LAMPIRAN - Universitas Muhammadiyah Surakartaeprints.ums.ac.id/40967/17/LAMPIRAN.pdf · Lampiran 4....

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LAMPIRAN

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Lampiran 1. Surat Keterangan Ekstrak Kulit Manggis

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Lampiran 2. Blanko Angket Uji Respon Rasa Granul Effervescent BLANKO ANGKET PETUNJUK PENGISIAN

1. Isilah data identitas Anda pada tempat yang disediakan dengan lengkap!

2. Berikan tanda cek(√) yang tersedia dengan tepat. Identitas Diri

Nama : Umur : Pekerjaan : Alamat : Tanda tangan :

Setelah mencicipi dan merasakan formula I, II, III, IV, dan V granul

effervescent ekstrak kulit manggis dan buah tomat bagaimana pendapat saudara/i tentang rasa dari kelima formula granul effervescent tersebut?

Granul

effervescent Tanggapan rasa

Sangat manis Manis Kurang manis Hambar Formula l Formula ll Formula lll Formula IV Formula V

Setelah anda merasakan kelima formula tersebut, formula mana yang paling anda sukai dan menurut anda dapat di pasarkan?

Tanggapan responden

Jenis granul Formula l Formula ll Formula lll Formula IV Formula IV

Sangat suka Suka Kurang suka Tidak suka

Dari kelima formula tersebut, formula manakah yang memiliki warna

granul terbaik setelah dilarutkan?

Tanggapan responden

Jenis granul Formula l Formula ll Formula lll Formula IV Formula IV

Sangat baik Baik Kurang baik Tidak baik

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Lampiran 3. Data Hasil Perhitungan Tanggapan Rasa effervescent Dari 20 responden yang terpilih untuk memberikan penilaian terhadap granul effervescent kulit manggis dan buah tomat adalah sebagai berikut:

a. Rasa sediaan Tanggapan

Rasa F1

(responden) F II

(responden) F III

(responden) F IV

(responden) F V

(responden) Sangat manis 0 0 0 0 0

Manis 5 0 12 1 6 Kurang mnis 15 9 8 12 14 Tidak manis 0 11 0 7 0

b. Kesukaan

Tanggapan suka

F1 (responden)

F II (responden)

F III (responden)

F IV (responden)

F V (responden)

Sangat suka 0 0 0 0 0 Suka 10 3 14 4 5

Kurang suka 18 6 6 10 11 Tidak suka 2 11 0 6 4

c. Warna sediaan

Tanggapan warna

F1 (responden)

F II (responden)

F III (responden)

F IV (responden)

F V (responden)

Sangat baik 0 0 0 0 0 Baik 8 17 3 9 3

Kurang baik 11 2 13 10 15 Tidak baik 1 1 4 1 2

Formula I ada 5 responden yang memilih manis dan 15 responden memilih kurang manis, maka dapat dihitung prosentasenya: Formula I: Manis : 5/20 x 100% = 25% Kurang manis : 15/20 x 100% = 75%

Lampiran 4. Perhitungan Asam Basa Dibuat 500 granul dengan berat 300 mg tiap granul effervescent

Perhitungan asam dan basa untuk setiap formula.

Asam yang digunakan adalah asam sitrat dan asam tartrat serta bagian

basa digunakan natrium bikarbonat. Berikut adalah reaksi asam sitrat dan asam

tartrat dengan natrium bikarbonat:

H3C6H5O7.H2O + 3NaHCO3 → Na3C6H5O7 + 4H2O + 3CO2 asam sitrat + Na-bikarbonat → Na-sitrat + air + C. dioksida H2C4H4O6 + 2NaHCO3 → Na2C4H4O6 + 2H2O + 2CO2 asam tartarat + Na-bikarbonat → Na-tartat + air + C.dioksida

Berdasarkan reaksi diatas, dapat diketahui bahwa untuk menetralkan 1

mol asam sitrat dibutuhkan 3 mol natrium bikarbonat. Serta untuk menetralkan 1

mol asam tartrat dibutuhkan 2 mol natrium bikarbonat. Maka perbandinganya

adalah:

a) Asam sitrat

Jika 2 gram asam sitrat (BM 210) bereaksi dengan 2,4 gram natrium bikarbonat

(BM 84) dengan perhitungan:

x = 2,4

b) Asam tartrat

Jika 2 gram asam tartrat (BM 150) bereaksi dengan 2,24 gram natrium bikarbonat

(BM 84) dengan pehitungan:

x = 2,24

Maka dapat disimpulkan bahwa natrium bikarbonat yang dibutuhkan untuk

bereaksi dengan 2 gram asam sitrat dan 2 gram asam tartrat adalah 4,64 dengan

perhitungan:

2,4 gram + 2,24 gram = 4,64 gram natrium bikarbonat.

Maka perbandingan asam sitrat : asam tartrat : natrium bikarbonat adalah 2:2:4,64

Untuk berat total asam- basa granul effervescent 2 : 2 : 4,64 = 8,64 = 9 gram

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Formula I

Asam sitrat = 2/9 x 2 g = 0,444 g = 0,5 g

Asam tartrat = 2/9 x 2 g = 0,444 g = 0,5 g

Na. Bikarbonat = 4/9 x 2 g = 0,888 g = 1 g

Formula II

Asam sitrat = 2/9 x 2 g = 0,444 g = 0,5 g

Asam tartrat = 4/9 x 2 g = 0,888 g = 1 g

Na. Bikarbonat = 2/9 x 2 g = 0,444 g = 0,5 g

Formula III

Asam sitrat = 4/9 x 2 g = 0,888 g = 1 g


Na. Bikarbonat = 2/9 x 2 g = 0,444 g = 0,5 g

Formula IV

Asam sitrat = 1/9x 2 g = 0,222 g = 0,25 g


Na. Bikarbonat = 4/9x 2 g = 0,888 g = 1 g

Formula V

Asam sitrat = 3/9 x 2 g = 0,666 g = 0,75 g

Asam tartrat = 1/9x 2 g = 0,222 g = 0,25 g

Na. Bikarbonat = 4/9x 2 g = 0,888 g = 1 g

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Lampiran 5. Perhitungan Aktivitas Antioksidan Kontrol Positif (Vitamin E) Dan Sediaan Granul Effervescent.

A. Aktivitas antioksidan kontrol positif vitamin E 1. Absorbansi

Kontrol negatif (DPPH) : 1,264 Kontrol positif (vitamin E) :

a. Orientasi : 0,187

b. Replikasi 1 : 0,173

c. Replikasi 2 : 0,126

d. Replikasi 3 : 0,094

e. Replikasi 4 : 0,142

f. Replikasi 5 : 0,187

2. Perhitungan % aktivitas antioksidan

b. Data 1 (0,187)

% aktivitas antioksidan = x 100% = 85,20%

c. Data 2 (0,173)


d. Data 3 (0,187)


Rata-rata = 85,57% SD = 0,673 RSD = 0,745%

B. Aktivitas antioksidan ekstrak kulit buah manggis dan buah tomat Kontrol negatif (DPPH) : 0,561 Absorbansi ekstrak

a. Replikasi 1 : 0,229

b. Replikasi 2 : 0,230

c. Replikasi 3 : 0,230

Perhitungan % aktivitas antioksidan a. Data 1 (0,229)


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b. Data 2 (0,230)

% aktivitas antioksidan = x 100% = 59%

c. Data 3 (0,231)

% aktivitas antioksidan = x 100% = 59%

Rata-rata = 59,06% SD = 0,103 RSD = 0,174%

Karena dengan ekstrak tomat 300 mg dan buah tomat 500 mg sudah

memiliki aktivitas antioksidan lebih dari 50 % maka dapat digunakan dalam

formula.

C. Aktivitas antioksidan sediaan granul effervescent

Formula 1

DPPH : 0,561

Basis : 0,432

Effervescent 1 : 0,191



Perhitungan aktivitas antioksidan basis


Effervescent 1


Effervescent 2


Effervescent 3


Rata-rata replikasi = 60,25%

SD = 0,13

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Formula 2

DPPH : 0,561

Basis :0,403






Effervescent 1


Effervescent 2


Effervescent 3

% aktivitas antioksidan = x 100% =54,36%

Rata-rata = 54,19%

SD = 0,14

Formula 3

DPPH : 0,341

Basis :0,215






Effervescent 1


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Effervescent 2


Effervescent 3


Rata-rata = 64,80%

SD = 0,46

Formula 4

DPPH : 0,461

Basis :0,367






Effervescent 1


Effervescent 2


Effervescent 3


Rata-rata = 59,12%

SD = 0,27

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Formula 5

DPPH : 0,341

Basis : 0,249






Effervescent 1


Effervescent 2


Effervescent 3


Rata-rata = 61,17%

SD = 0,40

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Lampiran 6. Hasil Uji Sifat Fisik Granul Effervescent.

1. Waktu alir Replikasi Waktu alir granul (detik)

Formula I

Formula II Formula III Formuala IV

Formula V

1 11,11 10,18 11,13 11,39 11,44 2 11,23 10,15 11,14 11,35 11,21 3 11,28 10,21 11,11 11,38 11,65

Rata-rata 11,23 10,18 11,13 11.38 11.44 SD 0,08 0,03 0,01 0,02 0,22

2. Indeks kompresibilitas

Formula

Replikasi

Vo (mL)

M (g) Vk (mL)

rk(mL) (M/Vk)

ro(mL) (M/Vo)

C% rk - ro/ rk x 100 %

SD

1 1 100 74,55 96 0,77 0,74 4,70 2 100 74,55 98 0,76 0,74 2,72 1,50 3 100 74,55 99 0,75 0,74 1,72 2 1 100 70,35 97 0,72 0,70 3,47 2 100 70,35 96 0,73 0,70 4,47 0,99 3 100 70,35 98 0,71 0,70 2,47 3 1 100 68,50 97 0,70 0,68 3,69 2 100 68,50 98 0,69 0,68 2,70 0,99 3 100 68,50 96 0,71 0,68 4,69 4 1 100 63,15 96 0,65 0,63 4,22 2 100 63,15 97 0,65 0,63 3,22 0,57 3 100 63,15 97 0,65 0,63 3,22 5 1 100 59,80 97 0,61 0,60 2,66 2 100 59,80 98 0,61 0,60 1,67 0,57 3 100 59,80 97 0,61 0,60 2,66

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4. Waktu larut granul effervescent

formula Suhu air

100 270 600

1 177 123 51 1 178 120 51 1 177 121 49 2 176 118 46 2 176 117 47 2 175 118 48 3 180 125 51 3 181 124 52 3 182 125 52 4 189 135 60 4 189 135 60 4 191 136 61 5 201 144 70 5 199 145 69 5 200 143 68

5. Waktu larut granul

formula Suhu air

100 270 600

1 312 204 120 1 313 204 123 1 313 203 121 2 325 246 132 2 327 247 135 2 324 245 134 3 366 259 146 3 367 257 145 3 368 259 143 4 375 272 166 4 376 271 165 4 374 271 163 5 387 312 189 5 386 314 190 5 388 311 192

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6. Gambar larutan

Urutan tingkat kejernihan larutan granul effervescent : F2, F4, F1, F3, F5

Gambar larutan granul

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Lampiran 7. Hasil Uji Statistik Anova 1. Uji waktu alir

Post Hoc Test Multiple Comparisons

waktu.alir LSD

(I) formula

(J) formula

Mean Difference (I-

J) Std. Error Sig.

95% Confidence Interval

Lower Bound Upper Bound

formula 1

formula 2 2.05000* .08446 .000 1.8618 2.2382

formula 3 .08667 .08446 .329 -.1015 .2749

formula 4 -.14333 .08446 .121 -.3315 .0449

formula 5 -.20333* .08446 .037 -.3915 -.0151

formula 2

formula 1 -2.05000* .08446 .000 -2.2382 -1.8618

formula 3 -1.96333* .08446 .000 -2.1515 -1.7751

formula 4 -2.19333* .08446 .000 -2.3815 -2.0051

formula 5 -2.25333* .08446 .000 -2.4415 -2.0651

formula 3

formula 1 -.08667 .08446 .329 -.2749 .1015

formula 2 1.96333* .08446 .000 1.7751 2.1515

formula 4 -.23000* .08446 .021 -.4182 -.0418

formula 5 -.29000* .08446 .006 -.4782 -.1018

formula 4

formula 1 .14333 .08446 .121 -.0449 .3315

formula 2 2.19333* .08446 .000 2.0051 2.3815

formula 3 .23000* .08446 .021 .0418 .4182

formula 5 -.06000 .08446 .494 -.2482 .1282

formula 5

formula 1 .20333* .08446 .037 .0151 .3915

formula 2 2.25333* .08446 .000 2.0651 2.4415

formula 3 .29000* .08446 .006 .1018 .4782

formula 4 .06000 .08446 .494 -.1282 .2482

*. The mean difference is significant at the 0.05 level.

37

Oneway

ANOVA

waktu.alir

Sum of Squares df Mean Square F Sig.

Between Groups 10.893 4 2.723 254.515 .000

Within Groups .107 10 .011

Total 11.000 14

2. Uji pengetapan / indeks kompresibilitas

Oneway

ANOVA

Pengetapan


Between Groups 3.635 4 .909 .917 .491

Within Groups 9.914 10 .991

Total 13.549 14

3. Waktu melarut 100

Oneway

ANOVA

Melarut


Between Groups 6249.067 4 1562.267 1233.368 .000

Within Groups 12.667 10 1.267

Total 6261.733 14

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Dependent Variable:waktularut

(I) formula

(J)

formula

Mean

Difference (I-

J) Std. Error Sig.


Lower Bound

Upper

Bound

Tukey

HSD

formula 1 formula 2 2.00000 .81650 .179 -.6872 4.6872

formula 3 -3.00000* .81650 .028 -5.6872 -.3128

formula 4 -12.00000* .81650 .000 -14.6872 -9.3128

formula 5 -22.00000* .81650 .000 -24.6872 -

19.3128

formula 2 formula 1 -2.00000 .81650 .179 -4.6872 .6872

formula 3 -5.00000* .81650 .001 -7.6872 -2.3128

formula 4 -14.00000* .81650 .000 -16.6872 -

11.3128

formula 5 -24.00000* .81650 .000 -26.6872 -

21.3128

formula 3 formula 1 3.00000* .81650 .028 .3128 5.6872

formula 2 5.00000* .81650 .001 2.3128 7.6872

formula 4 -9.00000* .81650 .000 -11.6872 -6.3128

formula 5 -19.00000* .81650 .000 -21.6872 -

16.3128

formula 4 formula 1 12.00000* .81650 .000 9.3128 14.6872

formula 2 14.00000* .81650 .000 11.3128 16.6872

formula 3 9.00000* .81650 .000 6.3128 11.6872

formula 5 -10.00000* .81650 .000 -12.6872 -7.3128

formula 5 formula 1 22.00000* .81650 .000 19.3128 24.6872

formula 2 24.00000* .81650 .000 21.3128 26.6872

formula 3 19.00000* .81650 .000 16.3128 21.6872

formula 4 10.00000* .81650 .000 7.3128 12.6872

LSD formula 1 formula 2 2.00000* .81650 .034 .1807 3.8193

formula 3 -3.00000* .81650 .004 -4.8193 -1.1807

39

formula 4 -12.00000* .81650 .000 -13.8193 -

10.1807

formula 5 -22.00000* .81650 .000 -23.8193 -

20.1807

formula 2 formula 1 -2.00000* .81650 .034 -3.8193 -.1807

formula 3 -5.00000* .81650 .000 -6.8193 -3.1807

formula 4 -14.00000* .81650 .000 -15.8193 -

12.1807

formula 5 -24.00000* .81650 .000 -25.8193 -

22.1807

formula 3 formula 1 3.00000* .81650 .004 1.1807 4.8193

formula 2 5.00000* .81650 .000 3.1807 6.8193

formula 4 -9.00000* .81650 .000 -10.8193 -7.1807

formula 5 -19.00000* .81650 .000 -20.8193 -

17.1807

formula 4 formula 1 12.00000* .81650 .000 10.1807 13.8193

formula 2 14.00000* .81650 .000 12.1807 15.8193

formula 3 9.00000* .81650 .000 7.1807 10.8193

formula 5 -10.00000* .81650 .000 -11.8193 -8.1807

formula 5 formula 1 22.00000* .81650 .000 20.1807 23.8193

formula 2 24.00000* .81650 .000 22.1807 25.8193

formula 3 19.00000* .81650 .000 17.1807 20.8193

formula 4 10.00000* .81650 .000 8.1807 11.8193

*. The mean difference is significant at the 0.05 level. 4. Waktu melarut 270

Oneway

ANOVA

Melarut


Between Groups 6249.067 4 1562.267 1233.368 .000


Total 6261.733 14

40



(I) formula (J) formula

Mean

Difference (I-J) Std. Error Sig.

95% Confidence

Interval

Lower Bound

Upper

Bound

Tukey HSD formula 1 formula 2 3.33333* .91894 .030 .3090 6.3576

formula 3 -3.66667* .91894 .017 -6.6910 -.6424

formula 4 -14.66667* .91894 .000 -17.6910 -

11.642

4

formula 5 -22.66667* .91894 .000 -25.6910 -

19.642

4

formula 2 formula 1 -3.33333* .91894 .030 -6.3576 -.3090

formula 3 -7.00000* .91894 .000 -10.0243 -3.9757

formula 4 -18.00000* .91894 .000 -21.0243 -

14.975

7

formula 5 -26.00000* .91894 .000 -29.0243 -

22.975

7

formula 3 formula 1 3.66667* .91894 .017 .6424 6.6910

formula 2 7.00000* .91894 .000 3.9757 10.024

3

formula 4 -11.00000* .91894 .000 -14.0243 -7.9757

formula 5 -19.00000* .91894 .000 -22.0243 -

15.975

7

formula 4 formula 1 14.66667* .91894 .000 11.6424 17.691

0

formula 2 18.00000* .91894 .000 14.9757 21.024

3

41

formula 3 11.00000* .91894 .000 7.9757 14.024

3

formula 5 -8.00000* .91894 .000 -11.0243 -4.9757

formula 5 formula 1 22.66667* .91894 .000 19.6424 25.691

0

formula 2 26.00000* .91894 .000 22.9757 29.024

3

formula 3 19.00000* .91894 .000 15.9757 22.024

3

formula 4 8.00000* .91894 .000 4.9757 11.024

3

LSD formula 1 formula 2 3.33333* .91894 .005 1.2858 5.3809

formula 3 -3.66667* .91894 .003 -5.7142 -1.6191

formula 4 -14.66667* .91894 .000 -16.7142 -

12.619

1

formula 5 -22.66667* .91894 .000 -24.7142 -

20.619

1

formula 2 formula 1 -3.33333* .91894 .005 -5.3809 -1.2858

formula 3 -7.00000* .91894 .000 -9.0475 -4.9525

formula 4 -18.00000* .91894 .000 -20.0475 -

15.952

5

formula 5 -26.00000* .91894 .000 -28.0475 -

23.952

5

formula 3 formula 1 3.66667* .91894 .003 1.6191 5.7142

formula 2 7.00000* .91894 .000 4.9525 9.0475

formula 4 -11.00000* .91894 .000 -13.0475 -8.9525

formula 5 -19.00000* .91894 .000 -21.0475 -

16.952

5

42

formula 4 formula 1 14.66667* .91894 .000 12.6191 16.714

2

formula 2 18.00000* .91894 .000 15.9525 20.047

5

formula 3 11.00000* .91894 .000 8.9525 13.047

5

formula 5 -8.00000* .91894 .000 -10.0475 -5.9525

formula 5 formula 1 22.66667* .91894 .000 20.6191 24.714

2

formula 2 26.00000* .91894 .000 23.9525 28.047

5

formula 3 19.00000* .91894 .000 16.9525 21.047

5

formula 4 8.00000* .91894 .000 5.9525 10.047

5

*. The mean difference is significant at the 0.05 level. 5. Waktu melarut 600

Oneway

ANOVA

Melarut

Sum of Squares Df Mean Square F Sig.

Between Groups 2960.667 4 740.167 584.342 .000


Total 2973.333 14

43




Mean

Difference

(I-J) Std. Error Sig.


Lower Bound Upper Bound

Tukey HSD formula 1 formula 2 3.66667* .91894 .017 .6424 6.6910

formula 3 -1.33333 .91894 .612 -4.3576 1.6910

formula 4 -9.33333* .91894 .000 -12.3576 -6.3090

formula 5 -18.33333* .91894 .000 -21.3576 -15.3090

formula 2 formula 1 -3.66667* .91894 .017 -6.6910 -.6424

formula 3 -5.00000* .91894 .002 -8.0243 -1.9757

formula 4 -13.00000* .91894 .000 -16.0243 -9.9757

formula 5 -22.00000* .91894 .000 -25.0243 -18.9757

formula 3 formula 1 1.33333 .91894 .612 -1.6910 4.3576

formula 2 5.00000* .91894 .002 1.9757 8.0243

formula 4 -8.00000* .91894 .000 -11.0243 -4.9757

formula 5 -17.00000* .91894 .000 -20.0243 -13.9757

formula 4 formula 1 9.33333* .91894 .000 6.3090 12.3576

formula 2 13.00000* .91894 .000 9.9757 16.0243

formula 3 8.00000* .91894 .000 4.9757 11.0243

formula 5 -9.00000* .91894 .000 -12.0243 -5.9757

formula 5 formula 1 18.33333* .91894 .000 15.3090 21.3576

formula 2 22.00000* .91894 .000 18.9757 25.0243

formula 3 17.00000* .91894 .000 13.9757 20.0243

formula 4 9.00000* .91894 .000 5.9757 12.0243


formula 3 -1.33333 .91894 .177 -3.3809 .7142

formula 4 -9.33333* .91894 .000 -11.3809 -7.2858

formula 5 -18.33333* .91894 .000 -20.3809 -16.2858

formula 2 formula 1 -3.66667* .91894 .003 -5.7142 -1.6191

44

formula 3 -5.00000* .91894 .000 -7.0475 -2.9525

formula 4 -13.00000* .91894 .000 -15.0475 -10.9525

formula 5 -22.00000* .91894 .000 -24.0475 -19.9525

formula 3 formula 1 1.33333 .91894 .177 -.7142 3.3809

formula 2 5.00000* .91894 .000 2.9525 7.0475

formula 4 -8.00000* .91894 .000 -10.0475 -5.9525

formula 5 -17.00000* .91894 .000 -19.0475 -14.9525

formula 4 formula 1 9.33333* .91894 .000 7.2858 11.3809

formula 2 13.00000* .91894 .000 10.9525 15.0475

formula 3 8.00000* .91894 .000 5.9525 10.0475

formula 5 -9.00000* .91894 .000 -11.0475 -6.9525

formula 5 formula 1 18.33333* .91894 .000 16.2858 20.3809

formula 2 22.00000* .91894 .000 19.9525 24.0475

formula 3 17.00000* .91894 .000 14.9525 19.0475

formula 4 9.00000* .91894 .000 6.9525 11.0475


6. Antioksidan

Oneway

ANOVA

Antioksidan

Sum of Squares Df Mean Square F Sig.

Between Groups 162.783 5 32.557 389.582 .000

Within Groups 1.003 12 .084

Total 163.786 17

45

Post Hoc Test

Multiple Comparisons

Dependent Variable:antioksidan


Mean

Difference (I-

J) Std. Error Sig.


Lower Bound

Upper

Bound

Tukey HSD formula 1 formula 2 6.06333* .20929 .000 5.3603 6.7663

formula 3 -4.23333* .20929 .000 -4.9363 -3.5303

formula 4 1.13667* .20929 .002 .4337 1.8397

formula 5 -1.18000* .20929 .001 -1.8830 -.4770

ekstrak 1.19667* .20929 .001 .4937 1.8997

formula 2 formula 1 -6.06333* .20929 .000 -6.7663 -5.3603

formula 3 -10.29667* .20929 .000 -10.9997 -9.5937

formula 4 -4.92667* .20929 .000 -5.6297 -4.2237

formula 5 -7.24333* .20929 .000 -7.9463 -6.5403

ekstrak -4.86667* .20929 .000 -5.5697 -4.1637

formula 3 formula 1 4.23333* .20929 .000 3.5303 4.9363

formula 2 10.29667* .20929 .000 9.5937 10.9997

formula 4 5.37000* .20929 .000 4.6670 6.0730

formula 5 3.05333* .20929 .000 2.3503 3.7563

ekstrak 5.43000* .20929 .000 4.7270 6.1330

formula 4 formula 1 -1.13667* .20929 .002 -1.8397 -.4337

formula 2 4.92667* .20929 .000 4.2237 5.6297

formula 3 -5.37000* .20929 .000 -6.0730 -4.6670

formula 5 -2.31667* .20929 .000 -3.0197 -1.6137

ekstrak .06000 .20929 1.000 -.6430 .7630

formula 5 formula 1 1.18000* .20929 .001 .4770 1.8830

formula 2 7.24333* .20929 .000 6.5403 7.9463

formula 3 -3.05333* .20929 .000 -3.7563 -2.3503

formula 4 2.31667* .20929 .000 1.6137 3.0197

ekstrak 2.37667* .20929 .000 1.6737 3.0797

46

ekstrak formula 1 -1.19667* .20929 .001 -1.8997 -.4937

formula 2 4.86667* .20929 .000 4.1637 5.5697

formula 3 -5.43000* .20929 .000 -6.1330 -4.7270

formula 4 -.06000 .20929 1.000 -.7630 .6430

formula 5 -2.37667* .20929 .000 -3.0797 -1.6737


formula 3 -4.23333* .20929 .000 -4.6893 -3.7773

formula 4 1.13667* .20929 .000 .6807 1.5927

formula 5 -1.18000* .20929 .000 -1.6360 -.7240

ekstrak 1.19667* .20929 .000 .7407 1.6527

formula 2 formula 1 -6.06333* .20929 .000 -6.5193 -5.6073

formula 3 -10.29667* .20929 .000 -10.7527 -9.8407

formula 4 -4.92667* .20929 .000 -5.3827 -4.4707

formula 5 -7.24333* .20929 .000 -7.6993 -6.7873

ekstrak -4.86667* .20929 .000 -5.3227 -4.4107

formula 3 formula 1 4.23333* .20929 .000 3.7773 4.6893

formula 2 10.29667* .20929 .000 9.8407 10.7527

formula 4 5.37000* .20929 .000 4.9140 5.8260

formula 5 3.05333* .20929 .000 2.5973 3.5093

ekstrak 5.43000* .20929 .000 4.9740 5.8860

formula 4 formula 1 -1.13667* .20929 .000 -1.5927 -.6807

formula 2 4.92667* .20929 .000 4.4707 5.3827

formula 3 -5.37000* .20929 .000 -5.8260 -4.9140

formula 5 -2.31667* .20929 .000 -2.7727 -1.8607

ekstrak .06000 .20929 .779 -.3960 .5160

formula 5 formula 1 1.18000* .20929 .000 .7240 1.6360

formula 2 7.24333* .20929 .000 6.7873 7.6993

formula 3 -3.05333* .20929 .000 -3.5093 -2.5973

formula 4 2.31667* .20929 .000 1.8607 2.7727

ekstrak 2.37667* .20929 .000 1.9207 2.8327

ekstrak formula 1 -1.19667* .20929 .000 -1.6527 -.7407

47

formula 2 4.86667* .20929 .000 4.4107 5.3227

formula 3 -5.43000* .20929 .000 -5.8860 -4.9740

formula 4 -.06000 .20929 .779 -.5160 .3960

formula 5 -2.37667* .20929 .000 -2.8327 -1.9207


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