neraca massa pabrik alkil poliglikosida

kapasitas 80000 ton/tahun dalam patii sagukapasitas kg per hari 242424.2 kg/hari pati 84.70%kapasitas kg per jam 10101.01 kg/jam air 14%basis (pati kering) 1000 kg/jam impuritis 1.30%berat pati 1180.638 kg/jam mol pati kering 6172.84 mol/jamair 165.2893 kg/jamimpuritis 15.34829 kg/jam 1. mixerberat pati 1180.638 kg/jammol pati:air #1:8mol air 49382.72 mol/jamberat air 888888.9 g/jam pati sagu 1180.638berat air total 888.8889 kg/jam komp pati 1000berat air yang ditamba 723.5996 kg/jam air 165.2893mol pati: butanol #1:8,5 impuritis 15.34829mol butanol 52469.14 mol/jamberat butanol 3882716 g/jamberat butanol 3882.716 kg/jammol pati:AL #1:6 2. butanolisismol AL 37037.04 mol/jamberat AL 6902963 g/jam pati 1000berat AL 6902.963 kg/jam air 888.8889pati:pTSA B #1:0.02326 butanol 3882.716mol pTSA B 143.5802 mol/jam impuritis 15.34829berat pTSA B 27311.83 g/jamberat pTSA B 27.31183 kg/jampati:pTSA T #1:0,0167 x=98% reaksi note: dalam reaksi harus molmol pTSA T 103.0864 mol/jam 6049.383 Pati Butanol BGberat pTSA T 19609.1 g/jam mula 6172.839506173 52469.14 -berat pTSA T 19.6091 kg/jam bereaksi 6049.382716 6049.383 6049.383mol pati:NaOH #1:0,0829 sisa 123.4567901728 46419.75 6049.383mol NaOH 511.7284 mol/jamberat NaOH 20469.14 g/jamberat NaOH 20.46914 kg/jam 3. transasetalisasi pTSAmol air:APG kasar#pela #1:1 Dodecanolberat H2O2 2% dari APG kasar

pati 20air 997.7778butanol 3435.062pTsa 27.31183BG 1592.574impuritis 15.34829

2835.951x=46,88% reaksi note: dalam reaksi harus mol

mixer1

2

reaktor butanolisis3

4

reaktor transasetalisasi

BG Dodecanol APG Butanol6049.383 37037.03703704 - -2835.951 2835.951 2835.951 2835.9513213.432 34201.08603704 2835.951 2835.951

e = 90% 4. polishing filter memisahkan pati,impuritis,

patipati 20 airair 997.7778 butanolbutanol 3644.922 pTsapTsa 46.92093 pati 18 BGBG 845.9751 impuritis 13.81346 impuritisimpuritis 15.34829 DodecanolDodecanol 6374.398 APGAPG 988.2438

5. separator memisahkan butanol dan air dengan produk atas berupa butanol 7.7% dan air 92,3%pada produk atas berupa air sebanyak kandungan air pada pati

0.105 aire= 98% butanol

butanol 3882.716 pati 2air 723.5996 air 997.7778

butanol 3644.922pTsa 46.92093

pati 1000 BG 845.9751 patiair 888.8889 impuritis 1.534829 airbutanol 3882.716 Dodecanol 6374.398 butanolimpuritis 15.34829 APG 988.2438 pTsa

pTsa 27.31183 BGimpuritisDodecanol

mol berat APGpati 123.4568 20air 6049.383 997.7778 6. tangki netralisasi NaOH 20.4691358butanol 46419.75 3435.062 Air 20.4691358pTsa 27.31183BG 6049.383 1592.574impuritis 15.34829

dalam reaksi harus mol pati 2 patiair air 19.95556 airbutanol 72.89844 butanol6049.383 pTsa 46.92093 pTsa6049.383 BG 845.9751 BG

impuritis 1.534829 impuritisDodecanol 6374.398 Dodecanol

19.6091 APG 988.2438 APG6902.963 NaOH

NaPTSx=100% reaksi note: dalam reaksi harus mol

NaOH pTSA NaPTS airmol berat m 511.7284 246.666 - -

pati 20 b 246.666 246.666 246.666 246.666air 997.7778 s 265.0624 0 246.666 246.666butanol 2835.951 3644.922pTsa 46.92093 e=98% al terdistilasi menjadi produk atas butanolBG 3213.432 845.9751 8. distilasi 1 Dodecanolimpuritis 15.34829 AirDodecanol 34201.09 6374.398 totalAPG 2835.951 988.2438

total 12933.59 kg/jam pati 2dalam reaksi harus mol air 44.86468

mixer 3

reaktor butanolisis

5

separator

tangki netralisasi

Distilasi

total umpa 13917.47 kg/jam butanol 72.89844BG 84.59751impuritis 1.534829 patiDodecanol 6374.398 airAPG 988.2438 butanolNaOH 10.6025 BG

memisahkan pati,impuritis, NaPTS 5.234746 impuritistotal 7584.375 Dodecanol

APG2 NaOH

997.7778 NaPTS3644.92246.92093845.97511.5348296374.398988.2438

Distilasi

memisahkan butanol dan air dengan produk atas berupa butanol 7.7% dan air 92,3%pada produk atas berupa air sebanyak kandungan air pada pati

977.8222 0.923 mol APG in 2835.9513572.024 0.077 9. Pelarutan air 51.04712

pati 2 pati 2air 0.897294 air 51.94441butanol 1.457969 butanol 1.457969

2 BG 84.59751 BG 84.5975119.95556 impuritis 1.534829 impuritis 1.53482972.89844 Dodecanol 127.488 Dodecanol 127.48846.92093 APG 988.2438 APG 988.2438845.9751 NaOH 10.6025 NaOH 10.60251.534829 NaPTS 5.234746 NaPTS 5.2347466374.398988.2438

0.50.5 7.penyaringan memisahkan BG dengan efisiensi 90 %

mol berat2

246.666 44.86468 pati 2 pati 272.89844 air 44.86468 air 44.86468

0 0 butanol 72.89844 butanol 72.89844845.9751 BG 845.9751 BG 761.3776 BG 84.597511.534829 impuritis 1.534829 NaPTS 47.11271 impuritis 1.5348296374.398 Dodecanol 6374.398 Dodecanol 6374.398988.2438 APG 988.2438 APG 988.2438

265.0624 10.6025 NaOH 10.6025 NaOH 10.6025246.666 52.34746 NaPTS 52.34746 NaPTS 5.234746

71.440476246.91

43.967396362.318

butanol 1.428809

tangki pelarutan

Dodecanol 124.9382e 98% distilasi 2 Air 0.879348

20.8972941.45796984.59751 pati 21.534829 air 0.897294

127.488 butanol 1.457969988.2438 BG 84.59751

10.6025 impuritis 1.534829 pati 25.234746 Dodecanol 127.488 air 0.017946

APG 988.2438 butanol 0.029159NaOH 10.6025 BG 84.59751NaPTS 5.234746 impuritis 1.534829

Dodecanol 2.549759APG 988.2438NaOH 10.6025NaPTS 5.234746

Distilasi

e=90%10. bleaching

H2O2 19.76488 0.3air 46.11805 0.7total 65.88292

pati 2air 0.017946butanol 0.029159BG 84.59751impuritis 1.534829Dodecanol 2.549759APG 988.2438 patiNaOH 10.6025 airNaPTS 5.234746 butanol

BGimpuritisDodecanolAPGNaOHNaPTS

Bleaching

kapasitas 50000 ton/tahun dalam patii sagukapasitas kg per hari 151515.15152 kg/hari pati 84.70%

kapasitas kg per jam 6313.1313131 kg/jam air 14%basis (pati kering) 11122.263449 kg/jam impuritis 1.30%berat pati 13131.361805 kg/jam mol pati ke 68655.95air 1838.3906528 kg/jamimpuritis 170.70770347 kg/jamberat pati 13131.361805 kg/jammol pati:air #1:8mol air 549247.57774 mol/jamberat air 9886456.3993 g/jamberat air total 9886.4563993 kg/jamberat air yang ditambahkan pada butanol 8048.0657465 kg/jammol pati: butanol #1:8,5 komponenmol butanol 583575.55134 mol/jamberat butanol 43184590.8 g/jamberat butanol 43184.5908 kg/jammol pati:AL #1:6mol AL 411935.6833 mol/jamberat AL 76776572.654 g/jamberat AL 76776.572654 kg/jampati:pTSA B #1:0.02326mol pTSA B 1596.9373323 mol/jamberat pTSA B 303769.41934 g/jamberat pTSA B 303.76941934 kg/jampati:pTSA T #1:0,0167 komponenmol pTSA T 1146.5543185 mol/jamberat pTSA T 218097.56247 g/jamberat pTSA T 218.09756247 kg/jammol pati:NaOH #1:0,0829mol NaOH 5691.5780243 mol/jamberat NaOH 227663.12097 g/jamberat NaOH 227.66312097 kg/jammol air:APG kasar#pelarutan #1:1berat H2O2 2% dari APG kasar

komponen

patiimpuritispTSABGtotal

mix point 6

komponen masuk9

fraksi

pati 0.000617impuritis 0.000474pTSA 0.016858BG 0.982051Dodekanol 0total 1


komponen masuk14

fraksibutanol 0pati 0.000117impuritis 8.983E-05pTSA 0.005493BG 0.186241Dodekanol 0.80806APG 0total 1

pemisahan

komponen masuk15

fraksibutanol 0.024788pati 0.000118impuritis 9.064E-05pTSA 0.005542BG 0.099823Dodekanol 0.752912APG 0.116726total 1

separator

komponen masuk16

fraksibutanol 0.027536pati 0.000131impuritis 0.000101pTSA 0.006157Dodekanol 0.836405APG 0.129671total 1

mix point 7

komponen masuk19

fraksipati 0.000135impuritis 0.000104pTSA 0.006331Dodekanol 0.860088APG 0.133342NaOH 0air 0total 1

reaktor netralisasi

komponen masuk21

fraksipati 0.000134impuritis 0.000103pTSA 0.006296Dodekanol 0.855363APG 0.13261NaOH 0.002747air 0.002747NapTS 0total 1

distliasi 1

komponen masuk keluar22 23

fraksi laju fraksipati 0.000134 11.12226 0impuritis 0.000103 8.535385 0pTSA 0.00063 52.1867 0Dodekanol 0.855363 70897.74 0.995976APG 0.13261 10991.51 0NaOH 0.001555 128.8974 0air 0.003283 272.1077 0.004024NapTS 0.006322 524.0014 0total 1 82886.1 1

distilasi 2


fraksi laju fraksipati 0.000729 11.12226 0impuritis 0.000559 8.535385 0pTSA 0.00342 52.1867 0Dodekanol 0.232282 3544.887 1APG 0.720229 10991.51 0NaOH 0.008446 128.8974 0NapTS 0.034336 524.0014 0total 1 15261.14 1

bleaching

komponen masuk26 27

fraksi laju fraksipati 0.000935 11.12226 0impuritis 0.000718 8.535385 0pTSA 0.004388 52.1867 0Dodekanol 0.014903 177.2443 0APG 0.924161 10991.51 0NaOH 0.010838 128.8974 0NapTS 0.044058 524.0014 0h2o2 0 0 0.3air 0 0 0.7total 1 11893.49 1

filtrasi


fraksi laju fraksipati 0.000881 11.12226 0impuritis 0.371203 4686.912 1pTSA 0.004133 52.1867 0Dodekanol 0.014038 177.2443 0APG 0.5 6313.131 0NaOH 0.010209 128.8974 0NapTS 0.041501 524.0014 0h2o2 0.040625 512.937air 0.017411 219.8301total 1 12626.26 1

pelarutan

komponen masuk30 31

fraksi laju fraksi

pati 0.001385 11.12226 0impuritis 0.011669 93.73823 0pTSA 0.006496 52.1867 0Dodekanol 0.022064 177.2443 0APG 0.785891 6313.131 0NaOH 0.016046 128.8974 0NapTS 0.06523 524.0014 0h2o2 0.063853 512.937 0air 0.027366 219.8301 1total 1 8033.088 1

mix point 2

komponen

masuk keluar1 2 3

fraksi laju fraksi laju fraksi lajuair 1 8048.066 0 0 0.157089 8048.066

mol/jam butanol 0 0 1 43184.59 0.842911 43184.59total 1 8048.066 1 43184.59 1 51232.66

mix point 3komponen masuk keluar

3 4 5 6 Butanol fraksi laju fraksi laju fraksi laju fraksi laju Air

air 0.157089 43184.59 0.14 1838.391 0 0 0.152881 9886.456 totalbutanol 0.842911 8048.066 0 0 0 0 0.667791 43184.59pati 0 0 0.847 11122.26 0 0 0.171991 11122.26impuritis 0 0 0.013 170.7077 0 0 0.00264 170.7077 pTSApTSA 0 0 0 0 1 303.7694 0.004697 303.7694total 1 51232.66 1 13131.36 1 303.7694 1 64667.79

reaktor butanolisis separatorkomponen masuk keluar komponen masuk keluar

6 7 7 8fraksi laju fraksi laju fraksi laju fraksi laju

air 0.152881 9886.456 0.225088 11097.55 butanol 0.225088 11097.55 1 38205.66butanol 0.667791 43184.59 0.774912 38205.66 air 0.774912 38205.66 0 0pati 0.171991 11122.26 0.012094 222.4453 total 1 49303.21 1 38205.66impuritis 0.00264 170.7077 0.009281 170.7077pTSA 0.004697 303.7694 0.016516 303.7694BG 0 0 0.962108 17695.38total 1 64667.79 2 67695.52

sentrifusemasuk keluar e

7 10 11fraksi laju fraksi laju fraksi laju

0.012094 222.4453 0.565798 211.323 0.000617 11.122260.009281 170.7077 0.434202 162.1723 0.000474 8.5353850.016516 303.7694 0 0 0.016858 303.76940.962108 17695.38 0 0 0.982051 17695.38

1 18392.31 1 373.4953 1 18018.81

mix point 6

masuk keluar9 10 11 12laju fraksi laju fraksi laju fraksi laju

11.12226 0 0 0 0 0.000117 11.122268.535385 0 0 0 0 8.983E-05 8.535385303.7694 1 218.0976 0 0 0.005493 521.86717695.38 0 0 0 0 0.186241 17695.38

0 0 0 1 76776.57 0.80806 76776.5718018.81 1 218.0976 1 76776.57 1 95013.48


masuk keluar14 15

laju fraksi laju0 0.024788 2334.122

11.12226 0.000118 11.122268.535385 9.064E-05 8.535385

521.867 0.005542 521.86717695.38 0.099823 9399.78876776.57 0.752912 70897.74

0 0.116726 10991.5195013.48 1 94164.68

pemisahan

masuk keluar15 16 17

laju fraksi laju fraksi laju2334.122 0.027536 2334.122 0 011.12226 0.000131 11.12226 0 08.535385 0.000101 8.535385 0 0

521.867 0.006157 521.867 0 09399.788 0 0 1 9399.78870897.74 0.836405 70897.74 0 010991.51 0.129671 10991.51 0 094164.68 1 84764.89 1 9399.788

masuk keluar16 18 19

laju fraksi laju fraksi laju2334.122 1 2334.122 0 0 butanol11.12226 0 0 0.000135 11.12226 pati8.535385 0 0 0.000104 8.535385 impuritis

521.867 0 0 0.006331 521.867 pTSA70897.74 0 0 0.860088 70897.74 Dodekanol10991.51 0 0 0.133342 10991.51 APG84764.89 1 2334.122 1 82430.77 total

masuk keluar pati19 20 21 impuritis

laju fraksi laju fraksi laju pTSA11.12226 0 0 0.000134 11.12226 Dodekanol8.535385 0 0 0.000103 8.535385 APG

521.867 0 0 0.006296 521.867 total70897.74 0 NaOH 0.855363 70897.7410991.51 0 0 0.13261 10991.51

0 0.5 227.6631 0.002747 227.66310 0.5 227.6631 0.002747 227.6631

82430.77 1 455.3262 1 82886.1

masuk keluar21 22 pati

laju fraksi laju impuritis11.12226 0.000134 11.12226 pTSA8.535385 0.000103 8.535385 469.6803 Dodekanol

521.867 0.00063 52.1867 9.106525 APG70897.74 0.855363 70897.74 NaOH10991.51 0.13261 10991.51 air227.6631 0.001555 128.8974 total227.6631 0.003283 272.1077

0 0.006322 524.0014 reaksi82886.1 1 82886.1 pTSA

2743.4922469.142274.3492

52.1867

keluar23 24

laju fraksi laju0 0.000729 11.12226 fraksi laju0 0.000559 8.535385 pati 0.000134 11.122260 0.00342 52.1867 impuritis 0.000103 8.535385

67352.85 0.232282 3544.887 pTSA 0.00063 52.18670 0.720229 10991.51 Dodekanol 0.855363 70897.740 0.008446 128.8974 APG 0.13261 10991.51

272.1077 0 0 NaOH 0.001555 128.89740 0.034336 524.0014 air 0.003283 272.1077

67624.96 1 15261.14 NapTS 0.006322 524.0014total 1 82886.1

15261.14

keluar25 26

laju fraksi laju0 0.000935 11.122260 0.000718 8.5353850 0.004388 52.1867 fraksi laju

3367.643 0.014903 177.2443 pati 0.000729 11.122260 0.924161 10991.51 impuritis 0.000559 8.5353850 0.010838 128.8974 pTSA 0.00342 52.18670 0.044058 524.0014 Dodekanol 0.232282 3544.887

3367.643 1 11893.49 APG 0.720229 10991.51NaOH 0.008446 128.8974NapTS 0.034336 524.0014

22

24

total 1 15261.14

masuk keluar27 28

laju fraksi laju0 0.000881 11.122260 0.371203 4686.9120 0.004133 52.18670 0.014038 177.24430 0.5 6313.1310 0.010209 128.89740 0.041501 524.0014 fraksi laju

219.8301 0.040625 512.937 pati 0.000935 11.12226512.937 0.017411 219.8301 impuritis 0.000718 8.535385

732.7671 1 12626.26 pTSA 0.004388 52.1867Dodekanol 0.014903 177.2443APG 0.924161 10991.51NaOH 0.010838 128.8974NapTS 0.044058 524.0014total 1 11893.49

keluar e 98%29 30

laju fraksi laju fraksi laju0 0.001385 11.12226 pati 0.000881 11.12226

4593.173 0.011669 93.73823 impuritis 0.371203 4686.9120 0.006496 52.1867 pTSA 0.004133 52.18670 0.022064 177.2443 Dodekanol 0.014038 177.24430 0.785891 6313.131 APG 0.5 6313.131 impuritis0 0.016046 128.8974 NaOH 0.010209 128.89740 0.06523 524.0014 NapTS 0.041501 524.0014

0.063853 512.937 h2o2 0.040625 512.9370.027366 219.8301 air 0.017411 219.8301

4593.173 1 8033.088 total 1 12626.26

masuk keluar31 32 laju air 72% APG

laju fraksi laju

26

28

29

30

0 0.000884 11.12226 fraksi laju0 0.007452 93.73823 pati 0.001385 11.122260 0.004149 52.1867 impuritis 0.011669 93.738230 0.014091 177.2443 pTSA 0.006496 52.18670 0.501897 6313.131 Dodekanol 0.022064 177.24430 0.010247 128.8974 APG 0.785891 6313.1310 0.041658 524.0014 NaOH 0.016046 128.89740 0.040779 512.937 NapTS 0.06523 524.0014

4545.454 0.378842 4765.284 h2o2 0.063853 512.9374545.454 1 12578.54 air 0.027366 219.8301

total 1 8033.088

fraksi 1 fraksi 1

air 8048.066 butanol 43184.59

berat fraksibutanol 43184.59 0.842911air 8048.066 0.157089total 51232.66 1

fraksi berat fraksi berat0.842911 43184.59 Pati 0.847 11122.260.157089 8048.066 Air 0.14 1838.391

1 51232.66 Impuritis 0.013 170.7077total 1 13131.36

fraksi berat1 303.7694 laju fraksi

air 9886.456 0.152881butanol 43184.59 0.667791pati 11122.26 0.171991impuritis 170.7077 0.00264 air 0.225088pTSA 303.7694 0.004697 butanol 0.774912

keluar total 64667.79 1 total 19

fraksi laju fraksi laju0 0 air 0.152881 9886.4561 11097.55 butanol 0.667791 43184.59 pati1 11097.55 pati 0.171991 11122.26 impuritis

impuritis 0.00264 170.7077 pTSApTSA 0.004697 303.7694 BGtotal 1 64667.79 total

reaksi x=98 %pati butanol BG air

m 68655.95 583575.6 0 0b 67282.83 67282.83 67282.83 67282.83s 1373.119 516292.7 67282.83 67282.83 mol

222.4453 38205.66 17695.38 1211.091 kg/jam

95%fraksi laju

fraksi laju

1

3

2

6

5

4

3

6 7

7 11

10

pati 0.012094 222.4453impuritis 0.009281 170.7077pTSA 0.016516 303.7694 fraksi laju pati 0.000617 11.12226BG 0.962108 17695.38 pati 0.565798 211.323 impuritis 0.000474 8.535385total 1 18392.31 impuritis 0.434202 162.1723 pTSA 0.016858 303.7694

total 1 373.4953 BG 0.982051 17695.38total 1 18018.81

fraksi lajupTSA 1 218.0976 fraksi laju

Dodekanol 1 76776.57

fraksi laju

pati 0.000617 11.12226impuritis 0.000474 8.535385pTSA 0.016858 303.7694BG 0.982051 17695.38 fraksi lajutotal 1 18018.81

pati 0.000117 11.12226impuritis 8.983E-05 8.535385pTSA 0.005493 521.867BG 0.186241 17695.38Dodekanol 0.80806 76776.57total 1 95013.48

fraksi laju fraksi laju

butanol 0.024788 2334.122pati 0.000117 11.12226 pati 0.000118 11.12226impuritis 8.983E-05 8.535385 impuritis 9.064E-05 8.535385pTSA 0.005493 521.867 pTSA 0.005542 521.867BG 0.186241 17695.38 BG 0.099823 9399.788Dodekanol 0.80806 76776.57 Dodekanol 0.752912 70897.74total 1 95013.48 APG 0.116726 10991.51

total 1 94164.68reaksi x 46.88%BG Dodecanol APG Butanol67282.83 411935.7 0 031542.19 31542.19 31542.19 31542.1935740.64 380393.5 31542.19 31542.19 mol9399.788 70897.74 10991.51 2334.122 kg/jam

10

11

12

14

13

1514

e 100%

fraksi laju fraksi lajubutanol 0.024788 2334.122 butanol 0.027536 2334.122pati 0.000118 11.12226 pati 0.000131 11.12226impuritis 9.064E-05 8.535385 impuritis 0.000101 8.535385pTSA 0.005542 521.867 BG 1 9399.788 pTSA 0.006157 521.867BG 0.099823 9399.788 Dodekanol 0.836405 70897.74Dodekanol 0.752912 70897.74 APG 0.129671 10991.51APG 0.116726 10991.51 total 1 84764.89total 1 94164.68

fraksi lajuButanol 1 2334.122

fraksi laju0.027536 2334.1220.000131 11.12226 fraksi laju0.000101 8.535385 pati 0.000135 11.122260.006157 521.867 impuritis 0.000104 8.5353850.836405 70897.74 pTSA 0.006331 521.8670.129671 10991.51 Dodekanol 0.860088 70897.74

1 84764.89 APG 0.133342 10991.51total 1 82430.77

fraksi laju fraksi laju tangki berpengaduk 0.000135 11.12226 NaOH 0.5 227.66310.000104 8.535385 air 0.5 227.66310.006331 521.867 total 1 455.32620.860088 70897.740.133342 10991.51

1 82430.77 fraksiNaOH 1

fraksi lajupati 0.000134 11.12226impuritis 0.000103 8.535385pTSA 0.006296 521.867Dodekanol 0.855363 70897.74APG 0.13261 10991.51NaOH 0.002747 227.6631air 0.002747 227.6631total 1 82886.1

fraksi laju0.000134 11.12226

15 16

17

16

19

18

2019

21

2221

0.000103 8.535385 fraksi laju0.006296 521.867 pati 0.000134 11.122260.855363 70897.74 impuritis 0.000103 8.535385

0.13261 10991.51 pTSA 0.00063 52.18670.002747 227.6631 Dodekanol 0.855363 70897.740.002747 227.6631 APG 0.13261 10991.51

1 82886.1 NaOH 0.001555 128.8974air 0.003283 272.1077

x 90% NapTS 0.006322 524.0014NaOH NapTS air total 1 82886.15691.578 0 02469.142 2469.142 2469.1423222.436 2469.142 2469.142 mol128.8974 524.0014 44.44456 kg/jam

fraksi lajudodecanol 0.995976 67352.85air 0.004024 272.1077total 1 67624.96

fraksi lajupati 0.000729 11.12226impuritis 0.000559 8.535385pTSA 0.00342 52.1867Dodekanol 0.232282 3544.887APG 0.720229 10991.51NaOH 0.008446 128.8974NapTS 0.034336 524.0014total 1 15261.14

fraksi lajudodecanol 1 3367.643

fraksi lajupati 0.000935 11.12226impuritis 0.000718 8.535385pTSA 0.004388 52.1867

22

24

23

26

25

Dodekanol 0.014903 177.2443APG 0.924161 10991.51NaOH 0.010838 128.8974NapTS 0.044058 524.0014total 1 11893.49

fraksi lajuh2o2 0.3 219.8301air 0.7 512.937total 1 732.7671

fraksi lajupati 0.000881 11.12226impuritis 0.000676 8.535385impuritis 2 0.370527 4678.376pTSA 0.004133 52.1867Dodekanol 0.014038 177.2443APG 0.5 6313.131NaOH 0.010209 128.8974NapTS 0.041501 524.0014air 0.040625 512.937h2o2 0.017411 219.8301

1 12626.26

fraksi lajupati 0.001385 11.12226impuritis 0.011669 93.73823pTSA 0.006496 52.1867Dodekanol 0.022064 177.2443

fraksi laju APG 0.785891 6313.1311 4593.173 NaOH 0.016046 128.8974

NapTS 0.06523 524.0014h2o2 0.063853 512.937air 0.027366 219.8301total 1 8033.088

fraksi lajuair 1 4545.454

28

27

30

29

31

fraksi lajupati 0.000884 11.12226impuritis 0.007452 93.73823pTSA 0.004149 52.1867Dodekanol 0.014091 177.2443 1000 567.6121APG 0.501897 6313.131 11122.26 6313.131NaOH 0.010247 128.8974NapTS 0.041658 524.0014h2o2 0.040779 512.937air 0.378842 4765.284total 1 12578.54

32

air 11097.55 0.163933butanol 38205.66 0.564375pati 222.4453 0.003286impuritis 170.7077 0.002522pTSA 303.7694 0.004487BG 17695.38 0.261397total 67695.52 1

11097.5538205.66 fraksi49303.21 butanol 1

fraksi laju separator

0.012094 222.4453 fraksi laju0.009281 170.7077 air 0.225088 11097.550.016516 303.7694 butanol 0.774912 38205.660.962108 17695.38 total 1 49303.21 fraksi

1 18392.31 air 1

4993.73210899.82

7

9

8

tangki berpengaduk fraksi lajuAir 1 227.6631

laju227.6631 fraksi laju

NaOH 0.5 227.6631Air 0.5 227.6631

455.3262komponen masuk keluar

33 35 35fraksi laju fraksi laju fraksi laju

NaOH 1 227.6631 0 0 0.5 227.6631air 0 0 1 227.6631 0.5 227.6631total 1 227.6631 1 227.6631 1 455.3262

33 35

34

laju38205.66

laju11097.55

KomponenAliran Proses

1 2 3 4 5 6

Tekanan (atm)Q (kJ/ kg)Laju Alir (kg/jam)

Neraca Massa Komponen (kg/jam)Butanol - 47503.05 47503.05 - - 47503.05Air 8852.872 - 8852.872 2022.230 - 10875.1Pati - - - 12234.49 - 12234.49Impurities - - - 187.778 - 187.7785pTSA - - - - 334.146 334.146Butil Glikosida - - - - - -Dodekanol - - - - - -Alkil Poliglikosida - - - - - -Sodium Hidroksida - - - - - -NaPTS - - - - - -Hidrogen Peroksida - - - - - -Total 8852.872 47503.050 56355.922 14444.498 334.146 71134.565

Temperatur (oC)

Aliran Proses7 8 9 10 11 12 13

Neraca Massa Komponen (kg/jam)47503.05 42026.23 42026.23 - 42026.2 - -10875.1 12207.3 12207.3 - - 12207.3 -

12234.49 244.6898 - 244.6898 - - 244.6898187.7785 187.7785 - 187.7785 - - 187.7785334.146 334.1464 - 334.1464 - - 334.1464

- 19464.92 - 19464.92 - - 19464.92- - - - - - -- - - - - - -- - - - - - -- - - - - - -- - - - - - -

71134.565 74465.065 54233.530 20231.535 42026.230 12207.300 20231.535

Aliran Proses14 15 16 17 18 19 20

Neraca Massa Komponen (kg/jam)- - - - - - 2567.534

- - - - - -232.4553 12.23449 - - 12.23449 12.23449 12.23449178.3896 9.388924 - - 9.38892 9.38892 9.38892

- 334.1464 239.9073 - 574.0537 574.0537 574.0537- 19464.92 - - 19464.92 19464.92 10339.77- - - 84454.23 84454.23 84454.23 77987.51- - - - - - 12090.66- - - - - - -- - - - - - -- - - - - - -

410.845 19820.690 239.907 84454.230 104514.827 104514.827 103581.151

Aliran Proses21 22 23 24 25 26 27

Neraca Massa Komponen (kg/jam)- 2567.534 - 2567.534 - - -- - - - - - 250.4294- 12.23449 - - 12.23449 - -- 9.38892 - - 9.38892 - -- 574.0537 - - 574.0537 - -

10339.77 - 10339.77 - - - -- 77987.51 - - 77987.51 - -- 12090.66 - - 12090.66 - -- - - - - 250.4294 -- - - - - - -- - - - - - -

10339.770 93241.381 10339.770 2567.534 90673.847 250.429 250.429

Aliran Proses28 29 30 31 32 33 34

Neraca Massa Komponen (kg/jam)- - - - - - -

250.4294 250.4294 826.8310 826.831 - - -- 12.23449 12.23449 12.23449 - 12.23449 12.23449- 9.38892 9.38892 9.38892 - 9.38892 9.38892- 574.0537 574.0537 574.0537 - 574.0537 574.0537- - - - - - -- 77987.51000 77987.51 77987.51 3704.407 194.9688 194.969- 12090.66000 12090.66 12090.66 - 12090.66 12090.66

250.4294 250.4294 141.7822 141.7822 - 141.7822 141.7822- - - 576.40160 - 576.4016 576.4016- - - - - - -

500.859 91174.706 91642.460 92218.862 3704.407 13599.490 13599.490

Aliran Proses35 36 37 38 39 40 41

Neraca Massa Komponen (kg/jam)- - - - - - -- 564.2307 564.2307 564.2307 564.2307 - 5000

12.23449 - 12.23449 12.23449 12.23449 - -9.38892 - 5155.603 5155.603 257.7801 4897.823 -

574.0537 - 574.0537 574.0537 574.0537- - - - - - -

194.969 - 194.969 194.969 194.969 - -12090.66 - 6944.444 6944.444 6944.444 - -141.7822 - 141.7822 141.7822 141.7822 - -576.4016 - 576.4016 576.4016 576.4016 - -

- 241.8132 564.2307 564.2307 564.2307 - -13599.490 806.044 14727.949 14727.949 9830.126 4897.823 5000

Aliran Proses42

Neraca Massa Komponen (kg/jam)-

5241.81312.23449257.7801574.0537

-194.96886944.444141.7822576.4016564.2307

14507.709

komponenaliran

1 2 3 4 5 6 7

Tekanan (atm)Q (kJ/ kg)Laju Alir (kg/jam)

neraca massa komponen (kg/jam)Butanol 47503.05Air 8852872PatiImpuritiespTSAButil GlikosidaDodekanolAlkil PoliglikosidaSodium HidroksidaNaPTSHidrogen PeroksidaTotal

8,888,888

Temperatur (oC)

aliran8 9 10 11 12 13 14 15 16 17

neraca massa komponen (kg/jam)

aliran18 19 20 21 22 23 24 25 26 27


aliran28 29 30 31 32 33 34 35 36 37


aliran38 39 40 41 42


neraca massa pabrik alkil poliglikosida

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