2801.

f/;Si:eAJd <_

ver Nichols~~~iron. Engr. NC Superfund Section

P. 0. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-4996 An Equal Opportunity Affirmative Action Employer




Delmer and Joanna Cauble 14840 Short Cut Road Gold Hill, NC 28071

Dear Mr. and Mrs. Cauble:

5 November 1992

William L Meyer Director

on 23 September 1992 I took samples of water from your well and sent them to the state Laboratory For Public Health for analyses. on 29 October 1992, I received the final results of the analyses from the laboratory, and now I want to transmit those results to you.

1. There were no detectable levels of inorganic elements (metals) or PCB in the samples, except barium, which was detected at a concentration of 0. 06 milligrams per liter. According to the NC Epidemiology Section, this concentration is well below the Maximum Contaminant Level (MCL) of 1 milligram per liter. The MCL is the maximum permissible concentration of a substance in water that is delivered to any user of a public water supply.

2. The only organic chemical detected in the samples was 1,1-dichloroethane, at a concentration of 1.3 micrograms per liter. According to the NC Environmental Epidemiology Section, this concentration is well below the calculated health protection level of about 700 micrograms per liter and is not a health risk.

since several area residents reported a "rotten egg" taste and smell to the water, I suggest that the water be tested for iron and sulfur bacteria by the Cabarrus County Health Department, telephone 704 786-8121. If you have any questions about these results, please call me at (919) 733-2801.

Sincerely, j1 ~

~:::/!!~o~viron. NC Superfund Section


Engr.



James G. Martin, Governo~ William W. Cobey, Jr., Secretary

Ms. Paula Sue Smarr 14638 Short Cut Road Gold Hill, NC 28071

Dear Ms. Smarr:

5 November 1992


On 23 September 1992 I took samples of water from your well and sent them to the State Laboratory For Public Health for analyses. On 29 October 1992, I received the final results of the analyses from the laboratory, and now I want to transmit those results to you •.

1. There were no detectable levels of inorganic elements (metals) or PCB in the samples.

2. The only organic chemical detected in the samples was chloroform, at a concentration of less than 1 microgram per liter. According to the NC Environmental Epidemiology Section, this concentration is well below the Maximum Contaminant Level (MCL) of about 100 micrograms per liter and is not a health risk. The MCL is the maximum permissible concentration of a substance in water that is delivered to any user of a public water supply.

Since several area residents reported a "rotten egg" taste and smell to the water, I suggest that the water be tested for iron and sulfur bacteria by the Cabarrus County Health Department, telephone 704 786-8121. If you have any questions about these results, please call me at (919) 733-2801.

JJ;;;i,~ Sincerely, ~

o~ichols , Environ. Engr. C Superfund Section





5 November 1992

To: File

From: Grover Nicholson

Re: Well sampling results around s&s Metals


On 14 October 1992 I spoke with Dr. Luanne Williams of the NC Environmental Epidemiology Section. We discussed the possible causes of the health problems experienced by three residents around the S&S Metals site. We were trying to find some connection between these symptoms and possible contaminants in the well water. Hair loss seemed to be the common symptom, and Dr. Williams discovered that excess selenium can cause hair loss and other health problems. However, selenium was not found in any of the samples.

on 3 November 1992 and on 5 November 1992, I again spoke with Dr. Williams about the contaminants that were found in the well water. These were chloroform, 1,1-dichloroethane, p-xylene, and m-xylene. Dr. Williams told me that the MCL for chloroform is about 100 ugfl, that the health protective level for 1,1-dichloroethane is about 700 ugfl, and that the MCL for xylene is about 10000 mgfl. We also continued to discuss possibilities concerning the causes of the health problems since there were no contaminants of consequence found in any of the samples. Finally, we decided that the most logical next step would be to have the well water analyzed for iron and sulfur bacteria.


• Memo to file 3 November 1992 page 4

• 2 • Cauble Well: PCB and inorganics were below the

detection limits, except barium, which was detected but at a concentration below the MCL. The only organic detected was 1,1-Dichloroethane, at a concentration of 1.3 ugjl. Again, according to Dr. Luanne Williams, this concentration is well below the calculated health protection level of about 700 ugfl.

3. Knight Well: PCB and all inorganics were below the detection limits. The only organics detected were chloroform at a concentration of less than 1 ugjl, and a trace of p-xylene and m-xylene. Again, the concentration of chloroform is below the MCL and the other two contaminants are at concentrations too low to be quantified.

Ken Henson, the Cabarrus County Health Department representative, supplied us with a bacteriologic analysis of a sample of water taken from Ms. Smarr's well on 29 October 1991. The analysis showed that no total coliform and no fecal coliform were present. The same sample was analyzed for volatile organics but none were found. I also checked with Colonel Leslie Everette, the state Aviation Officer for the NC National Guard, 919 664-6000, concerning the reported helicopter activity near the site. He told me that National Guard helicopters were used in pairs to search for drugs in that area.

I also checked with Dr. Luanne Williams of the NC Epidemiology Section twice about possible causes for the residents' illnesses. A possible cause of hair loss and diarrhea is selenium, but no selenium was found in the well water samples. I also checked with Bob Cheek, a hydrogeologist with the NC Ground Water Section, who has much experience dealing with drinking water wells. He suggested that the smell and taste or the water described by the residents could be caused by either iron or sulfur bacteria. Dr. Williams also suggested that these bacteria could cause gastrointestinal illnesses.

Based on the laboratory analyses and the other information gathered, I do not believe that any of the three wells are contaminated with inorganic or organic chemicals. We did not analyses for pesticides or herbicides since we do not think they were disposed at S&S Metals. I do not have any evidence that the well water is the source of the reported health problems, but I do recommend that the health department sample all the wells and analyze for iron and sulfur bacteria.

J

J I

I

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Department of Environn1ent, Health, and Natural Resources Division of Solid Waste Management

James G. Martin, Governor William W. Cobey, Jr. , Secretary

5 November 1992

Mr. Ken Henson, Specialist Environmental Health Program Cabarrus County Health Department PO Box 1149 Concord, NC 28026-1149

Dear Mr. Henson:

William L. Meyer D irector

Please find attached a copy of my memorandum report on t he sampling of three residential wells in the Gold Hill community. The report describes our actions in response to the reported contamination and discusses the results of the sample analyses. In summary, our analyses did not find any contaminant in the well water that could cause a health effect. As I told you today , I have sent all three residents the laboratory results and recommended to each that t hey have their well water tested for iron and sulfur bacteria.

Thank you for your assistance on 23 September 1992 during our interviews with Ms. Smarr, and for your help in e xamining h e r well. If you have any questions about the report, or if you discover any additional data that may be pertinent to the problem, please call me at (919) 733-2801.

Attachment

q:yv~{c drover Nicholso:! ::ron. Engr.

VNC Superfund Section

P. 0. Box 27687, RAle igh , No rth Caroli na 27611-7687 Telephone 919-733-4996 An Equal Opportu nity Affirmative Action Employer

State Laboratory of Public Health - Division of Laqoratory Servi ces ~.; N.C. D€' partment of Environment, Health, and Natural Resources 1,.

P.O. Box 28047-306 N. Wilmington St.- Raleigh, N.C. 27611 -8047

~ DRINKING WATER DESCRIPTION .BLA'Nk _::.~FILLED IN BY SENDER COLIFORM ANALYSIS- PRIVATE SUPPLY

County Cc- /; .. , •..-v

Type of ~am piing Point --'-""""---"---'--/ 1 __ +----"""--r--<-------------,......---r~ /

Co II ected By ~/??...:._:__L. _______ D_A_T_E_/_:e.-~· -='2=-rrr --'7-:..L";.;_T_I_M_E~j_: _(.,l.::._t·'--'__..l.---11

Source: E]'W'e l!

Signed By:

Ad

DEHNR 1294 (Revised 1 0/ 90) Laboratory

Zip

ALL INFORMATION REQUESTED MUST BE GIVEN.

I -..- :

BACTERIOLOGIC ANALYSIS

RESULT CONTAMINANT PRESENT ABSEf'

TOTAL COLIFORM

FECAL/E. COLI

\

t

0

0

REPORTED,

Do not write on thi s side of form. HOV 4 1991



James G. Martin, Govemo~ William W. Cobey, Jr., Secretary 3 November 1992

William L. Meyer Director

To: File

From:

Re:

Grover Nicholson 5'~ Sampling of three residential wells around S&S Metals Recycling Company, NCO 093 334 969, Gold Hill, Cabarrus County, NC.

On 17 September 1992, the NC Division of Solid Waste Management received a call from Barbara Hollinsworth, an attorney in Concord, NC, 704 788-8240. Ms. Hollinsworth represents Paula Sue smarr of Gold Hill, NC. Ms. Hollinsworth notified the Division that Ms. Smarr believed her well to be contaminated, possibly by contaminants from a nearby CERCLA site. This notification was referred· to the NC Superfund Section and, after some further investigation, I determined that Ms. Smarr's house and well were within about 1500 feet of S&S Metals Recycling Company. The NC Superfund section had performed a site investigation of the S&S Metals site in February 1987. At that time, the nearest well to the site, owned by Dr. Houghton, was sampled and found to be uncontaminated. However, soil on the site and some sediments around the site were found to be contaminated with chromium and lead and, in May 1987, the site investigation report was forwarded to the us EPA with a recommendation that further investigation be conducted at the site.

Ms. Smarr had reported that she and her children had been ill, and that she suspected that the reason was contamination in her well water. I called Ms. Houghton, whose well we had sampled before, and found that several other houses had been built around the site since our investigation in 1987. I discussed all this with Mike Kelly, the Deputy Division Director, and we both felt that the best course of action would be to sample three wells around the site. I made arrangements to sample the wells on 23 September 1992. Ken Henson of the Cabarrus ·County Health Department agreed to meet us at the site. Ms. Smarr could not be contacted because she has no telephone, and Ms. Hollinsworth was on vacation. However, Feli ta Reid, Ms. Hollinsworth's secretary, managed to send a letter to Ms. Smarr. other residents were not contacted, since I did not know their names or addresses.

P. 0. Box 27687, Raleigh, North Carolina 27611-7687 Telephone 919-733-4996 An Equal Opportunity Affinnative Action Employer

• Memo to file 3 November 1992 page 2

• Grover Nicholson and Harry Zinn of the NC Superfund Section

arrived at Ms. Smarr's mobile home at 1045 on 23 September 1992. Ken Henson arrived about 15 minutes later. Her address is 14638 Short Cut Road, Gold Hill, NC, 28071. Ms. Smarr was at home and we discussed her concerns about her well. She told us the following:

1. S&S Metals (the site) is owned by Mr. Schwartz of Concord.

2 • Joanna Cauble lives closest to the site, on the east side.

3. Paint sludges were dug up at the site last year.

4. Terry Beachum, a nearby resident (telephone # unknown) knows of transformers being buried at the site.

5. Military helicopters circle and land at the site.

6. Ms. Smarr and her son have seen men around their property at night using high intensity red lights. These lights have been shone into her house.

7. Four men in suits driving a car with a permanent license tag were walking around the site in June or July 1992.

8. Ms. Smarr and two of her sons, who all live at the mobile home, have had health problems. These problems were described as general sickness, red skins rashes, and loss of hair.

9. Ms. Smarr's well was drilled in 1973. It is 6 inches in diameter, 104 feet deep, and has a submersible pump.

Ms. Smarr's well and holding tank were unenclosed but partially wrapped in insulation and plastic. Based on surface probing by Ken Henson, the well's annular space is ungrouted. There was no well construction tag on the casing. We purged the well by letting it run for 15 minutes and then collected water samples for inorganics, and for volatile and semi-volatile organics. Then we went to locate Joanna Cauble's house, which was just on the east side of the site.

• Memo to file 3 November 1992 Page 3

• Delmer and Joanna Cauble live at 14840 Short Cut Road, Gold

Hill, NC, 28071. We met Joanna Cauble at her house and she gave us permission to sample the well. The well and holding tank were protected by a small cover, and a concrete pad was in place around the well. The well construction tag told us that the well was drilled on 16 September 1987 by Teague Well Drilling of Kannapolis, NC, #101, and that it is 6 inches in diameter, 115 feet deep, and has 30 feet of casing. Water is pumped out of the well by a jet pump on the surface. Ms. Cauble told us that the well water smelled and tasted bad, like rotten eggs, and that she used bottled water for drinking. After purging the Cauble well we took samples just as we did at the Smarr well.

After sampling the Cauble well, we reconned the south side of the site until we found the closest well. The well is at the home of Mae R. Knight, 3710 Gold Hill Road East, Gold Hill, NC, 28071. Ms. Knight was not available, but her daughter, Becky Cooke, had been living there for three months with her husband and her four children. We spoke with Ms. Cooke and she told us the following:

1. Since they had been living at the house, the Cooke's had experienced a more than normal amount of sickness, especially stomach problems and diarrhea. The youngest son (less than 2 years old) had gastritis three times and another son had hair loss.

2. The well water smelled like sulfur and tasted bad. It stained clothes a rusty color. About every two months, they would treat the well by pouring clorox into it, letting it stand for a while, and then purging it.

The well and tank were protected by a well house with a concrete floor. The well house looked clean. After purging the well, we sampled the water as we did the other two wells.

All samples were delivered to the NC Laboratory for Public Health on 24 September 1992. Final analyses were received on 29 october 1992. These data reveal the following:

1. Smarr Well: PCB and inorganics were all below detection limits. The only organic found was chloroform at a concentration of less than 1 ugfl. According to Dr. Luanne Williams of the Environmental Epidemiology Section, this is well below the MCL of about 100 ug/1.

• Health and Natur~Resources N.C. Dept . of Environment, Division of Laboratory Services

State Laboratory of Public Heal th P.O. Box 2804 7, Raleigh, N. C. 27611

Environmental Sciences Analysis Report EIN 5f3-(JC;J02St

Name of Own er, Pati ent or Suppl y; PCA lA. lo. s ~ Gt r,..

Address : ...:.1_:_7'~&~3~8ot_ _ _:.S:::.....Lhuour-:..lt=:....:c!.-<A..>t-=.._.--L!o.£=-.!cJ.~. _

Counly: _£_g_Lr- "'-.r

Report To: /Yl -Ji o,..,-.p .J '' I

Addres s :

.... " ; .

Date Collected: 27 ,

Coll ec ted By:

Analysis Desired:

I '7 9/

Labor a tor·y Sample Sample Description Number Number - s-13886

61tfrtf21e -S13887 111 b ' jj]A_J_ --- -- ---

-

- - -

------ ·-·--·--~ --

---··· ·- - - -- -- --- - -- f-- ---- - ·--

- -

- - -

-

or Remarks

?m~

- -

Results In

~ILE COMPOUNDSIUUUltWI

~ - ----

- -- ----- - ---

Date Received !o- 3o-qr AA Date Reported /./- 6' -9 I Date Extracted

DEHNR Fo rm 2364 Revi sed (9-89) Laboratory

Date Analyzed ~ ~ Reported By : j;- ~

l_

---------~-- -~ - -- -·- · ------- · ~ ·--·--- - - -------

N. C . .... 0 TMENT OF ENVIRONMENT, HEALTH, & NAT'~RESOURCES DIVISION~LABORATORY SERVICES, ENVIRONMENTAL S~CES SECTION

- ·- ·---- ----- --,

laboratory No . 9 P.O. BOX 28047- 306 N. WILMINGTON ST, RALEIGH, N.C. 27611

j__ 3 )._ Q 9 PURGEABLE COMPOUNDS Date of Analysis

COMPOUND lJg/1 COMPOUND lJg/1

Dichlorodifluoromethane u Ch1orobenzene "' Chloromethane Ethv1benzene VVinyl Chloride l l 1 2-Tetrachloroethane Braocmethane P-Xv1ene Chloroethane m-Xvlene Trichlorofluoromethane o-Xvlene

yJ 1-Dichloroethvlene Stvrene Hethvlene Chloride Bromoform tert-Butyl Hethvl Ether Isooroov1benzene trans-1 2-Dichloroethvlene l 1 2 2-Tetrachloroethane Isopropyl ether Branobenzene l 1-Dichloroethane n-Proov1benzene 2 2-Dichloroorooane 1 2 3-Trich1oroorooane cis-1 2-Dichloroethylene \ 2--Ch1oroto1uene Chloroform lK. ., l 3 5-Trimethv1benzene (BCM) Bromochloromethane -~- 4--Chlorotoluene

Yl 1 1-Trich1oroethane tert-Butvl Benzene l 1-Dichloroprooene Pentachloroethane

Ycarbon Tetrachloride l 2,4-Trimethvlbenzene YBenzene sec-Butvl Benzene Yl,2-Dichloroethane p-Isopropvltoluene YTrichloroethvlene l 3-Dichlorobenzene

1 2-Dichloropropane Yl 4-Dichlorobenzene Bromodichloromethane n-Butvlbenzene Dibraocmethane l 2-Dichlorobenzene Toluene Bis (2--Chloroisooroovl) Ether l l 2-Trichloroethane l 2-Dibromo-3--Chloropropane

Tetrachloroethylene l 2 4-Trichlorobenzene l 3-Dichloropropane Hexachlorobutadiene Dibromochloromethane Naphthalene 1 2-Dibromoethane (EDB) 1 2 3-Trich1orobenzene \

1--Chlorohexane \

MDL- Minimum Detection Limit for water (EPA Method 502.2), is 1.0 llg/1.

J - Estimated value. K - Actual value is known to be less than value given. l -Actual value is known to be greater than value given . U - Material was analyzed for but not detected. NA - Not analyzed . 1/ -Tentative identification. y - Re~ulated VOC T - Tr1halomethane

N.C. Dept. of Environment, Health, & Natural Resources DEHNR 3068-0 (Rev. l/91 Laboratory Services)

--- - - ----. -- - ------ - - ---- - - - - -

-------- - --- -----·- ----

N. C . .... 0 TMENT OF ENVIRONMENT, HEALTH, & NATI~RESOURCES DIVISION~LABORATORY SERVICES, ENVIRONMENTAL S~CES SECTION

P.O. BOX 28047- 306 N. WILMINGTON ST, RALEIGH, N.C. 27611

923:2 /:J_ PURGEABLE COMPOUNDS Laboratory No . Date of Analysis

COMPOUND vg/1 COMPOUND

Dichlorodifluoromethane u. Chlorobenzene Chloromethane Ethyl benzene

v'Vinyl Chloride 1 1 1 2-Tetrachloroethane Braocmethane p-Xyl ene Chloroethane m-Xvlene Trichlorofluoromethane o-Xylene

-/"1 1-Dichloroethvlene Stvrene Methylene Chloride Bromofonn tert-Butyl Methyl Ether Isopropyl benzene trans-1 2-Dichloroethvlene 1 1 2 2-Tetrachloroethane Isopropyl ether JJ Branobenzene 1 1-Dichloroethane I _1, n-Propylbenzene 2 2-Dichloropropane / J 1 2 3-Trichloroorooane cis-1 2-Dichloroethvlene 2-Chlorotoluene Chlorofonn 1 3 5-Trimethvlbenzene (BCM) Bromochloromethane 4-Chlorotoluene

-1"1, 1, ]-Trichloroethane tert-Butvl Benzene 1 1-Dichloropropene Pentachloroethane

-/"Carbon Tetrachloride 1 2 4-Trimethvlbenzene -/"Benzene sec-Butvl Benzene -/"1 2-Dichloroethane o-Isopropvlto 1 uene -/"Trichloroethylene 1 3-Dichlorobenzene

1 2-Dichloroprooane -/"1 4-Dichlorobenzene Bromodichloromethane n-Butvlbenzene Dibraocmethane 1 2-Dichlorobenzene Toluene Bis (2-Chloroisooroovl) Ether 1 1 2-Trichloroethane 1 2-Dibromo-3-Chloroorooane

Tetrachloroethylene 1 2 4-Trichlorobenzene l, 3-Di ch 1 oroorooane Hexachlorobutadiene Dibromochloromethane Naphthalene l 2-Dibromoethane (EDB) 1 2 3-Trichlorobenzene 1-Chlorohexane -u

MDL- Minimum Detection Limit for water (EPA Method 502.2), is 1.0 JJQ/1.

J - Estimated value. K - Actual value is known to be less than va lue given. l -Actual value is known to be greater than value given. U - Material was analyzed for but not detected. NA - Not analyzed. 1/ - Tentative identification . -/" - Regulated VOC T - Trihalomethane

N.C. Dept . of Environment, Health, & Natural Resources DEHNR 3068-0 (Rev. 1/91 Laboratory Services)

------- -- ·--- --- - - - - - --------------· ·-

-l

JJQ/1

lA

~

- -----_I

L

N. C. ~0TMENT OF ENVIRONMENT, HEALTH, & NAT~ RESOURCES OIVISION~~ABORATORY SERVICES, ENVIRONMENTAL S~CES SECTION

Laboratory No .

5? P.O. BOX 28047- 306 N. WILMINGTON ST, RALEIGH, N.C. 27611

t2.. j :J_ /3 PURGEABLE COf1POUNOS Date of Ana 1 ys is

<X>HPOUND lJQ/1 <X>HPOUND

Dichlorodifluoromethane lA Chlorobenzene Chloromethane Ethvlbenzene

VVinyl Chloride l 1 1 2-Tetrachloroethane Braocrnethane o-Xvlene Chloroethane m-Xvlene Trichlorofluoromethane o-Xvlene

vl 1-0ichloroethylene Stvrene Methylene Chloride Bromoform tert-Butvl Hethvl Ether Isooroovlbenzene trans-1 2-0ichloroethvlene 1 1 2 2-Tetrachloroethane Isopropyl ether Brarobenzene 1 1-0ichloroethane n-Proovlbenzene 2 2-Dichloroprooane 1 2 3-Trichloroorooane cis-1 2-Dichloroethvlene 2-Chlorotoluene Chloroform \k. .,.. l 3 5-Trimethvlbenzene (BCH) Bromochloromethane u 4-Chlorotoluene

vl 1 ]-Trichloroethane tert-Butvl Benzene 1 1-0ichloroprooene Pentachloroethane

vCarbon Tetrachloride 1 2 4-Trimethvlbenzene vBenzene sec-Butvl Benzene vl 2-0ichloroethane o- Isooroovltoluene vTrichloroethylene 1 3-0ichlorobenzene

1 2-Dichloropropane vl 4-Dichlorobenzene Bromodichloromethane n-Butvlbenzene Dibraocrnethane 1 2-Dichlorobenzene Toluene Bis (2-Chloroisooroovl) Ether 1~_1,2-Trichloroethane 1 2-Dibromo-3-Chloropropane

Tetrachloroethylene 1 2 4-Trichlorobenzene 1 3-0ichloroorooane Hexachlorobutadiene Oibromochloromethane Naphthalene l 2-0ibromoethane (EDB) 1 2 3-Trichlorobenzene 1-Chlorohexane II

MDL- Minimum Detection Limit for water (EPA Method 502.2), i s 1.0 lJg/1.

J -Estimated value. K - Actual value is known to be less than value given. L - Actual value is known to be greater than value given. U - Materia l was analyzed for but not detected. NA - Not analyzed. 1/ - Tentat i ve identification. v - Regulated VOC T - Trihalomethane

N.C. Dept . of Environment, Health, & Natura l Resources OEHNR 3068-0 (Rev. 1/91 Laboratory Services)

lJg/1

l

.v J +ra l'_ e2-

J 11

\

N. C •• 0 THENT OF ENVIRONMENT, HEALTH, & NAT1.RESOURCES DIVISION~ LABORATORY SERVICES, ENVIRONMENTAL S~CES SECTION

Laboratory No. f P.O. BOX 28047 - 306 N. WILMINGTON ST, RALEIGH. N.C. 27611 'it ! 2JJ- /5 PURGEABLE COMPOUNDS Date of Analysis ~ (J ~ 9.P

COMPOUND pg/1 COMPOUND

Dichlorodifluoromethane lA Chlorobenzene Chloromethane Ethvlbenzene ~invl Chloride 1. 1. 1,2-Tetrachloroethane Braranethane _p-Xylene Chloroethane m-~lene

Trichlorofluoromethane o-Xvlene "1.1-Dichloroethvlene Styrene Hethvlene Chloride Bromofonn tert-Butvl Hethvl Ether Isooroovlbenzene trans-1 2-Dichloroethylene 1. 1,2,2-Tetrachloroethane Isooroovl ether Bromobenzene 1. 1-Dichloroethane n-Proovlbenzene 2 2-Dichloroorooane 1 2 3-Trichlo ne cis-1 2-Dichloroethvlene 2-Chlorotoluene Chloroform 1 3 5-Trimethvlbenzene (BCH) Bromochloranethane 4-Ch 1 oro to 1 uene

"1. 1. 1-Trichloroethane tert-Butvl Benzene 1 1-Dichloroorooene Pentachloroethane

"carbon Tetrachloride 1 2 4-Trimethylbenzene ~nzene sec-Butyl Benzene "1 2-Dichloroethane _p-I~rQQYltoluene ~richloroethvlene 1 3-Dichlorobenzene 1.2-Dichloroorooane "1 4-Dichlorobenzene Bromodichloranethane n-Butvlbenzene Dibraranethane 1 2-Dichlorobenzene Toluene Bis (2-Chloroisaprapyl) Ether 1 1 2-Trichloroethane 1.2-Dibromo-3-Chloropropane Tetrachloroethvlene 1 2.4-Trichlorobenzene 1 3-Dichloroorooane Hexachlorobutadiene Dibromochloranethane Naphthalene 1 2-0ibromoethane (EDB) 1~ ~3-Tri ch 1 orobenzene 1-Chlorohexane \If

OOPIENTS:

HDL- Minimum Detection Limit for water (EPA Method 502.2), is 1.0 pg/1.

J - Estimated value. K - Actual value is known to be less than value given. L - Actual value is known to be greater than value given. U - Material was analyzed for but not detected. NA - Not analyzed. 1/ - Tentative identification. " - Re~ulated VOC T - Trlhalomethane

N.C. Dept. of Environment. Health. & Natural Resources DEHNR 3068-0 (Rev. 1/91 Laboratory Services)

pg/1

L

-·· · - - -- ·-----------

N.C. Departr:·:e~t of Environment, llca::h , & 1\:atural Resources

So li.:: Waste ManJgcmcnt Division

. AMPLE ANALYSIS REQUEST • _ State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Stree t


-S.it~ ~umber )./C)) !)'7.3 3.3-1- t:f b 9

Name of SiteS~ S /i1~?$ il:c-Ycti/J~ Collected By c;; , AfiCtfOL.:50~ ID# 3'=1

Field Sample Number _ _.s._/..=:::5=-3=-9!~0=:::.._ _______ _

Site Location Gt> L.- r:> f/1 L L

Date ColJected 23 sEP <=j 2-

Jt.JG Time I ;5o

Agency: Hazardous Waste Solid Waste ){_Superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results (mg/1)


X Ground water (1) c:?m ft /2_12_ WELL --

_Solid (5) Cadmium --Chromi • ~ " --

__ Surface water (2) _Liquid (6) Lead .vb.u , &::;. L./ --_Sludge (7) hEAP r;;

__ Mercury o cT , ,.,,..._,.,

_Soil (3) /HJ.&-J.. YSE 70 Selenium I 1 ) 1::1::1L. --

__ Other (8) J)/a~IIVC, dJfrr£12__ Silver -- SUPE" u _,r.C _Other (4) Ul --

J... 1/tl. I TS ----

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1) J(_ P&T:GC/MS Arsenic benzene -- --

Acid:B/N Ext. Barium carbon tetrachloride -- -- --MTBE Cadmium chlordane -- -- --


-- __ Copper o-cresol --Fluoride m-cresol -- -- --Iron __ p-cresol -- -- Lead cresol -- -- --

-- __ Manganese -- 1,4-dichlorobenzene

-- __ Mercury -- 1,2-dichloroethane

-- Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene -- --Silver heptachlor -- --

Radiochemistry Sulfates hexachlorobenzene -- --·······-·· Zinc hexachlorobutadiene -- --

Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone


------ __ pyridine


-- __ trichloroethylene Parameter Results (Col/lOOml) -- __ 2,4,5-trichlorophenol

-- -- __ 2,4,6-trichlorophenol

-- -- -- vinyl chloride endrin --

q_ 2)/ - Cfl M? Repo,tcd b~~ lindane

Date Received --__ methoxychlor

-- toxaphene D:.tlc Extraclc.: cl Date Reported / ,1- g-f ?-- 2,4-D --

Dale Analyzed VDl/.J.-.5 )9~\ 923209 2,4,5-TP (Silvex)

Lab Number --D II S 31'11 (Revised 2/Y) i

L -- -------- J

N.C. Pepartrne.nt or Environment, llcarth, & Natural Resources


.. ernPLE ANALYSIS REQUEST •. State Laboratory or Public Health P.O. Box 28047, 306 N. Wilmington Street


s'ii~ N~~ber NC:D 12'13 :6.3-1- '16 9 · Field Sample Number_ ..... /_5_..::3::;.._":1-_/ _______ _

Name of Site 5 ~ S /J?Eti!Jt.$ Jli:.,YC(,.1,1.)ry ·.Site Location Gt>LP ·. f!tLl- ·

Colle~ted By ~ , IJICtf()Le50J\JID# ~=~-- Date Collected 2-"3 sgP <JZ.. Time__,./...:./......;§;;...._tJ __

Agency: Hazardous Waste Solid Waste -- Xsuperfund TCLP Compounds


Barium L Ground water (1) ,;5 ~wv1-e R- t(_}ez-L --__ Solid (5) Cadmium --

.. . . .. Chromium --__ Surface water (2) _Liquid (6) Lead -

_Sludge (7) I LEI't$~ JI..J.ML't[F Mercury

_Soil (3) 77J --Selenium --_ Other (8) dJRJ fJ K.f}.) <:; dJAre£

Silver --_Other (4) --~At tiS --

--Organic Chemistry Inorganic Chemistry --

.. Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) P&T:GC/MS Arsenic benzene

K Acid:B/N Ext. -- --

carbon tetrachloride Barium -- --.. MTBE Cadmium chlordane -- --JLPc.B <o.ooo/oo,., Chloride chlorobenzene -- --I I

Chromium chloroform -- --__ Copper o-cresol -- --Fluoride m-cresol -- -- = p-cresol -- Iron --

.. . Lead cresol -- -- Manganese = 1,4-dichlorobenzene ---- __ Mercury __ 1,2-dichloroethane

Nitrate __ 1,1-dichloroethylene -- --Selenium __ 2,4-dinitrotoluene --Silver heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --··-- Zinc hexachlorobutadiene

Results (PCI/1) =pH --Parameter hexachloroethane

__ Gross Alpha __ Conductivity -- methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- -- pentachlorophenol TOC --

-- __ pyridine


-- __ trichloroethylene Parameter Results (Col/100ml) __ 2,4,5-trichlorophenol ---- -- __ 2,4,6-trichlorophenol


q- ~({ .. C{& ~ Reported by lindane --Date Received __ methoxychlor

Bll/fi __ toxaphene Date Extracted q :~-9&> SA.WG- Date Reported __ 2,4-D

~eeq -.:l?-7.z.. vPJJV\. _ 2,4,5-TP (Silvex) Date Analy; ?l-..z?-9 .. Z:JIP ;./ Lab Number 923210 DIIS 31'.11 (Revised 2/91l/PJAJO·tr9J..81JJ. --

I

- ---~- -~ --~-----

N.C. Department of Environment, llcalth, & Natural Resources


. AMPLE ANALYSIS REQUEST • State Laboratory of Public Health

P.O. Box 28047, 306 N. Wilmington Stree t RBieigh, North Carolina 27611

Site Number A/C)) /213 33-+ '1 b 9

Name of Site 5 ~ S /f7 EFTiil$ &YC?IJ.k?j

Collected By c;;; , )J;(_ t10Lt6'0t.J ID#_ 3'=1

Field Sample Number _ _ .....:/:.......!::b:.....=5::.._:_/ .....:G=----------

Site Location Gv L. r:> f/1 L L

Date Collected 2;3 sEP Cj 2-

NG Time /ISO

Agency: Hazardous Waste Solid Waste _K__superfund TCLP Compounds -- --Sample Type Inorganic Compounds Results (mgjl)


J{_ Ground water (1) 5MA~'ie WELL --

_Solid (5) Cadmium --Chromium - -

__ Surface water (2) _Liquid (6) Lead ---P~atSG t'/-V4-L YS"~

__ Mercury _Soil (3) _ Sludge (1) Selenium --

Silver Other (8) 7o P/2/IJ!ci.Vt; ~ --

_Other (4) -- --J.J//1(75 . - -

--Organic Chemistry Inorganic Chemistry --

Parameter Results(mg/1) Parameter Results(mg/I)(Wg 'h) Organic Compounds Results(mg/1) P&T:GC/MS X Arsenic Lo.oY benzene - - -- --

- - Acid:B/N Ext. 1_ Barium LD , C :-J -- carbon tetrachloride MTBE 1_ Cadmium "'-.<:::),C)y chlordane -- - -

Chloride chlorobenzene -- - - - -_x_ Chromium ~ o .oY. chloroform -- - -

-- __ Copper o-cresol --Fluoride m-cresol -- -- - -Iron _ _ p-cresol -- - -

-- _x_ Lead L...a . aL.\ cresol ---- __ Manganese - - 1,4-dichlorobenzene

-- ~Mercury <'t2.. aoa::l -- 1,2-dichloroethane Nitrate

o;;: 1,1-dichloroethylene - - -- - -

1_ Selenium L..o-a&..\ 2,4-dinitrotoluene --_x_ Silver L..o .c.C:::. __ heptachlor

Radiochemistry ___&_ Sulfates \?:, hexachlorobenzene --· · ·~·-·-- ·-· Zinc hexachlorobutadiene -- --

Results (PCi/1) Parameter pH hexachloroethane -- - --- Gross Alpha __ Conductivity - - methyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- --TOC pentachlorophenol --NaGke...J

- -X ~ o .aS __ pyridine

Microbiology -- tetrachloroethylene

-- __ trichloroethylene Parameter Results (Col/100ml) - -

_ _ 2,4,5-trichlorophenol 2,4,6-tricWorophenol - - -- --

- - -- -- vinyl chloride ~r.;1 :t-IUIPU JJ endrin - -u __ ._, ......... "" ....

lindane

OCT 2 9 1992 --Date Received Reported by methoxychlor - -

Date Reported ~nrMtrmlO ~OfiOW -- toxaphene

Date Extracted 2,4-D ---- 2,4,5-TP (Silvex)

Date Analyzed Lab Number --D IIS 31'J I (Revised 2/Y I)

L __ OiS504 SEP 24 92 -~J

N.C. Departmt.nt of Environment, Jlea)th, &. Natural Resources

• Soli~ Waste Management Division

rPLE ANALYSIS REQUEST • State Laboratoey of Pub lie Health P.O. Box 28047, 306 N. Wilmington Street


..

'sit~ Number A/C'J) !Jt:f.3 :6.3-+ t:f 6 9

Name of Site S ~ S /r!Ef71/t..$ &){Cl.l)}if;

Collected By ~ , 1JIC.ItOLc50VID# ~=1-

Field Sample Number. ___ /_!J_.--..;_3_9-_2... ______ _

Site Location GoLr:> fiiLl- NG . Date Collected Z-3 sEP 2 z. Time I 2-5 0

Agency: Hazardous Waste Solid Waste _x_ Superfund TCLP Compounds


C~tu~Lt. tuct.L Barium

£ Ground water (1) --

_Solid (5) Cadmium -- Chromium --__ Surface water (2) _Liquid (6) Lead ---_Sludge (7) /{£}7-Sif 4JJALY$E 7?J

Mercury _Soil (3) --Selenium --

_ Other (8) 7J LZI N JC tiJ y IJ.4tz-GFI2 Silver --

_Other (4) --L,At t-r> ----

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)

P&T:GC/MS Arsenic benzene )( Acid:B/N Ext. -- -- carbon tetrachloride Barium -- --MTBE Cadmium chlordane -- --~pc::,E; Chloride chlorobenzene <a.ooo/ J¥!!!1 -- Chromium

-- chloroform -- --Copper ---- o-cresol --

Fluoride m-cresol -- -- = p-cresol Iron -- -- Lead cresol -- -- ---- __ Manganese __ 1,4-dichlorobenzene


-- Nitrate __ 1,1-dichloroethylene -- Selenium __ 2,4-dinitrotoluene -- Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --

Zinc hexachlorobutadiene --Results (PCi/1) Parameter _pH hexachloroethane

__ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- .- pentachlorophenol TOC --

-- __ pyridine




Date Received Cf-. ))f-f'LU/;. Reported by lindane

_ methoxychlor

6H(~ __ toxaphene Date Extracted -c9B-q'd SA. WG Dale Reported __ 2,4-D

Peat 9-,?.Y--?;L 1/~ _ 2,4,5-TP (Silvex) Dale Anai/Zc1f9-,2t]-9.2.yP .pab Number 923211 --DIIS 3191 (Revised 2/91) f)ftl/}-ltJ -C, -92.8

N.C. Department of Environment, llca)th, &. ·Natural Resources

' So~id_ Waste Management Division

WPLE ANALYSIS REQUEST • State Laboratory of Public: Health P.O. Box 28047, 306 N. Wilmington Street


Site Number NC1? !J9.3 :6.3-1- t:f b 9

Name of Site 5 ~ S /i1t;;71Jt$ &vct.INry Collected By ~ , IJIC.tft>Le50I.J ID# :S=l-

Field Sample Number. _ __.~...(-!::5'_.:::.3---!..":f.....:3:..._ ______ _

Site Location GDL"&>. #ILl-·.

Date Collected 2-"3 SEf? --J 2-

Agency: __ Hazardous Waste __ Solid Waste _K__ Superfund

Sample Type Environmental Concentrate Comments

_1_ Ground water (1) _Solid (5) UV/)t....£ UJc:L-·L

_ Surface water (2) _Liquid (6) -----------

-Soil (3) _Sludge (7) ft.e::ttsE Jfv.nLY'€ A: _Other (4) _Other (s)&J. .. hCtVt; tl.J~rrez...

Organic Chemistry

Results(mg/1) Parameter )( P&T:GC/MS

_ Acid:B/N Ext. ----MTBE

Radiochemistry

Lth'lltS

Inorganic Chemistry

Parameter __ Arsenic

Barium -- Cadmium ----Chloride

Results(mg/1) (mg/kg)

__ Chromium __ Copper __ Fluoride __ Iron

Lead __ Manganese __ Mercury __ Nitrate

Selenium -- Silver --Sulfates

··--·-------------1 Zinc _pH Parc~meter Results (PCi/1)

__ Gross Alpha ------Gross Beta

Microbiology

Parameter Results (Col/100ml)

Date Received q_ },lf _q'l, ~

__ Conductivity ------_TDS

TOC

Reported by _______ _

Date Extracted Dale Reported ------------------------ --------------------------Date Analy.t:cd if/25 ~ -voc. ) ~ DIIS 3191 (Revised fjfi')J

Lab Number 923212

TCLP Compounds

Inorganic Compounds Arsenic -- Barium -- Cadmium -- Chromium -- Lead

--Mercury --Selenium -- Silver

Organic Compounds benzene -- carbon tetrachloride

Results(mg/1)

Results(mg/1)

-- chlordane --------chlorobenzene -- chloroform o-cresol m-cresol

-- p-cresol --cresol -- 1,4-dichlorobenzene -- 1,2-dichloroethane -------- 1,1-dichloroethylene -- 2,4-dinitrotoluene ------

= heptachlor hexachlorobenzene hexachlorobutadiene -- -------hexachloroethane

-- methyl ethyl ketone --nitrobenzene -------- pentachlorophenol __ pyridine

tetrachloroethylene -- trichloroethylene --2,4,5-trichlorophenol --2,4,6-trichlorophenol -------- vinyl chloride -- endrin -- lindane

methoxychlor =toxaphene ____ 2,4-D _ 2,4,5-TP (Silvex)

N.C Department of Environment, llealth, &. Natural Resources


rPLE ANALYSIS REQUEST • State Laboratol)' of Public Health P.O. Box 28047, 306 N. Wilmington Street


,- "'·' ' I. ! ~ .

Sit~ Number A/C..J) !Jtf.3 3~""/- 9 b 9 Field Sample Number /6 6/::;.

Name of Site 5 ~ S /t1EF71Jt.~ Jd:c:ict,.1Ntf; Colle~ted By ~ , IJ/Cft()L$0VID# '3=1-

Site Location Gt>t-~ fltLl-- AJG Date Collected .2.-3 sEP ., z.. Time___;I~Z.:;..J.;:;_tJ __

Agency: Hazardous Waste Solid Waste __K_ Superfund TCLP Compounds --Sample Type Inorganic Compounds Results(mg/1)

Environmental Concentrate Comments Arsenic --Wc'-L...

Barium L Ground water (1) (lAVBLE

--Cadmium Solid (5) --

. ' Chromium --__ Surface water (2) _Liquid (6) Lead ---Sludge (7) /l.El}S ~ Av1JLY5c 7CJ

Mercury Soil (3) --Selenium --

_Other (8) /{a;NJC/JJ~ t{Jr~ Silver

_Other (4) ----

.6/111'-rS ----Organic Chemistry Inorganic Chemistry --

Parameter Results(mg/1) Parameter Results(mg/IH•:"e Organic Compounds Results (mg/1) _P&T:GC/MS X Arsenic ..!..o .Q'-\ benzene

Acid:B/N Ext. 7Barium --

carbon tetrachloride O-otsl --MTBE _lL Cadmium 4-~.Q~ chlordane -- --Chloride chlorobenzene -- --

-- _lL Chromium ~o.o4 chloroform ---- __ Copper o-cresol --Fluoride m-cresol -- -- = p-cresol Iron -- ---- L Lead 4.o.oa..). cresol ---- __ Manganese __ 1,4-dichlorobenzene

-- _LLMercury ~~taaa~ __ 1,2-dichloroethane Nitrate

< __ 1,1-dichloroethylene --

~ Selenium . 4-o,~~ __ 2,4-dinitrotoluene Silver L.o .~5 __ heptachlor

Radiochemistry L Sulfates 8o hexachlorobenzene --··-- Zinc hexachlorobutadiene Parameter Results (PCi/1)

-- -- hexachloroethane _pH __ Gross Alpha __ Conductivity -- methyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- -- pentachlorophenol TOC 7 N1<:.ke l ~o_o;, __ pyridine

Microbiology :if:;:S!t?MZ : k E __ tetrachloroethylene

-- __ trichloroethylene Parameter Results (Col/100ml) __ 2,4,5·trichlorophenol ---- -- __ 2,4,6-trichlorophenol

.,

__ vinyl chloride -- -- endrin --lindane --

Date Received Reported by __ methoxychlor __ toxaphene

Date Extracted Dale Reported 2,4-D - 2,4,5-TP (Silvex)

Date AnalyLcd Lab Number --DIIS 3l'Jl (Revised 2/91)

01.5505 SEP 2 4 9 2

N.C. Departml:nt or Environment, ll'ca)th, &., Natural Resources

• So~i~. Waste Management Division

· I"PLE ANALYSIS REQ~ST • State Laboratoxy or Public: Health P.O. Box 28047, 306 N. Wilmington Street


. · .. Site Number A/C.J) !293 :6~~. t:f 6 9 Field Sample Number.~/:......::?::::..-__::3~~-4-....:...._ ______ _

NameofSiteS~ S /J1EFT1Jt$ &'fCtl}.)t? ·siteLocation Goi..p'· f!ILL NC Collected By ~ • IJI(tf()Lc5oiJID# ~::}- Date Collected 2-"3 sEP 2Z..' Time Is "?0

Agency: _Hazardous Waste Solid Waste >( Superfund TCLP Compounds


X Ground water (1) _Solid (5) k:"rJ t<; tf -r -- Cadmium Wt=l.-1._ -- Chromium --__ Surface water (2) _Liquid (6) Lead ---_sludge(7)pl.Df&E ~Y$E h

Mercury Soil (3) --Selenium --

_ Other (s)dtu~ K I A..JG {j_J A 7CR Silver --Other (4) --

f.LMtfS ----

Organic Chemistry Inorganic Chemistry --Parameter Results(mg/1) Parameter Results(mg/l)(mgjkg) Organic Compounds Results (mg/1) XP&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- --. ' MTBE Cadmium chlordane -- -- --

Chloride chlorobenzene -- -- --Chromium chloroform -- --

-- __ Copper a-cresol --Fluoride m-cresol -- -- = p-cresol -- Iron - Lead cresol -- --

-- __ Manganese __ 1,4-dichlorobenzene

-- __ Mercury __ 1,2-dichloroethane Nitrate __ 1,1-dichloroethylene -- - Selenium __ 2,4-dinitrotoluene -- Silver heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --.. Zinc hexachlorobutadiene

Parameter Results (PCI/1) =pH -- hexachloroethane

__ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- = pentachlorophenol TOC --

-- __ pyridine

Microbiology - __ tetrachloroethylene



C[l)f-fL, M& lindane Date Received Reported by _ methoxychlor

__ toxaphene Date Extracted Date Reported _2,4-D

vCC-~ ) ~ 92321.3 2,4,5-TP (Silvex)

Lab Number Date Analyzed q J5 9 'll'\ --DIIS 3191 (Revised 2f ) r~

N.C. Departmo:nt of Environment, I fc;lth, &. Natural Resources

~li~. ~aste Management Division

rPLE ANALYSIS ~QUEST .• State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street


:sit~ Numb~r A/Cj) !)93 B.3+ tf 6 9

Name of Site S ~ S /!lEFTIIt$ &Yc~l!.!&j Collected By ~ 1 /JI(.ft()L.$'0/U ID# ~=/-

Field Sample Number __ !..../....::5~3~?-~~:;__· ------Site Location Gel-p · 1ft LL NC . Date Collected 2..'3 sEP 2 2-' T~e 13$0

-·Agency: _Hazardous Waste Solid Waste _K_ Superfund TCLP Compounds


2(_ Ground water (1) Solid (5) tc)J 1c;H T p..JELL -- Cadmium -- Chromium --__ Surface water (2) _Liquid (6) Lead -

_Sludge (7)-pl..f:A~ £ ~Ac.YSt Mercury

_Soil (3) --Selenium --_ Other (8) f;;, D~ ( }J ~I )..2) ~

Silver _Other (4)

----

(..t)rt~ l l~tA(~ ----

Organic Chemistry Inorganic Chemistry --·Parameter Results(mg/1) Parameter Results(mgjl)(mgfkg) Organic Compounds Results (mg/1)

P&T:GC/MS Arsenic benzene )r:Acid:B/N Ext. -- --

Barium carbon tetrachloride -- Cadmium -- chlordane · · MTBE

~ --Chloride -- chlorobenzene .x__ 4:; 0 I 0 (} (} l.;p.Jtll --Chromium -- chloroform -- --

-- __ Copper o-cresol --Fluoride m-cresol -- -- = p-cresol -- Iron -- Lead cresol -- -- Manganese -- 1,4-dichlorobenzene -- ---- __ Mercury __ 1,2-dichloroethane

-- Nitrate __ 1,1-dichloroethylene -- Selenium 2,4-dinitrotoluene -- Silver = heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --.. Zinc hexachlorobutadiene Parameter Results (PCi/1) =pH

--hexachloroethane

__ Gross Alpha __ Conductivity -- methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- -- pentachlorophenol TOC --

-- __ pyridine




q..,.. Z...<f-7 'i !J/b Reported by lindane

Date Received _ methoxychlor

/}~A __ toxaphene Date Extracted - Q6-qQ SA,WG Date Reported _2,4-D

Pt!.ll;r f-~ P-1'.Z.11e»1 _ 2,4,5-TP (Silvex) Date Analy.lCfc;-:.29-9..?]1P Lab Number ,. •.• . . DIIS 3191 (Revised 2/91)(JM9/0 ·u-~!l. /ii!J 9;G3214 --

N.C. Department or Environment, llealth, & Natural Resources

Sol!~.'~'aste Management Division

.• \MPLE ANALYSI_S REQUEST •. State Laboratory or Public Health P.O. Box 28047, 306 N. Wilmington Street


.. c, .. ~ ; .: , '!-. • -

'sit~ Number A/C.)) tJtl3 :6.3-1- tf b 9 Field Sample Number. _ __:_/..:6~·..::::.~:....·:...1!::::::&:....__ ______ _

Name of SiteS~ S /J1£TT~Jt$ lJi:,YCt,.INry. Site Location GDLP .· fiiLL' A/G Colle~ted By r:; I 1JIC.ff()L6"oiJID# 3=1- Date Collected 2..3 sEP .-,z.. Time /~ '3o

Agency: __ Hazardous Waste _Solid Waste _Lsuperfund TCLP Compounds

Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic -- Barium X Ground water {1) k':J1t;z HT Wet-L -- Cadmium _Solid (5) --

. , .. Chromium --__ Surface water {2) _Liquid (6) Lead ---_Sludge (7) ft.f:ASE k;Ai.Y)f; If>

Mercury Soil {3) --Selenium --

_Other (8) J:R,~~tl'-'6) W~r-ree__ Silver

Other (4) ----

LJM\T~ ----

Organic Chemistry Inorganic Chemistry --·Parameter Results(mg/1) Parameter Results(mg/1) 'au l!w Organic Compounds Results(mg/1) _P&T:GC/MS L Arsenic L..o o<-} benzene --_ Acid:B/N Ext. ..L Barium L.o. o:l carbon tetrachloride --· · · MTBE L Cadmium ~o.IT-1 chlordane· -- --

Chloride chlorobenzene -- --}( Chromium -- ..(o.a'-4 chloroform ---- __ Copper o-cresol --

Fluoride m-cresol -- -- = p-cresol -- Iron

-- 'I Lead <o.c::t\ cresol ---- __ Manganese __ 1,4-dichlorobenzene

-- ..£Mercury < 0#- (2 OQ '::J __ 1,2-dichloroethane Nitrate

... 1, 1-dichloroethylene -- --

)( Selenium ""--o.Q~ __ 2,4-dinitrotoluene _x_ Silver L..c:>. 0 s __ heptachlor

Radiochemistry L Sulfates d--0 hexachlorobenzene --.. Zinc hexachlorobutadiene .. --Parameter Results (PCI/1) _pH hexachloroethane __ Gross Alpha __ Conductivity = methyl ethyl ketone

Gross Beta TDS nitrobenzene -- -- -- pentachlorophenol TOC X NJc.kt...l L..o .oS __ pyridine

Microbiology «s I .. __ tetrachloroethylene

-- __ trichloroethylene Parameter Results (ColflOOml) __ 2,4,5-trichlorophenol -- 2,4,6-trichlorophenol -- -- = vinyl chloride -- -- endrin --

lindane Date Received Reported by = methoxychlor

__ toxaphene Date Extracted Date Reported 2,4-D

- 2,4,5-TP (Silvex) Date Analy.lCd Lab Number --DIIS 3191 (Revised 2/91)

Ot5506 SEP 24 gz

N.t. bepartment of Environment, • • Health, & Natural Resources

SOlid Waste Management Division

.PLE ANALYSIS REQUEST • State Laboratory of Public Health P.O. Box 28047, 306 N. Wilmington Street


Site Number A/C.1? ~<f3 E~+ 'f 6 9

Name of Site S ~ S /tJ~Fl~Jt$, J?R:.-'IC?I.JJ'?

Collected By t:; , )J/Ctf()L$Ot..}ID# ~=/-

Field Sample Number. ___ /.t......;...S_..::'3_=?-___.;.b _____ _

Site Location GDLP f!JLL

Date Collected 2.."3 sEP 2 2.. Time I I '$E) ____ ....;;.... __ _ Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds

Sample Type Inorganic Compounds Results(mg/1) Environmental Concentrate Comments Arsenic ---

$utrJ\.Jk: Barium

__ Ground water {1) _Solid (5) /IGIP - Cadmium -- Chromium --__ Surface water (2) _Liquid (6) Lead -Mercury

_Soil (3) Sludge (7) --Selenium - Silver 4._ Other (4) Other (8)

-----Organic Chemistry Inorganic Chemistry --

Parameter Results(mg/1) Parameter Results(mgfl)(mgfkg) Organic Compounds Results(mg/1) D P&T:GC/MS Arsenic benzene -- --_ Acid:B/N Ext. Barium carbon tetrachloride -- -MTBE Cadmium chlordane -- -- --

Chloride chlorobenzene -- -- -Chromium chloroform -- ---- __ Copper o-cresol -Fluoride m-cresol -- -- = p-cresol -- Iron -- Lead cresol -- -- = 1,4-dichlorobenzene -- __ Manganese

-- __ Mercury _ 1,2-dichloroethane

-- Nitrate _ 1,1-dichloroethylene --Selenium __ 2,4-dinitrotoluene --Silver heptachlor --Radiochemistry Sulfates hexachlorobenzene -- --··-- Zinc hexachlorobutadiene -- -Parameter Results (PCI/1) _pH hexachloroethane

__ Gross Alpha __ Conductivity = methyl ethyl ketone Gross Beta TDS nitrobenzene -- -- = pentachlorophenol -- TOC

-- __ pyridine

Microbiology -- _ tetrachloroethylene

-- _ trichloroethylene Parameter Results (Col/100ml) __ 2,4,5-trichlorophenot -- 2,4,6-trichlorophenol -- -- = vinyl chloride -- -- endrin --

q_, ])J -9i- fJb Reported by lindane

Date Received = methoxychlor _toxaphene


Dale AnalylCd "'tl-f15}9~ Lab Number 923215 __ 2,4,5-TP (Silvex)

--DIIS 3191 (Revised 2 ) I

Purpose: Enforcement and co.nce with the N.C. Solid and Hazardous .e Management Rules. . .

Preparation: A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic,. organic, microbiology, radiochemistry). For sampling conditions which require more than one {1} container (i.e., ground or surface water) a sample label must be affiXed to one of the containers. The collector must then write the site and sample number on the duplicate container.

Do not submit an analysis request form without any parameters indicated.

Equivalent measurements: ppm = .ug/ml = mg/1 = .ug/g = mg/kg ppb = .ug/1 = .ug/1000g = .ug/kg

DEFINITIONS/INSTRUCfiONS


Field Sample Number - A unique six-digit sample identifier which is pre-printed on the sample label.

Name of Site - Name of facility, landfill, etc.

Site Location - City and county.



••

Environmental - A sample of a naturally occurring substance such as ground water, surface water, or soils which may be contaminated.

Concentrate - A sample of a waste, including but not limited to, sludges, resins, treatment effluents, or drummed wastes. -

Comments - Lists details regarding sample or sample point (e.g., sample location, well number, phase separation, . and/or odors.

Inorganic Chemistry - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided.

Organic Chemistry - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided.

TCLP Compounds - Check ( ./ ) the desired parameters to be analyzed. If not listed, enter the element/compound in the space provided. TCLP can only be performed on solid or semisolid samples. For totals of the inorganic parameters, check ( ./ ) the corresponding parameter under Inorganic Chemistry.


Distribution:

l>isposition:



Additional forms may be ordered from: Solid Waste Management Division Hazardous Waste Section P.O. Box 27687 Raleigh, NC 27611

• _,.._. '··~ J "..,. .l ...

., BASE/NEUTRAL AND ACID

EXTRACT ABLES COHPOUNO

N-nitrosodimethvlamine bis(2-chloroethvllether 2-chloroohenol phenol 1 3-dichlorobenzene 1,4-dichlorobenzene 1 2-dichlorobenzene bis(2-chloroi~ UDvllether hexachloroethane N-nitroso-di-n-oroovlamine nitrobenzene isoohorone 2-nitroohenol 2 4-dimethvlohenol bis(2-chloroethoxv)methane 2 4-dichloroohenol 1 2,4-trichlorobenzene naphthalene hexachlorobutadiene 4-chloro~resol

hexachlorocvclooentadiene 2.4.6-trichloroohenol 2-chloronaPhthalene acenaphthylene dimethvl Phthalate 2 6-dinitrotoluene acenaphthene 2 4-dinitroohenol 2,4-dinitrotoluene 4-nitroohenol fluorene 4-chloroohenvlPhenvlether diethyl phthalate 4,6-dinitro-o-cresol diohenvlamine azobenzene 4-braroohenvlphenvlether hexachlorobenzene pentachloroohenol phenanthrene anthracene dibutvl ohthalate f1 uor an thene

J - Estimated value.

• STATE lABORATORY OF PUBLIC HEAL T. DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES

P.O. BOX 28047-306 N •. WILMINGTON, ST., RALEIGH, N.C. 27611

ORGANIC CHEHICAL ANALYSIS

FIELD 11 1 S.37 1 1 s: ~7 .2- 1 r~ TYPE J./J (/) _i/) ( J UNITS ( lJQ/1 ~ :,Pg/1 )~ :r lJQ/1 ~ )JQ/1. )J_9/kg

$0//hSO l!tJ/330

to/~3o I

So/Jt,5o I0/330

lt1/~3D

I

\ ' ''I

K - Actual value is known to be less than value given.

( ) ( ) )JQ/1 lJQ/kQ llQ/1 lJQ/kQ

L - Actual value is known to be greater than value given. U- Material was analyzed for but not detected. The number is the Minimum Detection Lim1t.I?)2)L. NA - Not analyzed. - - - _ 1/ -Tentative identification. ~I- On NRDC List of Priority Pollutants •

. .

N.C. V.i.v.<A.i.on a6 HeaLth Svr.v.i.~u VHS 3068-0 (4/86 Labo~aftyl

\ t:.. ,._ ..

BASE/NEUTRAL AND ACID EXTRACT ABLES

COMPOONO

pyrene benzidine butvl benzyl phthalate benz{a)anthracene chrysene 3.3-dichlorobenzidine bis(2-ethylhexyl)phthalate di-n-octyl phthalate benzo(b)fluoranthene benzo(lc)fluoranthene benzo(a)ovrene i ndeno ( 1, 2 3-cd) pyrene dibenzo(a~h)anthracene

benzo(g h i)perylene

aniline benzoic acid ben~l alcohol 4-ch loroani 11 ne dibenzofuran 2-n-ethylnaphthalene 2~thvlohenol

4-methylphenol 2-nitroani line 3-nitroani line 4-nitroani line 2,4,5-trichloroohenol

• • STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RES<XJRCES

P.O. BOX 28047- 306 N. WILKINGTOH, ST., RALEIGH, N.C. 27611

ORGANIC CHEMICAL ANAL YSlS

FIELD II /537/ JS:.~J,)._ J ... \37.._) TYPE ( J ) _(_ J ) ( / ) ( J

1/0/.330 -u - ~t ... -u.__ 1s-n/JhSO 10/.330

J sobMfJ 1/()/.330_ i/t>/.J~o

~I _\I

S"allhSO lA- lA-

~ ~-/IJ '.3;10

"' So/J"S"o

I

"" ' 'I \

m1H-J - Estimated value. H.oi.SciL K - Actual value is known to be less than value given. l - Actual value is known to be greater than value given. U- Katerial was analyzed for but not detected. The number is the Minimum Detection Limit. NA - Not analyzed. 1/ - Tentative identification. ~I -On NROC List of Priority Pollutants.

N.C. V.iv-W.ion o6 He.a.Uh SVLv.ic.e.-6 VHS 3068-0 (4/86 Labo~o~y)

1 ) ( ) lJQ/1 lJQ/IcQ _l)_g/ 1 lJg/lcQ

• • SOLID WASTE MANAGEMENT DIVISION SUPERFUND SECTION

CERCLA Receipt for Samples

The samples described below were collected in conneqtion with the administration, enforcement, and documentation of the:

( ) North Carolina Hazardous Waste Management Rules, 10 NCAC lOF ( ) North carolina Solid Waste Management Rules, 10 NCAC lOG ()() Comprehensive Enviro!lmental Response,. Compensation and

Liability Act (CERCLA). ( Toxic Substances Control Act (TSCA) .15 u.s.c. §2601. et.seg.,

specifically Section 11 of TSCA, 15 U.S.C. § 2610.

G12o.v~R. N J~f!bl-St... N Inspector's N,ame Inspector's Address

Name of Firm Firm Address

Firm Owner~ Operator, or Agent Title

SAMPLE COLLECTED SAMPLE TYPE DUPLICATE SAMPLES SAMPLE LOCATION NUMBER DATElTIME WATERlSOILlOTHER OFFRDlACCPTlREJECTED

C-111/ill£ 1· ZJ,"'tz /'2-Jo X X X. ~.AJ£1..L

----- :-----__~ ~ :.--

~ ~ ~

~ ~

·-----Rece1pt for the sample(s) descr1bed abov is hereby acknowle ged:

,__c)J~

Title

_;::;>< ----- ------

Title

ON:-SITElOFF-SITE

X

~ ..........

'--.... .......

..

COMMENTS: ____________________________________________________________________ _

• • SOLID WASTE MANAGEMENT DIVISION

SUPERFUND SECTION



Location of sampling: Generator ---Treatment Facility ===Disposal Facility

CERCLA

__ Transporter ___ storage Facility

Landfill

Other=----------------------------~------Company's Name ____________________________ Telephone: ______________ __

Address ________________________________________________________________ _

Collector's Name __________ ~ _____________ Telephone: ______________ __ signature

Date sampled _____________________________ Time Sampled ______________ _

Type of Process Generating Waste ____________________________________ _

Field Information: -----------------------------------------------------

'Field sample No. ------


signature title inc],.usive dates


signatUJ;e title inclusive dates

Results Reported:

.. s~gnature title date

Instructions: Complete all applicable information including signatures, and submit with analysis request forms.

j.

• ~~-----------· --· ·--- --- ·-

• SOLID WASTE MANAGEMENT DIVISION

SUPERFUND SECTION CERCLA

Receipt fo r Samp les

The samples described below were collected in connection with the administration, enforcement, and documentation of the:

( ) North Carolina Hazardous Waste Management Rules, 1 0 NCAC lOF ( ) North Carolina Solid Waste Ma nagement Rules, 10 NCAC lOG (X) Comprehensive Environmental Response, Compensation a nd

Liabilit y Ac t (CERCLA ) ( ) Toxic Substances Control Act (TSCA) .1 5 U.S.C. §2601. et . seq .,

specifical l y Section 11 of TSCA , 15 U.S . C. § 26 1 0 .

Inspect or ' s Name 771 0 ~ t>l-J> HILL IGP

Gu.P HILL NC.. J."bl>-=f-1 Name of Firm 901- 4~;$- I ~<=t+

J<. KAI'I~#T Fi r m Owner , Opera tor, or Agent

.Bcc.K'/ c6t!Jkt

64J.pspector' s Addre ss

:5 \ .;; )1. er A ·L. 5'

Firm Address

12LA/ P' c ::e Title

SAMPLE COLLECTED SAMPLE TYPE DUPLICATE SAMPLES SAMPLE LOCATI ON NUMBER DATE:TIME WATER:SOIL:OTHER

K!f)'6tH7 '1·l3 j'jj{) X

Rece1pt f or the sample(s) descr1bed abov · s hereby acknowle ged:

~ [ !J,·c/, 4---

~UI ~,._,. ~6}? · Title

OFFRD:ACCPT:REJECTED ON~SITE:OFF-S ITE

)( X X

Recelpt jreJeCtlon of dupl1cate or split samples is ~er by acknowledged:

Signature or Agent

ot»,.,ER-Title

coMMENTs: li&metPcK WGl.-+= ]?p, LUA:tf C: /~6 / _l)E;l;e RlJ / eA-SrA/t:; b,.. .J?//l YI£LD

• • SOLID WASTE MANAGEMENT DIVISION

SUPERFUND SECTION



CERCLA

Location of Sampling: Generator Treatment Facility

___ Disposal Facility

___ Transporter ___ Storage Facility

Landfill Other: __________________________________ __

company 1 s Name ____________________ ,--_____ Telephone: ___ _

Address -----------------------------------------------------------------. . Co 11 ector 1 s Name __________ -=--------'---------Tel ephone.: ____ _ ________ _

signature . . ..

Date sampled ·.Time sampled ----------------------------~ ~-------------

Type of Process Generating Waste ______________________________ ~--~·-·-

Field Information: ----------------------------------------------,-------

Field Sample No. _________ __


signature

signature

signature . \

Results Reported:

signature

title inclusive dates



title date

Instru6tions: Complete all applicabie information .. inclu~ing s~gnatures, and submit.with analysis request.f9rms.

.... ·~ ... . ..

• • SITE HEALTH AND SAFETY PLAN

A. General Information

Site NameS & S Metals Recycling Co., Inc.

Location SR 2455 (Shortcut Road), Gold Hill,

Cabarrus County, NC 28071

ID # NCD 093 334 969

Proposed Date of Investi9i',tion September 23, 1992 ,_

Date of Briefing September 22, 1992

Date of Debriefing =S~ep~te~mb~e~r~2~4~,~1~9~9~2~------------------

Nature of Visit (check one): Off Site Sampling X

Health Department Official ContactedMr ~~·~K~e~n~H~i~n~s~o~n~--------------------

Date of Contact September 18, 1992

Site Investigation Team: All site personnel have read the Site Health and

Safety Plan and are familiar with its provisions.

Personnel

Team 1 Grover Nicholsn

Team 1 Harry Zinn

Responsibilities

team leader, sampling

sampling

Signature

1};;c;i£L

• • B. SITE/WASTE CHARACTERISTICS

Waste Type(s) ---'Liquid _x_solid __ sludge Gas --- ___ Vapor

Characteristics _____ Corrosive ____ Ignitable ____ Radioactive

____ Volatile __ X_Toxic ___ Reactive Other

List Known or Suspected Hazards (physical, chemical biological or

radioactive) on Site and their toxicological effects. Also, if known, list

chemical amounts

HAZARD WARNING PROPERTIES

Chromium Odor Threshold (OT) no data

Barium OT no data

Lead OT no data

Cadmium OT no data

EXPOSURE

LIMIT

. 3 O.OSmg/m

3 O.Smg/m

3 O.OSmg/m

3 O.OSmg/m

• • ID # NCD 093 334 969

Facility Description: Size 15 acres

Disposal Methods Being Investigated

application onto roads.

Buildings _.y~e~s~----------------Storage in holding ponds, then

Unusual Features on Site (dike integrity, power lines, terrain, etc.):

none known

History of the Site: The company recycled aluminum and engaged in oil

reclaiming activities. Emulsified cutting oil that was separated from the

aluminum scrap during processing was kept in three holding ponds on-site.

The company decided to dispose of the oil in the ponds by using it to

control dust and stabilize the roads on the facility. Reportedly, after

all the oil was removed from the ponds, the ponds were filled in with dirt.

C. HAZARD EVALUATION

The site can be toured and sampled in level D protection. PE or PVC gloves

will be worn while collecting water samples. Steel toed hiking boots may

be worn while collecting residential drinking water well samples.

D. WORK PLAN INSTRUCTION

Map or Sketch Attached? .y~e~s ______ _

Perimeter Identified? no =-------Command Post Identified? no

~-------

Zones of Contamination Identified? no =-------

Personal Protective Equipment/Level of Protection: ___ c --=-=x--'D

Modifications Wear goggles, face shield, and PVC gloves while preparing

acid preserved samples, goggles and PVC gloves while collecting acid

preserved samples. Avoid breathing acid vapors. Rinse pipetts with

deionized water before disposing of in trash bag.

• Surveillance Equipment:

--------- HNU

--------- OVA

---------- Explosirneter

Decontamination Procedures

• ID # NCD 093 334 969

---------- Detector Tubes and Pumps

---------- 02 Meter Radiation Monitor ----------

------~Level C Respirator wash, respirator removal, suit wash (if needed),

suit removal, boot wash, boot removal and glove removal.

X Level D --~--~

Boot wash and rinse and boot removal, suit removal, glove

and goggle removal.

Modifications Dispose of trash properly, on-site if possible.

Work Schedule/Visit Objectives The purpose of this visit is to determine

if the site poses a threat to the public health or environment because of

releases of contaminants to soil, surface water, groundwater, or air.

Sampling may consist of residentail drinking water well sampling.

EMERGENCY PRECAUTIONS

Route of Exposure

Eyes

Skin

Inhalation

Ingestion

First Aid

irrigate immediately

soap and water wash

fresh air and artificial respiration

get medical attention immediately

• • ID # NCO 093 334 969

Locat ion of Nearest Phone: unknown ( nearby residences/businesses )

Hospital (Address and Phone Number)

Cabarrus Memorial Hospital , 920 Church Street North, Concord, NC 28025

( 704) 786- 2111

Emergency Transportation Systems (Phone Numbers)

Fire 911 ~~----------------------------------------

Ambulance 911 ~~-----------------------------------

Rescue Squad 911 ------------------------------------Emergency Route to Hospital Turn left onto SR 2455, left on SR 2450, then

right onto Route 49 and travel west. Get off 49 at Route 73 and travel

west to Business 601 North. The hospital is about 20 miles from the site.

PREVAILING WEATHER CONDITIONS AND FORECAST Part l y cloudy with a chance of

rain, highs in the lower 70s.

EQUIPMENT CHECKLIST ______ Air purifying respirator

Cartridges for respirator __ X=--- Eye Wash Unit

HNU ______ OVA ______ Explosirneter

Radiation Monitor X Decontamination __ :..::...._ __

Materials

X First Aid Kit X 3 gal . Deionized H20 X Rainsuit X Gl oves (PE/PVC/nitrile/cloth) X Boots/Boot Covers

Coveralls ( tyvek/saranex) X Eye Protection (goggles/shield)

Hard Hat ----

Poison Control Center - State Coordinator Duke University Medical Center

ASHEVILLE 704 - 255 - 4490

CHARLOTTE 704 - 379 - 5827

DURHAM 1- 800- 672-1697

GREENSBORO 919 - 379 - 4105

safeforrn.201

Telephone: 1- 800 - 672 - 1697 Box 3024

Durham, NC 27710

Western NC Poison Control Center Memorial Mission Hasp. 509 Biltmore Ye. 28801

82-01

Duke Univ. Med. Center Box 3007, 27710

Moses Cone Hospital 1200 N. Elm St . 27420

HENDERSONVILLE 704-693 - 6522 Ext . 555,556

HICKORY 704-322 - 6649

JACKSONVILLE 919 - 577 - 2555

WILMINGTON 919 - 343 - 7046

Margaret R. Pardee Memorial Hospital Fleming St . , 28739

Catawba Mem. Hasp . Fairgrove Chur . Rd 28601

Onslow Mem. Hospital Western Blvd. 28540

New Hanover Mem. Hospital 2131 S . 17th St. 28401

• •

0 w A N c 0 u N T y

I I ~

I'UI.POUS ~

j ~

J

• • HAZARDOUS SUBSTANCE INFORMATION FORM

Chemical Name: Chromium (VI), insoluble salts

I. PHYSICAL/CHEMICAL PROPERTIES

Chemical Formula varies with compound

Natural Physical State at 25 c solid

Vapor Pressure NLA mm Hg at 20°C

Melting Point OF/OC Boiling Point

Flash Point (open or closed cup)

Solubility - H2o not soluble in water

Other

Reference

1

1

1

----------------------------------------

Physical Features: (odor, color, etc.) Properties vary depending upon

specific compound. Compounds include: zinc chromate, lead chromate,

calcium chromate etc.

II. TOXICOLOGICAL DATA

3 Standards: 0.05 mg/m (2) TLV 3 0.5mg/m (4) PEL

Routes of Exposure: Inhalation and ingestion

3 500 mg/m IDLH

Acute/Chronic Symptoms: Chronic: fibrosis of the lung and epidemiological

studies have shown increased incidence of lung cancer among workers in the

manufacture of chrome pigments

First Aid: Inhalation: artificial respiration; Ingestion: get medical

attention immediately; Eye contact: irrigate immediately; Skin contact:

soap and water wash immediately

3

• • Chemical Name: Chromium (VI), insoluble salts

III. HAZARDOUS CHARACTERISTICS

A. Combustibility Yes

Toxic by-products

No X

B. Flammability LEL N/A UEL ____ _

C. Reactivity Hazard strong oxidizers

D. Corrosivity Hazard yes/no pH:

Neutralizing agent:

E. Radioactive Hazard Exposure Rate

Background yes/no

Alpha particles yes/no

Beta particles yes/no

Gamma radiation yes/no

IV. REFERENCES

1. The Merck Index, 11th Edition, 1989.

2. Threshold Limit Values and Biological Exposure Indices

for 1991-1992 ACGIH

3. Pocket Giude to Chemical Hazards, NIOSH, 1987

4 .. 29 CFR 1910.1000

Reference

3


Chemical Name: Barium (soluble compounds)


Reference

Chemical Formula Ba 1 -=----Natural Physical State at 25°C properties vary depending

0 Vapor Pressure mm Hg at 20 C on compound ..... =2 ______ _

Melting Point °F/°C Boiling Point °F/°C

Flash Point (open or closed cup) °C/°F

Solubility - H2o vary ..... =2 _____ _

Other var --~2 ___ _

Physical Features: (odor, color, etc.) Vary depending on compound(2)


3 Standards: 0.5 mg/m (3) TLV 3 0.5 mg/m (4) 3 PEL 1,100 mg/m (2)

Routes of Exposure: Inhalation, Ingestion, skin and/or eye contact

IDLH

Acute/Chronic Symptoms: Upper respiratory irritation, GI irritation, muscle

spasms, slow pulse, premature contractions of the heart, extrasystoles,

hypokalemia, irritation of eyes, skin burns. (2)




• • Chemical Name: Barium


A. Combustibility Yes No

Toxic by-products

depends on compound

B. Flammability

C. Reactivity Hazard

D. Corrosivity Hazard

Neutralizing agent:

E. Radioactive Hazard

Background

Alpha particles

Beta particles

Gamma radiation

IV. REFERENCES

LEL ___ _ UEL ____ _

depends on compound

yes/no

yes/no

yes/no

yes/no

yes/no

pH:

Exposure Rate

1. The Merck Index, 11th Edition, 1989

2. Pocket Guide to Chemical Hazards, NIOSH, 1990

3. Threshold Limit Values and Biological Indices

for 1991-92 ACGIH.

4. 29 CFR 1910.1000

Reference

2

2


Chemical Name: Lead, inorganic dusts


Chemical Formula Pb ~~---------------------------

Natural Physical State at 25°C solid ~~~-----------

Vapor Pressure N/A rom Hg at 20°C

Melting Point 327.4 °F/°C Boiling Point

Flash Point (open or closed cup) N/A

Solubility - H2o N/A

1,740 °Fj°C oC/oF

Other ~N~A~--------------------------------

Reference

1

1

1

1

Physical Features: (odor, color, etc.) appearance and odor vary depending

upon specific compound.


suspected or confermed human carcinogen 3 3 Standards: .15 mg/m {2) TLV 0.05 mg/m {3) PEL N/A {4) IDLH

Routes of Exposure: inhalation, ingestion, eye contact, skin contact(3)

Acute/Chronic Symptoms:Acute: lassitude, pallor, constipation, abdominal pain,_

gingival gum line, tremors. Target organs: GI tract, CNS, kidneys, blood.(3)




• Chemical Name: Lead, inorganic dusts



Toxic by-products

No X

•

B. Flarranability LEL ---'N:..:..~/:...;;A.:....__ UEL

C. Reactivity Hazard ___ N~o~n~e __________________________ _


Neutralizing agent:

E. Radioactive Hazard

Background yes/no



Garrana radiation yes/no

IV. REFERENCES

(1) The Merck Index, 11th Edition, 1989

Exposure Rate

(2) Threshold Limit Values and Biological Exposure Indices

for 1991-1992 ACGIH.

(3) 29 CFR 1910.1025

(4) Pocket Guide to Chemical Hazards, NIOSH, 1987.

Reference


Chemical Name: Cadmium dust (as Cd)


Reference

Chemical Formula Cd --~~-------------------------

Natural Physical State at 25°C solid --~~~----------

Vapor Pressure N/A mm Hg at 20°C

Melting Point °F/°C Boiling Point __________ °F/°C

Flash Point (open or closed cup)

Solubility - H2o not soluble

Other

1

1

1

Physical Features: (odor, color, etc.) appearance and odor vary for

specific compound.


3 Standards: 0.05 mg/m (2) TLV 3 0.2 mg/m (3) PEL potential IDLH 4

carcinogen

Routes of Exposure: Inhalation and ingestion, skin contact, eye contact

Acute/Chronic Symptoms: cough, tight chest, headache, chills, muscle

aches, nausea, diarrhea. (4)




• Chemical Name: Cadmium dust (as Cd)



Toxic by-products

B. Flammability

No X

LEL ____:N:..:..~/:..:.A=----

• Reference

2

UEL

c. Reactivity Hazard strong oxidizers, elemental sulfur, --~2 ____ __

selenium and tellurium.


Neutralizing agent:

E. Radioactive Hazard Exposure Rate

Background yes/no



Gamma radiation yes/no

IV. REFERENCES

{1) The Merck Index, 11th Edition, 1989.

(2) Threshold Limit Values and Biological Exposure Indices

for 1991-1992 ACGIH.

(3) 29 CFR 1910.1000

{4) Pocket Guide To Chemical Hazards, NIOSH, 1987.

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• • Site Name: S&S Metals Site Number: NCD 093 334 969

Site Location: Goldhill, N.C. Rowan County Latitude: 35 28 44.0 Longitude: 80 19 45.0

Date: July 06, 1992

Calculation Results

Distance from Population Number of Households Site Location Per Ring Cumulative Per Ring Cumulative

0 to

>1/4 to

>1/2 to

>1 to

>2 to

>3 to

Note:

1/4 mile 3 3 0 0

1/2 mile 12 15 3 3

1

2

3

4

mile 55 70 21 24

miles 395 465 155 179

miles 922 1,387 313 492

miles 1,650 3,037 516 1,008

The populations and number of households within specified target distance rings were calculated for the NC Superfund Section by the NC State Center for Geographic Information and Analysis using the 1990 US Census data. These values were calculated by summing the popul ation and the number o f households data for each census block located within each target ring. For census blocks lying only partially within the ring, the per cent area of the block within the ring was multiplied by the population and household densities of the block.

FINAL84.RP

- - --- -·---~

. , . . • • . - . . --- ·· - . .. -:-. ·-J .. .. _.-· . . . --- .; .... ---~ .-:-:~ .. --· - . ' ·: _ .·: ·:-··. -~ ..: ~- -~ - - : __ . - · _· ; ~- ; - - - - ~-::~~ --~-~~~-- -

: ."" • t ~-·.: :....::. _- • LATITUDE ' AND · LONGITUDE CALCULATION WORKSHEET . I2 LI USING ENGINEER'S SCALE (1/60)

sITE NAME: __ 5_ &_ 5_ r()_ .£_t_a.._/s _ _,_~.=/:,zV~c.~~!...!:·:9..!.4---- CERCL Is I:

AKA: _________________________________________ ssio: ________________________ __

~D~ss: ________ 5~h~o~t·~t~c=v-~t~R~· ~~~~J=---------------------------------------CITY: (J/J/J z?'/1 STATE: ____ .:......:N __ C-_ ZIP CODE: ____ ~z_g~0~7_,_/ ______ _

SITE REFE~NCE POINT: irJiA -~dim · 1 USGS QU ~ HAP NAME: ____ K~C:.L/.!::JJ~ffu..'!:.aC'j'-"~tf----- TOWNSHIP: N/S RANGE:

SCALE: 1:24,000 HAP DATE: /:J'a/ SECTION: 1/4 1/4 1/4

HAP DATUM: 6)1983 (CIRCLE ONE) MERIDIAN: __________________________ _

COORDINATES FROM LOWER RIGHT (SOUTHEAST) CORNER OF 7.5' HAP (attach photocopy):

LONGITUDE: ~o _L2_ · ~0 " LATITUDE: 35 ° 22 ' 30 "

[ cOORDINATES

LLONGITUDE:

FROM LOWER RIGHT (SOUTHEAST) CORNER OF 2.5' GRID CELL:

LATITUDE: ]5 o _3]_ • 3 0 "

CALCULATIONS: LATITUDE (7.5' QUADRANGLE HAP)

A) NUMBER OF RULER GRADUATIONS FROM LATITUDE GRID LINE TO SITE REF POINT: 12~

B) MULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS:

A X 0.3304

C) EXPRESS IN MINUTES AND SECONDS (1'= 60"): ~· /f- .L_"

D) ADD TO STARTING LATITUDE: 35 o )7 ' 30 ._0 ___ " + --12/_ ' /1-.!L_

SITE LATITUDE: ...J!i...o...2..E_ •__f!/:_ ._()_"

CALCULATIONS: LONGITUDE (7.5 ' QUADRANGLE MAP)

A) NUMBER OF RULER GRADUATIONS FROM RIGHT LONGITUDE LINE TO SITE REF POINT: 4 0&'

B) MULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS:

A X 0.3304

C) EXPRESS IN MINUTES AND SECONDS ( 1 '= 60") : ___f_6_' /f-. _ff___ " II

D) ~D TO STARTING LONGITUDE: ~o_LZ_ ' 3o . _Q__ " + ~·~. J[__

SITE LONGITUDE: __zjLo_jJ_ ' 13._0_" .

INVESTIGATOR: _________ ~~~~f~L~~~- {u- ~40~~=-~------- DATE:

E-10

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•••• "'! • •• ..

. ~. ':'· .:·; ... .- .. ··: . :

TOPOGRAPHIC t-.tAP QUADRANGLE NAME: __ __:...._!.~~=------ SCALE: 1:::!4,000.

COORDINATES OF LOWER RJGHT-HAND COR~ER OF ::!.5-MINUTE GRJD:

LATITUDE: 35 o :t7 ' }/) • LONGITUDE: _ffLo Jl_' '<0 .•

E-ll

DATE:

'IO:

F.RCM:

RE:

• 27 April 1989

File

Grover Nicholson r ·,_,l. f--· Telecon with Kelly cain

Acme United is recommended for an SSI.

S & S Metals is recommended for an ISI .

Toisnot SWamp may be done 3rd quarter 1989 .

•

Delete United Organics from EPA list. It may become a CERCLIS site. (Note: Upon further checking, it was determined not to add United Organics to CERCLIS. )

GN/ ds/ grover.docj p. 24

/

/

/

• • LWI'E: 27 April 1989

'10: File

FRCM: Grover Nicholson

RE: Telecon with Kelly cain

Acme United is recommended for an SSI.

S & S Metals is recorrnnended for an lSI.

Toisnot swarrp may be done 3rd quarter 1989.

Delete United Organics from EPA list. It ma.y become a CERCLIS site. (Note: Upon further checking, it was detemined not to add United Organics to CERcLIS. )

GN/ds/grover. dcx::jp. 24

I

I I

/

I

I

• • North Carolina Department of Human Resources

Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091

James G. Martin, Governor David T. Flaherty, Secretary

Ronald H. Levine, M.D., M.P.H.

Ms. Denise smith EPA NC CERCLA Project Officer EPA Region IV waste Division 345 courtland street, N.E. Atlanta, GA 30365

Dear Ms. Smith:

SUBJECT: Site Inspection Report

28 May 1987

s & s Metals Recycling company NC D093334969 Shortcut Road Gold Hill, cabarrus county, NC 28071

State Health Director

submitted herewith is the Site Inspection Report for the subject site. Based on our review of the available data, we have concluded the following.

s & s Metals R~cycling company, now out of business, is located on a 15 acre tract off SR 2455 in northeastern cabarrus county. ostensibly the company recycled aluminum; which consisted of melting scrap aluminum in an on-site furnace. The melted aluminum was then cast in ingots and sold. The company also engaged in oil reclaiming activities. Emulsified cutting oil (97% water, 3% cutting oil) that was separated from the aluminum scrap during processing was kept in three holding ponds on the site. originally, the oil and water were to be separated by evaporating the water using a.dehydrator with the remaining oil to be recovered. DUe to mechanical problems with the dehydrator, an estimated 200 gallons of emulsified oil was spilled into an unnamed creek bordering the southeastern side of the site. The North carolina Department of Natural Resources and community Development (NRCD) fined the firm as a result of the accident.

In April of 1980, s & s Metals started a landfarming operation on the east side of the facility adjacent to the unnamed creek as a method of disposing of the.~il contained in the ponds. Reportedly, runoff carried oil from the landfarm into the creek. NRCD issued a warning to the firm and the landfarming operation was discontinued.

Ms. Denise smith 28 May 1987 Page 2

• •

The company then decided to dispose of the oil in the ponds by using it to control dust and stabilize the roads on the facility. s & s Metals ~isposed of all of the remaining oil from the ponds in this manner. Reportedly, after all the oil was removed from the ponds, the ponds were filled in with dirt.

In addition to the oil reclaiming and aluminum recycling processes, there have been reports of other activities engaged in by the company, at the site. Reports indicate that old transformers and batteries, among other things, may have been burned in the furnace late at night. Also, waste oil, other than the emulsified oil, may have been kept in the holding ponds. There is also a report that drums containing unknown materials are buried on the site.

In January 1980, NRCD collected a water sample from a well north of the site and sediment samples from streams in the immediate area of the facility. Elevated levels of metals, grease, and oils found in a sediment sample from a roadside ditch adjacent to the property can probably be attributed to automobile traffic. Lower levels of metals and oils were detected in downstream samples.

In May of 1981~ personnel from the NC DHR, solid and Hazardous waste Management Branch and the Cabarrus county Health Department visited the site. They noticed sludge oozing from the ground in several places, and drums that had been left on the property. A sludge and a composite soil sample collected from the site revealed extractable levels of chromium, barium, lead, and cadmium. chromium and lead levels were significantly above EP Toxicity. There were no measurable levels of extractable metals found in a background soil samp~e-collected north of the site by NC CERCLA Unit personnel on February 3, 1987.

In March 1981, an EPA Field Investigation Team (FIT) inspected the site. Elevated levels of chromium was detected in a composite soil sample collected from the site and a sediment sample collected downstream of the site. Total chromium levels detected in the soil sample were noticeably higher than total chromium levels detected in a background soil sample collected north of the site by NC CERCLA Unit personnel on February 3, 1987.

Ms. Denise Smith 28 May 1987 Page 3

• •

DUe to the hydrology of the area and the contaminants found on the site, the potential for groundwater contamination in the vicinity of the site does exist. The sole aquifer in this area is the carolina Slate Belt aquifer which consists of saprolite overlying fractured bedrock. In the area of the site, depth to the saturated zone is approximately 20 feet beneath land surface. The nearest well is approximately 1000 feet north of the site and is used for drinking water purposes. There are approximately 1349 residents within a three mile radius of the site using groundwater. There are no alternate unthreatened sources of water available.

If you have any questions, please contact me at (919) 733-2801.

CAM/tb/037lb

77;7;;. ;-------Cheryl A. McMorris, Environmental Chemist CERCLA Unit Solid and Hazardous waste Management Branch Environmental Health section

• \.

2 Copies- I for main flle,

for period covering ~~1u~y . .Lti:f-to~ /9?7 . (Month)(De ) <Year> <Month><Day) (Ye~r)

Expenses:

• s1TE NA.v.::fuS Ot4:Js Rtt (/(1 (,11CJ- {' 0 101 Ale u D'J 2, ~. <,4'16'1 , o ,

Site lnvestlgetlon Dete ,.::),/.=?/ g-..:J · r ~ :

{ (_9Jty> . ~

Travel: Date: ;L 3{£+ To:(:;O\d H-1 f J $ Cost for trevel CNote whether meps~ '51' film~ etc.) <from expense report>~ 0~.00 'frav:' (

I

l. Background Search

II. Prepare Study Plan & Safety Plan

! I I. Coordinate Site VIsit

.. I y • Conduct Field Work

v. Review Analvtlcal Data

\'\-, Perform Analyses

\' I I • Comp I I e, evaluete dete, write report

VII !.Perform Hezerd Ranking System Scoring

x. SUPERVISOR REVIEW

-

DATE POSTED TO CR

Attach Breakdown ano Telephone List

. Rev. 8/6/86

Round off to nearest hour

I I

-,. (' '' " ·'I'/ •. .::J,'Jv ,,,._,r ~ Date Hours/Tasl< -

J I(~ . II 3 :~: ~ I: ------..:- -d7 .. . ~

:;tJ;;;.Jz.::; 7 I h/'7'

1/ ,..-; __ , ) 0,5 ,.-.. ,-, t I· - c-.t ~/.· I ' ..

.

TOTAL HOURS ON Sl ~'f'f,s

-

.... . -·. .. •••••• \ . • ____________ 5± 3 -0~~-\ ~~----- ------ ------ -----------------

_ _ .J-ltoJ_U 7, 5----bK~_it~-----.-----21 t-J bK ·J. -------

- _ J_J_?>_O TI ________ c:;_ - ________ _

. -~---- ---~-J_;tj %-1: --- 7 . _______ 2 j_6j__¢ ::t·- -----~--------· ___________ : _______________ _

--------- dJ~/_C(+_ _________ -___ i=-=-=--=~-=~-===-_;2_/~ / __ ?!_ - - ---- ---- I -~}J!}r-t· '-t 3)J?)11" 5

LfLf, 5

- ------- ---- ---------- -- ------- ----------------- --._.,

. ______________ _:___ __ _ -------------------------- -- ---------------------- ---. -----------------~--- --

--.:

-- -----·------- -- .·--· ·-- -----~ .• --- ---- -- --- --- ----

------------- -- --------- ----------------

. -·--- - -· -~- ------·-------- - ------- k

- --~--- ----- -- --------- -------------------------- . - -- . l: r~

. - -- ----- -- - - --- ---------·---- -- ------------------ . ---------------- ---------- ------ ·---------~_:

t:

• • DATE

I . a

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' \ \

•

30 January 1987

TO: Cheryl McMorris

FROM: Lee Crosby jP-J RE: EPA Site Investigation (SI) Approval

S&S Metals Recycling

'

The site investigation known as S&S Metals Recycling scheduled for 3 February 1987 has not been approved by EPA Region IV. Please call Denise Smith or Bob Howard for approval as soon as possible. Notification has not been made to the County Health Director. Please do not go to the site without coordinating notification with me.

cc: Bill Meyer


Division of Health Services P.O. Box 2091 o Raleigh, North Carolina 27602-2091

James G. Martin, Governor Phillip J. Kirk, Jr., Secretary

Hr. Bob Ferris Environmental Health Supervisor Cabarrus County Health Dept. P.O. Box 1149 Concord, NC 28025

I

Dear Mr. Ferris:

Ronald H. Levine, M.D., M.P.H .. State Health Director

30 January 1987

Confirming our telephone conversation of today, the CERCLA Unit of the Solid and Hazardous Waste Management Branch will conduct a site investigation at S&S Metals Recycling in Gold Hill on Tuesday, 3 February 1987. A copy of the preliminary assessment has been enclosed for your information.

If you l:uive any additional questions, please do not hesitate to contact Grover Nicholson, geologist, or me at (919) 733-2801.

u;J Lw

Euclosure

·'

Sincerely,

~ Cn.o~"t .. Lee Crosby, CERCLA Um.t Manager CERCIA Unit Solid and Hazardous Waste Hanagement Brauch 'Environmental Health Section

• .· :~Si~ii 4

·-~"'"- .

'j~~~J~t "!- i\ '- ' ··~\ ~"' ..... ~~ . ~ ~ t • ., ~ · 'l -:... . - ....:. ...

· ··::--.::-~: ;;../

• North Carolina Department of Human Resources

Division of Health Se rvices P.O. Box 2091 • Raleigh, North Carolina 27602-2091

, ames G. Martin, Governor hillip J. Kirk, Jr., Secretary

Mr. Bob Howard EPA C CERCLA Projec t Officer Wa ste Division - Region IV 345 Cour tland St reet, N. E. Atlanta, GA 30365

Dear :1r . Howard :

Ronald H. Levine, M.D., M.P.H. State Health Dir€ctor

5 Decembe r 1986

I understand t hat you are extremely conce rned about the s elec tion of sites for invest i gations for t he January- Harch 1987 reporting qua r t er.

lt'Lough t he sites scheduled for inve stigations are al1vays listed in the qu~rterly report an submitted to EPA Region I V during t he first 20 days following the end of the previous quarter, site investigations planned for January - l arch 1987 are also l isted below .

NCD980 7296 77 1 CD991278839

CD991278755 NCD0931376 36 !-l"CD980503106 NCD053 530234 NCD0 617956 96 NCD079044426 NCD048184451 NCD0034 71158 NCD040049173 NCD000770032

Knob Creek Harth State Che ical Hartin' s Bat ter Salvage Genera l vlood Preser ving Sanitation Services Landfill NE Chemical Company Uni tex Genera l Elec tric Company Lighting System Burlington Furni t ure Home Chair Plant 196 Nor th Chemi cal Company Amoco Oil Company Ame rican Pe t rofina 1arketing/ Selma Term

Please contact me immedia t ely if t hese sites a r e unsat i sfactory . I may be r eached a t (919) 733- 2801 .

LC/pc

cc: i1s . Denise Smith :1r. Bob Jourdan

Sincerely ,

:::sbyCJ..ohb'\ CERCL.A. Program ·1anager Solid & Hazardous Wa ste Management Branch

... _I I

I i


Division of Health Services P.O. Box 2091 • Raleigh, North Carolina 27602-2091

James G. Martin, Governor Phillip J. Kirk, Jr., Secretary

Ronald H. Levine, M.D., M.P.H.

4 March 1986

Ms. Denise Bland EPA NC CERCLA Project Officer Air and Hazardous Material Division 345 Courtland Street, N.E. Atlanta, GA 30365

SUBJECT: Preliminary Assessment Report S & S Metals Recycling Co. NC D093334969 Shortcut Road Gold Hill, Cabarrus County, NC 28071

Dear Ms. Bland:

State Health Director

Enclosed please find the Preliminary Assessment report for the subject site. This priority is based on review of available data.

S & S Metals Recycling Company began operations in the late 70's as an aluminum recycling facility. This facility was located on a 15 acre tract off SR 2455 in northeastern Cabarrus County. During their few years of operation,•S & S Metals received several citations from the NC NRCD, including a fine for spilling 200 gallons of emulsified oil into an unnamed tributary of Big Bear Creek. They were also warned for landfarming waste oil on the property. In 1979, S & S Metals dug several pits to hold emulsified waste cutting oil (reportedly 97% water). This oil was eventually disposed of by spreading it on the roads around the facility to control dust. The pits were filled in.

S & S also apparently handled drums of solvents and caustics. One incident involved about 120 55-gallon drums of solvents that were stored on the property. S & S's claims for off-site disposal could not be verified. In addition, there are reports from former employees who said drums were emptied and buried on-site. A nearby resident reported hearing bulldozers operating in the night and seeing trucks taking drums to the back of the property.

Ms. Denise Bland Page 2

• • In January 1980, NRCD collected surface and well water samples from

the S & S property and surrounding property. Well water samples showed elevated levels of manganese. Water samples from a roadside ditch adjacent to the S & S property showed presence of metals (lead 800ppb, cadmium 90ppb, cobalt lOOppb, chromium 90ppb, copper 540ppb) and grease and oils 36ppm; however, automobile traffic probably contributed to the levels of some of the above constituents. Lower levels of metals and oils were detected in downstream samples.

In March 1981 an EPA Field Investigation Team (FIT) inspected the site (contract 68-01-6056, TDD F4-8102-12). Upstream and downstream water and sediment samples were collected. In addition, soil and groundwater samples from six wells were taken. Analyses revealed detectable levels of many inorganic and organic compounds; however, the results did not clearly implicate S & S Metals as the source of contamination.

In May of 1981, Rick Doby, Waste Management Specialist with the NC Solid and Hazardous Waste Management Branch and William Archer of the Cabarrus County Health Department visited the site and noticed sludge oozing out of the ground in several places. There were also some drums left on the property. Sludge samples revealed extractable levels of chromium, barium, and lead at 100, 33, and 18ppm, respectively. A composite soil sample had extractable levels of 53ppm chromium, 33ppm barium, and 12ppm lead. Samples from the drums showed residues of both chlorinated and non-chlorinated solvents and formaldehyde.

Based on the available information a medium priority is suggested for a follow-up site inspection. Additional soil, surface water, and groundwater sampling is recommended.

On 4 March 1986, this Preliminary Assessment was reviewed by CERCLA Unit personnel and by the following representatives from the North Carolina Department of Natural Resources and Community Development, Division of Environmental Management: Fay Sweat, Groundwater Section; Glen Ross, Air Quality Section; and Howard Bryant, Water Quality Section.

If you have any questions, please call me at (919) 733-2178.

SA/tb/0184b

Sincerely,

Stan T. Atwood, Toxicologist Solid and Hazardous Waste Management Branch Environmental Health Section

• • &EPA

POTENTIAL HAZARDOUS WASTE SITE I.IDE~:TiriCAT!ON

PRELIMINARY ASSESSMENT 01 STATE,_oz SITE NUMBER

PART 1 ·SITE INFORMATION AND ASSESSMENT Nr lnnq·B3Ll969

II. SITE NAME AND LOCATION

01 SITE NAME (LegB!. common. oraescnptwe "''"'of stte) 02 STREET. ROUTE NO .. OR SPECIFIC LOCATION IDENTIFIER

S & S Metals Recvclers Co. Inc. Shortcut Road OJ CITY 04 STATE I 05 ZIP CODE 106COUNTY 107COUNlOB CONG

CODE DIST

Gold Hill NC 28071 Cabarrus 13 8 09 COORDINATES LATITUDE

I LONGITUDE

3.2. 28_ 39_._:_ __ 80 19_ A.=L._ 1 0 DIRECTIONS TO SITE rsr.nmg tram nearest pubhc rood)

NC 49 W about 1 mile fran Caba.rrus/Stanly County line to SR 2450. Turn right and go about 1~ miles to SR 2455 (Shortcut Road). Site is located on the right aboUt ~mile from intersection.

Ill. RESPONSIBLE PARTIES

01 OWNERtlllrnownl 02 STREET (8uu•oss, maRmQ. rosirlomW)

Charles Sehorn (present property owner) Rt. 3, Box 439 03CJTY 04 STATE I 05 ZIP CODE 06 TELEPHONE NUMBER

I Harrisburg NC 28075 17041 455-5452 07 OPERATOR (fftnownon<l<lofferon!lromownerj 08 STREET C8u..,ess, moiling, rolldenoal)

S & S Metals Recvclers Co •• Inc. Shortcut Road 09 CITY 10STATEI'1 ZIPCODE 12 TELEPHONE NUMBER

I Gold Hill NC 28071 ( I

13 TYPE OF OWNERSHIP CCnect one)

){A. PRIVATE. 0 B. FEDERAL: OC.STATE OD.COUNTY 0 E. MUNICIPAL (Agency n•rne)

0 F. OTHER: 0 G. UNKNOWN (Specify}

14 OWNER/OPERATOR NOTIFICATION ON FILE (COact olltnot oppty)

0 A. RCRA 3001 DATE RECEIVED: I I 0 B. UNCONTROLLED WASTE SITEcCERCLA !03 cJ DATE RECEIVED: .1_ I )!(c. NONE MONTH DAY YEAR MONTH DAY YEAR

IV. CHARACTERIZATION OF POTENTIAL HAZARD

01 ON SITE INSPECTION ~C,.ct d tnot apply)

. ,MvEs DATE 03 £23£81 A. EPA 0 B. EPA CONTRACTOR OC.STATE 0 D. OTHER CONTRACTOR

ONO MONTH DAY YEAR · 0 E. LOCAL HEALTH OFFICIAL 0 F. OTHER:

(5p«/ty)

CONTRACTOR NAME(S):

02 SITE STATUS rcnoct onol 03 YEARS OF OPERATION

I 0 A. ACTIVE )(B. INACTIVE 0 C. UNKNOWN -1978 1980 0 UNKNOWN BEGINNING YEAR ENDING YEAR

04 DESCRIPTION OF SUBSTANCES POSSIBLY PRESENT, KNOWN, OR ALLEGED.

s & s Metals recycled aluminum. At least three pits were used to hold emulsified cutting oil. The waste oil was landfanned or used to control road dust and the pits were filled in. There are also reports that drums of solvents, caustics were buried or PTTTDtiffi on the · ·· Soil and water samples taken by NC NRCD and EPA contained

OS DESCRIPTION OF POTENTIAL HAZARD TO ENVIRONMENT AND/OR POPULATION

many organic and inorganic canpounds; although m::>st were at low levels. However in May of 1981 sludge was seen oozing out of ground in several places. Samples taken detected chromium (100 ptm), barium (33 thpm), lead (18 ppm), and cadmium (0.8 ppm). There are several wells on-site and in e surroundinq area. Run-off enters two stream:

V. PRIORITY ASSESSMENT which converqe at the southeast comer of the site. 01 PRIORITY FOR INSPECTION (Check me.lf 11ip1t or,.tllum II Cheeked. c"""to Pot! 2 • W01ro lnlonnorlOn.,., Port3 • O.tcrO>tlOn oJ ""zor<tout Concllt""'s MttlncO»ntoJ

0 A. HIGH )(B. MEDIUM 0 C. LOW 0 D. NONE (lrrsp•ctk>tt reouit«J ptomptlyJ (Inspection 19Qulred} (lns,.et 0" tmt ,.., ... f:H basfsJ ("'o luttMr KfiOIJ neec~ed. comptet• current drspostriQit lotmJ /

VI. INFORMATION AVAILABLE FROM

01 CONTACT 02 OF (A~ncy'Orpln,ntiOI'IJ 03 TELEPHONE NUMBER

Rnn MrMi 1 1 i ;:m RPni nnr~ 1 ~- • != nr NC NRCD/Environmental Mcnnt. 704 1663-1699 04 PERSON RESPONSIBLE FOR ASS~SSMENT OS AGENCY 06 ORGANIZATION 07 TELEPHONE NUMBER 08 DATE

Stan Atw::xxi/Gro:ver Nicholson NC DHR/DHS SHW Mgmt. Br. 1919) 733-2178 l2 •3Q£85 MONTH DAY YE,t.R

EPA FORM 2070·12 (7·81)

• •• POTENTIAL HAZARDOUS WASTE SITE

I. IDENTIFICATION

$EPA PRELIMINARY ASSESSMENT 0NCATE!Coo~H334969

PART2·WASTE INFORMATION

II. WASTE STATES, QUANTITIES, AND CHARACTERISTICS 01 PHYSICAL STATES tChoc.,n '""apply) 02 WASTE QUANTITY AT SITE 03 WASTE CHARACTERISTICS rc•oc.,nr••••oo•;l

I Measures ot wnre ou•'"""a >(A. TOXIC )(A SOLID LJ E. SLURRY must be ~~tdtDtndftflfJ L: E. SOLUBLE .:. I HIGHLYVOLATILE

lJ B. POWDER. FiNES ::>(F. LIQUID TONS G B. CORROSIVE C F. INFECTIOUS ~ J. EXPLOSIVE

XC. SLUDGE L; G. GAS C C. RADIOACTIVE C G FLAMMABLE ::: K. REACTIVE xD. PERSISTENT U H. IGNITABLE .:._ L INCOMPATIBLE CUBIC YARDS - ~ M NOT APPLICABLE LJ D. OTHER

ISDtcdy/ NO. OF DRUMS

Ill. WASTE TYPE

CATEGOPY SUBSTANCE NAME 01 GROSS AMOUNT 02 UNIT OF MEASURE OJ COMMENTS

SLU SLUDGE

OLW OILY WASTE Unknown laooons filled in-contents sorea~ on prop.

SOL SOLVENTS Unknown Dnnns of solvents were alleqed

PSD PESTICIDES to have been emptied or buried

occ OTHER ORGANIC CHEMICALS on-site.

IOC INORGANIC CHEMICALS

ACD ACIDS

BAS BASES

MES HEAVY METALS

IV. HAZARDOUS SUBSTANCES tSeoAs>poiKI,.tormollfroouonrtrcno<ICASNumberr/

01 CATEGORY 02 SUBSTANCE NAME 03 CAS NUMBER 04 STORAGE/DISPOSAL METHOD 05 CONCENTRATION 06 MEASURE OF CONCENTRATION

MES Chranium 7440473

ME'S Lead 7439921

MES 'Rrlri llTTl . . .

SOL 1,1~1-trichloroethane 71556

SOL Tetrachloroethylene 127184

MES cadmium 7440439

.. . .

V. FEEDSTOCKS {Sot Append.• lor CAS Numbers)

CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER .

FDS FDS

FDS FOS

FDS FDS

FDS FDS

VI. SOURCES OF INFORMATION (Cno IPtcnrc ttltttncos. o.g., stalt l~os. sample anatr"'· reports I

1. Pennanent files, NC Solid and Hazardous Waste Mgmt. Branch, Raleigh, NC. 2. Files NC NRCD - Environrrental Managerrent. Morganton, NC.

3. EPA FIT Report, Contract No. 68-01-6056, March 23-26, 1981. TDD F4-8102-12 • .

. EPAFORM2070·12 (7·811

. a. ~ .. • • • POTENTIAL HAZARDOUS WASTE SITE L IDENTIFJCA TION

&EPA 01 STATE I 02 SITE NUM8ER PRELIMINARY ASSESSMENT Nr nnq·:n14qhq PART 3 ·DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS

IL HAZARDOUS CONDITIONS AND INCIDENTS 01• ~A. GROUNDWATER CONTAMINAnoN 02 0 OBSERVED (DATE: ) p(POTENTlAL 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

Alleged and observed on-site· disp:>sals of cutting oil and solvents.

I

01 ~B. SURFACE WATER CONTAMINATION 02 ~OBSERVED (DATE: .lY -/ Y ) ~POTENTIAL 0 ALLEGED 03 OPULATION POTENTIALLY AFFECTED: 04 ARRATIVE DESCRIPTION

Oil spill in creek, run-off fran !andfanning of waste cutting oil.

.•

01 0 C. CONTAMINATION OF AIR 02 0 OBSERVED(DATE: ) 0 POTENTIAL 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

01 0 D. FIRE/EXPLOSIVE CONDmONS 02 0 OBSERVED (DATE: ) 0 POTENTIAL 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

~

01 0 E. DIRECT CONTACT 02 0 OBSERVED (DATE: ) 0 POTENTIAL 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

01 ~F. CONTAMINATION OF SOIL O~~OBSERVED(DATE: .lYP:.:I x ) 0 POTENTIAL ~ALLEGED 03 AREA POTENnALL Y AFFECTED: 04 NARRATIVE DESCRIPTION

(Acrea} •

*landfanning waste oil. Emptying and burying drums on site,

.

011 ~G. DRINKING WATER CONTAMINAnoN 02 0 OBSERVED (DATE: ) ](POTENTIAL 0 ALLEGED

03 OPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

Drinking water wells near site.

01 0 H. WORKER EXPOSURE/INJURY 02 0 OBSERVED(DATE: I 0 POTENTIAL 0 ALLEGED 03 WORKERS POTENTIALLY AFFECTED: · 04 NARRATIVE DESCRIPTlON

01 0 I. POPULATION EXPOSURE/INJURY 02 0 OBSERVED(DATE: ) OPO~ 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION

EPA FORM 2070·12(7·81) .. - ~ ... ..

• •• ·, ... ,

&EPA POTENTIAL HAZARDOUS WASTE SITE L IDENTIFICATION

PRELIMINARY ASSESSMENT 01 STATEI02 SrTE NUMBER .

PART 3 ·DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS NC 0093334969

D. HAZARDOUS CONDmONS AND INCIDENTS ~

01 0 J. DAMAGE TO FLORA 02 0 OBSERVED (DATE: I I D POTENTIAl. D ALLEGED 04 NARRATIVE DESCRIPTION .

•

01 0 K. DAMAGE TO FAUNA 04 NARRATIVE DESCRIPTION tln<:ludl-trJolfPKIHJ

02 0 OBSERVED (DATE: I D POTENTIAl. D ALLEGED

-

01 0 L CONTAMINATION OF FOOD CHAIN 02 0 OBSERVED (DATE: I D POTENTlAL D ALLEGED 04 NARRATIVE DESCRIPTION

. 01 0 M. UNSTABLECONTIUNMENTOFWASTES D POTENTIAL D ALLEGED 02 0 OBSERVED (DATE: I

(Sp/hlnmofllllotldlnQ lquldo/IHJIJng 1/rutMJ . ' 03 POPULATION POTENTIAU.Y AFFECTED: 04 NARRATIVE DESCRIPTION

01 0 N. DAMAGE TO OFFSITE PROPERTY ~

I • 02 0 OBSERVED (DATE: I D POTENTlAL 0 ALLEGED 04 NARRATIVE DESCRIPTION

01 0 0. CONTAMINATION OF SEWERS, STORM DRAINS, WWTPs 02 0 OBSERVED (DATE: I D POTENTIAL D ALLEGED 04 NARRATIVE DESCRIPTION

01 0 P •. ILLEGAUUNAUTHORIZED DUMPING 02 D OBSERVED (DATE: I 0 POTENTIAL D ALLEGED 04 NARRATIVE DESCRIPTION

05 DESCRIPTION OF ANY OTHER KNOWN, POTENTIAL. OR ALLEGED HAZARDS

..

IlL TOTAL POPULATION POTENTIALLY AFFECTED: i

IV •. COMMENTS ' .. . . .. .

.. .... . . . . . ....

V. SOURCES OF INFORMATION taro,_,.,_,,.:, .. -.-. ...,..~ . .-~

As previously cited.

EPA FORM 2070-12(7·811

1000

( f/"":'.. ·'-I.~ r-' II '.,;,- .

RICHFIELD, N.C. N£.14 MOUNT PLEASANT 1!5' QUADRANGLE

N3522.5-W8015/7 .5

1000 4000 5000 6000

Lubricants

• Figure 2.

80000 60000 40000

20000

10000 8000 6000 4000

2000

1000 800 600 400

800

_1\\

~ ., " \\ \

''-\_ \\\.

\\' ~ ~2

" ~

~

i' .... ~

....... ~ ~I

~'"-"-.._

""""" -........ 14_~ ~~ I' .... ..... ........ ...

Heat radiation from fire at grade in different spill conditions of LNG and at a wind speed ot 48 km/h. 1. Fire in 175m sou are x 5 m high dike. Flame height above dike 177 m. 2. Fire in 72 m diameter x 35 m high dike. Flame height above dike 95 m. 3. Fire in 62 m x 35 m high tank. Flame height above tank 86 m. 4. Fire in 60 m diameter below-ground tank with capacity of 1 00 000 m3 • Flame height above tank 84 m. 0 100 200 300 400 500 600 700 800 900 1000 1100 12001300

presr,nce of LHG vapour. Seam welds. coupling pieces and other elements of cargo tanks are constantly inspected. Tank cover plates and heat insulation are made of fire-resistant materials. Remote control of pu,nps and other equipment is provided. Safety valves are fitted to relieve the LHG vapour generated at maximurn heat !oad. And in order to meet the risk of fire a comprehensive fire protection system is installed.

Statistics show that accidents occur in the operation and repair of manufacturing. storage and transport equipment. They also happen as a result of collisions or of running off the rails. In the majority of cases the accidents are caused by inflammation of air-gas mixtures. produced during leakage of liquefied gas. On leaking, liquefied gas evaporates quickly, spreading over the water or the ground. absorbing their heat and the heat of the atmosphere and of solar radiation. Although LHG vapours are colourless the cloud will be white because of condensation and freezing of water vapour. contained in the atmosphere. Figure 1 shows how a vapour cloud spreads downwind in different spill conditions. Special instruments for detecting LPG and LNG leakage are available and transducers detect the appearance of gas in the air at a concentration of 15-20% of the lower limit of inflammability, and give an alarm to a panel; when the concentration reaches 40-50% of the lower explosive limit. all operating processes are automatically stopped. and the air-gas mixture is treated with substances having a sufficient energy of absorption (water vapour. water. inert gas). Fire is a result of inadequate control of gas concentration in air in case of accident. Inflammation of LPG and LNG is accompanied by the transmission of great heat to surrounding objects. Figure 2 shows the specific heat radiation a ground level from fire sources of different configurations in various spill conditions. Fire-fighting measures are based either on localisation of the source. heat absorption or extinguishment of the fire Special chemical powders containii1Q sodium bicarbonate. potassium bicarbonate. monoaminophosphates and other substances are used for extinguis\lment. LPG and LNG complexes are usually equipped with fire prevention systems consisting of sta!ionary posts (reservoir fire extinguishers} and fire engines. Reservoir fire extinguishers are situated around t'le most dangerous places. Stationary posts are r-'Nitched on automatically by means of heat detectors. Fire prQtection systems are equipped with water supply posts for cooling equipment (tanks) in case of fire. ·r echnical directive5 for the safe operation of LPG and LNG complexes include safety engineering programmes.

1248

contingency plans for the com"Tol of possible accident and the training of safety personnel.

KUTSYN, P. V.

General: General Report. Report I, Petroleum Committee. Ninth Session

(Geneva. International Labour Office. 1980). 170 p. lllus. Safety and health: CIS 81-61 3 LPG-The hazards anclprecautions (Fire Protection

Association. Aldermary HousY.-!. Queen Street. London) (1980). 58 p. 44 ref.

Safe transport and storage of t:'C;Iuefied natural gas (Obespecenie bezopasnosti pri tram'Tlorte i hpanenii sjijennogo prirodnogo gaza). Racevskij. R.5. VNIIEgazprom (Moscow. 1981 ). 40 p. 8 ill us. 36 ret. (In RiJJssian)

"Careful accident assessment: ~Y to LNG storage safety". Closner.J.J. OilandGasJou::mai(Tulsa).1978, 76/6 (47-51 ).

Transport and storage of fiquefiediflydrocarbon gases (Transport i hranenie uglevodorodnvtr-:sjijennyh gazov). Racevskij. B. 5.; Racevskij, S.M.; RadCit..l:l. I. (Moscow. Nedra. 1974). 256 p. 119 illus. 75 ref. (In Rt;SS'ian)

CIS 79-1223 The safety aspects'C'!f.:the supply and storage LNGLPG (Ministerievan Sociale Zz~n. Oirectoraat-Generaalvan de Arbeid. Postbus 69, Voorf:~-rm. Netherlands) (Oct. 1978). 154 p. lllus.

CIS 81-318 Storage and handfirqr-Liquefied petroleum gases: 1979. ANSI/NFPA 58 (NatiQX:'&l Fire Protection Association. 470 Atlantic Avenue. Bo!rt~ Massachusetts) (16 Jan. 1980). 181 p.

Liquefied natural gas and liquef:Vied petroleum gas. Views and practices. policy and safetv·: US Coast Guard Comdtinst M1661.4 (old CG-478) (Vi2shington. DC. 1980). 38 p. 26 ref.

lubricants Lubricants are solid. plastic or liquid compounds which are interposed between tvl~o sliding surfaces. Their main purpose is to minimise friction. although they may also have important secondary-functions. such as conducting away heat. or facilitating ·the removal of waste material. Many substances can ao as lubricants such as soaps.

.,JC . '· 9= 41 .G! -,

l.

l I I I· I I I j

I

, . graphite or even water. but in ustry the commonest lubricants are oils and they may conveniently be divided into mineral oils. vegetable and animal oils. synthetic oils. solids and greases.

Mineral oils refer to the lubricating oil fractions of crude petroleum and are prepared from crude oil. This is a complex mixture of hydrocarbons in which are compounds of sulphur. oxygen and nitrogen. together with traces of many metals.

Crude oil is refined by a process of separation and conversion and products ranging from bitumens to propane gas are obtained. including the base oils from which most lubricants are prepared.

In modern machining. by far the greatest number of app!ica~ions require oil of high stability and this is achieved by solvent extraction and by the use of additives. Further treatment with acids removes many of the aromatics. which renders the oil less carcinogenic. The types of additives used in the formulation of lubricants include:

Additive

Corrosion inhibitors

Anti-foam agents Emulsifiers Antioxidants

Detergents

Viscosity Index Improver Anti-wear agents Extreme pressure agents Bacteriocides

Example

lead napthenate. sodium sulphonate polyorgano siloxanes fatty oils. fatty acids 2.6-ditertiary butyl paracresol. phenyl naphthylamine metal sulphonates. metal phenates

tricresylphosphate sulphurised fatty oils phenols

Soluble oils· use the same base oil as the straight cutting oils. but are diluted with water in ratios between 1 : 10 and 1 : 80. They are essentially emulsions with large quantities of emulsifiers to maintain stability. The presence of water and surfactants in the composition may require additional additives to control foaming and bacterial activitv.

Animal and vegetable oils from a variety of sources are available for a very limited number of industrial uses and they are frequently compounded with mineral oils.

Syr.thetic lubricants are blends of non-petroleum chemical materials in water. Their formulations are extrama!y complex because of the numerous additives they contain to provide the properties necessary with any cutting fluid. They form true solutions in water.

Semi-synthetic lubricants contain many of the same additives as are found in the synthetic fluids. but they also contain 10-15% of mineral oil.

Greases are made from a combination of superfined fat 3nd liquid lubricant.

Uses. Lubricating oils vary from thin spindle oils to thick oils required for steam driven plant: As a lubricant. oil is used on a ·large scale in industry for cooling the cutting edges of machine tools. and in lubricating dies and moulds to facilitate the release of the formed metal. Oil is used in the dressing and polishing of leather and in some countries whale oil is still used for this purpose although suitable substitutes are available. To give some idea of the amount of oil used in the machine tool cutting industrv alone it has been estimated that in the United Ki:~pdom some 67 million litres are used annually.

(}i1 mist iubrication. The techniques of oil mist lubrica:ioli 3rc b.sccming more widely used. The oils principally used are of mineral origin. Although strenuous efforts are made to protect the oper~tor from exposure to mist. these

Lubricants

are not altogether. I. The diameter of droplets in oil mist has been reported tn be within the 1-4 microns range and as such is respirable and retained in the alveoli.

Harmful effects of lubricants. Oil. more because of its wide use than because of any special irritant properties. is a common cause of skin rashes.

The lighter kerosene type of oil acts as a degreaser. removing the fatty layer of the skin and leading to redness. itching and a chronic eczematous rash. The thicker oils tend to block the pores of the skin. particularly on the face. chest. forearms and thighs. Inflammation of the pores (folliculitis) may occur and may lead to pus formation and acne in the sebaceous glands.

The original work on the malignant effects of mineral oil on animal skin was done in 1915 and most of this work was conducted on coal tar and shale oil products. The lubricants used in the cotton industry in the United Kingdom were almost certainly of shale oil origin and many cases of cancer developed in exposed workers (Mule Spinners· Disease). Further impetus to this work was given by Cruickshank and Squires in 1951 when they noted the increase in scrotal cancer amongst workers continuously exposed to neat cutting oils. and the relationship between oil and skin cancer is now well recognised.

Continuous exposure to thicker oils can produce warts on the forearms. backs of the hands and scrotum. Although they are relatively uncommon. they are precancerous and the resultant cancers are liable. if untreated. to spread into other organs. The incidence of skin cancers is greatly reduced if solvent refined oil. that is oil treated with acid. is used.

With the increased use of oil mist lubricating techniques. interest has developed in the health hazards these may present. Cases of lipoid pneumonia have been reported since 1925 and the possible effects of oil on the lungs have been summarised as:

(a) diffuse acute-interstitiaF proliferative inflammation with or without associ at€ pneumonia:

(b) diffuse chronic-a proliferative fibrosis:

(c) chronic localised-a paraffinoma consisting of large globules of oil in hyaline fibrous tissue.

Most researchers conclude that there is no increase in respiratory symptoms or diminution of respiratory performance in persons exposed to oil mist. Whether or not there is an increased incidence of lung cancer in persons so exposed has yet to be fully evaluated. Oilwater emulsions provide good growth media for bacteria and yeasts. and counts of up to 109 /ml have been· recorded. The dominant organisms are human commensals. mainly pseudomonas. klebsiella and the like and although there is no epidemiological evidence that inhalation of these can cause any harm. the possibility of extrinsic allergic alveolitis must be considered. With the increased use of immuno-suppressant drugs. there is a. possibility of individuals taking these developing active diseases from such commensals. Many lubricating oils contain bacteriocides but these are not always as effective as is hoped or claimed and they are merely introducing a further chemical dimension to an a! ready complex solution. The health hazards due to microbial infections of oils may thus be summarised under four headings:

(a) they may change the composition of the formulation so that it is directly injurious:

(b) harmful bacteria from animals. birds or man may be introduced;

1249

. 1 I

! I I

,I 'i i I ,, I

I !

~ L function·rests

(c) they may aggravate ng skin complaints:

(d) the presence of heavily infected lubricant aerosols of respirable size may result in disease.

Other additives introduced by the refiner or blender may be a potential risk to health. The presence of chlorinated compounds can be directly irritant to the skin. Tri-orthocresyl phosphate has caused outbreaks of nerve palsies when lubricating oil was accidentally used in mistake for cooking oil.

Synthetic lubricants consist mainly of sodium nitrate and triethanolamine. together with additives which are formulated according to the material being worked. although practically every such fluid can be used on cast iron and steel. Commercial triethanolamine always contains diethanolamine which can react with sodium nitrite to form a carcinogen. N-nitrosdiethanolamine. It is not yet known whether exposure to this relatively weak carcinogen under working conditions poses a significant hazard but the possibility of this. as well as synergistic and antagonistic interactions with other carcinogens. cannot be d_iscounted. The problem is further complicated by microbial contamination of such fluid.

The position at present is that nobody has shown that synthetic cutting fluids present any hazard. but neither has anyone shown that they are completely safe.

As has been previously noted. semi-synthetic lubricants contain a small quantity of oil in the formulation and this presents added problems as regards health.

HE4LTH AND SAFETY MEASURES Skin contacts with lubricants should be minimised by the use of suitable guards on machines. by the use of adequate protective clothing and by the provision of suitable washing and changing facilities. The use of strong detergents on the skin should be avoided and the common practice of cleaning the skin with paraffin and other solvents should be actively discouraged. Barrier creams are of extremely limited use in an industrial situation. although the use of skih reconditioning cream after work may be helpful. Medical advice should be available as soon as any skin complaint arises but the routine examination of workers for lesions on the skin and scrotum is of little value ·except in a few highly selected groups. Workpeople who are exposed to oil should be taught self-inspection and encouraged to seek medical advice if they discover any new lesions. In the United Kingdom a leaflet is provided by the Health and Safety Executive warning workers of the dangers of oil.

In work areas the oil mist concentration should be kept below the TLV and oil fume should be minimised by the prevention of overheating.

Lubricants therefore present several health problems. but considering the quantity and range of their use they are not undu!y hazardous. Furthermore, with good housekeeping, adequate protection where necessary and a·knowledge of their dangers. the risks can be easily controlled.

SMITH, D. L. KIPLING. M.D.

Report on a study of occupational skin cancer. Brown. A. J.; Waldron. H. A.; Waterhouse. J. A. H. (University of Birmingham. 1975). Copies can be obtained from the Univcrsitv Department of Cancer Studies. Birmingham. !.Jnil8d Kingdom.

'"Oi! and cJncer". Kipling, M. D. Annals of Royal College of Surgeons of England (London). Aug. 1974.55/2 (71-79). li!us. 73 ref

i250·

"Polycyclic a rbons concentration of some mineral oils. corresponding hazard" (Concentra-tion en hydrocarbures podycycliques aromatiques cancerogenes de quelques huires minerales. Etude du risque correspondant). Thony. C.: Thony, J.; La!onta!r~e. M.; Limasset. J. C. Archives des maladies professionnelles. de medecine du travail et de securite socia!e (Paris). Jan.Feb. 1975. 36/1-2 (37-52). tllus. 14 ref. (In French)

Oil. A workers' guide to the health hazards and how to fight them (London. British Society for Social Responsibility in Science. 1975). 93 p. lllus.

Precautionary advice on the handling of used engine oils. Kahsnitz, R.; Allen. R. L: Collings. A. J.; Eyres. A. R.; lmbeaux. E.; Mills. A. L.; Schoenmakers. J. M. J. CONCAWE Report 3/82 (The Hague. CONCA WE. Feb. 1982). 12 p. 5 ref.

Oil mists: CIS 76-1249 "External respiratory function and lung gas

transfer in workers exposed to lubricating oil aerosols" (Vnesnee dyhanie i gazoobmen u rabocih. podvergajuscihsja vozdejstviju aerozolej smazocnyh masel). Bruskin. Z. Z.; Demcenko. V. G. Gigena truda i professional' nyezabolevanija (Moscow). Apr. 1975. 4 (28-30). 11 ref. (In Russian)

CIS 81 -1400 "Cancermorbidity among men exposed to oil mist in the metal industry". Jarvholm. B.; Lillienberg, L.; Sallsten. G.; Thiringer. G.; Axelson. 0. Journal of Occupational Medicine (Chicago). May 1981. 23/5 (333-337). 21 ref.

CIS 77-642 "Removal of oil mist" (Eiiminer les brouillards d'huile). Elman-Duflos. I. Usine nouvelle (Paris). Dec. 1976 (142-150). lllus {In French)

Lung function tests The lung is the site of entry into the body of inhaled dusts and vapours; these may be inert or may impair the function of the lung either acutely or by giving rise to pneumoconiosis. The changes may be aggravated by smoking or by medical conditions. including bronchitis. emphysema and asthma; they are often most marked in elderly subjects. since the rung also deteriorates with age.

Assessment of lung function is recommended as part of the preplacement and periodic examination of those who may be exposed to a respirable hazard. The preplacement assessment may indicate the need for special measures to conserve the health of the individual concerned; it also provides a basis for comparison on the results of the periodic examinations. By this means · changes in function may be detected at the stage when they are still reversible. The study of groups of subjects may also contribute to the safety of the workplace. by revealing the presence or strongly suggesting the absence of minor degrees of lung damage in people working at particular sites. In combination with the environmental measurements. this information provides a basis for the establishment of safe conditions.

In the diagnosis of occupational lung disease. lung function tests are of particular value for those conditions where findings on chest radiography are not specific. e.g. byssinosis and extrinsic allergic alveolitis. including farmer's lung. The tests are also of use for assessing the severity of respiratory impairment and may be of diagnostic value when other conditions coexist. e.g. obstruction to the lung airways or advanced generalised emphysema. In the treatment of respiratory insufficiency. lung function tests are indispensable for the control of

• 18 February 1986

TO: File

FROM:

RE:

Grover Nicholson 9,.._.__ ,t(J;J 1~ Trip Report: S & s Metals Recyclers Co. Inc.

SR 2455 (Short cut Road) Gold Hill,· NC 28071 NC D093334969

•

On 10 February 1986, Grover Nicholson, Pat DeRosa, and Jack Butler of the NC CERCLA Unit visited this site. Prior permission to enter the site had been gained from site owner Charles Sehorn. The site had been occupied by an aluminum reclaiming facility from 1978 until 1980. The Preliminary Assessment of the site indicated that contamination by metals, oils, and organics may exist on-site and may be moving off-site via groundwater.

Nicholson, DeRosa, and Butler walked over the site during the visit. They attempted to· locate areas on the site where past activities may have caused contamination, such as the on-site lagoons, furnace areas, slag disposal areas, and so forth. Although only sketches of the former reclaiming facility were available and some areas had been filled or re-graded, a few of the areas of concern were identified.

While on-site, the CERCLA personnel took photographs and planned possible sampling strategy. It was decided that sampling the site would be difficult because the soil over most of the site was well mixed with metal shards and other fragments, probably resulting from the former reclaiming activity and from re-grading of the site. Additionally, on-site and off-site sampling data is available from a FIT investigation done in 1981 (contract 468-01-6056). It was decided that these analyses and the background data gained from the visit may be sufficient to rank the site using HRS guidelines.

. ..

TO:

FROM:

RE:

• • 10 February 1986

File

Jack Butler~~ Telephone conversation to Cabarrus Co. Health Dept. about s & s Metals NC 0093334969.

The Cabarrus co. Health Dept. was contacted on Feb. 7 & 10, 1986 to inform them of our visit to S & S Metals on Feb. 10. Mr. William F. Pilkington, Health Director, was not in on either occasion but messages were left with Ms. Francis Taylor and Mr. Bob Farris on Feb. 7 & 10, respectively.

JB/tb/0214b

• •

: ~./A.-c.-(_ t.-V/ A~-J.._ Do~ ~ z.j~/'3'ts:. ~ s:~s

;v;kkfs. j(/c_ -;-q 'f"-- ezc~_,_,o .4 ~A~.

0~ />--kf ~;-~ ~ci9 .;'?<!.~- ~· h'~LfP~ .4~ ~~ .. ~ ...

• • 29 January 1986

TO: File

FROM: Grover Nicholson 1-- A.l~/~ RE: S & S Metals Recyclers Co. Inc. - Site Visit

· I contacted Mr. Charles Sehorn, the present property owner, on 29 January 1986 at about 8:30 p.m. He gave his permission for members of the CERCLA unit to visit the site on 10 February 1986 and observe, photograph, and sample in any fashion necessary.

GN/tb/0210b

• • DATE: December 23, 1985

TO: File

FROM: Stan Atwood ~~ SUBJECT: S & S Metals Recyclers Co.

I called the regional NRCD office in Morganton (704) 663-1699 to see if they had additional information in their files reagarding S & S Metals. I spoke with Ron McMillian, Regional Supervisor. The latest information in the CERCLA files was dated July, 1981. Mr. McMillian said he would mail me copies of anything in their files dated after July, 1981.

SA/tb/0158b

• • DATE: December 13, 1985

TO: F II e

FROM: Stan Atwood

SUBJECT: S & S Metals NC D093334969

I cal led the Cabarrus County Health Department ((704) 786-81211 and spoke to Carl Measmer, Sanitarian. He told me that they first started Investigating S & S Metals In 1979 and bel leved they started operations In 1977 or 1978.

SA/tb/0221b

• • SITE SAFE.TI PLAN A. GENERAL INFORMATION

Site Name S & S Metals Site NUmber NC D093334696 Location Date 2/7/86 ___,::....;..:.. ___ _

Gold Hill, NC Cabarrus County

Purpose of Visit PA X SI Other ---Proposed Date of Inspect1on 2/10/86 --~~-----------------

Date of Briefing _....;:2:..:.../..:...:7 /....;:8;...;;.6 ______ _

Priority RBnking ---Site Investigation Team

Personnel

Grover Nicholson

Pat DeRosa

Jack Butler

PLAN PREPARATION:

Low Meditnn ---X ___ High

Responsibilities

Team Leader

Prepared By _M_a~_G_,i....__ __ ~"'-'-~t---c....~-L-..1f-~;...;;._=

Approved By---------------

B. SITE/WAS1E CHARACTERISTICS

Solid Gas Waste Type(s) X Liquid -~

__ Sludge --Characteristics Corrosive Ignitable Radioactive

X Volatile X Toxic React1ve Other

List Known or Suspected Hazards (physical,chemical biological or radioactive) on Site and their toxicological effects. Also, if known, list chemical amounts

HAZARD cutting oils

various metals - Cr

EFFECT(S) not unduly hazardous

acute toxici~ with high concentrations

symptoms are similar to food poisoning.

formaldehyde irritation of eyes and mucous membranes

_c_hl_o_r_in_a_t_ed __ s_o_l_ve_n_t_s_.,...._ __ \) narcotic effects

1, 1, 1-trichloroethane, PERC

TCE & 1, 1 dichloroethane 1

• • Facility Description: Size 15 acres Buildings one ----------------Disposal Methods Being Investigated leachate pond, surface dumping of sol vents

burial of drums.

Unusual Features on Site (dike integrity, power lines, terrain etc.):

History of the Site: Site was opened in 1978 as an aluminum recycler. The

company spilled 200 gal. of cutting oil in 1979, also in 1979, pits were dug

to hold cutting oils. The oil was later used to control dust on the property

and the leachate ponds were filled in. Solvents & caustics were handled,

approx. 120 barrels of solvents were alledged to be emptied and buried on site.

This site was sampled on 1/80 by NRCD, 3/81 by EPA (FIT), and 5/82 by NC DHR

Solid and Haz. Waste Mgmt. Branch

C. HAZARD EVAilJATICN

This is a site investigation to an inactive facility. The facility has been

inactive since 1980. Sampling has been done by various agencies. Levels

detected of chemicals has been low. No augering for samples has been planned

for this trip. Level D protection will be adequate. Surveillance with the

HNu with the 11.7 lamp.

D. WORK PLAN INS'IRUCTI<N

Map or Sketch Attached? Yes Perimeter Identified? No Command Post Identified? No Zones of Contamination Identified? No

Personal Protective Equipment

Level of Protection A ---- B --- ___ c X D ----Modifications Vacate site if HNu readings are above .5ppm.

• • Surveillance Equipment:

X H Nu ___ Explosimeter ___ TID

Detector Tubes and Pumps 02 Meter (Radiation Monitor)

Decontamination Procedures

Level A ---

Level B

Level C

X Level D

Modifications

Segregated equipment drop, boot cover and glove wash, boot cover and glove rinse, tape removal, suit and hard hat removal, SCBA backpack removal, inner glove wash, inner glove removal, inner clothing removal, field wash, redress

Segregated equipment drop, boot cover and glove wash, boot cover and glove rinse, tape removal. boot cover removal outer glove removal, suit/safety removal, SCBA backpack removal, inner glove wash, inner glove rinse, facepiece removal, inner glove removal, inner clothing removal, field wash, redress.

Segregated equipment drop, boot cover and glove wash, boot cover and glove rinse, t~e removal, boot cover removal, outer glove removal,suit/safety. boot wash, suit/safety boot rinse (Canister or Mask CHange), safety boot removal, splash suit removal, inner glove wash, inner glove rinse, facepiece removal, inner glove removal, inner clothing removal. field wash redress.

Segregated equipment drop. boot and glove wash, boot and glove rinse.

------------------------------------------------------

Work Schedule/ Limitations no sampling is planned. No augering for soil

samples will be done.

:ENERGENCY PRECAUITONS

Acute Exposure Symptoms

cutting oils

Metals

Solvents

First Aid

wash immediately

if skin contact wash immediately

If skin contact wash immediately

if inhalation, remove to fresh air

• Hospital (Address and Fhone Nt.nnber)

Cabarrus Cotmty Memorial Hospital

Fmergency Transportation Systems (Phone Numbers) Fire use 911 Ambulance use 911

use 911

•

it will turn into Church Street 2 which also becomes 29 & 601 Hospital on rt.

PREVAILING WEA1HER OONDITICNS AND FORECAST ..::Co.::.:l:::;;:d::.......::;;an::.:d:;.....;::;cl:::;;:o:..::u:.=.dyl--______ _

:EemPMENI' CHEOO..IST

X Air purifying respirator X First Aid Kit X Cartridges for respirator X 3 gal. Distilled H20

3M 8710 Respirator X Personal Protective 02 Indicator Clothing Detector TUbe & Pump Boots or Boot Covers

--- Eye Wash Unit Coveralls ( tyvek) X H Nu X Eye Protection

pH Meter Hard Hat --- Explosimeter Decontamination

Radioactive Monitor Materials. --- Poison Control Center - State Coordinator

ASHEVIlLE 704-255-4490

CHARLOTTE 704-379-5827

DURHAM 1-800-672-1697

GRErnSBORO 919-379-4105

1-800-722-2222

Duke University Medical Center Telephone: 1-800-672-1697

Box 3024 Durham, NC 27710

Western NC Poison Control Center Memorial Mission Hasp. 509 Biltmore Ave. 28801

Mercy Hospital 2001 Vail Ave, 28207

Duke Univ Medical Center Box 3007, 27710

Moses Cone Hospital 1200 N. Elm St, 27420

HENDERSONVILLE 704-693-6522

Ext. 555, 556

HICKORY 704-322-6649

JACI<SONVILLE 919-577-2555

~N

919-343-70!.6

Margaret R. Pardee Memorial Hospital Fleming St., 28739

Catawba Mem. Hosp. Fairgrove Chur. Rd 28601

Onslow Mem. Hospital Western Blvd. 28540

New Hanover Mem. Hospital 2131 S. 17th St, 28401

:. • (!_·_:.~.---.··. __ . - ~.

.tL ~

-~r/c__,

:Hay 21.. 1.980

.S & S Metal Recyclers Co., Inc. P. 0 •. Box .157 Shortcut Road Gold Hill;-NC 28071

-Attn:. -:Hr. Donald R. Smith·

- -Dear Mr. Smith:

We are unable_ to determine the ~inal destination of the 55-gallon. drums of solvents that was. stored on your property ·o·n Sho:.:.tcut Road, Cabarrus County. He also .do not have records of a privatt! hauler by the naree of John Crutchfield which you supplied to the office of Natural Resources and Community Development.

The delivery receipt ·dated April 19, 1980, to John Crutchfield. indicates no address or telephone number for this individual~ . Please submit to this. office ve-rification of :Hr.· Crutchfield's telephone and address by June 1, 1980.

Your cooperation in furnishing this-office'with the n=eded information will be appreciated. Thank you.

CRD:ns cc: Mr. Everett Calloway ·

:Hr.·o. w. Strickland Ur. Julian H. Foscue, III Hr. Mike-Groves

Siilcerely,

c. Richard Doby, Sr. -District Sanitarian for Solid·.

and Hazardous 'Haste Hanagement l69-B P.osehaven Court Concord, NC 28025 ·

N.., Carolina Depa~nt of Natural Resources &Community Development James B. Hunt, Jr., Governor Howard N. Lee, Secretary

Dr. Gerald Houghton Route 2, Box 238-A Gold Hill, North Carolina 28071

Dear Dr. Houghton:

DIVISION OF ENVIRONMENTAL MANAGEMENT t1arch 13, 1980'

Attached is a copy of the chemical analyses made on the water samples we collected from your well. The first sample Nas collected on January 22, 1980 and a partial analysis was made. On February 4, 1980, staff members of the Mooresville Regional Office collected a second sample utili~ing the proper collection containers for the various constituents.

The analyses indicate that your water is normal groundi'later for that hydrogeologic area. The only constituent that exceeded a recommended limit was manganese. The recommended limit for manganese, based on aesthetic quality (fixture staining) is 0.05 mg/1 (milligrams/liter) or,50 ug/1 (micrograms/liter).

The attached list contains a summary of the National Primary and Secondary Drinking Water Standards as required by the Safe Drinking Water Act. These standards apply to public water systems only. They do not apply to private \'tater systems, ho\'tever, they can be used to judge the quality of water being obtained from a well serving a single family residence. ·

Comparison of the quality of your \'tater with the standards shows that you \·till probably have manganese staining problems and some hardness pi"oblems.

Our analysis found no evidence of any hazardous or toxic, inorganic or organic compounds in your well water.

In addition to sampling your well water we are sampling and monitoring the surface water runoff onto your property and the stream \'later quality at various locations in the immediate area. Our sampling is not yet complete and we cannot make a statement about possible stream pollution resulting from activities at S and S Metals. When our sampling is completed \'te \'till send you copies of the analyses and our i~terpretations of the sources of any contaminants found.

Mooresville Regional Offi~e 1119 North ,\lain Stree!, \loor~;;ille, N.C. 28115 Telephone 704/664-4627 •

An Equ,71 Oprortunily .4 !':r~u:o..: ,.J.c,·ior. Employer

Dr. Gerald Haught~ Page Two March 13, 1980 •

If this Office can be of any further assistance, please contact us.

Sincerely,

MRG:sj u

Attachments

cc: Mr. L. P. Benton, Jr. Mr. William Ross Mr. 0. W. Strickland Cabarrus County .Health Department Mr. George Moe~, EPA Mr. Joe Young,JEPA Mr. Rick lbby \ Mr. Don Smith r1r. Vance Holt

~/-CL Michael R. Groves Hydrologist

For: Richard R. Peace, Jr. Regional Supervisor

?7]~ rr\ :·~ ~---

/f: .. ::}:J~.*~~~ N__.,;~l Carolina Oapart•':~!:'~nt of Natural·/·--~-- .. ·.,.~~·- -~--:1 ~ \....1 ;,J .

-~;;~~~V Resources & CommLinity Developrnent ~~ James B. Hunt, Jr., Governor Howard N. Lee, Secretary

DIVISION OF ENVIRON~1ENTAL MANAGHiENT

February 20, 1980 I

I ~-"\. ' I 5" "i· 5 ., , ~- L . .(_,, -~

fvtr. Joe Young Environmental Protection Agency Hazardous Haste Section Disposal Site Unit 345 Courtland Street Atlanta, Georgia 30308

Dear Mr. Young:

Per our telephone conversation of this date, enclosed are the analyses of surface water at the S & S Metal Recycling Company in Cabarrus County, North Carol ina.

If you have any questions, please do not hesitate to contact me.

RRP :sju

Enclosure

cc: Mr. L. P. Benton, Jr., Chief Operations Section

Sincerely,

' .:, ~

'·' •' !· Z:' .... y.~:-.;;.. ~;·1 <" ; I /_··tt .::,.·:,<.'.. /'· , :- ~t;· t; {. / ·

Richard R. Peace, Jr. Regional Supervisor

:.1oore;,ill~ Rcgiona! Office 1119 ;'>;or:h :\bin Street, ~bor~;villc, :\.C. 28115 T~le;:>honc 704/664·4527

An £qual 0{',"''J'lunity Atlirm•J!i•·-: Act/or; Employ<!!'

••• ••

MEMO. DATE:---------

..?11~ North Carolina Deportment of Natural ~~~ Resources &Community Development

. 'i I

.rY _________ ~-~·~·~--·~·~·:~--------,·,/·I .. ,

:UVER !lASl~·---------::l...t.../:...1.:..1_· _______ _

RF.PORT TO: (C:Irclr Clnr}

ARO, WSRO, l!lic<i mo, t'nRO, lHIW, RRO, TS, DM

AM, OTIII::R ---------------

/ ·•' COLLECTOR--~~-'·-~)_,_·~(-~_·: _____________ __

/ BOD MNCE ------SEED -------

CHLORINATED __ -t...:A~J...:"":.!..-------Station Ko, Date Dccin Tir:•ll Degin

ss ('<

N. C, DEPT, OF NATURAL RESOURCES & CQ}U1UNITY DEW:LOPHENT

DIVISION OF ENVIRONH£NTJJ. HAIIACEN,r.Nt

FIELD/LAB J.'OIUI

Ocmm 0 COHl'l.IANCE D SPLIT

'=; (/(· ) ·() "" c-,-.. LAD NUHllEJ\0 .,~: ,\~t..t ,\'../

IJ •Tr. l'l'('r.lV"D /- 25 • ';'('~) " •.. ' ·. ,,., .. _._:.._...:.:.,.:;.;;..._..:..:....;;:;_ __ _ RECEIVED 13Y. __ -_c·-~{;..: ·-· ----· "_ • ..;.~....;·;..;,;...· .,:.;D;;._

DAlA ENTRY DVl.........;',.,.;:(_-'-("-(...:~:...7_ ,.,,. /'

CK t,\,-()

2- . ,I ·.: r:;~" DATE REPORTED·---..::.:::..-_;.._,.(1::;.;;; -i:::l-+--

D INTimSIVE S, .o EMERGENCY _..,, •.~ ,.. ·,\··

~'--' ~ • ')~- A' :.,l.t I v •t STATION LOCATION-~~:::=c.~#J4--7';J::-=:.::.:.:.....__.....J'.t!-:.~~:h~~...t::::::~~~~:::::::....d::_,_ ___ ~·--yl_'/'--

R~~------------------------------------------------------------------Date End T1me End Depth DM DB mm Value Type_ T1 5 1 cr B S:unple T

I A II L C @ CN

1 :. 2

J

4

5

6

7

\(

X BODt; "'n \ \ mr./l

?.n. rnv./1

Chloride uo rnr,/1 NIIJ n!! N 012 rncll Mn - llnnr,nnN•!.' 10!'15 -

ur~/1 lTV.~' ,.,~ N "!?.~

ll

9

10

11

12

'3 14

: I 17

10

r.on .. ~ n

Coliform, HF Fecal '""'" Coliform, HF Total31!!t'M

CoU form Tuhn Fecnl.,l.,l'<

Coliform, Tube Total 3 1.,0 ., . / .-..: Residue Tot11l "''"' ir>4-

VC&lnt:lle 505

Fixt'cl !110 ,, Residue Susnr.nded Q ,, !130

Volntilc !13!5

F:l.xr.d !540

'.< lnH 1....3 Acid 1 tY to pll ,,,s Acidity to pll 8.3

·- ~JknJinfty tCI pJI 8·, 3

IA1knHn1tv to nlf 1.,5

TOC 11110

s~~pl1nr. Point Temp. cu

1\rF:t'nir 1002

/lOOml Chl a Tri 32210

/lOOml Chi u Corr 32211

/lOOm! Pheonhvtin a 322ta

/lOOm! Color (True) ao

MP.fl Chro~lum Hexava1~~~2

rnro/] levan:! de __ 72o

rn"/1 Flour:lde D!lt

mr./1 ForD'.aldehyde 71aeo

mroll Crease nnd Oils e!lo

.rnr,/1 Hnrdnces Tc>tnl 1100

unit~; ~ffiAS ""A!!OO

mP./1 Pht>nolA :U.,.!!!O

mR/1 Sulfato D4!1

mr./1 SuJ.fido 7A!I

ru~/1 l':noc:l fie Cc>nd P!l

mr./1

n.o. pll trnitR

mf'/1 ~!a - Uobbdcouc 10111:

ur./l NO,+NO't ns N tl:lO mr-/1 r~a - Sc>dium 1120

u~/1 POl as P '7050.,. mP./1 Ni - Nickel tOE<.,.

uv/l I' Total us P r;"" r.lP./1 l't> - J.e:ld 1051

units Ar. - Silver t077 UJ>/1 Sb - Antimorl\' tn<>'7

ur/J Al - Alt:m:lnum 110!1 uc/1 Sn - Tin 1102

rnr./1 ll:t - Barium 100'7 II I'll liT - \',.n 'I.! i "'" 10!l7 I

mv/1 nc - n('rvJ.] ium 1012 "" /] Zn - ?.fnc 1092 u

mr,/1 Cn - Calcium QIO mP./1 Pr.sticfdes (Sprdfv)

my./1 Cd - Cadmium 1027 ur/1

n•r./1 Co - Cobalt 103? uPil

rnv./1 Chrom:lum - Tot.11 10'" II I'll Orr.nnics (Sued fv~

ur./1 Cu- Connorlo42 11r./l fliJI./l

1- !.'_r. - Iron 104!1" uc/ 1_

!IIJ>./1 llr. - H<?r~urv ?tono tu·ll

ti'HIIOS/cm T.1 - J.fthlum 113:?. 111'./1

Hr. - Mngncsiurn 027 mr./1

ph 1,,5 pll 4.5 Acidity pll a.J Turbidity llach Pr % I

A~3 1210~~------~--------~~--------------~~------------~~----------~~~--------~~~-----------e~~------------~~-----------soo .coo .C38 .C3~ 76

Sccchi Dink H 1 llr. Set, SCilida

[l.78 !1001)6

Strr••m flow St'Verl.ty

Cloud Cov,•r

c 1.3~1 3:7.

Odor-Atmos netr.rft>nt Sutln . Severity Scvt'r ty

01330 130!1

D}IJ/REV, 9-78

Conductivl.ty UMIIOS

l'rccl.p1tntion Inch~s

Dead Fish Severity

13.CO

Salinity S/L Strc.nm·Stnce I •·tow, Inat. IJ}•dro J::ll·r.. Flow1 Jr<:D •·c. CFS Di!m Dill. c•·s 7030!1 (J!I Ill ?20.34 :100!'11

Wind Df rc:r. tion Turbl,!Hy 011-C:nn:Je SJ ud!;l' Flo11t1.n~ llt·brJs 1-'rom Jlorth Severity St'verity Severity Sevc:rlt

311 1.3:10 131!1 13<4!5 Streuo: Color

1. Silt or ·SedJrnent

Susp, Severity Sed, Severity

I . Identity Aquntic Vecct.\tiut'

Suppc:rt Mediu~ Suvt'rJty I

------· ·I f CllliNn' _____ t;__·'.;..' ...:.i_._,·~· ··~··~l;_t .:...' ..:.._ ____ _ ""' r'!<. N, C~. Tllil~1'. 01' NA'L'\JIU\1. n~:l:OUUCHS C. CmiNlJIIITY lli\VJ·:J.~JI'M·;Ill' l.AU NIH Ill Ell n (.-' .I ,·t

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nm.u/1.1\n l'OIIM 1JA1'1~ JU·:crn Vr·:u _ _,_/_..J7:...(.~3~.-.;$i}"-f>b'i,:._ ____ _ lti'CJ;IVW UY ______ I·..;'r.._·_, _______ _ l'QQIIT_'fllj (CI rrl <• 011<'}

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;,._·._.-'._('_._J._:· ___ ·._· ----

IlO:> RANCE ------- SEED ------ STATION LOCATIONI_.:;....f;k~:a.::::~;t:-.#~~~-~~!:_....:::~-LJ~~~~~====:!__::_d,.f..:.:;z::::.__

. ,\ ,. ·' IU:~~:\.....!::..b~.L.E:t':I:.,.:~=...-L.!;;:..:...L.-.:..E;!....;t-~::...:...~---------=--------------.t J CHLORINATF.D ---.!.'..:·..-~)---------

D~tc Begiu . \I\ \..'\ ..... ,\.

.. Tit•a Begin•·:·- Date· End •'r·:IDle End Depth .OM DB DMB

1'cmp. pH Units Alkal.:fnity

A~3·----LL-----C~----------~~~~-----------~~----------~~~----~·----~'4~1~0----------~~----------~~~------------~~--------------pit 8.3 Turbid.ity llach Fl'U

435 78

Scec:h1 Diok M 1 llr. Set. St'lida fif~g~ctivity Salinity S/L ~~~cam·Stllge I H~w, 870 30!1 G!S 61

Inst.

Strenm Flow Precipitation ~ind Direction Severity Inches From ~lorth

C I.J::JI

bdor-Atmos · )icvcrity

01330

DHl/RF.V. 9-78

Dead Fish S11verity

1340 Streolt Color •

Turbidity Severity I on-crease

St'ver ty

1300 Identity

1lydro1Ele8ts

Dalll D s. Flow, ~IGD

72034 !100!11

Sludr,l' Floatfn~ Pl•brJs Severity Sc\'cr t

1315 134::1 A~ualic Vctct.stfuy Suppcrt tc~ um Scvl'r ty

ccu::T't c·rJ)c-\·{ '(·\;1.-~=------!UV£1( llASlN \.. { r,.d/!,.j; r)._,

,. ~ .. 'I

~~::-~.u~~amt~"---.... 1_;. rL..;.:,_-.. ~7~:...· ~~-llA'm i!ECI~lVJ·:n ___ _,_{_· --~~~:..:G~ . ..:..~ _· _.·;.:.~:..:../_"..:..) __

N nf.1"1'. o~· tlhl'URAL. UE!>OURCES & COHNUNlt'Y lJi·nHENT . . ...... ·' .... _ ~'

DIVtSION OF l~NVllt(lNHJ·:NTAJ, MAN.\CEHEN'C

'I Fmi.IJ/LAU ~'UilM 1\Jo:Clil\'l·:o uv, _____ ....._.....;._.....; ____ _ rn:rorn TO; (Cirrl" Onc-)

,\RO, l.'SRO,,.~ FRO, WaRO, WU:O, IU\0, TS, DH CK ____ _.,. DATA I(N'J'RY n._ ____ _

AH, OTIIER __ •••.. ----··-.. --·----I

DA TJ·: RF.l'OH1'f.DI _ _J.I_-_c-.L.,2 .s.L~) ·--..... 8tJJ-t..::..' P ___ i. ' /'

COLLECTOR •' .. - 'I,

tOO RANGE s~:r.o .. .. .. J

CHLORINATED -1.~ .. D S'tntilm ~o. Dote Dl'ciu Tit1a Begin Date End T:hne F.nd Depth DH DD mm Valua Type T, s, or .B Sample Typ

' .. .. . ---:a '<! tJ,., .

:::·:. ... ~)/ ·t •. ' ... II L c (C!) GNXX ;· .... ., ) ·';/ ,'

'=· \'-':}r I 'I ,, : I

Temp. co pH l'nitB pll O.J Tcrbidity Uach l'TU S.-IT'pllnr. Point

1 PT %

A~J J2 ro~---------------~~2---------X•~o~o~------~~---------~~-----~~--------~~~---------~~---------.3!1 711

rtrcmn·Stiii\C I gpnw, Sccchi Jlf11k 11

870

Stream flow St>vr.r l ty

c 13!11

Odor-/ltc:oG Severity

Dt33o

DNI/REV, 9-70

1 llr. Set, ~oUds

!IOOOG

Cloud Covcr

3:l

Dctcr~cnl Sut~~' Sever ty

130!1

Prf.!cir1totfon Inches

Daud Fish St'verity

13.CO

Salinity S/l.

7030!1

30

\.'htd Of rcr.tion Jo'roP• tlorth

Strcalt Color

11.1'. Inut, ll)'dro J:h·8· now, t!Gil IC, • ·S ll11m OJ u, 'f:i

61 7203.C !100!11

Turbi~ity Sever ty Sl udr;i Sc\'cr ty

no."ltln~ [ll•brJs Sl'\'t'ril

13!10 131!1

Silt of Sedfment Susp, Sever ty Sed, Severity

Identity Acu:atic Vt-ect.uiot' Suppct·t llcdiuc1 Scvl'r Jt)'

COUNT\' __ 1_. _' -' ·---~'----------

RIVER DAS!N __ '/,_._1""'·,).!1_ 1 ·.-J _______ _

BfPOBT lQl__Jr.lrc)r On~)

IIRO, WSRO(MRO,: l'RO, W.1RO, lHltO, RRO, .. -.

COLLECTOR i· ~. f I ; ( I,. ·'

. '. ~ , ... ------i·~:.' I

BOD RANGE SEED

CHLORINATED ·&.o . Sto:tticn No. Date De&iu

<96· 6' (0 . ,~if

Temp. co

~

i •

. , NcP~l'T. OF NATURAL RESOURCES & cm!NUNITY nO~IENT

DIVISION OF JWVIROillii::NTAL Z.W<IIGENEl/T (1r.._~ FIF.LD/LAD roRH J ~-V. t.p

') ~{J \

rarDc~ ~~'7 0 CONl'LIANCE D Sl'LIT

0 INTl::NSI.VE S. ~ E~RGZNCY

~"·:.JTATION LOCATION .S·f_ ·r, ;.{cc. • iC/<: . )

REMARKR .Somt'lfc, «•<;cr'\. \?or,-1 ·,a re'>pn .. s.'< ......•

/. : . ·., /I/ r"/.1 LAD NUl-DlER~D-----"-->--------

1 · If J r"i /.1 DA1r: RECEI\'ED __ .;,.._I:....,.....,·..~,)_. ---'"/;....,;.;;·'---

1:.1(1. R~:ct:IVI::U llY. ____ -L._;....:._.... ____ _

DATA ENTRY BJ----'..;,··-- CK---

DAn: RJ:POH.TI;01 _ _:./_·---3t.::..'(_::;...1.:....'-~(~:.;:.o;.;...;...'-

(Oiiy,) Jc, I o-l-1

, D.1tc Jo:nd T:lrno F.nd Depch DM DD DUll Value Type ·r, s, C'r n I So:tmple T)'l

1-~ GNX ;,•. I

3ut.:yr../ A H L I c ·;·

pH l'nitll

A~3·----L£----~·~----------------~~------------~~----------~~~--------~~----------~~----------~~------------~~----------Secr.hi Disk 11 n~eam·Stage I Hgw. Inst.

115 81

Sot. SC\lida Salinity S/L

' Sever .ty ·· l h .. b l1rom llorth Severity Scvl~rHy

11\'d ro1Elc~ 1• p,,m II a. "rS i

!itruT. Flow rnrlle'J:!IlftDtfon ~fnd nfrt~r.tioh Turbfr!Hy I ClJ.l-C:ren!lc

c 13!11 1300

·~~--------~~------------~~------------~-----------~---------J~~-------~~------~~~---------~~-------Odor-Atmo:; · nc tr.r(!c-nl :>m:n ncnd FiRh Strmur. Color Sfl t or Scdftuent I' IdentHy A~l!.'lt lc Vt·&ct.H J nt' Severity Scvcrit:y Severity Susp. SeverJty SecJ. Severity . Suppctt ~.t>diulll Sl!vcrJt)'

01330 I lOti 1340

Dm/IIEV. 9-78

(" / '·._ .. ~/ .•. ;,(·l_.. .~::::._·· ./ : '-····~:::..::. ... , LJ\0 NUHDEH.""~-~~~r-:--.'5

N. }~:PT. O}o' Nh'fl!F~•J. ltF.SOUFCF.S &-cmNUNITY~DJ:\__ jHENT . ~ - "'"' --

·-· . 1>1\IISWN Of I·:NVTRONJ-mll'f.\1, MANACI!HENT •• )(j~"\.r DATI:; l<ECl·:lVtm __ _,,'-.. l../..-:1-u.~-· ;a;.)_. ~&L.· .:::D~------J1TJo:l.ll/J.hD I'O!UJ t ,f #~\ !/0

BErQr-1' i'O; fClr<"~<' On!') SJ \' IU·:Ct:IVJ.::D llY-------'l..\-+~:~o._--------ARll, FSr:o,{MJ:_,ol, FIW, W;l!\!), 1111\l.l, l\HO, TS, mt SMD'll' 1'Y '·' • •o::.Cl!'t . .:Hr• lW- 1 "~<- •-:~ .. •· '''"""' x_\ f\j )''2"' '-.:..:~ '•/ E1 -- ..._ .. ··""'..._._......__. .. ...........,_ .. ....., -~ IIATA t:tffltY nv411'\ CK----~A{'j·(_t-'::::-

1 • .. ·.· 011·' :.!\'!'1.'1,'· •. ·• WATEII ANllWNT Ot:oitt·: 1-.-::J (~ _(Q'' /"\ N-, cnm:R ----···-··--·----...-- ."J ·~1 '\ (._ 1 , , ... :~.':.:=.~.::· :.; 1> O SEDIM.I-:N! 0 cgNPJ.IANcE 0 SPLI'r DAn: REPOR'n:o•--..!.--..:.-4:...w.;._-::...z..::...:... ___ _

cottr.cnw. -~~D=~JU_·.:...;·:..::/2;.;:.·.:..::..:~'::.:-·::..:-?::::·_,~:;_ ______ • • !· .• · .... :.,·.·i:·;:.:OTisstm 0 INTENSIVE-~· ~·ENEncm:cv d.~ ~:,.;., BOD F..,\NGE ------ SEm ---~~ .: .:_.:.:..J STATION LOCATION • 515 £t~('.li&·(o:, . . •

. . .r , • . , .1. . • ;;,.~·Lr-... ~· ·' . 1 J' , J • gOld.srd A. di-/cb. adJac.enf< TO Sy;£ ,(l('(~[C/t:'Y~LJ:I-C .,_ k n Pbec1~ )<'f/t:_r;._.

COli:\~'Y ____ ~_.:"'...:-,J.....:(''-~;.;-r....:...!.f....:\~lr _____ ---

\/jJ)fJ. r' / 1'\. ' ~-l----------RIVF.R ll!tSl~

CHLORINATED -.....-LfJ~··~·{);__ _______ _

T:lme End Depth D:i DB mm Value Type ·r, s, t-r B S:~mple Type Station No.

A II L C C CNXX

Sl'a-p inr, l'oJnt

1

Temp. C0 pll l'nitli AlkalJnfty PT % I ~3 lz 10~----------~~~----------~4~0~0~·------~~--------~A~IO~-------~~~--------~~-------L~~------------CCChJ DfPk ~~ 1 nr. r..~t. Hnl1d11 fiNrH\l!'~tivlty SnUnity S/L R.P, ~{~amn·!:tuscl H·sw, Jnnt.

o _______ ~~~~-----------~~-----------~7~o~30~5~----~~~------~~65~-------~e~•----------~~~---------~~~~~~~~~ trt'nm Flow I ClouJ Covt!r P::ccirftotJon t.'ind nfrcctton Turbit!Hy I OU-C:rense t:'Ver f I}' Inchell J'ro111 tlorth Severity Severity 135132 30 1350 1300 Jor-Jitc:u:> ll<!tert:t·nt :; ... ;,. l>cnd Fi11h Streorr. Color Silt or Sediment Identity r.v~rity Scvcrlly Severity Susp, Scver:lty Sed. Severity

ll3~--------Jlll~0~5~-----------_J!I3~4~0~----------~--------------~------------~------------~------------~----------------~----------------ONI/REV, 9-78 . '

· .. ,. ··y "':) .:· • ,j, I ..• ·-----~~"- '7 __________ _

i:t \'tk UASHL.--::.J.V.Lt~!){.L\,,Ll~·i~-------!,\:"l'\lf\1' 'l'O: .(Citrll' {1,,£.}

MW, 1-'St:O,~ FRO, 1-/:~J:O,

A.':, iJTIIf.ll ------

CO!.LF.CTOR

tn 1:0, m:o, TS , nH

BOD RA!:CE ---~--- Sf.l:D ----

cm.ormrArr.n

N. ()l·;J{ \w ·N~~.'UI~~~~ ltESOUR~;.:s ··~ C;l~l:I~Jllll,/;;,.;i),;N'l' ·~ . IHVISlOit 01' JmVIltllNI·Il:NTAI. HMACJ·:m-::rr

1f.f

FIEI.Il/I.AU I'OilH , Jl '{f' \ ~\

.·.·.·n SEIYlHF.NT 0 COMl'L!AUCE 0 SrJ.l'l'

·"--~})···,.... ,Jr;.r!-1.1\U tiUHHl~J(,!!__ r;':.>..tfJ-7l-j -s··~}-~}·-"'·:t..;.:;;d:._ .. ----DATI~ Jtt:Cl~l VJ-:1.1

RI·:t:ElVI·:u llY. ______ \y\£~'.,.· :::i-~11.-------DA'I'A t:NTIW ll ..._..;........;___ CK-..-----· ·-·;...··-:--

/ ·- ~ ~ ...,. 1-"(..)J {i DATI~ REl'ORTED'--L---..::.:...::I·_~'il;...,:~-----

. SA)Zw~~~: Csuho·r·] ~ • :~~:N~'!-1 l'nro~0~ud ' 0 TlS!lliE 0 INl'HNSIVE S ', m EHT::RGENC.!Y ' ;In· ;.'Jf..,,..,

STATICN LOCATION ~·'51.:£ ~"('.J ,_f'!:,Q_:;:.9:::-__________ ,"'r."'!_~.-.----------------

Station Ko. .. Tir.•a llegin. · ·

RuiJ\RK~\.....--""J.Jda~wn~Sil.L;:;t:U,~,.D::==--'I-ll~~: .a.10~~)~~ko;a~l:,A.._h,~P1.1..4-op~(Jffh:.JJ.Jl~·l 0::.1-1 ~(j.:...ui '~\ ,.!.;;JPr~\c~c\,.;r..J·o+\ ..!.!,I.~,J.J.J<'l~H~k;....._ .' _: · Qntc End Time End Depth DM DB DHB Vol ue Type T, S, l.'r B Semple Typl'

:,~l)() g_ ~~l)~ A II L C •. G j GNXX .. : ....::::...4-;:l-~~--'--..t.U.o;;~x;;;4-...1.....t:..J..:::::::...;=----'-~~t..:;;;:.:L-_..l-~;.:_~---l------....L.-----·-"'--------L-_;.:.._;.'---[\j\\~

;~n·pllnr{oJnt I Tenlp. C0

AlknHnJty ph 4.5 I pll 4.5 . Acidity pH a.J

A~:~ J:z _IO~-----------------J~~------------~~-----------_J~~----------~'·~·~o----------~4~38~-----------~~----------~~------------Sccchi DJsk H 1 Jlr. SClt. !:olids flrdlg~cttvity Salinity S/L f~~onm·Stagc I tl·~w,

05 70305 85 01 870 !50006

Inst.

5 t rl'mn Flow Cloud Cov~r Scverlty

Cl3:st 3:Z

· Odor-Atmos I DctcrfcnL f\ar!n · $t:vcrity Sever ty

Ci 13:10 1:10!1

DHl/R&V, 9•78

rruJ:irHntfon Inches

J)l!ad fish SC'ver ty

13 .. 0

38

'-'ind Direction FroDI •:orth

Strcatt Color r

Turbi~it:y Severity .

1:150

Sflt or Sedfru11nt Susp. Sever1t)'J Setl, Sovcr~ty

I on-c:Iensc Sever ty

1300

Identity

7203A

1315

I ; tt .

Sl ud&r;> Scver1ty

Flow, tiGD

!50051

Floatinc ~·brh Severity

ll'l.~o:at1c Vr:ectatiot-Suppcrt Hcdiu~ s~verlty

'- s"' .. e;L a . < • f. ; hi

I P.O. Box 1149 • 715 Cabarrus Ave. W.

Concord, North Carolma 28025

Area Code 704 I 786-8121

Cabarrus County Health Department ·.

ALBERT J. KLIMAS li.S.P H., Dtrector

Mr. Bill Meyer Department of Human Resources Division of Health Services Solid and Hazardous Waste Section Box 2091 Ralei g h~ N.C. 27602

Dear Mr. Meyer:

•

July 15~ 1981 '

I have worked with Rick Doby from your office in the past concerning potentially hazardous waste materials that may have been buried on the former site of S & S Metal Recyclers on Shortcut Road~ Cabarrus County. Several weeks ago Rick and I collected samples of material from several drums left on the property and from a sludge-like material that was oozing out of the ground. We have not received any results of the sample analyses.

From the appearance of the property and discussions with neighbors~ I feel that the situation is a potentially hazardous one that should be investigated in more detail very soon. The underlying rock in the area is a fractured slate material that could allow extensive groundwater contamination if hazardous materials were buried illegally.

I realize that your office is very busy~ but I think the potential problems at this site require some immediate action to rule out the existence of buried hazardous wastes.

Thank you for your help in this matter.

Sincerely~

William M. Arche r Environmental Health Supervisor

lw

An Equal Opportunity Employer

. orth Ca ro 1 i na Department of H. n Resources Div ision of Health Services

Occupat i onal Health Laboratory

ANALYSIS REPORT

Company : _ ____;;.::?=:;.,....+~2~A_t:e.~~-~--=-------------------Address : ---=10~~.:;.._,:.~~--:.:0!/=..::' ::...:.....-.£_/ _,Jt/_,~C~"---------servi ce Requested: ~~~~~

Samp l e Taken On: .£,/~ ,/?? ! .

·Submit ted To Laboratory On: 5 h/<f fa. . .tn · By: -------------------------Date of Ana 1 ys 1 s: -.....:.4;,LL.....:7.,L

7/_B;:__/ _-----"5:::...,

1,L.../ ...:.../ .:...;.L-A ..::.'P.Lt ____ _ Date Reported : :Jj;z j £1./

- -?,'---;;'---------

Ana l yzed By: /1/£/J.L , p /:IN :;;

~ABORATORY SAMPLE NUMBER NUMBER

02271 I

L2972 ~ \~ f'..~ 2--

DESCRIPTION

tflu.J. oL-<.- Jt?fr~...;! ,P.er.r.. / - C.4

/./u . . .J.~ IV

;; y h-e a//dtq b nnn73 \.>'.,-;;.,~ 3

~ ~ ~

CuMMENTS:

DHS Fo rm 144 0 (Rev . 2-75 ) Oc cupationa l Hea lth

J "/ I J/ • // .J_... _ _,

... "'~ .... '1'&.- ~

REMARKS RESULTS IN

icA/M.U'~ £¥.>'"~ ~--, -~· . . ""'" #1../:t.. t7 ~ ~ A. J1 fig_, :;T;;p

/nt~J,-.-w ~r~«;~~ ~~~ '/l'llf.t:: ~

r-,..-../ ,rv-...e~vz) '6

rf~~rev; ""'"~b~ - c.

P.r.b~~

..... .;7Uf,...-e;.

A, 7a~rJ,. v

• •

Source:

:.cdress:

County:

?.eport To:

1~ddress:

STATE. LABORATORY OF PUBLIC HEAl.TU

•

DIVISION OF IIEII.LTH SERVICE. • DEPARTi1ENT OF UUNAN RESOUH

P.O. BOX 280l•7- 306 N. t·!ILHD~GTON ST., RALEIGH 2.{611

CHE~1ICAL ANALYSES - SOLID AHD HAZARDOUS t-U\STE

Remarks· ~ .

.J!J V/4~ :/1./c_ c:tf { ~:fs)[LJy-;

- Zip .

'f2 n W ~- h . ·'d1~ ~<-(4........___ 1-

/ {.ej .i j ~t·-/-ed. sb'-f lc) e. vt..

• -

... ' l'"'-

Zip + lc L.- \M.\J ~f:le..... f u v ""''t:::,C. -L I J ;j eJ rBf:/

Telephone Number: ( ) \1f if1- i-f-•AJ 0 ::J y ~""'-~/ y7-ed -·~·aL .

Collected By:

~e AN .

Date Collected: 5/~ /q ( PM -Location of Sampling Point:

.... -

. .::f" Extractable Hetals Results expressed in ppm unless otherwise ) Total Hetals Results indicated.

~esults

Arsenic Solids, dissolved v·Barium <7 Solids·, suspended

-.-- Cadmium -() Q Solids, total Chloride Solids, total volatile -- Chromium . -l!J() Spec. Conductivity Color z~nc

Copper F.ndrin Flammability Lindane. Fluoride :Hethoxvchlor Iron Toxaphene

........-Lead Ill 2,.4-D l1aneanese 2,4,5-TP l!ercury Nitrate --. t>H Selenium Silver

:~.te Received ?- /li.. }' f--'( Date Reported 8 Iv \t. e,.. $ { Reported By _____ _

Laboratory tlu:=tber ! '8238 --------------------------~--~--~

.

STATE. LABORt~TORY OP PUBLIC Hc;At.TH

·' •

DIVISION OF liEJI.LTH SF.RVIC. . • DEPAHTi1ENT OF IIUNI\N RESOUF .

BOX 280lt7 - 306 N. \-!II.NINGTOi'! ST. • RALEIGH 2J611 P.O.

CHE~liCAL ANALYSES - SOLID AND HAZARDOUS t·!ASTE;

Source: +S MJ~c4 Remarks:

;.ddress: }/o/J ~H fi/'c· 4- ~ h~ ~y~il-Zip ~ -

County: QOVJ~IA. . •

?.eport To: ;;!?~~~~ ... /

j',ddress:

-Zip

Telephone Number: ( ) -·;{;ck ~t:L, .

Collected By: I AN -

Date Coliected; 5/{/ Y'l Time PM -Location or Sampling Point:

:f5 Extractable Metals Results expressed in ppm unless otheJ:wise ) Total Hetals Results indicated. Results

Arsenic Solids, dissolved v·Barium ~7 Solids, suspended

·...--cadmium fJ.LJ Solids, total Chloride Solids, total volatile - Chromium r~ Spec. Conductivity Color Zl.nc . Copper F.ndrin Flammability Lindane Fluoride Methoxvchlor Iron Toxaphene

-Lead I ::J 2.4-D Mam!anese 2,4,5-TP Uercury Nitrate pH Selenium .. Silver

~te Received ? ;t{'k~l ~{ · Date Reported 8 ,yut,_e_ f:{ Repor~ed By ____ _

Laboratory Nuober f-'8'239 -------------------------------------------------

, 1 / .l~f4 NoJfJ Carolina Oepor~f.ent of Natural • ~m~~S~:.~~~v~9ommun~ty ~~~?~~~.7.!~~

Dr. Gerald Houghton Route 2, Box 238-A Gold Hill, North Carolina 28071

Dear Dr. Houghton:

DIVIS ION OF ENVIRONHENTAL MANAGEMENT

r~arch 13' 1980

Attached is a copy of the chemical analyses made on the water samples we collected from your well. The first sample \•tas collected on January 22, 1980 and a partial analysis was made. On February 4, 1980, staff members of the Mooresville Regional Office collected a second sample utilizing the proper collection containers for the various constituents.

The analyses indicate that your water is normal ground:Jater for that hydrogeologic area. The only constituent that exceeded a recommended limit was manganese. The recommended limit for manganese, based on aesthetic quality (fixture staining) is 0.05 mg/1 (milligrams/liter) or 50 ug/1 (_micrograms/liter).

The attached list contains a summary of the National Primary and Secondary Drinking }Jater Standards as required by the Safe Drinking ~Jater Act. These standards apply to public water systems only. They do ·not apply to private \'tater systems, however, they can be used to judge the quality of water being obtained from a \'tell serving a single family residence. ·

Comparison of the quality of your water with the standards shows that you will probably have manganese staining problems and some hardness pr·oblems.

Our analysis found no evidence of any hazardous or toxic, inorganic or organic compounds in your well water.

In addition to sampling your well \'later we are sampling and monitoring the surface water runoff onto your property and the stream \'later quality at various locations in the immediate area. Our sampling is not yet complete and we cannot make a statement about possible stream pollution resulting from activities at S and S Metals. When our sampling is completed we \'till send you copies of the analyses and our interpretations of the sources of any contaminants found.

Mooresville Regional Office 1119 North MJ.in Stree:, ~.loor~sville, N.C. 28115 Telephone 704/664-4627

An Equal Oprortunity A fhr-n.;cive Ac;ior. Employer

.·

.. !"

; Dr. Gerald Houghton. Page Two r~arch 13' 1980 •

If this Office can be of any further assistance, please contact us.

MRG:sj u

Attachments

cc: Mr. L. P. Benton, Jr. Mr. William Ross Mr. 0. W. Strickland Cabarrus Count~y-Heal th Mr. George Moei , EPA Mr. Joe Young, EPA Mr. Rick ll:>by ~ Mr. Don Smith Mr. Vance Holt

Department

Sincerely,

~/-d_ Michael R. Groves Hydrol_ogist

For: Richard R. Peace, Jr. Regional Supervisor

.,_

-: .

•.... ,~

.. •····:::· . ..

Hay_21, 1980 .

." · .S & S Hetal Recyclers . P. 0 •. Box .l.57 .o..

Co., Inc •

Shortcut Road ·' G'?ld Hill;: NC 28071 ..

.. ..

· :·Attn:.· Mr. Donald :R.. smith·

:·Dear Mr. Smith:

· ·We are unable. to determine the final destination of the 55-gallon. drums of solvents that was. stored on your property ·on Sho:.:.tcut Road, Cabarrus County. l-le also .do not have records of a privatt~ hauler by the nan:.e of Joh:l Crutchfield which you supplied· to the office of Natural Resources and Comcunity Development.

. .

. ·The delivery receipt -dated April 19, 1980, to John Crutchfield indicates no address or telep:tmne nunber for this individcal.. . Please submit to this. office verification of ~tt.· Crutchfield's telephone and address by June 1, 1980.

Your cooperation in furnishing this office-with the n~eded infomat~on will be appreciated. Tha~ you •.

CRD:ns cc: l-Ir. Everett Calloway ·

:Hr.· 0. W. Strickland l!r. Julian H. Fescue, III Hr. Mike Groves

Siilcerely,

C. Richard Doby, Sr. District Sanitarian for Solid . . and Hazardous "Taste 1 'anage:Jent 169-B Rosehaven Court Concord, NC 23025 ·

• • A.ffadavit concerning S&S Metal Recyclers, Short Cut Road, Cabarrus County, ~orth Carolina

1. In la~e February or early March of 19b0 G questioned Mr. Feace of the Mooresville office of the Division of Environmental Manage:nent about some metal drll.!Ils mentioned in articles in the Salisbury Post (January 24) and the Charlotte Observer (January 26). Mr. Peace said there were about 200 drums (first noticed by Mooresville agents January 21, 1980), that S&S officials said the drums contained an oil emulsion like that in the holdin~ lagoons, and that s&S had been ordered to remove the drums from its property as it bad no permit for handling materials in drums, and that the drums were under constant surveillance by his office. 2. On Friday, April 11, M saw a flatbed loaded with metal drums drive into S&S about 6:15p.m. The gates, normally locked at that tiQe, were standing open; the truck drove toward the back of the property and out of sight. The drums were rusty-red in color. G reported the incident to the Mooresville

... office on Ji.or:day. He was later told by flr. Peace that agents went to S&S later in the week but saw no such drums. 3. On Saturday, April 19, bulldozers began worKing about ' 10:30 p.m. somewhere to the rear of the S&S property. All the outdoor lights at S&S normally turned on every.night were off; the property was totally dark. The bulldozers continued worKing all night. Early Sunday morning G went around to the rear of the property to see what was hapoeninf,. As soon as G reached a vantage point, the equipment was shut down. There was no activity of any kind all day Sunday; about 9 p.m. all outdoor lights were extinguished and the bulldozers started working again and continued until about 5 a.m. f/ionda;v. G called Mr. Peace to see if he knew why they were workine in such a secretive manner. Mr. Peace later said that S&S had filled in a large excavation that had been intended to be a fourth oil lagoon; the work had been done at ni~bt to avoid

interfering with normal work of employees and would provide

·.

• -2- • them with a parking area. However, no employees ever parked there; the area was covered almost immediately with piles of scrap metal. 4. On Friday morning, April 25, Y~. Peace told G we would no

lonfer need to worry about those drUDs, that S&S notified agents who went tbere on Thursday, April 24, that the drums had been taken to Winston Container in Charlotte to be_ incinerated. G called Winston Container that afternoon end was informed they could incinerate only emot:v drucs. G notified Mr. Peace of that fact and also reported it to rlr. Doby of Solid 7Jaste 1vi3.naEement. 71e were later told by Mr. Do by that iVins ton Container had never received any drums from S&S; subsequently the company was requested by a lftter from the state to provide evidence of the whereabouts of the drums and they apparently sent to the Mooresville office a receipt for 126 drums of i•solvents", signed by a man whom agents have been unable to locate. s&S officials deny any knowledge·of him, saying (according to Mr. Doby) that be showed up on a Saturday morning, driving a flat-bed trailer truck, offered to take the drums off their bands and drove away with them (the drums). 5. Thursday, October 30, the Salisbury Post published an

-article which included the following: "They (area residents) also complained of the danger of barrels which were hauled in. The state has said it didn't know what was in barrels but they are now gone. Peace said he doesn't know what happened to them. Donald R. Smith said they were disposed of at SCA services in South Carolina but no record of tbeo was found. 'They have not showed up anywhere else.' Peace said." ~bout 6:30 that evening a man called our home, introducing n~mself as a former employee of S&S, and told M that he is convinced the drums had been buried on s&S property. According to his account, he worked at night on the furnace crew. One ni~ht about 6 months ago, when be and the others on the- crew reported for work, they were told to return home - some repair work was

to be done on the furnace. Several pieces of heavy equipment,

• -3- • including bulldozers, were near the furnace. When he

returned to work the following niFht, the earth-moving equip

cent had moved and there was a large expanse of newly-leveled

ground behind and to the right of the furnace. The drums were

also gone. He is uncertain of the dete or day of the week.)

~· In another conversation on Sunday, Nove~ber 2, the same ~an added that he bad also cut the tops off drums and other

employees were seen pouring the contents (whi~h he described

as solvents, lacquer thinners and that kind of stuff) onto the

ground behind and to the left of the office trailer. He said

that later the soil on w~icb the material was poured was pushed in the direction of the arrows shown in Figure 1. Be

also said tbat another employee told him of a drum blowing up

while being cut open. He estimated that about 150 drums were

e~ptied onto the ground at point B in Figure 1, where they had

earlier been moved from point A. He did not know what was done

with the e~ptied drums.~He believes about 200 drums were

buried in the ground to tbe rig~t of the furnace as shown in

Figure 1; he further stated that edges and rims of drums were

visible in the Eround under the brush and loose dirt near where the bulldozers were standing. Next day a new dry pond

_had been du~ on the other side of tbe adjacent roadway.)

(7· Thursday, October 30, we also recelved a call from a neighbor about a former employee who had information about the

burial of drums; G went to talk witb him about 9:00 that night

and again aoout 7:00 Sunday evening, November 2. According to his account, he saw a large hole (about tbe size of his living

room) being dug by earth-moving equinment and asked some other

employees what it was for.~hey told him that they thought it

was for burying some drums. He left soon after that; the fol

lowing day the hole had been filled in and the ground levelled.

Ee described the hole as beinE to the right and back of the

furnace, across a s~all road leading around the furnace to the

rear of the property (see Figure 2). He is uncertain of the

date, but thinks it was about 6 months ago. He also said that

. ~

• -4- • while he worked there, in the winter and early soring, drums were bein~ brought in from time to time. Fart of the job of soEe employees was apparently to mechanicall~ cut ~he tops off the drums; one employee told him that some of the drQ~S contained

a yellow material.) . (s. Another ex-employee, at the time the first articles about

S&S appeared in the Salisbury Post last winter, called the newspaper reporter and told him that while worki~g there, the enployee had once been sent to collect some metal drums from a chemical company in Charlotte, and also remembered seeing drums labelled "Caustic Sludge" on S&S proper~y. We informed the Mooresville office about this.) 9. On Tuesday, Nove~ber 1&, a phone call from a neighbor led G to visit a former S&S employee who provided the phone number, but not the na~e, of another former S&S e~ployee who might talk to us a bout the drums. 0!1 Friday, 1~ove=nbe r 21, G talked by phone to this employee, who also believed stronflY that drums were buried on ~....:.8 property. .Although this employee bad not seen them buried, he named the person whom be believed had buried them and specified that i~ was doue over a Sunday night; the ~urial location ~~~ ~ dry lagoon nearest the furnace

·towards the back of the· S~S pronerty. He estimated about 75 drums were involved. He also stated that he had learned that the contents of drums were being dumped on the ground inside the S&S property as early as October 192~; on one occasion the coLtawinated dirt was put in trucks and hauled to a land fill. He said that another, S&S employee had told him that two other other sites were bein~ used by S&S in Winston-Salem. The employee agreed to meet G on Saturday, November 22, to provide more details, but did not appear; when G called him at 6:30p.m. Sunday, Nove~ber 23, the employee put down the phone when he

heard G's voice. 10. All these former employees are reluctant to have, or refuse to have, their.names revealed for fear of reprisals.

One said he knew that another employee had been threatened for

.. • -5- • talking about S&S. We cannot be surprised at such concern; G was once told by an S&S employee that if he (G) kept coming out on the road (Short Cut Road) at night, someone would "shoot the bell" out of hi!!!. 11. Mr. Feace told a Salisbury Post reporter in January and again in October that the state does not know what was in the drums. Eowever, in a letter to M dated April 25, 1980, be said, "Staff of the L'iooresville Regional .•. ·have seen the m~terial contained in the drums." 12. Through most of September and October and part of llovember, bulldozers were working ~n S&S property, presumably to fill in the oil lagoons; again the work has been continued on weekends and sometimes after dar~. On Sunday, November 9, for instance, the sound of a bulldozer could be heard from about 9 a.m. until about 9 p.m. 13. The information in the foregoing affidavit has been provided at the request of Mr. Rick Doby of the Solid Waste Management Division of the State of North Carolina.

The undersigned, being first duly sworn, depose and say that the foregoing information is true and accurate to the best of their knowledge, with the exception of that information given to them by other people·, in which case the information is set down as they understood it.

This 24th day of November, 1980

-~.&~a~~c;;;o (M) Mildred Sherz Jiou~

~H~ Subscribed and sworn to before me this 24th day of November, 1980.

Cduu~ ~-~;-£ Notary Fublic ('!_

t.~:v com:n)ssion expires: r lcf, 11J>I

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P. 0. Box 157-Shortcut Rd. Phone (704) 279-7254

GOLD HILL, NORTH CAROLINA 28071

MIL. Rlc.ha.ILd R. Pe.a.c.e., JIL. · Reglond! Supe.IZ.v~&oiZ. NC Vepa.IZ.tmenz on Na.ZuJta.l Re~OUIZ.Ce~ And Communlzy Veve.lopmenz 1119 No~tzh Ma..tn SziLe.~ f.{ o o ILe~ vltte. N C 2. 811 5

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1 a.m l> ending you a. c..o PY' o ~ z!ie do cume.nz .tli.a..t we o bta.i:ne.d when the ba.ILJtel~ weJte·IZ.e.move.d 6~tom our.. piLem~&e~.

AL> 1 dl.oc.ul>~ed w~tft you a.nd your.. pe.ople,I ma.de ce.Jtta..tn tha.Z the tlquld wa.& go~ng xo be. dl~po~ed o6 piZ.ope.IZ.ly, Tn oJtde.Jt xo ma.ke. a.bL>olute.ly c.e.~tza.ln, MIL. Sok.otocv~k.C fla.d tfi..e ~ndl.v.idua.t who Jte.move.d xfte&e. oa.JtJte.!~ ~lgn a. L>.ta.temenz a.~·li:ultl.ng IL"e.~pon&l-bltlty. .

·We. hope .tha.Z we. h.a.ve not lnco•tven.:te.nc..ed you a.nd ~tegJte.t zW we ha.ndled .th.i.~ ma..te.Jt.C.a.t. Unde.Jt no c.iiLc..um.&:za.nce..& do we. .C.n.te.nd to fta.ndle. a.ny moiLe. ma..te.ILl.a.l o0 tru~ type..

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ORDER NO .

DELIVER TO

ADDRESS CUSTOMER ORDER ~NJ'· . L .

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P.O. Box 157~hath:ut nd. • Phone (704) .279·1254

GOl.b WLL, NOttTH CAROLINA 2oo71 . .' ·.··

TIME PA(~,~USED .4-a

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MAT,IAL LISTED ADOVE RECEIVED IN GOOD ORDER

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DID YOU 0 URCHJ\Sf. OTHERWISf Af:OU!'C~. OR MOVE INif.l THE Cour;Ty DUf\li~f, fHt: PRECEDII\;G CALEI\'[)t.R yr-p:~ r;::·,· PROPERTY INCLUDffliN 2 THROUGH S AROVP IF YES r.rr ;,el-f Ai·; ITEMIZED SCfiEfHJLE SHOI';Ir<G 1N_•· COST INSTALLED AND THE DATE OF ACOLJISITION AND STATir~c; 1"1'iETHER TI~E PROPERTY Wt.S PUPCHASEl> NEW OR USED . DID YOU HAVE RE1.10VALS OF PROf'ERTY DURING THE Pi-:ECEDI~<l; CALENDAH Yfi•R' _ .If YE~. r,TTf•C'I t,N lTC." !ZED SCHEDULE SHO\VIi\!G YEAR INSTALLED, YOUF\ COST.Ot,TL Of RU.10Vfd. ,\;:p Till ii!~f'()',I!Hlr,•

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IMI'OiiT AN'T -DO Ytlll Hl\\'1 PII'Hl.CI/\1111 I'Lll[;(JNAL l'!!('lf'[l!TY ON YOUH PHEMISLS /\ND 7NEI> tn· ~NU fHEH TJ\Xf'AYE:H?

NO ~ YES ,_;IF YES. ATTACH SCHEOULIC

SHOW: LESSOR. TYPE PROPERTY, RENTAL PAID

IMI'Oil T /\NT --

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VEHICULAR EQUIPMENT

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!·lr. Don R. Sr:rf th Plant il?..nager

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s .e~ s ''atal Recyclers, Inc. Post Office Bcx 157 f'-ol d Hi 11, H. C. 2J071

Dear !k. Smith:

• DI VISIO!: OF Ei-li!I RO.r ::::·!Ttl ~tn.::r~cE::E:JT

Hay 1 , 1930

This Office has been unable to confirm the pre~ent location of the ap!)roX1Mately 120 metal dru:-:15 that \·!~T":;! r:movert from your l')rory~rty on or a!:>out t·,;Jril 19, 198~. ~~e re':}uest ti!at yf'u SU:J~ly us ~:ith v!ritt~n docur•;:nta!:ion and verification as to \>!ho hrwl~t.! t:H~ drtF·~:; fror,i your :-,rJ:'c!"(" e'l·-i to •::here t;1~·: ('r:.r:s •·:cr'= tram:;"lort2·.·. ~·1-..::.s:: r·.=spo1-:l to tr1is ;~e>--::::::::t : .'' · ,,, ~~, 1?;:-.~.

If yn~! have c.ny 0u-.:-stio:1s f~out ti.is r,:qt::st~ ( .... ~"':~:.:·~: :""r:;:-:lf ('•r ~3'1:.

,;,~;·.ins at t::1:3 >oor~sviil·~: .:·.:!~ir.:-lc:l i~i':-:-fic::, t~1·~J:1.--),,,..; (/~ -~ .-.·.~-·~-:7.

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P. 0. Box 157-Shortcut Rd. • Phone (704) 279-7254

GOLD HILL, NORTH CAROLINA· 28071

Feb~ua~y 29, 1980

M~. C. R. Voby Vi~t~ict Sanita~ian Vivi~ion o6 Health Se~vice~ Conco~d, NC

Ve.a~ MIL. Voby;

ConceJtning in~pe.ction by yoult~e.l6 and Mit. A!tche.~ on 2/21/80, we a~e ta~ing app!top~iate action to dihpo~e o6 plahtic bagh and I would li~e to ~now what pe~mlth a~e needed to dl~po~e o6 ~olid wahte at yoult land6ill.

1 would alho li~e to than~ you no~ you~ help and conce~n ~ega~ding the ~ule~ and ~egulationh on holid wahte dihpohal. 1 ~eg~et that 1 Wah unable to meet with you on you~ ~ecent vi~it to ou~ plant.

1 am loo~lng fio~wa~d to a ~etu~n lette~ ah we have th~ee (3) t~uc~loadh o6 bagh that need to be ta~en ca~e o0.

Plea~e 6eel 6~ee to contact me at anytime to anhwe~ any quehtionh you may have.

Since~ely, / ( ( t- I / . ( ;, , . II , L /~

Von R. Smiih Vice P~ehident S & S Metal Recycle~h Co., Inc.

VRS/WW

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iiAL HAZARDOUS W-ASTE SIT

SITE I~SPECTIOH REPORT

GE~-l~RAL IHSTRUCTIOHS: Coo~lete Sections I and UI throuih XV oC this Conn as completely u ~~~the inform•· tla.a 011 thiS form to develop a Tertt•t'v" Dl•poaition (Sec lion 11). File this Corm ln ita entirety in the regional Haze:dous Waste Lo~ Fitc. D~ EUte to includn all ap('l'Orri .. te ::.upplemental Reports in the file. Submit • copy or the forma to: u.s. Environmental Protection A(lency; Site Tuckinlt Sratem; Hazardous Waste Enforcement Tack Force (EN·335); 401 M St., SYI; Washlncton, DC 2046').

z. TELEPHONE NU~BE"

e. z•;-cooE

z. TELEPHONE NUMBER

- --.C. STATE

0 I, FEDERAL 0 z. STATE 0 3. COUNTY D 4. MUNICIPAL C;2rs. PRIVATE

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EPA F "'"' T:7070-3 11 0·79) PAGE 1 OF 10 Continue On Rt"vere"

. . .. ~ - ••• Contlnu~d From Front . . ' . ~ ~ IQ. IHSPECTIOH INFORMA 'ont'nu•t; 1

I D, OI!:NI!:AATOI'IIN,.ORMA I (eourcn ~w .. re)

I• 'lo NAMC Z TCLILP' o ")r. £ NO, 3. AOOAES:I I4.WASTE TYPE CENE:'lAT£0

S:J..{;~ Sre.'-'' .... J tc. (_,), "'!;, ~.... ~ f-e-...,_ I ;V C. v· ::,r ~i'r ( .. . ~ LA 'b '·~" ;--<;.I '::, ,./,l(:qT c le ct..-11 o(' v-<.

' .$ c:: r" a p /) h· ,u ,1 <..' .n,

i E. TRMISPORTER/HAULER INFORMATION

I NAMC 2 TULII:PHONC NO, ll. AOORES!I I•. wAsTE TYPE: TRANSPORTEe

. F, IF WASTE IS PROCESSED ON SITE Al40 ALSO SHIPPED TO OTHER SITES, IDENTIFY OFF·SITE FACILITIES USED FOR DISPOSAL

I, t~AMII: z. Tl!:l..ll:PHOtiE NO, 31 AOORESS .

I Go ~:.,:ify; i~~~~TION H TIME OF INSPECTIO~ I, ACCESS GAINEOBY:(0Cietitlata musl b,. shown In ell ceaea)

<6: 3D et.-w- ":gJ -v 1. PERMISSION ·o 2. WARRANT •

IJ, l'IEATI'iE,R .,

Fc:...,...-,wc,,-W\.. ' IV. ~A.MPLIHG IHFORMATIOH

, Mark 'X' Co1· tha types oC aamples t11ken and Indicate where they have been sent e.g., regional lab, other EPA lab, contractor, etc. and estimate v.•hen the results will be available.

z,SAMPI..£ •• OATE

t,IAMPI..E TYPI[ TAKEN '3.SAMPLE SENT TO: i RESULTS (marlr'X') AVAILABLE .

a, QROUNDWATKR WellS ~ ~~;;_;_:, L·"~:t6Y"'( c':;~ :t.f;cttt!L(+i c AJ«c D ..L

~-Kk1~d~~i:~:'s b, SUA,.ACE WATER X II If I;

e, WAITE 0 '.1 /Ylp,{~o, )< IC. 1~f:D~ by fL7"'~ .s r;-cr~r'*i{8?!'/{~f,L lA-t. ~J. u:i ~J ~1'1 ~~~- ~~v~I~ v

d, Aln

e. I'IUNOI" ..

f. SPILL

C• lOlL

h, VII:GRTATION

& OTHCA(•:---·~y)

iB• ,.II!:LO Ml!:t.SUREMENTS TAKEN f••f•• redloecrlvlly, •Jf'Pio•l"lly, PH, etc.)

I T~P_I: 2. LOCATION 0,.. <EASUR EMENTS :J, RESULTS

. .

:

fPA For.., T2070-3 110·791 -

.. ... ... • • • • Cont,IUl"d Prom Ps~., 2

z. PHOTOS IN CUSTOOY OF:

Db. AE .. IAL

0 YES. SPECIFY LOCATION OF MAPS:

• COORDINATES

t. LA TIT UO IE (d"f••mln,•aec:,) z. I..ONGITUOE (dejj.·min,·sec.)

A. SITE s ~I, ACTIVE (Those lnduc:trlat or ~nicopa/ :Sttea which ere be/njl ua"d lot w••t•. treatment, arora,e, or dispo•al on • conrrnuinl ba1ls, even lllnlr•• quenr/y,)

0 2. INACTIVE (Those altea which no lonf2er receive w••t•••).

0 3. 0 THE R (specify)'--..----:-.,-=-=..,...:---:-:--:--::---,.-:-:--(Those aile" that include suc:h me~dents like "midn:j!ht dumpinQ" where no rej!u/tJr or continulnj! use of the .file for M"ltste dispo•al he" occurred,).

TE7 B. IS GE

0 I. NO 0 2. YES("pecify jlenerlltor'" four-dig/o SIC Code)'-----------

C. AREA OF SITE (In acr .. ) D. ARE THERE BUILDINGS ON THE SITE? b ( lVl ~ )'V\ 0 I 'E. D 1. NO LC>J 2. YES(apec:lly):

E. SUPPLEMENTAL RE S: ~f th" •it" falle within any of the co'egorle• listed below, which Supplemental Report• you have filled out and attached to tlu• for ••

~I, STORAGE

0 CHEM/810/ 6. PHYS REATI·fENT

A. WASTE TYPE

~I. LIQUID

D 2. INCINERATION

D 7. LANDFARM

(8J 2. SOLID

0 "f:::7f SURF ACE 3• LANDFILL J,L:)< 4• IMPOUNDMENT

0 8. OPEN DUMP D 9. TRANSPORTER

D 3. SLUDGE D 4. GAS

0 5. DEEP WELL

~ 10. RECYCLOR/RECLAIMER

D 2. IGNITABLE

D I. REACTIVE

0 3. RADIOACTIVE r:g: 4. HIGHLY VOLATILE

0 7, INERT ~ 8. FLAMMABLt::

fl\ '\C~ •( w • f"'- I-Ll cd-e v- •

PAGE 3 OF 10

c; Fr~m Fron; .... WASTE RELATED INFORM~ • ,.. . ···•

:z. Elltlmete_!_'!~_lll~ll_t~P~_c:_it~ un!! ~-:_~u~ or wast~ by cat~ ~ory; mark 'X' to _!rl_dicat~wh_j£h wnt~s ar~ pr~sent. ' e, SLUDCE b. OIL _I c. SOLVENTS d, CHEMICALS e. SOLIDS f. OTHER

AMOUNT ; AMOUNT I b )I !)cJ"() AMO~~T • AMOUNT AMOUNT AMOUNT

ol-~ 1 -<: ,,--1 IS 0 d. f"v' Hl S --v

UNIT o,.- MEAIU"I:

~ PAINT, ,-- U ~IQMI!:NTI

UNIT OF MEASURE

I PICKLING z LIQUORS

31 CAUSTICS

•1 PESTICIDES

UNIT OF MEASURE

" -Ill FL.YASH

121 ASBESTOS

Ill MILLING/MINE TAILINGS

I FERROUS $MELT 41

lNG WASTES

UNIT OF MEASURE

~Ill L.A I'IORA TORY. PHARMACEUT.

121 HOSPITAL

131 RADIOACTIVE

LIST S~DSTANCES OF GREATEST (..0NCERN WHICH ARE ON THE SITE (place In duc~nding orr!~t of hazard)

2. FORM 3 ,~~-~~~.~:.y (mark 'X') ''"~'" ~ ~

t. SUBSTANCE ... so· b. ,c .vA· •· b. c. d LID L IQ, IR HIGH MED, LOW . NONE

4. CAS NUMBER S. AMOUNT

y IX

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Vlll. liAZARD_DESCRIPTIOH

FIELD EVALUATION HAZARD DESCRIPTION: Plac~ an 'X' in th~ box to indicate that th~ list~d hazard ~xists. D~scub~ th~

hazard in th~ space provided.

EPA F.,,. T 0 ~

'1-lj 1'-cc:f fv : fJ ro •"" c(,,; a (<e r p r s S11{ f'j tJ 0 s '(" C ''I' I i y 4_ f'(j) L l-1\ tf p.J .t ~

0 C. WORKER ltlJURY/t:XPOSliRE

3 ,,

1

Ci. CONTAMINATION OP' SURFACE WATER

~--e- V' -e.. h (.(_ v '(__ b -o -e. h.

. ('e s t..J {i--.e cR· 1 'h 6 6th -e.- 6

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-1-wD~~~p~IJ:~ ~ ci r-''fh c <e. ~Ja h,r

I!PA Pora T2070·l (10·79) PAGE 5 OF 10 Conrmue On verse

.. ··~

:. FISH KILL

\ . ' K. NOTICEABLE OOOAS

0; l

L. CONTAMINATION OF SOIL • rl • . I

["--v\: ' I ~ f I • '3 , A f .so

M. PROPERTY OAMAC;E

EPA Fcwm T2070•J (1 0·79) PAGE 6 OF 10 Continue On Plf/le 7

'.

N, FIR£ OR EXPLOSION

P. SEWER, STORM DRAIN PROBLEMS

\ [J Q, EROSION PROBLEMS

R. INADEQUATE SECURITY

J { CJ .(' e /;L c t ·:-, J ... t- t9 "' ., c.( s ·, I 'e.. •

S. INCOMPATIBLE WASTES

EPA Form T2070•J (1 0.79) PAGE 7 OF 10

• T, MIDNIGHT DUMPING

0 U. OT.HER (epeclty):

A. LOCATION OF POPULATION

I.IN RESIDENTIAL AREAS

PUIU .. IC Ul~ AREAl 4 ' (perlre, echoole, ere,)

0 I. NON•CONMUNITY • < 15 CONNECTIONs-

o J. SUR,.ACI!: WAT!:R

I! PA , Of Ill T207().3 (I 0·79)

•

B. APPROX. NO. OF PEOPLE AFFECTED

• •

APPROl(. NO. OF PEOPLE AFFECTEO WITHitl

UNIT AREA

PAGE 8 OF \0

\

. •· ,

D. APPROX. NO. OF BUILOINGS

AFFECTED

...

E. QISTANCE TO SITE

(specify units)

\..Y

onrrnue On Pa~t' 9

.. .

• • •

I,)'Y>'\.-e..l et

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COM ... UN• ITY

(marl< 'JC')

-e. 'i fs o · h"- ve.. ~----------~-----------+~~~--~----~------------------~----·----. ·---·-1-------+-------~

0 C. 100 YEAR ~·l '~·::lr· '~ '' i.-~~ O. WETLAND

·.vu:; ;,~-,. r.,::e: .I,QUIFER

·a "= n/ .tee,)

0 E, LOW (.1 to .001 t:m/ .. t:o) 0 F, VEFI'(! (Ji/ o 0·.1 !o .00001 emiue,)

~~~~~~.-----------~~------------------------~~-------···· 3. COMMENTS:

3. COMMENTS:

J, JPECII"Y OIR£CTION 01" SLOPE, CONOITICiN OF SLOP£, ETC.

EPA 'orlft T2C70..3 (I 0..79) PAGE !il OF 10 ever.se

•

1!:, t!:XPIR,.TION O,.TI!:

(mo,,day,tt.yr.J

NOTE: Lased on the information in Sections III through XV, fill out the Tentative Disposition (Section//) information on the first page of this form. ·

E Form T2070.J (10•79) PAGE 10 OF 10

...

SURF POU TS SITE INSPECTION R (Supplemental Report)

?. FVIOENCE OF SITE 8 1 f'tC.)

OSAL OF IGNITABLE OR RE.AC"!"IVE WASTE

,

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EPA form T2070·3C (I 0·79)

bu l 11

IHSTRUCTIOH Answer and Explain os Necessary.

'( t.'""v • '(- We<

a.C(I9rti''j

r

Sv J'

STORAGE FACILI ES SITE INSPECTION REPORT cSur:•lt•mt'IIWI R··po.~rr 1

7. NOTE LABELING ON CONTAINERS

;J IYu._ v1. o-:P -c-cf -

0 YES

;Jo

9. DIRECT VENTING OF

DYES D NO

0. CONTAINERS HOLDING INC0!.1PATIBLt:: SUI:'STANCES (If "l'es", document evidence •. Deacrlbo wasteo .Take PHOTOGRAPHS.)

D 'VE5 ~NO

II. INCOMPATIBLE SUBSTANCESSTOR haurdoua weare, . Take PHOTOGRAPHS.)

D YES )8:1. NO

12. ADEQUATE CONTAINER WASHI~G AND REUSE PRACTICES

D YES D NO .;{,' / A

Y (ll "Yea .. ,. document evidence.

13. AD

DYES

SAL OF EMPTY STORAGE AINERS

EPA Form T2070·3D (10·79)

INSTRUCTION · Answer und Explain as Neccssnry.

at/on end Identity of hazardous

identity of

•..

"

• STATE BOARD OF H.TH SANITARY ENGINEERING DIVISION

RALEIGH, NORTH CAROLINA

REPORT OF INVESTIGATION OR INSPECTION OF 5 and 5 f1etal Recyclers Co., Inc.

Place visited .5 & 5 Metal Recyclers Co. ,Inc. . D feb. 21, 80 ---------------------------------------------------- ate ________________________ 19 ___ _

Address __ _r:.!· __ f:!;--~~=--!~.?_: __ _?_~~=-t:_-~~-~-_R-~_:_! ___ ~~}_~--~~~!_!.~~-~:- TI~e- spent -~--~--~::_·_:~-~--:- _ William Archer, Engineer, Cabarrus Co. Health Dept.,

By whom ____ ,C_. __ B_. __ Q_p_q_~-'--~!'-•_L _ _!)_!_~_!:.f..!E_t_,?_a_~ it a r ian , Division of He a 1 t h 5 e r vi c e s -------------------------------------------------Roy T. Sokol\1/ski, V.P.

Persons contacted ----------------~-(Q;;;;,-~~~-~~~-~~;;ie;~~the~)------------------------------------

R f . . Routine Inspection eason or VlSit --------~----------------------------------------------------------------------------

Copies to:

REPORT:

William Archer 0. W. Strickland Bill Meyer Ray T. Sokolo\1/ski

On february 21, 1980 Mr. William Archer, Engineer \1/ith the Cabarrus County Health Department and I inspected 5 and 5 Metal Recyclers Co., Inc., Gold Hill, ·North Carolina. We spoke \1/ith Mr. Ray Sokolo\1/ski, Vice President, and \1/alked over most of the property inspecting the aluminum seperaton and the 3 NRCD approved lagoo~s for \1/aste oils •. Mr. Sokolo\1/ski described the oils as mineral oil and \1/ater coolants \1/ith a very small amount of petroleum oil floating on top of t\1/o lagoons •

. Our inspection indicated no spills or leakage through the lagoon \1/alls. No promiscuous or unauthorized disposal of liquid \1/aste \lias seen. Approximately 150-55 gallon drums of oils and liquids \1/ere numbered by NRCD and \1/aiting for advice from NRCD for disposal at an approved facility.· ·

- . There utas a ·sig'n"ificant accumulation of solid \1/aste including \1/aste cans and plastic bags \1/hich \liaS requested to be taken to the Cabarrus County Landfill. A letter of intent from 5 & 5 Metals \lias requested by this off ice.

"Fora 434 SBH Fora 1489 Saoltarr En&lneerlD&

-~ -- ~--- ---

• ' STATE BOARD OF HEALT:H SANITARY ENGINEERING DIVISION

RALEIGH, NORTH CAROLINA

REPORT OF INVESTIGATION OR INSPECTION OF 5 and 5 Metal Recyclers Co-., Inc.

Place visited 5 & S Metal Recyclers Co. ,Inc. , . , D te feb. 21, 80 --------------------------------------------------- a ____ .:...:.:_.:..·---------------- 19 ___ _

Address _::__f:! __ q;--~~~-..:!~J..:~ _ _:>_~~!'_t:_E_u_~-~-~~j--~~~-~~~~~]-_·!.~-· =c-.: Tici~- ;pent .:..---~--~=~~:.-~----- _: William Archer, Engineer, Cabarrus Co. Health Dept., ,

By whom ____ _c_.__B_. __ Q_pJ:?.~-'--~!'-•_L.P_:!:.~_!:.!_~~-~-_?_a_~}_t ar ian, Divis ion of He/a·l t h Services ---------------------------~-------------------

Reason for visit

Copies to:

REPORT:

Roy T. Sokolwski, V.P.

Routine Inspection ----------------------------------------------------William Archer O. W. Strickland Bill Meyer Ray T. ~okolowski

On february 21, 1980 Mr. William Archer, Engineer with the Cabarrus County Health Department and I inspected S and S Metal Recyclers Co., Inc., Gold Hill, ·North Carolina. We spoke with Mr. Ray Sokolowski, Vice President, and walked over most of the property inspecting the aluminum· seperaton and the 3 NRCD approved lagoons for waste oils. Mr. Sokolowski described the oils as mineral oil and water coolants with a very small amount of petroleum oil floating on top of two lagoons.

Our inspection indicated no spills or leakage through the lagoon walls. No promiscuous or unauthorized disposal of liquid waste was seen. Approximately 150-55 gallon drums of oils and liquids were numbered by NRCD and waiting for advice from NRCD for disposal at an approved facility. ·

. There \1/as a ·sig'n"ifi.cant accumulation of solid waste including \1/aste cans and plastic bags which was requested to be-taken to the Cabarrus County Landfill. A letter of intent from S & 5 Metals was·requested by this off ice.

'For• 434 SBB For• 1489 Sanltarl EnclueerlDC

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'• • • Affadavit concerning S&S Metal Recyclers, Short Cut Road, Cabarrus County, North Carolina

1. In late February or early MHrch of l9b0 G questioned Mr. Peace of the Mooresville office of the Division of Environmental !Y.anage:nent about some metal drU.!Ds mentioned in articles in the Salisbury Post (January 24) and the Charlotte Observer

·(January 26). Mr. Feace said there were about 200 drums (first noticed by t~ooresville agents January 21, 1980), that S&S officials said the drums contained an oil emulsion like t~at in the holdinr- lagoons, and that S&S had been ordered to remove the drums from its property as it had no permit for handlinE materials in drums, and that the drums were under constant surveillance by his office. 2. On Friday, April 11, M saw a flatbed loaded with metal drums drive into S&S about 6:15p.m. The gates, normally locked at that til7le, were standing open; the' truck drove toward the back of the property and out of sight. The drums were rusty-red in color. G reported the incident to the Mooresville office on Mo~day. He was later told by Mr. Peace that agents went to S&S later in the week but saw no such drums. 3. On Saturday, April 19, bulldozers began working about ' 10:30 p.m. so~ewhere to the rear of the S&S property. All the outdoor lights at S&S normally turned on every.night were off; the property was totally dark. The bulldozers continued worKing all nisht. E?.rly Sunday morning G went around to the rear of the property to see what was hapoeninr,. As soon as G reached a vanta~e point, the equipment was shut down. There was no activity of any kind all day Sunday; about 9 p.m. all outdoor liEhts were extinguished and the bulldozers started working again and continued until about 5 a.m. Monda:v. G called Mr. Peace to see if he knew why they were workinr in such a secretive manner. Mr. Peace later said that S&S had filled in a large excavation that had been intended to be a fourth oil lagoon; the work had been done at ni~ht to avoid

interfering with normal work of employees and would provide

• • -2-

them with a parking area. However, no employees ever parked there; the area was covered almost im~ediately with piles of scrap metal. 4. On Friday morning, April 25, Mr. Peace told G we would no lonrer need to worry about those druns, that S&S notified agents who went there on Thursday, April 24, that the drums had been taken to Winston Container in Charlotte to be. incinerated. G called Winston Container that afternoon and was informed they could incinerate only empty druos. G notified Mr. Peace of that fact and also reported it to 1~r. Do by of Solid ·.vaste Msna[ement. ~e were later told by Mr. Doby that Winston Container had never received any drums from S&S; subsequently the company was requested by a lEtter from the state to provide evidence of the whereabouts of the drums and they apparently sent to the Uooresville office a receipt for 126 drums of "solvents", signed by a man whom agents have. been unable to locate. S&S officials deny any knowledge of him, saying (according to Mr. Dob;y) that he showed up on a Saturday morning, driving a flat-bed trailer truck, offered to take the drums off their hands and drove away with them (the drums). 5. Thursday, October· 30, the Salisbury Post published an article which included the following: "They (area residents) also complained of the danger of barrels which were hauled in. The state has said it didn't know what was in barrels but they are now ~one. Peace saij he doesn't know what happened to them. Donald R. Smith said they were disposed of at SCA services in South Carolina but no record of theD was found. 'They

. have not showed up anywhere else.• Feace said." ~bout 6:30 ~that evening a man called our home, introjucing n~~self as a

former employee of S&S, and told M that he is convinced tbe drums had been buried on S&S property. According to his account, he worked at ni~ht on the furnace crew. One ni~ht about 6 months ago, when be and the others on the crew reported for work, they were told to r~turn home - some repair work was

to be done on the furnace. Several pieces of heavy equipment,

•

• • -3-

includin~ bulldozers, were near the furnace. When he returned to work the following ni~ht, the earth-moving equipoent had moved and there was a larf,e expanse of newly-leveled ground behind a~d to the right of the furnace. The drums were also rene. l!e is uncertain of the date or day of the week.)

(6. In another conversation on Sunday, nove::~ber 2, the same man added that he had also cut the tops off drums and other employees were seen pouring the contents (which he described as solvents, lacquer thinners and that kind of stuff) onto the ground behind and to the left of the office trailer. He said that later the soil on w~ich the material was poured was pushed in the direction of the arrows shown in Figure 1. He also said that another employee told him of a drum blowing up while being cut open. He estimated that about 150 drums were e~ptied onto the ground at point B in Figure 1, where they had

earlier been moved from J..._oint A. He did not' know what was done with the e~ptied drums. He believes about 200 drums were buried in the ground to the rig~t of the furnace as shown in Fif.ure 1; he further stated that edges and rims of drums were visible in the rround under the brush and loose dirt near where the bulldozers were standing. Next day a new dry pond had been du~ on the other side of tte adjacent roadway.)

{7· Thursday, October 30, we also received a call from a neighbor about a former employee who had information about the burial of drums; G went to talk with him about 9:00 that night and again aoout 7:00 Sunday evening, November 2. According to his account, he saw a lar~e bole (about the size of his living room) beine dug by earth-moving equinment and asked some other employees what it was for.~hey told him that they thought it was 1'or burying some drums. He left soon after that; the following day the hole had been filled in and the ground levelled. He described the hole as beinE to the right and back of the

furnace, across a s~all road leadin~ around the furnace to the

rear of the property (see Figure 2). He is uncertain of the

date, but thinks it was about 6 months ago. He also said that

• -4- • while he wortt;ed· there, in the winter and early soring, drums were beinr brou£ht in from time to time. Fart of the job of some employees was apparently to mechanically cut the tops off the drums; one employee told him that some of the dr~~s contained

a yellow material. J (o. Another ex-employee, at the time the first articles about

S&S appeared in the Salisbury Post last winter, called the newspaper reporter and told him that while working there, the enployee had once been sent to collect some metal drums from a chemical company in Charlotte, and also remembered seeing drums labelled ''Caustic Sludge" on S&S property. We informed the Mooresville office abo~t this.) 9. On Tuesday, November lfr, a phone call from a neighbor led G to visit a forner S&S employee who provided the phone number1 but not the name, of another former S&S e.nployee who might talk to us about the drums. On Friday, November 21, G talked by phone to this employee, who also believed stronr,ly that drums were buried on ~j.S property. Although this employee had not seen tbeffi buried, he named the person whom he believed had buried them and specified that it was doue over a Sunday night; the burial location was the dry lagoon nearest the furnace . --·- - -; ~ -- -towards the back of the SuS property. He estimated about 75 drums were involved. He also stated that he had learned that the contents of drums were being dumped on the ground inside the S&S property as early as October 197~; on one occasion the

•.

contaminated dirt was put in trucks and hauled to a land fill. He said that ancther S&S emoloyee had told him that two other

other sites were beinr used by S&S in Winston-Salem. The employee agreed to meet G on Saturday, Nove~ber 22, to provide more details, but did not appear; when G called him at 6:30p.m. Sunday, Nove~ber 23, tbe em~loyee put down the phone when he

heard G's voice. 10. All these former employees are reluctant to have, or refuse to have, their names revealed for fear of reprisals.

One said he knew that anothfr employee had been threatened for

• -5- • talking. about S&S. We cannot be surprised at such concern; G was once told by an S&S employee that if he (G) kept coming out on the road (Short Cut Road) at night, someone would "shoot the bell" out of hi!!!. 11. Mr. Feace told a Salisbury Post reporter in January and again in October that the state does not know what was in the drums. ~owever, in a letter to M dated April 25, 1980, he said, "Staff of the I.:ooresville Regional .•• have seen the m8terial contained in the drums." 12. Through most of September and October and part of November, bulldozers were workinf on S&S property, presumably to fill in the· oil lafoons; again the work bas beeD continueJ on weekends and so~etimes after dar~. On Sunday, November 9, for instance, the sounj of a bulldozer could be heard from about 9 a.m. until about 9 p.m. 13. The information in the foregoing affidavit has been provided at the request of I~r. Rick Doby of the. Solid Waste Management Division of the State of North Carolina.

The undersigned, being first duly sworn, depose and say that the foregoing information is true and accu~ate to the best of their knowledge, with the exception of that information given to them by other people, in which case the information is set down as they understood it.

This 24th day of November, 1950

;;z riL ~ <G~z:gifti2-c Subscribed and sworn to before me this 24th day of November, 1980.

~~~-~;-£ Notary Fublic ~

r,~y commission expires: Ju1U..--lt'. 11J>I

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L"Jll\ No~ Carolina Oeparl~~nt of Natura!P=" W~f!lf Resources &Community Development

""~ James B. Hunt, Jr., Governor Howard N. Lee, Secretary

Mr. Joe Young Environmental Protection Agency Hazardous Waste Section · Disposal Site Unit 345 Courtland Street Atlanta, Georgia 30308

Dear Mr. Young:

DIVISION OF ENVIRONMENTAL MANAGEMENT February 20, 1980

Per our telephone conversation of this date, enclosed are the analyses of surface water at the S & S Metal Recycling Company in Cabarrus County, North Carol ina.

If you have any questions, please do not hesitate to contact me.

RRP :sju

Enclosure

cc: Mr. L. P. Benton, Jr., Chief Operations Section

Sincerely,

·? ··I "' .//;. ," /?. ;; ::';

(: •/d;·:;:-. !:'· ~ce; <rt ;· Richard R. Peace, Jr. Regional Supervisor

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Moores,ille Regional Office 1119 North Main Street, ~1:Joresvillc, N.C. 28115 Telephone 704/664-4527

An Equal Opportunity Affirm.;tiv~ Action Employer

• ••

MEMO. DATE:---------

~~ North Carolina Department of Natural ~r Resources &Community Development

,, . • fi __________ ~:-·~,~·--·-·~·~·~· ~·! __________ _

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,. ~IVER BASIN. _____ ~-'~·~------

BF.PORT TO: (Cfrclr Onr) -·· ')

MO, WSRO, ~~tO, FRO, WaRO, lURO, RRO, TS, BM

AM, OTHER ----------------

..i /.1' COLLECTOR ___ ,_"-~,.-}-~--'~·J( __ : ________________ __

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BOD RANCE------ SEED -----

CHLORINATED ___ A~)~..,~------

.. -· ··-----~---' ........... '--~-----·----· ----------------·-------

N. C, DEPT, OF NATURAL RESOURCES & COHMUNITY DEVELOP~IENT

DIVISION OF ENVIRONMENTAl. MANACE~I.F.NT

FIF.LD/LhB l-'ORM

Ocozu: 0 COMPLIANCE D SPLIT

LAB NUMilER 8 • ~Pn o o so DATE llECElVED_...;/...;-_2 __ .:;;5:;._· ....;;-(_~;:.;.) ___ _

RECEIVED BY. __ -q--:.:_·· ____ ·_;;..' ;...~ .:...· ;...;...;:;D:;.__

DATA ENTitY nv.___..,.,, C:.;...o....c~..(.;...l.,.._ CK r't(ytf 2 a

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DATF. REPORTED•---..!:;;;::::.-...:...~g..,;....;,t-'-1---

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STATION LOCATION·-.!.::~~-~1f!J4-...:;/-,::.-=.::~· __..Y~'¥:.:::;.:h~"7J::.. ::;::::;""4;,;,:::~~-=----:;,--yl-')-·\ __

R~.a-------------------------------------------------------------------Station No. Date Begin Tit•e Degin Date End T1rne End Depth DM DB D}m Value Type T, s, or B Sample Typ

C @ GNXX s·s l-< 1- .2 5- 'J.) --_;..--------~ • 1

2

3

4

5

6

7

8

9

1 0

1

1

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14

1

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tt 7 1

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BODe; ~1n \ \ con ........ ?n. Coliform, HF Fecal .. , .. , ..

Coliform, MF Total:l"'""

Coliform, Tube Fecal~tsl~

Coliform, Tube Total~,~ ... ~

Residue Total !lon In-q:: VC1latile sos

Fixed 510

Residue Susn~nded 530 Q Volntile 535

FixC'.d 540

lnH /....3 Acidity to uH 4.5

Aciditv to nil 8.3

Alkalinitv to oH 8,3

All<nlinit-v to nH 4,5

TOC eeo

£1.78 !100'36 StrenT. Flow St'VCr .ty

Cloud Cov{•r

c 1351 3:;>.

Odor-Atmos Deterf<'nt Suds . Severity Sever ty

01330 130!1 . DMI/REV, 9-78

Jfoo

rog/1 Chloride o.o&o

mf'./_1 Ar.,cnic 1002

/lOOrnl Chl a Tri 32210

/lOOml Chl a Corr 32211

/lOOml Pheophytin a 32218

/lOOml Color (True) M

I'IP.Il Chro~iurn Rexaval~~~2

mr>./1 levanide '720

111"/1 Flnuride 051

mr./1 Fonr.aldehvde 71880

mf'./1 Grease nnd Oils sse

.mf'./1 Hardness Total ooo

unitR ~mAs ~'"'60

mP../1 Ph<.>nols 32730

mBil Sulfate 045

mr./1 Sulfide 745

1'11'./1 !':pccific C:C'nd os

mr./1

I A II L

rnr,/1 Nih as N "'n '"" /1 Mn - Hl!nl'l!nt>R<' 1n~5 II

urdl ITY.II' "" }J "'25 . "'" /1 IMn - ~!n1vhr!,..,.,,M 1062 Ill

ug/l NO,+NO'I as N 4530 mP/1 Ntt - SC'dium !l29 n:g

uz,/1 POt. as P -.osn.,. tnPfl Ni - Nickel 1067 u

11<;1./1 p Total as P '""" mt:dl Pb - Lt>nd 1n51 U!~

units Ag -·silver 1077 ur./1· Sb - Antimony '"".., ur.

uJ>.Ll Al - Alt:mi num 1105 uP./1 Sn - Tin 1102 ug

m.PJ.J. IRn - ll:trium 100 .. .... ,, 111 - \':~nnrli""' 10A7 u

mtdl Be - Bcrvllium 1012 uro/1 Zn - Zinc 1092 u,.

mr./1 en - Calcium 016 rnro/1 Pesticide.>!! (Snccifv)

mv./1 Cd - Cadmium 1027 ur/1

rnf'./1 Co - Cobalt 1037 UJdl

tr:f'./1 Chrom:l.un• - Total 10'~4 U!!/1. Orr.anics (Sr>ec:l fv)

ur./1 Cu - Conner 1042 UP./1

mro/l Fe - Ircn 104S ue/1

fiiV./1 llr. - Mercurv 71ooo uv./1

tiMIJOS./cm Li - Lithium 1132 UJ!/1

Mg - Magnesium 1127 mr./1

ph 4.5 pll 4.5 .Acidity pH 8,3 Turbidity P.ach FTU

Turbiclity Severity

Flow, Inst. CFS

Oil-Grease Severity

13!10 1300

Silt or ·SedJment Identity Su8p, Sever:!ty Sed •. Severity

435

72034

131!1

76

IJydro Ehc. Dam Uis, CFS

Flow, l!GD

!100!11

Slud!;<.> Float:l.ny D(•brJs Severity Sever it

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RIVER BASIN. ____ _..:I;.....:-';..;'f~.;_· -------

REPORT TOj Cr.frcl~ On~)

ARO, WSRO,' Mno) mo, WnRO, WJI\0, HHO, TS, BM '··· -· -

AM, OTHER ----.,,..-------------l t'

COLLECTOR ___ ~-r~-··-~-~_ .. _L_.:_. __ '_.:_· .. _. ____ _

BOD RANCE------ SEED-----. .t)

CHLORINATED ---t..'':..J_)t.._ _____ _;_ __

Date Begin

Temp. co

""~ I o • ... ~ I 'YlJO

DIVISION m· lmVJIWNHiili'fAl. ~lhNAGl'Hl~~T

Jo'It-:J,Il/1.1\B l•'OIIM

Depth DM DB DMB

pH Units

lJATl~ R~CE1Vlm_.J-/_J~S.;-.$~ilt.bJ~-----ltlO:CEIVI::U UY _________ ..;I.,..·".:.t'.,..'-----------

llA'l'A ~:N'I'ItY uv 1 ' • . CK ______ (':;;...:-;..;·1,_'

DATr; REPORTEDI _ _;;·',.,_~ ......;·_· ,:_1_·__;;:.:;;:;).;__ ____ 0_

Value Type T, S, or B Sample Typt'

A H L c G GNXX

pH 8.3 Turbid'ity Ho1ch FTU u-plin& Point

1 PT %

A~3 fz I0~-------------~~------------~~4=o=o-----------~~---------~~~--------~~~----------~~--------------~~---------------43!1 7&

Secchi Disk M

B7e Stream Flow Severity

Cl:l!SI

• Odor-Atmos • Jicverity

DHl/REV. 9-78

1 Hr. Set. Solids

!10006

Cloud Cover

32

Detcrr.C'.nt Sucln Severity

130!5

Conductivity tmHOS

Precipitation Inches

Deitd Fish St'verity

1340

Salinity S/L

7030!5

3G

t.'ind Direction From North

Strea~e Color ,

R,P,

81&47

Wind Force Beaufort

Stream•Stagel Flow, Ft. CFS 6!!1 61

Inst.

Turbidity Severity

13!10 I Oil-Grease Severity

1300

Silt or Sediment · Susp. Severity Sed. Severity

Identity

Hydro Elec. Flow, ~!CD Da:n Dis. CFS

72.034 !100!5.1

Sludge Floating D"bris Severity Sever ty

131!!1 134~

A~uatic Vct:Ct.1tioy Suppcrt fcdium Sever ty

. . I .,

h2'Cl 1 !·l.•\ COUNTY · C'n:bC-\-'( X·'-1. ~ RlV.ER llASlN l {cd/?..j: ('..,

N 0:or'J'"1'. OF ~IATURAL IU·:SOURCES & CmiMUNUY lJnHI::NT ~-/ -J

~r;m.:n.ER~ll ___ lt..,;'!l.,.;..,_·:·_.lt... .. -?-' ___ _

I f-1: . ;:)/ /\ tll\'l'l~ REc~:xvm> ___ _.{_· ..;..;'~b.>;.:;. ~·-' .... @4;J--... /. __ _

REPORT TO i ( Ct rc 1 r:o One-)

ARO; WSRO,,e FRO, WaRO, WLRO~ llRO, TS, DM . . . ~ . '

Al-l, OTHJ.m ---------------I. . ,, .

~ . : . . ' I ~

COLLECTOR· · .• ·• . :' , ; • --~~~----~~~-------..

BOD RANGE -----.-- SEED -----· _ _.'

CHLORINATED ---'A~·:_.--::...;'t;...'> ______ _

i . .. J

Station No, Tit•a Begin

A.!P

Secchi Dft~k M

870

Stream Flow Sever! ty

c 13!11

Odor-Atr..os Severity

01330

D~ll/REV, 9-78

·;:-.. I / ....

Temp. C0

1 Hr. Set. :>ol:lcls

!IOOOG

Cloud Covl'r

32

Dctcrycnt Sucb Sever ty

1305

Prcci pit o t fen Inches

Dend Fish SI.'Verity

DIVlSlON OF llNVLIWNm:NT/11, MAN.\CI.':HEN'£

Date End

pH l'nitll

SnUnfty S/L

\o.'fnd nf rcc:tien !-'rem North

Strcatt Color

FII~Lil/LAU l•'OitM

Depth DH DB DNB

.J/

rtremn·Stai\C I ··c. 6!1

Turbic!ity Severity

'I R~:CElVJ>U UY: _____ _.__·.;../ _ _.;. ____ _

CK----""'""",.::..,., i)

DATE REl'Ol!TED•--L/_----t,5;.,~,C...:.)_· ·-_,8[:.1.'-/.::;..J) __ __.:.,:;I,

DATA r:N1'RY D'------

Value Type T, s, or .B A 11 L

Sample Type

C .·® GNXX

pll 8.3 Tcrbidity llach FTU

43!1 711

Fbnw, c s IuHto Hydro J:h•l'. Dun• Ul11. Cfs

now, t!Gil

Ill 72034 500~1

Oil-Grease Severity

Sl ud~;l Sever ty

Float.ln~ Dl·bds Sever it

13!10 1300 131!1

Silt of Sedfment Identity Susp. Sever ty Sed, Severity

Actcatic V~:eet.!tiut-Suppcrt Mcdiu~ Scv~rltY

., (• i I. . . ' .. COUNTY __ .._ ___ _..._ _____ ---

R1VER DASIN___.;'/;..;.;_J,:.&.).;.;!•....;.r.;;; • .J;.... ______ _

B&PORI TO: (Circle On~) .· . ARO, WSRO(MRo,: FRO, W.1RO, WiRO, RRO, .......

COLLECTOR ..;.,___;·_; ~-~-·· __ ,:..l_f.:,.' ._/ ,:,.Lw;..,b·~, ,.._ __ _

BOD RANGE------- SEED ------r~::;: . i.

CHLORINATED __ _,.f:..~f'.·.-0,;._ _____ _ Station 1\o, Data Begin

Disk M 1 Hr. Sot. Solids

878 !1000~

t(~~:. ( . I /. ':('( . , .•.... ·:·, .,

N CPEPT. OF NATURAL RESOURCES & COHMVNITY DOME~T DIVISION OF EliVII\ON!"'"TAl. MAIIACEI!ENT I.,~:{!

1/r. </., LM N~IDER~D------~-~-~~~---------1 .. I·"" <""·J·(.

DATE RECEIVED __ ....;..._;..I .. ~ _,')'-·-·-··~:-.; _...-::..'----

Rr:CEIVEil llY.r ____ ~/.-1....:...('_..---. ___ _ Fim.D/LAB FORM i~)l\

~,.7 OcoRE 0 COHl'LIANCE D SPLIT

DATA ENTRY B'z....---' ;...-' -- C;"'----•"' DATE RI-:PORTEDt _ __:./_·--__ 3e:L::..'.;..·--·.::.O[_~·)::;.....;.., __

,.. . .. D INTENS~VE s. ~EMERGENCY : ···s'rATION LOCATION , S·/ <. £2f<. • icl-s- ·

' REMA~s .So m 'PI<- c:, C• <; £!"\. ·.2pcrl ' n • • • . i

re_ '>J>c. ·s l" (r)m·p lc· 'cd: D3tc End T1rno End Dopch DM on mrn Value Type T, S, or D S:~mplc Type

A H L c t· CNXX

pH l'nits

Salinity S/L Stream·Stagel F!ow, Inst. rt. crs 61 70305

llydrc Elec. Flow, ~IGD D.1m l>is. CFS

:500:51

Stream Flow • Severity

Cloud Cover Precipitation Inchea

t.'f nd D:l rec: tion l'rom North Severity Severity

Turb:lr!Hy I ou-r.rcllSC

c 13:51

Odor-Atmos Severity

01330

Octcr~rnl .SuciR Severity

I:JO!I

DClld F!Rh Se-verity

13-40

1300 134:5

Str~nll'. Color Silt or Sediment ~- IdentJty Susp. Severity Sed. Severity A~cnt 1c Vt·&et..\t J ur

Sup pet t l.C'd.i uw Seve-r J t)'

COUN!Y ___ :sJ...J.~;..:.C;;.:.:-:n:..:....:.../ ~:>.j~i...----·--RIVER DASIN..__-f\f.fl),.!,j:f)I..U.\K..:..f'-f\14--------

l.'e LAD NmiDER~0~--~·~~·~·~·~~~:2~--~--------~--DATE ld':C~:l Vr-:1>_--..J/~:...'"..J.Q_• Llo.. ~_.1· ~;..'..:.&L.i :::;/):;.._ ___ _

ll!::CI::IVI::D llY.: _____ L)\1-C::i..'-------RET'OI\T 'l'O; fClr<'1e One>)

ARO, w~no,®~1<o, W.:JRO, tn1w, rm?.• '•

Station No. ,Date B.:gin .; :' ... . ... . . . . . . . ., .. · . '. Tit•e Begin . , · ".:.,;,,1 Date End

':i/o'~···'·~· ·-· :1r oc.J~ Depth DM DB DHB

r ...... g c.o/c:;J. il A

Value Type

It L

·r, s, or B

c Sample Type

G CNXX

Temp, co pll l'nita

~3·----~-----L~----------------~~~----------~~4~o~o-·----------~~----------~~----------~~----------~~------------~~~-------------SccchJ Hr. scr. Solids finnt\H'~tivity Snl:lnity S/L R.P, H~cmn·Star.el lJsw, Innt.

78 70305 6!1 lSI

Strl'am Flow Cover P::cciritotJ on t;ind IH rection Turbit!ity I 011-C:re<Jsc SeverJ ty Inche$ from l'lorth Severity Severity

13~5~1--------~~------------------~~-------------C3~G~----------~~-----------J~I3~5~0 1300 1315 134!1

Odor-Atmos Suri:; Dead Fish Strearr. Color Silt or Sediment Identity cyerity Sc;>verity Susp. Sever.it)' Sed, Severity Ac:tl!aiic Vt:ectat:lot'

Suppcrt Mcd.u~ Sevl'rlty

DMl/REV. 9-78

.; i r

1..1\B NUM!li!I(.::_B _ _.~~: c:;:. wJ±;· ~«.;..· __ · ______ ,., COIJNl'Y- ......-56~·[._,\~,.;~~~·/~--------. )

RIVL:k llAStN_ '{t[fJ!uy/ I G

RF.PQRT l'O: ':::::! <:f rrl <' On£)

t.RO, WSI:O,~ FRO, W:JIU1, I~JI:O, 1:1~0, TS, DH rar J.';och TypP)

. Qa'wATER 0 cotu;

J ·t~l~·J:!~~---l.~! IU·:ClllVI·:U DY·------,1.~~..,.;.-.L<-------

DATA ~:Nl'HY B.___._,·_· _._· -- CK.~~---· ...;' '7,.+

DATP. RF.PORl'ED• _ _,/'--_..;;~~?':..,_..,..._~::t..' -· •:....;)J;..,_ ___ L_',_/ A!1, OTUF:R -------·-------- · ·. TI sEntHF.NT D coMPLIANCE D srr.n COLLECTOR

BOD RA!:CE ------- Sf.ED ----

CHLORINATED

Station 1\o.

Sec chi

870

Strentn Flow Sever:l.ty

Cl3!51

bdor-Atmos - Severity

DHl/REV. 9-78

/ql! •. Date llr-;~in

Temp. C()

1 llr. Set. Solids

Covo.'r

. 0 TIS::UE 0 INl'Jo:NSIVE s •. m Efo!ERGENL'Y

STATION LOcATioN ;if;, ~~~~:t ·. . REt~RKS downS::: :~~~sh+Dh:p{l\PCs~

Tir.•e Begin ·l,lnte End Time End Depth DM DB mm Value Type

A II L

Alkcl1nJty I pll 4.5

1410 436

ijf~g~ctivity Salinity S/L R.P. ~~~enm·Stagcl tP~w, 8!! . 61

Inst,

9!5 7030S

Pr~cip1tat1on Wind Dfrc~tion Inches From North

4!! 36

Turbi~ity I Oil-Crease Severity . Severity 13!!0 1300

Strcnrt Color Dead Fish St>verity Silt or Sedfrucnt

Susp. SeverHy Sed. Severity Identity

1340

T, S, or D Semple Type

pH S.J

H}•dro lUe~. Flow, t!CD Dam llitl. c.:l'S

7203A !!00!51

Sludc~ Floatfne Ilc:brfs Severity Sever ty

131!! 134!!

Aq \!:tlic Ver.eta tiot' Sup pert tlcd U111 s~vt>rl t)'

-·--

.. < cr'-'...w. \o fti.u c ·

STATE OF NORTH CARO.A ' ,

DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES - t. ~. - .

R<llt·igh :!7fi II

I AMES E. HARRINGTON

SECRETARY

JAMES LIIOL~IlOUS[R.IR.

,..... · .... ·: . TELEPHONE

AREA CODE 919-829-4984

Mr. L. D. Kiker Route 1, Box 149 ~id1and, North Carolina 28107

February 19, 1973

Subject: Voiding of Permit No. 2309 Industrial Wastewater Lagoon Mr. L. D. Kiker

GOVERNOR

Gabarrus County, North Carolina

Dear Mr. Kiker:

Permit No. 2309 was issued to you on April 26, 1972 for the operatio~ of a leaching and evaporation lagoon to receive industrial waste. The 1

original expiration date of this Permit was June 30, 1973.

By letter from ~~Chief, Water ,Quality Division, on September 11, 1972 yol:lvrere--i-nst.ruc ed to· cease all further use of the lagoon because of violations in the conditions of the Permit. Subsequent inspe~tions by the staff have confirmed that although problems with the lagoon continue to exist it is in fact no longer being used for the disposal of additional wastewater.

Therefore, since the facility is no longer in operation, Permit No. 2309 issued to Hr. i.. D. Kiker, Cabarrus County, is hereby declared null and void. This voiding of Permit shall not be construed as freeing the owner from responsibility for conditions existing and caused during the period the Penmit was in force. ·Also, you are further instructed to take whatever measures are necessary and available to insure that no discharge occurs from the lagoon into the surface waters of. the State, and you are to proceed to backfill this lagoon with dirt as fast as the water level permits until the lagoon is completely filled and the wastewater is no longer evident.

If we can offer further clarification do not hesitate to contact us.

Sincerely,

6-t:~~ E. C. Hubbard ----... "-.._ Assistant Director

cc: ,......Cabarrus County Health Department Mr. L. P. Benton, Jr. Mr• W. E. Long, Jr. Mr. Robert Van Tilburg Mecklenburg County Health Department Piedmont Regional Office

~-"

STATE OF NORTH CARO. •

DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES Box 27fi87 Raleigh 27611

CHARLES W. BRADSHAW, JR.

SECRETARY

ROBERT W. SCOTT GOVERNOR

Office of Water and Air Resources

September 11, 1972

CERTIFIED MAIL ltE'nJRN RECEIPT RaQUESTED

Mr. L. D~ Kiker Route 1, lox 149 Midland, North Carolina 28107

Dear Mr. Kikert

Subjeetl

GEORGE E. PICKETT, DIRECTOR

TELEPHONE 829-3003

1'\ tr-!"') r•,.. .-r'. "\ • \" ( • :. ... . . - () ........

Permit Ro. 2309 Mr. L. D. Kiker Cabarrus County

Thla letter ia to adviae you that your leachin& and evaporating lagoon operation is 1n violation of the te~ and conditions of Permit No. 2309.

The subject 4tapoaal 1yatem vaa eonatrueted ud ba1 lteen operated in aueh a manner and bas received wastes of a nature that have been very conduciYe to the creation of offensive odors. These odors have contributed fully or ln part to the nuisance conditions that axlst ln the vicinity of the lagoon.

Condition Ro. S of your Permit 1tatea that if offensive odors or nuiaance conditions arlee, that the uae of the facility a1 a means of waat..ater dispo•al aball tmmedtately cease. M~era of the 1taff have determined that nuisance conditions axi1t and are caused fully or ln part at times by the odora from your facility. Thla alone is arouada for raquirlna that uae of the facUlty cease.

In addition• several other conditlona were aot aet. Condition No. 1 was Ylolated in that the f•~~llties were placed in operation without adequate fencing or an influent eoncxata apillway a1 shown in approved plans. Secondly, Condition Mo. 2 reatrlcta diacbarae to Do .ore than 2500 &•llona per day of waatewaterJ however, thi1 ha1 been exceeded on at laaat one occaaion. finally you have failed to provide aultabla aroundwater devices for aonitorlng purpose• as atated ln Condition Mo. 6.

Whether or not the additional violations led to the creation ~f offensive odors, they are nevertbelea1 violations of Permit Ro. 2309, and are also &rounds for raquiriua you to cease your operation.

DIVISION OF AIR QUALITY

DIVISION OF DIVISION OF DIVISION OF DIVISION OF DIVISION OF WATER MANAGEMENT WATER QUALITY • GROUND WATER WATERWAYS & SEASHORE PLANNING

FROM

NORTH CAROLif·"'. DEPARTMENT OF,HUMAN ktSOURCES

INTER OFFitE MEMORANDUM DATE __ _

------------------

''

''

'·· \_.

·q-sz·- -:)1~:;- ~· ._ ~--3~ -733'3

UJ-M ~· :,;..J. ~

-~ ;r-4'~~/(),ed (;~4) z79-:50f<f

~&tWCt-(r;&4-) ;J1tj-3 014

c r ~ ~ {)~~A-~

. . Mr. L. J). IU.ker • l'ag• Two • Saptemb~r 11, 1972

Since numerouz condltiona or your PerMit Jo. 2309 have been violated, thie Otfiee b hereby lnatrvctiDg you te eaaae ue of the leachin& aild evaporation la&oon oo or ~fore November 30, 1972. You ahould also take immediate atepa to prevent offanelve oaora enc! auiaanee coac!ltioa.a from ul.q created. A copy of this letter vlll be fo~rdcct to Cabnrrua County Health Depart:JDent cd to Chemical ~amcm Tank Ltces, be. ly copy of tbh letter, Cbf:mlcal &.ea.on Tank Liaes, Inc. 1~ being alvlaQd to contact this Office ao that appropriate means of handl1Ui UJeir waate can be arranged lf aueh a need will exist after Nov mber 30 r 1 c; 72.

lf you should fail to comply with the reqvlremcmta of thb letter, membarc of the Staff of the Water Quality Dl.vialon will have DO alternative but to report thh aatter to the Weter and Air Quality Cootrol Cocmnlttee of the Boe rd of Water and Air ke1ourcea.

Youn trvly,

». L. C::Olturn. Chlef1 Water- Quality Dlvleion

cc t 1=hentical Leamou Tank Lines, lnc. L/Mr. Albert KU.maa, Cab.arnus Cowty Health 'Department

Hr. Tom Ievina, Mecklenburg County Health Departnent Mr. John c. Murdock, Ill

. J

;·:s·tif.E GF ~ORTH CAROLINA ,. .. . -DEPARTMENT OF N.RAL AND ECONOI'v1IC .OURCES

Bu'll 27687 ' J{,do·l~h :.!7'1;11

CHAI'ILES W. BI'IADSHAW, JR. SECI'IET-'RY

I'!OIIERT W SCOTT C,(l\'[~N(l~

Offic:r. of Water ancl Air Rrsnurr.es

....

July 12, 1972 GEORGE E. PICKETT. DIRECTOR

TELEPHONE 829·3003

MEMORANDUM TO: Mr. John C. Murdock, I~Y\·(i Act_ing Regiona 1 Engine~\ v,~-.

FROM:

'SUBJECT:

Pie~mont Regional Office . .

.Dr. s. T. Mayne & Mr. James Regional Chemists

L. Cbocklet~~ .f.:t /1'1

Review and Background on Industrial Leac~ Pits Cabarrus County

Many industrial wastes are of such a nature as to be nontreatable by eonventicnal biolo~ical methods. Since this is the case for several industries in Cabarrus and Mecklenburg Counties, thes_e industries accepted the disposal alternative of evaporation and leach pits to dispose of nonbiological treatable wastes. Areas within Cabarrus County are being used to dispose of this type of waste from the following industries:

1. A. E. Staley Manufacturing Comp~ny Textile Division 5046 Old Pineville Road P. 0. Box 948 Charlo~te, N. C. 28201

2. Wica Chemicals Division Ott Chemical Company P. o. Box 506 (Orr Road) Charlotte, N. c. 28201

3. C & T Refinery 4918 South Boulevard Charlotte, N. c.

4. Chemical Leamon Tank Lines, Inc. Highway 29 North Charlotte, N. C.

5. Southern Latex 161 Buffalo Avenue, N. w. Concord, N. C. ·

One area owned by Mr. L. D. Kiker i~ located 0.3 miles off SR · 1153 at the end of the access road to the old Concord City Dump. (See attached map.) The access road is located 0.7 miles from the intersection of SR's 1153 and 1152. This site accepts liquid waste from only Chemical Leamon Tank Lines, Inc. This particular wastes consists

DIVISION OF DIVISION OF DIVISION OF DIVISION OF DIVISION OF DIVISION OF PLANNING AIR QUALITY WATER MANAGEMENT WATER QUALITY• G::tOUND WATER WATERWAYS & SEASHORE

.. . - . Mr. John c. Murdock, III !'age 2 July .12, 1972 • • of alkali wash sol~tions (NaOH) which remove and clean materials remaining in emptied tank trailer trucks. See attached sheet for products transported by Chemical Leamon.

The other area owned by J. Lee Pharr is located on SR 1152 0.3 miles from the intersection of SR 1 s 1153 and 1152. The evaporation and leach pits are located approximately 0.4 miles down an access road which fronts SR 1152 (see attached map). The other four companies haul the industrial waste to this area which was formerly used to accept garbage when Mr. Pharr ran the Cabarrus Disposa1 Company. The waste from Wica Chemicals con~ists of a liquid containing 5 to 7% solids, of which 90% is styrens - butadiene rubber and the majority of the balance is alum. Southern Latex deposits a semisolid latex waste into one pit which after an extended .period of time forms a rubbery mass that seals off the bottom of the pit. The third pit used by·A. E. Staley Manufacturing Company accepts a waste discharge with a solid content of 0.77% and having a percentage of 0.27 methyl naphthalenes. The solid content consists of sodium sulfate and emulsifiers. The •taste from C & T Refinery is a solid consisting of non-edible vegetahle oils impregnated into diatomaceous earth. This combination of oils has a very low flash point which requires this waste to be buried immediately upon delivery. These treatment facilities are designed for disposal of wastewater and waste products solely by evaporation and leaching into the soil. ·

This department's investigation by the staff of Water Quality Division and Air Quality Division, Piedmont Regional Office, began from an initial odo~ complaint registered by Mr. George w. Maxwell, Rt. #5, Box 545, Concord, North Carolina against industrial liquid waste disposal on Pharr's property (see attached sheet). Since the liquid waste originated from an industrial source, the final action as to the disposition of the problem will be handled by the Water Quality Division. Since this first complaint, Mr. Raymond Coley, Old Archibald Road, Cabarru~ County also registered a written ·complaint to this office regarding this odor problem (see attached sheet). Various verbal complaints concerning this problem have been made to this office and the County Health Department.

Shortly after these complaints against industrial waste disposal by these means which were located on Pharr's land, a complaint registered by the Concord Police Department to Raleigh against allowing Mr. L. D. Kiker to operate a similar waste treatment facility for disposal of Chemical Leamon Tank Lines, Inc. waste was made. Recommendations concerning this new facility by William c. Mills, Regional Engineer with this department and Mr. Dick Peace of the Division of Ground Water (see attached sheets) were in favor of issuance of a permit to dispose of liquid waste into another evaporation-leach pit. These investigations were made after this particular pit was built. After the issuance of a permit to Mr. Kiker and use of the facility by Chemical Leamon, additional complaints concerning both waste treatment sites were made to the newspapers at Concord and Charlotte, the Piedmont Regional Office of the Office of Water and Air Resources and the Governor's Office at Raleigh.

~ ... Mr. John c. Murdock, Ill 'Page 3 July 12, 1972 • • Both Mr. Pharr and Mr. Kiker were involved previous to the disposal of ljquid_industrial waste in the garbage disposal business. The areas used for this were in close proximity to the presenc evaporation and leach pits. Mr. Pharr's garbage dump is located below the pits and at the head waters of an unnamed tributary to Rocky ·River while Mr. Kiker's garbage dump previously run by the City of Concord (see attached sheet) is located uphill from the pit for Chemical Leamon's liquia waste. Both garbage dumps were poorly managed and not compacted during the operational life of the sites. When the pits were closed by the County Health Department, the areas were covered with a layer of top soil which ~llowed for infiltration and subsequent leaching of contaminat~d waters _into surface waters.

. . The subject industrial disposal pits operated by Mr. Pharr and Mr.

Kiker have received a thorough evaluation as to construction, operation, ·safety hazards and effectiveness •. Mr. ~harr's pits are crudely dug ·holes with little consideration given to the prevention ~f over-flows and the incorporation of catch basins and freeboard deptl's• There are no adequate means to provide run-off waters from entering the pits during heavy rains as well as protection means such as fences to provide controlled access to the pits. Emergency equipment such as pumps are not provided in case of emergencies such as over-flows or broken dikes. Supervision by Mr. Pharr or personnel associated with Mr. Pharr is not provided, and on several occasions this was needed. These pits are located in badly weathered soil with numerous gullies that can provide excellent means of spillage entering and combining with surface waterso The Pharr pits are also being used for the disposal of non-liquid waste products which include metal containers, rags and other refugee that not only hinders operation of and access to the pits, but also creates an unsightly appearance. It should also be noted that Mr. Pharr was observed by one of the writers inter-mixing the waste liquids from two different companies without consideration to the possible chemical reactions and future odor problems which may be produced. One final point with regards to the possible leach of contaminants from these pits into surface waters is that the leach from the garbage dump and the leach from the pits could not be distinguished between since these discharges are in such close proximity to one another. Staff from the State Board of Health related to the writers that the leach coming from the garbage dump was due to poor operation. Since this discharge will continue, differentiation between the two leaches is almost impossible. Observations and field tests shortly after a heavy rain could not determine violation of stream standards. Further investigations should be made in the future with reg~rd to surface water contimination.

Mr. Kiker has secured the services of a Consulting Engineer Mr. Tom Cox, for the design of the pit to be used by Chemical Leamon Tank Lines, Inc. More detail was given to the design and construction of this pit than to those operated by Mr. Pharr. However, all-the permit conditions stipulated for Mr. Kiker's pit have not been met as of the date of this report. Three of these conditions not met are a fence around the pit, construction of a sampling well below the pit, and a spillway for unloading liquid waste into the pito It has also

•

, r ... ·· . ·' ..

Page 4 Ju,ly 12, 1972

1 been observed by oth writers that the daily eff~t discharges,of 2,500 gallons per day has been exceeded on several occasions. Mr. Kiker or his representative have not been present during several unloading operations by Chemical Leamon Tank Lines, Inc., and some spillage during the unloading operation has occurred. This spillage has not received immediate remedial action. The Concord Pol~cemen's Association has shown concern before the pits operation and since that time over.the possible effects of such spillage on the aquatic life in their fishing lake which receives run-off from the vicinity of the garbage dump and pit. Field tests in the stream from this area shortly after heavy rains have shown no water water quality violations. As in the case with Mr. Pharr, the leachate from the garbage dump appears directly below the disposal·pit. Since this condition occurs, differentiation between leachate from the garbage dump and the pit can not be made. This leachate may contribute· to the heavy alga growth observed by the writers in the-policemen's pond. Further tests tiuring low flow conditions should be made for nutrients in this leachate which discharges to the stream above the policemen's pond.

CONCIIDSION:

Since both staff members have been involved with both disposal areas, and one acquainted with the odors associated with the water from both disposal areas, they can state that similar odors can be detected off the site and particularly along SR roads 1152 and 1153. These odors are present primarily during hot, low humid, windy days with the wind blowing west to east.

It is both writers' recommendation and opinion that evaporation ,and leach pits are not satisfactory means for the· disposal of industrial liquid waste. One contributing factor is the amount of evaporation and rainfall during a one year span is nearly equal• If this is true, there will be only minimum loss by process of evaporation. A statement by Mr. Dick Peace of the Division of Ground Waters relates that the gumbo clay used to line the pits is very impervious. This will allow for only minimum leach into the soil. The combination of these two processes makes for a giant holding pond filled with extremely high COD containing waste. Decomposition and bacterial action on this waste is and will continue to

·produce odors which are causing nuisance conditions. Both writers agree that technical means are available to pretreat this waste and produce an effluent which is biodegradable. Amsco Chemical Company which is located in Meckelnburg County pretreats waste which has similar characteristics to all wastes present at both locations. The pretreatment process involves flocculation of the emulsified discharge by iron flocculation which coagulates the latex and other emulsified products to pro_duce a tlear effluent which could be biologically treated. The iron floc which contains the emulsified products can then be disposed of by adequate burial in a properly operated landfill.

~

._ S~~T~-:'F NORTH CAROL. •

DEPARTMENT OF NATURAL AND ECONOMIC RESOURCES ··' 1

Dox 276R7 Rnlcigh 27611 ROBERT W. SCOTT GOVERNOR

CHARLES W. BRADSHAW. JR.

SECRETARY

Office of WF~ter F~nrl Air Resources GEORGE E. PICKETT, DIRECTOR

September 8, 1972 TELEPHONE 829·3003

CERTIFIED MAIL ~ RECEIPT !fBt!E§TED

E f.'.,-:-· ::r<7"'l>.

. -4 r. . ! ' F \: '·" li Jl ~~,v~.l I L:U' . .

Mr. J. Lee Pharr 1642 Old Charlotte Road Concord, North Carolina 28025

C/._ . . ~ . ., ' .. ,_ ' ~-' - ....... 1 .•.

Subject: Waste Disposal Pits Cabarrus County~ North Carolina

Dear Mr. Pharr:

Reference is made to the meeting in our Piedmont Regional Office on July 26, 1972·. In attendance at the meeting were Mr. Frank Cockinos, , Mr. H. L. Moorefield, Jr., Mr. James L. Chocklett and Mr. John c. Murdock, !II. During the meeting you discussed requirements for the construction and operation of waste disposal facilities. It was pointed out that numerous complaints had been received from the vicinity around the disposal site.

Since you have not filed an Application for Permit with final plans and specifications, and due to the nuisance conditions that exist in the vicinity, you are advised to cease use of the facilities on or before November 30, 1972. Failure to comply will result in this matter being referred to the Water and Air Quality Control Committee, Board of Water and Air Res_ources for appropriate action.

As Mr.- Murdock explained during the meeting, copies of this letter will be forwa.rded to all industries presently using disposal pits on

--your prop·erty. The companies are advised to contact Mr. Murdock in the poncord Regional Office to develop adequate programs for handling any wastewater problems that might arise as a result of your ceasing to use the existing facilities.

Should you desire to use any portion of your property for disposal sites for solid wastes, it is recommended that you contact the North Carolina State Board of Health and obtain the necessary approval from tha~ agency. Should you wish to construct any wastewater treatment facilities in the future, please contact Mr. John c. Murdock of the Piedmont Regional Office in Concord for a site investigation, and to

DIVISION OF AIR QUALITY

DIVISION OF WATER MANAGEMENT

DIVISION OF WATER QUALITY •

DIVISION OF DIVISION OF GROUND WATER WATERWAYS & SEASHORE

DIVISION OF PLANNING

Mr. J. Lee Pharr Page 2

. September 8, 1972

• obtain the specific information regarding filing Application 'for Permit. Failure to apply and obtain a permit prior to construction and operation of wastewater treatment facilities is in violation of N. c. Statutes Chapter 143, Section 215.1 (a) (2).

Yours truly,

~c/.~ D. L. Coburn .. Chief, Water Quality Division

· cc: A. E. Staley Manufacturing Company Wica Chemicals

J·

C & T Refinery Southern_ Latex

Jtabarrus County Health Department Mecklenburg County Health Department Mr. John c. Murdock, III

231SERBSF10,614 - 6 Feb 2017 14:55

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