3Stantec - Government of Nova Scotia

Source Emissions Testing —

Recovery Boiler and PowerBoiler, Winter 2015

3 StantecPrepared for:Northern Pulp Nova ScotiaCorporationP.O. Box 549, Station MainNew Glasgow, NS B2H 5E8

Prepared by:Stantec Consulting Ltd.102-40 Hightield Park DriveDartmouth, NS B3A 0A3

Project No. 121413456

April 10, 2015

SOURCE EMISSIONS TESTING — RECOVERY BOILER AND POWER BOILER, WINTER 2015

TABLE OF CONTENTS

EXECUTIVE SUMMARY II

1.0 INTRODUCTION 1

2.0 OVERALL APPROACH 1

2.1 SUBMISSION OF PRE-TEST PLAN2.2 ON-SITE SOURCE EMISSIONS TESTING 2

2.3 INFORMATION REVIEW AND REPORTING 2

3.0 TEST METHODS, EQUIPMENT, AND CALIBRATIONS 3

3.1 SAMPLING PROCEDURES AND EQUIPMENT 33.1.1 Total Particulate Matter 33.1.2 Combustion Gases 5

3.2 QUALITY ASSURANCE AND QUALITY CONTROL 5

4.0 RESULTS AND DISCUSSION 6

4.1 EXHAUST STACK SAMPLE LOCATION DETAILS 6

4.2 RECOVERY BOILER 7

4.3 POWER BOILER 9

4.4 SUMMARY OF RESULTS 10

5.0 CLOSURE 10

LIST OF TABLES

TableE.1 Summary of Scope HTable 2.1 Source Emissions Testing Matrix 2Table 4.1 Sample Location Details 6Table 4.2 Source Testing Results - Recovery Boiler - Particulate Matter 7

Table 4.3 Source Testing Results - Recovery Boiler - Combustion Gases 8Table 4.4 Source Testing Results - Power Boiler - Particulate Matter 9

Table 4.5 Source Testing Results - Power Boiler - Combustion Gases 10

LIST OF FIGURES

Figure 3.1 Source Emissions Testing Methad 5 Sampling Train 4

List of Appendices

Appendix A Pre-test PlanAppendix B Calibration DataAppendix C Field Data SheetsAppendix D Calculations

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SOURCE EMISSIONS TESTING — RECOVERY BOILER AND POWER BOILER, WINTER

EXECUTIVE SUMMARY

Northern Pulp Nova Scotia Corporation, referred to herein as Northern Pulp, retained StantecConsulting Ltd. to conduct source emissions testing at the Kratt pulp mill in New Glasgow. NovaScotia. Source emis5ions testing were conducted on the Recovery Boiler and the Power Boiler tofulfill the conditions specified in the current Certificate of Approval to Operate (C0A) 20 11-076657-R03. The source emissions testing campaign was performed according to the pre-testplan submitted to the Nova Scotia Department of Environment. The testing was conductedduring the week of March 9th, 2015.

In this report, source emissions testing data are presented for measurements which includecombustion gases and total particulate matter (PM) as well as exhaust gas temperature,exhaust flaw rate, moisture content, velocity, and volumetric flow rate. The scope of work forthe testing campaign is summarized in Table E.1.

Table E.1 Summary of Scope

Number ofSource Samples per Parameter Sampling Method

Source

. 3 Total Particulate Matter (PM) EPS 1 /RM/8Recovery Boiler3 Combustion Gases EPS L’RM/lS

. 3 Tatal Particulate Matter (PM) EPS 1 /RM/8Power Boiler3 Combustion Gases EPS 1 /RM/ I 5

The average measured concentration of PM from the Power Boiler was 155 mgIRm3 (correctedto 11% 02), which is above the respective regulatory stack limit of 150 mg/Rm3 presented inTable 1 of the facility’s Approval. The measured concentration of PM from the Recovery Boilerwas 833 mg/Rm3 (corrected to 11% 02), which is above the regulatory limit of 375 mg/Rm3presented in Table 1 of the facility’s Approval.

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1.0 INTRODUCTION

Northern Pulp Nova Scotia Corporation, referred to herein as Northern Pulp, retained Stantec

Consulting Ltd. (Stantec) to conduct source emissions testing at the Kraft pulp mill in New

Glasgow, Nova Scotia. Source emissions testing were conducted on the Recovery Boiler and the

Power Boiler. The source emissions testing campaign was performed according the pre-test plan

submitted on February 23d, 2015 to the Nova Scotia Department of Environment, following

methods published by the United States Environmental Protection Agency and Environment

Canoda. The testing was conducted during the week of March 91h, 2015.

In this report, source emissions testing data are presented for combustion gases (oxygen, carbon

dioxide, nitrogen oxides, sulphur dioxide, and carbon monoxide), total particulate matter (PM),

exhaust gas temperature, exhaust flow rate, moisture content, velocity, and volumetric flow

rate.

This report is in five sections. Section 1 contains the introduction and the scope of work for the

project. The study approach and a brief description of the various parts of the project are in

Section 2. Section 3 contains a brief description of the testing methodologies, equipment, and

calibration techniques used during the source emissions testing program. In Section 4, the results

of the source emissions testing are presented and discussed, and concluding remarks are

presented in Section 5. Appendices A through D contain supporting information for the report.

2.0 OVERAll APPROACH

The project consisted of five parts:

1. Submission of the Pre-test Plan:

2. Site Preparation and Preliminary Survey;

3. On-site Source Emissions Testing;

4. Laboratory Analysis; and

5. Information Review and Reporting.

Each of these parts is described below.

2.1 SUBMISSION OF PRE-TEST PLAN

The on-site testing was conducted in accordance with the Pre-Test Plan submitted on February

23’d, 2015 to Nova Scotia Environment (NSE). The Pre-Test Plan outlined the contaminants to be

tested, as well as the methodologies proposed for conducting the source testing on the exhaust

stacks. Appendix A provides a copy of the plan.

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2.2 ON-SITE SOURCE EMISSIONS TESTING

Stantec set up the source emissions testing equipment and conducted a preliminary survey tomeasure the exhaust gas temperature, velocity, and flue gas composition for those sourcesrequiring particulate testing. The data from this survey was used to determine the appropriatenozzle size to conduct isokinetic sampling (where the velocity of the gas entering the nozzle isequal to the gas velocity in the stack) for particulate matter sampling.

Three (3) tests for total particulate matter were conducted at defined sampling locations withinthe cross-section of the exhaust stacks of the Recovery Boiler and the Power Boiler. Three testsfor combustion gases were also conducted, near the centre of the exhaust stacks of theRecovery Boiler and the Power Boiler. All testing was completed in compliance with thesampling methods presented in Table 21, in accordance with the Air Quaflty Regulation, underthe Environment Act, Section 112 issued by Nova Scotia Environment (NSF) and the requirementsof the facility’s approval (201 1-076657-R03) issued by the NSF.

The methodologies used for testing the emissions from each exhaust stack are summarized inTable 2.].

Table 2.1 Source Emissions Testing MatrixNumber of ApprovalSource Samples per CondItIon Parameter Sampling Method

Source

. 3 6. a) Total Particulate MatterEPS 1 JRM/BRecovery Boiler (PM)

3 - Combustion Gases EPS ]/RM/]5Total Particulate Matter

. 3 6. al EPS 1 /RM/8Power Boiler 1PM)3 - Combustion Gases EPS ]/RM/]5

2.3 INFORMATION REVIEW AND REPORTING

The data collected in the field, along with data from the laboratory analyses, were entered intothe Stantec’s source emissions testing spreadsheets for analysis. Emissions calculations were thenperformed to produce the detailed source emissions testing information. Spreadsheetcalculations were verified by hand, and numerous spot checks of spreadsheet formulas wereconducted to ensure the accuracy of data. Summary tables were prepared and incorporatedinto this report for submission to Northern Pulp.

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3.0 TEST METHODS, EQUIPMENT, AND CALIBRATIONS

This section contains a description of the methods and equipment used to conduct the source

emissions testing campaign. The calibration procedures used to ensure the quality of the source

emissions testing data are also summarized in this section.

3.1 SAMPLING PROCEDURES AND EQUIPMENT

The following sub-sections contain brief descriptions of the sampling equipment and

methodologies used during the source emissions testing campaign.

3.1.1 Total Particulate Mailer

Particulate matter emissions from the exhaust stacks were measured in accordance with the

Environment Canada Reference Method EPS 1/RM/8, entitled Reference Methods for Source

Testing: Measurement of Releases of Particulate from Stationary Sources.

The sampling train, used specifically for isokinetic sampling of particulate matter, is described in

detail in EPS 1/RM/B, and is generally referred to as the ‘Method 5’ sampling train for particulate

matter, named after the United States Environmental Protection Agency (US EPA) protocol. The

sampling train consists of several different components which include: a heated sampling probe

(a nozzle, stainless steel liner, thermocouple, and pitot tube assembly), a heated sample case

containing a filter, an ice box containing impinger glassware, and an umbilical card leading to

the pump and control console. A schematic of the sampling system is shown in Figure 3.1. The

operation of the Method 5 sampling train can be generally described as follows.

Exhaust gases are drawn through the probe nozzle at or near isokinetic conditions (i.e., where

the gas velocity in the nozzle is at the same velocity as the gas in the stack). The gases are then

drawn through the inner stainless steel liner of the electrically heated sampling probe to the

other components of the sampling train.

A pitot tube assembly is attached to the probe next to the nozzle to measure the exhaust gas

velocity in the area of the probe nozzle. Using the differential pressure reading on the control

console, the desired nozzle flow rate is determined from the differential pressure across a

calibrated orifice.

The exhaust gases are drawn from the probe liner through a pre-weighed glass fiber filter, in the

hot side of the sampling unit, and then through pre-weighed impingers in an ice bath to cool the

gases and condense the moisture in the gas, before the gas enters the umbilical cord.

The umbilical cord carries the filtered, cooled exhaust gases from the sampling site to the control

console. The control console contains a fiber vane vacuum pump, which is used to draw the

exhaust gases through the sampling train. A calibrated dry gas meter records the volume of gas

sampled.

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SOURCE EMISSIONS TESTING — RECOVERY BOILER AND POWER BOIlER, WINTER 2015

After completion of testing, the impingers are re-weighed, with the difference in moss

corresponding to the mass of water collected. This measurement is used to calculate the

moisture content of the exhaust gas.

Prior to the particulate matter testing, filters were conditioned and pre-weighed. Following the

testing, particulate mailer was recovered from the nozzle, the sampling probe and the in-line

filter. Following testing, the filter containing the particulate sample, was conditioned and

weighed, and the net weight of the collected particulate matter was determined. After each

test, the probe and nozzle were rinsed with acetone and this acetone was collected, placed

into a pre-weighed container and evaporated until dry. The amount of particulate for each

part of the sample was determined gravimetrically, and the mass of particulate matter

collected for each test was calculated as the sum of the particulate matter collected in the

filter, probe, and nozzle rinse. The contents of the water filled impingers were also recovered

gravimetrically for particulate matter and reported separately as requested by the NSF. These

recoveries were performed at Stantec’s laboratory in Fredericton, New Brunswick. Appendix B

contains the equipment calibration data.

3.1.2 Combustion Gases

The combustion gases (02, C02, CO. NOx, and 502) from the boilers were sampled according to

the Environment Canada reference method EPS 1/RM/15, entitled Reference Method for the

Monitoring of Gaseous Emissions from Fossii Fue-flred Burners. In this method, samples of flue gas

are drawn through a probe, non-isokinetically, from a single point near the centre of the stack.

An FNFRAG Model 500 Micro-Fmission Analyzer, manufactured by ENFRAC Inc., was used to

conduct the sampling. The Model 500 is equipped with a flue gas probe that has an integrated

filter trap and condensate trap, and a housing unit that contains the pump and the

electrochemical cells which are used to measure concentrations of sulphur dioxide, nitrogen

oxides, carbon monoxide, carbon dioxide, and oxygen. The ENERAC Model 500 Micro-Emission

Analyzer is manufactured and calibrated to confirm accuracy. Calibration data is included in

Appendix B.

3.2 QUALITY ASSURANCE AND QUALITY CONTROL

Throughout the source emissions testing program, quality assurance and quality control

procedures were applied to ensure the collection of reliable and accurate emissions data.

Quality control checks were performed at several stages during the testing program to ensure

the collection of representative samples and the generation of valid results.

The Quality Control (QC) checks included the following:

• use of standardized checklists and field notebooks to ensure completeness, traceability, and

comparability of the process information and samples;

• field checking of standardized forms by a second person to ensure accuracy and

completeness;

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• strict adherence to sample chain-of-custody procedures:

• testing for cyclonic or reverse flow, as well as stratified flow conditions: and

• leak checks of sampling train.

Equipment was calibrated according to the protocols and schedule as prescribed by NSF,Fnvironment Canada. and the US FPA. These calibrations include the following:

Pilots: Calibrated in a wind tunnel with probe and nozzles attached.

Gas meters: Calibrated using a critical orifice calibration set.

Nozzle: Four diameter measurements made using a micrometer across the sharpened edges.

Thermocouples: Calibrated using a potentiometric technique.

Gas Analyzers: Calibrated against reference gases using standard calibration gases within theexpected range of concentrations from the source.

Calibration data are in Appendix B of this report.

4.0 RESULTS AND DISCUSSION

The results of the source emissions testing campaign are provided and discussed in this section.

Appendices B through D contain supporting information including calibration information, fielddata sheets, and calculations.

4.1 EXHAUST STACK SAMPLE LOCATION DETAILS

Table 4.1 provides a summary of the sample location details for each exhaust stack sampled.

Table 4.1 Sample Location Details

Parameter Recovery Boiler Power BoilerStack Height—Above Grade (ni) 69 51Stack Diameter at Sampling Ports (m) 3.51 1.93Stack/Duct Description Circular CircularStack Orientation Verticol VerticalNumber of Sample Ports 4 2Sample Port Diameter (m) 0.1 0.1Location Upstream from any Disturbance >2 >2Location Downstream from any Disturbance 1.45 >4Ideal or Non Ideal Flow Characteristics at The Sample

Non Ideal Non IdealLocation’

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Table 4.1 Sample Location Details

Parameter Recovery Boiler Power Boiler

Total Number of Sample Points for PM 24 24

Number of Sample Points per Traverse for PM 12 12

Sample lime per Point for PM (mm) 5 5

Sample time per Test for PM (mm) 120 120

Sample time per Test for TRS (mm) NA NA

Sample time per Test for gases (mm) 30 30

Diameter confirmed while testing during the week of March 91h

4.2 RECOVERY BOILER

The results of the source emissions testing for total particulate matter and combustion gases from

the Recovery Boiler exhaust stack are in Tables 4.2 and 4.3, respectively.

Table 4.2 Source Testing Results - Recovery Boiler - Particulate MatterStack

Emission LimitParameter Test #1 Test #2 Test #3 Average (Table 1 of

Approval)

Test Date Mar. 10, 2015 Mar, 10, 2015 Mar. 11, 2015 - -

Test Start 9:00 AM 12:15 PM 9:20 AM - -

Test Duration (mm) 120 120 120 120 -

Volume of Gas Sampled(Rm3) 1.8? 1.87 1.75 1.8? -

Average Isokineticity (%) 105 102 104 103 -

Total Volume of MoistureCollected in Impingers -

(mL) 540 542 541 541

Particulate Matter FromFilter and Probe Wash 1mg) 2,474 2,779 2,220 2,491 -

Particulate Matter FromImpingers (mg) 1.94 4.54 3.27 3.25 -

Exhaust Gas Parameters

Exhaust Gas Temperature(°C) 67.6 67.8 63.9 66.4 -

Exhaust Gas MoistureContent (%) 28.9 28.3 29.5 28.9 -

Exhaust Gas Velocity (mIs) 13.7 14.5 13.7 14.0 -

Exhaust Gas VolumetricFlow Rate (Rm3/s) 83.3 88.6 81.7 84.6 -

Oxygen - 02 (%) 4.80 4.50 4.39 4.56 -

Carbon Dioxide - C02 (%) 1 5.6 15.9 1 6.1 15.9 -

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Table 4.2 Source Testing Results - Recovery Boiler - Particulate Mailer

StockEmIssion UmitParameter Test #1 Test #2 Test #3 Average

(Table 1 ofApproval)

Total Particulate Matter -

PMConcentration at 11% 02(mg/Rm3) 842 898 759 833 375*

Emission Rate (kg/hr) 411 474 373 419 -

Legend:Degrees Celsius.

mis Metres per second.Rm3/s Dry cubic metres per second at reference conditions (25°C and 101.3 kPa).mg/Rm3 Milligrams per dry cubic metre at reference conditions (25°C and 101.3 kPa).kgihr Kilograms per hour.For the period between the issuance of Approval No.201 l-076657-R03 and the commissioning of the recovery boiler

precipitator system, the particulate emission limit for the Recovery Boiler is 375 mg/Rm3.

The average measured concentration of particulate matter was 833 mg/Rm3 (corrected to 11%02). which is above the stack emission limit of 375 mgIRm3 presented in Table 1 of the facility’sApproval.

Table 4.3 Source Testing Results - Recovery Boiler - Combustion GasesParameter Test #1 Test #2 Test #3 Average

Test Date Mar. 10, 2015 Mar. 10, 2015 Mar. 11, 2015 -

Test Duration (mm) 30 30 30 30Exhaust Gas VolumetricFlow Rate (Rm3/s) 83.3 88.6 81.7 84.6Sulphur Dioxide - 502Concentrotion (ppm) 8.14 6.14 27.9 14.0Concentration (mgiRm2) 13.1 9.72 43.8 22.2Emissions Rate (kg/hr) 6.40 5.14 21.5 11.0Nitrogen Oxides - NOConcentration (ppm) 23.7 46.1 52.1 40.7Concentration (mg/Rm3) 27.4 52.4 58.8 46.2Emissions Rate (kg/hr) 1 3.4 27.7 28.9 23.3Carbon Monoxide - COConcentration (ppm) 1,772 2,817 3,083 2558Concentration (mg/Rm3) 1,248 1,947 2.116 1770Emissions Rate (kg/hr) 609 1 .029 1 .039 892Legend:Rr&/s Dry cubic metres per second at reference conditions (25°c and 101.3 kra).mg/Rm3 Milligrams per dry cubic metre at reference conditions (25°C and 101.3 kro).kg/hr Kilograms per hour.NA Not Applicable

The emission rates for SO2. NO and CO for the Recovery Boiler were 11.0kg/hr. 23.3 kg/hr and892 kg/hr. respectively.

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4.3 POWER BOILER

The results of the source emissions testing for total particulate matter and combustion gases from

the Power Boiler exhaust stack are in Tables 4.4 and 4.5. respectively.

Table 4.4 Source Testing Results - Power Boiler- Particulate Mailer

StackEmission Limit

Parameter Test #1 Test #2 Test #3 Average(Table 1 ofApproval)

T tD tMar. 10, Mar.11, Mar.11,

es ae 2015 2015 2015 - -

Test Start 8:47 AM 1 2:00 PM 2:52 PM - -

Test Duration (mm) 1 20 1 20 I 20 1 20 -

Volume of Gas Sampled (Pm3) 1 .50 1 .34 1 .48 1 .44 -

Average Isokineticily (%) 107 108 105 106 -

Total Volume of Moisture -

Collected in Impingers (mL) 291 260 285 278

Particulate Matter From Filter andProbe Wash (mg) 220 239 229 229 -

Particulate Matter From Impingers -

1mg) 4.8 3.0 4.2 4.0

nExhaust Gas Temperature 1°C) 64.7 65.1 63.9 64.6 -

Exhaust Gas Moisture Content (%) 20.8 20.8 20.7 20.8 -

Exhaust Gas Velocity (mIs) 18.9 17.1 19.1 18.4 -

Exhaust Gas Volumetric Flow Rate(Rm3/s) 38.2 34.4 38.5 37.0 -

Dxygen-02 (%) 10.8 11.4 97 10.6 -

Carbon Dioxide - CO2 (%) 9,79 9.26 I 1.0 10.0 -

Total Particulate Matter - PM

Concentration at 11% 02

(mg/Pm3) 143 185 137 155 150

Emission Rate (kglhr) 20.1 22.1 21.5 21.2 -

Legend:°C Degrees celsius.rn/s Metres per second.Rm3/s Dry cubic metres per second at reference conditions (25°c and 101.3 kPa).mg/Pm3 Milligrams per dry cubic metre at reference conditions (25°c and 101.3 kPo).kg/hr Kilograms per hour.ND Non-delectable

The overage measured concentration of particulate matter (corrected to 11% 02) was 155

mg/Pm3, which is slightly above the stack emission limit of 150 mg/Pm3 presented in Table 1 of

the facility’s Approval (No. 201 l-076657-R02J. Only one out of the three tests was above the

limit.

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Table 4.5 Source Testing Results - Power Boiler - Combustion GasesParameter test #1 1 Test #2 Test #3 Average

TestDate Mor.10,2015 Mar.11,2015 Mar.l1,2015 -

Test Duration (mm) 30 30 30 30Exhaust Gas Volumetric FlowRate (Rm3/s) 38.2 34.4 38.5 37.0Sulphur Dioxide - SO2Concentration (ppm) ND ND ND NDConcentration (mg/Rm3) ND ND ND NDEmissions Rate (kg/br) ND ND ND ND

Nitrogen Oxides - NOConcentration (ppm) 16.1 21.0 26.3 21.1Concentration (mg/Rm33 29.7 41.0 43.7 38.1Emissions Rate (kg/hr) 4.18 4.89 6.86 5.31Carbon Monoxide - COConcentration (ppm) 1,734 2,079 1,936 1,916Concentration (mg/Rm3) 1,940 2,470 1,960 2,123Emissions Rate (kg/hr) 273 295 307 292Legend:Rm/s Dry cubic metres per second at reference conditions (25CC and 101.3 kPa).mg/Rm3 Milligrams per dry cubic metre al reference conditions (25CC and 101.3 kPoj.kg/hr Kilograms per hour. -I

The overage emission rates of NOx and CO from the Power Boiler were 5.31 kg/hr and 292 kg/hr.respectively. No 502 was detected.

4.4 SUMMARY OF RESULTS

Currently there ore specified regulatory limits in the facility’s approval (201 1-076657-R03) foremissions of PM for the Recovery Boiler and the Power Boiler. The measured concentration ofPM from the Power Boiler was slightly above the regulatory stack limit. The measuredconcentration of PM from the Recovery Boiler was above its respective regulatory limit.

5.0 CLOSURE

This report has been prepared for the sole benefit of Northern Pulp Nova Scotia Corporotion. Thisreport may not be relied upon by any other person or entity without the express written consentof Stantec and Northern Pulp Nova Scotia Corporation. Any use of this report by a third party, orany reliance on decisions made based upon this report, ore the responsibility of the third party.Stantec accepts no responsibility for damages, if any, suffered by any third party as a result ofdecisions made or actions based an this report.

Stontec makes no representation or warranty with respect to this report, other than the work wasundertaken by trained professional and technical staff in accordance with generally acceptedengineering and scientific practices current at the time the work was performed. Any

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information or facts provided by others and referred to or utilized in the preparation of this report

was assumed by Stantec to be accurate.

This study was undertaken exclusively for the purpose outlined herein ond was limited to those

contaminants and sources specifically referenced in this report. It should be noted that the

measurements were taken over a relatively short time period on-site, and the emissions results

may be considered representative only for the conditions present at the time of testing. This

report cannot be used or applied under any circumstances to another location or situation or for

any other purpose without further evaluation of the data and related limitations.

This report was developed by Gillion Hatcher, M.A.Sc. and reviewed by Vicki Corning, P.Eng. and

Mark Scaplen, P.Fng.

If you have any questions regarding the contents of ihis report, or require any additional

information, please do not hesitate to contact the undersigned.

hwmYalckc)

Gillian Hatcher, M.A.Sc. Vicki Corning, P.Eng.

Project Manager Associate, Environmental Services

Tel: (902) 468-7777 Tel: (506) 452-7000

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Appendix APie-test Plan

Stantec

Stanlec Consulting Ltd.102 - 40 Highfield Park DriveDartmouth NS B3A 0A3Tel: (902) 468-7777Stantec Fax: (902) 468-9009

February 20, 2015FUe: 121413456

Attention: Mr. Marc TheriauliNova Scotia Environment20 Pumphouse RoadPictou, NS B2H 5C6

Dear Mr. Theriault,

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp,Pictou Mill —2015 Calendar Year

Please accept this Pre-test Plan for the completion of source emissions required at the Pictou Mill in

New Glasgow, Nova Scotia for the 2015 calendar year.

Introduction

Northern Pulp is required to perform source emissions testing on the Recovery Boiler, Ume Kiln,

Smelt Dissolving Tank, Power Boiler and the High Level Roof Vent to fulfil the conditions specified in

the current Certificate of Approval (C0A) to Operate 201 1-076657-R03. The required annual

testing for 2015 consists of:

• Recovery Boiler and Power Boiler particulate matter testing 4 times per year;

• Lime Kiln and Smelt Dissolving Tank particulate matter testing 2 times per year;

• Ume Kiln, High Level Roof Vent and Smelt Dissolving Tank total reduced sulphur (TRS) testing 2

times per year;

• One PM2S testing event per year on the four stacks noted above for particulate matter; and

• One Chlorine (Cl) and Chlorine Dioxide (CIO2) event per year on the bleach plant exhaust

(High Level Roof Vent being the source of these emissions).

Test Program Organization

The source emissions testing will be performed for:

Company Name: Northern PulpCompany Address: P.O. Box 549, Station Main, New Glasgow, NS, B2H 5E8Contact Name:Position: Environmental/Technical LeaderTelephone Number: (902) 752-8461[mail: &northernpulp.com

Design with commLnity n mind

c3February 20, 2015Mr. Marc TheriaultPage2of 12

Reference: Pre-Test Plan for Source EmIssIons Testing Northern Pulp,Pictou Mill —2015 Calendar Year

Sampling Company: Stantec Consulting Ltd.Project Manager: Gillian HatcherTelephone Number: (902) 468-7777Fax Number: (902) 468-9009Email: Stantec.comKey Sampling Team:

. (withsupport from other staff as needed)

Source Emissions Testing Program

The proposed source emissions testing methodology and proposed sampling timeframes arepresented in Table 1.

Table 1 Source Emissions Testing Matrix

NumberNumberSource of Tests Parameter SamplIng Method Proposed Tlmeframeof Visitsper_Visit

Total Particulate Winter, Spring,4 3 EPS 1 /RM/8Matter (PM) Summer, FallRecoveryWinter, Spring,Boiler 4 3 Combustion Gases EPS 1/RM/15Summer, Fall

1 3 Particle Size Analysis Microscopic technique FallTotal Particulate Winter, Spring,4 3 EPS 1/RM/8Molter (PM) Summer, FallPower

Winter, Spring,Boiler 4 3 Combustion Gases EPS 1/RM/15Summer, Fall

1 3 Particle Size Analysis Microscopic technique FallTotal Particulate2 3 EPS 1 /RM/8 Spring, FallMatter_(PM)

2 3 Combustion Gases EPS 1/PM/is Spring, FallLime Kiln1 3 Particle Size Analysis Microscopic technique Fall

Total Reduced2 3 US EPA Method 1 6B/C Spring, FallSulphur_(TRS)Total Particulate2 3 EPS 1 /RM/8 Spring, FallMatter_(PM)

Smelt 2 3 Combustion Gases EPS 1/RM/15 Spring, FallDissolving1 3 Particle Size Analysis Microscopic technique FallTank

Total Reduced2 3 US EPA Method 1 6B/C Winter, SummerSulphur_(TRS)

Total ReducedHigh Level 2 3Sulphur (TRSI

US EPA Method 16B/C Spring, FallRoof Vent

2 3 Combustion Gases EPS 1/RM/15 Spring, Fall

Design wilh community in mind

3February 20, 2015

Mr. Marc Theriault

Page3of 12

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp.Plctou MllI—2015 Calendar Year

Table 1 Source Emissions Testing Matrix

NumberNumber

Source of Tests Parameter Sampling Method Proposed Tlmeframeof Visits per Visit

Chlorine and NCASI Special Report 91-1 3

chlorine dioxide 07Spring

Note:Timeframes are as follows based on the approval deadfines-Winter: January-March 31, 2015, Spring: April — June 30, 2015,

Summer: July-September 30, 2015, FoIl: October-December 31 2015

Details of each of the methods identified in Table I, in addition to the preliminary testing

methodology, are provided in the sections that follow.

Preliminary Testing: Upon arrival at each sampling location, Stantec will setup the source emissions

testing equipment and conduct a preliminary survey to measure the average velocity, flue gas

composition, and moisture content in the stack gases using EPS 1 /RM/8 Methods B, C, and D,

respectively. The data from this survey will be used to determine the appropriate nozzle size to

conduct isokinetic sampling (where the velocity of the gas entering the nozzle is equal to the gas

velocity in the stack) for particulate matter during the official testing part of the work. Verification for

cyclonic or reverse flow will also be conducted during the preliminary survey, according to

procedures outlined in the Environment Canada reference method [PS 1 /RM/8.

Should fluctuations in the velocity pressure at a selected traverse point exceed 20% of the

average pressure for that point; the diameter of the testing cross section will be reduced to

include only those areas along the traverse which meet this requirement (less than 20% of the

average). Although the diameter maybe reduced, the number of sampling points along each

traverse will remain the same as determined from [PS 1 /RM/8, Method A, using the equivalent

diameter.

Volumetric flow and exhaust gas emissions will be calculated using the full cross sectional area.

Particulate Matter: The source emissions testing of the Recovery Boiler, Lime Kiln, Smelt Dissolving

Tank, and the Power Boiler for total particulate matter will be conducted in accordance with the

Environment Canada reference method EPS 1 /RM/8, entitled “Measurement of Releases of

Particulate from Stationary Sources”. In addition the alignment approach, as specified in the US

EPA Guidance Document — GD-00B, will be applied when source testing the Lime Kiln due to the

cyclonic flow this source exhibits.

The particulate sampling train, used specifically for isokinetic sampling, is described in detail in EPS

1/RM/8, and is generally referred to as the “Method 5’ sampling train for particulate matter (after

the US EPA protocol). The sampling train has several different components which include: aheated sampling probe (a nozzle, stainless steel liner, thermocouple, and pitot tube assembly), a

heated sample case containing a filter, an ice box containing impinger glassware, and on

Design wilh community In mind

February 20, 2015Mr Marc TheriaultPage 4 of 12

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp.Plctou MIII —2015 Calendar Year

umbilical cord leading to the pump, and control console. A schematic of the sampling system isshown in Figure 1.

For all source tests, leak checks of the sampling train will be performed as per accepted US EPAand Environment Canada methods. For each official test, two (2) traverses with up to twelve (12)sampling points per traverse will be used. Sampling will be conducted for five (5) minutes persampling paint, up to a maximum sampling time of 120 minutes per test.

The amount of material caught in the impingers will be determined grovimetrically and reportedseparately from the calculated total particulate matter emissions. All particulate matter sampleswill be recovered and analyzed at the Stantec laboratory in Fredericton, NB.

Microscopic Analysis (Fine Particulate, PM2.s): As per the facility’s Industrial Approval to Operate.the Environment Canada EPS 1 /RM/55 or an alternative method acceptable to the Department isrequired for PM2.5 testing. As the method quoted in the approval is not valid for stacks withpotential for entrained water droplets in the exhaust (which applies to boilers and dissolving tankat Northern) or cyclonic flow (which applies to the Lime Kiln), we propose microscopic analysis offilters as the viable option. This method involves analysis of total particulate matter filters (collectedas described above) for fine particulate percentage.

The particle size analyses will be performed by MVA Scientific Consultants, based in Duluth, GA.using a JEOL JSM-6500F field emission scanning electron microscope operating in automatedmode under the control at a Thermo Scientific Noran System SIX x-ray analysis system, using theirautomated particle size analysis method.

Total Reduced Sulphur: The source emissions testing of the Ume Kiln, the Smelt Dissolving Tank andthe High Level Root Vent for total reduced sulphur will be conducted in accordance with US EPAMethod 1 6B. In this method, the sample is extracted from the exhaust gas of the stack through aheated Teflon line. The sample is chilled and then posses through an 502 analyzer to measure SO2from the source. The sample exits the analyzer and is then passed through a furnace where allsulphur compounds in the gas stream are thermally oxidized to SO2, this SO2 is measured in asecond inline analyzer. The difference in the initial 502 and the final 502 measurement is the totalreduced sulphur concentration (reported as H25). The analyzers are both Western Research SO2non-dispersive ultra-violet (NDUV) continuous analyzer. Monitoring will be conducted continuouslyover a 24 hour period as required by the approval condition.

Chlorine, Chlorine Dioxide (C12, dO2): Samphng will be conducted in accordance with NCASI’ssampling method which consists of the extraction of a sample bubbling through midget impingersand subsequent analysis by titration. The sampling train for the Cl2 and C102 consists of series ofthree mini impingers, connected by Teflon tubing. The first two impingers each contain 20 ml ofpotassium iodide (KI) solution buffered with potassium di-hydrogen phosphate (KH2PO4). The thirdimpinger contains silica gel to remove any remaining moisture from the gas stream. The impingersore cooled by an ice bath, and the dried gas is then drawn through the sampling train with acalibrated pump. Total sampling time for each test is sixty (60) minutes.

Design with cammunify in mind

3February 20, 2015Mr. Marc TheñaulfPage 5of 12

Reference: Pre-Test Plan br Source Emissions Testing Northern Pulp,Plctou MIII —2015 Calendar Year

Following completion of each test for C12 and Cl02, the contents of the first two impingers are

combined in a pre-cleaned beaker. Subsequent analysis via titration will be performed onsite by

Stantec. The combined impinger solutions and de-ionized water rinse of the sample line and

empty impingers would be titrated with sodium thiosulphate solution (0.010 N). The volume of

titrant required to reach the first colorless endpoint would be recorded on a recovery data form.

Five (5) ml of 10% sulphuric acid would be added to the sample and the titrotion continued. The

volume of titrant required to reach the second colorless endpoint would be recorded on a

recovery data form. These titrations would be conducted on site shortly following sampling by one

of the field staff during the testing due to the instability of the samples, which begin to degrade

after 24 hours.

Combustion Gases:

The combustion gases (02, C02, CO. NOx, and 502) will be sampled according to the Environment

Canada reference method F’S 1/RM/15, entitled Reference Method for the Monitoring of

Gaseous Emissions from Fossil Fuel-fired Burners. In this method, samples of flue gas are drawn

through a probe, nan-isokinetically, from a single point near the centre of the stack. An ENERAC

Model 500 Micro-Emission Analyzer, manufactured by ENERAC Inc., will be used to conduct the

sampling. The Model 500 is equipped with a flue gas probe that has an integrated filter trap and

condensate trap, and a housing unit that contains the pump and the electrochemicol cells which

are used to measure concentrations of sulphur dioxide, nitrogen oxides, carbon monoxide,

carbon dioxide, and oxygen.

In accordance with the regulatory requirements for compliance testing. three replicate tests for

each contaminant will be conducted on each stack.

Reporting

As per Approval No. 2011 -076657-R03, actual particulate matter emission rates will be reported in

units of g/s. The concentration released to the atmosphere will be reported in units of mg/rn3 atreference conditions of 25 °C and 101.3 kPa corrected for 11 % oxygen for the Recovery Boiler ond

Power Boiler and in units of kg/adubmt for the Lime Kiln and the Dissolving Tank. Fine particulate

matter concentrations far the Lime Kiln, Dissolving Tank, Power Boiler and Recovery Boiler will bereported in units of mg/rn3 at reference conditions of 25 °C and 101.3 kPa corrected for 11 %

oxygen. Total reduced sulphur will be reported in units of parts per million by dry volume (ppmdv).

Emission rates of chlorine and chlorine dioxide from the High Level Roof Vent will be reported in

units of g/s and the concentrations released to the atmospheric will be reported in units of mg/m3.

Results of each source emissions testing event will be documented in a final report for submission

to Nova Scotia Environment (NSE) for review and approval within 60 days of completing the

testing.

Design wilh cornmuniiy In mind

(3February 20, 2015Mr. Marc ThehaultPage 6 of 12

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp.Pictou MIII — 2015 Calendar Year

Sampling Locations

The number and location of sample points along each traverse were previously determinedaccording to EPS 1 /RM/8. Method A, using the exhaust stack diameter. A diagram of a typicalsample location is provided in Figure 2.

Figure 1 Source Emission Testing, Method 5 Sampling Train

Design wiih community In mind

February 20, 2015Mr. Marc ThehaultPage 7 of 12

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp,Picicu MIII —2015 Calendar Year

Figure 2 Source Emissions Testing, Sample Location Details

nL r.oa,

Design wilh community in mind

February 20,2015Mr. Marc TheriaultPage8af 12

Reference: Pre-Test Plan for Source Emissions resting Northern Pulp,PIctou MIII —2015 Calendar Year

A summary of the sample location details is provided in Table 2.

Table 2 Sample Location Details

PowerRecovery me

Boiler High LevelParameter Lime Kiln DissolvingBoiler Scrubber Roof VentTankStack

Stock Height — Above Grade (m) 69 37 51 51 65Diameter / Equivalent Diameter

3.51 1 .22 I .22 1 .93 1 .83

StacklDuct Description Circular Circular Circular Circular CircularStack Orientation Vertical Vertical Vertical Vertical VerticalLocation of Source Testing In Stack In Stack In Stack In Stack In StackNumber of Sample Ports 4 2 2 2 1Sample Port Diameter (m) 0.1 0.15 0.1 0.1 0.1Location Upstream from any

>2 2 >2 >2 -Disturbance,Location Downstream from any

1 45 8 6 >4 -Disturbance,Ideal or Non Ideal FlowCharacteristics at The Sample Not Ideal Not Ideal2 Nat Ideal Not Ideal -

Locatiant

1 (forTRSTotal Number of Sample Points 24 (for PM) 24 (for PM) 20 (for PM) 24 (for

and Cl,1 (for TRS) I (far TRS) PM)00’)

Number of Sample Points per12 12 10 12 NATraverse (PM sampling)

Sample lime per Point for PM5 5 5 5 NAsamples mm)

Sample time per Test for PM (mm) 120 120 100 120 NA30 (for

Sample time per Test for30 30 30 30

TRS)combustion gas (mm) 60 (for Cl,

002)Sample time per Test for TRS (mm) NA 1,440 1,440 NA 1.440‘ The exhaust gas tlaw characteristics at the sampling location are referred to as being “Ideal” ii the sample ports arelocated in a straight section of stack at east eight stack diameters downstream and two stack diameters upstream ofany flow disturbance.

2The lime kiln sampling locatian has been changed from ideal to not ideal due to the cyclanic flaw.measurement — to be confirmed during the Winter/Spring Event

Quality Assurance / Quality Control

Throughout the stack testing program, rigorous quality assurance and quality control procedureswill be applied to ensure the collection of reliable, representative, and reproducible emissionsdata. All equipment will be calibrated according to the protocols as prescribed by EnvironmentCanada, and the US EPA. These calibrations include the following:

Design with cammunity In mind

‘3February 20, 2015Mr. Marc TheriaultPage 9 of 12

Reference: Pre-Test Plan for Source Emissions Testing Northern Pulp,Pictou MIII —2015 Calendar Year

Pitots: calibrated in a wind tunnel with probe and nozzles attached;Gas meters: calibrated against a critical orifice set;Thermocouples: calibrated using a potentiometric technique:Nozzle: four diameter measurements made using a micrometer across the

sharpened edges: andCombustion Gas Analyser: 2 point calibrations using span gases of known concentrations.

Calibration data will be provided in the final report.

Quality control checks will be performed at several stages during the testing program to ensure

the collection of representative samples and the generation of valid results. These checks oreperformed by test personnel throughout the program under the guidance of the source testingcrew chief. The Quality Control (QC) checks include the following:

• Use of standardized checklists and field notebooks to ensure completeness, traceability, ond

comparability of the process information and samples collected;

• Field checking of standardized forms by a second person to ensure accuracy andcompleteness;

• Strict adherence to sample chain-of-custody procedures;

• Use of appropriate field blanks (e.g., filter and solution samples); and

• Leak checks of sample trains.

All internal quality assurance and quality control procedures will be strictly adhered to during alltest programs to ensure the production ot useful and high quality data throughout the course ofthe program.

Qualifications of Source Testing Team

The successful completion of this project requires the skills of competent and experienced

professionals who have a strong commitment to complete the project quickly and efficiently andto produce high quality results. The source testing team we have assembled to meet the

challenges of this assignment consists of highly trained professionals who bring a broad range of

expertise and experience to the project. The following paragraphs provide brief descriptions ofthe qualifications of the source emissions testing team:

Senior Reviewer:

Design with community in mind

February 20, 2015Mr. Marc TherjaultPage lOaf 12

Reference: Pre-rest Plan for Source Emissions Testing Northern Pulp,Pictou MHI—2015 Calendar Year

Project Manager and Report Writer:

Destgn with community in mind

February 20, 2015Mr. Marc ThehaultPage 11 of 12

Reference: Pre-test Plan for Source Emissions Testing Northern Pulp,Plctou Mill —2015 Calendar Year

Source Testing Team:

Schedule

Table 3 provides an overview at the proposed schedule to complete the testing, as described inthe above sections, for the 2015 calendar year. Stantec will confirm actual test dates, in writing,with NSE within thirty days prior to the testing commencing.

Currently we are proposing to conduct the winter testing event within the week of March 9th,


<3February 20, 2015Mr. Marc TheriaultPage l2of 12

Reference: Pre-Test Plan for Source Emissions TestIng Northern Pulp.P(ctou MIII —2015 Calendar Year

Table 3 Proposed Schedule

Event Proposed Date ScopeWinter

February-March 31 (March 9th week)Recovery and Power Boiler PM, gases,dissolving tank TRS

SpringApril-June 3Q Recovery, Power Boiler, kiln, dissolving tank

PM, gases, kiln, HLRV TRS, HLRV chlorineS urn me r

July-Sept. 30 Recovery and Power Boiler PM, gases,dissolving tank TRS

FallOctober-Dec. 31 Recovery, Power Boiler, kiln, dissolving tank

PM, PM?.5, gases, kiln, HLRV TRS

Closing

Your timely wdffen approval of this pre-test plan is greatly appreciated. If you have any questions.please do not hesitate to contact me directly at (902) 468-7777.

Regards,

STANTEC CONSULTING LTD.

hw9ojkJ UGillian Hatcher Vicky CorningFroject Manager — Environmental Services Team LeadPhone: (902) 468-7777 Phone: (506) 457-3200Fax: (902) 468-9009 Fax: (506) 452-7652

stantec.corn stantec.corn

v:\t2I4\ccthe\12t4’3\I2t4I3456_.2OI5sccK.’esi9gnp\’eoo’t;ng\e-est par\e’tes p:sn nahe,r cutcDt5vtocx



Appendix BCalibration Data

Stantec

VALLEY ENVIR ONMENTAL CALIBRA TION SER VICESPITOT TUBE CALIBRATION REPORT

aC

—x

wE

C

0

CLIENT -

PROBE ID -

NOZZLE -

DATE -

0.00

12.1

13.7

15.2

16.6

18.1

0.00

8.70

11.20

13.90

16.50

19.70

S (an Ice81 FT MS#6- 0.1875”March 3,2015

0.00

13.00

16.80

20.70

24.70

29.90

rechnician: T. Ryan

Signature

VALLEY ENVIRONMENTAL SERVICES160 Pony Drive #1

Newmarket, Ontario L3Y 7B6

PH: (905)8300136FAX: (905) 830 0137

FAN SPEED STANDARD PROBEPITOT PITOT

mIs (mm H2O) (mm H20)

PITOT FACTOR Cp = 0.816

PITOT - 8-1 FT MS NOZZLE - #6- 03875”March 3, 2015

353025201510

50

0 5 10 15 20 25

STANDARD PITOT DP (mm H20)

TunnelStd. Pilot Cp

VES0.999

Static -0.25BarometricTemperatureAbs Static

29.165

29.08

Data 114/2015Barometric Pressure, Pb 30.06

Model Number: 1646Calibrated By : JB

Orifice Manometer Dry Gas Correction Orifice Pressure Differential (delta H@) Orifice

Setting, deitaH Factor, gamma yielding 0.75 cfm of air at 6SF and 29.92 in.Hg Coefficient

(in. H20) (Tolerance = 0.95-1.05, +1-1.5% of avg) as in. H2O (Tolerance = +/-0.15 In.) Ko

1.0 1.023 1.668 0.742

1.5 1.018 1.762 0.725

2.3 1.021 1.755 0.724Average 1021 1.728 0.730

Pre-Test Dry Gas Meter - Control Unit Calibration

Job #:

Calculations

Pre-Test Dry Gas Meter - Control Unit Calibration

Date : 114(2015Barometric Pressure, Pb : 30.06

Model Number: 1848Calibrated By JB

Job #:

Orifice Diy Gas Meter Temperatures (F) Time,Manometer Volume, Vm (cu.ft) Diy Gas Meter theta

Setting, deitaK Total Outlet, Average, (mm)(In. Ff20) to tm

0.9 5.293 59 59 101.5 5230 61 62 82.3 5657 53 63 7

Calculations

Orifice Manometer Dry Gas Correction Orifice Pressure Differential (delta H@) Orif IceSetting, deltaFf Factor, gamma yielding 0.75 cfm of air at 6SF and 29.92 in.Hg Coefficient

(In. H2O) (Tolerance = 0.95- 1.05, +1-1.5% of avg) as in. Ff20 (Tolerance = +1- 0.15 In.) Ko0.9 1.057 1.608 01541.5 1.049 1.759 0.7272.3 1.054 1.751 0.725Average 1.053 1.706 0.735

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9677

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,,(s

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cal

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V(s

td),

and

the

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ratio

n(t

or,

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hese

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tions

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inth

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2015

’02’

04-1

646.

xlsX

Calibration DataEnerac 500 Combustion Analyzer

Stantec Consulting Ltd.Location: Fredericton, NBDate: March 11,2015

Pre-Test Calibration Post Test Check

G Date 11-Mar-is Date 11-Mar-15Parameter Unit

pan asPersonnel NGM Personnel NGM

Concentration Ambient Air Span Gas Ambient Air Span GasReading Reading Reading Reading

Co ppm 200 0 193 0 2001000 1012 1001

SO2 ppm 200 0 178 0 200

NOX ppm 200 0 198 0 200

VALLEVENVIRONMENTAL CALIBRATIONSER VICES

35

25

E’ 20Lu 15mao 10

500

PITOT TUBE CALIBRATION REPORT

CLIENT -

PROBE ID -

NOZZLE -

DATE -

0.00 0.00

8.90 14.10

11.10 17.80

13.70 21.80

16.70 26.40

19.70 31.10

Technician: T. Ryan

Signature jZ,w.ec __

VALLEY ENVIRONMENTAL SERVICES160 Pony Drive #1

Newmarket, Ontario L3Y 786

PH: (905)8300136FkX: (905) 830 0137

TunnelStd. Pitot CpStatic

BarometricTemperature

VES0.999-0.25

29.1565

Stantec2FT MS#8- 0.250”Fcbruary 23, 2015

FAN SPEED STANDARD PROBEH PITOT PITOT

rn/s H: .(rnrnH2O) (mmH2O)

0.00

12.2

13.6

15.1

16.7

18.1

PITOT FACTOR Cp = 0.794

PITOT - 2Ff MS NOZZLE - #8- 0.250”February 23, 2015

0 5 10 15 20 25

STANDARD PITOT OP (mm H20)

Abs Static 29.13

Stantec Consulting Ltd.Steel Nozzle Calibration Data Sheet

NozzlelD Nozzle_Diameter_(inches)

Set - 1 <1> <2> <3> <4> Hi-Lo Avg.

1-4 0.125 0.124 0.125 0.125 0.001 0.125

1-6 0.175 0.173 0.165 0.175 0.010 0.172

1-8 0.236 0.232 0.234 0.232 0.004 0.234

1-10 0.307 0.305 0.308 0.305 0.003 0.306

1-12 0.367 0.372 0.367 0.371 0.005 0.369

1-14 0.434 0.434 0.433 0.434 0.001 0.434

1-16 0.500 0.497 0.503 0.501 0.006 0.500

QNQC Check

Each Diameter Measured To Within = 0.001 InchesHigh - Low <1= 0.004

Prepared By: JJB Date: Feb 05, 2015


Appendix CField Data Sheets

Stantec

MOISTURE FIELD DATA SHEET

Moisture Data

Impingor No. Impinger Final Weight Tare Weight Weight ofContents (g) (g) Moisture (g)

I IOOmLH2O

2 100mLH2O L/3, I3 Blank 1o5t jOg

4 200gSiNcaGeI 99 U i 3

Total Weight Gain (g)

Moisture Volume (niL) IS

—‘ Volume H20 Collected:

xo.045 =

ml

51 ft3H1O(Vwc)

DGM Final SO 8i ft3

DGM Initial a q

Final - Initial = - 9 ft3 (Vmc)

Moisture =

(Vwc + Vmc)

0’ 130g

Project No.:

Client:

Plant:

Location:

thfb.’9 9t’jlit F] MIPnakr €o.l.r

Test: (‘Ax — I

Stantec

Date: fr0.r ID ip,5

Analyst: ‘16 i-?

Moisture = Vwc

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COMBUSTION GAS ANALYSISCONCENTRATION FIELD SHEETSampling Methodology: Environment Canada EPS 1/RW15 (3 Stantec

ConcentrationsTime 02 CO2 CO SO2 NOx NO NO2 THC

(%) (%) (ppm) (ppm) (ppm) (ppm) (ppm)

0 c) 13 32S (i_I a 0

. (NW:.10 0 0 ‘flc 6 U coja

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if tI

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Client:

Plant:

Location:

Test No.:

Date:

Fs1

o& WI1kw (6/IS

Fuel Type:

Time Start:

Time Finish:

Personnel:

21’-i5• 3:13

WI

Project No.:

Client:

• Plant:

Location:

Test

Analyst: g/77Xg


Moisture Data

Impinger No. Impinger Final Weight Tare Weight Weight ofContents (g) (g) Moisture (g)

1 100mLH2O 3 7311L)

2 IOOmLH2Q a32—

3 Blank 659.54 ZOOgSiiicaG&

Total Weight Gain (g) 2nD

IMoisture Volume (mL) 1 t .

Volume H2O Collected:

XO.048 =

ml

12 .,‘Vi ft!HOwwc)

Final - initial =

Moisture =

ft3

ft3

ft3(Vmc)

Vwc(Vwc+Vmc)

Moisture = Q

M0tM.t t/gd, &hij; trpy,

Pn-”ZDate: ‘4cr It 2o;5

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COMBUSTION GAS ANALYSISCONCENTRATION FIELD SHEETSampling Methodology: Environment Canada EPS 1IRMI15 (3StantecProject No.:

Client:

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li-i

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b iSIS zssl SS Lf9 19fo 51 jç 8,c LIA ISAn L2I 9 23

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COMBUSTION GAS ANALYSISCONCENTRATION FIELD SHEETSampling Methodology: Environment Canada EPS 1/RM115 StantecProject No.:

Client:

Plant:

Location:

Test No.:

Date:

Ijdkr PMIPPch41 MS’

RQton 4o(ttr

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Time 02 CO2 CO SO2 NOx NO NO2 THC

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ProJectNo.:7I9I3gSClient: I’nr-1l—r!N P1.ApPlant:

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Moisture Data

impinger No. Impinger Final Weight Tare Weight Weight ofContents (g) (g) Moisture (g)

1 100mLH2O 995. VSO-S 2’5

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Stantec

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ent:

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hem

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pJo

bN

um

ber

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1345

6

Pla

nt:

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erB

ode,

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sonnel

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inis

h:

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r.B

arom

etri

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ress

ure

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bar

(in.

Hg)

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ckS

tati

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stat

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n.H

20)

koble

nt

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p.

(F)

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me

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lecte

d.

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(ml)

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per

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enE

very

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ulat

ory

Age

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ver

seP

oin

t

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icula

teC

oll

ecte

dtr

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ther

(fig

):P

atti

cula

teC

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ecte

dfr

om

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be

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h(m

a):

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icula

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ole

cted

from

imp

ing

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mg)

:

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cula

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dm

g):

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050

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DATA ENTRYNorthern Pulp

Plctou, NSFuel: Fuel oil

Operating Conditions:Emission Control Equipment:Stack Height from Grade: m

Stack Diameter: m

Reference Temperature, Tref (F): 77(K): 298

Reference Pressure, PrefQn.Hg): 2992(Bar): 1.0

Parameter Symbol Units Test 1 Test 2 Test 3 Average

Test ID- - PM-2 PM-a PM-4 -

Date- - 10-Mar-iS I 1-Mar-15 1 1-Mar-i S n/a

Start Time- 8:47 AM 12:00 PM 2:52 PM a/a

End Time- - 10:47 AM 2:00 PM 452 PM Va

Total Sampling Time- mm 120 120 120 120

Stack Diameter D in. 76 76 76 76Average Stack Gas Temperature Ts F 149 149 147 148Mtragt thy Gas Meter Temperature Tm F 43 52 57 SIBarometric Pressure rhar injig 29.55 29.38 29.35 29.43Stack Static rressure Pstatic in.l120 0.20 0.20 0,20 0.20Average Pressure Drop (head) dP in.hI20 1.13 0.95 1.15 1.08Average deltall Orifice dli in.1I20 0.60 0.49 0.61 0,57Average Meter Temperature Tm F 43 52 57 51Gas Sample Volume Vm cuSs 47.77 4367 46.66 46.70Ayes-see laokmne,ics I Ta 107 108 105 106

Nneale Diameter Di. in. 0 172 0.172 0,172 0.172Pitottoefficiens Up - 0.816 0 816 0,816 0816Gamma, meter constant y — 1.053 1.053 1.053 1.053

Reference Temperature Tref R 537 537 537 537Reference Pressure Pref intl8 29.92 29.92 29.92 29.92

Stack Ga. Ongen Contene CoZ 10.8 11.4 9.7 10.6Stack Gas Carbon Dioxide Content CcoZ V. 9.8 9.3 11.0 10.0Stack Gas Nitrogen Content CnZ ¼ 79.4 79.4 793 79,4Stack Gas Sulphur Dioaide Content CsoZ ppm 0.0 0.0 0.0 0.0StackGeeNitrogenOaidesContent Coos ppm 16.1 21.0 26.3 21.1Stack Gas Carbon Monoxide Content Cci. ppm 1733.9 2079.0 1936.1 1916.3

Volume of Water Collected Vw ml 291 260 285 278Particulate Collected from Filter

- ong 198.6 211.4 1843 198.1Particulate Collected ri-nm Probe Vash - mg 20 9 27.8 45 0 31 3Particulate Collected rrnm Impinger Wash

— mg 4.8 3 0 4.2 4 0Total Particulate Collected (excluding impingen) Sip mg 220 239 229 229

Legend: F - degrees Fahrenheit n,[120 - inches atwaterK - degrees Kelvin cu,ft - cubic FeetBar - ban R - degrees Rankmnin.Hg - inches of mercury NOx - as N02in. - inches

CALCULATIONSNorthern Pulp

Plototu, NSFuel: Fuel oil

0per91219 Conditions.Emission Control Equipment:

Stack Height from Grade: mStack Diameter: in

Vadeble Symbol UnIts Calculation Test I Test 2 Test 3 Average

Sink Are. A, 1q11 4e — Pit I(ohlOi’2 4 31.50 31.50 31.50 31.S0

I.e A,),q.ml.Ai).,fl)sbOIZt 293 293 293 293

B.rnciricPewure PS., kP. Pbur)kfll•Pb.rdntbj.IJN 1001 995 994 998

t.ck Stitic Pn..ne Ps,r.k k11. N.m kPEe Ptnrk 1.1120)1 C!) 0 Os 0.05 005 005

Ant. Stack Tcmpcretsn Ti K Ti Ri eTc fl • 14* 809 809 807 808

At1. Meter Temperittire In K Tn lliTe IFI°44* 503 512 517 511 0

NonkDismeirr 0s D.iel-Dsibislld 4 4 4 44

C., Meicr r echOiC Pm tIlt Pm — Pbn+l 411 i 13.’) 29 59 29.42 29 39 2947

Simple Volnac et RefCond Yst ‘tO Vme’Tnr!Pnru{Vm s Pm .yiIte 53.09 47.30 5225 509

‘I.e Vec(amIt020J3nvee)e,n) 1.50 1.34 148 1.44

Volume trwster Vepoor voc twit t’wt fiNd uvo, 13.94 1248 13.87 13.38

Woter Fraction Boo Bet—Vet! I V*t + Vet) 0.200 0.208 0 207 0 2

Meleccil.r Wricht. Dry Rd bIb-er) Md— &41 irish •ti: (Coo), bIt Cell 3000 2994 30.15 300

3tokctl.r Weibo. Wet Mi 1616-md ‘(nIld II’ loot clii t 0..) 27.50 2745 27.83 27.5

Stick Pn.eun P. iRa P. — PIer • P.1.115! 03.11) 2954 29.39 2938 2944

(tick Ca V.kdtp Ci 16. Ce • 19.33 I Cp I (NP I Tilt’s t orts 62 07 54.19 02 72 60 3

en Ce ie!•1 53- 11U11161 I 1092 17.13 19.12 104

Anal Stub U.. Fine Rile Q .ri Q—lCs LisA. 117,330 100 218 113 558 114035

Dry Stick C.. Ftto, Rite 9. R,rm Q. —0 lI’S—ti u )TnUTeI r (ri/Pitt) 81.820 72,822 81,607 78.408

Rn-s Q.ite...1b811047250.(Rifroe 3825 3437 3052 370

Sulphur Ditside. SO!502 Me,,ii red Concentration C.ul ppm Mr.,.nen,t From lim Cee An.).r 000 0 00 0 00 0.00

U,correc it’d 1) Ref Cond C.u3 chess C,.0)e0/Rrm( — Ccii ppm) I 342 0.00 000 000 000

SO! Eminion Rile cR113 1/’ ERiti • Ceo3!I0ce • QI 000 000 000 000

hfl, eRetllkflfl.ibt CR1006/el 000 0.00 0.90 000

502 Ccdetttr.licnCorrected 1.11% 02 C.u3 stir. Cm3t11%roI.C,.3 ).WR.metiltbI)i/l0tt-C31 000 0.00 000 0.00

orrrctrd 0.3% 02 L.a eWRsm Cu3 )r403) • C..3 (nt/Ram) • atea,00.1t31 DM0 000 000 000

Corrected 1112% C02 Cml mWRse CeO 113% COllm CaiO isp/Rem), ill/tea) 000 000 DX 000

NiIrnenr anN., . NOt

NOr Matured Cnncrnlratioe Cm. ppm Mreooree.ot Ins lii. Ce. AIim., 1014 2100 26.29 21 14

Uncorrrcoed 61 RrFCosd Cm. ma/Rn- tort lmpjmtsnl— Cm, ppm) r 1.103 30.38 39.52 49.47 3979

Not Emission Rely 1Km’ Wi cRoon — Cts./lom s Qu 1 16 1 38 191 1.40

1/br Ktstikflr(.ien Emmila/if 4.15 489 8.06 5.31

NO. Centre caRomCorrected toIl ¼ 02 Cm’ mpltm Cm, 111% 03). Cmi (ma/ten) I i0fl.I 1)1 ifll.colt 2970 41.00 4373 38.14

:rretted oJ% 02 Cm, siRen Cen (3+1.021. Cen ieflt.l • )lfl,O(/c21.)Ca31 5389 74 13 7900 6496

Correctid 1012% C02 Cm. st/Is. Cm, 113% COOl — Cm, ieeia.i 5 )iLtctI) 3728 5123 5397 4740

CsrbortMsnmtide-COCOMr.uurrdCrectolr.iioo Cc. ppm Ma.an.nhlmn.ICSA.Jpn 173300 2379.00 1938.14 191833

U.esrncte,161R.fCad ci. se/On- cm)etRn-i-reev,sJ.Ilal 198527 235048 221688 219429

CO Emieeion Ret. ERrs LIce — Cn(bIi0 sQ. 7593 01.82 0539 01 05

•fl, Ipso ha/hi —30s eflco (e) 27334 294.56 307.41 291 V

CO Cenren trail.,Correcled 1.11% 02 Coo mg/Ire Csulll%09).Cro)ms/ReeII)351.lI)!00.9-C031 194046 2469.54 195957 2123.19

Corrected to 3% 02 Coo mg/Rim 00(3% 03)— Ceo ma/Rem), 3554) I 1359-CoO) 350552 4485.13 3543.05 3038.90

Corrected 1012% C02 Cc. mt/Rem Cc.(13% CD!). Ceo )m1Imim) I il/troll 243449 3005.78 2419,42 264823

PsnktIsleCooc,olndot C, si/mis Ci— MpIVmo 14801 17019 15492 15974

Piniedsie Emisoiou Rite LIp a/c LRp—Ct.lsQ, 554 813 597 509

wait !Rpêtirisjeo ER1)g/.e 20.10 2200 2148 2122

Penletlote CoecmtnliooCormted i.II’. 02 Ci edge C. pifl’. 031C.. tlbI-tI)lt3OICo3t 14272 18498 13594 15487

Corrected IoJ% 02 Ci m14em Ci (31’. 031°C.. (30.54)! (2t.t-C13l 25004 33442 24759 10002

Corrected it 2% C02 Ce mt/hem Ci 12% COO). Ccl (13/Ceo3I 17905 231.11 16900 19305

I.ute.dl sql -squire feel nb-0 - motto or mercury m0IRcm-ml9n.ms per dry relerence cube mel.

oqm-oqu.r. meorn II ‘cubic rot 9!..000m, per secyol

P,.1142 Cu 0’ rube main Nor- is (02

deretl Rink. Rot Coot -melerence lemp. ‘lure in FIssure 25 C sod 101 3 mel ecrm.nlcul rube feel per trundle

pym-paitipomitism Rome- dlyr.remncecunicm.frio pereoroed

Rtlm -dry melmoence cube feet per miour.

OFFICIAL STACK TESTING RESULTSNorthern Pulp

Pictou, NSFuel: Fuel oil

Operating Conditions:Emission Control Equipment:Stack Height from Grade: m

Stack Diameter m

N SE N VParameter Test I Test 2 Test 3 Average Limits

Test ID PM-2 PM-a PM-4 - -

Test Dale 10-Mar-i 5 1 1-Mar-15 1 1-Mar-15 - -

Stack Gas Temperature (C) 64.7 65.1 63.9 64.6 -

Moisture Content (%) 20.8 20.8 20.7 20.8 -

Velocity (ntIs) 18.9 17.1 19.1 18.4 -

Volumetric Flow (Rems) 38.2 34.4 38.5 37.0 -

Ongen - 02 (%) 10.8 11.4 9.7 1 0-6 -

Carbon Dioxide - C02 (%) 9.79 9.26 11.0 10.0 -

Sulphur Dioxide- 502502 Measured Concentration (ppm) 0.0 0.0 0.0 0.0 -

S02 Concentration at 11% 02 (mg/Rcm) 0.0 0.0 0.0 0.0 -

Emission Rate (lqz/hr) 0.00 0.00 0.00 0.00 -

Nitrogen Oxides - NOxNOx Measured Concentration (ppm) 16.1 21.0 26.3 21.1 -

NOx Concentration at 11% 02 (mg/Rcm) 29.7 41.0 43.7 38.1 -

Emission Rate (ku/hr) 4.18 489 6.86 5.31 -

Carbon Monoxide - COCO Measured Concentration (ppm) 1734 2079 1936 1916 -

CO Concentration at 11% 02 (mglRcm) 1940 2470 1960 2123 -

Emission Rate (kglhr) 273.3 294.6 307,4 291.8 -

Particulate Matter - PMParticulate Concentration at 11% 02 (mg/Rem) 143 185 137 155 -

Particulate Emission Rate (kg./hr) 20.1 22.1 21.5 21.2 -

Legend: C - degrees Celsius Ref Cond - reference temperature and pressure (25 C and 101.3 kPa)rn/s - metres per second mglRcm - miligrams per dry reference cubic metreRcms - dry reference cubic metres per second NOx - as N02ppm - parts per million ND - non-detectable

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DATA ENTRYNorthern Pulp

Plctou, NSFuel: Fuel oil

Cperating Conditions: NormalEmission Control Equipment: wet scrubber

Stack Height from Grade: 69 mStack Diameter: 3.51 m

Reference Temperature, Trot (F): 77(K): 298

Reference Pressure, Prof (in.Hg): 2992(Oar): 1.0

Parameter Symbol Units Test I Test 2 Test 3 Average

Test ID - - PM-i PM-2 PM-3 -

Date - - 10-Mar-15 10-Mar-15 il-Mar-IS nla

Staftilme - - 900AM 12:15 PM 9;20AM n/a

End Time - - 11:00 AM 2:15 PM 11:20 AM n/a

Total Sampling Time - mm 120 120 t20 120

Stack Diameter D in. 138 138 138 138

Average Sack Gas Temperature Ta F 154 154 147 152

Average Pt3’ C,as Meter Temperature Tm F 51 57 48 52

narometric Preature Pbar mug 30.13 30.12 29.55 29.93

Slack Static Preasure Potatic inliZO 1.10 1.10 1.10 1.10

Average Pressure Drop (Head) dP in.1120 0.59 0.66 0.58 0.61

Average deltall Orifice dli mIll0 0.83 0.94 0.62 0,87

Average Meter Temperature Tm F 51 57 48 52

Ge, Sample Volume Vm cu.ft SB 91 61.66 57.94 59.50

Average lsa&inetice I 105 102 104 103

Noale Diameter Da in- 0 234 0 234 0.234 0.234

Pilot Coeflident Cp - 0.794 0.794 0,794 0.794

Gamma meter constant y - 1.021 1.021 1.021 1.021

Rererence Temperature Tref Ii 537 537 537 537

Reference Pressure Pref mUg 29,92 29.92 29.92 29.92

Stack Gas Oxygen Content Cal 48 4 5 44 4,6

StackGas Carbon DioxideContent Cco2 V. 15.6 15.9 16,1 15.9

SeackGasNitrngenContent Cal 79.6 79.6 79.5 79.6

Stack Gas Sulphur Dioxide Content fbi ppm 8.1 6.1 27.9 14.0

Stack Ga, Nitrogen Oxide, Content Coos ppm 23.7 46.1 52.1 40.7

Slack Gas Carbon Monoxide Content Cco ppm 1772.3 2817.3 3083.0 2557.5

Volume ofWaler Collected Vw mL 540 542 541 541

Particulate Collected from Filter - mg 1743.4 1626.3 1505.2 1625,0

Particulate Collected from Prttbe Watts - mg 730.8 1152.8 714.6 866.1

Particulate Collected rrom Impinger Wash - mg 1.94 4,54 3.27 3,25

Total Particulate Collected (excluding impiogen) %lp mg 2.474 2,779 2,220 2,491

legend: F - degrees Fahrenheit in.1120 - indict nfwatcr

K - dcgrces Kclvin caft - cubic rcccBar- ban R - degrees Rankinin.Hg - inches of mercury NOx - as N02

in. - inches

CALCULATIONSNortism Put1,

Pktou, NSFuel: Fuel oil

Operating Conditions: NonnalEmission Control Equipment: wet scrubber


Vadablo Symbol Units Calculation Test I Tail 2 Teat 3 Averag.

tick Area Ac q.fl A,— hi ilOrI2rlVl 19387 10387 10367 10357M5 AI{Içst—A, io4flbt.ii 965 965 9.65 965

Birometric Penis,. floe 6Cc PbnlLP.tspb.rlmlI.luJ./Rt 1023 1920 103.1 1014Stack Static Pr.n.rc P,t.ilt LP. Pei.o6 bElt— htMl. blew.. I 31’ 027 027 027 027Ag. Stoek Temperature Ti Ti/mi—Tow). 064 814 614 607 612A.g. Meter Trmperoture Ti, II Ti, let_ Ta Fl, 060 511 517 508 511Nonle Diameter on as flu li,st Ian lb.) I 30.4 6 6 8 59

Con Meter Preuture Pm leit ho — Plot + dill ni 30.19 30.19 29.61 39.00Sample Volume ut RelCond Vine .160 Vine Trer/Pnea lOst Pm cyilT.. 63.79 6603 6192 639

rum Vnuicwmt16tltJ3eV.mleoSli 1.61 187 175 181Volume .1 Wiler Vapour Vine itO Vine — beset a Vu 25 92 26 90 25.95 25 96‘Vatir Fraction Boo . Sea—Vine/i VsctVse I 0 289 0 263 0.295 0.3

MakcoltrWdflt,Dr, Md fl-id Md-eolic,o21.33iru21+lzIicezi 3009 30.73 3075 307Iukoulor Weiibt. Wet 11’ t-.d ‘0. 11411. 0oi,° lit mu 2703 27 13 2898 270

Stick Censure N 16115 Pu— fl.rlPuauelI1ti 3021 3330 2963 30.01lack Cat VcIudt, Li WI Li — ILl’ . Cp I /4 P07,06?, M.lr41 45 90 47 58 45.02 45 9

ale U.ls,/,l—t)Oliut, WI) 1374 14S0 13.72 140Aciu,l Stock Cu, Fbi, Rile 13 IOta QbOiVnA’ 280,972 296,542 280.554 286.023Dry Slick G.e Flow Rite 131 tern Qi —13 011.00tH Tnt/Tel z Pt/Cnn 176,516 107,783 173.197 179.185

Ron, Qe lien,t_600473 tQu)Roflu) 63.32 8083 81.75 048

Sulphur Dioeide.502502 Meattored Coucrntrtt.’oa Coot ppm Moomuemeet trim Rho., Au.Iyner 8.14 614 27.88 1405Uncorrected ia Ref Cued Ciot se/Rein Clot lme/Rent Ccii tjipniu 242 21 33 1609 7299 2600502 Emliston Rite FReul Wi FR,ii ceozions I Qu 178 1.43 5.97 306

LIIr Fieollbflri—JCteR.uliWnl 840 5.34 2140 1100

502 CunceminfltoCorrected 10ll% 02 Cmi na/Ru. ClIlt¼OIi—Ctalimflu.ttlmn-Ilt/blte.Ct31 1312 9.72 4375 2220Cureected o3% 02 Ciol nw/Rem C.o2lJ%o3o—Cn2lne/nemt.liuntlo5.bcu3) 2372 1757 79.11 4013Curtated is 12% C02 Cmi nt/Ru. ClllO2VuColItCm2inflC.ltlIiuCutll 1637 12.14 5450 2767

Nitroern Otides - NO,NO. SI toured Cuncenir,te’eo riot ppm Me.onn.e.i Ira ha. 9m Anuipee 23,71 46.14 52.14 4087Uacurncled /8 Ref Cund Cm, me/Rim Cm0 me/Rest’ C.eu (pps}. tOni 44.63 8664 98.13 7653NO. minion Rile Limo i/i FRmu 5 riot/tIle uQe 3,72 7 70 6.02 6 48

kflr tRamu Ibsltri “16’ Cite, lgl 13.39 2771 20.88 2333

NO, Cuneimi rulionCorrected to ‘0% 02 Conu se/Or, Clout 00% 030 Cou. ne/Runt: (2,9-Ill lQt9.Col) 27.44 5242 5083 48.23Corrected 1,3% 02 Cue, ne/Rei, Cite, (2T’uO3i Ciii me/Runt u l28.9-Jl /11,9-Cdt 49.62 9478 106.37 8359Corrected to 12% C02 (mu st/nts Cm, 112% COil — Cmt line/Real, 112/null 34.24 6540 73.27 8768

C.tho. %Innonote- COCO Me.inrrd Conceourstins Cm pta Mm,s.seuI Fins hi, C.u Aautfler 1772.29 281729 3983 CO 2557.52L/neurreeird /8 RefCond Cm me/Ron Ceo 061/Rush Ceo pp.o e 1.141 2029.27 322579 353004 292836CO Liuinioo Rote em.. V. Fmn—Ceal000.Q. 10907 285.91 28856 24705

hi/Re iai.l4iriuJt I LRe.lri 60885 102929 193828 89227

CO CotteemiritiunCorrected 1001% 02 Ceo se/Rein CmlII% 03l Coo si/Rent, 1260-1 Ii) neC-Cult 1247.81 1947.28 2118.19 177043Corrected 03% 02 Ceo si/Rein Ce,{3% Oil • rellme/RomI u 369.3l/l3e9-Cu21 2256.14 352083 3028.24 320107Corrected 1002% C02 Ceo se/Rein Ceutli%COltCCulmu/nemltit3JCeeii 1556.70 243237 2635.76 2208.28

Pafliculote Concen Irallo, Ci se/Rem Ce— lop lOst 1369.58 148091 1265.99 1374 15Panheulote Emi,,ion Rite ERP e/e FOps Ci/1 u Q. 114.11 13179 193.49 11648

be/hr Fop lloirI 3.4 u (Op li/it 410.78 47444 372.58 439.27

Ponicolots Contrml riliunConnled lnbI% 02 Ci miles Ci mlI%000C, C i269-IliiiflO-C.2l 64215 89758 75894 83289Corettlent 1n3%02 C, mt/Rem ClU%OflsC.ent9-3,/12t0-Coi 152228 6z29O 137222 ‘50593Corrected is 02% COl C. si/Re. Ci i13%C03HCI tiI3/ndl 105082 1121 19 94527 Q39 03

Uied, ,cn-tqu.eCnt ot/R.rc’nonfrnmlfl IS.’ ‘9uaenp,erryrn04.rtucnnt.tIm .OIhI nm/rue 3- cube lint 1/i- WI—nm ..r ondP.0152 com.cuOnmmm NOo.nN03

Ret Cuni . ,.l’mnee em purl/ire ma presouu. /25 c •04 101 3 IP.l ‘tin. .ct,.i rube reel pit moultppm- pod. m mi//cnn Remu . /ry chit/ti cube metre, p.icotyot

Rclm . dry elihi000 cube bolt p.1mm/rote

OFFICIAL STACK TESTING RESULTSNorthern Pulp

Pictou, NSFuel: Fuel oil

Operating Conditions: NormalEmission Control Equipment: wet scrubber


0

Parameter Test I Test 2 Test 3 Average Limits

Test ID PM-i PM-2 PM-3 - -

festDate 10-Mar-15 10-Mar-15 11-Mar-15 - -

Slack Gas Temperature (C) 67.6 67.8 63.9 66.4 -

Moisture Content (%) 28.9 28.3 29,5 28.9 -

Velocity (ni/a) 13.7 14.5 13.7 14.0 -

Volumetric Flow (Rcms) 83.3 88.6 81.7 84.6 -

Oxygen -02 (%) 4.80 4.50 4.39 4.56 -

Carbon Dioxide- C02 (%) 15.6 15.9 16.1 15.9 -

Sulphur Dioxide - SO3SO2 Measured Concentration (ppm) 8.14 6.14 27.9 14.0 -

SO2 Concentration at 11% 02 (mg/Rcm) 13.1 9.72 43.8 22.2 -

Emission Rate (kg/hr) 6.40 5.14 21.48 11.00 -

Nitrogen Oxides - NOxNOx Measured Concentration (ppm) 23.7 46.1 52.1 40.7 -

NOx Concentration at 11% 0, (mgiRcm) 27.4 52.4 58.8 46.2 -

Emission kale (kgihr) 13.4 27.7 28.9 23.3 -

Carbon Mnnoxide - COCO Measured Concentration (ppm) 1772 2817 3083 2558 -

COComcentratioo.t1l%0,(mWkcm) 1248 1947 2116 1770 -

Emission Rate (kg/hr) 609 1029 1039 892 -

Particulate Matter — PMParticulate Concentration at 11% 02 (mwRcm) 842 898 759 833 375

Particulate Emission Rate (kg/br) 411 474 373 419 -

Legend: c - degrees celsiusmis - metres per secondRcms - dry reference cubic metres per secondppm - parts per million

Ref Cord - reference temperature and pressure (25 c and 101.3 kPa)mgiRcm - miligrams per dry reference cubic metreNOx - as N02ND - non-detectable

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3Stantec - Government of Nova Scotia

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Transcript of 3Stantec - Government of Nova Scotia