Pembahasan Skripsi Spektroskopi Mengenai "Pengukuran Kadar Nifedipin Dalam Sediaan Tablet...

7/23/2019 Pembahasan Skripsi Spektroskopi Mengenai "Pengukuran Kadar Nifedipin Dalam Sediaan Tablet Menggunakan Sp

1/86

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2/86

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3/86

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4/86

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5/86

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6/86

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7/86

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8/86

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9/86

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10/86

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wpfezyomozobfzyk vlzyh}kolfz# Jhlhb pfcflkzkhc zfywfivz jknvchehc pflhyvz ifyvph bfzhcol,

wfihi jhyk dhwkl oykfczhwk {hcn jklhevehc olfd pfcflkzk, ihke jk lhyvzhc hwhb bhvpvc ihwh,

jkpfyolfd lhyvzhc {hcn evyhcn afyckd $wfdkcnnh zkjhe bfbfcvdk w{hyhz pflhyvz+#

Hjhpvc hlhwhc pfcflkzk bfbklkd phcahcn nflobihcn 976 cb vczve pfcnvevyhc ehyfch

phcahcn nflobihcn zfywfivz, ckmfjkpkc bfbklkek cklhk hiwoypzk}kzhw bolhy $ + {hcn lfikd

ifwhy jkihcjkcnehc phjh phcahcn nflobihcn 77: cb# Jfcnhc cklhk hiwoypzk}kzhw {hcn ifwhy,

bheh pfcnvevyhc jhphz jklhevehc phjh eocwfczyhwk yfcjhd, wfdkcnnh jkpfyolfd wfcwkzk}kzhw

{hcn zkcnnk vczve bfzojf kck#

Wfiflvb jklhevehc pfcfzhphc ehjhy jfcnhc bfcnnvchehc bfzojf kck, pfylv

jklhevehc wghcckcn phcahcn nflobihcn bhewkbvb jhyk wfc{h~h vak zfylfikd jhdvlv,

bfwekpvc phcahcn nflobihcn zfywfivz wvjhd jkefzhdvk jk jhlhb lkzfyhzvy# Dhl kck jkwfihiehc

ehyfch phcahcn nflobihcn wvhzv wfc{h~h jhphz ifyifjh iklh jkzfczvehc phjh eocjkwk jhc hlhz

{hcn ifyifjh#


11/86

Jhyk dhwkl pfygoihhc {hcn jkjhphz zfyc{hzh pfcflkzk bfcjhphzehc phcahcn nflobihcn

bhewkbhl 976 cb jkbhch hiwoyihcwk {hcn jkdhwklehc wfifwhy 0,:7>0# Wflhcavzc{h, vczve

pfcfzhphc ehjhy ckmfjkpkc jhlhb wfjkhhc zhilfz {hcn ifyfjhy jk phwhyhc jklhevehc phjh

phcahcn nflobihcn bhewkbvb ckmfjkpkc IPMK jfcnhc hiwoypzk}kzhw zfyifwhy {hkzv phjh

phcahcn nflobihcn 976 cb# Bfcvyvz Whzkhjhybh $900:+, pfcfczvhc ehjhy jklhevehc jfcnhc

bfcnvevy wfyhphc phjh phcahcn nflobihcn bhewkbvb $pvcghe evy}h+, hnhy jhphz

bfbifykehc wfyhphc zfyzkcnnk vczve wfzkhp eocwfczyhwk# Iklh wvhzv wfc{h~h bfbpvc{hk lfikd

jhyk whzv pvcghe hiwoypwk bhewkbvb, lfikd jkvzhbhehc phcahcn nflobihcn hiwoypwk

bhewkbvb {hcn hjwoypzk}kzhwc{h zfyifwhy jhc bfbifykehc evy}h ehlkiyhwk lkckfy jhlhb

yfczhcn eocwfczyhwk {hcn yflhzkm lfihy#Wfzflhd jklhevehc wghcckcn phcahcn nflobihcn bhewkbhl, efbvjkhc jklhevehc

pfbivhzhc evy}h ihev ckmfjkpkc jhlhb pflhyvz bfzhcol jfcnhc eocwfczyhwk 1 :, =, 4, 80, jhc

89 n/bl phjh phcahcn nflobihcn bhewkbhl, jfcnhc bfzhcol wfihnhk ilhceo# Pfcfzhphc

ilhceo jkpfylvehc wfihnhk pfcnoyfewk hiwoyihcwk whbpfl hnhy jkpfyolfd hiwoyihcwk bvyck

{hcn jkwvbihcnehc olfd ckmfjkpkc $hiwoyihcwk zfyeoyfewk jkpfyolfd jhyk pfcnvyhcnhc

hiwoyihcwk lhyvzhc whbpfl/ ihev zfydhjhp hiwoyihcwk ilhceo+# Dhl kck jkpfylvehc wfihi ikwh

whah pflhyvz {hcn jknvchehc $bfzhcol+ bfbifykehc cklhk hiwoyihcwk zfyzfczv jhlhb pfcnvakhc#

Pfbivhzhc lhyvzhc ilhceo jklhevehc jfcnhc bfcnnvchehc pfyfhewk {hcn whbh, avblhd whbh

wfpfyzk pfcnvakhc qhz vak, chbvc zhcph bfcnnvchehc qhz vak#

Jhyk dhwkl pfbivhzhc evy}h ehlkiyhwk ckmfjkpkc jkpfyolfd dvivcnhc {hcn lkckfy hczhyh

eocwfczyhwk jhc wfyhphc jfcnhc eofmkwkfc eoyflhwk $y+ 2 0,;;;= jhc pfywhbhhc nhykw lkckfy { 2

0,06940> t % 0,009>;4# Phjh jhwhyc{h, wfivhd pfcnvakhc jkehzhehc ihke hphiklh eofmkwkfc

eoyflhwk $y+ {hcn jkjhphz bfcjfehzk 8# Jhyk dhwkl pfygoihhc {hcn jklhevehc pfcflkzk, jhphz

jkwkbpvlehc ihd~h zfyjhphz eoyflhwk/ dvivcnhc {hcn lkcfhy hczhyh efchkehc eocwfczyhwk

jfcnhc efchkehc cklhk hiwoyihcwk {hcn jkdhwklehc #


12/86

Wfzflhd jklhevehc pfbivhzhc evy}h ehlkiyhwk hzhv evy}h ihev, efbvjkhc jklhevehc

pfcnvevyhc hiwoyihcwk jhyk whbpfl vak phjh phcahcn nflobihcn bhewkbhl# Jhyk jhzh

hiwoyihcwk {hcn jkpfyolfd, cklhk zfywfivz efbvjkhc jkbhwveehc wfihnhk cklhk { phjh

pfywhbhhc evy}h ihev wfdkcnnh hehc jkjhphz cklhk t {hcn bfyvphehc ehjhy jhyk whbpfl vak

{hcn jkvevy wfghyh wpfezyomozobfzyke# Ifykevz ehjhy yhzh"yhzh {hcn jkjhphzehc wfzflhd

jklhevehc pfydkzvcnhc $pfydkzvcnhc jklhbpkyehc jk dhlhbhc iflhehcn+#

Co Chbh Wfjkhhc Ehjhy Yhzh"yhzh $&+ Ehjhy Wfifchyc{h $&+

8 Ckmfjkpkc Nfcfyke EM 80>,>6 80>,>6 8,;>0

9 Ckmfjkpkc Nfcfyke Jfth 80=,=; 80>,>6 8,;>0

7 Goyjhlhz 800,9= 80>,>6 8,;>0

: Ckmfjkc 806,>6 806,>6 0,808

6 Mhybhlhz 800,>= 800,>= 9,0:8

= Hjhlhz 800,09 800,09 7,0==

Jhyk jhzh jkhzhw, jkzvcaveehc ihd~h ehjhy ckmfjkpkc jhlhb wfjkhhc zhilfz nfcfyke

bhvpvc chbh jhnhcn, bfbfcvdk pfyw{hyhzhc ehjhy {hcn zfyzfyh jhlhb Mhybheopf

Kcjocfwkh Fjkwk K] zhdvc 8;;6 {hkzv zkjhe evyhcn jhyk ;0,0 & jhc zkjhe lfikd jhyk 880,0&

jhyk avblhd {hcn zfyzfyh phjh fzkefz#Efvczvcnhc pfcnnvchhc bfzojf wpfezyomozobfzyk V], hczhyh lhkc 1

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bfzojf kck bfcahjk zkjhe hevyhz#


13/86

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jkwkhpehc vczve pfcnvevyhc jfcnhc bfzojf kck#

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bfyvphehc wfc{h~h

ify~hych+


14/86

IHI ]

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jhlhb wfjkhhc zhilfz#

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& jhyk avblhd {hcn zfyzfyh phjh fzkefz#


15/86

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16/86

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17/86

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18/86

Goczod Pfydkzvcnhc Pfckbihcnhc Whbpfl

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T 8000 bgn/bl 2 400 bgn/bl

96bl

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efbvjkhc jkgvevpehc whbphk nhykw zhcjh#

Ehjhy lhyvzhc vak 2

7,6blt=:bgn /bl

96bl2 4,;= bgn/bl


19/86

Pfydkzvcnhc Eocwfczyhwk Pfcnvevyhc

Jkefzhdvk 1 cklhk hiwoypzk}kzhw $ + 986;0 B"8gb"8 $ Bfyge Kcjfew, 9008+

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Eocwfczyhwk vczve Pfcnvevyhc Phcahcn Nflobihcn jknvchehc > bgn/bl#


20/86

Ykch Hmyk{hch Wkyhkz 1 Pfcfyhphc Bfzojf Wpfezyomozobfzyk Vlzyh}kolfz Phjh Pfcfzhphc

Ehjhy Ckmfjkpkc Jhlhb Wfjkhhc Zhilfz, 900;#

PFCFYHPHC BFZOJF WPFEZYOMOZOBFZYK VLZYH]KOLFZ

PHJH PFCFZHPHC EHJHY CKMFJKPKC

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WEYKPWK

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CKB 06040:084

MHEVLZHW MHYBHWK

VCK]FYWKZHW WVBHZFYH VZHYH

BFJHC

900;


21/86






WEYKPWK

Jkhavehc vczve Bflfcnehpk Whlhd Whzv W{hyhz vczve Bfcghphk

Nflhy Whyahch Mhybhwk phjh Mhevlzhw Mhybhwk

Vck}fywkzhw Wvbhzfyh Vzhyh

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YKCH HMYK[HCH WKYHKZ

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MHEVLZHW MHYBHWK

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900;


22/86



PFCNFWHDHC WEYKPWK




Olfd1YKCH HMYK[HCH WKYHKZ

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23/86

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24/86

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38/86

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39/86

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40/86

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45/86

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ihd~h cklhk dhwkl vak lhcnwvcn hzhv wfzflhd jkolhd wfghyh bhzfbhzkeh, pyopoywkochl

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zfyzknnk jhc eocwfczyhwk zfyfcjhd hchlkz {hcn jhphz jkzfczvehc jfcnhc pyfwkwk,

hevyhwk, jhc eflkckfyhc $Whzkhjhybh, 900:+#


48/86

ttkt

IHI KKK

BFZOJOLONK PFCFLKZKHC

Bfzojf pfcflkzkhc {hcn jklhevehc hjhlhd bfzojf fewpfykbfczhl# Pfcflkzkhc

kck jklhewhchehc jk Lhioyhzoykvb Ekbkh Mhybhwk Evhlkzhzkm Mhevlzhw Mhybhwk

Vck}fywkzhw Wvbhzfyh Vzhyh#

7#8 Hlhz hlhz

Hlhz"hlhz {hcn jknvchehc jhlhb pfcflkzkhc kck hjhlhd hlhz"hlhz nflhw,

wpfezyomozobfzfy vlzyh }kolfz $V] bkck 89:0 Wdkbhjqv+ jhc cfyhgh hchlkzke $]kiyh

HA+

7#9 Ihdhc"ihdhc

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hchlkwkw jhyk F#Bfyge+, hevhjfw $Lhioyhzoykvb Ekbkh Mhybhwk Evhczkzhzkm+,

ckmfjkpkc ihev $IPMK+5 zhilfz ckmfjkpkc nfcfyke jhc chbh jhnhcn#

7#7 Pfcnhbiklhc Whbpfl

Pfcnhbiklhc whbpfl jklhevehc wfghyh pvypowkm {hkzv zhcph bfbihcjkcnehc

hczhyh whzv whbpfl jfcnhc {hcn lhkc, ehyfch whbpfl jkhcnnhp dobonfc#

Whbpfl {hcn jknvchehc hjhlhd zhilfz nfcfyke Ekbkh Mhybh jhc Jfth Bfjkgh

wfyzh zhilfz chbh jhnhcn Hjhlhz $Ih{fy+, Mhybhlhz$Pyhzhph Ckybhlh+,

Goyjhlhz$Ekbkh Mhybh+, jhc Ckmfjkc $Whcif Mhybh+#


49/86

ttt

7#: Pyowfjvy Pfcflkzkhc

7#:#8 Pfbivhzhc Lhyvzhc Kcjve Ihev Ckmfjkpkc IPMK

Wfavblhd lfikd evyhcn 96 bn ckmfjkpkc IPMK jkzkbihcn wfewhbh,

jkbhwveehc ef jhlhb lhiv zfczvevy 60 bl, jklhyvzehc jfcnhc bfzhcol lhlv

jkgvevpehc whbphk nhykw zhcjh jfcnhc bfzhcol jhc jkeogoe dobonfc, wfdkcnnh

jkpfyolfd lhyvzhc jfcnhc eocwfczyhwk 600 bgn/bl, lhyvzhc kck jkwfivz lhyvzhc

kcjve ihev $LKI K+# Jhyk lhyvzhc kck jkpkpfz 6 bl bhwveehc ef jhlhb lhiv zfczvevy

60 bl, fcgfyehc jfcnhc bfzhcol whbphk nhykw zhcjh wfdkcnnh jkpfyolfd

eocwfczyhwk 60 bgn/bl $LKI KK+

7#:#9 Pfcfczvhc Phcahcn Nflobihcn Wfyhphc Bhewkbvb

Jkpkpfz 7,6 bl jhyk lhyvzhc kcjve ihev $LKI+ KK $60 bgn/bl+ bhwveehc ef

jhlhb lhiv zfczvevy 96 bl, fcgfyehc jfcnhc bfzhcol whbphk nhykw zhcjh $>

bgn/bl+# Lhlv jkeogoe whbphk dobonfc wfdkcnnh jkpfyolfd lhyvzhc jfcnhc

eocwfczyhwk > bgn/bl# Efbvjkhc vevy wfyhphc phjh phcahcn nflobihcn 900":00

cb $dhwkl jhphz jklkdhz phjh dhlhbhc 88+#

7#:#7 Pfbivhzhc Evy}h Ehlkiyhwk

Jkpkpfz lhyvzhc kcjve ihev KK IPMK $60 bgn/bl+ 9,05 7,05 :,05 6,0 jhc =,0

bl, bhwkcn"bhwkcn bhwveehc ef jhlhb lhiv zfczvevy 96 bl, zhbihdehc bfzhcol

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nflobihcn bhewkbvb {hcn jkpfyolfd jhc wfihnhk ilhcneo jknvchehc bfzhcol

$dhwkl jhphz jklkdhz phjh dhlhbhc 87+#


50/86

tttk

7#:#: Pfcfczvhc Ehjhy Ckmfjkpkc jhlhb Wfjkhhc Zhilfz

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dobonfc# Efbvjkhc jkpkpfz 7,6 bl lhyvzhc, bhwveehc ef jhlhb lhiv zfczvevy 96

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ehlk yfplkehwk# Wfzkhp yfczhcn wpfwkmke bfcnhcjvcn >0& hchlkz whbpfl jhc 70&

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wfihnhk ifykevz 1

&Yfgo}fy{ 2G

IHt 800&


51/86

tttkk

Efzfyhcnhc 1

H 2 eocwfczyhwk whbpfl {hcn jkpfyolfd wfzflhd pfchbihdhc ihev

I 2 eocwfczyhwk whbpfl wfiflvb pfchbihdhc ihev

G 2 eocwfczyhwk ihev {hcn jkzhbihdehc

7#:#6#9 Vak Pyfwkwk

Vak pyfwkwk $efwfewhbhhc+ jkzfczvehc jfcnhc phyhbfzfy YWJ $Yflhzk}f

Wzhcjhyj Jf}khwk+ jfcnhc yvbvw 1

YWJ 2 &800tTWJ

Efzfyhcnhc 1

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T 2 Ehjhy Yhzh"yhzh Ckmfjkpkc jhlhb Whbpfl

$^DO, 8;;95 Kcjyh{hczo jhc [v~oco, 9007+#

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Vczve bfcfczvehc ihzhw jfzfewk $LOJ+ jhc ihzhw evhczkzhwk $LOX+ jhphz

jknvchehc yvbvw 1

WI 29+$9

c[k[

LOJ 2Wlopf

tWI7

LOX 2Wlopf

tWI80


52/86

tttkkk

Efzfyhcnhc 1

WI 2 Wkbphcnhc Ihev

LOJ 2 Ihzhw Jfzfewk

LOX 2 Ihzhw Evhczkzhwk

7#:#= Hchlkwkw Jhzh wfghyh Wzhzkwzke

vczve bfcndkcn Wzhcjhy jf}khwk $WJ+ jknvchehc yvbvw 1

$ +

8

9

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c

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cWJ

TT2

Jhwhy pfcolhehc jhzh akeh zdkzvcn zzhifl jhc iklh zdkzvcn bfbpvc{hk cklhk

cfnhzkm, jkzolhe akeh zdkzvcn " zzhifl#

Vczve bfcghyk ehjhy wfifchyc{h jfcnhc zhyhm efpfygh{hhc ;; pfywfc,

jfcnhc jfyhahz efifihwhc je 2 c 8, jknvchehc yvbvw1

2 T z $8"8/9 +jet cWJ /


53/86

tttk}

Efzfyhcnhc1

2 kczfy}hl efpfygh{hhc

T2 ehjhy yhzh yhzh whbpfl

T 2 ehjhy whbpfl

z 2 dhynh z zhifl wfwvhk jfcnhc je 2 c"8

2 zkcnehz efpfygh{hhc

je 2 jfyhahz efifihwhc

WJ 2 wzhcjhy jf}khwk

c 2 avblhd pfylhevhc


54/86

ttt}

IHI K]

DHWKL JHC PFBIHDHWHC

Bfcvyvz Bommhz $900:+, ckmfjkpkc bfbpvc{hk wpfezyvb wfyhphc

bhewkbvb phjh jhfyhd vlzyh}kolfz jhlhb lhyvzhc hwhb phjh phcahcn nflobihcn

976 cb $H 88 2 6;6 i+ jhc 774 cb $H8

8 2 8;6 i+# Bfcvyvz Bfyge Kcjfew $9008+ ,

jhlhb lhyvzhc hwhb bfbifykehc wpfezyvb wfyhphc bhewkbvb phjh phcahcn

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phcahcn nflobihcn 974 cb $ 2 90=00+ jhc 7:0 cb $ 2 6>:0+ jhc jhlhb

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wfghyh wpfezyomozobfzyk vlzyh}kolfz# Jhlhb pfcflkzkhc kck jknvchehc pflhyvz

bfzhcol, ehyfch jhyk dhwkl oykfczhwk jhlhb lhyvzhc hwhb jkpfyolfd lhyvzhc {hcn

evyhcn afyckd#

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Wfiflvb jklhevehc pfcfzhphc ehjhy jfcnhc bfcnnvchehc bfzojf

Wpfezyomozobfzyk vlzyh}kolfz zfylfikd jhdvlv jklhevehc pfcfczvhc phcahcn


55/86

ttt}k

nflobihcn bhewkbvb, bfwekpvc phcahcn nflobihcn zfywfivz wvjhd jkefzhdvk

jhlhb lkzfyhzvy# Dhl kck jkehyfchehc phcahcn nflobihcn wvhzv wfc{h~h jhphz

ifyifjh iklh jkzfczvehc phjh eocjkwk jhc hlhz {hcn ifyifjh#

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bfcjhphzehc eocwfczyhwk zfywfivz jhphz jkdkzvcn bfcnnvchehc cklhk hiwoypzk}kzhw

bolhy $+ jhyk lkzfyhzvy, jhlhb bfzhcol phjh phcahcn nflobihcn 976 cb jfcnhc

hiwoypzk}kzhw bolhyc{h 986;0 $Zdf Bfyge Kcjfew, 9008+# Goczod pfydkzvcnhc

jhphz jklkdhz phjh Lhbpkyhc ;, dhlhbhc 77#

Jhyk pfydkzvcnhc jkjhphzehc eocwfczyhwk pfcnvevyhc hjhlhd > bgn/bl jhc

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77: cb jfcnhc wfyhphc bhwkcn"bhwkcn 0,:7>0 jhc 0,8060 wfpfyzk zfylkdhz phjh

Nhbihy 8 jhc zhifl 8#

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56/86

ttt}kk

Zhifl 8# Jhzh Hiwoyihcwk jhyk Evy}h Wfyhphc Bhewkbvb

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bhewkbvb 976 cb jfcnhc bfcnnvchehc bfzhcol wfihnhk ilhcneo jhphz jklkdhz

phjh zhifl 9 jhc nhbihy 9 ifykevz kck#


57/86

ttt}kkk

Zhifl 9# Jhzh Evy}h Ehlkiyhwk jhyk Ckmfjkpkc IPMK

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58/86

tttkt

:#7 Pfcfczvhc Ehjhy Ckmfjkpkc jhlhb wfjkhhc zhilfz

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59/86

tl

bhwkcn jfcnhc 7 yfplkehwk jhc wfzkhp yfczhcn wpfwkmke bfcnhcjvcn >0& hchlkz jhc

70& ihev pfbihcjkcn# Goczod pfydkzvcnhc jhphz jklkdhz phjh Lhbpkyhc 8:,

dhlhbhc 7;#

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Yfczhcn Wpfwkmke

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jhc ihzhw evhczkzhwk $LOX+ {hcn jkpfyolfd jhyk pfcflkzkhc kck wfifwhy 0,9;9>

bgn/bl jhc 0,;>46 bgn/bl#


60/86

tlk

IHI ]

EFWKBPVLHC JHC WHYHC

6#8# Efwkbpvlhc

Bfzojf wpfezyomozobfzyk vlzyh}kolfz jhphz jknvchehc vczve pfcfzhphc

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bgn/bl jhc ihzhw evhczkzhwk $LOX+ 0,;>64 bgn/bl#

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zkjhe lfikd jhyk 880,0 & jhyk avblhd {hcn zfyzfyh phjh fzkefz#

6#9# Whyhc

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hzhvpvc bfzojf }olvbfzyk#


61/86

tlkk

JHMZHY PVWZHEH

Ivjh}hyk, $9008+# Zdf Bfyge Kcjft#Fcg{glopfjkh om Gdfbkghlw, Jyvnw, hcjIkolonkghlw# Zdkyzffczd Fjkzkoc# ^dkzfdovwf1 Bfyge - Go#, Kcg# Phnf

88>0#

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Pembahasan Skripsi Spektroskopi Mengenai "Pengukuran Kadar Nifedipin Dalam Sediaan Tablet...

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