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Koppers IncGeneral InformationID Branch SIC Jçounty Basin Start End876 lEnergy and Transportation 12491 IGrenada Yazoo River 111/09/198 1 1

Addressrphysical Address (Primary) Mailing Address1 Koppers Drive

P0 Box 160Tie Plant, MS 38960Tie Plant, MS 38960

TelecommunicationsType

Address or PhoneWork phone number1(662) 226-4584, Ext. 11

Alternate I Historic Al IdentifiersAlt ID Alt Name Alt Type Start Date End Date2804300012 Koppers Inc Air-AIRS AFS 10/12/2000096000012 Koppers, Inc. Air-Title V Fee Customer 12/11/2006096000012 Koppers Industries, Inc. Air-Title V Operating 03/11/1997 03/01/2002096000012 Koppers Industries, Inc. Air-Title V Operating 01/13/2004 03/26/2007096000012 Koppers Inc Air-Title V Operating 03/26/2007 01/01/2009MSR220005 Koppers Industries, Inc. GP-Wood Treating 09/25/1992MSD007027543 Koppers Industries, Inc. Hazardous Waste-EPA ID 08/27/1999HW8854301 Koppers Industries, Inc. Hazardous Waste-TSD 06/28/1988 06/28/1998HW8854301 Koppers Industries, Inc. Hazardous Waste-TSD 11/10/1999 03/26/2007HW8854301 Koppers, Inc. (Owner) Hazardous Waste-TSD 03/26/2007 09/30/2009876 Koppers Industries, Inc. Historic Site Name 11/09/1981 12/11/2006876 Koppers, Inc. Official Site Name 12/11/2006MSPO9O300 Koppers Industries, Inc. Water-Pretreatment 11/14/1995 11/13/2000MSPO9O300 Koppers Industries, Inc. Water-Pretreatment 09/18/200 1 08/31/2006MSPO9O300 Koppers Inc Water-Pretreatment 03/26/2007 02/28/2012MSUO81O8O Koppers Industries, Inc. Water-SOP 11/09/1981 11/30/1985

Regulatory Programs

EndProgram

SubProgram Start DateDateAir

Title V - major 06/01/1900Hazardous WasteLarge Quantity Generator 08/27/1999Hazardous WasteTSD - Not Classified 06/28/1988WaterBaseline Stormwater 01/01/1900WaterPTCIU 11/14/1995Water PT CIU - Timber Products

11/14/1995Processing (Subpart 429)WaterPTSIU 11/14/1995

Locational DataLatitude Longitude Metadata

S / T / R Map Links1I

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ENSEARCH - Agency Interesjtai1sPage 2 of 2

33 0 44’ 3 .00 89 O 47 ‘ 8 .06 Point Desc: PG- Plant Entrance Section: SWIMS(033.734167) (General). Data collected by Mike Hardy Township: TerraServer

(089.785572) on 11/8/2005. Elevation 223 feet. Justinside entrance gate. Range: Map It

Method: GPS Code (Psuedo Range)Standard Position (SA Off)Datum: NAD83

___________ __________

Type: MDEQ

__________ ________

4/3/2007 12:58:30 PM

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Mississippi Department of Environmental Quality(J Office of Pollution Control

1-sys 2000 Master Site Detail ReportSite Name: Koppers Industries IncPHYSICAL ADDRESS

OTHER INFORMATIONLINE 1: Tie Plant RoadMASTER ID: 000876LINE 2:COUNTY: GrenadaLINE 3:REGION NROMUNICIPALITY: Tie PlantSIC 1: 2491STATE CODE: MSAIR TYPE: TITLE VZIP CODE: 38960-HW TYPE: TSD

MAILING ADDRESS SOLID TYPE:LINE 1: P0 Box 160 WATER TYPE: INDUSTRIALLINE 2: BRANCH: EnergyLINE 3:

ECED CONTACT:MUNICIPALITY: Tie Plant Collier, MelissaSTATE CODE: MS

BASIN:ZIP CODE: 38960-

rA1RPRssiP [1 PSD EINSPS El NESHAPSEIMACT

1-sys Master Site Detail ReportPage 1 of 2

Mississippi Department of Environmental QualityOffice of Pollution Control

;—__---_----____- -------------------PROGRAM PERMIT TYPE PERMIT # MDEQ PERMIT CONTACT ACTIVEAIR TITLE V 096000012 Burchfield, David YESWATER PRE-TREATMENT MSP090300 Collins, Bryan YESHAZ. WASTE TSD HW8854301

YESHAZ. WASTE EPA ID MSD007027543

YESHAZ. WASTE TSD HW8854301 Stover, Wayne YES

Compliance Actions-_______MEDIA ACTIVITY TYPE SCHEDULED COMPLETED INSPECTED BHAZ WASTE Financial Record Review 1/18/00 1/18/00 Twitty, Russ

WATER CMI - PRETREATMENTWhittington, DarryailWATER CEI - PRETREATMENT 9/30/00 Twitty, Russ

WATER CEI - NA 9/30/00 Twitty, RussHAZ WASTE Compliance Evaluation Inspection 9/30/00 Twitty, RussAIR State Compliance Inspection 9/30/00 Twitty, RussWATER CEI - NA 3/2/99 3/2/99 Twitty, RussHAZ WASTE Compliance Evaluation Inspection 3/2199 3/2/99 Twitty, RussAIR State Compliance Inspection 3/2/99 312199 Twitty, Russ

1-sys Master Site Detail ReportPage 2 of 2

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.,,, IO)’PERS COMPANY. INC.

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to totem II..’ rhe noenorl wore,.oI. or. p.op.ly ,Io,.,l,,d rI,., ..I..d par boqed.nelted nod lolrolid erred ore .r. prot” uond,r,ue br I osprer r,r.uer,rr.,,i, to tie. erp.i.e.i-I.rikrltnnr Cr) Ihp tlepntrr,enb pI Jrnn.pnei.rr.oe.OPPflS COMPANY. Ok.. chl)).b,

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NOTICE OF SHIPMENt AiI’

FOR CHEMICAL EMERGENCIES. SPII’ lr

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This Memorandumis on osknowledgnr.nt that a Bill of Lading ho, bein iuued and is notthe Original 8.11 of Lading, nor o copy or duplicate, covering th propertynamed herein, and is intended so1eiy for filing or record.

F9TO BE PAID BY f-j PLACARDEDL.J SHIPPER [_JCONS1ONEEMT TO

RAIL

ole Where Ike late IS dependent an caine. shippers are required to stale specitically in writingreleased or declaled salue at the pIoserty The agreed or declaied value at the property is herebyleg hg the stripper to be not exceeding 165 cents per pnund or each disirihutlon package1 is a cerrif that the chore corned materIals are properly clarsified. dercribrd, parlcccgedirked and luinnird inr,d are, proper condition foi tranrpartntion according Ia the applicable5olotiunc of the Deportrnrnt of TiuniporlotionPPERS COMPANY. lNC., Shlpp,e,

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4—ORANDUM COPY OF STRAIGHTOF LADING—SHORT FORM

RECEIVED, oublect to I he classIfIcatIons and torlffo In effect on lb. dot, of lieu, of thu BIll at LadIng,FROM KOPPERS COMPANY, INC. AT ThiYi T - RO$t. L.1

KG35€75

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the property described below, in apparent good order, roerpr as noted iconfents end condition of contents aI packager onknorn, marked, consigned and destined as indicated below. whrc

said company the ao,d company being undersfoad throughout this contract as meaning any personal corporation in possession alike property under the conlractl agrees to carry to its asic

place of delinery at soid destination, fair crc aan road or its awn 001cr lice, otherwise to deticer to another carrie. on the route to said destination his mnintuatly agreed. as ra satin corrrer of

or any of seid property acer allot aoy portion of said route to destinotion, and as to each party at any time interested in allot airy af said property, that every serorce robe prrformed here’

under shall be coblect to all the conditions nor prohibited by arc, whether printed or written, hrre,n ceeroined, including clansificatnan bill, of lading condiliunc. which are hereby agreed

to by the shipper and accepted for hiwself and his ossigns

CONSIGNEDTO KOPPERS CO. INC.STREET ADDRESS .ri FLN LNJD bôDESTINATION GREhADA , MS.NAME OF

CARORVEh4.lN LNOCARRIER L)JUiI

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ROUTE

CONSIGNEE’S NOTIFICATION ADDRESS

HM DOT SHIPPING NAME/HAZARD CLASS / DESCRIPTION OF ARTICLES, SPECIAL(IF APPLICABLE) / MARKS & EXCEPTIONS

IF CHARGES ARE TOeE PREPALD WRITEOff STAMP HERE“TO BE PREPAID”

WEIGHTSCSJCCT TO COOsECTiOr.

CLASSOR f

RATECORROSIVE SOLID, NOS/CORROSIVE MATERIAL/UN 1759/OIL CRUDE COAL TAR

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NAPHTHALENE/ORM-A/UN 1334—

NAPHTHALENE/ORM-A/UN_1334/CRUDE_NAPHTHALENE 0OILc_CREOSOTE_COAL_TAR_SOLUTION0

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TAR_OR_PITCH,_COAL_OR_PETROLEUM._PAVINGr_ROOFING0CRUDE COAL TAR0OIL, CRUDE COAL TAR

COAL TAR DISTILLATE/FLAMMABLE LIQUID/UN 1 136/CRUDE HEAVY SOLVENT NAPHTHABINDER, ELECTRODE77 )RUM — OILr CREOSOTE

0COATING SOLUTION/FLAMMABLE LIQUID UN 1139/ 0—

ROOFING COATING ASPHALTr PITCH OR TAR BASECEMENTc ROOFING LIQUID/FLAMMABLE LIQUID/NA 1 133/ROOFING CEMENTc NOI 0ROOFING CEMENT, NOI

0FELT OR PAPERr BUILDING, ROOFING, OR SHEATHING 0—

PAINTS LACQUER OR VARNISHc NOI, LIQUID0

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PAINT/FLAMMABLE LIQUID/UN 1263/PAINT. LACQUER OR VARMSHNOI—PAINT RELATED MATERIAL/FLAMMABLE LIQUID/NA 1263/COMPOUND, PAINT OR LACQUER THINNINGPAINT, DRY, LUMP OR POWDERED

0COMPOUNDr_PAINT_THINNINGROOFING,_NOIBN,_COMPOSITION_OR_PREPARED

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C.O.D. S TENDEREDOR

BYPf,ACARO.TRIJCe

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ubiect to Section 7 of Conditions of appficoblc bill of lading, if this shipment in to be dohicered fa ii’tz’’’””SIfElL

r cons gnee aiirfiuut e000rse eli thir consignor, the consrgnur shall cute the fallowing statement,— OUTAGE

to sorrier shall flat make delieery of this shipment withos,I payment of freight and 01,1 y’jho, lawful chargesAL6$1t ‘‘fl’ r

DOMEKOPPERS COMPANY. INC.

‘ INNAGEOICOcr,ai.ni) pee —_* See.* below

rOTAL

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_AGENT

peenn,r’leur POST Cit FISt ,,liuef 5501 SiiiPPfK434 se’,Eeului AVeNili Pill 550009 ya 15219

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Shipper hereby ncrlifiec that this shipmrnr in rairectiy described. ccrieceright is sha,.n arid is roinlecr to serif inn lion ,ncrording Icc Liyirewc,il ninhniiidiclia

PERcy’ “ ,l i i i PER

CHARGES ADVANCED

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NOTICE OF SHIPMENTMEMO COPY OF BILL (1FOR CHEMICAL MRtJ(IC cn•e .5--.-

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MISSOUR EPARTMENT OF NATURAL RESOURCES

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isbn of Environmental Quality‘— Waste Management ProgramBox 176 Jefferson City, MIssouri 65102

314-751-3176HAZARDOUS WASTE MANIFEST

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Please prmt or type (Form designed for use on elite (12-pitch) typewriter.)Form Approved. 0MB No. 2050-0039, Expires 9-30-88

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INSTRUCTIONS FbR THE COMPLETIC QF1)4-. iRM ARE ON A“FPARAFE SHEE’f. -

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16 GENERATOR’S CERTIFICATiON: lherebydeciarethat the contents of this consignment are fuliyand accuratelydescrlbed above by propershipping nameand areciasaified, packed, marked, and

labeled, and are in alt respects in proper condition for transport by highway according to applicable inlernational and national government regulations and applicable state reguiationsIt lam a large quantity operator, I cerlity that I have a program in place to reduce ihe volume and toxicity of waste generated to the degree I have determined lobe economically practicable and that I

have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment; OR. ill am a

small quantity generator. I have made a good faith effort to minimize my waste generation and select the best waste management method available to me that I can afford.

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HAZARDOUS WASTE MANIFESTPlease print or type (Form designed for use on elite (12-pitch) typewriter.)Form Approved. 0MB No. 2050-0039. Expires 9-30-68

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. —, ,‘if.’ )‘LkIt’%4 •.IS. GENERATOR’S CERTIFICATION: I herebydeclare that thecontentsot thisconsignmentareful) and accurateiydescribedaove byproparshipping name and areclassitied, packed, marked, and

labeled, and are in all respects In proper condition for transport by highway according to applltabie international and national government regulations and applicable state regulations.

it Ian, a iarge quantity operator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined lobe economically practicableand that I

have selected the practicable method of treatment, storage, ordisposal currently available tome which minimizesthe presentand future threat to human health and the environment: OR, if I am a

small quantity generator, I have made a good faith effort to minimize my waste generation and select the best waste management method available to me that I can afford.Printed/Typed Name

SignatureMonth Day Year

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- , •I/III17. Transporter I Acknowledgement of Receipt of Materials

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INSTRUCTIONSJOR THE COMPLETIbNOFThto PORM ARE ON ASEPARATE SHEET.ThIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.


EMERGENCY RESPONSSU.S. COAST GUARD140O44a02CHEM TREC

1-O-424-s3OODEPT. or NATURAL RESOURC

314-634-2436

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I A 11 1 iForm 9700-22 (Rev. 9-86) MDNR-HWQ 10 PREVIOUS EDITIONS ARE OBSOLETE

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December 28, 1987

fir. Ron MurphyKoppere Co. Inc.6740 Stadium DriveKansas City, Missouri

64129

Subject: Tank Sludge testing

Dear fir. Murphy:

The following are the test results for the three samplescollected on December 4, 1987.

Parameter Tested:

Tank testedSample 1

#1 CylinderSample 2

#2 CylinderSample 3

#3 work tankBTU/pound 12,551 14,930 14,272ArsenicBoronCopperChromium, totalZinc

All Sample resUlts wereAll Sample results were

156 mg/kg 1367.7 mg/kg 5.1

334 mg/kg 325

less than 1 mg/kgless than 10 mg/kgmg/kg 142mg/kg 8.3

318Should you have any questions, please feel free to call us at anytime. Thank you for the opporIun1ty to assist you in yourtesting needs. If you should need additional analytical set-vices,especially in the area of hazardous waste analysis, we wouldappreciate the opportunity to provide assistance.

Yours very truly,BLUE VALLEY LABORATORIES

Waymon E. Hofheins

1 •, IJLUL V4)QLY LAIJOIIATflOES12(5

Mi.ccion, Knncns (i(222I i’clcplwuc (91:3) :302-1:313

mg/kgmg/kgmg/kg

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MISSOURI DEPARTMENT OF NATURAL RESOURCESiNSTUCTIONOR THE GOM- -3ion of Environmental QualityPLETIOFTI4?SbRUAREONA

Ste Management Program EMIROENCYReSPONSEU.S. COAST GUARD1-800-424-sacs

sa.i’ssH.116. Jefferson City, Missoui,651Q2

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THIS JUitMt1ST BE USED

‘4451-1761-eoo-424-gaoo

FOR ALL MISSOURI-DESTINED

DEPT. OF NATURAL RESOURCHAZARDOUS WASTE MANIFEST

_______

Please print or type (Form designed for use on elite (12-pitch) typewriter.)Form Approved. 0MB No. 2050-0039, ExpIres 9-30-88

UNIFORM HAZAR DOUS I 1. Generators US EPA ID No. ManifestDocument No.

WASTE MANIFEST1,

. 1 Ii I3, Generator’s Name and Mailing Address

KO,P9t Co. Tru.

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16. GENERATOR’S CERTIFICATION: thereby declare that the contents of this consignment are fully and accuratelydescribed above by proper shipping name and are classified, packed, marked, and

labeled, and are in all respects In proper condition for transport by highway according to applicable international and national government regulations and applicable state regulations.

If lam a large quantity operator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined lobe economically practicable and that I W

have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment: OR. itt ama

Small quantity generator. I have made a good faith effort to minimize my waste generation and select the best waste management method available to me that I cart afford. z

Printed/i’ ad NameSignature

.

Month Day Year 217. Transporter 1 Acknowledgement of Receipt of Materials

Date

Printe4’Typed NameSIgnature

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Prlntedrryped NameSignature

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‘orm 8700-22 (R& 946) MONR-HWG 10 PREVIOUS EDiTION ARE OBSOLETE

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BLuE VLDQiy LABo1tATOChsP.O. Box 1205Mission, Kan.sns 90222Telephone (913) 392—1313

December 28, 1987

Mr. Ron MurphyICoppers Co, Inc.6740 Stadium DriveKansas City, Missouri

64129


Dear Mr. Murphy:


Parameter Tested:

Tank testedSample 1

*1 CylinderSample 2

*2 CylinderSample 3

*3 work tankBTU/pound 12,551 14,930 14,272

mg/kgmg/kgmg/kg

Should you have any questions, please feel free to call us at anytime. Thank you for the opportunity to assist you in yourtesting needs. If you should need additional analytical services,especially in the area of hazardous waste analysis, we wouldappreciate the opportunity to provide assistance.


Waymon E. Hofhelns

efr’

Arsenic All Sample results were less than 1 mg/kgBoron All Sample results were less than 10 mg/kgCopper 156 mg/kg 136 mg/kg 142Chromium, total 7.7 mg/kg 5.1 mg/kg 8.3Zinc 334 mg/kg 325 318

,_,._..--

- I

MISSOURI ARTMENT OF NATURAL RESOURCES

Qion of Environmental Quality

vaste Management ProgramBox 176 Jefferson City, Missouri 65102

314-751-3176

HAZARDOUS WASTE MANIFEST

____

Please print or type (Form designed for use on elite (12-pitch) typewriter.)Form Approved. 0MB No. 2050-0039, ExpIres 9-30-86

ENERAT0R

Ii. Generator’s US EPA ID No. Manifest 12. Page ._....L. Information in the shaded areasn 7 ocmept N { ot ._.i.._. is required by State law.I I I I I I I I I I I

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‘“ir ilii’ ‘t” ‘i flt”lRflt itich I JjrnlFl 1 rr’Tfc, frTprotct1ov..1.t,rn1tm fici1.1l’ Tot,erq Co. Inc. 74(’) ‘r. City, ‘o.16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked, andlabeled, and are In all respects In proper condition for transport by highway according to applicable international and national government regulations and applicable State regulationsIll am a large quantity operator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that Ihave selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health end theenvironment; OR, 111am asmall quantity generator, I have made a good faith effort to minimize my weate generation and select the best waste management method available to me that I can afford.Printed/Typed Name

Signature. - .., Month Day Year{t ‘t

. -(.) i I ,t I IT 17. Treneporter 1 Acknowledgement of Receipt of MaterIals-

. Date

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F Date 3Printed/Typed Name

SignatureMonth Day Year( Y Ic 1 • L //( (/ ( ( I i I

INSTRLTIONr FOR THE COMPLEtQN OF T BP0RM AREON ASEPARATE SHEET.THIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.


0 EulaGascy RUoNUU.S. COAST GUARD

1-8O0424CHEIS TREC14ea

DEPT. OF NATURAL RESOURCI314-534-243e

3. Generator’s Name and Mailing Address

ot,perc o. Tric.P.O. Box gan, City, M12q

4. Generator’s Phone

5. Transporter 1 Company Name6. US EPA ID Number

— ‘ I jiI7. Transporter 2 Company Name

8. US EPA ID Number

1111111111119. Dealgnsted Facility Name and Site Address 10. US EPA ID NumberVopner Co. Inc.Tie Plant flo.A (off )!irhay 51)Crena#ia, . I v P ‘ 7 0 g J,A11. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. C -

for Matetmca t.tst.ø AtSOsIiandOnØ Codee for Wastes LtItbd

‘A Form 8700-22 (Rev. 9-68) MDNR-HWG 10 PREVIOUS EDITIONS ARE OBSOLETE

BLUE \T/)Gy LAiJO1IATQP.O. Box 1205Misio,i, Knn5ns 002221ClC1)hOI)C (913) 302-1313

December 28, 1987

Mr. Ron MurphyICoppers Co, Inc.6740 Stadium DriveKansas City, Missouri

64129


Dear Mr. Murphy:


Parameter Tested:

Tank testedSample 1

*1 CylinderSample 2

*2 CylinderSample 3

413 work tankBTU/pound 12,551 14,930 14,272ArsenicBoronCopperChromium, totalZinc

All Sample results were less than 1 mg/kgAll Sample results were less than 10 mg/kg156 mg/kg 136 mg/kg 142 mg/kg7.7 mg/kg 5.1 mg/kg 8.3 mg/kg334 mg/kg 325 318 mg/kgShould you have any questions, please feel free to call us at anytime. Thank you for the opportunity to assist you In yourtesting needs. If you should need additional analytical services,especially In the area of hazardous waste analysis, we wouldappreciate the opportunity to provide assistance.


Waymon E. Hofhelns

1.’,,,/,mw/ ,,ith ,,, f/iii4/iq

SNERAT0R

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper

shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according

to applicable international and national government regulations.Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization certification

under Section 3002(b) of RCRA, I also certify that! have a program in place to reduce the volume and toxicity of waste generated to the degree

I have determined to be economically practicable and I have selected the method of treatment, storage, or disposal currently available to me

which minimizes the present and future threat to human health and the environment.Printed/Typed Name

I Signature

Month Day YearRobert Mcrgan I :..:?‘f 1’ ‘; I najit I j

r 17, Transporter 1 Acknowledgement of Receipt of Materials

1Printed/Typed Name

Signalure.

Monlh Day YearBob Coffey I g 1618. Transporter 2 Acknowledgement of Receipt of MateaIs

fi/I oR I IS I (R

T Printed/Typed Name

I Signature

Month Day Year

SR

IIII

19. Discrepancy Indication Space

FAC

20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

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Printed/Typed Name

Signature,. -.

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UNIFORM HAZARDOUS 1. Genó.’s L EPA ID No.WASTE MANIFEST WrvV81q2

(N:__\)proved. 0MB No.2000-0404. Expires 7-31-86Manifest Document N—’ Page 1 I lntormation in the shaded areas1002 8 88 is not required by Federal law.

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3. Generator’s Name and Mailing AddressA. State Manifest Document NumberraCe

002888P0’x 0, Meriweather Rd. Guthr Ky k.23Li. B. StateGeneratorsiD

4. Generato?sPhone( 50, M36. USEPAIDNumber

5. Transporter 1 Company NameIrt Trurildng C •J /f tivyjg3c$7 0. Transporter’s Phon

238 83E. State Transporter’s ID

7. Transporter 2 Company Name8. US EPA ID NumberI F. Transporter’s Phone

9. Designated Facility Name and Site Address 10. US EPA ID Number G. State Facility’s IDKoppers Co Inc

NSflOO7O27513Box 160 Tie Plant toad

H. Facilitys PhoneTie Plant, Ms. •38960

—— M8DOO7O27SI3 1601 226 k58b________12. Containers 13. 14.

I I. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) Total Unit Waste No.

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No. Tvp Quantity WtNot —__________

a.

‘i‘,i ‘?) P

(on Hazardous process waste containing (b. Uad creosote—

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d.

J. Additional Descriptions for Materials Listed AboveK. Handling Codes for Wastes Listed Above

R Q Hazardous Substance, Liquid(of solid) NOS 0*1) .ENA 9188(ontsins Creosote)

15. Special Handling Instructions and Additional InformationWhen handling, wear protective equiptnent such as impervious gloves & eyeprotection. NON-HAZARDOUS WASTE-FOR TRACKING PURPOSES ONLY

Style F15R-6 Labelmaster. Div. of American Labelmaric Co Inc. 60646EPA Form 8700-22 (Rev. 4-85) Previous edition is obsolete.

cP

SPECTRIX MONROEVILLE

=TABLE 1: SUMMARY OF ANALYTICAL DATA PRODUCED ON 12/10/87 AT 15:02

=======================—====== ================—=========SAMPLE * RSLT.LNE

SOURCECROSS HEAT OF COMBUSTION87110583 I3TU/lb: 5620

SLUDGEARSENIC87110503 Arsenic. ug/Kg : <47500 SLUDGEBORON07110583 Boron, ug/g : 57000

SLUDGECHROMIUM871105B3 Chromium. ug/Kg : 39900

SLUDGECOPPER87110583 Copper. ug/Kg : 10800 SLUDGEZINC87110593 Zinc, ug/Kg : 48900

SLUDGEThe above I3TU results are on an as received basis.The above metal results are on a dr weight basis.

EMERGENCY RESPONSEU.S. COAST GUARD

1400-424-8902CHEM TREC

1-800-424-9300DEPT. OF NATURAL RESOURCES

314-634-2438

Form Approved, 0MB No. 2050-0039, ExpIres 9-30-88Information In the shaded areasIs required by State law.

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Please print or type (Form designed for use on elite (12-pitch) typewriter.)UNIFORM HAZARDOUS

WASTE MANIFEST

MI- EPARTMENT OF NATURAL RESOUFICES).. ivision of Environmental QualityWaste Management Program

P.0, Box 176 Jefferson City, Missouri 65102314-751-3176

HAZARDOUS WASTE MANIFESTii Generator’s US EPA ID No. ManIfest 2. Page —Document No.

3. Generator’s Name and Mailing AddressKcp1.S Cr it’c..‘c!5 5’)<c3i4$ CC “ cyslt?

4. Generator’s Phone (‘ c ) I S g’c

5. Transporter I Company Name a. us EPA ID Numberc. I’c ICtDttottCtd1tSt)tt(o7 Transporter 2 Company Name 8. US EPA ID Number

IlIttitti lii9. Designated Facility Name and Site Address 10. US EPA ID NumberQ.s Lt’c.

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15 Special Handling Instructions and Additional information,

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16 GENERATOR’SCERTIFICATION: I hereby declarelbat the contents 0! this consignment are fully and accuratdfydescrlbed above by propershipping name and are classified, packed, marked, andlabeled, and are in all respects in proper condition lot transport by highway according to applicable Inlernationat and national government regulations and applicable stale regulations.111am a large quantity operator, I certify that I haves program in place to reduce the volume and toxicity oI waste generated to the degree I have determined lobe economically practicable and that Ihave selected the practicable method of treatment, storage, or disposal currently available to me which minimizeslhe present and fuiurethreat to human health and the environment. OR. ill em asmall quantity generator. I have made a good failh effort to minimize my waste generation and select the beat waste management method available to me that I can altordPrinted/Typed Name

Slgnature,.Month Day Years I I

Date

T 17. Transporter 1 Acknowledgement 01 ReceIpt of MaterialsR

Month Day Year

A PrInted/Typed Name

£ l 11J12’Date

0 18. Transporter 2 Acknowledgement of ReceIpt of MaterialsPrlnledfTyped Name

I SignatureMonth Day Year

EIR

I I liii19. Discrepancy IndIcation Space

FAC

L 20. FacIlity Owner or Operator: Certification of receipt of hazardous materials covered by this merilfest except as noted In Item 19.I

DateT

PrInted/Typed NameSignature

Month Day YearC*y , ftiCc.LeUA-A/p ii‘A Form 8700-22 (Rev. 9-86) MONR-HWG 10 PREVIOUS EDITIONS ARE OBSOIETE a

INSTRUCTIONS FOR THE COMPIOtCiF1HiSFbA$AARE ON ASEPA1AIESHEE_..THIS DOCUMENT MUST BE USEDFOR ALL MISStURI-DESTINEDSHIPMENTS.

0’ENERAT0R

UNIFORM HAZARDOUS

WASTE MANIFEST3. Generator’s Name end Mailing Address

ç .Lls-

c’4. Genereto?s Phone ( ‘

Please print or type (Form designed tor use on elite (12-pitch) typewriter.)

MISSQURI RTMENT OF NATURAL RESOURCES(.. “ . )on of Environmental Quality\,,) Waste Management ProgramP.O. Box 176 Jefferson City, Missouri 65102

314-751-3176


C

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U.S. COAST GUARD

cHEM TREE1400424-9300

DEPT. OF NA11JtAL RESOURCES314-4-2436

Form Approved. 0MB No. 2050-0039, Expires 9-30-88

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5. Transporter 1 Company Name 6. US EPA ID Numbers c‘. I7. Transporter 2 Company Name 8. US EPA ID Number

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II. Generators US EPA ID No. ManIfest 2 Page InformatIon In the shaded areasDocument No. —_isi ‘cii ;i1jLol tart stew.

[9 DesIgnated Facility Name and Site Address

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t%’1 )iL116. GENERATOR’S CERTIFICATION: I herebydeclare Ihst the contents of this consignment are fully and accuratetyiescribed above by propershipping name nd are classified, packed, marked, andlabeled, and are in sit respects In proper condilion for Iraneporl by highway according to applicable International arid national government regulallons and applicable stale regulations.111am a targequanlilyoperalor, I certify thaI I have a program in place 10 reduce the volume snd tosicilyol waste generated to the degree I have delermlned lobe economically praclicableand Ihal Ihave selected the practicable method of trealrnenl. storage, or disposal currently available tome which minimizes the present and tuture lhrat to human health and the environment: OR, 111am asmall quantity generalor, I have made a good faith elton to minimize my waste gerrerallon and select the besl waste management method avsilable tome that lean afford.

-aU

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Printed/Typed Name Signature - Month Day Year—

vi. t”f3. ‘.

.-,,.-17. Transporter 1 Acknowledgement of Receipt of MaterialsDatePrinted/Typed Name SIgnature . Month Day Yearrr L

n .; :118. Transporter 2 Acknowledgement of Receipt of Materials .. . . DatePrinted/Typed Name Signature Month Day Year

11111 ti19. DIscrepancy Indication Space

CDt

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I20. FacIlity Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except aa noted in Item 19.

Data 3Printed/Typed Name Signature Month Day Yearc.y L. 41(LLL/ ,9‘

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A Form 8700-22 (Rev. 9-86) MDNR-HWG 10 PREVIOUS EDITIONS ARE O5SOLETE

BLUE4ALLEY LAnoiAhuEsP.O. Box 1265Mission, Kansas 66222Telephone (913) 362-1313

November 12, 1987

Mr. Ron MurphyKoppers Co, Inc.6740 Stadium DriveKansas City, Missouri

64129


Dear Mr. Murphy:

The following are the test results for the twoon October 30, 1987.

Parameter Tested:

samples collected

Tank testedSample 4if 6 tank

Sample 5if 7 tank

BTU/ pound 13,903 14, 877

ArsenicBoronChromium, totalCopperZinc

All Sample results wereAll Sample resu1ts were

2.6 mg/kg65.2 mg/kg

224.0 mg/kg

less thanless than

1.19.1

54.2

1 mg/kg10 mg/kgmg/kgmg / kgmg/kg

Should you have any questions, please feel free to call us at anytime. Thank you for the opportunity to assist you in yourtesting needs. If you should need additional analytical services,we would appreciate the opportunity to provide assistance.


Waymon E. l-lofheins

fr’af,u,n/ ,‘-•h ,•q

MISS RI f-ARTMENT OF NATURAL RESOURCESr on of Environmental Quality‘.-iste Management Program

P.O. Box 176 Jefferson City, Missouri 65102314-751-3176

HAZARDOUS WASTE MANIFESTPlease print or type (Form designed for use on elite j12-pitch) typewriter.)Form Approved. 0MB No. 2050-0039, Espires 9-30-88

3. Generator’. Name and Mailing Address

Krpi(& C. 1’.vI’)’.”

4. Garc PJ( s?i; 7. ,,_1.

]ijneator’e us EPA ID No.- Manifeat 12. Page _._L Information In the shaded areasDocument No. I

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of _._.....L... Is required by State law.

5. Transporter I Company Name6. US EPA ID Number

(‘,. f4( I !7. Transporter 2 Company Name

8. us EPA ID Number

I i9. Designated Facility Name end Site Address 10. us EPA ID NumberI.’ L C- •‘, ‘I

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I I II I I I I t III19. Discrepancy Indication Space

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DalePrinted/Typed Name

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. Month Day Year(i,.Y E. fi’t LLt.L //1r(.((uf,:,( I :j ; ‘1:7..;

INSTRUCTIONS FOR THE COMpLEt,)aorT 0RMAREONASEPARATE SHEET.THIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.


ENERGENCY RESPONSEU.S. COAST GUARD1-acO.424-aaC2CHEM TREC

1-500-424-9300DEPT. OF NA1URAL RESOURCE

314-634-2438

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16. GENERATOR’S CERTIFICATION: thereby declare that the Contents of this Consignment are fully and accurately described above by proper shipping name and are ctas4itied, packed, marked, andlabeled, and are in all respects in proper càndilion for transport by highway according to applicable international and national government regulations and applicable slate regulations.If lam a large quantity operator, I certify that I have a program in place to reduce Ihe volume and toxicity of waste generated to the degree I have determined lobe economically practicable and thaI Ihave selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR. 111am asmall quantity generator, I have made a good faith ellort to minimize my waste generation and select the best waste management method available to me that I can afford.

. Form 8700-22 (Rev. 9-86) MDNR-HWG 10 PREVIOUS EDITIONS ARE OBSOLETE

BLUEA2LEY LABoRAQIEsP.O. Box 1265Mission, Kansas 66222Telephone (913) 362-1313

November 12, 1987


64129


Dear Mr. Murphy:


Parameter Tested:

samples collected

Tank testedSample 4ft 6 tank

Sample 5ft 7 tank

BTU/pound 13,903 14, 877ArsenicBoronChromium, totalCopperZinc

All Sample results wereAll Sample results were

2.6 mg/kg65.2 mg/kg

224.0 mg/kg

less than 1 mg/kg.less than 10 mg/kg

1.1 mg/kg9.1 mg/kg

54.2 mg/kgShould you have any questions, please feel free to call us at anytime. Thank you for the opportunity to assist you in yourtesting needs. If you should need additional analytical services,we would appreciate the opportunity to provide assistance.

Yours very truly,•BLUE VALLEY LABORATORIES

1<Waymon E. Hofheins

,,P,i/i’ frta/,,,,w/ ,,, ,,, ‘ty

MISS RI P ARTMENT OF NATURAL RESOURCES)on of Environmental Quality

daste Management Program.0. Box 176 Jefferson City, Missouri 65102

314-751-3176


_________

Please print or type (Form designed for use on elite (12-pitch) typewriter.) Form Approved. 0MB No. 2050-0039, Expires 9-30-88

BNBRAT0R

3. eratoia Name and Mailing AddressI ppere Co. T’TC.

P.O. Rox a057

4.oqneP )!O• 641 ri

5. Traneporter I Company Name 6. us EPA tD Numbert)irt Trutkin ETh. I’rtc. IL fl iinrttt fi icg nt7. Transporter 2 Company Name 8. US EPA ID Number

I i I I -t9. DesIgnated Facility Name end Site Address io. us EPA ID Number

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-‘taqoi,e itc 1’or Tr 1in Proes Only

Printed/Typed Name Signature ‘1 Month Day Year.T’qr ‘• rr,r

A 1T 17. Transporter 1 Acknowledgement of Receipt of Materials f DateA Printed/Typed Name Signature--

Month Day Year1rI)10.1 !. kL- .‘ ?‘f- ‘. . ei - I I i1) 10 18. Transporter 2 Ackno’4edgement of Receipt of Materials

DateT Printed/Typed Name SignatureMonth Day YearE

R11111119. Discrepancy Indication Space

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20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted In Item 19.

Date, Printed/Typed Name Signature Month Day Year- . . ..• . - I . 1 .1

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III

I

INSTRUCTIONS FOR THE COMPEflON OFi1S FORM ARE ON A!PARA1 HET.IHIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.

SMIROENCY RESPONSSU.S. cOAST GUARD

1400-424-8502CHEM TREC

1-e00-424-9300DEpt. OF NATURAL RESOURCES

314634-2436

UNIFORM HAZAR DOUS Ii. Generators US EPA ID No. Manifest 12. Page ...........L I Information in the shaded areasWASTE MANIFEST I i I I I I I I I I I i1I init 0

‘W1)flfl 71 517 DocumentNo. ._L isrequiredbyStatelaw.

Koppers Co. . Tc.‘te Plant “oa’ (off

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16. GENERATOR’S CERTIFICATiON: I hereby daclarethat the contents of this conaignmentere fullyandaccuratelydescribed above by propershipping nameand areclassifled. packed, marked, andlabeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations end appilcebie state regulations.If lam a large quantity operator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I have determined lobe economically praclicabie and that Ihave selected the practicable method of treatment, storage, or dlaposai currently available to mewhich minimizes the present and future threat to human heaith and the environment; OR, If lam asmall quantity generator. I have made a good faith effort to minimize my waste generation and select the best waste management method available to me that I can afford.

-J04U.

A Form 8700-22 (Rev. 9-86) MDNR-HWG 10 PREVIOUS EDrtIONS ARE OBSOLETE

BLUE QALLEY LABoRAQIEsP.O. Hox 12(35Mission, Kansas 66222Telephone (913) 362-1313

November 12, 1987


64129


Dear Mr. Murphy:


Parameter Tested:

samples collected

Tank testedSample 4fl 6 tank

Sample 5# 7 tank

BTU/pound 13,903 14, 877ArsenicBoronChromium, totalCopperZinc

All Sample results wereAll Sample results were

2.6 mg/kg65.2 mg/kg

224.0 mg/kg

less than 1 mg/kgless than 10 mg/kg

1.1 mg/kg9.1 mg/kg

54.2 mg/kgShould you have any questions, please feel free to call us at anytime. Thank you for the opportunity to assist you in yourtesting needs. If you should need additional analytical services,we would appreciate the opportunity to provide assistance.


k<Waymon E. Hofheins

p

(1(?frf f’iili,iiw/ p4ta fI,/,,

. Generator’s Name and Mailing Address

I Icoppers Co., Inc., 465 W. 56th Ave., Denver, CO802164. Generator’s Phone 33 > 295—28265. Transporter 1 Company Name 6. US EPA ID NumberJ. C. Thucking, Inc. 1C0D00C6.95•106

7. Transporter 2 Company Name 8. US EPA ID Number

9. Designated Facility Name and Site Address ‘ 10. US EPA ID Number

11. US DOT Description (Including Proper Shipping Name, Hazard Class. and ID Number)

. Hazardous Substance

A. State Manifest Document Number

B. State Generator’s ID

C. State Transporter’s ID

D, Transporter’s Phone

E. State Transporter’s ID

F. Transporter’s Phone

G. State Foclflty’s ID

I

UNIFORM HAZARDOUS 1. Generator’s US EPA ID No.Docume

2. Page 1 jig;freos isWASTE MANIFEST C. 0. fl 007077175. . 880809of 1

.

H. Fodlhy’s Phone,

.‘ p12. Containers 13. 14.

Total UnittIM -

No. Type Quantity ft/l Waste No.°‘ R.Q Solid N.O.S.OPM-E, NA 9188 46 DM 23,OOO p

— (contains creosote) QcP’’ . .. 4J . . —

I:. . .. . . .

.

IC. Handling C

tne inateria aescri Do e ss tieci as

16. GENERATORS CERTIFICATION: I hereby declare that the contents of th,s consignment are fulIyend accurately described above by proper shipping name and ore classified, packed.marked, ond labeled, and ore in all respects in proper condition for transport by highway according to applicable international and notional governmental regulations.If I am a large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicableand that I hove selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment;OR, ill am a small quantity generator, I have mode a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I canafford.t

Printed/Typed Name gnatureMonth Day yearF. L. Brown .3 S Ii ‘2 Ii 9 I R’1’ 17. Transporter 1 Acknowledgement of Receipt of Materials

iaTj Month Day Year

) 18. Transporter 2 Acknowledgement of Receipt of Materials 7 J’7Printed/Typed Name Signature1 Month Day Year

/ 11’119. Discrepancy Indication Space

FA

1 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by ths manifest except as noted in Item 19.

nted/Typed Name

•, USignot

ORIGINAL-RETURN TO GENERATOR

odes for Wastes Listed Above

Additional Descriptions for Materials listed Above When handling, wear protectiveequipnent such as impervious gloves and eye protection.NON-HZABDOUS WAS’fl ( EXCEPT IN COLORADO) - FOR IRACKINGPURPOSES, ONLY.

—

15. Special Handling Instructiops and Additional Information Al ‘-hazardous waste in Colorado, it is.iaws ana reouiations.crenacia L”U.5iSs1PD1, ior aispósai raclilty. will

Mississippi for energy recovery.

.1.

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MIS’”’EPARTMENT OF NATURAL RESOURCES. ,Jivision of Environmehtal QualityINSTRUCTIONS FOR THE COM

EMERGeNCY RESPONSEPLETIONOFTHISFORMAREONA Waste Management Program

IJ.S. COAST GUAnDSEPARATE SHE. P.O. Box 176 Jefferson City, Missouri 65102CHEUTREC

1-800424-8802THIS DOCUMENT MUST BE USED314-751-3176 I 1-800-424-9100

FOR ALL MISSOURI-DESTINED

I DEPT.OFNATURAtRESOUCEtSHIPMENTS. HAZARDOUS WASTE MANIFEST [Please print or type (Form designed br use on elite (12-pitch) typewriter.) Form Approved 0MB No. 2050-0039, Expires 9-30-88UNIFORM HAZARDOUS

WASTE MANIFEST

_________

3 Generators Name and MailIng Address

K’ppafts C 1%.‘‘ %r7 Th5 j/

5. Tranaporler 1 Company Name 6. US EPA ID Number

o’1’ Io4oicE7. Transporter 2 Company Name 8. US EPA ID Number

I t I9. DesIgnated Facility Name and Site Address 10. Us EPA ID Number

,rYS 94-a

___

___

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number)

ENERAT0R

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\ja- F 11p ts Ly16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are tullyand accuratelyde’cribed above by proper shipping name and are cIasified, packed, marked, andlabeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and applicable state regulations.It lam a large quantity operator, I certify that I have a program in place to reduce the volume and toxicily olwastegenerated to the degree I have delermined to beeconomically practicsbleand that Ihave selected the practicable method of treatment, storage, or disposal currently available to mewhich minimizes the present and luturethreat to human health and the environment; OR, ill amasmall quantity generator, I have made a good failh effort to minimize my waste generation and select the best waste management method available to me that I can afford.Printed/Typed Name Slgature

Month Day Year- S ct (‘{\ C L

- / I U 1191‘F 17. Transporter 1 Acknowtedgement of Receipt of Materials (‘ / /‘ DaleA Printed/Typed Name Slgnalu--‘ /7 / Month Day Year

i. KLcw. 1t4) 2j/O 18. Transporter 2 Acknowledgement of ReceIpt of MaterialsDateT PrInted/Typed Name

SignatureMonth Day YearE

-


FAC

-

1 20. FacIlily Owner or Operalor: CertificatIon ol receipt of flazardoua meterlela covered by Ihis manliest except as noted In Item 19.

DatePrinted/Typed NameSignatur

Month Day Year: GiY . 1(CGLELLttlJ12 ii

Ii. Generator’s US EPA ID No. ManIfest 2. Page ..L.,. Information in the shaded areasL Document No.kr Cl LitO I c ‘ 14 .S 1 ‘)IO G Di of .J......... is requiredbyStatelaw.

A. Miout ManifestI

I,

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l9L12. Containers

tq 74

13.Total

Quantity

14.Unit

WtiVot.

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PA Form 8700-22 (Rev. 9-86) MDNR-FIWG 10 PREVIOUS EDITIONS ARE OBSOLETE 0

Please print or type (Form designed tor use on elite (12-pitch) typewriter.) Form Approved. 0MB No. 2050-0039. Expires 9-30-88UNiFORM HAZARDOUS

WASTE MANIFEST3. enerator’s Name and Mailing Address

ppers Co. INC.P.O. Box 80574J,,Qflç(ITY 11o. 64129 816 861—58805. Transporter I Company Name 6. US EPA ID NumberDart Trucking Co. Inc. I

_________________________—

Ifli T-lThTtflt ItRi ciRt9 ic7. Transporter 2 Company Name 8. US EPA ID Number

I i9. Designated Facility Name and Site Address 10. US EPA tD Number

Koppers Co. Inc.Tie Plant Road (off highway 150)

M4.mm Qfl11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12. ContaIn

NO.aNON Hazardous Process Waste Containingused Creosote

lb.

J1AA

13.Total

Quantity

J Additional Descriptions (or Materials Listed Aboveoda. tot Wasx.,.iiisx.a—”—

RQ Haard-o-.u Sub8tancc Liqui-d—(or Solide)- :‘

. I 1 I IbN 0.5. ORME NA 9J&& I I I 1 1 I I4 cont-al aa Cr eo-e-e#e-)-— I I I I-—————-—--..———--.._— —--.--—-—. ..-... ------..-—-—.— - I I -15. Special Ha dung In truqtions nd Additional InformationWhen ctancfling wear protective equipment such as impervious glovesand eye protection aj

NON—Hazardous Waste For Tracking Purposes Only

Month Day YearPrinted/Typed Name SignatureJAMES M. COLE

Qfr, ‘)7Z. CO..Q)Date

T 17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed Name

Month Day YearA

1xr1O.t).4 I. f<CrkL Vc

0 18. Transporter 2 Ackxt)wled9ement of Receipt of MaterialsOatePrinted/Typed Name Signature Month Day YearER I I I I19. DIscrepancy Indication Specs

FAC

L 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manliest except as noted In Item 19.IDatePrinted/Typed Name Signature Month Day Yearm- i, i .

INS’lRUCTiONS FOR THE COMPLETION OF THIS FORM ARE ON ASEPARATE SHEET.THiS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESIINEDSHIPMENTS.

MIS U”-\DEPARTMENT OF NATURAL. RESOURCES)ivision of Environmental Quality

m Waste Management ProgramP.O. Box 176 Jefferson City, Missouri 65102

314-751-3176


CD

1. Generator’s US EPA ID No, Manifest

I M0D007146517 DocumentNo.I I lilt flAt flq

EMERGENCY RESPONSEU.S COAST GUARD

l-O-424-6aO2CHEM TREC

1-600-424-9300DEPT. OF NATURAL RESOURCE

314-634-2436

2 Page ....L. Information in the shaded areasot _...L.. is required by Stw.

GENERAT0R irt1 V1

(1IVgfI,Or

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by propershipping name and are classified, packed, marked, andlabeled, and are in all respects in propar condition for transport by highway according to applicable international and national government regulations and applicable state regulations.111am a large quantity operator. I certify that I have a program in place to reduce thevolume and toxicifyof wastegenersted to thedegree I have determined lobe economically practicable and that Ihave selected the practicable method of treatment. slorage, or disposal currently available tome which minimizes the present and future threat to human health and the environment: OR, if lam asmall quantity generator, I have made a good faith effort to minimize my waste generation and select the beat waste management method available to me that I can afford.

EPA Form 8700-22 (Rev. 9-86) MDNR-HWG 10 PREVIOUS ED1TIONS ARE OBSOLETE F

EMERGENCY RESPONSEU.S. COAST GUARD

1-800-424-9802CHEM TREC

1-900-424 5300DEPI OF NATURAL RESOURCES

314-834-2436


Year

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INSTRUCTIONS FOR THE COMPLETION OF THIS FORM ARE ON ASEPARATE SHEET.iHIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.

Please print or type (Form designed for use on elite (12-pitch) typewriter.)

MISSO R EPARTMENT OF NATURAL RESOURCESision of Environmental Qualityaste Management Program

P.O. Bux 176 Jefferson City, Missouri 65102314-751-3176



3. Generator’s Name end Melting Addresi<cc3s e‘P ?&

c.t I94. Gen reior’aPhone( L) —

I Generator’s US EPA It) No. Manifest 12. Page ....L_ I Information in the shaded areasDocument No Icrj 00’) t 9 i i Icsc of ..L...... is required by State law.

J1

5, Transporter 1 Company Name e. us EPA ID Number

cc C7 Transporter 2 Company Name 8. us EPA ID Number

_____________________

1111111111119 Designated Facility Name and Site Add 10. Us EPA ID Number

ec ;cs)m.

11. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. ContaIners

No. Tvp

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16 GENERATOR’S CERTIFICATION: thereby declare that the contents of this consignment are fully and accuratelydescribed above by propershipping name and areclassified, paclred,1marked, and

labeled, and are In all respects in proper condition for transport by highway according to applicable international and national government regulations and applicable stale regulations.

If lam a large quantity operator, I certify that I haves program in place to reduce the volumeand toxicity of waste generated to the degree I have determined to be economically pract cable and that I

have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment: OR, ill am a

small quantity generator, I have made a good faith etfort to minimize my waste generation and sejt the best waste management method available to me that I can afford.

Printed/Typed Name Month Day Year-sc-c. . C_ LSl9nat/

lurePrinted/Typed Name Month Day Year

i’A /2 (AClC,i

SØ

A iI1iln

T 17. Transporter 1 Acknowledgement of Receipt of Materials ,,4? - Dale

0 18. Transporter 2 Acknowledgemenl of ReceIpt olMaterlals I i I Date- - . -

Printed/Typed Name Signature Month Day

II19. DIscrepancy indication Space

FAC

L 20. Facility Owner or Operator: Certification of receIpt of hazardous materlats covered by this manifest except as noted in Item 19.

I DaleT

Printed/Typed Name Signature Month Day Year

/12 t ,v,f”é +‘)M/öt’ /i-ti iIIt19 ts

EPA Form 8700-22 (Rev. 9-86) MDNR-HWG 10 PREVIOUS EDITIONS ARE OBSOLETE

ENERAr0R

C. State Trens. ID

_________________

PA-AH 1021918. US EPA ID Number D. Transporter’s Phone I fl) 2437I E. State Trana. ID

10. US EPA ID Number PAAH I IF. Transporter’s Phon. I

G. State Facility’. ID Not RequiredW S. U. 0. 0. 7. 0 2 7. 5. 6 H. Facjya Phone I I

________—

12. ContaIners11. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number)

No. Type• W RQ-fien flaatar4ou Process Waste

NO.5. Liquid OR.H.-E HA 91R8 9 Q.._. (cantainaUiedcresot —

4140 O_b.

, I21-u . . . . . . .

—

d

J. Additional Description, for Materials Llated Above (include physical state end hazard code) K. Handling Codes for Wastes Listed AboveHas. Code Physical Slate Has, Code Physical State

a.LII III c.IIIIII ab.III III d.III III b.


WIWfl ANE>T.TN(, t.T1AR PROTVCTTV E17TT’)WNT Stcp AS TKPYRV!flTiS (T,0VlSAN” IYW T’1flTCTTflN


- 20. Facility Owner or Operator: Certification of receipt of hazardous material, covered by this manifest except as noted In Item 19.

I’ Printed/Typed Name fignature / Month Day Year

- /1/i //A) 11 Iii IJ7IPA Form 8700- 22 (Rev. 9.86) roots ,‘rl,Imos ,-I,oolpto

ER S’ 6.81


PENNSYLVANIA DEP TMENT OF ENVIRONMENTAL RESOURCESLi of Waste Management

P. 0. Box 2063Harrisburg, PA 17120

Please print or type. (Fonht designed for use on elite (12 pilch) typewriter.)

1. Generator’s (IS EPA ID No. Ooc,o.P.A.T’.ft . 6 7 23-2.6.51 1 oo.r.


Vnppers Ca., Tne., r.o. !ox 189, noery, P.. 17752

Forni approsed

0MB No. 2050 0039

Ehplres 930 88

2. Page 1 I Information in the shaded areas

of I Is not required by Federat lawi hut I. recinlrsd hv State law.

4. Generator’s i_L.717 i _47—jj5. Transporter 1 Company Namert Trttckfnji Co.., The.

7. Transporter 2 Company Name

9. Designated Facility Name and Site Address

apers Co. The., P.O. Trx 160(renada, MS 3R96fl


PAB 5438370

6. US EPA ID Number

I 0flDI9é5825

B. Stete Gin. ID

PAD 0567232é5

13.Total

Quantity

14.Unit

Vt!VolWaste No.

16. GENERA’i’OR ‘S CERTiFICATION: I IaioI,y ,I01’I,IlI. li-il II ‘ 1,1,1 1.111’; lii IriS ills Iliolil 1110 hIlly furl al’r’lrrahIuIy ills, nod 01,1,00 IV h1l1’IUl SIlIhlhllilfI 11111111. :11111 1110

‘lascnhlol io loll n,anF el fill IaI,plo,I .11111 lIe II, .111 11191009 iii jirnlhii’rrninin hiluliur Ill, 11011011111 I II)’ IlilhIwOy fcc 1111111111 1(1 al’hnIun:aIIIO ,irlerllflIr,,n,al i,,il nlflwI,,Il Qnl.-l’lllIIIehlI u1qi,lliulul’;

II I .1111 .1 lainti’ 11,11111 I) pIne, .11,11 I ii lily (liii I In_I’ II a 111011.) 1111 111111 0 II ll’,Ilo,e 1111 mu 111111? 11111 InoIr nly il .50511’ (I0hl0l.lllrlI In lInt 1101)100 I I1,iv,1 II iliiiir,ni,i’l Ill Ill’ 1111111111111 OIly.11,11. itoh loll I,,,,’’ ci I rI tIll 11.0 II nil,. p,u’lI,,,ul il 110,11110111 olIrraIll’. III uliSpoSrul l;l,ulohllIv av,rnIalnli In 11111 wInot, luuIIllfllliuui liii’ lnlI’su’IlI ;i,unl I 1,1111,’ O.,i’,il Ill Ii Illilall l,,ralII,

II,.’ ‘US fllII0hIl.ll I OR. ii liii , ,iun,iIl 110.011111.1)11111,111i1 II, 111.111 .ini’ a 11,1,11 haitI, 1111)11 II, III 1I011IlTh lIn .5,15111 l’nlolahllnuIl .111,1 101011 liii 1,11’ll .5515111,111.1 ulOlIlOllOhIl no.111,11 liii is111111.1111,1111,11 I Ill

Signature__:

,

Printed/Typed Name

7. 0, LOALWQitt17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed Name

18._Transporter2Acknow ementofRecegof Mate,iaisPrinted/Typed Name

Month De -o

Copy 6 - 1St) Facility: Retain This Copy

wI.-.

ZO0i-

IiUI

ox

UI

I

UI.ø4)wZ

o

I-ia.

‘iRUCTIONS FOR THE COMOLETION OF THIS FORM ARE ON ASEPARATE SHEET.THIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.

Please print or type (Form designed for use on elite (12-pitch) typewriter.)

MISSOU DEPARTMENT OF NATURAL RESOURCES

4 vision of Environmental QualityWaste Management Program

P.O. box 176 Jefferson City, Missouri 65102314751-3176



3 Generator’s Name and MalEng Address

KopIe’l?s-Ti, Yfl. //

4. Generator’s Phone

I Generator’s US EPA ID No ManIfestDocument No.

roDo1’7 i ‘1L .51 i7Iooooi


EMERGENCY RESPONSEU S. COAST GUARD

1-800-424-8802CHEM TREC

1-800-424 9300DEPT. OF NATURAL RESOURCES

3)4.834-2436


2 Page ...L... Information in the shaded areas

ot _L.. Is requIred by State law.

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c\c, %% Cc Iç.7 Transporter 2 Company Name 8. US EPA tD Number

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10. US EPA ID Number

6. US EPA ID Number

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9 Designated Facility Name end Site Address

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Ii. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12. ContaIners

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GENERAT0R

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I I I15 Special Handling Instructions and dditional Information ..—. - - ‘ —‘ —.

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-z>s bJisTh — F cka’t i’ucSis cYNLy16. GENERATOR’S CERTIFICATION: thereby declare that the contents of this consignment arefutly and accurately describedbove by proper shipping name and are classitied, packed, marked, and

labeled, and are in alt respects In proper condition for transport by highway according to applicable International and national government regulations and applicable state regulations

It tam a large quantity operator, I certify that I haves program in place to reduce the volumeand toxicityof waste generated to the degree I have determined lobe economically practicable and that I

have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR, if I am a

small quantity generator, I have made a good faith effort to minimize my waste generation and select the best waste management method available tome that I can afford.

MonthPrinted/Typed Name I Signatured)7 cii. Ii iS’

19, DIscrepancy IndIcatIon Space

Month Day YearPrinted/Typed Name SIgnature

IT 17. Transporter I Acknowledgement of Receipt of Materials . - Date

Printed/Typed Name SIgnature Month Day Year

E111111

18. Transporter 2 Acknowledgement of Receipt of Materials Date

FAC

L 20. Facility Owner or Operator CertifIcatIon of receipt of hazardous materIals covered by thIs manIfest except as noted In Item 19.

,Printed/Typed Name Signature Month Day Year

G+y EI4ccLELLAATh idLJEPA Form 8700-22 (Rev. 9-86)Mt7NR-HWG 10 PREVIOUS EDITIONS ARE OBSOLETE (

MISSpL!j”—qEPARTMENT OF NATURAL RESOURCES

( )vis;”i of Environmental Quality‘—----“z. Wasle Managr ‘ogramP.O. Box 176 Jefferso. ., Missrn,ri 65102

314-751- i

HAZAR)OUS WA FE r NIFFST

Month Day Year

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TRUCTIONS FOR THE COMlION OF THIS FORM ARE ON A

f’ARATE SHEET.THIS DOCUMENT MUST BE USEDFOR ALL MISSOURI-DESTINEDSHIPMENTS.

Please print or type (Form designed for use on elite (12-pitch) typewriter)


FMIRQENCY IESPONS8US. COAST GUAnO

1-8fl0 424-8802CHEM TREC

1-8004249300DEP1. OF NATURAl. RWSOURCES

314 834-2438

Ii Gener PAONo. Manifest f2. Page _L_ Information In the shaded areas

fr Document No.On s r 9 , c I 71n of _J is required byState law.


—— —.

Z._•3 Generetors Name and Maillir Address A. Ml88O4JrI Menibit flcument -Koppers Co. 9Inc.

.. IP.O. Box 8057

4 o 64129 (6i --1xv

5 Transporter 1 Company Name 6 tJS ETA ID Number-iLS Q

-.7 Transporter 2 Company Name A US EPA ID N.rrnber-

tt-

arNarnf 9nd Site AddresS 10 U EPA It) Number o4leIe F .

Tie Plant Road (off flighway 51)Tie Piant,Ms. 38960 - 601-226—4584 H “.

4:L___- 5i‘ 1-2264584ii US DOT De3crlptlon (Including Proper Shipping N nw, iIezerd des., And (V Numtirr) W Contelnrs 13 14. —

Total (trill I.‘ Quantity WI/Vol. -

Ft. 7rJon—Hazardous Process Wastenvkt.

( Contains uaed creosote ) 4,11 “)- 4

b Ii .- I j1 V — LL tjJ 0 /JhJ L

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I- 114

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J Aldntbnal OvrriiptlonE for M91er1915 I. sled Ahoe

or .Sf)1..id_). 1 0,S...,ORM’-E_.----NA9-18-—- .(cntains..reosote )... . —

K HrnllIng Cod4e for WC8tea Liatéd Above

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1..[ .J.-----—.-.----—--.-, l._.LL..L.1LI_.LIP Spn’cial Handling lq”tyuctionx and AdJiti’,nal tntormatiorr.When [iaitd!iug, wear proleclive eqii:’ r tmenl: such as ii’tperviotis gloves, and eye pro tectJ on

lON—IIAZARPOIIS WASTE—FOR ‘l.flACKTflf PIJPPOS ES ONLYlternrtte TSI) facility: Kopper Co. Inc. 6740 Stndium Pr. Kansas City, Mo. 641296 GENErATORS CEll) IFICATION: I herebydeclarn hat lhecr,ntenlot I iscrinsignmenlarelullyandacciiraleiydeavrlhedabovehypropershipping narneand areclassitied, packed, marked, andlabeled and arc in alt respects In proper condition tar transport by highway according to applicable international and national gnvernmnent regulations and nippii.nhle state tequiritiona.

ft sin a largequanlily operator, I cerlity lhat I haves program in ptacotn redun:n Ihvolunieand tosicityol wnsIeqniiratd to ttnedegree I have determined to hercorrornically practicnt,lc and that Ihavenclected the practicehie mr’t1nnd nttraInipril, storage, or dinpnantlcrirrenittysvailab’oto me which minimiz— ttrc present and fiture tl,rnal to human health arid lhenvironmet.t, On, if lam asmall quantity generator, I havn cads a good tnilh eltort to minimize my waste generation and setect the best waste managennierit nnetIl-’l available to me thrill can attord.Pniritnillvped ‘‘errie 1 gnatu7T Merritt thy ‘YearJAMES M CDLE J IQ ?io ;‘r

J/ z0 Ia. Transporter 2 Acknowledgement of Receipt of Mntriats /‘ DeteT Signature

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19. DIscrepancy tndlcaf inn Space

21). Facility Owner or Operator. drltfleetion rrcetpt ef hnzardous mnlnrIl co”’ ly this met :.ipt as riotOd In Item 19.

—_________________________________________ - —-____________________________Date

Signature

h’,9A /A’ f) La ii..

Month Day Year

.Ic-cEPA Form 8700-22 (Rev. 9-86) MOFJF1 HWG 10 PREVIDUS EDITIONS ARE OBSOLETE /

MISURI DEPARTMENT OF NATURAL RESOURCESINSTRUCTIONS FOR THE COM- (‘ ThpIvlsion of Environmental QualitypLETIONOFTHISFORMAREONA Waste Management ProgramSEPARATE SHEET. P.O. Box 176 Jefferson City, Missouri 65102THIS DOCUMENT MUST SE USED

314-751-3176FOR ALL MISSOURI-DESTINEDSHIPMENTS.

HAZARDOUS WASTE MANIFESTPlease print or type (Form designed for use on elite (12-pitch) typewriter.)

4, Generator’s Phone I )

EMERGENCY RESPONSEU S. COAST GUARD

1-500.424-5802CIIEM TEtEC

1-800-424.9300DEPT. OF NATURAL RESOURCE

3j4534.2435

Form Approved. 0MB No. 2050-0039, Espires 9-30-88

3 Generator’s Name and Mailing AddressI A. MISSOUrI Manliest Oockim,rn Number u ,,v

Koppers Co. Inc. Io-.P.O. Box 8057 Kansas City, Mo. 64129

I-’

UNIFORM HAZARDOUS 1. Generalor’s US EPA ID No. ManlIest 2. Page ..L._. Information In the shaded areasWASTE MANIFEST M 0 D 0 0 7 1 4 6 5 1 7 It 4 ot i..._. is required by State law.

‘:‘:- !:_5. Transporter 1 Company Name 6. US EPA ID Number C. MO. T

7. Transporter2Company Name 8.US EPA ID Number

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,

9 DesIgnated Facility Name and Site Address 10 US EPA ID Number

—

Highway 51)IMS1D10101710127 01

—

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and IV Number) 12. ContaIners 13. 14. . Z# Total Uflil . .1, Quantity WI/vol. . -. ILa. a1i

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Non—Hazardous Process Waste f41J/ T 95’ 1?’6 (Contains used creosote) 4V P

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n.e.J Additional Descriptions for Materials Listed Above L.. 1310 a S) . tdt(ng Codes for Wastes Listed Abovea. Q zpc1c\o.’sb. iP ( c9is CeLcs,Tt) I I

15. SpecIal Handling inslruclions and Additional Information

When handling, wear protective equiptment such as impervious gloves, and eyeprotection. Alternate TSD facility: Koppers Co. Inc. 6740 Stadium Dr. Kansas City, Mo.16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of thIs consignment are fully and accurately described above by proper shipping name and are classifIed, packed, marked, andlabeled, and are in all respects in proper condillon for transport by highway according to applicable International and national government regulations and applicable state regulations.ill am a large quantity operator, I certily that I have a program In place to reduce the volume and toxicity of waste generated Ic the degree I have determined to be economically practicable and thaI Ihave selected the practicable method of lreatmenl, storage, ordisposal currently available tome which minimizes the present and future threat to human health and the environmenl: OR, if lam asmall quantlly generator. I have made a good faith effort to minimize my waste generation and select the beat waste management method available to me thaI I can allord.

Month Day Year

Printed/Typed Name Slg ture

4t\.S VL ‘m G&1.. o i25 I?-

DateRT 17. Transporter I Acknowledgement of Receipt of Materials

Day YearA Prioed/Typed Name Signature

I15I. fThO k9. ‘yq

Date0 1 . Transporter 2 AcI1owIedgement of ReceIpt of MaterIals

. Month Day YearPrinted/Typed Name SignatureE IR I 11111119. Discrepancy Indication Space

FAC

L 20. FacilIty Owner or Operator: Certification of receipt of hazardous malerlala covered by this manifest except as noted in Item 19.I

I DatePrinted/Typed Name Signature Month Day YearGARY E.. MCOLEUANP . iogizyis

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1.-u.EPA Form 8700-22 (Rev. 9-86) MONR-HWG 10 PREVIOUS EDITIONS ARE OBSOLETE I

ounui net

-‘ 2600 Bull Street. Columbia, SC 29201and L:nvironmental Control Phon (803)734-5200Emergency & HoNdays (803)734-5424

UNIFORM HAZARDOUS 1. Genorator’s U.S. EPA ID No. Dmflll%1O 2. Page 1 InformatIon In the shaded &eaa Is notWASTE MANIFEST 5 o 3 3 3 O 2. of requiredbyFederaltaw.butisbyStatetawa Generato?s Name and Mailing Address i’( ( C.c .—‘ i’j A. Sleli Mwide.LOom.r N bItc. .ieX

.‘.• .

:‘. .Ffic .s.c.4. GeneratorsPhone(o3 )(o( —3t.& Transporter 1 Company Name L U.S EPA ID Number ¶<oycS Cc--aviy1 •PiA) 1015 , Ii l2.i1.$. i.7. Transporter 2 Company Name 8. U.S EPA ID Number

II I I I I I I I I I I9. Designated Facility Naineand Site Address 10. US. EPA ID Number

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icc -ç \4i’f.S 3(C) —V’LS’I

11. U.S. DOT Descnption (uwiuding Proper Shipping Name. Hawd Class, and ID Number) 12. Containers ia Total Quanthy 14. Unit 1. 4No. Type WVVd .

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e GENERATOR’S CERrIFICATION: thereby declare that the contents of this consignment are fully end accurately descdbed above by proper shipping nam, and are classified.packed. mariced. and labeled, and are in all respects In proper Condition for aneport by highway according to applicable International and national government reguladoria andth• laws of the Stat, of South Carolina.U I am a large quanUty generator. I certify that I have a program in place to reduce the volume and toxicIty of wast, generated to the degree I have determIned to be economicallypracticable and that I have eelected tie practicabl, method of treatment, storage, or disposal currently available to me which minimizes the present .nd futur, threat to humanhealth and the envlronmentrOR, Ill ama small quanUtyganerator, I have made a good faith effort to minImize my waste generation and select tie best waste management methodthat Is vallubIe to me and that I can afford.

Printed/Typed Name.. Isy Month Day Year

Io1c).,Z,3 [I7. Transporter 1 Acknowledgement of Receipt of MaterialsName

Month Day YearC HI F I5b0 )8. Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed Name j Signature Month Day Year

1111119. Discrepancy IndIcation Space

a11111jIbacj11_1jfIbs.

bi t i i I’ dl i i i i

3. Facility Owner or Operaior Certification of receipt of hazardous materials covered by this manifest except as noted In hem 19.Printed/Typed Namo I Signature Month Day YearGA’f . hfCCL ELL MID I £. (YZJ

LEASE PRINT or TYPE (Form desiqnod for use on elite (12-pitchi tvoewritert FormAp roved. 0MB No. 2050.0039 Expires 9-30.88

pproved 0MB No.2000-0404. Expires 7-31-86Please print or type. (Form designed for use on elite

UNIFORM HAZARDOUS l.Gen. rU EPAIDN0.

WASTE MANIFEST KYD006383392Manifest Document NL /‘—‘. Page 1 Information in the shaded areas

1002 8 88 of is not required by Federal law.3. Generator’s Name and Mailing Address A. State Manifest Document NumberKoppers Co

002 8 88P0 Box 8, Meriweather Rd. Guthr, Ky I223)4 B. StateGenerator’slD4. Generator’sPhone( co2 ) I83 21 KY]YJ063833925. Transporter 1 Company Name 6. US EPA ID Number C. State Transporfë?s IEbfop986582IDart Trucking Co 04—AJC., I flflflfl9PfStJ25 D. Transporter’sPhon 800 238 837. Transporter 2 Company Name 8. US EPA D Number E. State Transporter’s IDI F. Transporter’s Phone9. Designated Facility Name and Site Address 10. US EPA ID Number G. State Facility’s IDKoppers Co Inc

MSD0070275L3Box 160 Tie Plant !oadTie Plant, Ma. 38960 I MSD0070275L.3

11. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)

on Hazardous process waste contaused creosote

I Descriptions for Materials Listed AboveR Q Hazardous Substance, Liquid(of saud) NOS ORNENA 9188

( aontains Creosote)

15. Special Handling Instructions and Additional InformationWhen handling, wear protective equipment such as impervious gloves & eyeprotection. NON-HAZARDOUS WASTE-FOR TRACKING PURPOSES ONLY

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurate(’described above by propershipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway accordingto applicable international and national government regulations.Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization certificationunder Section 3002(b) of RCRA, I also certify that I have a program in place to reduce the volume and toxicity of waste generated to the degreeI have determined to be economically practicable and I have selected the method of treatment, storage, or disposal currently available to mewhich minimizes the present and future threat to human health and the environmt.Printed/Typed Name I Signature Month Day YearRobert Morgan

108 115 I 8817. Transporter 1 Acknowledgement of Receipt of Materials-.

TRANSP0

Y Printed/Typed Name Signature Month Day Year


FAC

20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.Printed/T ped NameMonth Da YearGk1 . MccLLLftAJp

Signatu

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Month Day YearPrinted/TyPed Name Signatu, f_,e.1’ I 08 115 I 88

Bob Coffey18. Transporter 2 Acknowledgement of Receipt of Materials If /

F

GENE

AT0R

Style F15R-6 Labetmaster. Div. of American Labelmark Co. Inc 60646 ci EPA Form 8700-22 (Rev. 4-85) Previous edition is obsolete.

ORIGINAl PcTIIDM rr

Koppers Company, Inc.465 West 56th AvenueDenver, CO 80216 B. State Generator’, ID

5. Transporter I Company Name 6. US EPA ID Numbe; C. State Transporter’s IDDart Trucking Company, Inc.. 011D009865825 . . . . 0. Transporl.r’sPhon. 800—238—83577. Transporter 2 Company Name 8. US EPA ID Number E. State Transporter’s ID

I F. Transporter’s Phone9. Designated Facility Name and Sit. Address 10. VS EPA ID Number 0. State Facility’s IDKoppers Company, Inc.Box 160, Tie Plant Road

H. Facility’s Phone.

Tie Plant, MS 38960 (601)226—454. . MSD007027543. .

1 1. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. ContainersTotal Unit

t-lMNo. Type wjyi Waste Na.

.

.

Nonhazardous process waste containing used Creos te 85 DM—‘‘

..L..6.

- Ak’ -8/2-g8. . . . .. —._____

Jof2 /G5/i0

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-

€ 6b - — —

JAdditionalk.Hondling Codes for Wastes Listed AboveR. Q. Hazardous Substance, Liquid & Solid, N.O.S.,ORM—’E, NA 9188 53 Liquid(contains creosote) 32 Solid

Printed/Typed Name Signatur(&V E. MCLELLPriJU c. i

3. Generator’s Name and oilIg Address

1. Generator’s US EPA ID No.

C0D007077175

4. Generator’s Phone 303 ) 295—2826

ManifestnNo

2.

I

Page 1 Information ip ... r.5.4qd oreos iiof not required by Federai low.

A. Stale Manifest Document Number

15. 5pecia Handling Instructions and Additional Information

When handling, wear protective equipnent such as impervious gloves and eye protection.NON—HAZARDOUS WASTE - FOR TRACKING PURPOSES ONLY.16. GENERATOR’S CERTIFICATION: $ hereby declare il,oi the contentS at this consigrrnre.rI sire toiiy and accurately described above by proper shipping name and are nlassitierl. parherd.rnorl,ed. nod labeled, and we in all respects in proper condition 1w transport by highway according to applicable international and notional governmental regulationsItt am o large quantity generator, I certify Itrot hare a program in place to reduce the volume and torridly 01 waste generated to the degree I have determined to be economically practicabteand that I have selerted the practicable method ot treatment, storage. or disposal currently available tame which min,mizes tire preserrt and future threat to human health and the environment;OR, ill am a smolt quantity generator, I hove made a good faith ellort to minimize roy waste generation ond select the best waste management method that is availoble to me and that Iranallord.

Printed/Typed Name noturnth 3F. L. Brown

4”v.”l, bo I ô IT 17. Transporter 1 Acknowledgement of Receipl of Materials-—

Printed/Typed Naytz7-) ,:yt125A1 r Si9aw/) C. (1Dart Trucking Company, c.- (‘

—_-

- --L bo I I R0 18. Transporter 2 Acknowledgement of Receipt of MaterialsT Printed/Typed Name Signature

Month Day YearE


FAC

i. 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest escepl as noted in Item 19.TV

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-7 Month Day Y.ar


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IJ1L UI AHKANSA

Department of Pollution and Ec&ogy

P. 0. Box 9583 LIttle (‘‘)}aflsas 72219Telephone 501 -562-7444’

(Form designed for use on elite (12-pitch) typewriter.)

G nerstor’s US EPA ID Nb.Ii


3. Generator’s Name and Mailing AddressA’,Oe P (‘ca _Ztr’c’ -

f’.c, Bt’X /9f94. Generator’sPhone( 5) )q4/g4cççj’/ jP-Ig

7223,

7. Transporter 2 CompaNe ( 8. US EPA ID Number

I I I I I I I I I I I I10. USEPAtONumber

Designated Facility Name and Site Address

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19. Discrepancy indication Space

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00Form Approved. 0MB No. 2050-0039. ExpIres 9-.30-88


LA# 7iiit’nj4 C06. USEPAIDNumber

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Manifest I 2 Page 1 Information In the shaded areas is notof ) requIred by Federal law

A. Stat* Manitest Document Number

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r,. I11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number)

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No. Type

13.’Tot

Quantity

14.Unit

WilVot Waste No.a.A/’A//5aZ’/Pci$ toe &CiS7 ‘---.

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if no alternate TSDF, return to generator15. Special Handling instr lions and Additional Information

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pfti-)fofr i LJ4$7é- k iiacf,v4 tio.sc w4iGENERATOR’S CERTIFICATION: I hereby declare that the contents of this naignment are fully and accurly described above by proper shipping name and are classified,packed, marked, and labeled, and are in alt respects in proper condition for transport by highway according to applicable international and national government regulations and Arkansas slate regulations.III am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practIcable method of treatment, storage, ot diapoeai currently available tome which minimizes the present and future threat to human health andthe environment; 011, if I am a small quantily generator, I have made a good faIth effort to minimize my Waste generation and aelect the best waste management method that Taavailable to me and that I can afford.

PrintediTyped NameMonth Day Veer

1Signature

h” MAn*— ‘-

. .—-— t,.-.-.-t-— -‘

IT. Transporter I Acknowledgement of Receipt of MaterialsPrlntedtTyped Name

Month Day Veer[Si9nature

18. Transporter 2 Acknowledgement of Reipt of MaterialsPrlntedlTyped Name SIgnature

Month Day Year

11(111

FAC

i 20.FeclIity Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.PtInledlTyped Name I Sign

Month Day YearG/. cLEli AVD I

E;A Form 8700-22 (Rev. 9-86) PrevIous edItIon Is obsolete.1. (i.IdI i Si ‘ 7 S &I

NOTICE: THE ORIGINAL AND NOT LESS THAN TWO (2) COPIES MUST MOVE WITH THE HAZARDOUS WASTE SHIPMENT. ONCE DELIVERED, THE TREATMENT/STORAGE.”DISPOSAI. FACILITY MUST RETURN THIS ORIGINAL COPY TO TI4F CFNPATfl5

______ __________________________ __________________________________

Form Approved 0MB No. 158 S80004fiA—in aaa ore spaced for elite type, Le., 12 ch

_____________________________________________ ___________________________________________

4VlRONMENTAL PROTECTION AGENCYFDRM

I EPA! D NUMBERHAZARDOUS WASTE PERMIT APPLICATIO

Pluese prilt or type in the

eEP1\ Consolidated Permits ProgramRCRA (

FOR OFFICIAL USE ONLY

This Information is required under Section 3005 of RCRA.)

APPLI,..,., ,.,,. DATE RECEIVEDAPPtJFt1 I (,,‘ mn .8 dnvI

L.1 I i1iJII. FIRST OR REVISED APPLICAT1ON

Place an “X” in the appropriate box in A or B below (mark one box only) to indicate whether this is the first application you are submitting for your facility orrevised application. If this is your first application end you already know your facility’s EPA LD. Number, or if this i5 a revised application, enter your facility’sEPA I.D, Number in Item I above.FIRST APPL.ICATJ ON (place an “X” below and prouida the appropriate date)

1. EXISTING FACILITY (See instructions for definition of “existing” facIlity. z.r’w FACILITY (Complete item below.)71 Complete item below.)7’ FOR NEW FACILITIE

__________________

PROVIDE THE DATEI . I MO. I I FOR EXISTING FACILITIES, PROVIDE THE DATE (yr., mo.. & day) i ..o. I I OY j (yr., mo., & day) OPER

I I I TION BEGAN OR IS81 101 41 I 01 1 I 10 I 1 OPERATION BEGAN OR THE DATE CONSTRUCTION COMMENCED I I 1 j I 1 EXPECTED TO BEGII’i . 7. 761 177 .1 (use the boxes to the left)

. . . I IB. REVISED APPLICATION (place an “X” below and complete Item I aboue)I. FACILITY HAS INTERIM STATUS

C2. FACILITY HAS A RCRA PERMIT72__7!

_____________________________

—

Storage:CONTAINER (barrel, drum, etc.)TAN KWASTE PILE

SURFACE IMPOUNDMENT

Disposal:INJECTION WELLLANDFILL

LAND APPLICATIONOCEAN DISPOSAL

SURFACE IMPOUNDMENT

SOl GALLONS OR LITERSS02 GALLONS OR LITERSSOS CUBIC YARDS OR

CUBIC METERSS04 GALLONS OR LITERS

079 GALLONS OR LITERS080 ACRE-FEET (the uolume thatwould cover one acre to a

depth of one foot) ORHECTARE-METER

D8I ACRES OR HECTARES082 GALLONS PER DAY OR

LITERS PER DAY083 GALLONS OR LITERS

OTHER (Use forphysical, chemical,thermal or biological treatmentprocesses not occurring in tanks,surface impoundments or incinerators. Describe the processes inthe space prouided; Rein 111-C.)

TOl GALLONS PER DAY ORLITERS PER DAY

T02 GALLONS PER DAY ORLITERS PER DAY

T03 TONS PER HOUR ORMETRIC TONS PER HOUR:GALLONS PER HOUR ORLITERS PER HOUR


UNIT OFMEASURE

CODF UNIT OF MFASURF

A.

COMMENTS

A. PROCESS CODE — Enter the code from the list of process codes below that best describes each process to be used at the facility. Ten lines are provided forentering codes, If more lines are needed, enter the code(s) in the space provided, If a process will be used that is not included in the list of codes below,thendescribe the process (including its design capacity) in the space provided on the form (Item Ill-C).B. PROCESS DESIGN CAPACITY For each code entered in column A enter the capacity of the process.1. AMOUNT — Enter the amount.

2. UNIT OF MEASURE — For each amount entered in column B(1), enter the code from the list of unit measure codes below that describes the unit ofmeasure used. Only the units of measure that are listed below should be used.PRO- APPROPRIATE UNITS OF PRO- APPROPRIATE UNITS OFCESS MEASURE FOR PROCESS CESS MEASURE FOR PROCESSPROCESS CODE DESIGN CAPACITY PROCESS CODE DESIGN CAPACITY

Treatment:

TAN K

SURFACE IMPOUNDMENT

INCINERATOR

UNIT OF MEASURE

UNIT OFMEASURE

CODEGALLONS G LITERS PER DAY V ACRE-FEET ALITERS L TONS PER HOUR 0 HECTARE-METER FCUBIC YARDS Y METRIC TONS PER HOUR W ACRES BCUBIC METERS C GALLONS PER HOUR E IIECTARES aGALLONS PER DAY U LITERS PER HOUR HEXAMPLE FOR COMPLETING ITEM III (shown in line numbers X-1 and X-2 below): A facility has two storage tanks, one tank can hold 200 gallons and theother can hold 400 gallons. The facility also has an incinerator that can burn up to 20 gallons per hour.

UNIT OFMEASURE

UNIT OF MEASURE CODE

. DUP

A. PRO’B. PROCESS DESIGN CAPACITY

A. PROB. PROCESS DESIGN CAPACITYhi css FOR hi FOR2. UNIT OFFICIAL 2. UNIT OFFICIAL(from list 1. AMOUNT OFMEA-

UI 1. AM OU NT OFM:A

z code) a o e)code)‘1. .. .L “ 27 ii. 5. —. — 21. ‘4 1 I’

27 — 26 26 —- 22X-1S02 600 G 5x-:To3 20 E 6

i S 0 4 130,650 c 7

2D80 0.73 A8

, 93

4

21 — 12

10II It

27 26

Continued fr9m th front.

LII. PROCESS (continued)‘FOR EACH PROCESS ENTERED HERE

C. SP,(CE FOR j’ooITIoNAL PROCESS CODES ORINCLUDE DESIGN CAPACITY.

Note: 111.C. Line 1

650 cubic yards x 201 gal/yd3 — 130,650 gallons

3.,. EPA HAZARDOUS WASTE NUMBER — Enter the tour—digit number from 40 CFR, Subpart D for each listed hazardous waste you will handle. It youhandle hazardous wastes which are not listed in 40 CFR, Subpart ID, enter the four—digit number(s) from 40 CFR, Subpart C that describes the characteristics and/or the toxic contaminants of those hazardous wastes.

3. ESTIMATED ANNUAL QUANTITY — For each listed waste entered in column A estimate the quantity of that waste that will be handled on an annualbasis. For each characteristic or toxic contaminant entered in column A estimate the total annual quantity of all the non—listed waste(s) that will be handledwhich possess that characteristic or contaminant.

UNIT OF MEASURE — For each quantity entered in column B enter the unit of measure code. Units of measure which must be used and the appropriatecodes are:

ENGLISH UNIT OEMEASURE CODEPOUNDS PTONS T

METRIC UNIT OF MEASURE CO IDEKILOGRAMS KMETRIC TONS M

If facility records use any other unit of measure for quantity, the units of measure must be converted into one of the required units of measure taking intoaccount the appropriate density or specific gravity of the waste.

. PROCESSES1. PROCESS CODES:

For listed hazardous waste: For each listed hazardous waste entered in column A select the code(s) from the list of process codes contained in Item Illto indicate how the waste will be stored, treated, and/or disposed of at the facility.For non—listed hazardous wastes: For each characteristic or toxic contaminant entered in column A, select the code(s) from the list of process codescontained in Item III to indicate all the processes that will be used to store, treat, and/or dispose of all the non—listed hazardous wastes that possessthat characteristic or toxic contaminant.Note: Four spaces are provided for entering process codes. If more are needed: (1) Enter the first three as described above; (21 Enter in theextreme right box of Item IV-D(1); and (3) Enter in the space provided on page 4, the line number and the additional code(s).

2. PROCESS DESCRIPTION: If a code is not listed for a process that will be used, describe the process in the space provided on the form.

JOT!: HAZARDOUS WASTES DESCRIBED BY MORE THAN ONE EPA HAZARDOUS WASTE NUMBER — Hazardous wastes that can be described byriore than one EPA Hazardous Waste Number shall be described on the form as follows:1. Select one of the EPA Hazarfous Waste Numbers and enter it in column A. On the same line complete columns B,C, and 0 by estimating the total annual

quantity of the waste and describing all the processes to be used to treat, store, and/or dispose of the waste.2. In column A of the next line enter the other EPA Hazardous Waste Number that can be used to describe the waste. In column D(2) on that line enter“included with above” and make no other entries on that line.3. Repeat step 2 for each other EPA Hazardous Waste Number that can be used to describe the hazardous waste.

EXAMPLE FOR COMPLETING ITEM IV (shown in line numbers X-1, X-2, X-3, andX-4 below) — A facility will treat and dispose of an estimated 900 poundser year of chrome shavings from leather tanning and finishing operation. In addition, the facility will treat and dispose of three non—listed wastes. Two Wastesre corrosive only and there will be an estimated 200 pounds per year of each waste. The other waste is corrosive arid ignitable and there will be an estimated00 pounds per year of that waste. Treatment will be in an incinerator and disposal will be in a landfill.

A. EPA C.UNIT 0. PROCESSESJ HAZARD. B. ESTIMATED ANNUAL OF MEASURE 1. PROCESS CODES 2. PROCESS DESCRIPTION

Z 6 VASTE NO QUANTITY OF WASTE (enter (enter) (if a code is not entered in D(1))J z (enter code) code)—

— I I I I I I I-1 K05 4 900 F T03D80————— II II II Ii<-2D002 400 P T03D80—————

I II II I I-3D001 100 P T03D80—————

II II II II(4 D 0 0 2 included with above‘A Form 3510-3 (6-80)

C. UNITOPMEA

SURE(entercode) -

A. EPAHAZARD.WASTE NO(enter code)

Continuei from page 2.

N0TE: Photpcopy this page before completing lf/ /ave more than 26 wastes to lisL Form Approved 0MB No. 158S8QOO4&f EPAI. JMnEnicner frdn )age 1) ‘POR oFFIclAI USE 4ej

wLjIs 1° fo f0 f7 fo f2 f7 f5 I

___________________________________________________

IV. DESCRIPTION OF HAZARDOUS WASTES (côntinudI’.

B. ESTIMATED ANNUAL.QUANTITY OF.WAST PROCESS CODES . -

—, . (enterJ

“ D PROCESSES•

• .1 t .

2 PROCESS DESCRIPTION(Ito code I. not entered In D(1))

a u. 27 25 27 25 51—

‘ 27— I

-

1 2500 .

2 001 0 P •D80——

—— I I I I I I I I

-3.. ——

— — I I I I I I I

4—— —

——

— I I I I I I I

5—————

I I I I I I I

6I I I I I I I I

7

Ii I I II I I

8

ii-.9.. . I I I I I I

10I I I I I I I I

11., . I I —T I I I I

12.

- I I I I I I I I

13

IL I I I I II

1.

.- I I I I I I

15..- .

. . II ji II I I

16.

. I I I I Ii I

17

:::: :::II ••l I II II

21 — 22 27 — 25 27 29 27 — 29 27 — .29

EPA Form 3510-3 (6-80).

.PAGE-3T OFj5.-CONTINUE ON REVERSI

Continued from the front.

LV. DESCIÜPTION OF HAZARDOUSE. USE THIS PACE TO LIST ADDITIONAL OCESS CODES FROM ITEM D(I) ON PAG

Note: IV.B. Line 2

Wastes were last placed on May 13, 1987.

EPA 1.0. NO. (enter from pnge 1)r1.Jc

MlSlD1OlO17IO 1271514 131 61V. FACILiTY DRAWING

I.. I

All existing facilities must include in the space provided on page 5 a scale drawing of the facility (see instructions formare detail).

11 PHOTOGRAPHS

All existing facilities must include photographs (aerial or ground—level) that clearly delineate all existing structures; existing storage,treatment and disposal areas; and sites of future storage, treatment or disposal areas (see instructions for more detail).

111 fACILITY GE OG R . PHIC LOCATIONLATITUDE (degrees, minutes, & seconds) LONGITUDE (degrees. rninutcs, & seconds)

fill. FACILITY OWNER-

A. If the facility owner is also the facility operator as listed in Section VIII on Form 1, “General Information”, place an “X” in the box to the left andskip to Section IX below.

8. If the facility owner is not the facility operator as listed in Section VIII on Form 1, complete the following items:

1. NAME OF FACILITY’S LEGAL OWNER 2. PHONE NO. (area code & no.)

jIG

3. STREET OR P.O. BOX 4. CITY OR TOWN

.

‘ certify under penalty of law that I have personally examined and am familiar with the informat/on submitted in this and all attached

locuments, and that based on my inquiry of those individuals immediately responsible for obtaining the in formation, / believe that the

‘ubmitted information is true, accurate, and complete. / am aware that there are significant penalties for submitting false information,

ncluding the possibility of fine and imprisonment.

;. NAME (print or type) B. SIGNATURE C. DATE SIGNED

James Batchelder

C, OPERATOR CERTIFICATION .

certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached

iocuments, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the

ubmitted information is true, accurate, and complete. / am aware that there are significant penalties for submitting false information,


. NAME (print or type) B. SIGNATURE C. DATE SIGNED

6. ZIP CODE

‘A Form 3510-3 (6-80) PAGE 4 OF 5 CONTINUE ON PAGE 5

don injecPfrtm pg 4. ( ( Form Approved 0MB No. 158-S800134V.FACILEFYDRAWJNG( page 4)

I

.. .

j —. •

____

I (I

•1 I•1 /I

I 9/

is

a&

itiriucri from the front.

• DESCRIPTION OF HAZARDOUS WAST’

USE THISSPACE TO LIST ADOLTIONAL.,jCESS CODES FROM ITEM 0(1) ON PAGkJ

Note: .IV.B. ‘Line 2

Wastes were last placed on May 13, 1987.

, EPA L:NO. (enter front pn.e 1)

?1 C

jMSID 1° [o {7 0 [2715 l413FACILITY D RAWI G

_____________________________ __

existing facilities must include in the space provided on page 5 a scale drawing of the facility (sce instructions for more detail).

I PHOTOG R

________ ____

\ll existing facilities must include photographs (aerial or ground—level) that clearly delineate all existing structures; existing storage,

reatment and disposal areas: and sites of future storage, treatment or disposal areas (see instructions formore detail).

II ACIL1TY GEOGR .PFIIC L

____________ _____ _______________

LATITUDE (,kgrccs. ntfniilcs, & seconds) LONGITUDE (degrees. minutcs. & sccond.)

LLI1JL

94l7IJ 11911iII. FACILITY OWNER

_____________________ ________________________________

aaflnAa.. &‘.

A. If the facility owner is also the facility operator as listed in Section VIII on Form 1, “General lnformation’, place an “X” in the box to the left and

skip to Section IX below.

8. If the facility owner is not the facility operator as listed in Section VIII on Form 1, complete the following items:

I. NAME OF FACILITY’S LEGAL OWNER 2. PHONE NO. (arc code & no.)

t .

Li IJ-L I 1. I3. STREET OR P.O. OX 4. CITY OR TOWN 5.ST. 6. ZIP CODE

I ,. .

.

1 I • I 1 1‘( OWN ER CE RTI FIC ATI ON

‘ certify under penalty of law that / have personally examined and am familiar with the information submitted in this and all attached

3’ocuments, and that based on my inquiry of those individuals immediately responsible for obtaining the in formation, I believe that the

;ulimitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information,


. NAME (print or type) 1 . SICNAuRE 1 c. OA’rE SIGNED

James Bat chelder I - -

I -‘c-<. OPERATOR CERTIFICATION

• certify under penalty of law that / have personally examined and am familiar with the information submitted in this and all attached

focuments, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the

vbmirted information is true, accurate, and complete. / am aware that there are significant penalties for submitting false information,


‘..NAME (print ortype) B.SIGNATURE C.DATESIGNEO

‘A Form 3510-3 (6.80) PAGE 4 OF 5CONTINUE ONPAGEI

I i’i;i

Conlrol and Ecology

-1 P. 0. Box 9583 LIttle “‘ensas 72219

• Tétephoné SO14e2-7444-1

Plö print or type. (Form deSigned for use on elite (12-pitch) typewriter.)

no U

Form Approved. 0MB No. 2050-0039. ExpIres 9-30-88

3. Generatorri Nrne and Mailing Addresa

I bK1S41?O

4 Generators Phone( 50 I ) 94’55/ iVt’ñL£i717gxik’ 41

A. State Mantteet Document Number

ARa IR721B. Stale GeneraIori ID

.‘,• ‘: -:•

UNIFORM HAZARDOUS I I. Gener&ora US EPA ID No. Msnitet 2. POge I information in the shaded areas Is not

WASTE MANIFEST lb lnfl ot j required by Federal mw

5. TransPorter 1 Uompsny Name 6. US EPA ID Number C. StatS iranaponera IUD - 0

J Zv’c, 1oô9gc67. Tj,amler 2 Company Name ,l B US EPA ID Number F. State Traneport.r. lb

I i i i I I i i i i i

9. Designated Facility Name and Site Address tO. US EPA ID Number I ‘S

5%15-AS .

11QA7/Yj’ SiDCOi7ii74’’/i3 I &. .(j’24/ 12. Conta ners 13. 14.

II. US DOT Description (including Proper Shipping Name. Hazard Class, and ID Number) Total Unit p

.. No. Type Quantity WtlVol West. No.

Q a. Li-— UL —

..

2.arcAus iciø4 2A2 31r £!.

usep ciso7 ‘‘j2’ ..±... I 1 i —

°.

( .. ..(1

‘ fri -, -,

.t )j1 -

..‘fI..,’...I._..,. I I ...L.Ir.I.I I

d.* ‘zfó:e’ Z3€s’

- ..4 ;,.

I I .._L..,,.. I I I I —.

J A omit scrip a for MeteriatS SlId Above ‘ I K. NIBbling Codes for Wastes U!ted Above

4• ( r1YXL /j 4/FtC*464i( 4$fl7

g2zpsUQz -‘- -

If no alternate TSDF, retiirn to generator -

IS pecla tiandilnq nstriicilon r Additionsi tnlnrrnx?on . ,-

‘A (i) 114’)dli ‘?9j £ f-’fl/ I ..i2/(’(’h tiC ‘Ui,oI1ii’i4 .1 5 )171/3Ptl)irti.S

V /)i /-e c’ /7 “. 4J’-’rnI t..wJ ,i1v o, e’S’rnds, iF L//A1g,i’- //4ñO7)U3 i9.57 - /‘R 7?áthnq /ses 2n/q

TO.GENERATORS CERTIFICATION: I hereby deciare that the contents of this consignment are fully ai1d accurately described above by properhipping name and are ciassilied,

packed, marked, and iabeiect, and are In all respects in proper condition for transport by highway according to applicabie international and natlonat government reguiallona and Arkan

sas state regulations.111am a large q’iantiiy generator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I have determined to be econornicaily prac

ticable and that I have selected the practicable method of treatment, storage, or dtboaSt currently available to me which minimizes the present and future threat to human health and

the environment; Oil. ill am a small quantity generator, I have made a good faith effort to minimize my waste generation and select the best waste management method ihat is

available to me and thai I can ailord.

-7

Month (lay YearPrintedlType Npme Signature

17. Transporler

n2ari’i . ‘.1 .. A’&pi 41t2cknowiedgement ol Receipt ot Materials

Month flay YearPrintedl7tj ‘J-’me I si9nature/44, .

p0 18. Transporter 2 Acknowie4meni of Receipt of Materials

PrtntedlTyped Name Stgnature Month Day Veer

F 111111

10. Dlecrepancy Indication Space

PA . .

C

I.20. F.ciltiy Owner or Operator: Certiticatien of receipt of hazardous materials covered by this manifest except as noted In Item 19.

‘ PrlntadiTyped NemeMonth Day Year

• GMY E. /v) CGL L LL I, )Qi7)iOi8bEPA Form 8700.22 (Rev, gee) Previous edItion is obsolete.

NOTICEt THE ORIGINAL AND NOT LESS THAN TWO (2) COPIES MUST MOVE WITH THE HAZARDOUS WASTE SHIPMENT. ONCE DELIVERED. THE TREAT.

L MENT/STORAGEJDISPOSAL FACILITY MUST RETURN THIS ORIGINAL COPY TO THE GENERATOR.

J I. G nerator’s US EPA W NO. •, ManifeSt 2. P$ I inlOrm&ion n the hadod areas is not

oti::i leQtkirdbyIedaraIIaw

eftrQ f, ‘

i

A1c’..t I Company Name 6.

errccz

.—-.——..“-—

i:

-a.

hntedrryped NameMonth Day Year

. Al l1a1’rA/jrmura

,

— -. -. --

1, tranaporter I Acknowledgement of Receipt of MaterIals .

ViintódlTyped Name .iOflatute Month Day Year

01h tin1 iaiIIiiIi

1. transporter 2 Acknowledgement of Receipt g6Iatertals I-,——-j-_

tVL .— --

PrlfltedlTyped Name !Øfleture Month Day Year

V’VJV.. Ii I I IL

• STATE OF AUANSAS V.

Department dt OftutIo orI and Eáblbgy. 0. sa Little ) Aansas 1*êitelephone SOi S2.1444

sr type. (Form ‘e on elite (12-pitch) typewriter.)

•------‘s Phone (L/ /

•iJ)

cJ ••

FOtjOOO39EXPfres3O-88

..,,ter 2 Company Nthe

U

1.- bsignaled Facility Name and Site Address

c,j.. j;vc. •

f//,.,() 7fTA”it”-.

8.

i i.i__i• i i i i i i10.

a-

US EPA ID Number

US DOT Description (including Proper Shipping Name, Hazard Class and fDNilMB

L’1tUI OLi

- f44r4-) Cl 20 P*)(S L4.R2 :c7 i —‘W1 .A

No. Type

Is.Total

Quantity

14.Unit

WllVoi ,W,• No

14

O1’

LtettI TSDP,tii

_________

____

______________

_g

InstmctlonB and Informal n -V

c’s’ i(7t’ fr,,, (-

( t / I 7f4 stlf

AZAAPi,UI1,WS71êVOENERATORSCERTIFlCA•flON: I tieraby declare that the cont5nte of are fully and ecourateiy desoLed ebov5 by proper shipping name and are classified,

ØICked, marked, and iabeièd, and are In eb reSpecI In proper condition for traflepoli by highWay according to applicable intemationat mid national government regulations and Arkan

b State regulations.WI am a large quantity generator, I certify that I have a program in place to redUce ttW volume and toxicity of waste generated to the degm I have determined to be economically prec

Itcable and that I have selected the practicable method of treatment, storage, of dlpOeai Currently avallSble to me which minimIae the ptlaent and future threat to human health and

the Cnvironmenl; OR, if I am a amCii quantity generator, I have made a good faIth ClIorl to minimize my waste generation and seleCt the beat waste management method that Is

Iveitabie to me and that I can affOrd.

: DIscrepancy indication Space- V

,__

Vf . P#eility Owner or Operator Certtticatlon of receipt of hazardouS materials covered by this manifest except as noted In item 19.

‘ ‘intadITyped Name SiGnatureV Month Day Veer

‘Ai’i ., 11LEL11NL) J 5’ jr(j

!P*...V

?oo.22 (Rev. #48) Ptevioui adlUon Is obeolete. •, V

ITREATMENT/STORAGE/DISPOSAL FACILITY COPY

roIm pprh.aed 0MB No. 2050—0039 (ExpIre; 9-30-88)

UNIFORM HAZARDOUS US EPA ID No. Manliest

Pie. rint or type. (Fosm desI2n.d lot use on slit. c/_Y)ritar).

WASTE MANIFST

8022 A (1187)

700—22988) Previous editions are obsolete.

ISlQt( GLL

- ol

Department ot Health Servic..Toxic Substances Control Division

Sacramento, California

Information in the shaded areasis not required by Federal law.

3. Generator Name end lung Address

td Number

4. Generator’s Phone (916) Ss—‘S :‘

5. Transp net I Company Name8. US EPA ID Number hfl4 ‘7O4c+TrchqCb

— OttPt

7. Transporter 2 Company Na9. 8. US EPA ID Number

)-h -.I’ij-I I I I I I I I I I9. esignated Fecili Name and Site Addreae tO. US EPA ID Number . - .

‘

4D. 3Rn 7ZilSQt . •/4j4.1

12 Cont flare 13 Total 14.It. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) Quantity Unit Wait. No.No. Type WIIV0

a. ot iA5c&4d.d 1dO!,-‘, —

OpmcL J,’igcj)Jt44i2OvJIo pb.

- .—

133 - II I —

d. iJ-

.

tPAlOther. Addil nal 0. OrfØtiOI’ei .‘;

‘iifldfln OodI ot * .ia. Listed Above...acaipmr4

:-

iW-

15 Special iIandlg instruction. and Addiilpat)fcon

A H’.cu.ajL j.4,ri Ix 4k,vg.e j O1l.i4i.cI C7 O

2U çtkLi) * 1+ is cz. cArdopj c.uvç4e LtC n *ffcIeiS)Dt IV1 t( t(s.,%.. 7(-1OyJ. ka4c d -ø:4kiL’4osJ&,g&. ñiiAi. 110+ 4,á rI. c nm

a1t1ukand AaIfrZi marked, and labeled, and are in all respects in proper condition for transport by highway according to appiicabte

international and national government regulations.ill am a large quantity generator, I certify that I have a program in place to reduce Ihe volume and toxicity of waste generated to the degree I have

determined to be economically practicable and that I have selected the practicable method of trealment, storage, or disposal currently available to

me which minimizes the present and future threat to human health and the environment; OR, if I am a small quantity generator. I have made a good

faith effort to minimize my waste generation and select the beat waste management method that is available to me and that I can affordPth1edITped Name

I 1?Month Day Year

—

— —-—.—-I—1.——1—-- -

I?. Transporter I Acknowledgement of Receipt ot MaterialsB

ç Printed IT pd Nam

Month Day VeerB ,/

z/ iLir/ yj18. Transporter 2 Acknowledgeme Receipt of Matenicia

Month Day Year

Printed/Typed Name

I SInalure

I I

E£—

tO. Diecrepancy IndicatIon SpaceF

I

intl. i”I 20. Facility Owner or Operator Certification of receipt of hazardous materiata covered by this manifest axcepd/Typed Name

Day Veer

V4M’’ I

/ gWhite: ISOF SENDS THIS COPY TO DOHS WITHIN 30 DAYS

To: P.O. Box 3000, Sacramento, CA 95812

INSTRUCTIONS ON THE BACK

STATE OF ARKANSASDepartment of Pollutlo ‘ and EcologyP. 0. Box 9583 Utile L4,-4cansas 72219Telephone 501.562.7444(Form designed for use on elite (12’pltch) typewriter.)

5. Transporter 1 Company Name 8. US EPA ID Number

V’ 21 ThKi civ- Ti c, 1Mzoo,q1g41557. Transporter 2 Company Name 8. US EPA ID Number

I I I I I I I I I- 10. USEPAIDNumber9. Designated Faculty Name and Site Address

KopA3 Ci”. - 1vc8 X lirO 12 f 1P-31!rA 37tO

a..

b.5, Lx7 ci 2k!

u,.w Cf.. .1 I

C.

.11

rtptlOn.tbr Materials LiSted Above . .

“ , /!prus 6%4ta foul ‘A”S- -_r j_9Jif no alternate TSDF, return to generator

L

J

Lii’•7111e.

. I I I I

I I.. I I

b —

15. Special Handling instructions and Additional Information -

___________________________________________________

) ,I I

— r “ / I /

p .i457 I,/pcd9s 0v4

PrlntedlTyped Name Signature Month Day Year— I —K 1v M(ri/n,’ kn /A2n &‘v

T 17. Transporter I Acknowledgement of Receipt of Materials

PrlntedlTyped Name Signature Month Day Year

. i ii 7 2i / l’ I0 18. Transporter 2 Acknowledgement of Receipt

PrlntediTyped Name SIgnature Month Day Year

III III19. Discrepancy Indication Space

FAiiI.. 20. FacilIty Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted In Item 19.‘ PrtntediTyped Name Signature Month Day Year

(‘/ L /ji Lj L.t.. t.f?o’iw I ;‘/i’ jf1( i’i7ii 1c

EPA Form 6700-22 (Rev. 946) Previous edition Is obsolete.



3. Generators Name and Mailing Address .

.. .

3

4. Generator’s Phone ( ‘‘ /

1. Generator’s US EPA ID No. Manltesi 2. Page 1Ii II of /

Form Approved. 0MB No. 2050-0039. Expires 9-30-88

•/

A. State

Information in the shaded areas is notrequired by Federal law.

‘ Oocumenl N ,r

-

11. US DOT Description (including Proper Shipping Name, Hazard Class, and ID Number)

GENE

AI0R

i,tiicoOii•112, Containers

No. Type

d.

I IIC. Hdn0 Godes

I -.

IS.

i.

for Wastie Ustad i

GENERATOR’S CERTIFICATION: I hereby declare that the Contents of this consignment are fully and accurately desoilbed above by proper shipping name end are cieaalfied,packed, marked,and labeled, and are in all respects In proper condit ion for trsneport by highway according to applicable International and national government regulations and Arkanass State regulations.If lam a large quantity generator, I certify that I have a program in place to reduce the volume and toxIcity of waste generated to the degree I have determined lobe economically practIcable and that I have selected the practicable method of treatment, storage, or disposal currently avaiiabie tome which minimizes the present and future threat to human health andthe environment; OR, It I am a small quantity generator, I have made a good failh effort to minimize my waste generation and select the beet waste management method that isavailable to me and that I can afford.

TREATMENT/STORAGE/DISPOSAL FACILITY COPY

AMERICAN INTERPLEXCORPORATION

LABORATORIES3400 Asher Avenuelittle Rock, Arkansas 72204(501) 664-5060

Koppers Company, Inc. (C-62b)Post Office Box 15490North Little Rock, AR 72117

ATTh: Hr. Ken Martin

April 19, 1988

Control No. 15184

Description of Sample: One (1) sludge sample received on 3/29/88P.O. No. 29907

Results:

Parameter

Heat Content

Chromium

Copper

Zinc

Boron

Arsenic

Unit

BTU/lb

ppm

ppm

ppm

ppm

ppm

Method: ASTM D240, EPA 3050, 6010

I Chemistry — Metallurgy —- MicrobiologyMember: leading scientific societies

Creosote Process Sludgefrom Oil & Water Separator

M1ER!CAN IN ERPtEX CORPORATION

tb Director

3. Generator’s Name and Mailing Address . —.

1’ ,j,f6t

4. Generator’s Phone ( / ).

15( f f’JJ 4j 777.5. Transporter 1 Company Name 6. US EPA ID umber

DAR I . 1’-iMc i;6

UNIFORM HAZARDOUS I. Generators US EPA ID No. Manifest 2. Page 1 Information In the shaded areas is notWASTE MANIFEST 4i! ‘ w :“ I’ll ‘1 of / required by Federal law.

7. Trapaporter 2 Company Name ‘ 8. US EPA ID Number E. State Transporter’. ID

I I I I I I I I I 1 I F. l’ranspbrter’a Phone9. Deal nated Facility Name and Site Address 10. US EPA ID Number -0. Stat. FaCIitty’B

CO. I’C- If 7’p.. fj7/{7i1 H.

31&O IMoi2o7c/I3 3 ol 2f,”c?g12. Conta ners 13. 14.11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Total Unit

., No. Type Quantity WtNol Waste No.Ga.

—

&‘c (d2S7Z CIW?/,v/,v51 MOIII £A b.

USeD Ci?SQ7 i —

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. I I ._L._ liiiJ. AnescrlsforMaterl&sUaiedAboveib /;d A’ 45 K. HazdIingCod,bfoeWlLJ.tqdAbov

‘L’Z).-

i! no alternate TSDF, return to generator15. Specia’ Handling Jnslructions and Addlllonal Information

,. -Pu 1,6 / j /.‘

1/1 27 P’ ( Li I,’/17P* ‘S/Ji1/ 4 < ‘I 1 ‘—

• ( / (V)1 4//1:7/ 5D 1ff •7;tj_1 J?2/ 11flfi’

flt,’- iiU.3 J5iE F2,i? tI618. GENERATORS CERTIFICATION: I hereby declare that the contents of this consIgnment are fully and accurately described ebove by properlpping name end are classified,packed, marked, end labeled, and are in all respects In proper condition for transport by highway according to applicable International end national government regulations and Arkansas state regulations.

If I em a IerQe quantity generator, I certify that I have a program In place to reduce the volume and tosiclty of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health andthe envIronment; OR, if I am a small quantity generator, I have made a good faith effort to minImize my waste generation end select the best waste management method that Isavailable to me and that I can afford... -.

PrintediTyped N me Signature Month Day YearkG() /? i// /? ki A1,i,J/ZZ-, 1c’ i17. Transporte .cknowIedgement of Receipt of MaterialsT

RANSP0

- PrintedlTypad Name K— Signature 7 Month Day YeirE

,, 111111


AR- 1fi72-----..

S. State G.nrator’IID.

0. State Transporter’. ID o5 fjp0. transporters Phone I —XDO -11:? ‘


FAC

L

. 20. FacIlIty Owner or Operator: CertIfication of receipt of hazardous materials covered by this manifest except as noted In Item 19,

Month Day Year‘ PrintediTyped Name I Signature1

I 1(2 y t. ( ( L. i L 4 r) P ( ..—

EPA Form 8700.22 (Rev. 9.86) PrevIous edition I obsolete.

.UM EPrintediTjD M SIgnature J 7 Month --- Day Year1.4frrL1A

.. ;18. Transporter 2 Acknowiement of Receipt of Materials 7

STATE OF ARKANSASDepartment of Pollutio (‘Nnd EcologyP. o. Box 9583 Ut tie i-nsas 72219Telephone 501-562.7444

Please print or type. (Form designed for use on elite (12-pitch) typewriter.)

00Form Approved. 0MB No. 2050-0039. Expires 9-30-88

‘Al

F)

TREATMENT/STORAGE/DISPOSAL FACILITY COPY

AMERICAN INTERPLEXCOflPORAtONLAI3ORATORIES

00

3400 Asher AvenueUlile Rock, Arkansas 72204(501) 664-5060

Koppers Company, Inc. (C-62b)Post Office Box 15490North Little Rock0 AR 72117

ATTN: Mr. Ken Martin

April 19 1988

Control No. 15184

Description of Sample: One (1) sludge sample received on 3/29/88P.O. No. 29907

Results:

Parameter

Heat Content

Chromium

Copper

Zinc

Boron

Arsenic

Unit

BTU/lb

ppm

ppm

ppm

ppm

ppm


] Chemistry — Metallurgy — Microbiology) Member: leading scientific societies

2.3

2.6

Creosote Process Sludgefrom Oil & Hater Separator

9130

2.0

5.8

49

AMERICAN INTERPLEX CORPORATION

STATE OF ARKANSASDepartment of Pollutiol and Ecology

P. 0. Box 9583 Little F,1\Jansas 72219

Telephone 501.562.7444

Please print or type. (Form designed for use on elite (12-pitch) typewriter.)

UNIFORM HAZARDOUS E,PAi7.,

,

2. :i )_=areas is not

b. lransport,,kompany mama B. US EPA IU Numr .eivwtswr.tu ‘ç

P,IK/ )4,,e.’t,’•‘°‘ - sev;i4L

7. Transporter 2 Company Name ( B. US EPA ID Number 9 StAle ? mspoder’e ID .

. I I I I I I I I I I9. Designated Facility Name and Site Address 10. US EPA ID Number . S ,

gcqtpc-: i ,.y,,

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C jfl9 1k?I)I7IOI47312. Conta ners 13. 14. 1II. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Total Unit

, No. Type Quantity WtIVoij, asteNo.a.

A 1’A’/)aZ’,/f,f L ((i”if//i’/A/ tL 7 9 I’?R

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:_;if no alternate TSDF, return to generator ‘

3. Generator’s Name and Mailing Address1

t

- —. - ,. /4 Generators Phone ( ) ( / r fil,/ f, ri ‘ ;zj

A. Slate Manifest DOc&iment Number

AR- I R3*iA.- -

15. SpecIal Handling InstrIctlons and Addltin[fnfcnrnation — ..— -—Ac / ,. .‘,1L i

/

/ i ( —

I -

“r, / ;.i l ,p / F% ;r . i I ‘ <

1vJ- ‘ f. ‘ $ ‘OC16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and aocursly described above by proper shipping name and era classified,packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicable international end national government regulations and Arkansas elate regulations.

111am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined lobe economically practIcable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human heallh andthe environment; OR, If I am a small quantity generator, I have made a good faith effort to mfnimlze my waste generation and select the best waste management method that Isavailable to me and that I can afford.

Signature

T 17. Transporter 1 Acknowledgement of Receipt of MaterialsPrintediTyped Name Signature Month Day Year

L L, i1 ‘i tI.I 1/9 [iI ‘lL0 18. Transporter 2 Acknowledgement 01 Rqelpl of Materials

PrintedlTyped Name Signature Month Day YearE

I I I I [19. Discrepancy Indication Space

FA

L- 20. FacilIty Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

PrlntedlTyped Name Signature Month Day Year

6i1’( I ,kLLi!i ,Ai!) c.. ‘1Jt”it/(’, .EPA Form 8700.22 (Rev. 9.88) PrevIous edition I. obsolete. 1’

Form Approved. 0MB No. 2050-0039. ExpIres 9-30-88

Prlnted!TypedName . -

I )Month Day Year

ICI

TREATMENT/STORAGE/DISPOSAL FACILiTY COPY

AMERICAN INTERPLEXCOF1PORATION

LABORATORIES

00

3400 Asher Avenuelittle Rock, Arkansas 72204(501) 664-5060

Koppers Company, Inc. (C-62b)Post Office Box 15490North Little Rock, AR 72117

ATTN: Mr. Ken Martin

April 19, 1988

Control No. 15184

Description of Sample: One (1) sludge arnple received on 3/29/88P.O. No. 29907

Results:

rameter

ileat Content

Chr omi urn

Copper

Zinc

Boron

Arsenic

Unit

BTU/lb

ppm

ppm

ppm

ppm

ppm


] Chemistry — Metallurgy — Microbiologyi Member: leading scientific societies

Creosote Process Sludgefrom Oil & Water Separator

9130

2.0

5.8

49

2.3

2.6

AMERICAN INTERPLEX CORPORATION

Director

• South Car Ii a Department of Healthand onmental Control

PLEASE PRINT or TYPE (Form designed for use on eltte (12-pitch typewtiter)[1. Generator’s U.S. EPA ID No. 2. Page 1

15c..ooo 3 ,3 13Of

a Generator’s Name and Mailing Address i<) Ci C2 p z-P.o cX 72.$

.S.L. 2-9o.34. Generator’s Phone(c3 )(o9

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9. DesIgnated Facility Name and Site Address 10. U.S EPA ID Number

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11. U.S. DOT Description (including Proper Shipping Name, Hazard Class, and ID Number)

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a. GENERATORS CERTIFICATION: I hereby declare that the contents of this consignment are fully end accurately described above by proper shipping name end are classlited.packed, marked, end labeled. and are in all respects In proper Condition for transport by highway according to applicable International and national government regulations endthe laws of the State of South Carolina.Ill am a li-ge quantity generator. I certify that I have a program in piece to reduce the volume end toxicity of wastegeneratad to the degree I have determined to be economicallypracticable end that I have salected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to humanhealth and the envlronmentrOR, if I am a email quantitygenerator. I have mode a good faith effortto minimize my waSte generation and seiect the beatweale management methodthat Is available to me and that I can afford.

Printed/Typed NameMonth Day YearT csW I iM7jjc4e 01 iL 13

g17. Transporter 1 Acknowledgement of Receipt of Materials

IT ped NameMonth Day Year

- ( HI o r ISi9R7e2) Q_---> I i3t’18. Transporter 2 Acknowledgement of Receipt of Materials

PrintediTyped Name Signature Month Day YearR


Fa

i i l1 c[ i i iAc

bi d[ i i tL

20. Facility Owner or Operator; Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.Prinied/Typed Name

Month Day YearektY cL..jI12 IS1fnatt itj€e

UNIFORM HAZARDOUSWASTEMANFEST

Bureau of Solid a Hazardous Waste MgI.2600 Bull Street, Columbia, SC 29201Phone (803) 734-5200Emergency a HolIdays: (803)734-5424

Form Approved. 0MB No. 2050-0039 Esolres 9-30-83Information In the shaded areas Is notrequired by Federal law, but Is by State law.

12. ContainersNo. Type

ia Total Quantity 14. UnItWINd

I

V

00 D

SPECTRIX FIONRt)EVILLE

I3LE 1: SUMMARY OF ANALYTICAL DATA PRODUCED ON 12/02/87 AT 16:37 PACE I

MO] STURE711041371104147110415ROSS HEAT7110413‘1104141 10415

X Solids @103 CSolids @103 C

X Solids @103 COF COMI3USTIONI3TU/lbI3TU/lbI3TU/lb

CYL 5 CLEANOUTCREO I3LOWDWN TKPCP SEPARATOR

CYL 5 CLEANOUTCREO I3LOLJDWN TKPCP SEPARATOR

AMPLE $ RSLT. LNESOURCE

80.378.967.9

392072015600

e above results are on an as received basis.

oo

SPECTRJ X MONROEVILLE

ABLE 2: SUMMARY OF METALS DATA PRODUCED ON 12/02/07 AT 16:40 PAGE

AMPLE (t RSLT. LNE SOURCE

SENIC7110413 Arsenic, ug/Kg : 26300 CYL S CLEANOUT7110414 ArsenIc. ug/Rg 43200 CREO BLOWDWN TV7110415 ArsenIc, ug/Kg : 239000 PCP SEPARATORJRON7110413 Boron, ugfIg : <4930 CYL 5 CLEANOUT7110414 Boron. ug/Lg : <4250 CREO BLOWDWN Tc7110415 Boron, ug/Kg : <2430 PCP SEPARATORIROMIUM7110413 Chromium, ug/Vg : 25500 CYL S CLEANOUT7110414 Chromium, ug/Kg : 58900 CREO I3LOWDWN T7110415 ChromIum, ug/Kg : 343000 r-’

PCP SEPARATOR)PPER7110413 Copper. ug/g : 49300 CYL 5 CLEANOUTp110414 Coppers ug/Ikq : .77800 CREO I3LOWDWN TRp110415 Copper. ug/Ikg : 68300 PCP SEPARATORNc‘110413 Zinc. ug/g : 33800 CYL 5 CLEANOUT‘110414 Zinc, ug/L’q : 108000 CREO L3LOWDL’JN Tic‘110415 Zinc, ug/Ikg : 20800 PCP SEPARATOR

e above results are on a drij weight basis.

00cEvs1ONE ENVIRONMENTAL RESUURCES INC.

TABLE (iF CONTENTS PRODUCED ON 04/11/OS AT 14:32 PA(:E

SAMPLE ft SOURCE DESCRIPT DATE—COL DATE—REC ORD It08030701 12196 SEDIMENT 03/14/89 03/10/88 M080309580030702 12168 SEDIMENT 03/14/89 03/18/80 M880309589030783 12186 SEDIMENT 03/14/80 03/18/80 M9803095

KEYSTONE ENV 1 RUNMENT AL RESOURCES. INC.= = = = = = = = = = = = = =

TAI3LE 1: SUIIHARY 01: ANALYTICAL DATA PRODUCED ON 04/li/GB AT 14. 16

SAMPLE ft RSLT. LNE SOURCE

MOISTURE880307818803078209030783GROSS HEAT080307010003078289030783ARSENIC

‘‘ 98030781- 88030782

80030783BORON800307818803078288030783CHROII I UM080307818803070288030783COPPER800307819803079288030783ZINC880307818903078298030783

x Sblids @103 CX Solids @103 CX Solids @103 COF COMI3USTIONI3TU/lbI3TU/lbI3TU/lb

Copper, ug/KgCopper. ug/RgCopper, ug/Kg

•0’7q7

• o701•olrI

8350 9+I•e7640 ‘1--O6810 te

121961216012106

121961216012186

121961216812186

121961216812186

121961216812196

121961216812196

The above metal results are on a drj weight basis.

74.770.978.9

Ar sen I c,Ar sen j C.

Ar sen I C,

I3oron,Boron,Boron,

ug/Kgug /Kgug/Kg

ug/V.g

ug/Kg

121961216012186

Chromi urn.C hr om I urn,C hr om i urn,

ug /Kg

ug/Kg

<50000 50<50000 .50

<50000 50

13300 3.3OO

20300 ô.3OO44200 qq.00

245002260043800 q3.’O

4600033400 33./iIO

20900&O.9°

90900601006a1004500gti.50

Zinc,Zinc,Zinc,

u g / Kgug/Kgug/Kg

All other results are on an as received basis.

.‘ Staje CalfOrIa—’44iaflh nd Welfare Agenc.tFonti 4d)M$4o. 2050—003a (Expiree 9.3oseDr

0jJ or tp& POm deaigned for use on elite ewrlter).

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: UNIFORM HAZARDOUS 41L.-tor’B US EPA ID No.. Manliest ,.. •-ge 1 Information in the shaded areas

WSTE MANIFEST I iAi 9 i I 2iô 2 ° f is not required by Federal law.

3.GSflara’e Name end Mpillng Address

_.-jj”v’cc rC,. i.-,,

_________

;., ‘w. ‘c’. ‘ \jt

4. Gin.rator’e Phone(j)

Department of Health SeMdU’Toxic Subst.nóea Control DivlatoW

Sacramento, Califotttt&

eiraflsporter I Company Name 6. US EPA ID Number

.1’t’” Q(• ‘;.c L’ ibiict)ic’ii$ .i2 Company NaIe1 8. US EPA ID Number

I I I liLt LLI I10.

I IiI

8. D fted:Facily Name and Site Address US EPA ID Number •.

(t,

• if

112. ContaIners

II. US DOT Pmcrlption (Including Proper Shipping Name, Hazard Glees, and ID Number)No. Type

0ENFHA1’0A

a. cr... /( Lf . t. •Y

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16. Special Ha and Addiii,nal Information 4H 41, .-L.

tt. , L” ‘• . jç f j iic i 4’i L’14.ii‘ krl’ S. .

‘1 . •‘ i- ,

iLL’ 4 1W. 1 l4iiI Lt’s i.. i1e

hA4c’s RWlt’ON: 1 hebyd Ir iht O,èoñlo1 lIy ar adurt1’.11,b’andfChtaAjffWtked, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable

International and national government regulations.

If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I havedetermined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the eflvlreflment; OR, if I am a smell quantity generator, I have made a goodfaith effort to minimize my waste generation and select the beat waste management method that Is available to me and that I can afford.

PrLfll.edlTyped Nene SIgn,re • •- j f Month Day Year

SR \II II— — -

1?. Transporter 1 Acknowledgement of Aecàlpt of Materlala

o 18 Traitspotter 2 Acknowledgeme of Receipt of Materials •

. ,_

PrlntediTyped Naflie Signature , MoØth Day Year

•.. . .•. rJ • [ I I19, DIscrepancy IndIcation Space -U * •

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AC

I •••• • •. .— ...1.

I 20. FacIlity Owner or Operator libation of receipt of hazardous materials covered by thIs manifest excep a • ad In It 19. .

T a ITyped Name $,ga • lb Day Year

Imi . . Iomf#L’sOHS 8022 A (1/8?) ‘TSOf RETAINS .,... . .. INSTRUCTIONS ON THE BACKEPA 8700—22 -

(Rev. 9-86) PrevIous editions are obsolete.

4.

I CDDCurtis & Tompkins, Ltd., Analytical Laboratories, Since 1878• 290 DM1n Street. Son PronIsco, CA 94103, Phone (415) 861.1863

LEOrATORr NUMEER: 14027-1 bME RSCEIYED. 1/11/98cLXENT: KUPPRS CO. DATE DxEaTED 1/20/89aAMPLE to. On, PENIA ELUDGE DATE ANALYZED: 1/22/88DIiTE REPORTED: 2/1/98

/ PAG810f2Ketsl in Soils & Wastes by AtomIc Absorption SpectrophotometryDigestion Method: EPA 3050

METAL RESULT DETECTION METHODLIk!T

mg/kg mg/kgArsenic

4.4 0.50 EPA 7061Chromium (total) 14 1.3 EPA 7190Copper25 1.3 EPA 72101mb

100 2.3 EPA 7950

Boron55 1 EPA 6010

BTT.J/ POtJND— — — — — — — — . aa.. — — — — — — — a 9 4 93ASTM D240

QA/QC SUMMARY_. — _ — — — a — — — — a — — — — — — — — — — — —%RPD %SPflZ

%RPD %SPIKE• Arsenic 9.9 97 Copper 18 100Chromium 17 90 zinc 9.3 99Boron 32 93

Sin Pt*nclsco Wilmington Los Angeles

.‘P OD - QD cib cud & Tampkkis.

:QP1RY NUNRZRs 14027-2CLIENTs KUVP$R6 Co.SAMPlE IDa CaLLON lIT. SLUDGE

DkrE RECEIVED aDATE DxanTEDDATE A$A11TflDaDM1 AUORTIDI

PAQI 2 of 2

1/11/981/20/881/22/882/1188

ArsenicChromium (total)CopperZinc

Seron

Wastes by Atomie Absorption SpectrophotometryDigation)(tho4i EPA 3OScJIR*SULT DETECTION 141T110D

LIMITMg/kg mg/kg

4,8 050 EPA 706115 1.3 EPA 719019 1.3 EPA 7210

9 2.5 EPA 7950

44 1 EPA 6010

ETU /POUND— — — — — —— — — — — —. — — — — — — ———a — —6, 267AZTM b240

StJ)*UiRT— _a — a — — — a e — — a — a* — — — — — _e — — — — — _ — — — _ — _ — _ — — — — — — _ —

%RPD %SPIKE %RPD %SPIKB9.9 97 copper 18 10017 90 Zinc 8.3 9932 93

ArsenicChromium8ozon

I

Metals in Soils &

METAL

#—l, •,. •

tHeta ot CalIfornia—Health and Welfare AgencyDepartment of Health Services’,,

Form Approved 0MB No. 2050—0039 (ExpIres 93OBh ,—‘.,—,

Toxic Substances Control Olylsiall’Pt.. rint or type. (Form de.Ign.d for use on slit. ( V

‘ew4ter) ( Sacramento. CaliforniaUNIFORM HAZARDOUS ‘ ‘or’ US EPA ID No. Menifeat I information In the shaded areas1

WASTE MANIFEST II iioI% ni ol ( lsnolrequiredbyFe4erallaw. j3.

-

Generator’s Name and Mailing AddreasSOp4”bO f%C-.

cr*. Vr4. Generators Phone ) 3 3—5. Transporter t Company Name 0. US EPA ID Numberb4Vq c7. Transporter 2 Company N%ne 0. US EPA ID Number

I II I I I I I I9.10. US EPA ID Number

I Number—

Designated Facility Name Site Addr.as

j4& IjLerijgu. I.c.Ir.s’i IoD

I I

Ii

J I,Ii. US DOT Description (Including Proper Shipping Name, Hazerd Class, and tO Number)

itci itti21

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I

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15 Special Handling instructions and Additional Information *OI.,C_.. • CCtS c*i

4‘ R -.c’r3ii14 U rci

U,’‘-• Lq I.L.1

i t’$”V are fully arid accurately described above by proper shippingname and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicableinternational and national government regulations.Iii am a large quantity generator, I certity that I have a program In place to reduce the volume and toxicity of waste generated to the degrbe I havedetermined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat 10 human health and the environment; OR, if I am a small quantity generator, t have made a goodfaith aBort to minimize my waste generation and select the beat waste management method that is available to me and that I can afford

------

AANSP0ATF

Printed!Ty ad NameSIg era

Month Day YearI Lt Irsi17. Tranaporler I Acknowledgement of Aecelpi 01 Materials,_ X—Typed Name

Month Day Year

PrlISi9na(/

iOi( I[3’frialaIS. Traneporter 2 Acknowledgement of Rec p

Month Day Year


I I I I I19. DIscrepancy Indication SpaceFAC

II 20. Facility Owner or Operator Certification of receipt oi hazardoua materials covered by this manitest excepl as noted in Item 19.T Printed ITyped Name I Signature

Month Day Yearfl4 9 i.JA/) 4,cI i i,,I WIINSTRUCTIONS ON THE BACK

486022 ACt/al)iA 6700—22iv. 9’06) Previous editions are obaol.te.

White: TSDF SENDS THIS COPY TO DOHS WITH 30To P.O. Boa 3000, Socromento, CA 9582 ‘I

it

1)118 8022 A(l,87)EPA 8700—22(flew. 9-60) Pr.vioue edition. ar. obsolete.

Odfenile-4iealth dnd Wedha Agency\..—’ Department of Health Servicesved 0MB NO. 205O.—OOS9(Explths P Toxic Substances Control Oivtslon.. . one des ned for use on elite ‘ Sacramento, California

UNIFoRM HAZARDOUS lat0ra US EPA lb No. MenlteeiInformation in the shaded areasr . ASTE MANIFEST (1 t C q

‘ 7 613” *0 ° is not required by Federal law.. S Name an 44a111na Address A. ate went. if{t4?. f ‘ ( — i -f” .:.4. ‘ i I ‘ b’( - . ‘ø . , .

,

8 St - .

- ..: ..,- , .. . - .*. ._.,—

.. .. ,.i. - - --- -• ‘- f 4. Geeratore Phone ( i.’) ‘ I.

-: -

&tran ortçJ Company Name , 6. US EPA ID Number 0. State . . S

Vs-4 , 4 , i- C5 1-’i r ‘t. Trans .

7. Tfaneporter 2 Company N ,e 8. US EPA iD Number 8. State I I : ‘)(-

‘

F,Ttmnap • - . ,.

d. Oqigneted FacUlty Psme en Slt&Addreas 10. US EPA lb Number - -

- . .

5 -

JItr ‘ C 7Ci 112. Containers 13. Total 14 :0 11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Quantity Unit *aqle . ‘No. Type Wt!Vo . ,

a fV •j•j_SI

: !b

R • - -

,---.- . -

..-.5

.,

‘5...‘5 5 ‘5

55- :,--t- ‘

d.•

..4C“‘

.

‘5

tAJ4II I III’

o 4i’-; .5.

. 4.5..,, r - -r) I< .5- . -. -. V

Is-,, - . S -5;--ip. 15. SeacIel l-tendling lnatruction and A itlon P’I 1’V . “i’ ‘ . -. C< hr’.t 4s

ø’ LQz V ‘\. , 4t‘5. I . ‘. f 4 . .i ,. . , .

L.5,,1’.- C ‘ ‘ 4,1 ‘ k ‘ •— -, * %-‘I ‘

‘• ._%i. i, t, I. , , — -, . , ,‘4 1 . (s . . “C —

ci GENERATORS CERTIFICATION: I h&eby declare that iha ontenta of this consi nment are fully and accurately described above by proper shippingname and are classified, packed, marked, and labeled, and ate In all resecta In proper conditIon for transport by highway according to applicable,J international and national government regulations.If I sni a large quantity generator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I havedetermined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to0 me which minimizes the present and future threat to human health and the environment; OR, if I am a small quantity generator, I have made a good

> faith Short to minimize my Waste generation and select the beat waste management method that is available to me and that I can cHord.Pri,lte!Typd Name i - 8lgnure .

- .—.*. Month Day Yea‘4’. ‘‘s. i(,

RTraneorter I Acknowledgement of Receipt of Materials .

A PrIn Name SIgnal ‘ ....— Month Day Year12,-’ r . -- -.- I0 o 5. Tranapotter 2 Acknowledgement of Rec pt of Materials5/

Printed/Typed Name Signature Month Day YearE

19. Discropancy Indication SpaceF

C

LI 20. Facility Owner or Operator Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.I PrlntCds’Typ.d Ne e Signature Month Day YearV

2., / 7

WHITE; TSDF RETAINS •INSTRUCTIONS ON THE BACK

-

290 DMiIon Street. Son Francisco, CA 94103, Phone (445) 861.1863

Dk’.E RECEIVEDi 1/11/88DATE DIGEETEDs 1/20/88DATE ANALYZEDs 1/22/88DATE REPORTIDi 2/1/88

PAGE lot 2

Boron55

RESULT DETECTION METHODLXMXT

mg/kg mg/kg

ETTJ/POuND— — — — a — a — — — — — —— a — — a — — a a. — — — — — , 4 8 3ASTh D240

EPA 6010

— — a_a—a a — — a — as. — — — fl— — — —oaa aa — a_a__a_aaa — a — no— — a_a — —%RPD %SPIKE %RPD %SPIKEArsenic 9.9 97 Copper 18 100Chromium 17 90 Zinc 8.3 99Soron 32 93

00a

Curtis & Tompkins, Ltd., Analytical Laboratories, SInce 1878

00

LBORATORY NUMEER 14027-1CLIENTs KTJPPERS CO.SAMPLE Ifli OIL PENTA SLUDGE

11(etale in Soils & Wastes by Atomic Absorption SpectrophotometryDigestion Methods EPA 3050

METAL

ArsenicChromium (total)CopperSino

4.41425

100

0,501.31.32.5

1

EPA 7061EPA 7190EPA 7210EPA 7950

QA/Q(I SUMMARY

Ssn PincIeco Wilmington Los Anqele

OQ cb curtis a tompkins. Ltd.

LAflORATORY NUMBERi 1402 7-2CLIENTI KUPPERS Co.SAMPLE ID2 CELLON WT. SLUDGE

ArmeniaChromium (total)CopperZinc

DATE RECEIVEDsDATE DIQESTEDsDAT* ANALTZEDsDATZ RZPORTEDiPGE 2 of 2

Wastes by Atomic Absorption SpectrophotometryDigeetionethods EPA 3050•1

RESULT DETECTION METHODLIMIT

mg/kg mg/kg

4.8 0.50 EPA 706115 1.3 EPA 719018 .3 EPA 7210

9 2.5 EPA 7950

44 1 EPA 6010

BTU/POUND — — — — — — — asS — — — — — — — — a a —— — — — — 6, 267ASTI4 D240

Q(D

Metals in Soils &

METAL

1/11/881/20/882/22/882/1/88

oron

QA/QC SU)(ARYSan— — — — — e — n — — — naann— a_a— — — — — —%RPD %SPIKExeenic 9.9 97Chromium 17 90Boron 32 93

%RPD %BPIKECopper 18 100Zinc 8.3 99

LABORATORrrRT

2. Page 1 Information ip the ha4çd areas isof not required by Federal law.

k kot. Mdñlfasf boCumen, Number

L ,Stdi. Genrtitoe’s ID

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name end are classified, pocked.marked, end labeled, and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations

If lam a large quantity generator, I certify that I hove a program in place to reduce the volume and toxicity of waste generated to the degreel have determined to be eonomlcalIy practicableand that I hove sebcted the practicable method of treatment, storage. or disposal currently available tome which minimizes the present and future threat to human health and the environment;OR, if lam a small quantity generator. I hove made a good faith Cffort to minimIz waste generation and select the bett waste management method that is available tome and that Iconafford. %_...

Printed/Typed Name Month Day Year

Marvin D. Miller . I ni i n. IPrinted/Typed Name I Signat e Month Day Year

.17. Transporter 1 Acknowledgement of Receipt of Materialt

I 06 I 03 I 88James Thurston I18. Transporter 2 Acknowledgement of Receipt of Moterials

Printed/Typed Name Si Menlh Day Yeargnoture


20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

Printed/Typed Name

L . lit 9

Ii Generator’s US EPA ID No I ManifestI Document No.I C0DQ07077175 I ‘880601

4. Generator’s Phone ( 303 ) 295—2823

Koppers Company, Inc.465 West 56th AvenueDenver, CO 80216

5. Transporter 1 Company Name — 6. US EPA ID Number C. fbi*p 410

Dart Trucking Company, Inc. I •011D009865825 . . . ppO—23843577. Transporter 2 Company Name 8. US EPA ID Number E4 $tofansportat’f?D

I P. ipotit,. Phötté

. .9 Designated Facility Name and Site Address 10 US EPA ID Number 0 cfdflIIIO

Koppers Company, Inc.Box 160, Tie Plant Road Wft

.

Tie Plant, MS 38960 I MSD007027543 .-

4

11. US DOT Description (Including Proper Shipping Name. Hazard Class. and ID Number) I A ( 12. Containers 13. 14: i., i,i Total UnitIM No. Type Quantity fI WdsteNo.

a. /

— Nonhazardous process waste containing usJ&eosoti . •75• DM .4()J-’ Pb.

:

d. . . . . . .

.

JAdditlonol Descrlptloin for Motei4ok Ilited Aloi’e ‘$ KiHvs$lfl Cbdeê 1Weiited Above

R. Q. Hazardous Substance,Solid,NO1S6ORM-E,NA 9188(contains creosote)

15. Special Handling Instructions and Additional Information —.________

When handling, wear protective equipaent such as impervious gloves and eye protectionNON-HAZARDOUS WASTE - FOR TRACKING PURPOSES ONLY.


GENERAT0A

3. Generator’s Name and Mailing Address‘:;.i. rd ‘ ?::tfly,

-

4. Generator’s Phone : n6. US EPA ID Number

l?t t LXtl:.A) r’, I8. US EPA ID Number

io. us EPA ID Number


B. State Generator’s ID

I9. Designated Facility Name and Site Address

U4’ I tO, i.ic Plant ‘V’ H. cWity’sPh6f’’* .‘ . .

ijt t1nt., 33t’;’

______

.

11.I__. .F;t75&

us DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. Containers

No. Type ‘t,’yI Waste Na.

ctIrc.t: nc’’a ‘.it.i t’t fl)’j CiSCti. .7g.

I Descriptions for Materials Listed Above K. handling Codas fJ’Wgstes Listed Abovek ç. ‘U !ut t3r)c’:i’J.O.. OR—’,tu’

iLuii3 ecnt’)


13.Total

Quantity

:t’Ii lt l’ I 9’ , ‘t :.z’i’:f “ c.’J I ‘uc ‘ r4rv1 ‘c ç I rs,i’4 .s,,rn ç,.fld

lt’’7s’ r... y’r p’.-’r C- Y

P

,‘

‘; .

‘TA

S

IP01•EA

FA

IiTV

16. GENERATOR’S CERTIFICATION: I hereby declare that the contentsóf this consignment ore fully and accurately described above by proper shipping name and are classified, packed,marked, and labeled, and ore in all respects in proper condition for transport by highway according to applicable international and national governmental regulotons.Illam a large quantity generator, I certify that I have a program in place to reduce the volume and tosicityaf waste generated to the degree I have determined to be economically practicableand that I have sebcted the practicable method at treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment:OR, it lam a small quantity generator, I have mode a good faith effort to minimize my waste generation and select the best waste management method that is available tome and that Iconafford.

Printed/Typed Name J Signoture Month Day Year

aLvIn 1. ‘ijic.,r 1 I Gl ]i17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed Name Signature._.‘ Month Day Year

Jacs•:-‘ . . ‘“.• —..-• I I (13 I :‘j

18. Transporter 2 Acknowledgement of Receipt of MaterialsPrinted/Typed Name Signature Month Day Year

. I’Ll19. Discrepancy Indication Space

20. Facility Owner or Operotor: Certificotion of receipt of hazardous materials covered by this manifest except as noted in Item 19.

I Signature

‘H( (LLLL iw I )Wc(dt,J

u_WASTE MANIFEST

00

I

1. Generator’s US EPA ID No. Manifest


2. Page 1of f


Information p the shaded areas itnot required by Federal law.

C. State Transporter’s ID

D. Transporter’s Phone BOO—238’8357E. State Transporter’; ID

F. Tonsporter’s Phone

C. State Facility’s ID

Printed/Typed Name

‘i

.1

Month 0oy Year

I’.IcIr.’

T/S/D/F COPY

flTHE IIA)iJSTRIAL LABO TORES CO0

(?nalyhcal and Jonsul1Ing @henoosisP.O. Box 1 6207 1450 East 62nd Avenue

Denver, Colorado 80216 (303) 287-9691

ANALYSIS REPORT

SAMPLE MARKED:LIASTE OIL

ANALYSIS

TU

COPPER

RESULTS

14,000 /tt

55 PPM

CHROMIUM

ARSENIC:

BORON

ZINC

97 PF’Fi

95 PPM

80 PPM

9’3 PFII

NALYTICAL RESULTS ARE INDICATIVE OF THE SUBMITTED SAMPLE ONLY AND MAY NOTLECT RESULTS OF SEEMINGLY IDENTICAL MATERIAL UNLESS SAMPLEr’ ElY OUR REPRESENTATIYI

,‘EMBERS OF’ AMERICAN ASSN OF CEREAL AMERICAN CHEMICAL SOCIETY AMERICAN OIl. CHEMISTSSOCIETY ALSO OF OFFICIAL RACING CHFMISTOEAKERY ENGINEERS OF AMERICA INSTITUTE OF FOGS TECIINOLEOY SIGMA XItTHIS REPORT IS NOT TO BE REPRODUCED. IN WHOLE OR IN PART, FOR ADVERTISING PURPOSES WITHOUT OBTAINING PRIDES WRITTEN AUTIIORI7ATION.

KOPPERS DATE RECEIVED: .1..465 WEST 56TH

. DATE REPORTED: 01/07/00DENVER CO 8O21’ LAB NUMBER:MARY MILLER CUSTOMER P.O.:

PAGE:

ENERAT0R

UNIFORM HAZARDOUS1. Generator’s US EPA ID No. Manifest 2. Page 1 Informaton ip the hadçd areas is

r .Qgcuseni.No. not required by Federol law.WASTF MANIFEST . 2. . . of

3 Generators Name and Mailing Address — A State Manifest Document Number

.:t 5ri1l’

. B. State Generator’s ID4. Generator’s Phone( ‘. ) ,‘ .

5. Tronsporter 1 Company Name 6. US EPA ID Number C. Stoic Transporter’s ID‘• . ‘ ... I . . . .

.

7. Tronsporter 2 Company Name 8. US EPA ID Number E. State Transporter’s ID

I F. Transporter’s Phone

9. Designated Facility Name and Site Address 10. US EPA ID Number G. State Facility’s IDicpc .iit..

i’4..)X i lf’ 1n’t. ‘iH. Facility’s Phone

lc ‘li (‘i”1)..i....

1 1. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. ContainersTotal UnitM No. Type Quantity Wt/y,l Waste No.

0

41 cC— ‘i . - “ - ! ‘t’rn i inj ts ‘ci croE te 35 C 4.,.OOOi f’

b.

— — — —C

-‘.‘-

— —— — h.-.d.

. , . 4. s n..54

J.Additionol Descriptions far Materials tisted Above K. Handling Codes for Wastes Listed AboveP. ç. rJr1ni inc’o, I c.iti, I-4.O..‘)f’’F , :‘TR r quJd4itu cLJ.’.v’) 32 Ec1i’

15. Special Handling Instructions ond Additional Information

1)’fl U:’t, ‘ .r iti ‘vnt IW tr.rrv r4 ry.’)’e’ icrl.:i r’i!!’.5;

‘ Printed/Typed Name — Signature nth Sçr qm F.L.- .._‘‘ ‘— k Iuii Is

T 17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed Nomy_.7

. 7 / Stgnore ,,4_ -( Aosø vi ttsar.rL irttti,ir1 ?s_ c:’-. l .. . [4i1 I tl

0 18. Transporter 2 Acknowledgerient of Receipt of Materials

T Prined/Typed Name Signature Month Day YearER


FAC

. 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.TV

,.

00

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of thi consignment ore fully and accurately described above by proper shipping name ond are classified, pocked.morked, and labeled, and ore in all respects in proper condition for tronsport by highway according to applicable international and notional governmental regulations.Ill am a large quontity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I hove determined lobe economically practicableand that I have selected the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threol to human health and the environment;OR. ill ama small quantity generator, I hove mode a good faith etlort to minimize my waste generation and select the best waste management method that is available tome and that Iconafford.

Printed/Typed Name

(-,i:y [. ftft(L1LI_,i1,1fl)Signatup

/iáLt

I copy IMonth Day Year

Io’Ii •i’i

THE INOtTRIAL LABOIQ ORIIES Co.ow ylIca an 0fl314 ling ein.s13

1450 East 62nd Avenue(303) 287-9691

SAMPLE MARKED:

ANALYSIS

t.IASTE OIL

RESIJLTS

COPPER

CHROMILIM

14.200 /tt

55 PPM

97 PPM

ARSENIC

E1CIRON

2)

95 F’PFI

0.0 PPM

93 PPM

NALYTICAL RESULTS ARE INDICATIVE OF THE SUE1MITTED SAMPLE ONLY AFID MAY NOTLECT RESULTS OF EEMIN’3L.Y IDENTICAL MATERIAL UNLESS SAMPLEt’ E’V OUR REFRESENTATI’)

E”BE RS OF• AUFOICAN *000 OF C100AL CHI0TS A000ICAN CHEMICAL SOCIEtY AMENICAN OIL CHEMISTS SOCIETY ATTN OF OFFICIALNASHNY ENOINE005 OF AMEIIICA IN3TITOTE OF F000 TECHNOIOQY SIGMA El

‘THIS REPORT IS NOT TO SE REPRODUCED, IN WHOLE OR IN PART. FOR ADVERTISING PURPOSES WITHOUT QOTAINING PRIOR WRITTEN AUTHORIZATION.ft aft .,na.eIo IN 0 ,l lOIN lIft OP 101010 000111 WI All I10011001 II wrn,.I.,I .07*00 lOll PHI A 101111 101100 P11110*101 1111011 All l1lll*l,V 100*101* lAPn•*r

P.O. Box 16207Denver, Colorado 80216

ANALYSIS REPORT

KOPPERS DATE RECEIVED: 1-465 WEST 56TH DATE REPORTED: 01/07/DENVER CO 80216 LAB NUMBER:MARY MILLER CUSTOMER P.O.: 029w

PAGE:

Month 0oy YearIi.,ç1

UWASTE MANIFEST

I

d


1. Generator’s US EPA ID No Manifest

:. q. i. iI..’t:;

“pec Cot, fr’,,. “‘•,

4. Generator’s Phone ( li )5. Transporter 1 Company Name

s) C. ‘ i.ricj •

2.t’of


Inforinot ri

ion p Snuited by F’


6. C. State Transporter’s IDUS EPA ID Number

I ‘Lm’16S’,jUG- D. Tronsporser’s Phone

8. State Generator’s ID

8. US EPA ID Number E. State Transporter’s ID

F. Transporter’. Phone —_______

9. Designated Facility Name and Site Address 10 US EPA ID Number G State Facility’s ID

H. Facility’s Phone

1 1. US DOT Description (Including Proper Shipping Name. Hazard Class, and ID Number) 12. Containers 13. 14.Total Unit

No. Type Quantity ‘t/yl Wotte No.

F 5ç,. H1zr ‘r :i.’Y.. . .. .

•‘ .. , fi’ r”r ‘‘ :‘rs r’‘‘t.

.: 1 .. gcb&’’a

Descriptions for Materials Listed Above 4es j-rotct I’ve K. Handling Codes for Wastes Listed Above

(‘Ijl .“2(LL ‘1_’) ‘5 ;‘.i”t’J ‘US :i c’i.j” •)fltJ rrc’t; it1.*“7’; ‘J ti •j• ‘:‘.

— ‘‘

‘1

15. Special Handling Instructions and Additional Information‘ ‘..f’’’-i’ y,, ‘“:‘ ,.

.i. f , -,— ,, r . .i ,;;

. .. ‘, ‘

9 55 ._:.l)

•5 5

f•f .S . ,,‘

..,. S

•ts4k!;3 .o16. GENERATOR’S CERTIFICATION: I hereby declare lh0t the contents of this consignment are fully and occurotely described above by proper shipping name and ore classified, packed.marked, and labeled, and are in all respects in proper condition for tronsport by highway according to applicoble international and national governmental regulations.

If Ian, a large quantity generator, I certify that I hove a program In place to reduce the volume and toxicity of waste generated to the degree I have determined to be pcanomically practicableand that I have selected use practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future threat to human health asd the environment;OR, ft am a small quantity generator, I have made a good faith effort to minimize my waste generation end select the best waste management method that is available tome and that Iconafford.

TBA Printed/Typed Name

BTEB


L rr ..: *.--‘.-- I If7:Tran;pore?cnowledgement of Receipt of Moteriols

Signature / //

:‘

/‘ Mon th Day Year

If 1/ “ .. I ‘311 ‘ I18. Transporter 2 Acknowledgement of Receipt of Materials “


I’ I I19. Discrepancy Indication Space

F

1’V

20. Facility Owner or Operator: Certification of receipt of hazardous moterials covered by this manifest except as noted in Item 19.

Printed/Typed Name Signature

t 41( L LLLAA .1, ,‘%

T/S/D/F COPY

SAMPLE MARKED:

ANALYSIS

BTU

COPPER

CHROMILIM

ARSENIC

E1ORON

THE iQOSTRIAL LABOIOOCORIIES Co.

LIASTE OIL

( i• I JiV i. iViSJ iaiy1.cai omi L’onsu(IIng LIie,ntsls

1450 East 62nd Avenue(303) 287-9691

RESULTS

14.0O /tt

55 PPM

97 PF’M

95 PPM

!3..0 rrri

MEMBERS OF: AMERICAN MON QF CEREAL CHEMISTS AMERICAN CHEMICAl. SOCIETY AMERICAN OIL CHEMISTS SOCIETY ATTN OF OFFICIAL RACING CHEMISTSPERRY ENGINEERS OF AMERICA INSTITUTE OF FOOD TECHNOLOGY SIGMA XI

1THIS REPORT IS NOT TO BE REPRODUCED, IN WHOLE OR IN PART, FOR ADVERTISING PURPOSES WITHOUT OBTAINING PRIOR WRITTEN AUTHORI?ATION.II All IRCARRII mis RAYS lieU INTl Cl SIleNT UNLISI WI ASS NIOIJIITIA. IN WCITIIN. TN 511*1W lAIN ISP A LOuIS 151111. CIMmAILI IAUPII *55 OCUSLAY PISIASnIN

IOPPERS465 WEST 56THPENVERMARY MILLER

CO O216

PAGE:DATE RECEIVED:

DATE REPORTED:LAB NUMBER:

CUSTOMER P.O.:

.1.01/07/01 /26•/If

P.O. Box 16207Denver. Colorado 80216

ANALYSIS REPORT

ZINC 92 PPM

NALYTICAL RESULTS ARE INDICATIVE OF THE SU8MITTED SAMPLE ONLY AND MAY NOTtECT RESULTS OF SEEMINGLY IDENTICAL MATERIAL UNLESS SAMPLED ElY OUR REF’RESEI’ITATIYE

V3? ‘/I/

6 XZ OMB#: 2050-0024 Eplres 12-s E’

-- .- .- — —1

BEFORE COPYING FRM, ATTACH SITE IDENTIFICATION LABELU.S. ENVIRONMENTAL

SITENAME Koppers Company, Inc. \ / 1987HazardousWasteGeneratIoi

H i g h way 5 1 So u t h‘4( and Management Report

Ti P1nt, Mississippi 38960 FORMIDENTIFICATION AND

I I CERTIFICATiONEPAIDNO. M1 Si D OiOi7i 0i2 7 5) 4i31 I

t.

WHO MUST COMPLETE THIS FORM? Form IC must be completed by every site that receIved this package.

INSTRUCTIONS: Please read the detailed instructions beginning on pageS of the 1987 Hazardous Waste Generationand Management Report Instructions booklet before completing this form.

Complete Sections I through IV and Sections Vi through IX Immediately. Complete Section V,certifIcation, after you have finished the full report package.

SEC Site name and physical location which may differ from the mailing address. Complete items A through G.

I. Mark for Items A, B, C, 0, F, and G if same as label; If different, enter corrections. If label is absent, enter information.

A. site/comparry name 0. EPA ID No.

Same as label Sam. as lab.l ]

or___. or— 1111111111

C. Addr.ee number and Street name of pfrysleal location - II not known, .r,t.r induStrial peflr, building name or other pl’ty,Ieal location d.ealp(len

Same as label

or —

0. cay, town, village etc. E. County F. Stale 0. ZIp Code

Same as label Seine as label K] Sam. as label [XI

or....—. tor_I I I or I i I I I I—I I I I I

SEC. Mailing address of site.

II. Mark for A, B, C, and D if same as label; if different, enter corrections.

A. Number and street name of mailIng address

Sam. as label []or P.O. Box 160

9. CIty, town, village .lc. C. Stat. 0. Zip Cod.

Same as label s.m. as label ] Sam. as label [

or.—.. or.——.I I I or I i I i—I I I [ I

SEC. 111.1 Name, title, and telephone number of the person who should be contacted if questions arise regarding this report.

A. Please print: last n.m. FIrst name M.l. 9. Title C. TeIpliona

.Plant [6IOilII2l2I6l_14l51814]

Clayton, Jackie D. Manager - E..on I i

S CEnter the Standard Industrial Classification (SIC) Code that describes the principal products, group of products, produced or distributed, or the

,services rendered at the site’s physical location. Enter more than one SIC Code only If no one industry descriptIon includes the combined activities

‘ of the site. SIC codes are listed beginning on page 1 of the 1987 Hazardous Waste Generation, Shipment and Management Report Codebook.

A. B. C. 0. 5. F.

I2i4i9il] I I I I I I I I I I I I

I certify under penalty of law that I have personally examined and am familiar wIth the Information submitted In this and all attached documents,

SEC and that based on my Inquiry of those Individuals immediately responsible for obtaining the information, I believe that the submitted informationV. is true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, Including the possibility of fine

and Imprisonment.

A. Please print: Last n.m. FIrst name Mi. Title

Clayton, Jackie D. -- Plant Manager

!D.Dale of .lgnafUi.

I___

.

. Pagelofi

EPA Porm 8700- 13A/B (5-80) (Rev. 11.85) RevIsed (12.87)OVER —>

FORM icSC. Does this site’s EPA ID authorize hazardous waste generation?

D NO — SKIP TO SECTION Vii.

YES — Did this site generate any hazardous waste during 1987?

[j] YES — READ DETAiLED INSTRUCTION ON PAGE 4 OF THE 1987 HAZARDOUS WASTE GENERATION AND MANAGEMENT REPORTINSTRUCTiONS BOOKLET FOR ACUTE AND ACCUMULATION LIMITS. MARK (] NEXT TO THE HAZARDOUS WASTEGENERATION QUANTrri CATEGORY THAT APPLIED To THIS SITE DURING 1987.

Category 1: More than 1000 kg (2,200 ib) in one or more months

O Category 2: More than 100kg (220 Ib) but no more than 1000 kg (2,200 ib) in any single monthO Category 3: No more than 100 kg (220 ib) in any single month

Mark lxi If this site changed from Category I to Category 2 or 3 due to waste minimization activity conducted during 1986or 1987.

U NO — CONTINUE BELOW, MARK lxi NEXT TO ALL THAT APPLY.

O Generated, excluded or delisted wastesGenerated hazardous waste prior to 1987 but do not expect to generate in the future - MARK)XJFOR REASON IN ONE BOX BELOW

O Waste was from one-time event(s) (e.g. spills, remedial actions, etc.)Waste minimization activity undertaken during 1986 or 1987

O Out of business

O Generated hazardous waste prior to 1987 and expect to generate in the future

O Never generated before but expect to generate in the future

O Never generated and do not expect to generate in the future - MARK j FOR REASON IN ONE BOX BELOW

O Protective notifier only

fl Misunderstood the requirements

O Notified to secure transportation seMces

O Other EXPLAIN REASON FOR GENERATOR NOTIFICATION IN COMMENTS

SEC. Does this site have RCRA Interim Status or a RCRA permit to treat, store, or dispose hazardous waste?

fl NO — SKIP TO SECTION VIII

fJ YES — Did the site treat, store, or dispose (TIS!D) hazardous waste in RCRA-regulated units during 1987?

YES — SKIP TO SECTION VIII

j NO — CONTINUE BELOW, MARK lxi NEXT TO ALL THAT APPLY

Q T/S/D excluded waste during 1987

Q TIS/D hazardous waste In exempt units during 1987

fl T/S!D hazardous waste prior to 1987 but did not T/S/D waste during 1987. MARK lxi IN ONE BOX BELOW

Q T/S/D will resume In the future

fl Have notified of planned closure

fl Site is In closure or post closure

fl Never T/S/D hazardous waste prior to 1987 but: MARK IX IN ONE BOX BELOW

0 Expect to T/S/D hazardous waste In the future

Q Do not expect to T/S/D hazardous waste in the future - EXPLAIN REASON FOR INTERIM STATUS OR PERMIT IN COMMENTS

Do you wish to withdraw this site’s generator notification or EPA Part A permit application?

Withdraw generator notificatIon 0 Yes () No

Withdraw Part A permit application 0 Yes No

SEC Does this site have an area not requiring a F1CRA Part A or Part B permit that Is used exclusively for the short termIX. accumulation of hazardous waste?

] NO

J YES — DOES THE AREA HAVE:Containers III No J Yes ENTER THE NUMBER OF TANKS AND THEIR TOTAL CAPACITY iN GALLONS.Tanks No Yes — I

. I Number I I I . I I Gallon capacity

Comments:

Page 2 of 14

•1

i i i i t2iSiOiQ

B. *957 quanlily gen.(at.dPeg. 20

i i i i i i Si O

A. EPA ID No. ol lacifhly Ic MiIch.s .tilpped B. Numbei ol C. Tmn.poilInsli,ctlon Page ililpm.nlI mcd.

See comments Pag Pag.23

111111111 I..I I I I I_ L_....j

BEFORE COPYING FORM, ATTACH SITE 1DENTIflCAT1ON LABELOR ENTER:

SITENAME Kopers Company Inc.Highway 51 SouthTie Plant. Mississippi 38961

PAiDNO. 1M151D101017,O,2171514131 FORM

GM

U.S. ENViRONMENTALPROTECTION AGENCY

1987 Hazardous Waste Generationand Management Report

WASTE GENERATION ANDMANAGEMENT

WHO MUST COMPLE1t THIS FORM? Form GM must be oompleted by every site that generated hazardous waste on site or shippedhazardous waste off site durIng 1987.

[] Mark if you are not required to complete Form GM.

INSTRUCTiONS: Please read the detailed Instructions beginning on page 12 of the 1987 Hazardous Watt.Generation and Management Report instructions booklet before completing this form.

Make and complete a photocopy of this form for !! hazardous waste generated on site orshipped off site during 1987.Complete Sections I through IV. Throughout this form enter DK if the Information requested is notknown or Is not available; enter NA It the information requested Is not applicable.

Sec. &wa.i.de.cdpuon Bottom sediment sludge from the treatment of wastewaterI InrudIcnPgel2 from wood preserving processes that use creosote and/orpentachl_orophenol

fl. PA haardoui weal. cod. C. Stale hazazdou,e codePage *2 Page it

11(1010111 I I I I I I I L I I I I I I I I’<IOIOIlt I I LLl I I I I I i i i i i

0. SIC code E. Source code F. Wail. . o r N 85. . reaullaPet3 i2 i4i 9i ii gels 91 Pag.i3 1N1 8i 9i Pag.l3 Lai

—

Sec. A. O.gaika B. W.tac C. Total SolId. 0. Suap.nd.d Solid. E. BIt) F. To.fc Milala rII natruction Page 14 Peg. It Page It Page it P.2. IS Page IS Not. LJC C Mail High Low T.dHigh L.J High U High U High U High I I I I I I I

,. 1A I S1 itlow U low (jJ low iJci Low U low I I I I I I I ii it Tn ri ri 2.1 I U1 U Li UTW J Not. L!J Not• U Hot. J Note L±J U Not.

— 3.1T1C, U LiJ LiCI. pH H. Fiaihpolni I. Cwnld.. J. Halogen. K Radioeclh.Page Ia Pag. 18 Page 12 Page 20 Page 20

. Ji U L.J LiHigh I I l.L.J High I I I I °F Hh U_I h L_J ““ D i N1 I LiLow I I I. _J low I I I I °F Low .J Low U No []

LJ Not. UJ T.at U piq. jj e. ,H1 i_i iYi Li

Sec. A. 1988 quanhlly gnweledIII Inilnadlon Page 20

C. UOM 0. D.nilly E. W. odginPage 21 Page 2* Page 21 Code iAj

LPJ I l.LN1AIOn-ill. 1 I I I

0 I./gaI Qag I/B/D/n code

c. On-all. T/9/O/R cod.Page 2*

l.LSIOI4I 1N1A1 4.1 1N1A1 1N1A1 1N1A1 7.1N,A, •.

a

0. OS-elI. 1/S/D/R cod.Peg. 23

I I I II I I I

E. Total Ou.nlRy ebippedPeg. 23

(It ‘‘liii’

Comments All hazardous waste generated in 1987 was stored on site during 19871No hazard9us waste shipped off—site in l987MSection 11(F) Toxic fletals - AG,cD,PI,sEcl ppblSection 1(E)-KOOl waste I BA — Test not done (Section Ii (F) )

Page 3 of 4

Highway 51 SouthTie Plant. Mississippi .RFO

U.S. ENViRONMENTALPROTECTION AGENCY


--------—----- —I

BEFORE COPYING FORM, ATFACH SITE 1DENTWICATION LABELOR ENTER:

StFENAME Koppers Combany. Inc.

EPAIDN0. M,S, E01O, 7, 0,27,5,4, 31 FORM

WRI I WASTE RECEIVED FROM OFF SITE

WHO MUST COMPLETE THIS FORM? Form WR must be completed by every site that received hazardçus waste from an off-site sourceduring 1987.

[] Mark if you are not required to complete Form WR

INSTRUCTIONS: Please read the detailed Instructions beginning on page 24 ol the 1967 Hazardous WasteGeneration and Management Report Instructions booklet before completing this form.Photocopy and complete additional copies of this form If your site received more than twohazardous wastes from off site during 1967.

For each waste, complete boxes A through J. Throughout this form enter DK if the Informationrequested is not known or not available; enter NA If the information is not applicable.

A. Daicrlp4lon of hazi.rdoui. 8. EPA haiwdou,q. cod. C. 8*. t*zdou, cod.Waste njcton Page 24 P.g. 24 Pag. 25

Soil, sand, rock contaminated IU,015,1 I I I I Iwith creosote — spill cleanup ,

IlIllilIll 111111

0. C?-a8. source EPA ID No. E. 1987 OuaodIy r.c.h.d F. 1.7DM 8. D.nalyPaQ.25 Pag.25 Paq.25 P.q.25

I i 1.1 JII,L,D,01010,8,l,9,9,4,61 , ,,2,0,0I IJ Qaw/QaI Gag

H. Wail. fomi cod. I. Number of shipment. J. OneS. T/9/D/R cod.PeQ.25 Page25 Pag.2e

ii 510,11 21 N,A I 3 I ,N,AI 4 I ,N ,AIIH, , I 1010111 51 ,N1 Aj el , N(\ I 7 I i NAI 81 ,N ,AI

A. .,cilpf Ion of hazsrdous wail. B. EPA hazsrdous wail, cod. C. 9W. hazardouse cod.Waste Inslrucøon Pag. 24 P.9.24 Page 25

2:. 1111111111 1111111

1111111111 I ,,,,I0. OS-eS. source EPA ID No. E. 1967 Quaniffy r.c.Is.d F. UOM 0. D.nalIy

Pag.25 P.9.25 Pag.25 Pag29Shn. ai abcee []Ua,*tJnsarn..sInWast.i I 1.1

dt—>I_l , , , i i I I i I I........I [j.ItI I:)aga WW4, fomi cod. I. Nwnb.r of a14...rds J. On-ill. T/9f0/ code

P10.25 Pag.25 Psg.28

11111 21,11 31,,I 41,,I1111 51,,I 61,11 71i,I 81,11

Comments:

For use in test burn program.

Page 4 of 14

Higriway 51 SOUthTie P1ant Mississippi 38960

I liii IB. 88. ielIcnihIp cod.

Peg. 28

Li

E. Addmas ci offaII InstefietlonP.g. 28

Str..4

U.S ENVIRONMENTAL

____

PROTECTION AGENCY


FORMOFF-SITE IDENTIFICATION

0I

BEFORE COPYING FORM, ATTACH SITE IDENTIFiCATION LA8ELOR ENTER:

SrTENAME Koppers Company, Inc.

EPAIDNO. [,SD1opo1710121751413I

WHO MUST COMPLETE THIS FORM? Form 01 must be completed by every site that shipped hazardous waste off site and every site thatreceived hazardous waste from oft site durIng 1987.

Li Mark [] if you are not required to complete Form 01.INSTRUCTIONS: Please read the detailed instructions beginning on page 2’ of the 1987 Hazardous WasteGeneration and Management Report Instructions booklet before completing this form.

Complete A through E for each off-site installation to which you shipped waste or from which youreceived waste during 1987.Complete A through 0 for every transporter you used during the reporting year.Throughout this form enter DK if the Information requested Is not known or Is not available; enterNA” If the Information requested is not applicable. Make and complete additional copies of thisform if you need to identify more than four off-site installations or transporters.

Site I A. EPA V No. ci ott-sit. Instelistlon cc transpoci.r 8. N.m. ci ott-sit. Inilafl.tIon cc trsnspcit.cj___J Instn,cllon psg. 21 Pt.g. 27

li LiD1 OOjO 8i li9i9i4i61 Koppers Company, Inc.C. 8lt typ. cod. 0. SlI• rststlonshlp cod. E. Addr.is ci off-sit. InstifleflonPeg. 25 P.g.25 Peg. 28

N. Marion StreettiiJ LSJ city Carbondale jI Lj . iSi 29 Oil i—L

Site I A. EPA ID No. ci ci?.sfi. Installation ci trentpocl.r 8. N.m. oi off-sit. Installation 01 tranapocl.r..LJ Instruction peg. 21 Peg. 27

IIIIILIIIIIIIC. Sit. typ. code 0. Sb relationship cod• E. Addr..s ci off-sb lnsIaIlaIionPeg. 28 Peg. 28 Peg. 28

slr.st

I I ZipL.._...J L.........J city Stat. I I Cod. I I I I I—ISite I A. EPA ID No ci ott-sit. Ineleliatlon ci (ranspocl.1 8. N.m. ci oust. flsiIoq ci IrensporlarInstruction peg. 27 Peg. 27

IIIIIIIIIIIIIC. Sit. typ. cod. D. 88, r.Iatlon.hip cod. E. Addie,. ci off-iS. InstaflatlonPeg.28 Psqeae Pag.28

Slr,.4-. V

Li U city sw. LLi d. Ii I —ISit. I A. EPA II) No. ci elf-eli. InstallatIon ci tr.nsport.

Instruction peg. 27

I i I I IC. Si!. type cod.

Psg. 28

Li

9 N.m. ci off-SIc Instellalion ci transpoclarPeg. 27

ZipCIty Slat. I I 0od. L I I I .Ji—l

Comments:

V Page 5 of 14

1‘

FORE COPYING FORM, ATTACH SE IDE, )rlON LABEL 8% U.S. ENViRONMENTALOR ENTER- £% c PROTECTION AGENCY

rrENAME Kop.pers Company, Inc.H i h way 51 SO U t 1987 Hazardous Waste GenerationTie Plant, Mississippi 38960 L

andManagementReport

PA ID NO. 1M1 S1 D1 0 C 70i 2 7i 5i 44 31 FORMWASTE MINIMIZATION

PART I

WHO MUST COMPLETE THIS FORM? Form WM Part I, describing efforts unde,talen to Implement Waste minimization programs, mustbe completed by all g.nerators required to file an Annual/Biennial Report. Thle requirement wasestablished in respons. to statutory provisions Induded In the Hazardous and Solid WasteAmendments of 1964 (HSWA).

NOTE Generators shipping hazar4ous waste off site are required to certify, on Item 18 of theUniform Hazardous Waste Manifest, that they have a program in place to reduce, to the degreedetermined economically practicable, lb. volume and toxicity of hazardous waste generated. Asimilar certification must also be mad. by generators who have obtained a RCRA treatment,storage, or disposal permit. Conslst.nt with these certification r.qulr.m.nts, generators mustreport, on Form WM Part I, th. efforts undertaken to implement waste minimization programs.

INSTRUCTIONS: Please read th. detailed Instructions on page 29 of the 1987 Hazardous Waste Generation andManagement Report kistructions booklet before completing this form.

Answer questions I through 10. Throughout this form enter DK if the information requested is notknown or is not available; enter NA if the information requested Is not applicable.

Did this she create or expand a source reduction and recyclIng program?1987 1986 PrIor Years

Yes No Yes No Yes No

Create [] [] [] [1Expand []fl E][]

2. DId this she have a written policy or statement that outlIned goals, objectives and methods for source reduction andrecycling of hazardous waste?1987 1986 Pr$orYears

Yes

No [] [] []3. What was the dollar amount of capital expehdittir (plant and equipment) and operating costs devoted to source

reduction and recycling of hazardous waste? ENTER ZERO (0) IF NONE.1987 1986 PrIor Years

capital expenditures $ D K $ D K $ D K

Operating costs $ D K $ D K $ D K

4. DId this she have an employee traIning program or provide incentives (bonuses, awards, personal recognition, etc.)to Identify and implement source reduction and recycling opportunities and activities?1987 1986 PrIor Years

Yes No Yes No Yes No

Tradng. . U .. 0‘ Incentives fl fl

Page of 14

OVER—>

0 0 FORM WM - PART

5. DId this site conduct a source reduction and/or recycling opportunity assessment or audit? Note: an opportunityassessment or audit Is a procedure that Identifies practices that can be implemented to reduce the generation ofhazardous waste or the quantity which must subsequently be treated, stored or disposed.

1987 1986 PrlorYearsYes No Yes No Yes No

Slte-Wkie El LI [l ElProcess-Specific [] El El [l LI

8. DId this site Identify or Implement new SOURCE REDUCTION opportunities to reduce the volume and/or toxicityof hazardous waste generated at this site?

198? 1986 PrIor YearsYes No Yes No Yes No

Identify El El [] LIImplement [] [1 Li [] LI

7. What factors have delayed or prevented implethentation o SOURCE iEDUCTlON opportunities. MARK [} NEXTTO ALL THAT At’PLY.

E a. Insufficient capital to Install new source reduction equipment or implement new source reductionpractices.

b. Lack of technical Information on source reduction techniques, applicable to my specific productionprocesses.

[]c. Source reduction Is not economkalIy feasible: cost savings In waste management or production

will not recover the capital Investment.

Eld. Concern that product quality may decline as a result of source reduction.

E]e. Technical limitations of the production processes.

[]f. Permitting burdens.

[]g. Other (SPECIFY)

____________________________________________________________

8. Did this site Identify or Implement new RECYCUNG opportunities to reduce the volume and/or toxicity of hazardouswaste generated at this site or subsequently treated, stored, or disposed of on site or off site?

1087 1986 PrIor YearsYes No Yes No Yes No

Identify Li El tl LIImplement LI El [] LI

Page 7 of 14

I

FORM WM-PART

E’AtoNo. S, I10, 0,7,0,2, 1,5,4, l

9. What factors have delayed or prevented Implementation of on-site or off-she RECYCLING opportunities. MARK LX]NEXT TO ALL THAT APPLY.

[] a. insufficient capital to Install new recycling equipment or implement new recycling practices.

E] b. Lack of technical information on recycling techniques applicable to this site’s specific productionprocesses.

Li c. Recycling Is not economically feasible: cost savings In waste management or productionwifi not recover the capital investment.

[] d. Concern that product quality may decline as a result of recyding.

[] e. Requirements to manifest wastes inhibit shipments off site for recyding.

E] f. Financial liability provisions inhibit shipments off site for recyciing.

[] g. Technical limitations of product processes inhibit shipments off site for recyding.

[] h. Technical limitations of production processes inhibit on-site recycling.

[] I. Permitting burdens inhibit recycling.

[] J. Lack of permitted off-site recycling facilities.

[] k. Unable to Identify a market for recyclable materials.

[] i. Other (SPECIFY)

10. Has this she requested or received technical Information or financial assistance on souroe reduction and/orrecycling practices from any of the following sources? MARK (X] NEXT TO ALL THAT APPLY.

1987 1986 PrlorYearsTechnical Financial Technical Financial Technical Financial

a. Local government [] [] [] [] [] []b. State government [] [] [1 [] [] []c. Federal government fl [] [] [] [] [1d. Trade associations [] [] [i fl [] []e. Educational lnstltutkns [] [] [] [] [] []f. Suppliers [} [] [] [] []g. Other parts of your firm [} [] [] [1 [] []h. Other firms/consultants [J [] [} [] [1 []I. No request made [] [] [] [] [] [jjJ. Other (conferences, literature, [] 0 [] [] [] []etc.)

Comments: #4. Corporate program provides recognition/awards for variousinnovattye ideas, includingwaste•minimization.

#5. No formal audit program. This is addressed as part of corporate costreduction effort.

#8. Re—use technology has been in.effect for a number of years -

technology has not improved on effectiveness of methods used.PaQe 8 of 14_

ORE COPYJNIi FORM, ATrAcH SrrE iDENTIFiCATION LABELOfl NTER:

srrENAiE Koppers Company, Inc.Highway 51 SouthTie Plant, 1ississippi 38960

EPA ID NO. IN, S,D1 0, 0,7,0,27,5,4, FORM

WM

U.S. ENVIRONMENTALPROTEcTioN AGENCY

1987 Hazardous Waste Generationand ManagGment Report

wAsTE MINIMIZATION

PART II

Sec. k EPP taiwdou, *4. cod. B. Slit. hawdou, .it. cod. C. Product ci .Mcs da.ctipt)on 0. Product or ,.r,4e.I uctlonPag.31 Pig. 31 P.g.31 SICcod.P.g.31

IU105JI I I , I Wood preservationj2,49lJ

; IIIIIIIIII 1111111

. *i*. iomi cod. F. UOU 0. D.n&?y H. Beure. d..atp&n I. Sotac cod.r

:8,91 LeJ Iii0J .Io,oI U051 - Creosote spills I23I

EI/ DC. Production mb 0. To,dc*y thing. cod.

Pag.33 Pig.38

[ ,i q [2i. Wod. mintmizitlon: r.cyctlng F. Wait. mtnlmizlon inurc. r.ductton‘°‘ See Comment See Comment

Cod. Ou.nlltyr.cyciod Cod. 0uwt5ypm.r*.d

t.[•...J 2.[...._.J IllIllilli 1.L.j2.L..._J3.[..j Iiii,iI

Sec. k Ninth, daicnipilon at. minimization pro.cl on actMly and r.sull, achl..n.dIII Initniction P.g. 43

No U051 waste generated during 1986 or 1987. Following corporateprogram optimizing good housekeeping practices, etc.

. Page 9 .0114

ill I 11111

WHO MUST COMPLETE ThIS FORM?

LIINSTRUCTIONS:

Form WM Part II must be completed only by generators that engaged in an activity during 1987 thatresulted In waste minimization.

Waste minimization means:(1) reduction in the volume and/or toxicity of hazardous waste generated as a result of sourcereduction; and/or,(2) reduction in the volum, and/or toxicity of hazardous waste subsequently treated, stored, ordisposed as a result of on-site or off-site recycling.

Mark and do not complete this form if no waste minimiistlon results were achieved during 1987.

Please read the detailed Instructions beginning on page 30 of the 1987 Hazardous WasteGeneration and Management Report Instructions booklet before completing this form.

Make and complete a photocopy of this form for each hazardous waste minimized in 1987.

Complete Sections I through IV. Throughout this form enter DK if th. Information requested is notknown or is not available; enter NA It the Information requested is not applicable.

OVER—>

FORM WM PART II

Sec. instructions: Answer questions I through 4. Mark 11 next to the effects produced by the source reduction and/or recycling activity

IV. reported on this form In sectIons I through III.

1. What effect did this site’s source reduction and/or recycling activity have on the quantity of water effluent

produced by hazardous waste generation processes during 1987?

E] a. increase In the quantity of water effluent

E] b. Decrease in the quantity of water efUent

[j c. No effect on the quantity of water effluent

El d. Don’t know

What effect did this site’s source reduction arid/Or recycling activity have on the toxicity of water effluent produced

by hazardous waste generation processes durinO 1987?

El a. Increase in the concentration of há2àrdous constituents

[] b. Decrease In the concentration of hazardous constituents

[] c. No effect on the concentration of hazardous constituents

fl d. Don’t know

3. What effect did this site’s source reduction and/or recycling activity have on the quantity of air emissions

produced by hazardous waste generatIon prôceses during 1987?

El a. increase In the quantity of air emissions

[] b. Decrease In the quantity of air emissions

[] c. No effect on the quantity of air emiSsions

[] d. Don’t know

4. What effect did this site’s source reduction and/or recycling activity have, on the toxicity of the air omissions


El a. Increase in the concentration of hazardous constituents

fl b. Decrease in the concentration of hazardous constituents


O d. Don’t know

Comments:II A,B9E,F. — Effects of waste minimization program cannot be fully

evaluated by examining the quantities generated over time. This is becausethe generatton rates are highly variable and are primarily related to spillpcurrences.

It is Koppers policy that its plant operations optimize and upgrade existingsprocesses to the extent economically possible to achieve waste minimizationtand reduction.

PagelO of 14

SPORE COPYiNG FORM, ATrACH SITE IDENTIFICATION LABELOR ENTER:

StIENAME Koppers Company. Inc.

EPA ID NO.

Highway 51 SouthTie Plant, Mississippi 3896

IMi Siflif)i (17,j0i 2i7i5i 4131FORM

WM

C)U.S. ENVIRONMENTALPROTECTION AGENCY

1987 Hazardous Waste Generationand Managoment Report

WASTE MINIMIZATION

PART II

Sec. A. EPA haiasdou. wait, cod. 8. sat. haz,jdous waif, cod. C. Product or ..Mc. daicr$ptlon 0. Product or seivtcI ?nitnicflon Page 31 Pg.31 PaQ3l Sf0 cod.Pig. 31

IK.,01o11i1 I I Wood PreservationI24

11111 liii iitiil

Wiit. torn, cod. F. UOU 8. D.n.IIy H. 9Ouc d.,eslpftco: I. SoUrce cod.. Pii3t Ptg. Pig.32

[N18,51 [fj I10J .10101 KOOl—Bottom Sediment Sludge 12i91____ []Q.g

Sec. A. lee quantify genal.d 8. 1e? quantify g.nwr.d C ProductIon rub 0. Toidcify cI*ng. cod.II Initruct Ion Pa0. 33 Pig. 33 Pu9 33 P.g. 38

I 250i0I I , I lI.[30I I_QJE. Wait. rnInImIu*Ion: r.cycflng F. Wait. minimization: .owe. reduction

P.0e35 P.g.38

Cod. Ou.ntIfy mcyci.d Cod. Quantify p.d

i.[.QJ 2.L...J IllIllIlil 1.[.QJ2.[._j3.[__..j IIlllIIIl_1

Sec. A. Nwwtt daicrlptlon ct. minimizitIon prof.ct or .clMty and teiuifi .ch1,dlit tnitniction Pig. 43

See Comments.

-

.- .

Page 11. of 14

WHO MUST COMPLETE THIS FORM? Form WM Part II must be completed only by generators that engaged in an ectivtty during 1987 thatresulted in waste minimization.

LiINSTRUCTIONS:

Waste minimization means:(1) reduction in the volume and/or toxicity of hazardous waste generated as a result of sourcreduction; and/or,(2) reduction in the volum, and/or toxicity of hazardous waste subsequently treated, stored, ordisposed as a result of on-site or off-site recycling.

Mark and do nat complete this form If weate minlmiiation jesuits were achieved during 1987.

Please read th. detailed instructions beginning on page 30 of the 1967 Hazardous WasteGeneration and Management Report Instructions booklet before completing this form.

Make and complete a photocopy of this form for! hazardous waste minimized in 1987.

Complete Sections I through IV. Throughout this form enter .)f( if the Information requested is notknown or is not available; enter NA’ if the information requested is not appiicabie.

OVER—>

0 0 FORM WM - PART U

Sec. Instructions: Answer questIons 1 through 4. Mark [l next to the effects produced by the source reduction and/or recycling act)vfty

IV. reported on this form in sectIons I through III.

What effect dkl this site’s source reduction and/or recycling activity have on the quantity of water effluent

produced by hazardous waste generation processes durIng 1987?

[] a. Increase In the quantity of water effluent

[] b. Dec2ease in the quantity of water effluent

[] c. No effect on the quantity of water effluent

E] d. Don’t know

What effect did this site’s source reduction and/or recycling actMty have on the toxicity of water effluent produced

by hazardous waste generation processes durIng 1987?

[] a. Increase In the concentration of ha2ardous constituents

[] b. Decrease In the concentration of hazardous constituents


E] d. Don’t know

3. What effect did this site’s source reduction and/or recycling activity have on the quantity of air emissions


fl a. Increase in the quantity of air emissions

Q b. Decrease in the quantity of air emissions

[] c. No effect on the quantity of air emiasions

[J d. Don’t know

4. What effect did this site’s source reduction and/or recyding activity have on the toxicity of the air emIssions


[] a. Increase in the concentration of hazardous constituents

[] b. Decrease in the concentration of hazardous constituents


Q d. Don’t know

Comments:

IIIA. Effects of waste minimization program cannot be fully evaluated by

examining the quantities generated over time. This is because the

generation rates are highly variable and are primarily related to

spill occurrences. Additionally, the new wastewater treatment

system, which will result in waste minimization, has been in the

planning/design stage since 1986, but will not be operational until

1988. It is Koppers policy that its plant operations optimize and

upgrade existing processes to the extent economically possible to

achieve waste minimization and reduction.

Page 12 of_jj

,.

BEFORE COPYING FORM, ATTACH SIT_AF1CATiON LABEL .,° “%— U.S. ENVIRONMENTALOR ENTER:

Tj PROTECTiON AGENCYSENAME

Koppers Company, Inc.H i g h way 5 1 So u t h \ 1987 Hazardous Waste GenerationTie Plant, Mississippi 38960

anciManagementReportEPA ID NO. I M, S,D ,0 , 0 710, 2, 7,5 i 4 31 FORM

WASTE TREATMENT, STORAGE,PS DISPOSAL, OR RECYCUNGPROCESS SYSTEMS

WHO MUST COMPLETE THIS FORM? Form PS must be completed by every sits that, durIng 1987, had one or more hazardous wastemanagement systems, existing or under construction, composed of: (1) treatment, storage,disposal, or recycling processes subject to flORA Interim status or permit requirements; or (2)treatment, disposal, or recycling processes •x.mpt from flORA interim status or permitrequirements.

INSTRUCTIONS: Please read the detailed Instructions beginning on page 44 of the 1987 Hazardous WasteGeneration and Management Report instructions booklet before completing this form.Make and complete a photocopy of this form for each hazardous waste treatment, storage,disposal or recycling system operated or under construction during 1987.Complete Sections I through IV. Throughout this form enter DK If the Information requested is notknown or is not available; enter NA if the Information requested Is not applicable.

I

j A. Waxi. he.lm.nl, .ioag., dl.po.al c rmcycllng .y.l.m deacriprlonB. 8y.m ld.nlNIodIonI n,lniconPag.57 Generation and storage of KOOl waste in PQ,57 Numb( 1.11.1

Surface Impoundment I IC. On-eli. T/S/D/R codef.)

Peg. 55

,S10,4,1 I II I I II I I I

IllIlIlIllIllIl I

I;II—

&Ie7h,fluentquaritRyS commentInsiruction Psg. 50

rosi i i i5i3i9i3i.i7i5i

Rcn.A ii , .i 2i5 i i i i i I

C. 1957 eolldjeludg. re*idual querrillyPag.eI comments

To4ai I I I I I I I

0. F1.gul.*o.y .lahis cod.Peg. 55

LJ

B. UOllPeg. 51

jJ

F. p.relIonai slalu.Peg. 55

Cod. V..,

iiSi ii i9i8i7i

F. Numbac o month. .ysi.mo..r.donel during 1957pag so

1 ,2,

ILn* il i .i2i5i i i i_j i

0. Twdnu,nb.qotunllsP.O. 50

Tp. Numb.r

L till

U liii

0. 1957 aqu.ou$ .mu.nl quantityPeg52 See commentsTotsil III3lI7IF

FR*t II 111111

i I1IIflhtIIfllflIII i i i i i i i i

C. Umliallona on capacity 0. Cocnm.td& a..Jl.ll1ty F. Prcard c.pacfiyPeg. 95 cod. comrn.rcl&ty .w.$thl.

N/A Pig.95

I. U 2. U . U LPJ I I 101 S

Sec. A. ur. epeCtacyIV nsirucnon pag, its

—i__i]_i yew.

B. Exp.ct.d clang, In maximum capacity duringn.xt 5y..s hmugh 1992)Pa0. 95

XJ’” (CONTINuE WITH BOX C)

0 No (SKIP REMAINING QUESTIONS)

C. Inc.ax. or d.cmax. In maximum capacity cod.P.g. its

d2j

0. Amount o clang. I F. Exp.ct.d ye.ro clang. F. Future commercial sliablilty cod. 0. Perc.nt Mu,. capacity commerciallyP.g

See comment I feg.57

I .rIIIIIIIIII ili9i8i8i i.Q.i [ tt1Ji

Comments:Sect. II, A.C.D. — Based on 5000 gal/day of water to Surface Impoundment (5days/week) with’.-l.25 tons (2500#)K00l generated andretained in the bottom of the Surface Impoundment.Sect. IV D. — SurfacëImpoundment to be eliminated and is scheduled forclosure in 1988.

Page 13 of 14

BEFORE COPYING FORM, ATrACH SIT(’DF1CATiON L*BELOR ENTER:

srTENAME Koppers Company, Inc.Highway 51 SouthTie Plant, Mississippi 38960 andManagementReport

EPA ID NO. M, D, 0, 7, C 2, 7,5 4 3 I FORM j WASTE TREATMENT, STORAGE,PS DISPOSAL, ORPROCESS SYSTEMS

WHO MUST COMPLETE ThIS FORM? Form PS must b. completed by every site that, durIng 1987, had one or more hazardous wastemanagement systems, existing or under construction, composed of: (1) treatment, storage,disposal, or recycling processes subject to RCRA Interim status or permit requirements; or (2)treatment, disposal, or recycling processes exempt from RCRA Interim status or permitrequirements.

INSTRUCTiONS: Please read the detailed instructions beginning on page 44 of the 1987 Hazardous WasteGeneration and Management Report Instructions booklet before completing this form.Make and complete a photocopy of this form for hazardous waste treatment, storage,disposal or recycling system operated or under construction durIng 1987.Complete Sections I through IV. Throughout this form enter DK if the Information requested Is notknown or is not available; enter NA’ if the information requested is not applicable.

Sec. i. Weal. ltealm.n, aleteg., dl.poeal ec r.cllng wyslem criplion9. Byslem Id.ntlflcatlonInsln,cllon Peg. 57

Peg. 57 Numb. LeerContainer Storage (See Comments)C. On-die T/SIO/fl Code(s)

..0. R.guleloty ‘talus cod. E. Oprallona) ‘talus F. Numbr ot rnon*, iyW.m. 0. Typ. d numb.c ci unhiae e o mm e n S

during 1957 Peg. SQPeg. SQ

‘.7-[S101 1,, I I Ii I I I Cod. Year

‘‘‘1°lj_ 004iLJI II I I II I I It I tI.II1t9I8l8I See Comments._____

Sec. A. 1957 Ir,hluent quaritlly 0. UOM C. 1957 .oUd/shJdg. realduei quantIty 0. 1057 aqusou. .tIiu.nt quantItyInstruction Pig. 50 Peg. SI Peg. SI Peg. 82TotJ I I I I I I I I I Ot Total I I I I I I I I i0i Total I I I I I I I I 101FItDr1AIIIIII2I2IOIOI FED$tAIIIIIl2I2IflIfll FDRAIlIlIllll0l

-,Sec. & Maximum capacIty 0. Oprallonai capacity C. Umltatlona on capacity . 0. Coromrdal aaJIahlflty E. P.rcant capacityF’ag. 53 Pig. 54 Peg. 85 cod. c..mrnrd&Iy .r&labhaSee Comments See Comments See Comments PegeSS Pag.85

I I I I I I I I I I I I I I I I I I I I 1.)_,J 2._.._.J s.___j ,_ç..J iOiOIt%Sec. & UI. .xp.cI.ncy

Instnjct)on Peg. SQ

L0I K .. See Comments

B. Expected diang. In maximum capacity duringnestS years hrough 1902)PageSS

See CommentsQY.s (CONTINUE WITH BOX C)No (SKIP REMAINING OUESTIONS)

C. Increase or d.......e. In maximum cap.clIy cod.Pag.ee

U

0. Amount ci chw,g. E. Expected year ol change F. Future commercial arellabhisy cod. 0. Perc.nt Mute capacity cornmerr4aflyPig. 57 Page 87 Peg. 87 r.eJlabh•Peg. 87

‘IllIll’’’ 1119111 )......J 1111%

Comments: During November 1987, 4 drums of U051 were received from KoppersCarbondale, IL. plant for use as a fuel additive in a test burn program in1988 at Koppers Grenada, MS. The drums are being temporarily held in storage.at the plant until the time of the test burn. Additionally, a permanentRCRA container stora-g-e building is being built- for- storage of hazardouswastes generated from both on-site and off-site Koppers locations. A’RCRAPart “B” Application has been submitted for the Container Storage Facility.

U.S. ENVIRONMENTALPROTECTION AGENCY

1987 Hazardous Waste Generation

Page l’4 of 1 4

Koppers Company, Inc., Pittsburgh, PA 15219 / 41f

0

KOPPERS

May 19, 1988 EXPRESS MAIL

Mississippi Dept. of Natural ResourcesBureau of Pollution Control2380 Highway 80 WestJackson, MS 39204

Dear Sir or Madam:

The completed 1987 Hazardous Waste Report for Koppers Grenada, MSfacility is enclosed if you have any questions regarding thissubmission, please feel free to contact this office.

Sincerely,

..

lant Manager

JDC/jsw

End.

cc: R. Anderson — Keystone Environmental Resources — Pgh.D. King -

- N. Little Rock

Direct Dial Number 601—226—4584

F.

0 00MB : 2050-0024 Expres 12-31-88

United StatesEnvironmental Protection Agency \


(PACKAGE B)

FORMS

One report package must be completed for every site receiving this mailing:

Complete Package A - 1987 Hazardous Waste Generation and ShipmentReport - if, in 1987, hazardous wastes were notmanaged at this site, as defined in the box on page 1 ofthe instructions booklet.

Complete Package B - 1987 Hazardous Waste Generation and ManagementReport - If, in 1987, hazardous wastes were managedat this site, as defined in the box on page 1 of theinstructions booklet.

Submission of the appropriate Report package fulfills1987 RCRA Annual/Biennial Report requirements.

EPA Form 8700-13A/B (5-80) (Rev. 11-85) Revsed (12-87)

GEN

FtA1’

w.uruiwa-,leaIrn ano wellare AgencyNb. 2080—0080 (ExpIres 9-30-88)CFomi designed (or use on elite U’ “ewrifer).

k.1NIFORM HAZARDOUS ei. or’a US EPA ID No.

WASTE C ( ili iLi ti11 MA

b.

0. II

I I

Printed Typed Name SIgna)4re•. (L.k. t’&.t .- &..T — 17. Transporter I Acknowledgement of Receipt of MaterialsH

A Printed T pedlame Signatur&. / Month Day Year

jXs:.A ({tfj

,jjflo IS. Transporter 2 Ac nowledgement of Receipt of MatenalsPrinted/Typed Name Signature

Month Day YearL11111119. DiScrepancy Indication Space

‘.. :FAC

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L z-’.I 20. Facility Owner or Operator Certification of receipt of hazardous materials covered bytlllêfnaflhfest except as noted in item 19.T Print d/Typid Name Signature

Month Day Yea?Z &lt. ‘E; ft/ccL.LLA,JP IflitS 8022 A Cl/Si)

WHITE1 ‘5DF MEfAI’4s INSTRUCTIONS ON THE BACK -

EPA 8700—22:(Rev 9-86) PrevIous editiona are obsolete

.4

,.,..

.,44 . -..

•

.‘.. Department 01 Health S.r4OiTo*ic Substances Control DlvIiIQfl

Sacramento. Call2 I Information In the shaded areas’Of is not required by Federal law.r a ter’ Name end MsiiinQ Addreee

. . . .4‘,. -

k4- h 1.. •( . ‘? ) 4. !4 I.4—

,,., 4 ‘•4-4” “ sf44 -4. Generator’ePhone( 4 )

‘ [ U i 1. i8. Transporter 1 Company Name 6. US EPA ID Number 4t S. .,k‘.

jr a7. Tranaporter 2 Company Na. 8. US EPA ID Number L’ f•

I I II I I I I I, — i’ ‘w•-i’ .9. Designated Facility Name and Site Address 10. US EPA ID Number & itate FaaORys C -1 ‘ ‘ri.-I..Ltri ‘

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aacitya ‘.;‘

I L f(’L i i ur ic i7ici2i 1I141 —

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12. Contanera 13. Total 14. -‘s.11. Us DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Quantity Unit Waite No. .No. Type WI/Vo5. .•,• , . St*

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1 1111

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‘ -(ri-1_t.’j ItENERATOR’ C R’flFICAflON: (11ereby declare that the contents of this consignment are fully and accurately described abpve by proper shIppingname and are classified, packed, marked, and labeled, and are In all respects in proper condition for transport by highway according to applicableinternational and national government regulations.if I am a large quantity generator, i certify that I have a program In place to reduce the volume and toxicity of Waste generated to the degree I havedetermined to be economically practicable and that I have selected the practicable method of lreatrrient, storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment; OR, if I am a small quantity generator, I have made a goodfaith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Month Day Year

IcII i

:.. 00

Curtis & Tompkins, Ltd., AnaMicat Laboratories, Since 1878290 DMsIon Street. Son Fronsco. CA 94103, Phone (415) 861-1863

LABORATORY NUMBERs 14027-1C!aIENTS KtJPPERS CO.SAMPLE ID: OIL PENTA SLUDGE

.7)teLls in Soils & Wastes by Atomic Absorption SpectrophotometryDigestion Method: EPA 3050

RESULT DETECTIONLIMXT

mg/kg mg/kgAriGnicChtomiw (total)CopperZinc

Boron55 EPA 6010

BPtJ/ POtJtD— — — — — — — — — — —— — — — — — — — — —a— _a_ ‘8 , 4 8 3ASTM D240

flaS — e a — —fl— — .fl— set — a—nna— a_a — — —sasn — — a_aa — — —na— — — a aa

%RPD %SPIKE%RPD %SPIKB

Araônic 9.9 97 Copper 18 100Chromium 17 90 zinc 8.3 99Boron 32 93

METAL

DATE RECEIVED: 1/11/88DATE DIGESTED: 1/20/88DATE ANALYZED: 1/22/88DATE REPORTEDs 2/1/88PAGE 1 of 2

METHOD

4.4 0.50 EPA 7061.14 1.3 EPA 719025 1.3 EPA 7210100 2.5 EPA 7950

3.

QA/QC SUMMARY

San Francisco Wilmington Los Angeles

LABORATORY NUMBERs 14027-2CLIENTs KUPPERS CO.SAMPLE ID: CELLON W. SLUDGE

ArsenicChromium (total)CoppsrZinC

9

DATE RECEIVEDi 1/11/88DATE DIGESTEDs 1/20/88DATE ANALYZEDI 1/22/88DATE REPORTEDs 2/1/88

PAGE 2 of 2

BTU/POUND — — — — — — — — —6 , 26 7ASTM D240

QA/QC SUARY_

— _t___________ — — —a — — — a a__a__a_ —

AxeenicChromiumBoron

%RPD %SPIKE9.9 97

17 9032 93

%RPD %SPIKE18 100

8.3 99

LABORATORY tR71

00 °Curfls & Tompkins. 1k

METAL

Metals in Soile & Wastes by Atomic Absorption SpectrophotometryDigestion/(ethoth EPA 3050

RESULT DETECTION METHODLIMIT

mg/kg mg/kg

4.81518

Boron

0.501.31.32.5

144

EPA 7061EPA 7190EPA 7210EPA 7950

EPA 6010

CopperZinc

W87)

I Pr•vtoua d1Uan. are oboIeIe.

‘:4,

, 01 aII!OflJ5f155Itfl and Welfare AgencyDeW,ent of Health Servio•e; • Form Approved 0MB No. 2050—0039 (ExpIres 9-30-88) ToxIc Substances Control Division‘ pe dat or type. (Form deaIn.d tot us. on ellY’- •wrIt.r). Sacramento, California

UNIFORM HAZARDOUSV

.4rator’s US EPA ID No.D

Msnlfe. )otjInformation in the shaded areasWASTE MANIFEST Dp to F? 1 1 iZio ii?,il of Is not required by Federal law.

3. Generafor’s Name and Mailing AddressNumber

. co ‘4.r.ø.. ) 4 41.CJSQ(j,V

“V 4. Generator’s Phone (9’I(p ) g3 -‘S3SiJf 5. Transporter I Company Name 8. US EPA ID Numberr V• C. ic4iI, ic r

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‘i”12. Containers 13. 14. I.I I. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) C,.,....y Unit West. No.U. V

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15. Special Hang instruC jd Additional I formation (tI44re.i”4lr.a... ie (VV.uSSl w’ I:0 ENERATOR RTI ICATION ereby declare that the contents of this consignment are fully and accurately described above by thper shippingname and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway accordil4o applicable,j internationai and national government regulations.

If I ainertarge quantity generator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I havedetrmined to ao otip1iy practicable and thet I have selected the practicable method of treatment, storage, or disposal currently available tome which nut fK8m *tt and future threat to human health and the environment; OR, If I am a small quantity generator, I have made a good> faith ettort to minIrrttt ñi wiate generation and select the best waste management method that is available to me and that I can afford.

j Prlnt(TypedNnm

•. I SlQn\% Month Day Year

- Transporter 1 Acknowledgement of Receipt df-Materlaia “V

L Printed/Typed Name V

ure Month Day YearIV I I I I I1. Discrepancy Indication SpaoA V

V

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‘s’. GMY , IICCLtLLAA1I? I /Az LV Oi2jo’iS

0White: TSDF SENDS THIS COPY 1’O DOHS WITHIN 30 DAYS


INSTRUCTIONS ON THE BACK

0

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:4. Generator’s Phone (“‘i4) ‘ ‘ — t ,, ‘

L Trsnsp rter Company Name 6. US EPA ID Numbert448. US EPA ID Number

Department of Health ServicesToxic Substances Control Division

Sacramento. California‘‘-‘,I I 2.-.i’ge I information in the shaded areasOf J is not required by Federal law.

7.’ranaporter 2 Company Nale

I I I I I’ I I I I I I. D lte Address to. US EPA ID Number

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PrIr4e!Tyed Namy

— ‘ ,, i’-v’’- ,., ‘‘*c C’% b. t” 4,.Y’I hereby declare that the contents Of this consignment are fully and accurately deacribed above by proper shippingname and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicableInternational and national government regulations.If I am aJarge quantity generator, I certify that have a program In place to reduce the Voiume and toxicity of waste generated to the degree I haredetermined to be economically practicable and that I have selected the practicable niethod of treatment. storage, or disposal currently available tome which minimizes the present and future threat to human health and the environment; OR, if I am a smell quantity generator, I have made a goodfaith effort to minimize my waste generation and select the beat waste management method that is available to me end that I can afford.

Sli’àure.

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::A— Transporter I Acknowledgement of Receipt of Materials ,

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Signaimrb. “ . Month Day YearØ/4V#if‘

.‘ (DHS 8022 A(tIe7)

EPA 5700—22(Rev. 986) Prevtou editions are obaoiste.

• WHITE: TSDFRETAt4 INSTRUCTIONS

II

‘‘: “ ‘‘e’’’

ON THE BACK f.” .J•.‘I. , . ‘

...

a

a ,•

Curtis Bc npkIns, Ltd., AnaMicol Laboratories, Since 1878290 DMskn Street. Son FroncIco. CA 94103. Phone (44) 861-1863w w

DAtE RECEIVED. 1/11/89DArE DIGESPEDs 1/20/88DATE ANALYZEDs 1/22/88DATE RIPORTDs 2/1/88PAGElof 2Met1s In Soils & Wastes by Atomic Absorption SpectrophotonietryDigestion Methods EPA 3050

RESULT DETECTIONLIMIT

mg/kg mg/kg

Boron55

81tJ/ POLIND _e_ — a — — — — C..;_ewwa — — ..c_—..e acec__ — a9 4 8 3ASTM D240

EPA 6010

—

C — Ca — Ccci. — i — — cC —%RPD %SPIKE%RPD %SPIKB

Arsenic 99 97 Copper 18 100Chromium 17 90 Zinc 8.3 99Boron 32 93

Sin Pcanclwco Wilmington Lo# Angl•e

LRBORATORT NUMEERs 14027-1CLIENTs KtJPPERS Co.SAMPLE ID. OIl.. PENTA SLUDGE

/

)IBTAL

ArsoniaChromium (total)CopperZinc

4.41475

100

METHOD

EPA 7061EPA 7190EPA 7210EPA 7950

0.501.31323

1

QA/QC SUMMARY

‘—

Curtis & TompkklL Ltd.

LORATORY NUMBERs 14027-2CLXENT! KUPPERS Co.SAMPLE 10* CELLON Mr. SLUDGE

DATE RECRIVEDe 1/11/88DATE DIQESTEDs 1/20/88DATE ANALYZEDi 1/22/88DATE REPORTEDi 2/1/88

PAGE 2 of 2Metals in Soils & Wastes by Atomic Absorption SpeotrophotometryDigestion/4ethod* EPA 3050


mg/kg mg/kgArsenicChromium (total)CopperZinc

4.8 0.5015 1.318 1.3

9 2,5

EPA 7061EPA 7190EPA 7210EPA 7950

44 1

BTU/POUt4D— — — — —— — — — — — — —— — — — 6 , 26 7ASTM D240

QA/QC SUMMARY

EPA 6010

%RPD %SPIKE%RPD %SPIKBArsenic 9.9 97 Copper 18 100Chromium 17 90 Zinc 8.3 99Boron 32 g3

: C)

METALMETHOD

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4

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IN8ThUCTJONS ON ThE BACK

• 5 S)

. Department of Health ServicesToxic Sub.t5ncea Control Division

- Sacramento, Ceitfornia

—2 Pa I Informafloa In the ahaded areas

øV Is not-required by Federal law.

‘ Slijot Ccliiornia-—llealth end Welfate Agency- Poiftt Approved 0MB No. 2050—ô038 (Expires 9-3O-sp’% £‘‘i-P1 ‘ rnt or lape. (Fprpi dealaned fot Un on shift ipewfter).

—.-‘Generator’s U EP lb No.

WASTE MANIFEST

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.•—4 ‘,)‘r”44ne9nmows CERTIFICAflON: I hereby declare that the compntabI this consignment are fully and aocurBtely described above by proper shippingname and are classified, packed, marked, and labeled, end In all respects in proper condition ton transport by highway according to applicableinternational and national government regulations..

S Iif I am a large quantity g.nrtor, I certify that I have a program In place to reduce the volume and toxicity of waste generated to tha degree I hayedetermined to be economically practicable and that I have Celeoted the practicable method of treatment, storage, or disposal currently available tome which minimizes the prepent and future threat to human health ihd the environment; OR, if I am a small qàantlty generqtor, I have made a goodfaith effort to minimize my wbate ensratlon Snd select the management method -that is avilleble t me and that I can afford.

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Document No.1

WASTE MANIFEST- 9 i/il I2IOIiJIb IbI19

4.

3. Generators Name and Mailing Address

LGenerator’s Phone (C1( ‘>— s

Department of Health $ervlceiToxic Substances Control Diviolot

Sacramento, Caltfomk

Information in the shaded areasis not required by Federal law.

5. Transporter I Company Name , 6. US EPA ID Number)4çs kAA1Lic ( -NQ- ijWiiCsFt7. Transporter 2 CompI Na9e 8. US EPA ID Number

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NERAT0R

J Additional Descnip enS for M data List d Above ,t , K. 4ndtlnj Codes for Wastes Listed Above

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I -22-Si15. Special Handling Insiru’Ilons a’4Additional Informs-

(4 “ i-’.o+’ — cicr,kt tG.or j ‘ -kc. .s - p - -

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c-1fAsCA.s .t*ct.& &-, r.t ‘i. .4’ t16. •....‘

‘- •i2,._. 1e.., J-As.. c’ic— VJLlc.%b *..tGENERAToR’S CERTIFICATION: I hereby detat the àontenta of this consignment are fully and accurateTy described above by proper shippingname and are classified, packed, marked, and labeled, and are In all respects in proper condition for transport by highway according to applicableinternational and national government regulations.Iti am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I havedetermined to be economically practicable and that I have seleoed the practicable method of treatment, storage, or disposal currently available tome which minimizes the present and future thret to human health and the environment; OR, if I am a small quantity generator, I have made a goodfaith effort to minimize my waste genaratio and select the best waste management method that is available to me and that I can afford.

4, C,Printed/Typed Name

C aVa\e: A I sit:Month Day Year

i&1L1.rLf IIT — iy Transporter 1 Acknowledgement of Receipt of MaterialsR

Month Day Veer

A Printed/Typed Name

ØD T4i Isfi I

of Materialso lB. Transporter 2 Acknowledgement ofPrinted/Typed Name Signature

Month Day Year.—..,.—.....—..-—... I I I I I19. Discrepancy Indication Space

FAC

II 20. FaciIlIy Owner or Operator Centificetion of receipt of hazardous materials covered by this manifest except as noted In Item 19.T Printed/Typed Name j Signature Month Day Year4k)4’/’D I j’” )ijL—)k1Z,OHS 8022 A (1/87)

EPA 8700—22(Rev. 9.86) PrevIous editions are obsolete.

/White; TSDF SENDS fillS COPY TO DOHS WITHIN 30 DAYS


F INSTRUCTIONS ON THE BACK

b.

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.StCte OIlfCnl!--41ealth and Welfare Agency .:.. •. Department of Health 8ervloes.orEn Apptoved ÔMIJ No. 2050—0039 (Expires 9-3O.8). f Vj—., Toxl Substances Control DIvia)b*tSYPe. (Pami designed kir use on 01111/ ‘‘Y.L /ewr1te. (‘ ) Sacramento, Cafl1Om*

iNWORM HAZARDOUS /nuiator’a US EPA 40 No. Manifest 2.. .*ge 1 InformatIon In the shaded ereaeVt... WASTE MANIFEST [. i I ‘1 lbi ° / is not required by Federal law j; Gflerator’i Name and Mailing Address

_.. - .- .1. - ,_j____..-,..

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4 Generator a Phone C ..

i ift6. 1’ransportr I Company Name 6. US EPA ID Number

- , c,..,. Vit.-i iC(iiiLni27. Transporter 2 Company Name 1 8. US EPA ID Number

IIIIIIIIIVIII9. Designated Facility Name and SIte Address 10. US EPA ID Number .S)4C,

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- LL 1.1 1 I• a’.._

l LNI i 1ICIZI1ji4 ‘ IV

‘V. 12.. Total 14o ii. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Quantity UnitU..

No. Type

____________

___________

a.-(4j. ‘.-‘Ci\,. —

____________

__________

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.i. Add*Ionei Descriplions f-’

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____________

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16. SpecIal Handling Inst.... ....... 4 ,. VV, . . , .- • ,. . , .0<

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5_ •.. ‘ fo GENERATOi4 S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurate1, described above by froper shippingname and are classified, packed, marked, and labeled, and are in all respects In proper condition for transport by highway according to applicableinternational and national government regulations.If I am a large quantity generator, I certify that I have a program In place to reduce the volume and toxicity of waste generated to the degree I havedetermined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available too me which mInimizes the present and future threat to human he2ith and the environment; OR, if I am a amali quantity generator, I have made a goodfaith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.0

Printed/Typed Name‘ Stgpature (4

Month Day YearV

LI 2 iRANSp0RTE

-a--FA

‘11Y

17. Transporter I Acknowledgement of Receipt of MateriaiaPrinted/Typed Name SI ‘ •i J Month Day Year“r IzJc. Ii4(.LI18. Transporter 2 Acknowledgement of Icelpt of Materials V__

Pflnted/Typed Name Signature Month Day Year

I I I I19. DIscrepancy indication Space

20. FacilIty Owner or Operator Certification of receipt of hazsrdoua materials covered by this manifest except as noted in Item 19.Printed ITyped Name I Signature Month Day Yearfl1v$

V j) J6A 4 IOHS 8022 A (if 67)wHirm •J•5Øy4pJ5 V /

INSTRUCTIONS ON THE BACKEPA 8700—22 VV

(Rev. 9-86) Previous editions are obsolete.

VVV

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CuIs & Tompkins, Ltd., AnaMical Laboratories, Since 1878290 DIv)sgn Street, Son Francisco, CA 94103, Phone (415) 864-1863

DATE RECEIVED: 1/11/88DATE DIGESTED: 1/20/88DATE ANALYZED: 1/22/88DATE REPORTED: 2/1/88PAGE 3. of 2

RESULT DETECTION METHODLIMITmg/kg mg/kg

ArmeniaChromium (total)CopperZinc

Boron55 EPA 6010

ETtI/ POtflD— — — — — — — — —— ————— — — — — — — — aa._5 4 8 3ASTM D240

—— — — a_a__a—a_a — — —nnafla ana__a — a__a— — — 5_ —%RPD %SPI.E

%RPD %SPIKEArsenic 9.9 97 Copper 18 100Chromium 3.7 90 Zinc 8.3 99Boron 32 93

C 0

IAB0RATORT NUMBER: 14027-1Ct.XENTs KtJPPERS Co.SAMPLE ID: OIL PENTA SLUDGE

METAL

/tsle in Soils & Wastes by Atomic Absorption SpectrophotometryI)Lgestion Method: EPA 3050

4.4 050 EPA 706114 1.3 EPA 71.9025 1.3 EPA 72103.00 2.5 EPA 7950

1

QA/QO SUM?ARY

San Fr*nciscc Wilmington Los Angsl*s

LAEORATORY NUMBERs 14027-2CLIENT: KUPPERS Co.S1MPLE ID: CELLON NT. SLUDGE


mg/kg mg/kg

DATE RECEIVED: 1/11/88DATE DIGESTED: 1/20/88DATE ANALYZED: 1/22/88DATE REPORTED: 2/1/88PAGE 2 of 2

ArsenicChromium (total)CopperZinc

4.81518

o • 501.31,3

9 2.5

EPA 7061EPA 7190EPA 7210EPA 7950

Boron44

BTU/POUND—S — — — — —— — — — — — — — — — — ———— — — — — —— —— 6, 26 7ASTM D240

EPA 6010

— _ — S — — — — — a — a a —5_ — __ — — — __ — — — —— — — — — _ — — — — — _ —

— _ —%RPD %SPIKE%RPD %SPIKEAreenic 9.9 97 Copper 18 100Chrom.tum 17 90 Zinc 8.3 99Boron 32

fi 0 cOLCurtis & Tompkins. 1k

METAL

Metals in Soile & Wastes by Atomic Absorption SpectrophotometryDigestion/4ethod: EPA 3050

METHOD

1

QA/QC SU)*IARY

2200 CHURCHILL ROAD, SPRINGFIELD, ILLINOIS 62794-9276 (217) 782-6761 1L532-06l0P.O. BOX/R.V’)

LPC 62 8/81(Form designed for use on e )-‘p,,on) typewriter.) EPA Form 8700-22 (Rev. 9..,. ‘ Form Apprded. 0MB No. 2050-0039, ExpIres 9-30-88

A. ilhno Manest fl44flH. IllInois

.

Generator’s

I 01 7 ?i 8 0 01 0 Ofi

16. GENERATORS cERrjhcAnoPl hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highwayaccording to applicable international and national government regulations.If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present andfuture threat to human health arid the environment; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and selectthe best waste management method that is available to me and that I can afford.

- I DatePrinted/Typed Name Signature Month Day Year- Gerald Jlgler /I1.-e1.zI/J/ 0 415 8 8T 17 Transporter 1 Acknowledgement of Receipt of Materials

. .‘. - I ii DatePrinted/Typed Name Sigrtf-

“ Month Day YearJoefleafro .

. o4158’8O 18 Transporter 2 Acknowledgement of Recetpt of MatertalsDateT Printed/Typed Name Signature Month Day YearR

19. Discrepancy Indication SpaceFAC

L

20. Facility Owner or Operator: Certification of receipt of hazadàus materials covered by this manifest except as noted in item 19. Dale

--24 HOUR EMERGENCY AND SPILL ASSlSJCE NUMBERSSTRIBUTION. PART - 1 GENERATOR PART - 2 (EPA PART - 3 FACILITY PART - 4 TRANSPORTER PART - 5 IEPA PART - 6 GENERATORIV 7

GENERATOR COPY — PART 1-00 NOT REMOVE PART I FROM SET UNTiL COMPLETED.The Ag I -l i n to Ill Ron end RI t Cl p1 II I S 2 I th I the to m I on b Sm I I to hr Ag op F I to p v -t,, the to,,,,. Ion In. y me It I r it It, me me’Or operotflr ft II I’,I ‘I flIt .‘1 vi •j—,ImtI.r F.n’—itc,rt —mm vi Itt, irrtvmrmrntkm,r lIly mr’ ,,II m, a tint’ t,p to S5(.COY1 pem day 0) t’I.l,n,, trot itmp,i’,i,,,, II tIm ItO S tears 1)10 terre h,,s torn tIp t—,I Ih It’’, ItCoot’,

FACtIITV COPY PART 3


3. Generators Name and Mailing AddressIo.ay, Inc.

P. 0. flax 704. Generator’s Phone ( 618 )

45$,bo!w1ale. U. 62901.

UNIFORM HAZARDOUS 1. Generator’s lj EPJD No. Manifest 2. Page 1 Information in the shaded areas snotWASTE MANIFEST t °o°8]9 Dcj No,of 1 required by Federal law, butts required

5. Transporter 1 Company Name 6. US EP mer C. IllinoisT1anporter’s ID__________________Dart Trucking Co., Inc. I °“‘ D. ( 600 b0i08J Transporter’s Phone7. Transporter 2 Company Name 8. US EP ID Number E,IIlinolS Transporter’s ID

‘I t. ( ‘) Transporter’s Phone9. Designated Facilty Name and Sjte Addres 10. US EPA ID Number G. IllinoisKoppera company, inc. clIlty STie Plant Route 68

H Pa lilt ‘s PhonI

Grene’la, ssssip1i ‘° P131) 007027543( O) 2Z.Ji4

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 1 2. Containers 13. — 14.Total UnitNo, Type Quantity VI/Vo Waste No.a.

wonardous process iaate liquid )SN 1?. A. 9188 (co*taine used peatach1ezoencl) DM

28 01 )tdborlzatkih Number

E,

— III I’___ 11111R

b.on—ha r.ous ocees iaste ER 11W Number

A (creosote Siutig.) jfljf 20 TM 5 1 AuthorJzaUonmtherT r1— I I I — I I. I I 1c.0/11i

P\)’Ii I I IR

3 0I . -----d. fr’ 11W Number%a 3c3o XXm

J. Additional Descriptions for Materipl, irted Abo °‘ ‘9andiIn Listed Above

P—1 1 = Gailons 2 = Cubic Yards. /,, I : ;l’f’ I’.’ i;”. ‘‘. ‘‘ ‘it1(; ‘t H. I’lmt 1/ ‘‘ j’p *


Rubber gloves ar eye protection to be irn dten handling druas

Printed/Typed Name

,c/1.?’t &.. P1c-LFLLAWDI ILLINOIS: 217/ 782-3637

SignaturL. c ih”v’ái’tiMont Day Y arot?,

OUTSIDE ILLINOIS: 800 / 424-8802 or 202 / 426-2675

Z3/24/Iz2E 1102 PGH. KE’?STCHE 41222246 F.22

flVKEYsEFoNE\FNVIONMENTAL RESOURCES INC.

Phone: 412/227-2694 436 Seventh Avenue, SuIte 1940, PIttsburgh, PA 15219 Fax: 412/227-2436

March 24, 1988 Via FAX601—961—5190

Mr. David J. BockelmannHydrologistHazardous Waste DivisionMississippi Department of

Natural ResourcesBureau of Pollution ControlBox 103852380 Highway 80 WestJackson, Mississippi 39204

RE: Part A ApplicationKoppers Grenada, MS Facility

Dear Mr. Bockelniann:

with this FAX transmission are copies of revised pages 1 of 5 and2 of 5 of the Part A Application for Koppers Grenada, Mississippifacility.

If you need additional information, please feel free to contactme at (412) 227—2683.

Sincerely,

Wc4sstj 4i6wn%jRobert J. AndersonStaff Program Manager

RJA/CJV/ j sw

Enclosures

i. ENVtnONMENIAI. pQTEcTIQN AOtNc

8 EPA- HALARDOUS WASTE PERMIT APPLICATIONC’o7idiIdated PenvIts Ptogricsili I,,I’qi,’,itton la,quIrq4 under Seet$s,., 2005 ci RCit4,

4122272436 P.33

() omr Aprcred 0MB No,

Fl. EPA 1.D. NUM

iL 1ii L!J

CONTAINER (boweL drus, ejYANKWAC1! P11.1

IIJNFACI IMPOUNOMEISY

INJ lOTION W*h.i.1.ANOPIL.t,

LAND AP*1.ICATIONOCEAN OIIPO*A1.

1LS*ACX IMPOUNDMENT

33/24/1966 11 33 P3H. KESTGNEthW—ft,.ress ate rocic’ lot ethe

_________

3PiRA

cFOR OFFICIAL. USE ONI.Y.——.

[friMisiDiolo 17 l t. LTtCOMM EN TI

II, FIRST OR REVISED APPUCATION

_____

___________

Place in “X” in Pu• sproptiiti boz lie A or S below lrna,* One beN ovelyl to indicate ru’hath,r this is the first apUcatlon you are subnul11n for your lacility or ativi)id application. It this is your first application and you airiedy know your facility’S EPA 1,0. Number, ø II this is a revised appflcton. ante, your tiiIity’i

EPA ID. Number in tam I aboiq.A. FIR$TAPPL.iCATIONrPtX.an°Z”b.SOWwi4prou1ed*Aiscipro.r1et.i.ts)

“

--

I, CXII? INO rACILJTY (see hi ItPUCUOM OP drflnIflon o’ “ixiUInf” f.cWty, aNEW FACILITY (Complete tam bilow.)Camp WtS 4t.ne bilow,j

NEW PACIIITICI.

• ii5 S GA’’l N (place ore “X’ biloii ,d mplmfe ltim1 abo#qf -..•s. r’ACIi..ITV HAl INTERIM I?ATUIa. oIewV HAeACRA PIqMIT1L PROCESSES—CODES AND DESiGN CAPArmES _J

A. PROCESS CODE — dii codo from he list of process codes below that best describes ascii procesa to be used at she facility. Fan in,, are provided for

antirin codes, If more lines ire needed, lets, the codi(tJ In the spice provided. it a pcocs will be uaed hit Ia not included Ire she Iett of aodes,below, thendicoilbe the process llncIud1ivIoi deslps ciry In the pace provided on the form (Ifwv, lIbC).S. PROCESS DESIGN CAPACITY — For seds cede entered In column A enter the cepicity of the process.I • AMOUNT — Enter the imount.2. UNIT OF MEASURE — For a.i imount entesid in column 5(1), Intef the code from the list of unit m.mure codes below thiS describes the unit of

rn.vre used. Only the units of mure that we listed below should be aid.PRO’ APPROPRIATE UNrS OF

PRO. APPROPRIATE UNITS OPCESS MEASURE FOR PROCESS

CESS MEASURE FOR PROCESS_S D1l tlAperrv

fl1 DiI0r’&CAPACyY -

CCI •AL.I.ONI ON 1.111*1 TANK755 4A1..L.ON* PER DAY 0*

10* IALLONI ON 1.17CN$LITERS PEN DAY

CCI CUCIC YANDI 0* IURFACE (MPOUNDMINr Tel OAI.i.QrS DAY ORCURIO MIlENS

LITERS PIN OAV104 OAL.I.ONI 0* MTERS INCINCRA’ToN 101 tONS PEP NOUN ORMETRIC TONI PEN NOWISI

_______

OAI,1.0f41 PCN NOUN ONDie GALLONS OR ht,E.NS

lITEPI PER NOuN010 ACNg.FIZ1’(theUOI*rmithat O’rsqpi(LTeeforph,efcal &u.mlced. 704 GAI.I.ONS PER DAY ORwould cover on. acre toe diurnal or bioloiEoal trfealm,nt 1.17CN$ PER CAYdepth of one foot) 0* prgoeuee not cccorrfrei in fanhe..urlbce fmpowedm,nla or ffieln.Dit ACRISOR HECtANEI ClOTS. PMcr(bq tleppvccesac.ffiOil GALLONS PEN DAY OR the spae• poirld.d; Store, l11•C.)LITERI PER DAYDII GALLONS OR LITERS

UNSTOFUNITOFMEASURE

MEASUREçOO€’.’.7e FOPMEA$URS“ cOOE’ ‘ UNIT OF MEASURE.

GALLONI,,.. 0 UtERI PEN DAY,

,,, . V AGRI-FECT,. A

LITENI . , . , ,., .1. tONS PER HOUR .

, , 0 H*O’rANI.M1?t F

CURIO YANaC .Y • MITAIC1ONIPER NOUN.., W ,PU.... ,. .. .

CUIIC MItENC ,,p5,.r • 0AON* PW*NOUN r.5P,. I ‘.*f lANES .‘e

GA1.I.OHS PER DAY . ,., .-, .. • 1.511*0 PERNOUq.. ., . ..... • K’EXAMPLE FOR COMPLETING ITEM UI (msrt In Ifrejrnb.j’sXI andX2ft.IowI: A facility lies t storee tanks, area tank cars hold 200 gallon. and heether cm hold 400 gallons, The facility else us an lnciiwretor that can burn up to 20 gallons per hour,

UNIT OP MEASURE

4 :.-.

S PROCESS DESIGN CAPACITY •

S PROCESS OESIGH CAPACITYA.PRO’ r.-

A.PRO- -

GElS1 UNIT OFII4lAL. CESs

2. UNIT OFfICIAl.

.‘

‘ijQL

MN

X-1S02 00 ‘ ‘•. G 5

X- TOS- 20

. j•_-±.-:.. - -

L 13o, 650-

- --

2‘

83_

‘

- 94

I,___

II I • II

10

CONTINUE ON rr. “It

EPA Form 3510-3 IS-lOSPAGE 1 OI S

3/24/i96E ii:4 P--. KESTCNE

Cor’tln’.is from h front.

/__122272436 p.4

I—

C. SIACS on AoIrIor4AI. ppiocgel Coo’s C ran CCRtsNQ oricn nccusO øegJ “. pn CAI4 PoesSs ZNTtnSe HtC

IMCI.uO OCIIGN CAPACITY.

Note: Ill.C. Line I

650 cubic yards x 201 gal /yd3 = 130,650 gallons

A. MA NUUS ttATS NVMbLN — enter WI VOUt—O)It IfltmV TtOtfl 44J ijn, egbpart c tot each listea hIzat4OuI waste you mu handle, it you

hndia haw’douja watt$ which er, not listed In 40 CPR. Subpart 0, enter he four—digit numberf.J from 40 CPA. Subpart C that detoribee the chi(IctirIs.

flea and/or the toxic oentwiin..nte of those hazardous wastes.B. ES1’TMATEO ANNUAL CUAHfllY — Fe,’ aich lhd el entred in column A aitimete the quantity of that ww, ttuit wilt be handd on an armuel

bail;. For cad, thaeuiai.Ue or tole a naimknf intend In column A estimat, the tOtal annual quantity of iii the non—listed waste(s) that will be handled

which poisew thit cliarectirlitic or certtemlnin*.C. UNIT OF MEAJRE — For eath quantity antanid in column B enter the unit of measure code. Units of tom.ns which must be used end the appropriate

odeeare: i... . .

CNLiSWUNjF MASA1R— MBTRIeiJNt’rF MASURB

—

PO,Jl4O* .P KtL.OOAuI

* ,

TONS. ..‘ .,

.. - .,.,_ MITst(CTONj........ .. . . ,. •If facility record. use arty other unit øf measure for quantity, the units of meawre muwa be conrted into one of the required uniti of measure taking into

eccount the appropriate dendty or epoch Ic 9revhty of the wait,.0. PROCEES

1. PROCESS CODES:For li.esd haiwdou. waite: For each Ibd hazardous waits uttered in column A select the code(s) from the in of procwa codas cOrtt;Irt.d In itam iii

to indicate how the rains will be stOred, e.d, snd/or.dIipadOf,t the f5cIllty..f. “*““ . ._.... .

Fe,’ non—listed hazardous wee: Fr each dter,cssrirtk or tezie contaminant entered in column A salact ha code(s) fron, he list of process aode

cantelned In Item Ill to Indicate dl the proa that will be ueed to store, tilt, and/or dispoac of sit the non—listed hazardous wastes that possess

that eharicreristic or toalo contaminant.Noes: Four ‘picas are provided for entering pro codas. if more ire needed: (1) Enter th• first three as dwcrib.d above: (21 Enter “000” in the

satr,me right box of Item iV.O(i) end (3) Enter in the ca provided on page 4, the fine number and the additIonal coda(s).2, PROCESs OESCR IFTION Ifs code. not hated for a pres that will be used, describe the procies in the space provided on the form.NOTEt HAZARDOUS WASTES DESCRIBED BY MORE ThAN ONE EPA HAZARDOUS WAITE NUMBER - Hazardous wastes that can be described by

more then one EPA Haurdoua Waits Number shall be described on the form as follow,:I • Scat one of the EPA Hiwdoue Wese Numbers and enter It In column A. On the aim. line complete columns B.C. arid 0 by estlmatlrtq the total an,niici

quantity of the waite aid dausibing all the proai.e. ta be used ta trait, store, end/or dhapot of the wate,2. in column A of the next line enw the other EPA Hazardous Waste Number that con be geld to desorib. the waste, In column 012) on that line inter

9nduded with above” end mika no other enwim on that line.3, Repeat step 2 for uch other EPA Hazardous West. Number that can ba used to deacrib. the hazardous waste.EXAMPLE FOR CGMFLETIFdQ ITEM IV (abQewi ki huts ,nvT X4. k2. X.3 cod X.4 below) — A facility will aeat end dla,. of en estimated 900 pounds

pen year of chrome lflavin from leather tinning and finishing oparesion. In acflt1on, the facility will treat and dispose of three non—listed weste. Two westes

Ira corrosive only and there will be art estimated C0 poanda per yew of esdt west,. The otn.,, is i&• _.. jli bean estimated

100 ooun ow v of that iseata. ?,...uvi&1t ,dWh, mlndna.atw end dtspoaal aitilbe in • iandflff .“-AEPA —

- C.IJstrr —

D.PRSCESUIi a5 41L4’’ iPMA

— — - - - —.. -—

— -

- f i ri T1 T rX4X034 900 P T03D80— — — — — — -

— —

— I- i—I- -

— —P —i-—X-2.D002 400 P T03D80- - -

..— ---- -. : ...a—i-. EL.

,.,..

—

.3001 100 P r03D80.— — — — —.—

— —

— r ui —r - i— —

X4 L 0 0 2included with abQ’e

— — C -:-—

— — ——

-.—

-:-

EPAForm soio.z 1040)PAGE 2 OF 5 CONTINUE ON MG J

iL5’ 01310

G

N

FR

A

T

0

R

20. Facility Owner or Operator; CertficatbrtofTeceipt of hazardous materlatscevetedbythtsrllanlfest pt äs1Tätëf in iteñr 19 JZZP___Pri ted/Typed Name SignatureMonth Day Year

. f4c,CULLAWP o.3aggn24 HOUR EMERGENCY AND SPILL ASSISTAN NUMBERS°PART - 3 FACILITY - PART -4 TRANSPORTER PART - 5 EPASV. 7

GENERATOR COPY — PART 1-DO NOT REMOVE PART 1 FROM SET UNTIL COMPLETED.This Agency i nrrlrnrized In regain’. prIrWIrrI IC HhrnrrI9 Ilevisyd Stattrtr’n, Clrnyir’, III’ ‘i’rtnnl 21, hal this Inlo,nvrtron by sirbmi9od In lb, Cgcccy Fnil ire In i,,nvkle Ito lclrymnllon airy pout In 1 iMP p rip I,’ rir.ct’.lre , rvrrr’r

or opern?cr al in to ,d Ta,OrT3 pa, rIny cl vinlilian rafrec ilian ii’ thin ct .r ccr ii ‘liii tire rip hr l’Vrrn’lrr rr -ri. r I I rri.ri urn rgr In, yr’-n TIr’ rrnnr I’ I r’’,r’n’rri. .rc 1.Cenler

IEPA COPY - PART 2

2200 CHURCHILL ROAD, SPRINGFIELD, ILLINOIS (327949276 (2171 782-676 I‘ P0B9Y—2\

PC e’ enr iPlease print ol type (Form designed for use o )( -..A11 typewriter.) EPA Form 8700.22 (Rev.. -r96 Form Approved. 0MB No. 2050-0039, Expires 93088UNJFORMHAZARDOUS Ii. Generators U Mnlfest 2. 1 Information In the shaded areas is notWASTE MANIFEST ltDgf%No

O.nerrt No., I by Illinois law.

I requIred by Federal law, hilt Is required3. Generators Name and Mailing Address

.

.

4. Generator’s Phone ( 618 )1c31._Illinois 62901. i0inOt’ 00 O25. Transporter I Company Name 8. UEP ID.Ntwiber CIII

,‘D8rt Thuokl.ng ao p mo. OUD 0091i1.y3Z5

D.( .- ‘.r’8 Phdne7. Transporter 2 Company Name 8. US EPA ID Number E.IlIlno Tr ‘‘,,

I F. ç ‘ transporter’s Phone9 Designated Facility Name and Site Address 10. US EPA ID Number G.lnolsKeppers taotnpany, Inc..‘13e Plant, Route 68 I I I I I(renada, sissippi 38960 MB]) 007027543 (6O) %48b

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12 Containers - 13.‘Total Unit

-- No Type— Quantity

- VLIVo Vvste No.‘ —

EI3HWNumberRQ son-Hazardous process aete liquid NOB X X1 IN. A. 9188 (contains used pentaohlerohenol) “ DM“ 5 1 AuthartzatbnNumbdrb.

/ — /5C.

.-

-

‘ t’t I I

d— ‘

. . II I I

J. AdditIonal Descriptions for MaterIals Listed AbovendIIng &des ltr Listed AboveIn Item #141 = Gallons 2 = Cubic YardsOontmins sp.nt (uaed) psitachlcroçhnel

i i1_.15. Special Handling Instructions arid Additional Information

Rubber gloves and eye protection to be worn when handling drume16. GENERATOR’S CERTIFICATION: I hereby declare that the Contents of this consignment are fully and accurately described above byproper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by highwayaccording to applicable international and national government regulations

If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to beeconomically practicable and that I have selected the practicable method of treatment, storage, or disposal currently avaiiable to me which minimizes the present andfuture threat to human health and the environment; OR, if I am a small quantity generator. I have made a good tailh effort to minimize my waste generation and selecL__the best waste management method that is available to me and that I can afford.

_______

________

J’’ Date-- Pnnted/Typed Name

I 2lont Yr

T 17. Transporter 1 Acknowledgement of Receipt oL Materials

__________

r

_______

[, DatePrinted/Typed N me Si n ureMonth Day YearRonnie aohe,

0 3 0 8 8 8O 18. Transporter 2 Acknowledgement of Receipt of Materials

_____—_______

.

_____________

T Printed/Typed Name SignatureMonth Day YearR


I

TY

‘1 ILUNOIS: 217 / 782-3637

______

IISTRIBUTION: PART - 1 GENERATOR PART - 2 IEPA01 tTStflF III lIhiOlS’ Rflfl / 404-Rerlo nr 202 / 422J_

PART- 13 GENERATOR

0

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NEH

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PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL RESOURCESBuu/(Vaste Management

( ‘ ). Box 2063

“/. .lsburg, PA 17120

Please print or type. (Form designed for use on elite Ii 2-plichi typewriter.)Form Approved. 0MB No. 2000-0404. ExpIres 7.31-86

UNIFORM HAZARDOUS I Generator’s US EPA ID No. ManifestDocument No. 2. Page 1 I Information in the shaded areas

WASTE MANIFEST P ‘A’!” O’5 6 7 2’3 ‘2 6’ I 5’O 0 •

lie not required by Federal lawI “ ‘ —‘“—“ ‘‘ State law.

3. Generator’s Name end Mailing Address A. St.t. Manifest Document Number

PAB 2715845KOPPRS VOHPANY, INC., P.O • flflX 189 • HONTG(N’EEY’1, PA. B. State Gen. ID17752-0 1894. Generator’s Phone ( 717 I 547-165t ,‘ PAD 0S6723265

5. Transporter 1 Company Name 6. US EPA ID Number C. State Trans. IDPART TRUCKING CO., INC. 10 II ‘5.8.2.5 PA-AH 102 ‘1’9 i

7. Transporter 2 Company Name 8. US EPA ID Number D. Transporter’, Phone (5flQ) 21fi—M 357I E. Stat. Trans. ID9. Designated Facility Name and Site Address 10. US EPA ID Number PAAH I ‘ ‘ I

OPPVR( CO1IIPMAY, INC., P.O. EOX 160 F. Transporter’s Phone I )CRENAflA, 4S 38960 a. Stat. FaclUty’s ID Not RequIred

H. scflity’sPhon. F I12. ContaIners 13. 14.11. US DOT Description (including Proper Shipping Name. Hazard Class, and ID Number) Total Unit Waste No. -

No. Qusntlty fJtiVol‘ RQ—N HAZARPOT8 PROCESS WASTE

N.O.S. LIQUID ORM’-R NA 9188

—b.A

(cONTATW! US1) ‘70 DH ‘1 ‘) ‘0

. . .. • .,.r!

—C’

.5

, 4’ C flf

d./bA...

J. Additional DescrIptions for Materials Listed Above (Include physical state and hazard code) K. Handling Codes fo Wastes Listed AboveHa:. Code Physical State Hat. Code Physical State

. u i i i L. U LI I.

b. U I I I d. U I I I b. d.15. Special Handling instructions and Additional Information

(iTIRN NA1?DTING, WEAR T’ROTECTIVE EQTJIPMENT EQUIPMENT SlICE AS IMPERVIOUS GLOVESAN!) EY1 PROTECTTON

16. GENERATOR’S CERTIFICATION: I tiereiy declare that the contents ol this consignment are tulip and accurately described above by proper shipping name and are classilied.packed, marked and labeled, and are in all respects in proper condition br transport by highway according to applicable international and national government regulationsUnless I am a small quantity generator who has been eaencpted by Statute or regulation (corn die duty to make a waste minirnizaltoii certilication under Section 3002 Ibl ol RCRA. I alsocertely that I cave a program in place to reduce volum and toaicity ol waste generated to lice degree I haee determined to be economically practicable and I have selected the mettcod oftreatment, storage, or disposal currently available tome whiclr mircirnizes ttce present and future threat to truman health and the environment

Printed/Typed Name Signature Month Day YearTWflIAS H1. t,OATNAN

.- 11 711 ‘cIRRT 17. Transporter 1 Acknowledgement of Receipt of MaterialsPrinted/Typed Name

Henry 3. ReddIck III18. Transporter 2 Acknowledgement of Receipt of Materials

T Printed/Typed Name Signature Month Day YearE

IJ I19. Discrepancy IndicatIon Space

FAC

1 20. Facility Owner or Operator: Certification of receipt of hszsrdous materials covered by this manifest except as noted In item 19.TV Printed/Typed Name Signature Month Day Year

Eiii L. PI((LLLLFAIV . iIL’(AC(P

ER-SWM-51 :REV. 10184

-o>w

F’-)

C),00-

C),

FEPA Form 8100-22 13-84) COPY 4 - TSD Facility - Retained by TSfl F-IIIfu

utrMiiliVlti’Jl UF ENVIRONMENTAL. RESOURCESBureau of Wasle Management4ox 2063

jL,_i9.PA 17120

F Please prInt or type. Worm designer) for use on elite 12 pitch) typewriterI Form Approved. 0MB No. 2000 0404. Eapties 7 31 86

J. Additional Descriptions for Materials listed Above (include physical state and hazard cods)Ito,. Code Physical Stale lies. Code Physical State

__

H]

llh I IU h hN HI II NO*PABX2715834*

2 Page 1 I Information in the shadedis riot required by Federal law

- __ lew.A. State Manifest Document Number

_?AaJ158a4.B. State Qen, ID

PAD 056723265C. State Trans. ID

PA-AH 10 ‘2 1 •9

D._Transporters Phone 18001 238—8357S. State Trans. ID

PA All I 1F. Transporter. Phone I I0. Slit. Facility’s ID

Quantity

Phone I I13, 14.

Total Unitfill Vol

16. GENERATORS CERTIFICATION: I hereby declare that the contents of this consIgnment are fully and accurately described above by propershipping name and are classified, packed, marked, and labeled. art(l are In all respects in proper condition for transport byhighway according to applicable internatIonal and national governniental negulalinna. and all applicable State laws!re9ula!lOns. Date

Signe re Month üay

£) Io 2108 18817 Tnenponter1 Acknowledgement of Receipt of MaterIals—

— I [ —PdnWTypedhme

Sini jSy7tu nt

18.Tr!nsport2Acknowle!iqemgtufReceIpio(Materlals .

__

-Printed/Typed Nan,e SignatureMo,,th flay Yea,

__________

I_‘LI’19. DIscrepancy IndicatIon Space

Date --

Signal orMonth Day Veer

214y t.

ZARDOUSIANIFEST

1. Generator’s (IS EPA ID No.P’A’L}05’6’ 1’ 2326

8 ItS EPA ID Number

Manliestflorranant No.

•J 5().o,,()3. Generator’s Name end Molting Address

KOPPERS COMPANY INC P.O.BOX 189 MONTGOMERY, PA17752—0189

4. Generators Phone I 7l7 547—1651.8. Transporter 1 Company Name 6. US EPA Ii) Nmunlier

DART ThUCKING CO., INC 10.11.0.0.0. 9. 8.6. 5.8. Z 57. Transporter 2 Company Name

9. DesIgnated Facility Name and Site Address 10. US EPA ID NumberKOPPERS COMPANY INC P.O.BOX 160

GRENADA, MS 38960

IM’S’D0’0’7’&2 74311. US DOT Description (including Props? Shipping Nan,e, Ha,s,d Clnsg. end ID Number)

RQ-NON HAZARDOUS PROCESS WASTEN.O.S. LIQUID ORM-E NA 9188

- (CONTAINS USEL) CREOSOTE)

__

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H. FacIlIty’s12. Containers

No.

.7 0

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Waste No.

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b. U I I I d. U I I I15. Special Ilairilling lntsi,mtcllons and Additional lnfounatlon

WhEN IIAN1)LJNG, WEAR PROTECTIVE EQUIPMENT SUCh AS IMPEIWIOLJS GLOVESANL) EYE PROTECT TON

K. handling Codes for Wastes listed Above

a. c.

b. d.

Printed/Typed Nan,e

C. David ChioateYsnr

i’dnted/Typnd Nante

GARY . /flCCLtLLAIJD

20. Fecility Ownm,r or Operator: Certilicatlon of receipt of hesarrlotis materials covered by Ibis manifest escept as noted In Item 19.

A Form 870022 13 84) COPY 1 - Destination State - Malted by TSD Facility

rcior Iv?4IIM lJcrMn I IVIP1 i sjr tPl vIr1UIIVIIM IML HUUKI.t

Bureau ‘Waste Management

Box2063PA 17120

Please print or type. Worm designed for use on elite (12-pltchl typewriter.)Form Approved. 0MB No. 2000-0404. Expires 7.31.86ER-SWM-51 :REV. 10/84


00

KQPPIRS C1)lptdlY I:4c P.OjtOX 199 t1cv.Tt.;ui1ERy, PA1fl52’-0189

4. Generator’s Phone I71’) 54 7’165].


PAB 2715834B. State Gen. ID

PAl) 056123265

ManIfestUNIFORM HAZARDOUS 1. Generator’s US EPA ID No. Document No. 2. Page 1 I Information in the shaded areasIs not required by Federal lawWASTE MANIFEST ? “• P0 56’ i a • 2 6’ I 5O•0•0O of 1 I but Is reauired by State law.

5. Transporter 1 Company Name 6, US EPA ID Numbe C. State Trans. IDt)ARL’ TUCKPIG cu.. ‘i; jo 4P.’2. t PA-AH 10 2 19

7. Transporter 2 Company Name 8. US EPA ID Number D. Transporter’s Phone 1800) 238—8357I State Trans. ID

9. Designated Facility Name and Site Address 10. US EPA ID Number PAAK IKOPPERS CO!PA”4Y INC P.O.BOX 160 F. Transporter’s Phone I I

GE1DA, 15 389V0 G. State Fsciflty’s ID Not Requiredi ‘S D 0 0 •7 0 2 7 5 43 H. Facility’s Phone

12. Containers 13. 14.11. US DOT Description (lncuding Proper Shipping Name, Hazard Class, and ID Number) Total Unit Waste No.No. Type Quantity VtIV0Ia.

RQ-NU’17 flAZAR1XUS P!CS ‘7ASTEU.O.S. LIQUID O!4— ZA 910 7 fl I 4.4 .0 .0 0

(C’N°VATW(l tTfl (PPOCJTP)—

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N•. . .E

R c.AT0

.. . . . . .R d. ..

. , ,_____i

— —J. AdditIonal Descriptions for Materials listed Above (Include physical state and hazard code) K. HandlIng Codes for Wastes Listed Above

Haz. Code Physical State Has. Code Physical State

a. U I I I L. U I I I H. L.b. U I I I d. U I I I b. d.


WiEt1 TIANDLINCI, W1A1 PROTTIV1 T,’Q1JIP1’’TT SUC)! AS ViPRVIOUS GLOV)5AP3 FYT PRPVCTI(3N

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16. GENERATOR’S CERTIFICATION: I hereby declare thaf the contents of this consignment are fully and accurately described above by proper shipping name and are classified.packed, marked and labeled, and are in all respects in proper condition for lransport fry highway according to applicable international and national government regulationsUnless I am a small quantity generator who has been eirempted by statute or regulation from the duty to make a waste minimization certification under Section 3002 (b) of RCRA. I alsocertify that I have a program in place to reduce volrini and tooicity of waste generated to the degree f have determined to be economically practicable and I have selected the mel hod oftreatment. storage, or disposal currently available tome which niiriirnizes the present arid future threat to human health and the environment

Printed/Typed Name Signature j , , Month Day Year

C. David Choate ( ,r{ ... ,.i, L.(’’,, 117. Transporter 1 Acknowledgement of Receipt of Matel1Is ‘ ‘ ‘,

.

Printed/Typed Name Signjatgçre , Month Day Year

ichae1 1. Snith I02I0RIR’a18. Transporter 2 Acknowledgement of Receipt of Materials


I.’.’.

TRANSP0RTER

-t

a

19. DIscrepancy Indication Space

20. FacilIty Owner or Operator: Certiflcstlon of receipt of hazardous materials covered by this manifest except as noted In Item 19.

FA

F‘FV Printed/Typed Name Signature Month Day Year

G’1 . f’fr(L1LLAAfl1 f i11(4atd lc.IioI8S’EPA Form 8700-22 (3-84) COPY 4 - TSD FacUlty - RetaIned by TSD FacIlity

4STWALD LABORATORIES1 fl Lab. No. 88-01-18CHEMiL’c-iACTERIOLOGICAL ANALYSIS, .

1403-1405 W. FOURTH ST.WILLIAMSPORT, PA. 17701

PHONE 717-326-4001

SAMPLE IDENTIFICATION:Creosote DATE COLLECTED: 1/5/88

DATE RECEIVED: 1/5/88Koppers Inc. DATE REPORTED: 1/26/88PC Box 189Montgomery, Pa. 17752

ANALYSIS RESULTS

Arsenic < 0.0001 mg/g

Color Black

Odor Tar

Chromium mg/g 0.014

Copper 0.036

Zinc 0.207

B.T.U. Per Pound 12672

Boron 0.38 ppm

Michael Shifflet

• _..., ...,.. ,m. I JU IMvIflIJI’dIVIEPI IRL UUI1LtbBureauf’Waste Management

,r ). Box 2063}rrsburg. PA 17120

Please print or type. (Form designed for use on elite (12-pitch) typewriter.)Form Approved. 0MB No. 2000-0404. Expires 7-31-86ER-SWM-51 :REV. 10184


!)PPP’TE flTP’!Y, P!C., P.fl. ‘flX 19, flT(P4FPY, Pd’.17752—0 fl94. Generator’s Phone I 71 7 54 7—1651.


PAB 2715845B. State Gen. ID

PAT) 056723265

MsnifetUNIFORM HAZARDOUS I. Generator’s US EPA ID No. Document No. 2. Page 1 Information in the shaded areas

I is not required by Federal lawWASTE MANIFEST P ‘A’ T’ 0.5 6 7’ 2’ 3 ‘2 6 I 5 c o of-“‘ State law.

5. Transporter 1 Company Name 6. US EPA ID Number C. State Trane. ID‘ART TRTJCKThG Co.. WC. 10 i .O.o.0.’.86 ‘5..2.5 PA-AH 0 ‘2 ‘1.91

7. Transporter 2 Company Name 8. US EPA iD Number D. Transporter’s Phone (BOO) 23B—BS7I E. State Trans. ID9. Designated Facility Name and Site Address 10. US EPA ID Number PA-AH I1P’Vq C!PY, WC., P•’) • Tt’ 16(1

F. Transporter’s Phone IRTIAflA, ‘4 3R060

0. State Facility’s ID Not RequiredI 1 .3 J).Ø ‘O 7.02 ‘7• 5’4 3 H. Facility’s Phone 1 112. Containers 13. 14.11. US DOT Description (including Proper Shipping Name, Hazard Class, and ID Number) Total Unit Waite No.

No. Type Quantity iVtIVola.RQ—fl PAZAPflP PTCiCi’SS r,IASTN.fl.S. LW’TIP 0R—R TA 9118

(CONTATITS tYSET) CPEflSflT.) 70 D’N ‘ ‘2 “ ‘0 —

Gb.

EN

•. . . . . .E—R c.

—AT0

.• . . . . .

Rd. I , . , — —

—.1. Additional Descriptions for Materials Listed Above (Include physical state and hazard code) K. Handling Codes for Wastes Listed AboveHaz. Code Physical State Has. Code Physical State

a. U I I I c. U I I I a. Ic.b. U I I I d. U I I I b. d.


‘jnr, ,UrTG, rp PUIPtTFYT EQUTPMJWT STJT AS T?IPERVIOT!S GLflVPSANn ry’ t”n’rrCTTrv1

16. GENERATOR’S CERTiFiCATION: hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified,packed, marked and labeled, and ore in all respects in proper condition for transport by highway according to applicable international and national government regulations.Unless I am a small quantity generator who has been exempted by statute or regulation from the duty to make a waste minimization certification under Sect or, 3002 fb) of RCRA. I alsocertify that I have a program in place to reduce voIiim and tosicify of waste generated to the degree i have determined to be economically practicable and I have selected the method oftreatment, storage, or disposal currerrtty available to me which minimizes lie present and future threat to human health and the environmeril

Printed/Typed Name Signature Month Day YearTH0?’AS D. t.oAfl1AT

. - it a Ii I -a>

F\)

C),00

(-Ti

17. Transporter 1 Acknowledgement of Receipt of Materials, ,1 —Printed/Typed Name

Month Day Yeartienry 3. fletidtcI •5I.

iS T,.nnnre, A,,IvnnwI.dn.n..ne nf R.s.,Int nf 6r ,_4• f,,

TRANSP0

Printed/Typed Name Signature Month Day YearER

19. DIscrepancy Indication SpaceFAC

1 20. FacIlity Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.TV Printed/Typed Name Signature Month Day Year

fAi<’I E. N(EL[LLJUIJ) . ii(’(A((1(EPA Form 8700-22 (3-84)

7--COPY 4 - TSD Facility - Retained by TSD Facility

flOEWALD LABORATORIEflO Lab. No. Sr,P118CHEAL & BACTERIOLOGICAL ANALYSTSST. 1939

1403-1405 W. FOURTh ST.WILLIAMSPORT, PA. 17701

PHONE 717-326-4001

SAMPLE IDENTIFICATION:Creosote DATE COLLECTED: 1/5/88

DATE RECEIVED: 1/5/88Koppers Inc. DATE REPORTED: 1/26/88PC Box 189Montgomery, Pa. 17752

ANALYSIS RESULTS


Color Black

Odor Tar

Chromium mg/g 0.014

Copper 0.036

Zinc 0.207


Boron 0.38 ppm

Michael Shifflet

- — — —. . —.. . .. —. •1 I flP_ fl IOS.l SJfl t,Q

‘—95ureau of Waste Management

)P. 0. Box 2063

Harrisburg, PA 17120Please prinhur”type. (Form designed for use on elite (12-pitch) typewrite..


opper Co., The., r.’. fox 19, f*mtn1ery, Pm. 17752

4. Generator’s Phone I 717 ) 547—1651

Printed/Typed Name

7. D. LOAD!Ai?

20. FacIlity Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

Signature

it lfr4—1 t2’”iA’

ER-SWM-51:RE”. 6/87

Form approved.0MB No. 2050-0039ExpIres 9-30-88


PAR 5438370

B. State Gen. ID

PAD 056723265

Document No. 2. Page 1 Information in the shaded areasUNIFORM HAZARDOUS 1. Generator’s US EPA ID No. Manliest

I Is not required by Federal lawWASTE MANIFEST P . A. 7. f.. r 7 2 3 2. 6. 5 I 1 00 f). of I but Is reauired by State law.

5. Transporter 1 Company Name 6. US EPA ID Number C. State Trans. IDflart Truektn Co.,

— I 4 63•8.2.5 PA-AH I 02 l 9 I7. Transporter 2 Company Name 8. US EPA ID Number D. Transporter’s Phone ( BOO 218—.357._j E. State Trans. ID9. DesIgnated Facility Name and Site Address 10. US EPA ID Number PAAH J Itoppers Cr., Tne., P.O. Tri 1 60 F. Transporter’s Phone

Orenada, H 9M G. State FacIlity’s ID Not Required.S. D. 0.0. 7. C) 2 7. 5 H. FacNty’s Phone I I

12. ContaIners 13. 14.it. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) Total Unit Waste No.No. Type Quantity Nt/Vola RQ.-Nen fla rteus Process 7aete

N.0.S. Ltqutt! OR1-F PA 918. 9 1?(Centalns nsei 414 p•p —

Gb.—

EN

.. . . . . .E—R c.

—AT0 1 I I I

R d.—

-__— —J. Additional Descriptions for Materials Listed Above (Include physical state and hazard code) K. Handling Codes for Wastes Listed AboveHas. Code Physical State Haz. Code Physical State

a. I I I I I I Ic I I I I I I 5

b. I I I I I I d.1 I I I I I b. d.16. Special Flandiing Instructions and Additlonsi Information

flWP AWDL!PC, T’AR PRrrT’cTTVP E?UTP’WWT St’CH M IHPrRVI0US tLOVTArr PPOTrCT1o?

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignrrrerit are frilly arid accurately described above by proper shipping name and areclassified, packed, marked, and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulationsIf t am a large quantity generator. I cerrily that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economicallypracticable and that I have selected the practicable method ot treatment. storage, or disposal currently available to me which minimizes the present and future threat to human healthand the environment. OR, it I am a small quarrlrly generator. I have made a good faith effort to minimize my waste generation and select the best waste nranagemrnt method that isavailable to me arid that I can at lord.

Signature ,_/) ,

T 17. Transporter 1 Aclcnowiedgement of Receipt of MaterialsPrinted/Typed Name

Larry ATtender18. Transporter 2 Acknowledgement of ReceIpt of Materials

T Printed/Typed NameEH


Mont

Month Dat

Printed/Typed Name

EPA Form 8700-22 (Rev. 9-86) Previous editions are obsolete

Month Day Year

lie; Iiiki?

Copy 6 - TSD Facility: Retain This Copy

flEWALD LABORATORIESrL) Lab. No. 88-01-18CuE , BACTERIOLOGICAL ANALYSIS )1’I939

1403-1405 W. FOURTH ST.WII.LIAMSPORT, PA. 17701

PhONE 717-326-4001

SAMPLE IDENTIFICATION:Creosote DAlE COLLECTED: 1/5/88

DATE RECEIVED: 1/5/88Koppers Inc. DATE REPORTED: 1/26/88P0 Box 189Montgomery, Pa. 17752

ANALYSIS RESULTS


Color Black

Odor Tar

Chromium mg/g 0.014

Copper 0.036

Zinc 0.207


Boron 0.38 ppm

Michael Shiff1e’’

+

II WI

-

MOøR

SPEOISET 226 (

_______ ___________

_________________________EPArgrrna7*22LRa.g-aôID No. ManIfest 2 Page 1 lnfoimatloh hi ihê shaded areas Is fbi

No. requIred b Federsi law, but rdqulred

I of.L, . - r

I I P.O_,_ 70 .

I I &rbendai ,tllinøie 62901:1 I 4. raiortiône 618 4,7J,115 . ..

11 s. ‘ 6. 0mber

7 . 8. US EPA ID Number

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[1 dciresd 10 US EPA ID Number

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00O27 J1- WUS scrlflon (frkkdng ty€ Name, Hã Cfess, and ID Minber) 1.Gont

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15. SpecIal Hl1diing Instructions and Additronal Information

.. .

fl*bê 12a1$ and eye *ot.oU,w t. be imrn ithen handling 4ms

• 18. GENRAOR’S RèAflON: I hereby dre that the contents di th consignment are fully and accurately leseiibed above by

2 imper lpplng name and classified, paok4I, marked, and labeled, arid are In all respects in proper condition for transport by highwayaccofd)ti9 ló apptoable International and national government reuIattOns.

. If I api a Isrge quantity generator, I certify that I have a pmgPAm In pfae icr reduce the volume and toxicity of waste generated to the degree I have determIned to bd

edonàmioaliy preqiloeblé and that I have selected the practicable tt1hod of treatment, atorage, or dIsposal currently Available to me whlah mln$tnizes the present 8nd

..

future thraetthumèn health and the environmant OR, If I am d .tpall quantity gerleratck, I have made a ood faith effort to minimize fly waste generation arid aeleCt‘ the beat wastö nienagement method that is àvaI&le to me end tpat I can afford. I . Dale

.,

Snafu

T 17 ipansporter I Aoknowlktgemefit of Receipt of Matenalsi’

d/yedNarne . •* 8 ..

R18 Transporer2 Acknowledgement of Reclpt of Materlts bate

.-. I’rintsd/Typed Nahie .‘ . .. . Sigriatufe . ., V. Month Oy

, --. -

- IL LLL1 crep4Oy rndIóMltn spate q

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.‘V ‘ 20. iaoIiIty Owner or Operator: Certlrlcation of receipt of tovbred by this manIfeSt exàep as notd fri item 19. ..Date

“ V PrInted/Typednie . Signature Month ba’Vs

, . . 4 HOUR EMERG IbE IS: 800 / 44-86O2

2200 CHURCHILL ROAD, SPRINGFIELD, ILLINOIS 62794-9276 (217) 782-6761 1L532-0610

P.O. BOX LPC 62 8/81

(Form desiqned lot use on eliL. Jitc pewriler.) EPA Form 8700-22 (Rev. 9 m Apprnved. 0MB No. 2050-0039, Expires 9-30-88

4 UNIFORM HAZARDOUS 1. Generators U EPj No. Manifest 2. Page Information in the shaded areas is not

WASTE MANIFEST IL]) OOo81994o No.of

qu law, but is required

7. Transporter 2 Company Name 8. US EPA ID Number E.flhIois

i ) :!.. :porter:sPe

9. Desjnated Facilit. Name and Site Address 10. US EPA ID Number G.lllinois ... ‘.. toppers uompRny. Jfl0 FaciIitys’’’ ... .

Ti Plant ute 68 ID .1.

‘C•. 4. i

CrenMa, sisippi 319H FagçP - -

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12.Containers 13 14.Total Unit I

. No. Type Quantity vt,va. Waste No.G a . .

E RQ Non-Haaardot process waste liquid M)8N NA. 91738 (contain ed.p.iit*oh1orpi.nol) . 45631E . ‘

. I Ib.

,.

RI114

¶t.. —-

1J. cditot)al Oesqdptlons for Mate1lsListed Above ;‘ ... fl.niing (odes I’or Listed Abov. . . ., . . . Inltem#14

Contains spent (usad) p.ntaoloz’oimiol 1 = Gallons 2 = Cubic Yards

;1 ,.“r” .1 ,. .•‘,

1 . = lOibs.


Rubber gloves aM eye protection to be ,rn when handling drums. I 4

h’/9’Pi7’Sinure :;;;;

24 FIOU EMERG CY AND SPILL SI NCE NUMBERS (l iTIfl Iii ‘‘ 800 / 424-8802 or 202 I 426-2675)ISIR1BUTION: PART - 1 GENERATOR PART-2IEPA PART - 3FACIUTY PART - 4 ThANSPORTER PART -5IEPA PART - 6 GENERATOR

3. Generators Name and Mailing Address 0PP5X’ UOjIafly, .LflC.

P.OBex 70Carbondals, Illinois 62901

4. Generator’s Phone ( 618 )‘+57..14175

5.TraryNa 6. ber

A. llflncts

- .--. -B *‘1’eJ,i’

2C.lllinoisrlI I.

431:‘

D.( 1SpOrter’s Pfone

Pas ruiht or type.

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above byproper shlppinq name and are’dassif led, packed, marked, and labeled, and are in all respects In proper condition for transport by highwayaccording to applicable international and national gdvernment regulations.If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to beeconomibally practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present andfuture threat to human health and the environment; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and selectthe best waste management method that is available to me and that I can afford. Date

Month Ore’ YearPrinted/Typed NameClark J. Mitchell

Satuj,- 02 05

DateR

Month DaA Printed/Typed Name

T 17. Transporter 1 Acknowledgement of Receipt of Materials

2 0‘ ‘e

William A. Huckaby .-

, A /P

-Dateo 18. Transporter 2 Acknowledgement of Receipt of Materials

HT Printed/Typed Name Signature . Month Day YearE . IR .

. I— 19. Discrepancy Indication Space

F . ‘ IA -

C‘I r I ‘

..4 0. aility O* 6r Operator: Certification of receipt of hazardouatedals àve?ed y this manifet except as noted in item 19. Dtév Printed/Typed Name

)),,j’) ICN fli 217 / 782-3637

GENERATOR COPY — PART 1-DO IOT REMOVE PART 1 FROM SET UNTIL COMPLETED.m’s Merrcv is auttlarulyd to rtlqulre. rurs.rsrrt Is Illinois Rneisrrd Statutes. Chapter I I1” Serllnrr 21, hat this alternation be erberitled a the Asency. Polkas to pmvkte the Information onmy result in a cull penalty agaarrl the surera’ aprro’rr ci rut to ,mulaed 525.O’Y) re-I ‘Irry ri . dna’ Fnlslioatir,p nt thin iotormnatkrn mn.’ry r.,rnyt in a line op to $50000 per dry at vloL’Iios and IrrOmisor,rmmernt re to 5 pears Thi herr, rims born, ,rppraaed by he terra’ M’apermrorrtr,rnr•.r

. FACILITY COPY - PART 3

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4. Generator’s Phone ( 618)457_fl4a1ePI11iflOiC -_—_

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4

UNIFORM HAZARDOUS 1. Generator’s USPA lp)io. Maifest 2. Page 1 Information in the shaded areas snot

WASTE MANIFESTçJihnt No. 1 requwed by Federal law, but is required

5.TransP

ICqrnpanme 6 onn3ber CiHirt9 Ii

7. Transporter 2 Company Name —- 8. US EPA ID Number I.

. I Phone

9. Designated Facilijy Name and Sjt Address 10. US EPA ID Number s’’:Kbpprs LoMpny,Tie P1ant RDute Hr

I

Gren4dk, 3896 007027,03

11. US DOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12. Containers 13. 14. ‘

‘

. Total Unit /No. Type Quantity VtlVo -

G a.. — ElWNumber

E Rt flon-4lazardous prooeea ate liçuid )8 - L. I. I

N N A. g1 (coe.ina used pente.oh1oroz.ne1) .,w,

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. 1 = Gallons 2 = Cubic Yards1 *k sp.nt (iaed) pen iloz.phenol.

,;,,, 1 s3.. — 1 lbs.


- Rt$,.r cloves and eye px’oteotion to be iezn iehen harIing drums

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above byproper shipping name and are ilaSsif led, packed, mked and labeled, arid are In all mspects in proper condition for transport by highwayaccording to applicable international and national government regulations.

if I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to beeconomically fractlcable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present andfuture threat to human health and the environment; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and selectthe best waste management method that is available to me and that I can afford. I Date

- Pnnted/Typed Name Signature,lrhOD?j

Yer

T 17. Transporter 1 Acknowledgement of Receipt of Materials Date

Printed/Typed Name Signa re Month Day Year)onnie aoffey .; r’.s’j/ 0’, 0 8 8 8

o 18. Transporter 2 Acknowledgement 91 Receipt of Materials Date

r Printed/Typed Name , / Signature Month Day Year

19. Discrepancy Indication Spae

I l I f /

20. Facility dwnr or Operatth: Certification of receipt of hazardous materials ddvered by this manifest except as noted in item i. Date

H ,1Si9tur.1.

Month Day Year

03 O’01 ITIflF II I 1NOIS’ ROfl / 424-RRn2 nr 202 I 42A-2R7C

DISTRIBUTION. PART - 1 GENERATOR PART- 2 IEPA PART- 3 FACII,ITY PART -4 TRANSPORTER PART - 5 IEPA PARr -6 GENERATOR

aSa print tsr type.

2200 CHURCHILL ROAD, SPRINGFIELD, ILLINOIS 62794-9276 (217) 782.e761 1L532-05iO

P.O. BOX LPC628/8I

(Form designed for use on eL typewriter.) EPA Form 8700.22 (Rev. 9 ,f’- -. Form Approved. 0MB No. 2050-0039, Expires 9-3088

iN III ItbifliS 917 I 7R9-RTf7

Printed/Typed Name

GAIZY E. /VfrCLLLLAWP*24 HOUR EMERGENCY AND SPILL ASSlSTANNUMBE

GENERATOR copy — PART 1-DO NOT REMOVE PART 1 FROM SET UNTIL COMPLETED.rys Aycncy is aulhorin,,d to requim mIr ani to Ilijonig Relsrd Strtten Chote, Iii’, S,--tion 2!, thni ihs inin,moijo, be nubmilied to the Agency. Faliure to innuide he information nay mviii is a civil peuliy aqa,u5i the owneror epentor d nat to ascend $2P.00) r”r dny of volotnu Fafrjo,.iivrr cit ibis lriftrmaten”cy n,rit in a inn up in $5OjX)O pnr dcv 0! vioiaiion arid impiisonrneni up in 5 years This form iris born apinvumi b its tarn bf,rn,nt mciC.,niei FACILITY COPY - PART 3

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P.O. BOX LPC 62 8/81

int “pe. (Fbrm desned for use on eIypewriter.) EPA Form 8700-22 (Rev. QrmApped. 0MB No. 2050-39, Exms 9-30-88

Manifest 2. Page 1 I Information In the shaded areas is notE NIFORM HAZARDOUS 1 Generator’sU1S9E9No.No.

of 1 I by Illinois law.I required by Federal law, but is required

, WASTE MANIFEST 0008

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nerator’s Name and Mailing Address- Co1rs Cosii, i

• A. Illinois ManifestI1it4

P 0 Box IL

4 Generators Phorie( 618 L!+57’’°’U. 629o1 — BIUina1

015. Transporter 1 Company Name 6. US EP er C. Illinois_T n rs ID

.

Dert Txcking Co., Inc. OHD D( QO7. Transporter 2 Company Name 8. US EPt ID Number E.IlIinoIs I ‘S ID i

I fr.. -

....n,. 7fançrt Phone9. Deignated_Fad ity Name and ‘te Add rest 10 US EPA ID Number

EopperoJRPI32y,fle ,

T1.• Plant ibute 68 H F -

I .4% I 1..,...L

aEe!da, esiseipp& 389O .— ‘o .

11. US qOT Description (Including Proper Shipping Name, Hazard Class, and ID Number) 12.Containers 13. 14.Total Unit

No. Type Quantity Vt/Vo Waste No.

a. zardom process iist liquid *)S -

-

L A 9188 (cotaine uftd pectlozien,l)I

8, j .-I

b. won-bu*reus eoe.s imete Iv(or*ote Sludge) . c / i

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“-I’.’. d & 3 3O ) - i, ,. !. / l’

for Materials Listed Above‘

‘ -3 4idflri xles1 Listed Above

(*fltetfls spnt (iad) flt&h1OrO1*L.flD1 .

.. 1 = Gallons 2 = Cubic Yards.‘.“Lf i pj%

.,.,ii, I .r; ‘I ‘‘ ‘ ‘ 1. i. *..1 lbs. I


Rubber glovee and eye proteon to be ithen handling drum

16. GENERATOR’S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above byproper shippIng name and are classified, patkOd, marked and labeled, and are In all respects in proper condition for transport by highwayaccording to applicable international and national government regulations.If I am a ,large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to beéconomially practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present andfuture threat to human health and the environment; OR, if I am a small quantity generator, I have made a good faith effort to minimize my waste generation and selectthe best waste management method that is available to me and that I can afford. I DatePrinted/Typed Name Signature - .- Month Day Year

- ,ld Mier ,..

.

158T 1 7i Transporter 1 Acknowledgement of Receipt of Materials ri Date

Printed/Typed Name Sigrtst. I Month Day Year

Jo•Renfro . ‘‘ o4’1588O 18 Transporter 2 Acknowledgement of Receipt of Materials Date

T Printed/Typed Name Signature . Month Day Year

H ,.

— 19. Discrepancy Indication Space

F .

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20. Pacility Oner àr Operator: ter1ification of rebeipt of hazardous materialS cove,:ed , this manifest except as noted in item 19. Date

y Signatu

- .. . , , a “ . ‘/NYAf/4 .,I°24 HOUR EMERGENCY AND SPILL ASSlSTCE NUMBERS*

DISTRIBUTION: PART - 1 GENERATOR PART-2 IEPA -- PART - 3 FACILITY PART -4 TRANSPORTER PART -5 IEPA PART - 6 GENERATOR

L._

IN it INO1S’ 217 / 7M2-H7

Printed/Typed Name

g,?Y t.. IIICcLJiLLANL’

REV 7 GENERATOR COPY — PART 1-DO NOT REMOVE PART 1 FROM SET UN’flL COMPLETED.The Agency is euih,,rtzed to reqr,lre, urc,,or,i to Illinois flr,vinnd Stray,,,. Chapter 111/’ Srxtior, 21. that hi,, tr,tormation be subnritted to the Agency. Failure to pioakki the i,’torrn,-,fion may result in a clot penally ,gyri,,Ot hal owneror operator of not in ,,nnemt $25,000 pr, F,y of vielstirn FOlriflcaih.n ci lii,, ir,lor,natlon may in,r,lt In finn up to $50,000 per d’y of vlolntior, nnd i,np,Ir,onment up to 5 tory,,, Thin lerni Iron been opprnued by flu, Fe,n,s ManaqemOrrtCenter. FACILITY COPY - PART 3

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MISSl(Pl DEPARTMENT OF NATURAL RRCESBureau f IollUtion ControlP. 0. Box 10385Jackson. Mississippi 39209(601) 961-5171

November 10, 1988

CERTIFIED MAIL NO. P 962 284 477Mr. J. R. BatchelderVice President & ManagerTechnical & Environmental ServicesKoppers Company, Inc.436 Seventh AvenuePittsburg, Pennsylvania 15219

Dear Mr. Batchelder:

In order to settle certain environmental issues regarding KoppersInc., Tie Plant, Mississippi, you have agreed to the conditions oftive Order No. 1478-88, which is enclosed.

Company,Administra—

If you have questions about this matter, please contact Mr. Steve Spengler

at telephone #601/961—5171.

CHC :mh

Since1rely, 7)2c’ —

Charles H. ChisoimBureau Director

Enclosure

D CBEFORE THE MISSISSIPPI CISSIONON NATURAL RESOUDESBUREAU OF POLLUTION NTRDLJAcKsoN, MISSISSIPPIUN’I”f OF HINDS

IN THE MAITER OF:

MISSISSIPPI CCI4’4ISSION ONNATURAL RESOUI2ES

vs. 1478 88Koppers Ccznpany, Inc.MSD 007027543

RESPONDENT

AcREED ORDER

CCS NC THE Mississippi Conrnission on Natural Resources,Conplainarit, and Koppers Canpany, Inc., Respondent, in the abovereferenced administrative action arid would shew forth as follows:

1. On October 7, 1988, Respondent was contacted by Couplainantand notified of Caiplainant ‘ s intent to cite Respondent for a certainviolation and/or violations of requiretnts set forth in MississippiHazardous Waste Managatnt Regulations (MH’iR) Part 262 and Part 265,a copy of which is attached hereto and incorporated herein byreference; said violations being as follows:

a. Respondent did not construct and maintain a stonn waterrun-on/run-off managient systn or provide nans to control the winddispersal of hazardous waste ash which had been landfilled at its“boiler ash landfarm” as required by MH4R 265.302.

b. Respondent failed to provide adequate security at the“boiler ash landfarxn” in that the gate to the unit did not have a lockon it as required by MHIiNR 265.14.

c. Respondent stored at its designated less than ninety (90)day hazardous waste container/drum storage building six (6) drums ofthe listed hazardous waste U051 which did not have acciirn.ilation datesaffixed to then as required by MH4R 262.34.

D Cd. Respondent stored at its less than ninety (90) day

container/drum storage building six (6) drums of the listed hazardouswaste U051 for longer than ninety (90) days in violation of HW”IR262.34.

and,

2. Respondent suheitted a letter to Cauplainant, dated

September 22, 1988, which outlined actions that have been taken to

bring the facility into compliance with respect to the violations

cited in items a., b., and c. of paragraph 1.

and,

3. Complainant and Respondent do hereby agree, in lieu of a

filing of complaint by Caiplainant, to enter into this ?greed

, ( Order wherein Respondent agrees to pay and Complainant agrees to

accept, the sum of $6,000.00 as a full and canplete settlexrnt

thereof, said sum to be paid in its entirety on or beforeif

November 30, 1988.

and,

4. Respondent further understands and agrees that, as part

of the alxve referenced settlennt, Respondent shall properly manage

its less than ninety (90) day hazardous waste container/drum storage

building in accordance with the requirennts of MH4R 262.34 and

otherwise comply with the requirnts set forth in I1HR Part 262 and

Part 265.

5. Respondent understands and agrees that it is fully

entitled to an evidentiary hearing pursuant to Sections 49—17-3 1

and 49-17-41 of the Mississippi Code nnotated, and that it

agrees to the alove referenced settlennt only after having been

fully infornd of its right to said hearing; and

00

6. Respondent understands and agrees that this settlennt

agreeitent in no way is an admission of liability on its part,and is entered into for the sole purse of causing a swift

resolution of this administrative matter.

SO ORDERED, this the 9 day of 77&_(_...4.L , 1988.

MISSISSIPPI CCISSIONSESES

BY:

____

( r’• I1’IER, nt’( J‘%..xTYrIvE DIREU.tO1.J

ALREED to this the 7th day of November, 1988.

RS4?

Vice President & ManagerTechnical & Environmental Services

MISSl(ThPI DEPARTMENT OF NATURAL R URCESBureau of Pollution Control \

P. 0. Box 10385Jackson, Mississippi 39209

(601) 961-5171

November 10, 1988

CERTIFIED MAIL NO. P 962 284 477

Mr. J. R. BatchelderVice President & ManagerTechnical & Environmental ServicesKoppers Company, Inc.436 Seventh AvenuePittsburg, Pennsylvania 15219

Dear Mr. Batchelder:

In order to settle certain environmental issues regarding Koppers Company,Inc., Tie Plant, Mississippi, you have agreed to the conditions of Administrative Order No. 1478—88, which is enclosed.

If you have questions about this matter, please contact Mr. Steve Spenglerat telephone #601/961—5171.

Since,rly, 7)

ij/CCharles H. ChisoimBureau Director

CHC:mh

Enclosure

o 0BEFORE TRE MISSISSIPPI CXM1ISSIC

sssBUI€.U OF POLLtYrION (DNTLJ?CKS, MISSISSIPPIQDUNT OF HINDS

IN •!1 TER OF:

MISSISSIPPI iiissiai cRESS

iirr

1478 88 1Koppers Canpany, Inc.MSD 007027543

RESND

AGRD ORD

ca€s TI Mississippi Catznission on Natural Resources,

Ccnplainar)t, and Kcppers Ccuçany, Inc., Respondent, in the aheve

referenced administrative action and would slx,w forth as follows:

1. October 7, 1988, Respondent was contacted by Canplainant

and notified of Caxplainant ‘ s intent to cite Respondent for a certain

violation and/or violations of requirtEnts set forth in Mississippi

Hazardous Waste Manageent Regulations (MHIR) Part 262 and Part 265,

a copy of which is attached hereto and incorporated herein by

reference; said violations being as follows:

a. Respondent did not construct and maintain a stoma waterrun-on/run-off managetent systen or provide neans to control the winddispersal of hazardous waste ash which had been landfiiled at its“heiler ash landfa.rin” as required by MHI4R 265.302.

b. Respondent failed to provide adequate security at the“toiler ash landfam” in that the gate to the unit did not have a lockon it as required by MH 265.14.

c. Respondent stored at its designated less than ninety (90)day hazardous waste container/drum storage heilding six (6) drums ofthe listed hazardous waste L51 which did not have acc.sm.iJ.ation datesaffixed to then as required by iR 262.34.

0d. Respondent stored at its less than niriet (90) day

container/drian storage building six (6) drums of the listed hazardotiswaste U051 for longer than ninety (90) days in violation of MHPR262.34.

and,

2. Respondent subnitted a letter to Canplainant, dated

Septecber 22, 1988, which outlined actions that have been taken to

bring the facility into ccEnpliance with respect to the violations

cited in itens a., b., and c. of paragrapi 1.

and,

3. Caxplainant and Respondent do hereby agree, in lieu of a

fonxJ. filing of catplaint by Cat1ainant, to enter into this Pqreed

Order wherein Respdent agrees to pay and Caiplainant agrees to

accept, the sn of $6,000.00 as a full and carplete settlIEnt

thereof, said sun to be paid in its entirety on or before

Novtter 30, 1988.

and,


of the above referenced settlennt, Respondent shall properly manage

its less than ninety (90) day hazardces waste caitainer/drtan storage

building in accordance with the requirtents of MHI4R 262.34 and

othexwise catply with the requirnts set forth in I!R Part 262 and

Part 265.

5. Respondent understands and agrees that it is fully

entitled to an evidentiary hearing pursuant to Sections 49-17-3 1

and 49—17—41 of the Mississippi Code annotated, and that it

agrees to the above referenced settlenent only after having been

fully inforxred of its right to said hearing; and

0 66. Respondent understands and agrees that this sett1nt

agreertEnt in no way is an adsission of liability ci its part,

and is entered into for tt sole purpose of causing a swift

resolution of this aôninistrative matter.

SO OrEB, this the 9 day of, 1988.

ssissipi caiassIcAL RES

BY:____( JfL PMR, JRI\....ExtYrIVE DIL

to this the 7th day of November , 1988.

Vice President & ManagerTechnical & Environmental Services

0

BEFORE THE MISSISSIPPI C4ISSIONCN NATURAL RESOU1DESBUREAU OF POLLUTION CONTPOLJACKSON, MISSISSIPPICOUNTf OF HINDS

IN ThE MATI’ER OF:

MISSISSIPPI CCM’4ISSION Ct4NATURAL RESOUICES

ccir

1478 88 1Koppers Canpany, Inc.MSD 007027543

RESPONDET

A ORDER

CCLVIES NCW THE Mississippi Catrnission on Natural Resources,

Canplainant, and Koppers Company, Inc., Respondent, in tbe above

referenced administrative action and would skw forth as follows:

1. On October 7, 1988, Respondent was contacted by Canplainant

and notified of Canplainant’ s intent to cite Respondent for a certain

violation and/or violations of requirnts set forth in Mississippi

Hazardous Waste Managnt Regulations (MHWMR) Part 262 and Part. 265,

...C ...L.. . — ...._J_...1....... .. ••••

0

d. Respondent stored at its less than ninety (90) day

container/ck’in storage building six (6) drums of the listed hazardous

waste U051 for longer than ninety (90) days in violation of MHtNF.

262.34.

and,

2. Respondent sunitted a letter to Cauplainant, dated

September 22, 1988, which outlined actions that have been taken to

bring the facility into compliance with respect to the violations

cited in items a., b., and c. of paragraph 1.

and,

3. Complainant and Respondent do hereby agree, in lieu of a

formal filing of complaint by Canp].ainant, to enter into this .greed

Order wherein Respondent agrees to pay and Complainant agrees to

accept, the sum of $6,000.00 as a full and carlete settlerrnt

thereof, said sum to be paid in its entirety on or before

November 30, 1988.

and,


CD0

6. Respondent understands and agrees that this settlrent

agreerrnt in no way is an admission of liability on its part,

and is entered into for the sole purpose of causing a swift

resolution of this administrative matter.

SO ORDERED, this the 9 day of

_________________,

1988.

MISSISSIPPI CC’1ISSIONNflJRAL RESOUIES

BY:

____

( J41. P2IZ€R, JR?\...EcurIvE DIPECIC

AGREED to this the 7th day of November, 1988.

2 2 — — i. a S * — — — — — —

•22

IX. APPENDIX

PENALTY COQUTATION WORKSHEET

Company Name: Koppers, Grenada, MS

Regulation Violated 268.7

Aaesaments for each violation should be determinedon separate worksheets and totalled.

(If more space is needed attach separate sheet.)

Part I - Seriousness of Violation Penalty

1 • Potential for Harm: Moderate

2. Extent of Deviation: Major

z3. Matrix Cell Range: 8,000—10,999

Penalty Amount Chosen: 10,999

Justification for PenaltyAmount Chosen: Upper Point

4. Per-Day Assessment: NA

Part II Penalty Adjustments

Percentage Change* Dollar Amount

1. Good faith effortsto comply/lack ofgood faith: NA

_____

2. Degre. of willfulnessand/or iegligenc.: NA

_____

3. Hiiery of*.pUsi.: NA

______

4. t qse. f-t.ax.s: NA5:Tftcan for

‘Mageaments are applied to the dollarantziLLaed on line 4. Part I.

___________

- 23 •

PENALTY COMPUTATION WORKSHEET (cant.)

6. Adjusted Per-dayPenalty (Line 4,Part I + Line.1—4, Part II) : $10,999

7. Number of Day. ofViolation:

________

8. Multi-day Penalty(Number of days xLine 6, Part II):

________

9. Economic !enef it ofNoncompliance: 19,575

Justification: *See Attached

10. Total (Line. $ + 9, Part II): 30.574

11. Ability to Pay Adjustment:

Justification forAdjustment:

_________

12. Total Penalty Amount(must not exceed $25,000

30 5per day of violation):‘

‘

‘3

0 0Koppers

Grenada, MississippiPenalty Calculations

MHWMR 268.7 - Ash generated land disposed without analysis.Potential for harm — Major — Since prior wastes of the sametype were incinerated in the boiler and. disposed of ashazardous waste, and since the material received from offsite contained 1(001 characteristic hazardous waste, thepossibility exists for contamination of the landfill usedfor disposal. Extent of deviation — Major — regulations andpast history at facility should have dictated analysis ofwaste.

Economic Benefit Calculations

Disposal Costs @ 800.00/Ton x 38.6 Tons = $30,880.00Disposal Costs @ 125.00/Ton x 41.1 Tons 5,138.00

$36,018.00

Loading Costs 325.00

$36,343.00 =

Avoided Costs

36,343 x 0.54 = $19,625 Economic Benefit

Comment: Negotiations with the facility resulted in asettlement of 50% of the calculated non—economic benefitpenalty for a total of $25,075.

p1

0

.22.

IX. APPENDIX

PENALTY COQUtATION WORKSHEET

NA

NA

25%

NA

— 1987 — See Comments

0


Regulation Violated MHWMR 262.12(c)

Asessments for each violation should be determinedon separate worksheets and totalled.

(If more space is needed, attach separate sheet.)

Part I Seriousness of Violation Penalty

I • Potential for Harm: Moderate

2. Extent of Deviation: Ma-br

3. Matrix Ce].] Range: 8,000—10,999

Penalty Amount Chosen: $10,999

Justification for PenaltyAmount Chosen:


Part II - Penalty Adjustments

Percenta. Change* Dollar Amount

1.. Good faith effortsto comply/lack ofgood

faith:

______________________

2. Degree of willfulnessand/or egliience:

____________________

3. Hilliry of

4. qe C3j:

5. Ti apn for

- *ebMage 4jments are applied to the dollaron line 4. Part I.

$2,750

—-.

•23

PENALTY COMPUTATION WORXSREET (cont.)

6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1-4, Part II): $13,749

7. Nber of Day. ofViolation: NA

8. Multi-day Penalty(Number of day. xLine 6, Part II): NA

9. Economic Senef it ofNoncompliance:

________

Justification:

10. Total (Lines S + 9, Part II): $13,749


Justification forAdjustment: NA

12. Total Penalty Amount(must not exceed $25,000per day of violation): $13,749

0 0Koppers

Violations - PenaltyCalculations

l.A. MHWMR 262.12(c) - Receipt of hazardous wasteincorrectly classified and burned in facility boilers.Ash generated was not treated as a hazardous waste andwas sent to a municipal landfill facility (Grenada Co.Landfill without proper I.D. No.)

B. Seriousness: failure to trea.t boiler ash material ashazardous waste: Potential for harm — Moderate —

Hazardous waste ash generated was dumped in a landfillnot permitted to handle hazardous waste. The violationcould have serious impact on human health and theenvironment. Extent of deviation — Major — substantialnoncompliance from the regulations are noted sinceneither incoming waste nor ash waste generated fromburning were treated as hazardous waste. History ofnoncompliance — In 1987, similar material was burned inboilers; this ash became the basis for the boiler ashlandfarm RCRA unit.

Comment: Negotiated settlement resulted in a revisedpenalty of 50% of calculated amount or $6,875.

• 22 —

IX. APPENDIX

PENALTY COMPUTATION WORKSHEET

1. Good faith effort.to comply/lack ofgood faith:

2. Degre. of willfi.iln..sand/or .glig.nc.:

3. Hiiêry of

4. trqce.fc.as:

5. -iatn for


Regulation Violated Permit Condition IV.C.3.

Asessm.nta for each violation should be determinedon separat. worksheets and totalled.

(If mer. space is need.d, attach separat. sheet.)

Part I • Seriousness of Violation Penalty

1. Potential for Harm: Minor

2. Extent of Deviation:

_____________

3. Matrix Cell Range: 1500—2999

Penalty Amount Chosen:

_____________

Justification for PenaltyAmount Chosen: Lower Point



Mi or

$2,250

g


NA

NA

NA

NA

“-.—

—-.

an, applied to the dollarantaázlL&ied on line 4. Part I.

23

PENALTY COMPUTATION WORKSHEET (cont.)

6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1-4, Part II): $2,250

7. Number of Days ofViolation: NA

8. Multi-day Penalty(Number of days zLine 6, Part II): NA

9. Economic Benefit ofNoncompliance: 480

Justification:

10. Total (Lines 8 + 9, Part II): $2,730

1].. Ability to Pay Adjustment:


________


0 0Icoppers

Grenada, MississippiPenalty Calculation

Permit Condition IV.C.3. — Well R-l, improperly constructed,to be replaced with new well. Potential for harm — Minor —well is upgradient and used in determining statisticalanalysis. Extent of deviation — Major - Permit explicitlyrequired reconstruction within 30 days of effective date ofpermit.

Economic Benefit:

Delayed Costs: Cost of Well (COW)Cost of Plugging R—l = 4,000

Avoided Cost = 0IRS Interest Rate 0.12Assume T = 0.46

Economic Benefit = Avoided Cost (l-T) + Delayed Cost x 0.12= 0 + (4000)(0.12) = 480.00

Comment: Negotiations with the facility led to a settlementof 50% of the calculated non—economic benefitpenalty plus the economic benefit penalty for atotal of $1,605.

IX. APPENDIX


Company Name: Koppers, Grenada, •MS

Regulation Violated MHWMR 262.34



Part I Seriousness of Violation Penalty



3. Matrix Cell Range:



4. Per-Day Assessment:


Ma I or

SL500 — 2ggg

2,250

Midpoint

NA

C- 22 —

Percentea,. Chang.* Dollar Amount

1. Good faith effortsto comply/lack ofgood faith:

2. Degree of willfulnessand/or zeglig.nce:

3. Hiiiry of

4. erqce

5. atpn for

NA

NA

MA

NA NA

— -1

*jtageajents are applied to the dollaron lin.4. Part I.

- 23 -


6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1—4, Part II): $2,250


8. Multi-day Penalty(Number of days xLine 6, Part II): NA

9. Economic 3enef it ofNoncompliance: NA

Justification:




12. Total Penalty Amount(muse not exceed $25,000per day of violation): $2,250

0 0Koppers


MHWMR 262.34 - Facility stored six drums of tJO5l hazardouswaste at less than 90 day container storage area for greaterthan 90 days. Potential for harm — Minor — since materialwas in approved containers and labeled as hazardous waste,potential for release and endangerment to environment orhuman health, is minor. Extent of deviation — Major —

apparently the 90 day storage limit had been violated sincesome drums had been in storage for over a year. All drumsapparently met labeling regulations.

Comment: Negotiations with the facility led to a settlementof 50% of the calculated valve or $1,125.00.

•0

-22-

IX. APPENDIX

PENALTY COtQUTATION WORKSHEET




(If more space is needed, attach separat. sheet.)

Part I Seriousness of Violation Penalti


2. Extent of Deviation: Minor

3. Matrix Cell Range: 100-499

Penalty Amount Chosen: $250.00

Justification for PenaltyAmount Chosen: Midpoint


Part II - Penalty Adjust.nts

Percentage Change* Dollar Amourt

1. Good faith effortsto comply/lack ofgood faith: NA -—

2. Degree of willfulnessand/or .gligence: NA —NA

3. Hiitery of25%

_____

4. t’lir .faa,s: NA5:

forhrems:

— -7

Ihag.dadJents are applied to the dollar3-& ed on line 4 Part I.

-23 -

PENALTY COMPUTATION WORXSHEET (cant,)

6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1—4 Part II): 313



9. Economic !enef it ofNoncompliance: NA

Justification:

10. Total (Lines 8 + 9, Part II): 313



12. Total Penalty Amount(must not exceed $25,000per day of violation): 313

‘0

0 0Koppers


MHWMR 265.302 — Facility has failed to provide adequaterun—on/run--off and wind dispersal control systems.Potential for harm — Minor — holes in the cover as well asdirt placed on top of the pile provides an opportunity forexposure of contaminants to humans and animals. Extent ofdeviation — Minor — film mostly intact and run—on/run—offsystem in need of minor repair. Historical violation formaintaining adequate wind dispersal control noted.

Comment: Negotiations with the facility led to a settlementof 50% of the calculated total or $157.00.

.22—

LX. APPENDIX



2. Degree of willfulnessand/or negligence:

3. Hiitery of

4.5:

for

0 0

Company Name: Koppers, Grenada, MS -





1. Potential for Harm: Major

2. Extent of Deviation: Moderate

3. Matrix Cell Range: $15,000- $19,999

Penalty Amount Chosen: $15,000

Justification for PenaltyAmount Chosen: Lowpoint


Part II - Penalty Adjustment.

a

Percentaae Chan5e* Dollar Amount

NA

NA

NA

NA

..-.--

—-.

*

*utMageda4jment5 are applied to the dollarilw3&ed on line 4, Part I.

-23.


6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1—4, Part II): $15,000



9. Economic 5.nef it ofNoncompliance: NA

Justification:





e

0 0i: opperS


MHWMR 265.93 - Facility has failed to perform requiredstatistical analysis at the surface impoundment and hasfailed to notify the Director of the existence ofgroundwater contamination. Also facility has failed tonotify Director of the existence of groundwatercontamination at the boiler ash landfarm. Potential forharm — Major — Since a plan of corrective action cannot beimplemented until assessment of the extent of contamination,and since contaminants continue to migrate pendingassessment, and since migration may cause harm to theenvironment and human health, the potential for harm isconsidered Major. Extent of deviation — Moderate — violatorsubmitted reports on groundwater monitoring in a timelymanner — many other requirements met. Deviation from theregulations were moderately disregarded.

Comment: Negotiations with the facility resulted in asettlement of 50% of the calculated amount or$7 , 500.

-‘7

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,

-22—

IX. APPENDIX


Company Name: C ,;

Regulation Violated Jñ’ tsAsessments for each violation should be determinedon separate worksheets and totalled.

(If more space is needed, attach separate sheet.)Part I - Seriousness of Violation Penalty

1. Potential for Harm:

2. Extent of Deviation: 2fl1ji3. Matrix Cell Range: ?SOp gq


___________________

Justification for PenaltyAmount Chosen: 1


__________________


Percentage Change* Dollar Amount1. Good faith efforts

to comply/lack ofgood faith:

_____


3. History ofnoncompliance:

/4. Other unique factors: I

_____

5. Justification forAdjustments:

* Percentage adjustments are applied to the dollaramount calculated on line 4, Part I.

- -

6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1-4, Part II):

7. Number of Days ofViolation:


9. Economic Benefit ofNoncompliance:

Justification:

10. Total (Lines 8 + 9, Part II):11. Ability to Pay Adjustment:


12. Total Penalty Amount(must not exceed $25,000per day of violation):

0 cc— 23 —

PENALTY COMPUTATION WORICSREET (cant.)

15

/

1

/V/1J

.

•fty.- (-1OJ0

_JJ--

r

- 22 —

IX. APPENDIX





4. Other unique factor.:


* Percentage adjustments are applied to the dollaramount calculated on line 4. Part I.

Company’ Name:

Regulation Violated 22L /Asessinents for each violation should be determinedon separate worksheets and totalled.



_______

2. Extent of Deviation: JY i’


__________________


___________________



_____

Part It - Penalty Adjustment.

dT/52999V

zzo o

e

m


6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1-4, Part U):




Justification:

1.0. Total (Lines 8 + 9 Part II):

II. Ability to Pay Adjustment:


12. Total Penalty Amount(must not exceed $25 .000per day of violation):

o 00

—23-


IL )I

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A/

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r

- 22 —

IX. APPENDIX


Company Name:it-/I 7J-. 2

Regulation Violated riu,i; 2




_____






______


PercentaRe Change*

o_f/9

1ooo

* Percentage adjustments are applied to the dollar- arnount calculated on line 4, Part I.

Y

Dollar Amount1. Good faith efforts

to comply/lack ofgood faith:

2. Degre. of willfulnessand/or negligence:


4. Other unique factors:


/

/

00. 0Q

—23—


6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1—4, Part II):




Justification:

10. Total (Lines 8 + 9, Part II):




/

//

i/

I Ha

.b

-22—

IX. APPENDIX







oc

* Percentage adjustments are applied to the dollaramount calculated on line 4,, Part I.

Company Name: 2cc.9ts ; _1j .-I

Regulation Violated :





_____


___________________


___________________


___________________



_____


1)1

/Z?:5c


00

- 23 -

0Q

PENAI,TY COMPUTATION WORKSHEET (cont.)

6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1—4, Part II):




Justification:





Z5O.

_vI

I’ I /v / II?

1

/u//I

/i/?

n’?J

a

/2oJ


__________




_________


* Percentage adjustments are applied to the dollaramount calculated on line 4. Part I.

(J-)

qoJ fl\i / I—

4)

—22— .?Li •#) l

I

/>; /—

IX. APPENDIX

PENALTY COMPUTATION WORKSHEET -/C

Company Name: ))5

Regulation Violated 222Asesements for each violation should be determinedon separate worksheets and totalled.



____________________


___________________

3. Matrix Ccl]. Range:

__________________


___________________



_________________


/r

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.e

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-23-


6. Adjusted Per-dayPenalty (Line 4,Part I + Lines1-4, Part II):

___


________


_______


________

I,

Justification:


________



_________

/

12. Total Penalty Amount(must not exceed $25,000per day of violation);

________

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Date: :z

DRAFT- RCRA LAND RESTRICTIONTREATNIT, STORAGE, AND DISPOSAL RRQUIRENEN’rs dHEcKLIs’r

I. FACILITY IDENTIFICATION

1). _ cTht !‘ !B. Street (or other identifier)

B. General Facility Standards

1. General

a. Does the facility conduct waste analysis (total andTCLP) on-site or through_a commercial laboratory?J#b. Describe the frequency of sampling conducted by thefacility.

- 7q4 1— 4JA c ç2/t f4, c_,

—

/7

/e

2. Treatment Facilities

a. Has the tr.et.ent facility revised its wasteanalysis plIEi (1268.7(b)J to meet the requirementsof S264.13 or S265.13? . _Yes No*

(i) Is the treatment facility conducting TCLPtests for wastes specified in Appendix A(i.e., those prohibited wastes subject totreatment standards expressed as wasteextracts) per 286.7(b)(i)? _Yes No*

A. Facility NameN-- )‘:.

C. City D. State E. Zip Coe F. County NameI C- —i—- •/LL1 \ J ‘ I -/rf ‘- i 4G. Nature of business;Didentificatioñ o industri and waste management operations;relevant SIC codes

1fl5U o7t Z 75yH. EPA ID *

J 0-, 2 çgI. Facility Contact (‘Name and P one Number)

II.A. For onsite facilities, complete the generator checklist Coimen ts

* A potential violation is indicatedTSDF-l

Inspector: ) Q

_______

—

Conen ts

(ii) Is th.. treatment facility using the paintfilter test for the California waste residues(S268.7(b)(ii)1? _Yes No

(iii) Is the treatment facility testing the pH ofCalifornia waste residues? Yes _No

(iv) Is the treatment facility testing concentrations (not extracts) in the waste residuesfor prohibited wastes with established treatment standards expressed as wasteconcentrations 1S268.7(b)(3)j? Yes _No*

(v) Is the treatment facility testing extracts ofthe waste residues for prohibited wasteshaving established treatment standardsexpressed as extract concentrations(S268.7(b)(l)j _Yes _No*

3. Land Disposal Facilities

a. Has the facility retained all notices and certifications from generators, storage and treatment /facilities L268.7(c)(l)I? Yes No*

b. Are wastes and waste residues tested for compliancewith applicable treatment standards and /prohibitions (S268.7(c)(2)I? _.Xes VN0*

c Are they being tested in conformance with thefrequency specified in the waste analysis planL S268. 7(c)(3) I _jYes _No*

d. Are the appropriate tests (TCLP vs. total waste)being used 1S268.7(c)(2)I? _Yes jo*

C. Storage (S268.50)

1. a. Are restricted wastes exceeding treatment standardsstored (excepting wastee subject to no migrationexemptions, nationwide variances, case by caseextensions, soft-hammered vaste.)? /

fr’Yes No

If no, go to “c.”

.b. Are all containers clearly marked to identifycontent and date(s) entering storage

,-LS268.50(a)(2)I? Yes L/No*

* A potential violation is indicatedTSDF-2

J.u Numoer:Inn9-r: ,ç,.jJ

/2

Co..en tsc. Do operatinregords track the location, quantity — (I g4j-4A(, Y2r f,’V L-’L’

and dates that wastes exceeding treatment standardsentered and were removed from storage (S264 73 or, j (4S265.731? _Yes _L0*

d. Do operating records agree with container labeling? ‘ J,’,,1S268.5O(a)(2) or $264.73 or S265.731 /

_LYes 140*

e. Is waste exceeding treatment standards stored forless than 1 year? Jes _NoIf yes, can you show that such- accumulation is notnecessary to facilitate proper recovery, treatmi,or disposal? Yes _No

‘,‘.

, / / •L.If yes, state how — / C -- “-

- L1-_.f Was/is waste exceeding treatment standards stored.for more than one year? _Yes ,jRo

If yes, state the owner/operator’s proof that suchstorage was solely for the purposes of accumulationof such quantities of hazardous waste as arenecessary to facilitate proper recovery, treatment,or disposal:______________________________________

D. Treatment in Surface Impoundments ($268.4)

1. Are prohibited wastes placed in surface impoundmentsfor treatment?/

Yes

If no, go to E.

2. Is the only recognizable “treatment” occurring in theimpoundment either evaporation, dilution, or both(S268.4(b) and $268.31? _Ies* _No3. Did the faciltty submit a certification of compliancewith minimum technology and ground water monitoringrequirements, and the waste analysis “plan to theAgency (S268.4(a)(4)I? _Yes _No*

4. Have the minimum technology requifementsbeen met ($268.4(a)(3)j? Yes _14*

a. If the minimum technology requirements have notbeen met, has a waiver been granted for thatunit(s) [S268.4(a)(3)(iii)I? _Yes 140*


ID Number: ,hjb o()?asqDO

—

Coents5. Have the Subpart ?ground-vater monitoring requirements

been met ($268.4(a)(3)]? Yes No*

6. Have representative samples of the sludge andsupernatant from the surface impoundment been testedseparately, acceptably, and in accordance with thesampling frequency and analysis specified in the wasteanalysis plan and are the results in the operatingrecord for all wastes with treatment standards orprohibition levels L1268.4(a)(2)I? _Yes _No*

7. Did the hazardous waste residue (sludge or liquid)exceed the treatment standards or prohibilion levels?

Yes No

8. Provide the frequency of analyses conducted ontreatment residues:___________________________________

Does the frequency meet the requirements of the wasteanalysis plan [4264.13 or 4265.13)? Yes _No*

9. Does the operating record adequately document theresults of waste analyses performed (4264.13 or4265.13]? _Yes No*

10. Have the hazardous waste residues that exceed thetreatment standards and/or prohibition leve.s beenremoved adequately and on an annual basis(5268.4(a)(2)(ii)j? _Yes _No*

a. If answer to 6 is no and supernatant is determinedto exceed treatment concentrations, is annualthroughput greater than impoundment volume?(note: sludge exceeding treatment standards mustbe removed) _Yes No

11. If residues wer, removed annually, were adequateprecautions takn to protect liners and do recordsindicate that inspections of liner integrity areperformed? _Yes No

12. When removed, were residues of restricted wastesmanaged subsequently in another surface impoundment?

Yes No

a. Were these residues subject to a valid 268.8certification? Yes _No*

13. When removed, were wastes treated prior to disposal?Yes No

a. If yes, are waste residues treated on or offsite?Onsite OffsiteTSDP-4

Inspector: 3.noComments

b. Identify pment method —

E. Treatment

1. Does the facility operate creatment units (regulated orexempt) (not including surface impoundments)? /_Yes iLNo

If no, go to “P.”

2. Describe the treatment processes, including exemptprocesses.

3. Does the facility treat soft hammered wastes?Yes No

a. If yes, is treatment occurring as described in thegenerator’s certification/demonstration($268.8(c)(1))? _Yes _No*

b. Did the treatment facility certify he treated’thesoft hammered waste as per the generator’s demonstration and maintain copies of all certifications(268.8(c)(1)J? Yes _No*

c. Did the treatment facility send a copy of thegenerator’s demonstration and certification to thereceiving treatment, recovery, or storage facility[$268.8(c)(2)J? _Yes _No*

4. Does the facility, in accordance with an acceptablewaste analysis plan, verify that the residue extractfrom all treatment processes for the restricted wastesare less than treatment standards or prohibitionlevels (4268.7(c)(2)]? Yes _No*

5. Describe fr.qsncy of testing of treatment residuals.

6. Was dilution used as a substitute for treatment[S268.31? _Tes* No

* A potential violation is indicatedTSDY-5

ID Number: ;q —

I / 11

7. Are all notificstl..ons, certifications, and results ofwaste analyses kept in the operating record [4264.73(b)or 5265.73(b))? Yes _14o*

8. Are notices provided to land disposal facilities complete with Waste Number, treatment standard, manifestnumber, and analytical data (where available) submittedfor each shipment of waste or treatment residual thatmeets the treatment standard stating that waste hasbeen treated to treatment performance standards(5268.7(b)(4) and (5) and 5268.8(c)(1)j?

Yes

9. If the waste or treatment residue will be furthermanaged at another storage or treatment facility, hasthe treatment facility complied with the 268.7(a)notification and certification requirements applicableto generators 14268.7(b)(6H? _Yes _No*

F. Land Disposal

1. Are restricted and/or prohibited wastes placed in landdisposal units (landfills, surface impoundments** wastepiles, wells, land treatment units, salt domes/beds,mines/caves concrete vault or bunker?) Yes No

2. Did facility have the notice and certification fromgenerators/treaters in its operating record that allprohibited wastes disposed met standards fOt’ generationor treatment [55268.7(c)(l); 268.7(a),(b)J? /

Yes V No*

3. Did the facility obtain waste analysis data throughtesting of the waste to determine that the wastes arein compliance with the applicable treatment standar4s(4268.7(c)(2)) _Yes jNo*

If yes, was the frequency of testing as required by thefacility’s vaste analysis plan [5264.13 or 4265.13)?

Yes No*

4. Were prohibIted wastes exceeding the applicable treatment standards or prohibition levels placed in landdisposal units (268.301 excluding national pacityvariances (268.30(a))? jYes _No

If yes, did facility have an approved waiver based onno migration petition [268.61 or approved case—by—caseor capacity extension (268.51 or treatment standardvariance [268.44][4268.30(d), 4268.31(d), S268.32(g,,-§268.33(e)]? _Yes _No*

* A potential violation is indicated**Do not include SIs addressed under Section “0” of this

checklist.

Coen ts

I I ‘2

I1 4 /?

HiU

, a- -

h-cc

TSDF-6

Inspector:/ / 2/

oents5. Were restricted wastes subject to a national capacityvariance or caI—b’—case extension disposed? 4Yes iNo

If yes have the minimum technology requirementsbeen met for all units receiving such vastes[1268.30(c), 1268.31(c), 1268.32(d), 1268.33(d))?

Yes No*6. Were adequate records of disposal maintained /[1264.73(b) or 1265.73(b))? Yes jNo*7. If wastes subject to a nationwide variance, case—by—case extensions (268.5), or no migration petitions(268.6) were disposed, does facility have generator’snotices [268.7(a)(3)I and records of disposal?(1264.73(b) or 1265.73(b)) _Yes _No*

8. If the facility has a case—by—case extension, can theinsp..c:o- verify that the facility is making progressas described in progress reports? _Yes _No

9. If the owner/operator is disposing of a soft—hammervaste, is he maintaining the generators and treaters(if applicable) notices and certifications(1268.8(a)(2)—(a)(4)J? Yes No*

a. Is the facility disposing of any soft hammer wastesthat may be classified as California wastes?Yes No

b. Did the facility seek to verify whether thesewastes may be subject to all restrictions, e.g.,California ban? _Yes No


LIST OP APPENDICES ()(J)

APPENDIX A-i — - SGLVENT IDENTIFICATION CHECKLIST

APPENDIX A-2 - POTENTIAL F-SOLVENT WASTE MISCLASSIFICATION

APPENDIX 8 - TREATMENT STANDARDS FOR F-SOLVENTS

APPENDIX C - CALIFORNIA LIST RESTRICTIONS

APPENDIX D-i - SOFT HAMMERED RESTRICTED F AND K WASTES IN FIRST THIRDAPPENDIX D-2 - DESCRIPTIONS OF SOFT HAMMERED RESTRICTED P AND K WASTES INFIRST THIRD

APPENDIX E - FIRST THIRD WASTES FOR WHICH TREATMENT STANDARDS WERE SETAPPENDIX F - SOFT HAMMERED P AND U WASTES

APPENDIX G - POTENTIAL CALIFORNIA LIST APPLICABILITY TO SOFT HAMMER WASTES(F & K WASTES)

APPENDIX H - RESTRICTED WASTES SUBJECT TO NATIONAL VARIANCES

a

b

0• CRCRA Inspection Report

I. Inspector and Author of Report

David J. BockelmannEnvironmental Scientist

2. Facility Information

Koppers Company, Inc.P. 0. Box 160Tie Plant, Mississippi 38960MSD007027543

3. Responsible Company Official

Mr. J. D. “Rock” Clayton, Plant Manager

4. Inspection Participants

Mr. David J. Bockelmann, BPCMs. Karen McKinney, EPAMr. Leo Romanowski, EPAMr. J. D,. “Rock” Clayton, KoppersMr. Gary McClelland, Koppers

5. Date and Time of Inspections

December 12, 1988 — 9:15 a.m. CST

6. Applicable Requirements

Mississippi Hazardous Waste Management Regulations(MWHMR) Parts 262, 264, 265, and 268. MississippiHazardous Waste Management Permit No. 88-543-01.

7. Purpose of Inspection

This was a Compliance Evaluation Inspection todetermine the facility’s overall compliance with theapplicable interim status regulations and with thefacility’s Hazardous Waste Management Permit No.88—543—01 which covers the operation, closure andpost—closure requirements for the facility’s surfaceimpoundment.

8. Facility Description

Koppers Company, Inc. is located in the Town of TiePlant which is approximately 5 miles southeast ofGrenada, Mississippi. The facility uses creosote andoil borne pentachiorophenol in the pressure treatmentof wood products for railroads, utilities and others.

2

The primary product is treated railroad cross—ties.Raw materials and treated products arrive and leave byrail and truck. The hazardous wastes which aregenerated, treated, stored and, in the past, disposedof at the facility are bottom sediment sludge from thetreatment of wastewaters from wood preserving processesthat use creosote and/or pentachlorphenol (1<001), wastecreosote (U05l), and certain waste pentachiorophenol(F027). The facility has four hazardous wastemanagement units which are a less than 90 daycontainer/drum storage building, a surface impoundment,a spray irrigation field, and a boiler ash landfarri. Apermit for the operation of the surface impoundment wasissued on June 28, 1988. State administrative ordersrequiring the submittal of Part B permit applicationsfor the spray irrigation field and the boiler ashlandfarm were also issued on July 22 and 29, 1988. APart B permit application for the boiler ash landfarinwas received by the Bureau on November 9, 1988. Theadministrative order requiring the submittal of a PartB permit application for the spray irrigation field iscurrently under appeal by the facility.

The facility is currently in the process of closing thesurface impoundment which was operated as a wastewatertreatment lagoon and generated the listed hazardouswaste 1<001. Treatment of wastewater in the surfaceimpoundment was preceeded by a flow equalization tank,a pentachiorophenol and oil separator wherepentachiorphenol and oil are recovered and recycled, acreosote separator where creosote is recovered andrecycled, and a flocculation system. Since the startof closure at the surface impoundment, the facility hasbeen disposing of their wastewater by pumping it to aseries of two 10,000 gallon railroad tank cars wherethe wastewater is heated and evaporated to theatmosphere. The facility is currently in the processof constructing a wastewater pretreatment system andobtaining a Pretreatment permit to discharge thetreated wastewater to the City of Grenada POTW.

The spray irrigation field was the final stage in thefacility’s wastewater treatment system. It isapproximately four acres in size and is surrounded by alow berm for run—on/run—off control. The sprayirrigation field received effluent from the surfaceimpoundment which was land applied via six sprayirrigation nozzles. The field is covered with non—foodchain vegetation and was operated as a land treatmentunit for the biodegredation of effluent from thesurface impoundment prior to the start of closure atthe surface impoundment.

3

The facility operates a boiler for the thermalconversion of wood and various wastes into steam.Prior to October of 1986 these wastes included thelisted hazardous wastes KOOl, U051 and F027. The ashgenerated from this process is a listed hazardous wasteand, prior to July, 1987, was land disposed on theboiler ash lanctfarin located in the southern portion ofthe facility. Prior to November 19, 1980, two oldsurface impoundments located in the central portion ofthe facility were closed and the waste sludge removedduring closure was also disposed of at the boiler ashlandfarm area. The facility currently operates theboiler burning wood and various wastes associated withwood treating operations. These wastes have beenreported by the facility to be non—hazardous. The ashgenerated from this process is currently being disposedof at a local sanitary landfill. During thisinspection it was found that the facility hasapparently burned listed hazardous wastes along withnon—hazardous wastes in the boiler and that the ashgenerated from the burning of these apparentlyhazardous wastes was also disposed of at the localsanitary landfill.

The facility operates a less than 90 day container/drumstorage building located near the process area. Thebuilding is used to store drums of both hazardous andnon—hazardous waste.

9. Findings

An inspection and review of the facility’s records wasconducted. These records included inspection logs,personnel training records, waste manifests,groundwater monitoring records and reports, financialassurance and liability insurance records, closureplans and the facility contingency plan.

The facility’s inspection logs, personnel trainingrecords, closure plan and contingency plan werereviewed and found to be up—to—date and in compliance.

The facility utilizes the corporate financial test todemonstrate financial assurance for closure/post-closure and liability insurance. This iscurrently being revised to include closure/post—closurecosts and liability insurance for the boiler ashlandfarm and will be resubmitted as soon as it isavailable.

A review of the facility’s 1988 groundwater monitoringand analysis records for the surface impoundment,boiler ash landfarrn and spray irrigation field wasconducted. This review included data submitted by

004

Koppers as well as groundwater analytical datacollected by U.S. EPA in May, 1988. The findings ofthis review with respect to each unit is outlinedbelow.

Surface Impoundment. The facility was issued HazardousWaste Management Permit No. 88-543-01 for the surfaceimpoundment on June 28, 1988. Prior to this date thesurface impoundment was regulated under the interimstatus standards contained within MHWNR Part 265. Thefirst and second quarters of groundwater data weresubmitted under MHWMR Part 265 arid the third and fourthquarters of groundwater data were submitted under thepermit requirements. A review of this data found thatno statistical analyses were reported. Site specificconstituents were analyzed for during all fourquarters. These showed constituent concentrationlevels above method 8270 detection limit, listed inSW—846, for wells R—1, R—1OA, R—7, R—8A, R—9C and R—90in the first quarter and well R—l in the second, thirdand fourth quarters. In the absence of any statisticalanalyses, this data can only be interpreted as evidenceof groundwater contamination at the surfaceimpoundment.

Permit Condition IV.C.3. required that upgradient wellR—l, which was improperly constructed, be replaced witha properly constructed well within thirty days of theeffective date of the permit; this well has not yetbeen replaced. Additionally, because well R—1 isimproperly constructed, the analytical data from itcannot be reliably evaluated.

Boiler Ash Landfarm. Groundwater monitoring at theboiler ash landf arm was first started in 1988.Monitoring was done on an accelerated. schedule with onesampling event per month during February, March, Apriland May. A fifth sampling event was also conducted inJuly. A review of this data found that no MHWMR Part265 Appendix III parameters or EPA interim primarydrinking water standards were analyzed for during thefirst year sampling events as required by MHWMR265.92(c)(1). The indicator parameter of Total OrganicHalogen (TOX) was not included in any of the fiverounds of analytical data or in the statisticalanalysis submitted for the fifth round sampling event,as required byMHWMR 265.92(c)(l), 265.92(d)(2), and265.93(b). Site specific constituents were alsoanalyzed for and reported at the boiler ash landfarm.Low level concentrations of nearly all the sitespecific polynuclear aerornatic hydrocarbons (PAH’s)were repoted in all three downgrac3ient wells during thefirst, second, third, and fifth round sampling events.Low level concentrations of a few of the phenolic

005

compounds were reported for the first, third, fourthand fifth round sampling events, no phenolic compoundswere reported as being analyzed for in the second roundevent. Additionally, the U.S. EPA sampling eventconducted in May, 1988, found the following constituentconcentrations in downgradient well YW-3: 1600 ppbtrichloroethene, 57 ppb cis - l,2-dichloroethene, 6.5ppb carbon disulfide and 1.6 ppb chloroform. From allof the data presented, it appears that there isgroundwater contamination at the boiler ash landfarm.Because of the concentration levels reported fortrichioroethene and cis - 1,2—dichioroethene, it isrecommended that an analysis for these two constituentsbe included in all future sampling events at the boilerash !andfarm.

Spray Irrigation Field. The spray irrigation field isconsidered by the State of Mississippi to be aregulated hazardous waste management unit, Koppers iscurrently contesting this position.

Groundwater at the sprayfield was sampled on aquarterly basis during 1988. A review of this datafound that no statistical analyses were submitted forany of the four quarters. Site specific constituentswere analyzed for during all four quarters. Theseshowed constituent concentration levels above method8270 detection limit listed in SW—846 for wells SF—3and SF-4 in the first quarter, well SF—2 in the secondquarter and well SF-4 in the fourth quarter. In theabsence of any statistical analyses, this data can onlybe interpreted as evidence of groundwater contaminationat the surface impoundment.

A review of the facility’s waste manifests for 1988 wasalso conducted. These manifests were for wastes whichwere shipped to the Koppers Grenada facility to beburned in the facility’s boiler in conjunction withtheir fuel additives program. The ash generated fromthis process is currently disposed of at a local countylandfill. A review of these manifests, and the wasteanalysis sheets for each manifest, found that severalof the manifests were for wastes which appear to behazardous waste. The following is an outline of thesemanifests:

Manifest Source1 No. of Total Date ofDoc. No. of Waste Containers Quantity (lbs) Receipt

67212 Creosote Process 75 41,200 7/22/88Sludge from oil &water separator

67213 As described above 74 40,947 7/30/88

6

67214 As described above 83 46,940 8/9/8800182 PCP Separator 48 30,260 8/24/88

Sourcedescription is taken from the waste analysis sheet for eachindividual manifest.

It appears from the source descriptions that thesewastes are a KOOl hazardous waste which is defined as“bottom sediment sludge from the treatment ofwastewaters from wood preserving processes that usecreosote and/or pentachiorphenol”. Creosote orpentachiorophenol sludges from a wastewater separatorwould fit into this definition and would be classifiedas a 1(001 hazardous waste. The ash generated from theburning of a hazardous waste is also a hazardous waste.This being the case, Koppers appears to have improperlytransported and disposed of 1(001 hazardous waste at thelocal Grenada County landfill. Additionally, all 1(001hazardous wastes disposed of after August 8, 1988,would have been subject to the land disposalrestrictions contained within MHWMR Part 268.

Following the record review a visual site inspection ofthe facility was conducted. The site inspectionincluded the less than 90 day container/drum storagebuilding, the surface impoundment, the spray irrigationfield and the boiler ash landfarm.

The less than 90 day container/drum storage buildingcontained 34 drums labeled as non—hazardous and 6 drumslabeled as containing U05l hazardous waste. Four ofthese drums had an accumulation date of November 19,1937, and the other 2 drums had an accumulation date ofMarch 10, 1988. All six drums containing U051hazardous waste had been stored for longer than 90days.

The surface impoundment was inspected and is in theprocess of being closed. Sludges and associated soilshad been removed. No closure activities were beingconducted at the time of the inspection. A gap in thefence around the surface impoundment, created to allowthe entrance of equipment for sludge and soil removal,should be closed until such time as closure activitiesresume.

The spray irrigation field was inspected. It isrecommended that additional signs warning againstunauthorized entry be placed along the east side fenceline. It is further recommendedd that the gate berepaired as well as the west side fence line where some

7

small trees and limbs have fallen across the fence.The facility ceased operation of the spray irrigationfield after wastewaters were removed from the surfaceimpoundment and closure of the surface impoundment wasinitiated.

An inspection of the boiler ash landfarrn found thatcontaminated soils removed from various facilityprocess areas was being stored here on top of plastic.It is recommended that these soils not be stored in theboiler ash landfarm area.

10. Conclusions

Koppers Company, Inc. is in apparent violation of thefollowing requirements of the applicable MississippiHazardous Waste Management Regulations and therequirements of Mississippi Hazardous Waste ManagementPermit No. 88—543—01:

(a) MHWMR 265.93 - Preparation, Evaluation, andResponse — The facility has failed to perform therequired statistical analyses at the surfaceimpoundment and at the spray irrigation field andhas failed to properly notify the ExecutiveDirector of the existence of groundwatercontamination at these sites as required.Additionally, the facility has failed to properlynotify the Executive Director of the existence ofgroundwater contamination at the boiler ashlandfarm.

(b) MHWMR 264.71 and 264.72 - The facility failed tonote and failed to report a significant manifestdiscrepancy in that KOOl hazardous waste wasbrought on—site under manifests which described itas non—hazardous process waste containing usedcreosote or non—hazardous process waste containingused pentachiorophenol. (Note: This waste wassubsequently burned in the facility’s boiler)

(c) MHWMR Part 262 Subparts A, B and C - The facilityimproperly transported hazardous waste ash,derived from the burning of 1(001 hazardous wastein their boiler, to a facility, the local GrenadaCounty landfill, which did not have an EPAidentification number and was not permitted todispose of hazardous waste. In addition, thefacility had no records of these shipments beingproperly manifested, Labeled or mariced asrequired.

(d) MHWMR Part 268 - The facility did not have anyrecords or certifications that would have shown

8

that the two shipments of waste (identified byManifest Document Nos. 67214 and 00182) receivedon—site after August 8, 1988, the effective dateof land disposal restriction treatment standardsfor 1(001 hazardous waste, would have met the landdisposal restriction treatment standard for 1(001prior to disposal as required.

(e) MHWMR 262.34 - The facility stored six drums ofU051 hazardous waste at its less than 90 daycontainer/drum storage building for longer than 90days.

(f) MHWMR 264.14 — The facility did not maintain anadequate and continuous barrier around thepermitted closing surface impoundment.

(g) MHWMR 265.302 - The facility failed to provideadequate run—on/run—off control and wind dispersalcontrol systems for the boiler ash landfarm.

(1-i) Koppers needs to address the issue in PermitCondition IV.C.3. requiring that upgradient wellR—l be replaced with a properly constructed well.

(i) MHWMR 265.92 — Sampling and Analysis — Thefacility failed to analyze groundwater samplesfrom the Boiler Ash Landf arm Monitoring wells forthe indicator parameter of Total Organic Halogen(TOX) as required.

11. Recommendations are listed as follows:

Koppers need to break out their closure and post-closure cost estimates into specific units instead oflum sum. This would insure that all unit costestimates are updated accordingly.

12. Signed

/ / I / /r4’/ . -h

‘:; //

13. Approval

,

cc: Mr. James H. Scarbrough, EPA

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The

owner

or

opera

tor

must

dev

elop

andfo

llow

asch

edule

andpla

nfo

rin

spectio

ns.

c)T

heow

neror

opera

tor

must

take

rem

edi

al

actio

nupon

the

dete

ctio

no

fm

al

functio

nor

the

dete

riora

tion

of

equip

ment

andstru

ctu

res

when

ah

azardis

imm

inen

t.

d)T

heow

nero

ropera

tor

mu

stre

cord

insp

ectio

ns

inan

insp

ectio

nlo

gand

must

keep

the

record

sfo

rat

least

thre

ey

ears

from

he

date

of

insp

ectio

n.

t3ance

No

Not

apdic

a—

NAY

esN

oN

/AREO

UIREkA

.CITCO

MM

ENTS

00

SL

4/

L/

iii

:%Lzz:)Jr/t/

health

.

/////

IN

ot

incom

plia

nce

—N

oR

EO

UiR

EIL

..iH

ota

llic

al

—N

AY

esN

oN

/A265.1

6F

acility

Pers

onnl

Tra

inin

g

a)F

acility

perso

nnel

must

successfu

llyco

mplete

apro

gram

of

cla

ssroom

insc

ruc

cion

or

on—the—

jobtra

inin

gth

at

teache

themto

perfo

rmth

eir

dutie

sin

aw

aych

atensu

res

the

facility

’sco

mplian

cew

ithth

ere

quire

ments

of

Part

265.

b)T

hetra

inin

gpro

gram

must

beco

mpleted

with

insix

month

sof

the

effe

ctiv

e

Qdate

of

Part

265.

There

must

bean

annual

review

of

the

initia

ltra

inin

gin

(a)ab

ove.

d)

The

owner

or

opera

tor

must

main

tain

record

sof

train

ing.

if

e)T

rain

ing

record

son

curre

nt

perso

nnel

•m

ustbe

kep

tuntil

clo

sure

of

the

faci

lity.

265.1

7G

eneral

Req

uirem

ents

for

Ignita

ble

,R

eactive

or

Incom

patib

leW

astes

The

ow

ner

or

opera

tor

must

take

pre

cautio

ns

topre

vent

accid

enta

lig

ni

tion

or

reactio

nof

ignita

ble

or

reac

tive

waste

.

b)T

reatm

ent,

stora

ge,

or

disp

osa

lof

Ignita

ble

or

reactiv

ew

astean

dth

em

ixtu

reat’

com

min

glin

gof

incom

patib

lew

aste

sm

ust

be

conducted

soth

at

itdoes

not:

1)G

enerate

extrem

eheat

or

pre

ssure

,fire

or

explo

sion,

or

vio

lent

reactio

n;

2)P

roduce

unconfro

lled

toxic

mists,

fum

es,dusts,

or

gase

sin

suffic

ient

REQ

tJIREh.-.’4T.

265.1

7—

Continued—

—

quantitie

sto

thre

ate

nhum

an..h

ealth;

3)P

roduce

uncontro

lled

flamm

able

fum

esor

gase

sin

suffic

ient

quantitie

sto

pose

aris

kof

fireor

explo

sions;

4)D

amage

the

stru

ctu

ral

inte

grity

of

the

devic

eor

facility

conta

inin

gw

aste

;or

Thro

ugh

oth

er

like

mean

sth

reate

nhum

anhealth

or

the

enviro

nm

ent.

SUB

PAR

TD

—C

ON

TING

ENC

YPLA

NS

265.3

7,

faci—opera

ted

for

hazard

ous

waste

Pursu

ant

to265.5

6,

facilitie

sm

ust

hav

eontin

gncy

pla

ns

and

emerg

ency

pro

cedure

sbe

follo

wed

inth

eevent

of

are

lease

hazard

ous

waste

.

SUB

PAR

TE

—M

AN

IFEST

SYST

EM

,R

EC

OR

DK

EE

PING

,

265.7

1(a)(l—

5)

Ifa

facility

receiv

es

hazard

ous

waste

accom

pan

iedby

am

ani

fest,

the

owner

or

opera

tor

must

meet

the

require

ments

of26

5.7

1(a

)(l—5)

265.7

l(b)(l—

5)

Ifa

facility

receiv

es,

froma

rail

or

wate

rtra

nsporte

r,hazard

ous

waste

which

isacco

mpan

iedby

ash

ippin

gpaper,

the

owner

or

oper—1

ato

rm

ust

meet

tFere

quire

ments

of

265k

71.

Not

incom

pl’a

nce

—N

oN

otaplic

a—

NA

CO

MfE

NT

SY

es-

No

—N

/A

0OSU

BPA

RT

C—

PRE

PAR

ED

NE

SSA

ND

PRE

VE

NT

ION

I;

Pursu

ant

Co

265;3

0th

rough

lities

must

be

main

tain

ed

andand

pre

ventio

nof

rele

ase

sof

contro

lled

byth

eS

tate

.

I

12

AN

DR

EPO

RT

ING

/V

I

/kr’

,;J0z

)irtii

iLft-

S’-

AL

’’

/2çi

Inco

mplian

’”’—

Yes

Not

incom

p.4nce

—N

oR

EQ

UIR

EK

EN

T.

________

______________

Not

ap1ic

able

—N

ACO

MM

ENTS

265.7

2(a)

Upon

dis

covey

of

sig

nific

ant

manife

stdisc

repancy

1th

eow

ner

or

opera

tor

must

atte

mpt

tore

concile

the

disc

repancy

with

the

waste

genera

toor

transporte

r.

(b)

Ifa

sig

nific

ant

manife

stdis

crepan

cyis

not

resolv

ed

1th

eow

ner

or

opera

tor

must

notify

the

Dire

cto

r.

265.7

3(b

)T

heow

ner

or

operator

1must

keep

aw

ritten

opera

ting

record

at

the

faci-

licyw

hic

hm

eetsth

ere

quire

ments

of

265.7

3(b

).

265.7

4(a

)A

llre

cord

sm

ust

be

furn

ished

upon

request

andavaila

ble

at

all

times

for

insp

ectio

nby

the

Dire

cto

ror

EPA

.

a(c

)A

copy

of

record

sof

waste

dis

posa

llo

catio

ns

andquantitie

sm

ust

besu

bm

itted

toth

eD

irecto

rand

the

local

land

auth

ority

upon

clo

sure

of

the

facility

.I,

265.75T

heow

neror

opera

tor

must

subm

itan

annual

report

toth

eD

irecto

rin

com

plian

cew

ithth

ere

quire

ments

of

265.7

5.

265.76T

here

ceip

cof

any

unm

anife

sted

waste

must

bere

porte

dto

the

Dire

cto

r.

265.7?T

heow

neror

opera

tor

must

subm

ita

report

toth

eD

irecto

rif

any

of

the

follo

win

goccur:

a)re

leases,

fires,

explo

sions

b)gro

undw

aterconta

min

atio

nc)

facility

cio

sure

.

Yes

-N

oN

/A/

/

Iii

00

ji

1/

/1

VI

/

(i

:

v)---

—-

S-

rL

-

..,

Lnco

mplian

ce.—

Yes

No

tin

comç

ance

No

RE

QU

IRE

tEN

T.

____

__

_

Not

ap,lic

ab.L

e—

NA

COM

MEN

TS

SUB

PAR

TF

—G

ROU

ND

WA

TERM

6NIT

OR

INC

265.9

0O

wner

or

opera

tor

mudt

implem

ent

agro

undw

aterm

onito

ring

pro

gram

capable

of

dete

rmin

ing

the

facility

’sim

pact

onth

equality

of

the

upper

aquife

rw

Ithin

one

year

of

the

effe

ctiv

ed

ate

of

26

5.9

0.

265.9

1—

26

5.9

4T

heow

ner

and

opera

tor

mu

stin

sta

ll,opera

te,

andm

ain

tain

agro

undw

aterm

on

itorin

gsy

stemw

hich

meets

the

require

ments

of

26591.—

265.9

4.

26

5.9

0(c)

All

of

the

gro

undw

aterm

onito

rin

gre

quire

ments

may

bew

aived

Ifth

eow

neror

opera

tor

candem

onstra

teth

at

there

isa

low

pote

ntia

lfo

rm

igra

tion

of

hazard

ous

waste

constitu

ents

from

the

facility

via

the

up

perm

ost

aquife

rb

elow

the

facility

Cow

acir

sup

ply

wells

or

tosu

rface

wate

r.

UB

PAR

TC

—C

LOSU

RE

AN

DPO

ST—C

LOSU

RE

ED2

65

.11

1T

heow

nero

ropera

tor

must

clo

sehis

facility

ina

man

ner

that:

1)m

inim

izesth

eneed

for

futu

rem

ain

ten

an

ce,

and

2)contro

ls,m

inim

izes,or

elim

inate

spost—

closu

reesc

ape

of

hazard

ous

waste

.

Yes

No

N/A

H

00/

,;;,c9

265

.112(a)

The

owner

or

opera

tor

mu

sthav

ea

writte

nclo

sure

plan

onth

eeffe

ctiv

ed

ate

of

Part

265.

Inco

mplian

ca—

Yes

Not

inco

msn

ceN

oR

EQU

IRE1IEN

T.N

ot

aplic

able

—N

ACO

MM

ENTS

265;112

(a)C

ontinued——

Tie

clo

sure

pla

nm

Lst

inclu

de:

1)A

desc

riptio

nof

howand

when

the

facility

will

bepartia

llyclo

sed,

ifapplic

able

,and

ultim

ate

lyclo

sed.

2)A

nestim

ate

of

the

maxim

umin

ven

tory

of

wastes

insto

rage

or

treatm

ent

at

anygiv

entim

e.

3)S

teps

todeco

ntam

inate

facility

equip

men

t.N

-

4)A

sched

ule

for

final

clo

sure

which

must

inclu

de,

asa

minim

um,

antic

ipated

date

sw

henw

astesw

illno

longer

bere

ceiv

ed,

antic

ipate

ddate

for

com

ple

tion

of

final

clo

sure

,and

interv

en—

ing

mile

stone

date

s.

265.113(a)

Clo

sure

must

bein

itiate

dw

ithin

90day

safte

rre

ceiv

ing

the.

(b)T

heow

neror

opera

tor

must

com

plete

clo

sure

activ

ities

with

insix

month

safte

rre

ceiv

ing

the

final

volume

of

waste

s.

265.114U

ponco

mpletio

nof

clo

sure

,all

equip

men

tand

structu

res

must

bepro

perly

disp

osed

of

or

deco

ntam

inated

.

265.115T

heow

neror

opera

tor.

andan

inde

pen

den

tre

giste

red

pro

fessio

nal

engi

neer

must

certify

that

the

facility

has

been

clo

sed

inacco

rdan

cew

ithth

eap

pro

ved

clo

sure

pla

n.

Yes

-N

oN

/A

I

00

////V

I

//fin

al

volu

me

ofhazard

ous

waste

s.

(I

Ij

/!‘-‘

}r’

ji

RE

QU

IRE

KE

NT

265.1

17(a)

Post

clo

sure

,care

must

consist

of

at

least:

1)G

roundw

aterm

onito

ring

2)M

ainten

ance

of

the

conta

min

ant

sys

tern..

The

owner

or

opera

tor

must

hav

ea

post—

closu

repla

non

the

effe

ctiv

edate

of

Part

265an

dit

must

Inclu

de:

1)G

roundw

aterm

onito

ring

activ

ities

andfre

quency.

4

2)M

ainten

ance

activ

ities

andfre

quen

cie

sto

ensu

reth

ein

tegrity

of

the

cap,

final

cover,

or

oth

er

conta

inm

ent

stru

ctu

res,

andfu

nctio

ns

of

the

faci

lities

monito

ring

equip

men

t.

265.1

19

With

in90

day

safte

rclo

sure

,th

eow

neror

opera

tor

must

subm

ita

surv

eypla

tof

the

facility

.

265.120T

heow

ner

or

opera

tor

must

record

anotic

eon

the

deed

that

the

land

has

been

used

tom

anagehazard

ous

wasc

SUB

PAR

TH

—FIN

AN

CIA

LR

EQU

IREM

ENTS

26

5.1

42(a

)T

heow

neror

opera

tor

must

dev

elop

andm

ain

tain

acurre

nt

estlm

at

of

clo

sure

andpost—

closu

recosts

.

ag3

JW

.L

4c

•s

f(?)-%

L

A)

•‘)

‘i,ii

J-fi)J

..1L

I6ti4

Lf

ci)

:14ca.(_

(‘)(k,

1

in

com

pilarice

—

Not

inco

mp

1nce

—N

oN

otapolic

abi.e

—N

ACO

MM

ENTS

L.

A.

Si.(.

.

E.

I-

••

L

SUB

PAR

TI

—O

THER

FAC

ILIT

YSTA

ND

AR

DS

265.1

70

—265.1

72

The

conta

iner

must

becom

patib

lew

ithth

ew

asteto

bes

Cored

.

;Iq7(,

IL

i

Ii’’;

7:

‘/

*,,

I•

RE

QU

lR... N

T

26

5.1

73

Conta

iners

hold

ing

hazard

ous

waste

must

bekept

closQ

dand

must

no

tb

eo

pen

ed,

han

dle

d,

or

store

din

am

anner

wh

ichm

aycau

sea

ruptu

reor

leak

.

265.1

74

Areas

wh

ereco

nta

iners

are

store

dm

ust

bein

specte

dw

eekly

.

26

5.1

76

Conta

iners

hold

ing

ignita

ble

or

reactiv

ew

astem

ust

be

locate

dat

leasi

15m

ete

rsfro

mth

efa

cility

’spro

perty

line.

265.1

77(a)

Incom

patib

lew

aste

sm

ust

not

bep

laced

inth

esam

eco

nta

iner.

(b)

Asto

rage

co

nta

iner

hold

ing

ahazard

ous

waste

that

isin

co

mp

atib

lew

ithan

yw

asteor

oth

er

mate

rials

stol

nearb

ym

ust

be

separa

ted

or

pro

tecte

dfro

mth

eoch

erm

ate

rials.

SUB

PAR

TJ

—TA

NK

S

26

5.1

92

(b)

Hazard

ous

waste

must

be

pla

ced

ina

tan

kif

they

co

uld

cause

the

tan

ko

rits

liner

tole

ak.

(c)U

nco

vered

tanks

mu

sth

ave

ale

ast

two

feet

of

freeboard

unle

sso

ther

conta

inm

ent

stru

ctu

res,

ad

ram

a,

co

ntro

lsy

stem

,or

oth

er

div

ersio

nstru

ctu

res

with

acap

acity

that

equals

or

exceed

sth

evolu

me

of

the

top

two

feet

of

the

tan

k.

(d)

Tan

ks

wh

ichhav

ea

co

ntin

uous

feedsy

stemm

ust

beeq

uip

ped

with

am

eans

tosto

pth

ein

flow

.

1qa/

/6’-

/?

3/i

Not

inco

mplian

ce—

No

No

tao1i

le—

NA

II

00

CO

Q4EN

TS

;flJ

/L

IC

\

9(’)(1

‘—4--A

//

os

IU-

I’-,

-

REQ

UIR

EHI

;ota

piic

ab:N

AC

ON

NEN

TSY

esN

oN

/A-

265.193W

astean

aly

sism

ust

be

con

du

ctedpursu

ant

to265.l3

and265.1

93

(a)

265.1

94

Tan

ks

must

be

insp

ecte

din

accor-

dan

cew

ith265.1

94.

265.

197A

tclo

sure

1all

hazard

ous

waste

ii)and

hazard

ou

sw

astere

sidues

must

be

‘‘

remo

ved

from

the

tanks.

Q265.1

98

Ign

itab

leor

reactiv

ew

astesh

ou

l

Qnot

bepla

ced

ina

tank

unle

ss265

.I

198is

com

plied

with

,

26

5.1

99

Incom

patib

lew

astesm

ust

no

tbe

pla

ced

inth

esam

etan

kunle

ss265

.176

isco

mp

liedw

ith.

Ii-

_,-

ASU

BPA

RT

K—

SUR

FAC

EIM

POU

ND

MEN

TS‘.

26

5.2

22

Must

main

tain

at

least

two

feet

--‘°

of

freeb

oard

C>

..

Yk

)1j.

-k

265.2

3E

arth

en

dik

es

must

hav

epro

tec—L

ive

co

ver.

\,-

26

5.2

25

Mu

stco

nd

uctw

aste

analy

ses

andtr

ial

tests

inacco

rdan

ce

with

26

5.

225.

265.2

26(1

)M

ustin

sp

et

the

freeboard

level

atle

ast

once

eachopera

ting

day

.I

(2)

Must

insp

ect

the

surfa

ce

impoundm

ent

at

least

once

aw

eekto

de—te

ct

any

leak

s,dete

riora

tion,

or

failu

re.

265.228T

hesu

rface

impoundm

entm

ust

clo

s.

-*

UIn

acco

rdan

ce

with

265.

228.

/‘\)C

----

REQ

UIR

E!r

Not

appH

ça

-—

NA

C0fl’tE

NT

SIY

e9I

No

N/A

265.2

29

Ignita

ble

or

reactiv

ew

astem

ust;i.it

bepla

ced

ina

urfa

ce

imp

ou

nd

men

tiir.less

265.2

29

is!co

mp

liedw

ith.

265.230In

com

patib

lew

astesm

ust

not

bep

laced

inth

esam

esu

rface

impoundm

ent

unle

ss265.1

7(b

)is

com

plied

with

.

SUB

PAR

TL

—W

ASTE

PIL

ES

Q2

65

.25

1A

waste

pile

must

be

pro

tecte

dand

managed

toco

ntro

lw

ind

dis

pers

al.

265.252A

now

neror

op

era

tor

must

conduct

waste

analy

ses

un

less

the

facility

meets

the

exem

ptio

ns

of

26

5.2

52

.

265.2

53

With

inone

year’a

fter

the

effe

ctiv

edate

of

the

regula

tions

1le

achate

or

run—off

froma

pile

must

be

co

ntro

lled

pursu

ant

to265.2

53.

a

26

5.2

56

Ign

itab

leor

reactiv

ew

astem

ust

not

beplaced

ina

waste

site

un

less

26

5.2

56

isco

mp

liedw

ith.

Q2

65

.25

7T

here

qu

irem

en

tso

f265.

257fo

r

Oin

com

patib

lew

aste

sm

ust

beco

mp

liedw

ith.

SUB

PAR

TM

-LA

ND

TREA

TMEN

T

265.272(a)

Hazard

ous

waste

must

not

bepla

ced

at

ala

nd

treatm

ent

facility

unle

ssit

canbe

made

less

hazard

ou

sor

no

n—

hazard

ou

s.

(b)

Run—

onm

ust

be

div

erte

daw

ay/‘

fromoth

er

activ

eportio

ns

asof

oney

earafte

rth

eeffe

ctiv

edate

of

Part

265.

Not

inco

mplian

ceN

oR

EQ

u1

RE

hr

Not

ap

lica

—NA

COM

MEN

TSY

esN

oN

/A265.272

——

Co

ntin

ued

r/

(c)R

un—off

fromactiv

ep

ortio

ns

Vm

ustbe

colle

cte

das

of

oneyear

afte

rth

eeffe

ctiv

ed

ate

of

Part

265.

I

265.2

73

Waste

analy

sesm

ustbe

cond

ucted

pursu

ant

to265.2

73.

265.2

76(a)

An

owner

or

op

era

tor

must

no

tiiy

oj’

the

Sta

teD

irecto

rw

ithin

60day

safte

’th

eeffe

ctiv

edate

of

Part

265if

foodch

aincro

ps

aregrow

non

the

land

treatm

ent

facility

.

(b)

Food

chain

crop

sm

ustnot

be

grown

onth

etre

ate

dare

ao

fa

hazard

ou

sw

astelan

dtre

atm

en

tfa

cility

un

less

26

5.2

76

(b)

isco

mp

liedw

ith.

•(c)

Food

chain

crops

must

no

tbe

grown

ona

land

treatm

ent

facility

receiv

ing

waste

that

co

nta

ins

cadmium

unle

ss265.2

76(c)

Isco

mp

liedw

ith.

-

265.278T

heow

nero

ropera

tor

must

hav

eIn

writin

gand

must

implem

ent

anun—

satu

rate

dzone

mo

nito

ring

pla

npursu

ant

to265.2

78.

*

26

5.2

79

The

owner

or

opera

tor

must

keep

7reco

rds

of

the

applic

atio

ndate

s,app—

iV

licatio

nra

tes,

qu

an

tities,

andloca—

do

nofe

ach

hazard

ou

sw

astepla

ced

ina

faàillty

.7

(

265.280

Ala

nd

treatm

ent

facility

must

Vm

eetth

eclo

sure

andpost—

closu

rere

quire

ments

of

265.2

80.

-

REQU

I REK

EN

T

265.2

81

Ign

itab

leo

rr1activ

ew

astem

ust

no

tbe

placed

ina

land

treatm

en

tfaci

lityunle

ss2

65

.28

1is

com

plied

with

.

265.

2112Iitc

iuit,iiLI

hIi’

wii.a

(‘ii

ineiiilaiiiI

Ii

I)IUC

UL

IIn

the

uume

lun

dtre

atm

ent

ure

aunle

ss265.1

7(b

)is

com

plied

with

.

SUB

PAR

TN

—L

AN

DFIL

LS

265

.302(a)

Run—

onm

ustbe

div

erte

daw

ayfrom

the

activ

eportio

ns

with

inone

yr

afte

rth

eeffe

ctiv

edate

of

Part

265.(b)

Run—

offfrom

activ

eportio

ns

must

becolle

cte

dw

ithin

oneyear

afte

rth

eeffe

ctiv

edate

of

Part

265.

a(d

)M

ustcontro

lw

indd

ispersa

l.

26

5.3

09

The

owner

or

op

era

tor

must

meet

the

surv

eyin

gand

record

keep

ing

re

quirem

ents

of

265.3

09.

265.310A

landfill

must

comply

with

clo

sure

andpost—

closu

rere

qu

irem

en

tsof

26

5.3

10

.

265..312Ig

nita

ble

or

reactiv

ew

astem

ustn

ot

beplaced

ina

lan

dfill,

unle

ss2

65

3i2

Isco

mplied

with

.

26

53

13

Inco

mpatib

lew

astesm

ust

no

tbe

pla

ced

ina

landfill

un

less

265.

17

(b)

isco

mp

liedw

ith.

26

5.3

14

Bulk

or

non—

contain

erizedliq

uid

waste

,w

asteco

nta

inin

gfre

e—

liquid

s,or

conta

iners

ho

ldin

gliq

uid

waste

should

not

bep1ed

ina

landfill

unle

ssth

ere

qu

irem

en

tsof

265.3

14

--—

——

._4

1,

•,

—.

d—

No

tin

comp

‘mae

No

Not

apljc

ao..e

—N

AC

OM

NEN

TSY

esN

oN

/A

(\J/

LjA

1IR

V/

0

tjJ

/tDI

L.

RE

QJtR

EM

‘_____________________________

Nocap)licab’A

CO

MM

ENTS

Yes

No

N/A

SUB

PAR

TQ

—C

HE

MIC

AL

,P

HY

SIC

AL

,A

ND

BIO

LO

GI

CL

TR

EA

TtE

NT

N/A265.4

01(a)

Must

com

ply

with.

265.

.17(b

)I

II

(b)

Ilazard

ous

waste

must

not

be

pla

ced

inth

etre

atm

ent

pro

cess

or

equip

men

tif

any

failu

reof.

equip

ment

or

the

pro

cess

would

occur.

Q(c)

Aco

ntin

uously

—fed

pro

cess

must

be

equip

ped

with

am

eansto

stop

jth

ein

flow

.

265.4

02

Waste

analy

ses

andtr

ial

tests

must

beco

nducted

pursu

ant

to265.

602.

265.4

03

Insp

ectio

ns

must

bem

adepursu

ant

to265.4

03.

265.4

04

At

clo

sure

1all

hazard

ous

waste

andhazard

ous

waste

resid

ues

must

berem

oved

.

265.4

05

Ignita

ble

or

reactiv

ew

astem

ust

not

bepla

ced

ina

treatm

ent

pro

cess

unle

ss265.4

05

isco

mplied

with

.j

265.4

06

Incom

patib

lew

aste

sm

ust

not

bepla

ced

inth

esam

etre

atm

ent

pro

ces

unle

ss265.1

7(b

)is

com

plied

with

.

SUB

PAR

TR

—U

ND

ERGRO

UN

DIN

JEC

TIO

N..

265.4

30(a

)underg

round

injection

of

haz

ardous

waste

is

not

subje

ct

toth

eclo

sure

and

post—

clo

sure

or

financial

require

ments

of

Part

265.

Under—

•gro

und

inje

ctio

nis

subje

ct

toth

eoth

er

require

men

of

Part

265.

\/

,UIJ

iEV

-I

Not

aplic

able

—N

ACO

MM

ENTS

Yes

No

-N

/A265.315

(1)E

mpty

co

nta

iners

must

bere—

•d

uced

involu

me

asof

one

year

afte

rth

eeffe

ctiv

edate

oP

art

265.

StJBPA

RT

0—

INC

INE

RA

TO

RS

26

5.3

43

Must

be

acsc

eady

sta

teconditio

ns

befo

read

din

gh

azardo

us

waste

.

26

5.3

45

Waste

an

aly

ses

must

be

con

du

ctedp

ursu

an

tto

265.3

45.

(N

26

5.3

47

Mo

nito

ring

andin

spectio

ns

must

beco

nducted

asd

elin

eate

din

265.4

‘265.3

51

At

clo

sure

1th

eow

neror

opera

tor

must

remove

all

hazard

ou

sw

asteand

hazard

ou

sw

astere

sidues.

SUB

PAR

TP

-TH

ERM

AL

TREA

TMEN

T

4265.373M

ustbe

at

stead

ysta

teconditio

nbefo

read

din

gh

azard

ou

sw

aste

s.

265.375W

asteanaly

ses

mu

stbe

conducted

pursu

ant

to265.3

75.

26

5.3

77

Monito

ring

and

insp

ectio

ns

must

be

conducted

asd

elin

eate

din

265.377.

S

265.3

01

At

clo

sure

,th

eow

nero

ropera—

torm

ust

remo

ve

all

hazard

ou

sw

astere

sidu

es.,

265.382O

penb

urn

ing

of

hazard

ous

waste

isp

roh

ibite

dexcept

for

the

open

burn

ing

and

deto

natio

no

fw

asteex

plo

sives

No

tin

com

plian

ce—

No

RE

Qth

RE

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

__

No

pp

lica1

—N

ACO

MM

ENTS

jies

No

N/A

Oth

erq

uestio

ns

or

standard

s.

Are

there

anyoth

er

genera

tors

transp

ortin

gth

eir

waste

toth

ishazard

ous

waste

manage—

menc

facility

?

0

a

RCRA PERIT INSPECTION CCISTPART I

EPA ID Number —

Name

Address I

Major

_____Minor _____

Date of laspection

Name of EPA Inspector —

Name of Scare Inspector

Type of Violations Sip.

flL.Type of Handler

2 -iz.fr_ f’ J

______rT

Stare En.forcement Action —

Dare of Projected Compliance

Penalty Assessed.

_____

EPA Enforcement Action

Follow—up Visit

______

General Coents

________

Date of Actual Compliance

Collected

(

OQ

‘*ci D

I .) F

;, /

/ F

-2-00

EPA ID#

_________________________

Does the facili have a copy of the R peit on site?

NO

I. Monitoring and Records (264.13)

A. Sampling and Laboratory Procedures

1. Are samples and measurements taken?

2. Are the methods used for obtaining representativesamples in compliance with methods from Appendix I

/1

of 40 CFR Part 261?

____________

3. Are the laboratory methods those specified inTest Methods for Evaluating Solid Waste Physical!Chemical Methods SW—846; Standard Methods for theExamination of Water and Wastewater or an equivalentmethod as specified in-the attached Waste AnalysisPlan?

____________

B. Retention of Records

1. Are all records and reports required under RCRAretained for a minimum of three years?

____________

Conts:

C. Records of Monitoring Information

1. Dates

____________

2. Location

____________

3. Times of sampling or measurement

____________

4. Iniidua1s who perford the sampling ormeasurements

_____________

5. Dates anaylses were performed

___________

6. The individuals who performed the analyses

___________

7. Techniques or methods used

___________

8. The results or such analyses

____________

• Oc 300EPA IDII______________________

YES NO

II. Are any changes in the facility planned? (264.12) VI”

A. If yes, has the Regional Administrator been notified? /1/7

B. Will the change result in non—compliance?

__________

C. Eas the facility been in non—compliance with the

permit which may endanger health or the environment? VIII. Documents to be maintained at the facility sire

A. A copy of the RCA permit

___________

B. Waste Analysis Plan as required by 40 CFR. 264.13 and

the RCA permit 1

C. Personnel Traing Records (264.16)

___________

D. Contingency Plan (264.53)

__________

E. Closure Plan (264.112)

__________

F. Cost Estimate for Facility Closure (264.142)

___________

G. Operating Records (264.73) L/’

E. Inspection Schedule (264.15)

___________

PART IIGENERA..L FACfl.ITY CONDITIONS

I. Maintenance of Facility

Describe:

A. Are general waste analysis conducted according to

the Waste Analysis Plan. (264.13)

_____________

B. Does the facility provide adequate security through: (264.14)

1. 24—hour surveillance system

____________

2. (a) Artificial or natural barrier around facility? V(b) Means to control entry through entrances

_____________

Describe:• .‘ L /1 0”

, ‘1 i—•J’ I , •-• I’ ‘.‘

1• :

00 00—4—

EPA IDt

________________________

GERAL INSPECTION REOUIPNTS

NO

I. Does the Pernittee follow the inspection schedule attached

to the RCRA permit? (264.15) V

Coents:

II. Personnel Training (264.16)

A. Does the owner/operator m.ainraiu Personnel Training

Records at the facility?

____________

B. Eow long are they kept?

____________

C. If yes, do they include:

(1) Job title and written job description of each

position?

_____________

(2) Description of type and amount of training

____________

(3) Records of training given to facility personnel

____________

III. Requirements for Ignitable, Reactive or Incomoatible Waste (264.17)

A. Does the facility handle ignitable or reactive wastes?

____________

(1) I.f yes, is waste separated and con.fined from

sources of ignition or reaction, (open flames,

smoking, cutting, and welding, hot surfaces,

frictioning heat) sparks (static, electrical or

mechanical) spontaneous ignition (e.g. from heat

producing chemical reactions) and radient heat?

___________

(a) If yes, use narrative explanations sheet to

describe separations and confinement procedures.

(b) If no, use narrative explanation sheet to

describe sources of ignition or reaction.

B. Are smoking and open flame confined to specifically

designated locations?

C. Are No Sking” signs posted in hazardous areas?

____________

00 00—5—

EPA ID/fr

!ES ND

IV. Prevaredness and Prevention

A. Is there evidence of fire, explosion or contaminationof the enviroteut? (264.31)

____________

(1) If yes, use narrative sheet to explain.

B. Is the facility equipped with: (264.32)

(1) Internal counication or alarm system?

____________

(a) Is it easily accessible in case of emergency? 7

(2) Telephone or two—gay radio to call emergencyresponse personnel?

_____________

(3) Portable fire extinguishers, fire control equipment,

spill control equipment an decontamination equipment? V A

(a) Is this equipment tested to assure its proper 7operation?

_____________

(4) Water of adequatevolume and pressure and pressure for

hoses, sprinklers or water spray system?

___________

(a) Describe source of water:

C. Is there sufficient aisle space to allow unobstructed

vement of personnel and equipment? (264.35)

____________

D. Eas the owner/operator made arrangements with the local

authorities to familiarize the with characteristics

of the facility? (Layout of facility properties of hazardous

waste handled and associated hazards, places where facility

personnel would normally be working, entrances to roads inside

facility, possible evacuation routes). (264.37) 1

E. In the case that more than one police or fire department /

might respond, is there a designated primary authority? (264.37) /(1) If yes, list primary authority

_____________________

P. Does the owner/operator have phone numbers of and ag-reements

with State emergency response teams, emergency response

contractors and equipment suppliers? (264.37)

____________

(1) Are they readily available to all personnel?

____________

00 00—6—

EPA ID/fr

__________________________

, TES NOL

C. Has the owner/operatorà4ranged to familarize localhospitals with the properties of hazardous watehandled and types of injuries that could result fromfires, explosions, or releases at the facility? (264.37)

___________

H. If State or local authorities decline to enter, isthis entered in the operating record? (264.37)

___________

V. Contingency Plan and Emergency Procedures

A. Is a contingency plan maintained at the facility? (264.51)

__________

(1) If yes, is it a revised Spill Prevention Controland Countermeasure Plan?

3. Is there an emergency coordinator on site at all times?(264.55)

VI. Manifest System, Racord—Keeping and Reporting

A. Does the fac.ility receive waste from off—site? (266.71)

___________

(1) If yes, does the owner/operator retain copiesof all manifests?

___________

(a) Are the manifests signed and dated and returnedto the generator?

___________

(b) Is a signed copy given to the transporter?

___________

B. Does the facility receive any waste from rail or water(bulk shipment) transporter? (264.71)

__________

(1) If yes, is it accompanied by a shipping paper? J/i-7

(a) Does the owner/operator sign and date theshipping paper and return a cnpy to the generator? ,iim

(b) Is a signed copy given to the transporter?

___________

C. Has the owner/operator received any shipments of wastewhich were inconsistent with the manifest? (264.72)

___________

(1) If yes, has he/she attempted to reconcile the /descrepaucy with the generator and transporter?

____________

(a) If no, has the Regioa1 Administrator beennotified? c JQ CL ñiiH. /

D. Does the owner/operator keep a written operating recordat the facility? (264.73)

___________

(1) If yes, does it include:(a) Description and uaniy of each haz;rdous j /

waste received?(b) Location and quantity of each hazardous waste

at each location? /Cc) Records and results of waste analyses?

___________

00 00—7—

EPA ID#

__________________________

YES NO

(d) Report of incidents involving implementing of the /coticingency plan?

___________

(e) Records and results of required inspections?

____________

(f) ?1ouitoring, testing or analytical data?

Vu. Closure

A. Does the facility have a copy of the cJ.osure plan and the

annual cost estimate at the facility? (264.112)

___________

B. What is the anniversary date on which the first closure

cost estimate was prepared? (264.142)

C. Has the closure plan. been annually adjusted for inflation

according to Subpar 264.142(b)(l) and (b)(2)?

___________

D. Has there been any changes in the closure plan that

will require changing the cost estimate? (264.112)

___________

(1) -1± yes, was the cost estimate changed?

VIII. Storage in Containers

A. The permittee may store the following wastes in containers at the

facility subject to the terms of the permit: qo: .-.

/ -

1. 4• / 1 ‘T 7-; - -

2.

_________________

5.

________________

8.

3.

_________________

6.

________________

9.

B. Conditions of Containers (264.171)

Describe c&z>-I L:r- ,---.,

C. Compatibility of Wastes with Containers (264.172)

fi I /

Describe (iLiij&. c -‘iLL-/.

-8-PA iD(

____

D. anagemenr of Containers (264.173)

(1) Are all containers closed?

(2) Are containers stored in an acceDcable manner?

E. Concain: (264.175)

(1) Any cracks or gaps?

(2) Suffcienr to contain all spills, leaks, aridaccumulated precioi:atiou?

(3) Is the area sloped or nave the caaciry to be drained?

(4) Cn it contain 10% of oi,me fcou:ainers?

(5) Ruu—on prevent±on(a) Lf no, go to (4) above-

(6) Any suos or ocher co1lectio?(a) U yes, can they prevent an over1ov?

F. Containers holding ignitable or reac:ive waste mustbe loca:ad at Lasr 15 meters (50 fr) from the Facility’sproperty line. (264.176)

G. Are. you combin.ing incompatible ..&s:e (254.177)?

IX. Storage in Tanks

A. Waste- Identification

Describe (See- Permit) k-

NO

“7

‘V

iz

V//

ni/A./-

7

l txn

Li

00 00EPA ID,

B. Design of Tanks

Describe (See Peit) 14

C. General Operating R.eguiremenrs (264.192)

Describe (See Permit and At:achents)

_________________

D. Special Requireenrs for Ignitable and Reactive Wastes (264.198)

Describe (See Permit andAttachments)

_________________________

E. Special Requirements for Incompatible Wasce (264.199)

Describe (See Permit and Atachnts) /JJA

0 0

EUA INSPECI’ION REPORI’

1. Inspector and Author of Report

David J. Bocke].rnannEnvironnntal Scientist

2. Facility Infonnation

Koppers Canpany, Inc.MS0007027543P. 0. Box 160Tie Plant, Mississippi 38960

3. Responsible Catipany Official

J. D. “Rock” Clayton, Plant ManagerDave King, Environirntal Coordinator - Keystone

4. Inspection Participants

Dave Bockelrnann, MSDNRKaren McKinney, USEPAJ. D. “Rock” Clayton, KoppersDave King, Keystone

5. Date and Tine of Inspections

May 16, 1988 — 9:15 am. CST

6. Applicable Regulations

Mississippi Hazardous Waste ManagerrentRegulations 262 and 265.

7. Purpose of Inspection

This was a Catliance Evaluation Inspection to detexinine thefacility’s overall conpliance with the applicable interim statusregulations.

8. Facility Description

Koppers Canpany, Inc. is located in the TCMn of Tie Plant whichis approximately 5 miles southeast of Grenada, Mississippi. Thefacility uses creosote and oil borne pentachlorophenol in thepressure treatirent of od products for railroads, utilities andothers. The primary product is treated railroad cross-ties. Rawmaterials and treated products arrive and leave by rail and track.

0 0

The hazardous wastes which are generated, treated, stored, and/ordisposed of at the facility are bottan sediirent sludge fran thetreatnEnt of wastewaters fran wood preserving processes thatuse creosote and/or pentachlorophenol (1(001), waste creosote(U051), and certain waste pentachiorophenol (F027). The facilityhas four hazardous waste managrent units which are a less than90 day container/drum storage area, a surface impoundnEnt, aspray irrigation field, and a boiler ash landfam. At the tineof this inspection a permit for the operation of the surfaceirnpoundirent was under review and was subsequently issued on June28, 1988. Orders requiring the suhdttal of Part B permitapplications for the spray irrigation field and the boiler ashlandfarm were also issued on July 22 and 29, 1988.

The facility currently operates a surface impoundnent which isapproximately 0.78 acres in size and has an operating depth ofabout 6—7 feet. The surface impoundrrent is operated as awastewater treatrent lagoon and generates the listed hazardouswaste 1(001. Treatment of wastewater in the surface impoundirentis preceded by a flow equalization tank, a pentachlorophenol andoil separator where pentachiorophenol and oil are recovered andrecycled, a creosote separator where creosote is recovered andrecycled, and flocculation. Closure of the surface inipoundirentwill begin on or before November 8, 1988.

The spray irrigation field is the final stage in the facility’swastewater treatment system. It is approximately four acres insize and is surrounded by a low berm for run-on/run-offcontrol. The spray irrigation field receives effluent fran thesurface iitipounthent which is land applied via six sprayirrigation nozzles. The field is covered with non-food chainvegetation and is operated as a land treatment unit for thebiodegradation of effluent fran the surface impoundnent.

The facility operates a boiler for the thermal conversion of woodand various wastes into steam. Prior to October of 1986 thesewastes included the listed hazardous wastes 1(001, U051, andF027. The ash generated fran this process is a listed hazardouswaste and, prior to July, 1987, was land disposed on the boilerash landfam located in the southern portion of the facility.The facility still operates the boiler, burning wood andnon—hazardous wastes which care fran the process areas (cleaningof the treatrent cylinders and door pit areas, etc.) and disposesof the ash at a local landfill. Prior to November 19, 1980, twoold surface ixnpoundnents located in the central portion of thefacility were closed and the waste sludge renved during closurewas disposed of at the boiler ash landfam area.

The facility operates a less than 90 day container/drum storagebuilding located near the process area. The building is used tostore drums of non-hazardous waste which is burned in the boilerand drums of hazardous waste prior to being shipped off-site.

0 0

9. Findings

Pn inspection and review of the facility’ s records wasconducted. These records included inspection logs, personneltraining records, waste manifests, groundwater nonitoringrecords, financial assurance and liability insurance records,closure plans and a facility contingency plan. Records at thefacility were kept back to 1981.

Waste manifests, financial assurance and liability insurancerecords, closure plans and the facility contingency plan werereviewed and found to be in canpliance.

A review of the groundwater nonitoring records for the surfaceimpoundment and the spray irrigation field found that theserecords were kept for 3 years arid were up-to-date. Groundwaternonitoring at the boiler ash landfann began in February, 1988.Results of this rronitoring were not yet available.

A review of the personnel training records found that they werekept for 3 years and were up-to-date for all rployees with theexception of Mr. nroe Harper wbo had not received a trainingreview in 1987. Mr Harper needs to receive a training review andhave his training record updated.

A review of the inspection logs found that they were up-to-dateand kept in proper order. Hcwever, it is recctrnded that thefollowing additions be included in the inspection logs. Theinspection log for the surface impoundment should includenotations for inspecting the fence and signs. The inspection logfor the less than 90-day container/drum storage building shouldinclude notations for inspecting the conditions of the drums andshould note when no drums are being stored. The inspection logfor the boiler ash landfan should be nore specific and includenotations for inspecting the fence, signs, evidence of releases(fran run-off or wind dispersal) and catinents on general siteconditions.

Following the record review a visual site inspection of thefacility was conducted. The site inspection included the lessthan 90-day container/drum storage building, the facility processarea, the boiler ash landfann, the surface impoundaent and thespray irrigation field.

The less than 90-day container/drum storage building contained 6drums of hazardous waste (U051). Hazardous waste labels wereattached to the drums; hover, no accunnilation dates wererecorded on the drums. The storage building also contained 74drums of non-hazardous waste which is burned in the facility’sboiler.

The next area inspected was the facility process area whichincludes the treatment cylinders, process tanks and the boiler.A concrete pad adjacent to the boiler feed hopper contained drums

0

of non-hazardous waste which is fed into the boiler and burnedalong with scrap wood chips. Prior to October, 1986, this padwas operated as a less than 90-day container/drum storage areafor hazardous waste which was burned in the boiler. There wasno record of this pad having been cleaned-up or decontaminatedafter the facility ceased storing hazardous waste drums on theconcrete pad. This area needs to be closed in accordance withMississippi Hazardous Waste Managtent Regulation (MHWMR)265.111 and 265.114 and the closure procedure documented. Inaddition, there were no records available to document the cleanout or decontamination of the boiler in changing over franburning hazardous waste to burning non—hazardous waste. However,in subsequent conversations and meetings with Mr. Rob nderson(Keystone Environmental Resources, Inc.) and Mr. Pock Clayton(Plant Manager, Koppers Coitany, Inc.) the folling informationconcerning the boiler change over was presented. Koppers stoppedreceiving and stopped burning hazardous waste in the boiler inOctober, 1986. The boiler was shut dcn at 3:00 p.m. on April13, 1987. The boiler fire box was cleaned out and all the firebrick within the fire box was replaced. The ash collectionsystem and the ash collection bins were tied and cleaned out.The boiler started back up burning non-hazardous waste on May 7,1987. In July, 1987, the facility stopped placing ash on theboiler ash landfarm and began disposing of it at a local landfill.

The facility’s Part A listed an area within a concrete wall whichsurrounds the process tanks as an interim status container/drumstorage area. However, Mr. Dave King (Keystone EnvironmentalResources, Inc.) and Mr. Pock Clayton (Plant Manager, KoppersCaany, Inc.) explained that this area was never actively usedbecause of the difficulty in placing and retrieving drums overthe concrete wall which is approximately 3 feet high. Thefacility needs to document that this area was never activelyused, that no spills fran containers/drums occurred, and that thearea was effectively closed by the rDval of anycontainers/drums that were originally placed there.

The boiler ash landfanu is located in the southern portion of thefacility and has not been used since July, 1987. Prior to July,1987, it was operated as a hazardous waste landfill and as suchis subject to the regulations governing landfills (Subpart N ofPart 265 of the Mississippi Hazardous Waste ManagementRegulations - Z4H4R). The boiler ash landfaxm is not managedto control run-on/run-off or the dispersal of the ash by wind.Sar of the ash fran the unit could be seen on a facility roadrunning along the outside of the unit. 1dditionally, the unit issurrounded by a three—strand barbed wire fence which isinadequate security for a landfill. dditional signs are neededand the gate at the northern part of the unit did not have a lockto prevent entry. The unit has one background and threedowngradient ztxznitoring wells.

The surface inoundment is located in the east central portion ofthe facility and is surrounded by a fence on all sides.

C) 0Additional signs are necessary so that they can be seen fran allapproaches. The facility has received an operating permit forthe surface impoundment and will be required to close the surfaceiinpoundnent on or before Novanber 8, 1988. The unit has tobackground and six downgradient ironitoring wells.

The spray irrigation field is located at the northern end of thefacility and consists of six spray irrigation nozzles and issurrounded by a low berm to control run—on/run-off. Access iscontrolled by a three-strand barbed wire fence which is in poorcondition near the sprayfield gate. The fence near the gatehas apparently been knocked down due to the placenent and renovalof material fran a scrap pile which is located within thesprayfield fence. The fence in this area needs to be repairedand it is recarnended that the scrap pile be rextoved. Thenorthern portion of the sprayfield perirreter is bounded by apublic road and a residential area. The fence along the northernperimeter of the sprayfield is inadequate security because ofthe proximity of the public road and residential area. Extrasigns are also needed so that they can be easily seen fran allapproaches. The unit has one background and three downgradientnonitoring wells.

Koppers contends that the spray irrigation field is not aregulated unit and has operated it without having interimstatus. Subsequent to this inspection, an Administrative Orderhas been issued to Koppers requiring thexn to subnit a car?letePart B post-closure permit application for the spray irrigationfield.

10. Conclusions

Koppers is in apparent violation of the following requirextentsof the applicable regulations:

1. NHR Part 262.34 - Accunulation Tine - Koppersoperates a less than 90-day container/drum storagebuilding.’ Six drums of hazardous waste were beingstored at the tine of the inspection. These drumscontained hazardous waste labels but no accuniulationdates were recorded on the labels as required.

2. MHWMR Part 265.14 — Security - The facility hasinadequate fencing surrounding the boiler ashlandfam. Since the boiler ash landfarm is not locatedwithin the operating portion of the facility it needsto have better security to prevent unknowing entry.Additionally, there is no lock on the gate at theboiler ash landfam.

That portion of the fence that extends along thenorthern perirTeter of the spray irrigation field and isadjacent to the public road and residential area isinadequate security to prevent unknowing entry to the

0

unit. Pdditiona1 signs are also needed so that theycan be easily seen fran all approaches to the unit.

3. MHWMR Part 265 Subpart G - Closure arid Post-ClosureCare - The facility has not docunnted the closure ofthe original interim status container storage area(located within the concrete wall that surrounds theprocess tanks). The facility has not closed the lessthan 90-day container/drum storage area that waslocated on the concrete pad adjacent to the boiler feedhopper (this area is presently being used fornon-hazardous storage). The facility has not closedthe spray irrigation field (still being operated) orthe boiler ash landfam.

Subsequent to this inspection PidministrativeOrder 1440-88 has been issued, which contains a closureschedule for the spray irrigation field.

4. MHR Part 265 Subpart N — Landfills — The facility’sboiler ash landfam has been operated as a landfill andtherefore must canply with the landfill requirnts.The facility has not provided run-on/run-off control orneans to control wind dispersal of the ash.

5. Section 3005 Solid Waste Disposal Act - Permit foreatint, Storage, or Disposal of Hazardous Waste -The facility has operated the spray irrigation fieldwithout ever having interim status. The original PartA sutEnitted in 1980 did not include the sprayirrigation field arid the facility has riot sutwitted aPart B permit application to operate this unit.

Subseqent to this inspection, Mministrative Orders1438—88 and 1440-88 have been issued requiring thefacility to sutinit Part B permit applications forboth the spray irrigation field and the boiler ashlandfann.

11. Signed

DMSION OF SOLID WASTE

REwsWEDBY______

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_____

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION IV

4 1988 345 COURTLAND STREETATLANTA, GEORGIA 30365

4WD-RCRA

PkirrMr. Sara 1iabry, ChiefHazardous Waste BranchBureau of Pollution Control $ JL 18 7988Mississippi tpartrnt of Natural Resources Dep. of \atcraJ -P.O. BOX 10385 jeau of ?OUtjøn.Jackson, Mississippi 39209

Re: Koppers Canpany, Inc.MSD 007 027 543Canpli ance Evaluation Inspect ion Report

1ar Mr. flabry:

Enclosed please find the rerenced dowment which discusses violations atthe May 16, 1988, inspection conducted by EPA and MSDNR. Several violationswere fr)und at this facility. Specifically, at issue is the closure of thesprayfield and the ash landfarm and the fact that Kcppers is operating thesprayfield without ever having interim status for this unit. Additionalviolations re found and also need to be addressed. Per the Menorandumof Agreement, MSIDNR has the primary respDnsibility fr)r enforcement. Pleaseadvise us of your intended action.

If you have any questions concernirç this matter, please contact Karen McKinneyat (404) 347—7603.

Sincerely yours,

Allan E. Antley, ChiefWaste Canpliance SectionRCRA Branch

Enclosure

0 0RCRA. SITE INSPECTION

1) Inspection and Author of Report

Karen McKinneyEnvironintal Engineer

2) Facility Information

Koppers Ccrapany, Inc.HSD 007 027 543P.O. Box 160Tie Plant, MS 38960

3) Responsible Official

J.D. (Rock) Clayton, Plant ManagerDave King, Environrrcntal Coordinator — Keystone

4) Inspection Participants

Karen McKinney, USE PADavid Bockelrnann, MSDNRDave King, KeystoneJ.D. (Rock) Clayton, Koppers

5) Date and Time of Inspection

May 16, 1988 — 9:15 a.m. CST

6) pplicable Regulations

Mississippi Hazardous Waste Management Regulations (MHWMR) Sections 262and 265 (adopted by reference and therefore cited herein as 40 CFR).

7) Purpose of Inspection

This inspection was a USEPA Canpliance Evaluation Inspection (CEI) todetermine the facility’s overall con1iance with the applicable interimstatus regulations.

8) Facility Description

The Koppers Tie Plant facility is located abcxit five miles southeastof Grenada, Mississippi. The facility uses creosote and pentachloro—phenol—in—oil in the pressure treatment oE wood products for railroadties, utility poles and pilings. The hazardais wastes produced bythis facility are KOOl, U051, and F027 and consist of bottom sedimentsludge from the treatnent of wastewater fran wood preserving processesthat use crecote and/or pentachlorcphenol (1(001), and waste crecsote(U05l), or certain waste pentachlorcphenol (F027). The regulated wastemanagement units at the facility are a drum storage area, a surfaceimpounduEnt, an ash landfarm, and a sprayfield. The facility has apermit under review by the Mississippi Corrirnission for the operationof the surface iinpoundirent.

—2— 0The surface impoundment is used as a was tewater treatment lagoon. Itis abcut one—half acre in size and has a maximum operating depth of aboutseven feet. The surface impoundment generates KOOl (bottom sedimentsludge from the treatment of wastewaters from wood preserving processesusing crecsote or pentachlorcphenol). The surface impoundment is pre—ceeded by a mechanical oil,4qater separator and flow equalization whichrecaptures product and minimizes the amount of creosote which flowsinto the impoundment and becomes waste. Was tewater from the impoundmentis pumped to a sprayfield for treatment. Kcppers is in the process ofobtaining an operating permit from the State for the impoundment. Thefacility plans to close the impoundment in November 1988.

The sprayfield is located on the north—northwest section of the property.It is about four acres in size and surrounded by a low berm thatcontrols run-on/run-off. The field is covered with non—food chainvegetation. The sprayfield receives wastewater after it has beenpretreated by two separate processes. The production process includestwo oil/water separators which operate in series. The first separatorreceives an oil/water mixture and a flocculation agent. The solidsare removed, pentachlorcphenol and oil are recovered and recycledback to the process before the wastewater passes into a second separator.Here creosote is removed and recycled back to the process.

Effluent from the surface impoundment is periodically pumped to thesprayfield. The frequency of pumping depends upon water levels withinthe surface impoundment and climatic conditions. Spraying does notoccur during rainfall.

Koppers operates a boiler at its facility for the conversion of thermalenergy from wood and various wastes into steam. These wastes includedthe listed hazardous wastes KOOl, U051, and F027. The ash generatedfrom the operation of the boiler was placed on a landfarm until 1987.The landfarm had been used, prior to November 19, 1980, for the disposalof wood treating process wastes which came from old surface impoundmentsthat had been closed. The ash is a listed hazardous waste therebymaking the ash landfarm a regulated land disposal unit. Koppers stoppedburning the hazardous waste in July of 1987. The facility stoppedplacing the ash on the landfarm at that time. The facility still burnsnon—hazardous waste in the boiler which canes from the process areas(cleaning of the treatment cylinders and door pit areas, etc.) anddisposes of the ash at a local landfill.

The facility operates a less than 90—day storage building located inthe process area. Koppers previously had interim status for a storearea located near the holding tanks. This area was used only once andis no longer in use. Stored in the ne.q building are drums containingthe non—hazardous waste which is used in the boiler and hazardous wastewhich is stored until it is shipped off—site.

9) Findings

A record review of the inspection logs, personnel training records,manifests, closure plans, ground water monitoring records, and thecontingency plan was conducted. Records were kept back to 1981.

o -3- 0The inspection logs were kept in proper order. However, additions should

be made to the log for the surface impoundirent inspections to include the

fence and signs. Also, notations should be made into the storage log when

no drums are being stored arid include the condition of the dri.ims on thechecklist. The ash landfarrn log should be more specific and include

coiutents.

The personnel training records were maintained for three years or more.Cily one employee had not had training in 1987, Lionroe Harper who isthe assistant treating supervisor. Mr. Harper needs to have a trainingreview and his records updated.

Manifests, closure plans, and the contingency plan were found to be in

compliance. Financial assurance and liability insurance records were

inspected and found to be in canpliance.

The ground water nonitoring records were reviewed. The records were kept

for three years for the surface impoundment and sprayfield. The ashlandfarm began monitoring in February of 1988.

An inspection of the cperating area and rulated units follced the

record review. The first area looked at was the less than 90—day

storage area. Six drums of hazardous waste (U051) were being stored

at the tine of the inspection. Hazardous waste labels were used on

the drums however no accumulation dates were recorded on the labels.

Also stored in the building were 74 drums containing non—hazardous

waste solids which are I:urned in the boiler.

The next area looked at was the process area which includes thetreatment cylinders, creosote tanks, and the boiler. An area insidethe concrete wall surrounding the creosote tanks used to be the facility’s

old interim storage area. This area was used only once since it became

too difficult to lift the drums over the wall to store and remove them.

Therefore this area must be closed out in accordance with 40 CFR Part

265 Subpart G. Since the facility did not use this area to store

containers, it created a less than 90—day storage area next to theboiler. The hazardous waste was stored on the concrete pad near the

boiler until they fed it into the boiler along with the wood cfiips.The facility still uses the concrete pad to store the non—hazardouswaste until it is ready to burn. There was no record of a clean-upor decontamination of this storage pad after the facility ceasedburning hazardous waste. Additionally, records were not availableto docunent the decontamination of the boiler after the facility

stopped burning hazardous waste. However, Keystone (Koppers’Environnental Division) representative Rob Anderson told DavidBockelmann in a phone conversation after the inspection, that thefacility had cleaned cut the boiler after it ceased burning hazardous

waste. The facility should document the procedures used in the

process of the cleaning of the boiler.

After the process area was seen the ash landfana was inspected. The

ash landfarm is a land disposal unit and is therefore subject to the

landfill regulations (Subpart N of 40 CFR Part 265). The facilityhas no run-on and run—off control for the landfarm. Additionally,

o -4- 0the unit is surrounded by a three—strand barb—wire fence which isinadequate security for a landfill. The fence has a gate at the frontwhich contains no lock to prevent entry. There is no wind dispersioncontrol for the flyash and some of the ash could be seen on the roadsand outside the unit. More signs are needed at the ash landfarm.The facility has not begun closure of the ash landfam. There arefour groundwater nonitoring wells for the ash landfarm.

The surface impoundment is surrounded by a fence on all sides. Signsare posted along the fence, however, there needs to be rrore signsposted. The signs cannot be seen fran all approaches to the impound—rtent. At least two feet of freeboard was maintained. Kcppers is inthe process of receiving an cperating permit frcra MSDNR for thesurface impoundment. There are eight groundwater nonitoring wellsfor the impoundment.

The sprayfield was the last area obeerved at Koppers. The spray—field has four groundwater ronitoring wells. The unit is surroundedby a three-strand barb—wire fence which was in poor condition at thefront entrance to the sprayfield. The fence had been torn down toplace or remove material fran the scrap pile in the sprayfield.Additionally, the fence is inadequate at the north end cE thesprayfield since there is a public road near it along with severalhouses and a school nearby. There also needs to be nore signs postedespecially at the north end where the sprayfield is exposed to thepublic road and houses. There was a lot of vegetation overgrowtharound the sprayfield and fence.

The sprayfield itself consists of six spray nozzles located throughoutthe field. Around the nozzle there is brownish—black sludgy materialon the ground. There is a berm that surrounds the sprayfield forrun-on control.

The facility continues to use the sprayfield although it doss nothave interim status or a caaplete Part B filed with the state.

10) Conclusions

Koppers has violated the follcwing requirements of the applicableregulations:

— 40 CFR Part 262.34 — Accumulation Time — Koppers operates aless than 90—day storage area for its hazardous waste.The drums contain hazardous waste labels but no acaimu—lation dates are recorded as required.

— 40 CFR Part 265.14 — Security — The facility has inadequatefencing around the ash landfarra. Since this unit is notlocated within the qerating portion of the facility itneeds to have better security to prevent unknowing entry.Additionally, there is no lock on the gate at the ashlandfarm.The fence at the northern end of the sprayfield providesinadequate security to prevent unknowing entry to the unit.This is especially directed toward the area next to the publicroad where residential homes and a school are located.

C) -- 03

Additionally, re signs are needed at all units toprevent unknowir and unauthorized entry. Signs recovered by vegetation or nonexistant in sorae areassurrounding the units. Signs need to be placed so theycan be seen from any approach to the unit.

— 40 CFR Part 265 Subpart G — Closure and Post-Closure Care — Thefacility has not closed out the follin; units: the interimcontainer storage area (next to the creosote tanks); theless than 90—day storage area near the boiler (still beingused for non—hazardous waste storage); the ash landfarn;and the sprayfield (still beiixj operated). Additionally,post—closure care will be needed for the sprayfield andash landfarra.

— 40 CFR Part 265 Subpart N — Landfills — Koppers ash landfarra isconsidered a landfill and therefore must comply with thelandfill requirenents. The facility has not provided run—onand run—off control for the unit. Additionally, there isno control for wind dispersal of the ash. The facilityhas also failed to begin closure of the unit.

— Section 3005 Solid Waste Disosal Act — Permits for Treatment,Storage, or Disposal of Hazardous Waste — The facility hasoperated the sprayfield without ever having interim status.The original Part A submitted in 1980 did not include thesprayfield. The facility also has not submitted a Part Bpermit application to operate the regulated unit.

11) Signed

c/ñDate

12) Concurrence

càg7ylfT. Brittain, chiefWest aliance Unit

7/5/rDate

pproval

Allan E. Antley, ChiefWaste Compliance Unit

Karen McKinneyInspector

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cility

.

265.1

5In

spectio

nand

Monito

ring

a)T

heow

nero

ropera

tor

must

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ect

the

facility

for

malfu

nctio

ns

anddete

rio

ratio

n,

opera

tor

erro

rs1

or

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harg

ew

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may

becau

sing

or

lead

tore

lease

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hazard

ou

sw

asteconstitu

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een

viro

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ent

or

ath

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anh

ealth

.

c)T

heow

neror

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tor

mu

stta

ke

rem

edi

al

actio

nupon

the

dete

ctio

no

fm

al

functio

nor

the

dete

riora

tion

of

eq

uip

men

tan

dstru

ctu

res

when

ah

azardis

imm

inen

t.

d)T

heow

ner

or

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tor

mu

stre

cord

in

spectio

ns

inan

insp

ectio

nlo

gan

dm

ust

keep

the

record

sfo

rat

least

thre

eyears

from

he

date

of

insp

ectio

n.

Yes

No

N/A

I

hav

e:

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the

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265.

b)

The

train

ing

pro

gram

must

be

com

pleted

with

insix

month

sof

the

effe

ctiv

edate

of

Part

265.

There

must

be

anannual

revie

wof

the

initia

ltra

inin

gin

(a)ab

ove.

d)

The

ow

ner

or

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tor

must

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tain

record

sof

train

ing.

e)T

rain

ing

record

son

curre

nt

perso

nnel

must

bekept

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clo

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the

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.

265.1

7G

eneral

Req

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ents

for

Ignita

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,R

eactive

or

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astes

The

ow

ner

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must

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pre

cautio

ns

topre

vent

accid

enta

lig

ni

tion

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ignita

ble

or

reac

tive

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b)

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or

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ient

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EV

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265,3

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faci

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andopera

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andpre

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ases

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hazard

ous

waste

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lled

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.4

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PAR

TD

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are

lease

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ous

waste

.

PA

RT

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MA

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CO

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C,

ANDR

EPO

RT

ING

265.7

1(a

)(l—5)

Ifa

facility

receiv

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//

hazard

ous

waste

accom

pan

iedby

am

ani—1/

fest,

the

owner

or

opera

tor

mu

stm

eetth

ere

quire

ments

of26

5.7

1(a

)(l—5)

26531(b

)(l—5)

Ifa

facility

receiv

es,

Vfrom

ara

ilor

wate

rtra

nsporte

r,hazard

ous

waste

which

isacco

mpan

iedby

ash

ippin

gpaper,

the

owner

or

oper—aco

rm

ust

meet

tfere

quire

ments

of

265J1

.

IIn

com

plia

n”’

—Y

esN

otin

comp.

ance

—N

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KE

NT

Not

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able

—N

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TS

Yes

No

N/A

265.7

2(a)

Upon

dis

covey

of

sig

nific

ant

manife

stdisc

repancy

1th

eow

ner

or

opera

tor

must

atte

mpt

tore

concile

the

disc

repancy

with

the

waste

genera

toor

transporte

r.

/b)

Ifa

sig

nific

ant

manife

stdis—

crepan

cyis

not

reso

lved,

the

ow

ner

or

opera

tor

must

notify

the

Dire

cté

r.

1/\265.7

3(b

)T

heow

ner

or

opera

torm

usc

keep

aw

ritten

opera

ting

record

at

the

faci—lity

whic

hm

eetsth

ere

quire

ments

of

265.7

3(b

).

265.7

4(a

)A

llre

cord

sm

ust

be

furn

ished

upon

request

andavaila

ble

at

all

times

for

insp

ectio

nby

the

Dire

cto

ror

EPA

.

a(c)

Aco

py

of

record

sof

waste

dis—posa

llo

catio

ns

andquantitie

sm

ust

besu

bm

itted

toth

eD

irecto

rand

the

Vlo

cal

land

auth

ority

upon

clo

sure

of

the

facility

.

265.75T

heow

neror

opera

tor

must

subm

it/1

anannual

report

toth

eD

irecto

rin

com

plian

cew

ithth

ere

quire

ments

of

265.7

5.

265.76T

here

ceip

tof

any

unm

anife

sted

waste

must

be

reporte

dto

the

Dire

cto

r.

26527

The

owner

or

opera

tor

must

aubm

ita

report

toth

eD

irecto

rif

any

of

the

follo

win

goccur:

a)re

leases,

fires,

explo

sions

S

b)gro

undw

aterconta

min

atio

nc)

facility

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sure

.

i.nco

mpiian

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tin

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mce

No

iiR

EQ

UIR

EtE

NT

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otap)lic

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—N

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TS

Yes

No

N/A

SUB

PAR

TF

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ROU

ND

WA

TERM

6NIT

OR

ING

265.9

0O

wner

or

op

era

tor

mudt

implem

ent

agro

undw

aterm

onito

ring

pro

gram

cap

ab

leo

fd

ete

rmin

ing

the

facility

’sim

pact

onth

equality

of

the

upper

aq

uife

rw

ithin

one

year

of

the

effe

ctiv

edate

of

265.9

0.

/2

65

.91

—2

65

.94

The

ow

ner

and

opera

tor

/m

ust

insta

ll,opera

te,

andm

ain

tain

agro

undw

aterm

on

itorin

gsy

stemw

hich

meets

the

require

ments

of

265b91—

26594.

26

5.9

0(c)

All

of

the

gro

undw

aterm

onitor—in

gre

quire

ments

may

bew

aived

ifth

eo

wn

eror

opera

tor

candem

onstra

teth

at

there

isa

lowpote

ntia

lfo

rm

igra

tion

of

hazard

ous

waste

constitu

ents

from

the

facility

via

the

upperm

ost

aq

uife

rb

elow

the

facility

tow

acir

sup

ply

wells

or

tosu

rface

wate

r.

SUB

PAR

TC

—C

LOSU

RE

ANDPO

ST—C

LOSU

RE

26

5.1

ll

The

owner

or

opera

tor

must

clo

sehis

facility

ina

man

ner

that

1)m

inIm

izesth

eneed

for

futu

rem

ain.

cenan

ce,and

2)conto

la,

min

imizes,

or

elIm

inate

spost—

closu

reesc

ape

of

hazard

ous

waste

.

265

.112(a)

The

owner

or

opera

tor

mu

sthav

ea

writte

nclo

sure

pla

non

the

effe

ctiv

ed

ate

of

Part

26

5.

i.iiL

uIH

L1.L

dI1

Ce.

—

Not

inco

msn

ceN

oR

EQ

UIR

EtE

NT

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apilic

able

—N

AC

0fl1EN

TS

•265.1

12(a)

Continued—

—

TUe

clo

sure

pla

nm

.stin

clu

de:

1)A

desc

riptio

nof

howand

when

the

facility

will

bepartia

llyclo

sed

1if

applic

able

,and

ultim

ate

lyclo

sed.

2)A

nestim

ate

of

the

maxim

umin

ven

tory

of

wastes

insto

rage

or

treatm

ent

at

anygiv

entim

e.

3)S

teps

todeco

ntam

inate

facility

equip

men

t.

4)A

sched

ule

for

final

clo

sure

which

must

inclu

de,

asa

minim

um,

antic

ipated

date

sw

henw

astesw

illno

longer

bere

ceiv

ed,

antic

ipate

ddate

for

com

ple

tion

of

final

clo

sure

,and

interv

en—

•in

gm

ilesto

ne

date

s.

265.113(a)

Clo

sure

must

bein

itiate

dw

ithin

90day

safte

rre

ceiv

ing

the.

final

volume

of

hazard

ous

waste

s.

(b)

The

owner

or

opera

tor

must

com

plete

clo

sure

activ

ities

with

insix

month

safte

rre

ceiv

ing

the

final

volume

of

waste

s.

265.114U

ponco

mpletio

nof

clo

sure

,all

equip

men

tand

structu

res

must

bepro

perly

disp

osed

of

or

deco

ntam

inated

.

265.115T

heow

neror

opera

tor

andan

inde

pen

den

cre

gis

tere

dpro

fessio

nal

engi

neer

must

certify

chat

the

facility

has

been

clo

sed

inaccord

ance

with

the

appro

ved

clo

sure

pla

n.

‘fesN

oN

/A

I

I;

7/II/

VV

/

/•

-•

•--

—-

-

-

REQ

UIR

EttENT

-265.1

17(a)

Post

clo

sure

,care

must

consist

of

at

least:

1)G

roundw

aterm

onito

ring

2)M

ainten

ance

of

the

conta

min

ant

sys

tern..

The

ow

ner

or

opera

tor

must

hav

ea

post—

closu

repla

non

the

effe

ctiv

edate

of

Part

265and

itm

ust

inclu

de:

1)G

roundw

aterm

onito

ring

activ

ities

,and

frequency.

I’

2)M

ainten

ance

activ

ities

andfre

qi

cie

sto

ensu

reth

ein

tegrity

of

the

cap,

final

cover,

or

oth

er

conta

inm

ent

stru

ctu

res,

andfu

nctio

ns

of

the

faci

lities

monito

ring

equip

men

t.

265.1

19

With

in90

day

safte

rclo

sure

,th

eow

neror

opera

tor

must

subm

ita

surv

eypla

tof

the

facility

.

265.120T

heow

ner

or

opera

tor

must

record

anotic

eon

the

deed

that

the

land

has

been

used

tom

anagehazard

ous

wasiL

SUB

PAR

TH

—FIN

AN

CIA

LR

EQU

IREM

ENTS

26

5.1

42(a

)T

heow

ner

or

opera

tor

must

dev

elop

andm

ain

tain

acurre

nt

esc

imat

of

clo

sure

andpost—

closu

recosts

.

SUB

PAR

TI

—O

THER

FAC

ILIT

YSTA

ND

AR

DS

265.1

70

—265.1

72

The

conta

iner

must

becom

patib

lew

ithth

ew

asteto

be

/7

/.•

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RE

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26

5.1

73

Conta

iners

hold

ing

hazard

ous

waste

must

bekept

clo

s6d

andm

ust

not

be

op

ened

,h

an

dle

d,

or

store

din

am

anner

wh

ichm

aycau

sea

ruptu

reor

leak.

265.1

74

Areas

wh

ereconta

iners

are

store

dm

ust

bein

specte

dw

eekly

.

265.176C

onta

iners

hold

ing

ignita

ble

or

reactiv

ew

astem

ust

be

locate

dat

least

15m

ete

rsfro

mth

efa

cility

’spro

perty

line.

26

5.1

77

(a)In

co

mp

atib

lew

aste

sm

ust

not

bep

laced

inth

esam

eco

nta

iner.

(b)

Asto

rag

eco

nta

iner

hold

ing

ahazard

ous

waste

that

isin

co

mp

atib

lew

ithan

yw

asteor

oth

er

mate

rials

store

nearb

ym

ust

be

separa

ted

or

pro

tecte

dfro

mth

eoth

er

mate

rials.

Not

ap

lile-

NA

Yes

No

N/A

//I

V

/V/V

COM

MEN

TS

/t(

:.

SUB

PAR

TJ

—TA

NK

S

26

5.1

92

(b)

Hazard

ou

sw

astem

ust

be

pla

ced

ina

tank

ifth

eyco

uld

cause

the

tan

ko

rits

liner

tole

ak.

(c)U

nco

vered

tanks

mu

sthavea

least

two

feet

of

freeboard

un

less

oth

er

conta

inm

ent

stru

ctu

res,

ad

ram

ae

co

ntro

lsy

stem

,o

roth

er

div

ersio

nstru

ctu

res

with

acapacity

that

equals

or

exceed

sth

ev

olu

me

of

the

top

two

feet

of

the

tank.

(d)

Tan

ks

wh

ichh

ave

aco

ntin

uous

feedsy

stemm

ust

beeq

uip

ped

with

am

eansto

stop

the

inflo

w.

/

UI.

LII

CIJ

UIjJ

LL

aIIL

.C—

Ill.?

REQ

UIR

EM1

Not

ap1ic

ab

—N

ACO

MM

ENTS

Yes

No

N/A

265.193W

astean

aly

sism

ust

be

con

du

ctedp

ursu

an

tto

265.1

3’,

and265.1

93

(a)

265.1

94

Tan

ks

must

be

insp

ecte

din

accor—d

ance

with

265.1

94.

265.

197A

tclo

sure

,all

hazard

ous

waste

andh

azardo

us

waste

resid

ues

must

berem

oved

from

the

tan

ks.

265.1

98

Ignita

ble

or

reactiv

ew

astesh

oul

no

tbe

pla

ced

ina

tank

unle

ss265.

198is

com

plied

with

.

26

5.1

99

Inco

mp

atib

lew

aste

sm

ust

not

be

pla

ced

inth

esam

etan

ku

nle

ss2

65.

176is

com

plied

with

.

SUB

PAR

TK

—SU

RFA

CE

IMPO

UN

DM

ENTS

265.2

22

Must

main

tain

at

least

two

feet

Jo

ffre

eboard

.

26

5.2

23

Earth

en

dik

es

must

hav

eprocec—

tive

co

ver.

/2

65

.22

5M

ustc

on

du

ct

waste

an

aly

ses

andtr

ial

tests

inaccord

ance

with

26

5.

225.

7’265.2

26(1

)M

ustin

sp

et

the

freeboard

Vle

vel

at

least

once

eachopera

ting

day

.(2)

Must

insp

ect

the

surfa

ce

im—

poundm

ent

at

least

on

cea

week

tode—

tect

any

leak

s,d

ete

riora

tion

,o

rfa

ilure

.

265.228T

hesu

rface

impoundm

entm

ust

clo

sin

accord

ance

with

265.

228.

SUB

PAR

TL

—W

ASTE

PIL

ES

4

26

5.2

51

Aw

astepile

must

bepro

tecte

dand

managed

toco

ntro

lw

ind

dis

pers

al.

265.2

53

With

inone

yeara

fter

the

effe

ctiv

ed

ate

of

the

reg

ula

tion

sble

ach

ate

or

run—off

from

ap

ilem

ust

beco

ntro

lled

pu

rsuan

tto

26

52

53

.

26

5.2

56

Ignita

ble

or

reactiv

ew

astem

ust

not

beplaced

Ina

waste

site

unle

ss2

65

.25

6is

com

plied

with

.

265.2

57

The

require

ments

of

26

5.2

57

for

inco

mp

atible

wastes

must

beco

mp

liedw

ith.

SUB

PAR

TM

-LA

ND

TREA

TMEN

T

265

.272(a)

Hazard

ous

waste

must

not

bepla

ced

aa

land

treatm

ent

facility

un

less

itcan

bem

adele

ssh

azard

ou

sor

no

n—

hazard

ou

s.

(b)

Run—

onm

ust

bediv

erte

daw

ayfro

moth

er

activ

ep

ortio

ns

aso

fone

year

afte

rth

eeffe

ctiv

edate

of

Part

265.

-

-N

AN

oN

/A

II

-ffi-

_,I

—/

C3

tI

11

“7

L/

4N

ot

Yes

•R

EQU

1REt

I

265.2

29

Ignita

ble

or

reactiv

ew

astem

usta..t

bep

laced

ina

urfa

ce

imp

ou

nd

men

tur.le

ss265.2

29

is’co

mplied

with

.

265.230In

com

patib

lew

aste

sm

ust

no

tbe

pla

ced

inth

esam

esu

rface

impoundm

ent

unle

ss265.1

7(b

)is

com

plied

with

.

COM

MEN

TS

26

5.2

52

An

ow

ner

or

op

era

tor

waste

analy

ses

un

less

the

meets

the

exem

ptio

ns

of

must

conduct

facility

26

5.2

52

.I;

///

/1/

I

INO

C111

CO

mp

.I.laflC

eL

W

REQ

U1R

Ehi.dTN

otap

lica

NACO

MM

ENTS

II

_____

No

N/A

•1

265.272—

—C

on

tinu

edF

/7C

c)R

un—off

froii

activ

ep

ortio

ns

must

beco

llecte

das

of

oneyear

afte

rth

eeffe

ctiv

ed

ate

of

Part

265.

/

265.2

73

Waste

an

aly

ses

must

beco

ndu

cted1/

pu

rsuan

tto

265.2

73.

265.2

76(a)

An

owner

or

op

era

tor

mu

stnociy

/th

eS

tate

Dire

cto

rw

ithin

60day

safte

i1’

the

effe

ctiv

edate

of

Part

265if

foo

dch

aincro

ps

aregrow

non

the

land

treatm

ent

facility

.*

(b)

Food

chain

crops

must

no

tbe

grown

onth

etre

ate

dare

ao

fa

hazard—V’

ousw

astelan

dtre

atm

ent

facility

un

less

265.2

76(b

)is

com

plied

with

.

•(c)

Food

chain

crops

must

no

tbe

grown

ona

land

treatm

ent

facility

receiv

ing

waste

chat

conta

ins

cadmium

unle

ss2

65

.27

6(c)

isco

mplied

with

.

Ub‘-

265.278T

heow

neror

opera

tor

must

hav

eIn

writin

gand

must

implem

ent

anun

satu

rate

dzone

mo

nito

ring

pla

npursu

ant

to265.2

78.

26

5.2

79

The

owner

or

opera

tor

must

keep

/reco

rds

of

the

applic

atio

ndate

s,app—

licatio

nra

tes,

qu

an

tities,

andlo

ca

tion

of

eachhazard

ous

waste

placed

Ina

faéilic

y.

265.280A

land

treatm

ent

facility

mu

stm

eetth

eclo

sure

andpost—

closu

rere

quirem

ents

of

265.2

80.

•-

—_—

•_q.

..

REQ

UIR

EKEN

T

‘I

265.2

81

Ignita

ble

or

ractiv

ew

astem

ust

not

bepla

ced

ina

land

treatm

en

tfaci—

lityunle

ss265.2

81

isco

mplied

with

.

265.

2112Iw

uiip

iI

IhIp

wsiaa

Lt’n

iiiuI

iiiit

hi’p

lucu

dIn

thu

ucuiclu

nd

LruutiiiunL

urc

uunle

ss265.1

7(b

)is

com

plied

with

.

No

tin

comp

ince

—N

oN

ot

ap1ic

ao..e

—N

AY

esN

oN

/AC

OM

NEN

TS

SUB

PAR

TN

-L

AN

DFIL

LS

26

5.3

02

(a)

Run—

onm

ust

bediv

erte

daw

ayfrom

the

activ

eportio

ns

with

inone

yir

afte

rth

eeffe

ctiv

edate

of

Part

265.(b

)R

un—off

from

activ

eportio

ns

must

becolle

cte

dw

ithin

oneyear

afte

the

effe

ctiv

edate

of

Part

265.

(d)

Must

contro

lw

inddis

pers

al.

26

5.3

09

The

ow

ner

or

op

era

tor

must

meet

the

surv

eyin

gand

record

keepin

gre

quire

ments

of

26

5.3

09

.

265.3

10

Ala

ndfill

must

com

ply

with

clo

sure

andpost—

closu

rere

qu

irem

en

tsof

265.3

10.

265.312Ig

nita

ble

or

reactiv

ew

astem

ust

not

bepla

ced

ina

lan

dfill,

unle

ss265.3

12

isco

mplied

with

.

26531,3In

com

patib

lew

aste

sm

ust

no

tbe

pla

ced

ina

landfill

un

less

265.

17

(b)

isco

mp

liedw

ith.

265.3

14

Bulk

or

non—

contain

erizedliq

uid

waste

,w

asteco

nta

inin

gfre

e—

liquid

s,or

co

nta

iners

ho

ldin

gliq

uid

waste

should

not

bepliT

ed

ina

landfill

unle

ssth

ere

qu

irem

en

tso

f2

65

.31

4

/

//

/

(L

,

‘V‘V//

UiR

ltFI

265.315(1

)E

mpty

co

nta

iners

mu

stbe

re—ducedin

volu

me

aso

fone

year

afte

rth

eeffe

ctiv

edate

oP

art

265.

SUB

PAR

T0

—IN

CIN

ER

AT

OR

S

26

5.3

43

Must

be

at

stead

ysta

teconditio

ns

befo

read

din

gh

azardo

us

waste

.

26

5.3

45

Waste

an

aly

ses

must

be

con

du

ctedpursu

ant

to265.3

45.

(—N

265.3

47

Mo

nito

ring

andin

spectio

ns

must

\.

beco

nducted

asdelin

eate

din

265.3

“26

5.3

51

Ac

clo

sure

the

owner

or

opera

tor

must

remo

ve

all

hazard

ou

sw

astean

dh

azardo

us

waste

resid

ues.

SUB

PAR

TP

-TH

ERM

AL

TREA

TMEN

T

.265.3

73

Must

be

at

stead

ysta

teconditio

nbefo

read

din

gh

azard

ou

sw

aste

s.

265.375W

asteanaly

ses

must

be

con

du

ctedpursu

ant

to265.3

75.

7_—\265.377

Monito

ring

andin

spectio

ns

must

be

con

du

ctedas

delin

eate

din

265.

377.

26

5.3

01

ACclo

sure

,th

eo

wn

ero

ro

pera

tor

must

remo

ve

all

hazard

ou

sw

astere

sidu

es..

265.382O

penburn

ing

of

hazard

ous

waste

isp

roh

ibite

dexcept

for

the

op

enburn

ing

and

deto

natio

no

fw

aste

explo

sives

,licab

l—

NA

__

__

__

N/A

/

Not

apY

esN

oCO

MM

ENTS

/

RE

QIJIR

Ef

_________________________________

Not

nplic

ab’

—N

ACO

MM

ENTS

Yes

No

N/A

SUB

PAR

TQ

—C

HE

MIC

AL

,PH

YSIC

AL

.A

ND

BIO

LO

GI

CAL

TREA

TMEN

T.

265.4

01(a)

Must

com

ply

with

265.

.17(b

)

(b)

Hazard

ous

waste

must

not

be

pla

ced

inth

etr

eatm

ent

process

or

equip

ment

ifany

failu

re

of,

equip

ment

or

the

process

would

occur.’

(c)

Acontin

uously

—fe

dprocess

must

be

equip

ped

with

am

eans

tosto

pth

ein

flo

w.

265.4

02

Waste

analy

ses

and

trial

tests

must

be

conducte

dpursuant

to265.

402.

265.4

03

Inspectio

ns

must

be

made

pursuant

to265.4

03.

265.4

04

At

clo

sure,

all

hazard

ous

waste

and

hazard

ous

waste

resid

ues

must

be

rem

oved.

265.4

05

Ignita

ble

or

reactiv

ew

aste

must

not

be

pla

ced

ina

treatm

ent

process

unle

ss

265.4

05

iscom

plie

dw

ith.

/2654O

6In

com

patib

lew

aste

sm

ust

not

7be

pla

ced

inth

esa

me

treatm

ent

pro

ces

LI’unle

ss

265a7(b

)is

com

plie

dw

ith.

SUB

PAR

TR

-U

ND

ER

GR

OU

ND

INJE

CT

ION

,.,

/2ó5.4

30(a)

underg

round

inje

ctio

nof

haz

ard

ous

waste

isnot

subje

ct

toth

eclo

sure

and

post—

clo

sure

or

fin

ancia

lrequir

em

ents

of

Part

265.

,U

nder

gro

und

inje

ctio

nis

subje

ct

toth

eoth

er

requir

em

en

of

Part

265.

Ocher

qu

estio

ns

or

stan

dard

s.•

H

kreth

ereany

oth

er

genera

5tra

nsp

ortin

gV

[I

their

waste

toth

ishazard

ous

waste

man

ag

em

entfa

cility

?

C-

:1;

I

4

_..I

‘eS

i.’A.

DB: ir

0 0a. Koppers will suhuit a roore ãetailed schedule of events

concerning the switch-over frcm burning hazardous tonon-hazardous waste in the ioiler.

0 QSCHEDULE FOR WASTEWATER

PRETREATMENT SYSTEMKOPPERS COMPANY, INC.TREATED WOOD PRODUCTSGRENADA, MISSISSIPPI

Begin Construction July 23, 1988

Finish Construction October 13, 1988

Process Start—up October 19, 1988(cease using surface impoundment)

Full Operation November 2, 1988

C

MEETING AGENDA

Koppers Company, Inc.

June 15, 1988

1.) Surface Impoundment Permit.

a.) Submittal of schedule for completion of pretreatmentsystem and hook—up to POTW.

b.) Submittal of updated schedule for closure.

c.) Contingency plan for closure if pretreatment systemis not permitted or completed by November 8, 1988.

2. Boiler Ash Landfarm.

a.) Review groundwater sampling results.

b.) Closure & Post—Closure requirements.

1) Submittal of updated Part A.

2) Submittal of Part B.

3. Spray Irrigation Field

a.) Review existing data.

b.) Closure & Post—Closure requirements.

1) Submittal of updated Part A

2) Submittal of Part B

4. Unnamed Ditch

a.) Beiiewr existing data.

b.) Discuss interim measures for remediating contamination.

5. RFA/RFI for Solid Waste Management Units.

a.) EPA letter and comments

6. Boiler & Boiler ash

4-_n EXHIBIT 1

KEYSTONEENVIRONMENTAL RESOURCES, INC.

Interoffice Correspondence

To J. D. Clayton From D. L. King

Location Grenada, ‘S Location North Little Rock

Subject Waste Profile — CWM, Inc Date June 1?, 1983

Attached is a completed Waste Profile Sheet C Chemical Waste N’anagenient, mc)for the few drums of 1-lazartlous Waste (1J051) presently stored at the Grenadaplant. Please review the attached information and proceed as follows:

1) Collect a representative sample (one quart) from these drums andcomplete the Sample Certification attached to the back of theProfile Sheet, and siwi Profile Sheet at the bottom of the firsbpage.

2) Send sample CUPS), and Waste Profile Sheet to: Chemical WasteManagement, Inc. , Emelle Facility, P. 0. Box 55, Emelle, AL 35459

LI’ you have any questions, please call Rob or me.

Davia King

IJLK/dlk

cc: Ii. Anderson

ChemiolNWaste Managemen3nc.GENERALS WASTE MATERIAL PROFIIE(ET

PLEASE PRINT IN INK OR TYPE Eflto. 12pIIch.

F .1 5 3 9 7 7.Waste Profile Sheet Code

CWM Location of Original: _.

.. (SHAOED AREAS FOR CWM USE ONLY) CWM Sales Rep. #:- .--iI---’--- ,_rfl,” —

______________________________

Id C ..2,GeneratorUSEPAl?2Q23

___________

4. Generator State ID:

— — 5. Zip Code: 3 D

__________________

7 Title: ,1’/”r. 8..Phone:(’5J)4... -,c

A. GENERAL INFORMATION1 Gonerator Name: _1<.ç4’‘ .

3. Facility Address: &

—lTh ( L

6. TechnIcal Contact: . 0 I’C-n- p -. _;%.

——-,,——-S -. S

a.,.._,.uaa....w,w.a,aa_a__a-VUJ...sr Vg — —

B. MAIL CHEMICAL WASTE MANAGEMENT, INC. INVOICES TO 1. GeneratIng Facility (A, above), or2. Company Name: .• 3. Phone: ( ) - -

4. Address: - -.- ..

.. .. . .- .6. Zip Code:_I____ ... i.-.. S———

—— ——S —-

C. ‘I. NAMEOFWASTE S.... R.k—‘---- :±

2. PROCESS GENERATING WASTE . S ic.. i’,’u

3. Is this waste a Dioxin listed waste as defined in 40 CFR 261.31 (e.g., F020, F021, F022. F023, F026, F027, or F028)?C Yes ‘No if yes, DO NOT COMPLETE this form, Contact your Chemical Waste Management, Inc. sales representative forassistance.

_s &r .-. -- -: -.-.. ..- - .__S_—__ .-- -. -_

D. PHYSICAL CHARACTERISTICS OF WASTE1. Color: 2. Does the waste have a 3. PhysIcal State @ 70°F: 4, Layers: 5. SpecifIc Gravity: 6. Free Liquids:

1) r I. strong incidental odor? $ Solid C Semi-Solid C Multilayered 0 Yes NoNo C Yes (known, C Liquid C Powder C Bi-layereci Range: Volume:

.

- describe: ... Other: Tngle Phased .

--

- -%

7.pH: Q2 0>2-4 04-7 07 07-10 010- <12,5 012.5 ERange ‘p.. ONA

8.LiquidFlashPoint: 0<73°F C 73-99°F 0 100-139°F C 140-199°F D 200°F None 0 Closed Cup QpenCup

E. CHEMICAL COMPOSITION — RANGE F. METALS Indicate if this waste contains any of‘I, MIN, - MAX. the following:.. .CL.2_6’ —- / . - % 1. C EP TOX/TCLP or 2. Total

-1(’, L)j 10 ‘i Q. % METAL LESS THAN or ACTUAL. .. - % (PartsPerMllllon)

.,..______ - - - % Arsenic 0< 5 < 500 -.

.- - % Barium 0<ioo-.—— ,. - -. % Cadmium 0< 1 < 100

-.-- - -, % ChromIum 0< 5U... .. -—-- -. —- -- 0/ Lead C < 5 ‘< 500 —

.. --- - % Mercury 0< 0.2 < 20• - % Selenium 0< 1 < 100.__.— . - % Silver 0< 5•______ - % Chromium-Hex 0< 5 J< 500

Please note: The chemical composition total In the maximum Copper 0< 5column must be greater than or equal to 100%, TOTAL: % Nickel 0< 5 < 1342. Indicate if this waste contains any of the following; Thallium 0< 5 0< 130

NONE or LESS THAN or ACTUAL Zinc 0< 5PCE3’s ..L < 50 ppm -.-. — ppm 0<Cyanides 1 < 50 ppm -. — ppm 0<Phenolics C < 50 ppm ppm 0<Sulfldes < Soppm

...r, I

r1.V—2E.—8 FI 11 :4 KCIF’FER$ HLR P.04

GENERATOR’S MATERiAL PROFILE QET (Continued)

I H 53977Waste Profile Sheet Code

_...._ .LL,.... ...____

—— .• —. .. ——

G. OTHER HAZARDOUS CHARACTERISTICS1, Is this waste a listed solvent waste as defined by 40 CFR 261.31 (FOOl, F002, F003, F004, or F005)? C Yes No2. Does this waste Contain greater than 1000 ppm total hatogenated organic compounds? C Yes No3. Indicate if this waste Is any of the following:

C RORA Reactive C RadioactiveC Water Reactive C EtiologicalU Explosive U Pesticide Manufacturing WasteC Shock Sensitive C OtherPyrophoric None of the above - -

--.- I

K. COMPLETE ONLY FOR WASTES INTENDED I. OPTIONAL — RECLAMATION, FUELS, OR INCINERATIONFOR FUELS or INCINERATION PARAMETERS Provide if InfOrmation Is available.Range

LESS THAN or ACTUAL 1. Heat Value (BTU/lb): -. 2. Water:.Beryllium C < 5000 ppm ppm 3. Viscosity (cps):

. @ C °F 0 100°F C 1SOoFPotassium C < 5000 ppm - ppm 4. Ash:

- % 5. Settleable solids:Sodium C < 5000 ppm ppm 6. Vapor Pressure @ STP (mm/Hg):..

--Tots) Bromine C 2 %... 7, Is this waste a pumpable liquid? C Yes C NoTotal Chlorine C < 36 % Type of pump?

Total Fluorine C I % 8. Can thIs waste be heated to Improve flow? C Yes C NoTotal Sulfur. 9. Is this waste soluble In water? C Yes U No

10. Particle size: Will the solid portion of this waste pass througha 1/8 inch screen? C Yes C No

.--- .-.

.... .. . --. II_ ..:

J. TRANSPORTATION INFORMATION- j1, is this a DOT Hazardous Material? Yes C No 2. Anticipated Annual Volume/Units: .

‘ 03. Proper Shipping Name: g . . .c VV’t S +G. S’L3 (, ,

...

/-4 Hazard Class: .— 0 tr’ — 1.

... 5. LD, #; MP .9 1 i?6. AdditIonal DescriptIon; ( ..‘. ‘ ° t

..

7, Method of Shipment: C Bulk Liquid C Bulk Solid Orum (Type/Size): /- Other:8. CEPCLA Reportable Quantity (RO): — I ..

-. 9. RO Units (tb/kg); i I b-—

10. USEPA Hazardous Waste? EYes C No 11. USEPA Hazardous Waste Number(s): U. $ I12, Slate Hazardous Waste? ‘Yes C No 13. State Hazardous Waste Number(s); LiLcs_5 /

-

K. SPECIAL HANDLING INFORMATION . .-- /1S

- 4 .: Iç

.

.... C AddItional Page(s) Attached

—- ..--. r11. •—L._..__.. L. - —. - —. -.L. GENERATOR CERTIFICATION I hereby certify that all Information submitted in this and all attached documents contains true andaccurate descriptions of this waste material, and all relevant Information regarding known or suspected hazards in the possession ofthe generator has been disclosed.

-

... 2.Signature Title

__________

-. 4.__.Name (Type or Print) Date...--,.—-—-.—

.j__ J*LL.... ——Side2of2Form CWM-6000 1987 Chemical Waste Management, Inc.

P05I’

flSY—&—E13 FII 1 146 KOPPERS NLR

Chemical WaittManagement, Inc.P.O. Box 55Emelle, Al

Hail T!

1A ,

‘Technical Contadt:

Your Sample, Profi1ghi4er14Ath-M597,7, was receivedOn 06/24/88 at ouzj4boratory. ,YØUay expect a disposal decision withifrj’two weeks ótNhe receipt date.Please refer to our’fll[;Hwober Be-176-12 as well athe Waste Profile Shea (WE’S) humber when makinginquiries. Thank you

35459I

p. 3Ø.tog ±40 “j.

Grexda He

I

8ERVECI PROVIDEDEMLd’ oIPaSA FA1it

‘cOPPERS COMPANYPRO. BOX. 160ti. PLANt ROAR

IVZG€ QATE REFENENCt NO./OESC

NLRI‘li’l9

‘1f’q aI II’ r •. ItI

£11 r:I j IIII•

1bE UPON RECEIPT

47 1<OPFERSFRI 11

:;: ;,:.QHEMIAL YIASTE MANAMtNT, INCEMELLE FACILiTYEMaLi.E AL 35’159

III I.

RENAOA

•1’

INITZAL.t F.PfJ# OR CONTRACTS 0

RAT

It

S15es6 ‘

IiShft9bQ

•.:

UN UANfITY AMOUNT

MAR’H53911hOG 5O.oo5O,OG *s

A ioft4P 0 Box 10028SATLANTA

IAX(OISP TAX’Ffl’ ?AV(i..—.•——

PLEASE PA4iTHIS AMOUNt

SOti)NBHdV

tS9Ot.9flS(sa1:NtAJ

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June 10, 1988 CERTIFIED MAILReturn ReceiptRequested

Dear Mr. Hardage:

Mr. James HardageMississippi Department of NaturalResourcesBureau of Pollution Control2380 HGW 80 WestJackson, MI 39204

Re: Koppers Company, Inc.Grenada, Mississippi#MSD 007027543

I have enclosed a copy of a RCRA closure plan for the sprayirrigation system at the referenced plant. Please be advisedthat Koppers Company, Inc. continues to take the position thatspray irrigation fields at wood treating plants are not regulatedhazardous waste units under the Resource Conservation andRecovery Act, as amended (“RCRA”), and similar state statutes.Although Koppers is submitting this plan which addresses thesprayfield, we expressly reserve all rights to contest theclassification of the sprayfield as a RCRA unit. This submissionshall not be construed, or deemed to be, an admission by Koppersthat the referenced sprayfield is subject to RCRA.

Please feel free to call me if you have any questions or commentsconcerning this closure plan.

Yours truly,

/ ; ,jZd,i(

Robert J. AndersonStaff Program ManagerKoppers Treated Wood Products

DIRECT DIAL #412—227—2683

RJA / crEnclosure

cc: J. BatchelderJ. D. ClaytonMC Central FilesJ. Blundon (w/o enclosure)

,.•

—

0\YSTONE

EN1RONMENTAI RESOURCES, INC.

Phone 412/227 2694 436 Seventh Avenue, Suite 1940 Pittsburgh, PA 15219. t

0

CLOSURE PLANTREATED WASTEWATER SPRAYFIELD

KOPPERS COMPANY, INC.GRENADA, MISSISSIPPI

I. FACILITY/CONTACT INFORMATION

OWNER/OPERATORS NAME: Koppers Company, Inc.

EPA FACILITY ID#: MSD007027543

ADDRESS: P.O. Box 160Grenada, MS 38960

PHONE NUMBER: (601) 226-4584

CONTACTS:

Koppers Grenada, Mississippi Plant Contacts

J. D. Clayton, Plant Manager(601) 226—4584

Keystone Environmental Resources Department Contacts

Robert J. Anderson, Staff Program Manager(412) 227—2683

II. GENERAL

This closure plan is being submitted in accordance with U.S.EPA and applicable state regulations. Koppers Company, Inc.takesthe,position that spray irrigation fields at woodtreating plants are not regulated hazardous waste unitsunder the Resource Conservation and Recovery Act, as amended(“RCRA”), and similar state statutes. Although Koppers is.submitting this plan, which addressed the sprayfield at theplant, we expressly reserve all rights to contest theclassification of the sprayfield as a RCRA unit. Thissubmission shall not be construed, or deemed to be, anadmission by Koppers that the sprayfield is subject to RCRA.

III. BACKGROUND INFORMATION CONCERNING THE SPRAYFIELD

The sprayfield covers an area of approximately 6 acres, andis vegetated with natural grasses. (See Attachment (1) forlocation). Historically, the sprayfield was used as a finaltreatment step for pretreated wastewater; hazardous wastewas never applied to the sprayfield. The sprayfield waslisted as a hazardous waste unit handling KOOl sludge as aprotective filing as part of Koppers’ Part B permit

0 0application at the direction of U.S. EPA. As a result, theconstituents of interest are those listed in 40CFR261,Appendix VII, for 1(001 hazardous waste.

IV. RATIONALE FOR CLOSURE OF THE SPRAYFIELD

Because the sprayfield was operated to biodegrade anyremaining organic constituents in pretreated wastewater, anddid not receive hazardous wastes p Se, the closure processwill entail ceasing use of the sprayfield and allowingnatural biodegradation to reduce concentrations of residualorganic constituents to levels below levels of human healthor environmental concern, pursuant to 53FR9944. Theachievement of this goal will demonstrate that clean closurehas been accomplished.

V. METHOD OF CLOSURE

A. Following surface impoundment closure, use of thesprayfield will be discontinued.

B. A source of potable water will be connected to thespray irrigation system, and the sprayfield will beoperated for eight hours to flush any residualwastewater from the distribution lines and spray heads.

C. The spray irrigation system will be disassembled.

D. The sprayfield will be fertilized as necessary andmowed periodically to promote vegetative growth andbiodegradation of residual organic constituents. Ifnecessary, the field will be plowed and disced tofurther promote biodegradation.

E. After 180 days of operation, soil samples will becollected from 0 to 1.5 feet in depth at four locationswithin, the sprayfield. These samples will be analyzedfor Appendix VII KOOl constituents following SW—846methods. Results will be evaluated to determine if1(001 constituents are present at or above levels ofhuman health or environmental concern. This evaluationwill be presented as part of the engineer’scertification of closure. In the event that cleanclosure cannot be certified at that time, Koppers willsubmit an amended closure plan specifying either1). continued activities necessary to accomplish cleanclosure, or 2). activities necessary for closure withwaste constituents in place.

VI. DECONTAMINATION AND SAFETY PROCEDURES

A. All workers shall observe the safety procedures forhandling 1(001 hazardous waste as presented in theplant’s Contingency Plan and Personnel Training

—2—

0 0documentation, as included in the Part B permitapplication, and in accordance with the applicableregulations. At a minimum, workers will wearcoveralls, gloves, and boots. Due to the method ofclosure, no activities requiring equipmentdecontamination will be conducted.

VII. DOCUMENTATION

Certification of closure will be submitted to the state andU.S. EPA by Koppers and the state-registered professionalengineer within 60 days of conmpletion of closure.Certification will include a report of the findings from thesubsoil quality investigation.

VIII. SCHEDULE

A. Schedules of closure activities and related activitiesare detailed in Attachment (2). Attachment (2)includes in the schedule the final closure of thesurface impoundment system; sprayfield closure cannotbe initiated until this activity is completed.

—3--

0 QIX. CLOSURE COST ESTIMATE

1. Potable water connection,labor and materials

2. Flush irrigation system]. day @ $200

3. Dismantle irrigation system;30 man—days @ $200

4. Fertilize and periodic mowing

5. Soil sampling; 1 man—day @ $300

6. Soil analysis; 4 @ $750

7. Data evaluation; 16 hrs @ $60

8. Engineer’s certification; 16 hrs @ $100

Subtotal

Administration Costs (10%)

Contingency Costs (10%)

TOTAL ESTIMATED COST

$ 400

200

6,000

400

300

3,000

960

1,600

$12,860

1,290

1,290

$15,440

—4—

i-I

(1)

0 CATTACHMENT (2)

SPRAYFIELD CLOSURE SCHEDULE

Activity Completion Day

Completion of Impoundment Closure -0-

Flush irrigation system with potable water + 10

Dismantle irrigation system + 30Fertilize/Mow periodically +179Sample soil +180

Receive analytical results +240

Certify closure +300

—5—

— CSJ4 - -

,2 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION IV

345 COURTLAND STREET

)N 0 0 1G ATLANTA, GEORGIA 30365

4WD—RCRA

Mr. Sam Mabry, DirectorHazardous Waste DivisionBureau of Ekllution ControlMississippi tpartrent of Natural ResourcesP.O. Box 10385Jackson, Mississippi 39209

Attn: David Bockelmann

1ar Mr. Mabry:

Enclosed please find the draft results of the analysis of samples collected atKoppers Inc., as requested by Mr. David Bockelmann. These results are notfinal ar are therefore subject to QA/QC.

If you have any questions, please contact Hugh Hazen or Karen 1cKinney at(404) 347—7603.

Sincerely,

Allan E. PntleyRCRA BranchWaste Compliance Section

Enclosure

C.. . CUNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION IVCOLLEGE STATION RD.

ATHENS, GA. 30613

*****MEMORANDUf,f******

DATE: 05/28/88

SUBJECT: Results of Extractable Organic Analysis;88-173 KOPPERS

GRENADA MS

FROM: Tow B. Bennett, Jr.Chief, Organic Chemistry Section

TO: DOUG LAIR

Attached are the results of analysis of samples collected as part ofthe subject project. .

If you have any questions please contact we.

ATTACHMENT

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION IVCOLLEGE STATION RD.

ATHENS, GA. 30613

*****MEMORANDUM******

DATE: 05/13/88

SUBJECT: Results of Purgeable Organic Analysis;88-173 KOPPERS

GRENADA MS

FROM: Torn B. Bennett, jr.Chief, Organic Chemistry Section

TO: DOUG LAIR

Attached are the results of analysis of samples collected as part ofthe subject project.

If you have any questions pZease contact me.

ATTACHMENT

L :‘fldHO

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4 )—RCPA

Mr. Sam Mabry, DirectorHazardous ste Division&ireau of Pollution ControlMississippi Department of Natural IsourcesP.O. BDx 10385Jackson, Mississippi 39209

Re: Koppers Canpany, Inc.Grenada, MississippiMSD 007 024 543

Dear Mr. Mabry:

This letter is a follow—up to discussions held during the Mid—Year Reviewconcerning the referenced facility. Included is EPA’S position concerningthe current canpliance situation for three hazardous or solid waste management areas at the facility — the ash landfarm, the spray irrigation fieldand the unnamed stream which traverses the property. Additionally, EPA’srecanmendations as to how these areas should be addressed are discussed.

concerning the ash landfarm, EPA co4ersjthis aareu]ated landdiflit_cQntaining_a_1istdazardous waste. The landfar!sthere—fore subject to applicable closure and pa töIbure regulations. Closureof this unit should begin immediately. EPA recanrnends that tDNR set aclosure schedule and final closure date via an administrative order orin the closure plan approval process.

Regarding the spray irrigation field, EPA also considers this to be aregulated land treatment unit containing a listed hazardous waste. EPArecatimends that MSDNR require Koppers to begin closure of the unit,regardless of the company’s proposed action against EPA. t.’SDNR shouldaddress the closure of the unit as expeditiously as possible.

The last area of concern is the unnamed stream which was addressed inthe “Report of Findings — Unnamed Ditch Characterization” prepared bythe facility in October 1987. EPA concludes contaminant releases haveoccurred to the stream fran the solid waste managnent units locatednear the stream. EPA recanmends that Koppers address these releasesand implement interim measures to stop these releases until suchtime as the HSWA permit interim measures are effective.

0 0UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION IV

345 COURTL.AN STREETATLANTA, GEORGIA 30365

RECEI VED

JUN10 1968Dept. of Naturat HesourcesBureau of Pollut,, Control

1’•‘

-2-

As stated above EPA recorrnds that MSDNR require Koppers to addressthese issues in a timely and appropriate manner. If you have anyquestions, please contact Hugh Hazen or Karen McKinney at (404)347—7603.

Sincerely yours,

James H. Scarbrigh, P.E.Chief, RCPA BranchWaste &1anement Division

1. Release Location

77e IF971 /‘1S

9. Person reporting release:

Nm t1Cl1//1J

Date:

()ZARDOUS MATERIAL RELEASE REPOMISSISSIPPI EMERGENCY RESPONSE COMMI

2.Oefe 3. TimeJI

County

5. Contact for further information:

Ga.p’, 11’C/efk-,icl

4. Company Name

l<OPP-r5 C.

Te €r / fi frCl Po,

Address. Bo’ /60 ,O/y ),

c 7’ L

State S Zip 38 U 0

Phone: c,— 58 ‘1

C-ec’s’7e c! r,

6. Release Information

a) Name of substance:_

b) NA/UN_________

d) Date of Release: .5’—it—88

I) Dureaon of Release: I — IliW

g) Release occurred into C Air C Water Ground

h) Substance is extremely hazardous DYES C NO(per list in 40 CFR 355)

7. Recommended precautions

C) Est. Quantity: ./

8. Anticipated Health Risks

10. Notified:C pol I uti Os Coetrol

C RadIoIeLICll Seal-tb

TiUe: e jI

Address: BC>)( 1C ‘iT

city 77e Pta nY

State Zip:

Phone ‘4 b6’1

11. Eaergency Action Required:C Nose C stat. C Local -

12. )nret:

MERC - III- 1 [REV—APR88] F

C 0

June 9,

Is Ti’a Str1Depiirtrert r Pc1.1uticn (rrtrcJ.rt Fckxiv

P. C. Fr” ‘3TSttJ Pcck, zr:a 72O9

Drr t, i-.rk

FiwrinJ rrce ,rFpxr Ccrr’, Thr.Gric, iir1’pi

yir kt-cr of M? 3, 1!B cu crirtain c ri.or c cc.rreria1 urnce for Kcpperr Ccqy in Greni&, Thefo11cinq t]2e ft iho ci2iJorF.

lion 1 • F’ie ‘e 7ih the ct fcr the c1curet-c1cvre cunt t.wt. rittx. to

our grcy?

Y\r r. Yes, e aqre ith cpperr’ currert cIorur ‘i’post-cicvre cr, 1nvrr, 7E Ca!ie t’’atthese coBt re cnlv etiate ar a’r rrcireadjtrert.

(‘uestior 2. ri fircl the cc’t cecu’t€, e if thatias thr probkn with their tirr.to?

ICorr Ie rc ‘et bcçu ciornre of ti’& rhxou rte unift nn to eJ$.if th irtec. oEts ii I i1vhirier, e beliew the’,r hru1c he

(ietcr. 3. Di vrer’ the firncia1 tct ftorir requitio,?

Youz letter tt:er tJt vu are attertir to vziliate I1 of tecost et.irtc.r for f I1ce to

oZ re’u1t

C aMs. TiDprtnt of Pollution Controla Fcoiocjy

Page -2

If you rhoulc have arw ciuestions or if you shoulc3 recuire any

ckitional infonvtion, please citiot rr at (601) 961—17l.

Pincerelv,

Dvi J. ckejwrUaarc½us WaE5te Br?nch

0 STATF OF ARKANSAS 0DEPARTMINT OF POLLUTION CONTROL AND ECOLOGY

8001 NATIONAL DRIVE, P.O. BOX 9583LITTLE ROCK, ARKANSAS 72209

I’HONE: (50) )562 7444

May 3, 1988

Department of Natural ResourcesBureau of Pollution Control y ii iDivision of Solid Waste ManagementPost Office Box 10358 IJackson, Mississippi 39209 LATTN: Hazardous Waste Financial Assurance Division

Dear Sir:

The State of Arkansas is reviewing the use of the financial test ofKoppers Company, Inc. for closure/post—closure costs. I wouldrequest that you take a few minutes of your time to answer a fewquestions for me.

1. Have you agreed with the costs for the closure and post—closureamounts that Koppers has submitted to your agency? Our recordsshow that for the end of year report for 1987 Koppers showed atotal of $1,025,829 for closure of the facility in your state;and a total of $1,285,658 for post—closure of the facility inyour state.

2. Did you find the costs adequate, and if not, what was theproblem with their estimate?

3. Did Koppers pass the financial test according to yourregulations?

The cuirenL ciosuIe/post—ciosure costs for the Kopper’s facility inArkansas is $463,930 and $2,208,300 respectively. These costs,which were not reflected accurately in the 1987 financial test,should be used when reviewing any new submissions by the company.

(D Page 2

I hope that this is not an inconvience to you, as it will help ourDepartment compare the costs for closure and post—closure forKoppers Company, Inc. in the State of Arkansas. We are attemptingto validate all the cost estimates within the next forty—five daysand would be glad to share this information with you. If you haveany questions, please feel free to contact me.

Sincerely,

Lisa M. StarkAdministrative Assistant IHazardous Waste Division

ims :Ltr172

cc: Karen Deere, Manager, Enforcement Branch, HW Division

Phone: 412/227-2694 436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219 Fax: 412/227-2436

March 24, 1988

Mr. David J. BockelmannHydrologistHazardous Waste DivisionMississippi Department of



Dear Mr. Bockelmann:

With this FAX transmission are copies of revised pages 1 of 5 and2 of 5 of the Part A Application for Koppers Grenada, Mississippifacility.


Sincerely,

Robert J. AndersonStaff Program Manager

RJA/CJV/j sw

0 0\YSTONE

EN1IONMENTAL RESOURCES, INC.

Via FAX601—961—5 0

9 \44

Enclosures

[IT.i 1..I I! I. I.

tINVIRONMENTAL PROTECTION AGENCY “—‘II. EPA ID. NUMBERHAZARDOUS WASTE PERMIT APPLICATIONConsolidated Pe,mits Program

(ThL, informatIon Is required under SectIon 3005 of RCR.4.)

t,ANO APPLICATIONOCEAN DISPOSAL

SURFACE IMPOUNDMENT

GALLONS OR LITERSGALLONS OR LITERScu.pc aos eqCUBiC METERS

104 GALLONS OR LITERS

D71 GALLONS OR LITERS010 ACRE-FEET (th. volume that

would couer one acre to adepth of one foot) ORHECTARE-METER

Dli ACRES OR HECTARES052 GALLONS PER DAY OR


Please print or type in the unshaded areas only,.—.-—---(fill—in areas re spaced for elite type, i.e.. 12 ‘)tes/incfl).

FORM

3 fEPAFOR OFFICIAL USE ONLAPPLICATION I DAlE R(CEIVEw

APPROVED I (vr..mo..&deL -

Approved 0MB No. 758•S80004

flMISIDIOIOI71flf,I7IrJLIl1Z9T

COMMENTS

II. FIRST OR REVISED APPLICATIONPlace an “X” in the appropriate box in A or B bilow (mark one box only) to indicate whether this is the first application you are submitting for your facility or arevised application. If this is your first application end you already know your facility’s EPA 3.0. Number, or if this is a revised application, enter your facility’sEPA 3.0. Number in Item I above.A. FIRST APPLICATION (place an “X” below and provida the approprIate date)

I. EXISTING FACILITY (See Instruction, for defInition of exiating facUlty7’ Complete item below.)

. çJa.NEw FAtILITY (Complete item below.)FOR NEW FACILITIES,

_________________

PROVIDE THE DATE

_____ _____

I -i FOR EXISTING FACILITIES. PROVIDE THE DATE (yr.. mo., A day). I ..o. I I a (yr, mo., & day) OPERA’L i 1 I 0TI0N CEGAN OR THE DATE CONSTRUCTION COMMENCED I I I 3 TION SEGAN OP 3

! - . . - ..: . . 1-- -1r-7’i -

_____ _____

Ip I I (use the boxe, go the left)

_____ _____

t i EXPECTED TO BEGING. MV IDS.U ArrL.ILATILIVS (place an -- oeaowena compiera 11em1 aaouer

I. FACILITY HAS INTERIM STATUSQZ. FACILITY HAS A RCRA PERMIT

Ill. PROCESSES — CODES AND DESIGN CAPACITIESA. PROCESS CODE — Enter the code from th. list of process codes below that best describes each process to be used at the facility. Ten lines are provided forentering codes. If more lines are needed, enter the code(s) in the space provided, It a process will be used that Is not included in the list of codes,below, thendescribe the process (including ka d.e197 cspaclty) In the space provided on the form (itwn ill-C).

B. PROCESS DESIGN CAPACITY — For each code entered In column A enter the capacity of the process.1. AMOUNT — Enter the amount.-2. UNIT OF MEASURE — For each amount entered In column 8(1). enter the code from the flit of unit measure codes below that describes the unit ofmeasur. used. Only the units of measur, that are listed below should be used.

PRO. APPROPRIATE UNITS OF PRO. APPROPRIATE UNITS OFCESS MEASURE FOR PROCESS CESS MEASURE FOR PROCESSPROCESS CODE DESIGN CAPACITY IROCESS CODE DESIGN CAPACITYStorage:CONTAINER (bazrel, drum, etc.) SOSTANK SOSWASTE PILE 102

SURFACE IMPOUNDMENT

INJECTION WELLLANDFILL

UNIT OF MEASURE

Treetosent:TANK TOI GALLONS PER DAY OR

LITERS PER DAYSURFACE IMPOUNDMENT T02 GALLONS PER DAY OR

LITERS PER DAYINCINERATOR TOS TONS PER HOUR ORMETRIC TONS PER HOUR;GALLONS PER HOUR ORLITERS PER HOUR

OTHER (Use for physical chemical, ‘504 GALLONS PER DAY ORthermal or biological trealnsrnt LITERS PER DAYprocesses not occurring In tan kg,surface impoundment, or i,winer- -

ator,. Describe the processes Inthe apace provided; Item Ill-C.)

UNITOF UNITOFMEASURE .... MEASURE .cOo€- UNIT OFMEASURE -- CODE UNIT OF MEASURE

GALLONS G LITERS PER DAY V ACREFEET . ALITERS L . TONS PER HOUR 0 HECTARE’MLTER FCUBIC YARDS Y METRIC TONS PER HOUR W ACRES...... .....-, BCUIIC METERS ._- .-G-. z—_. GA4jL,ONS P -KOUq ‘-,P,- ,-,-r E - - I4C’TAWES’-, QGALLONS PER DAY

- - Lfl’ERS PgWltOIJR,. • . .‘ . HEXAMPLE FOR COMPLETING ITEM III (thosars In lIne numbeea X-7 ndX-2 below): A facility has two storage tanks, one tank can hold 200 gallons and theother can hold 400 gallons. Th. facility el.o flee an Incinerator that can burn up to 20 gallons per hour.

UNIT OFMEASURE.

CODE

j DUP

A PRO-B. PROCESS DESIGN CAPACITY .

PRO-B. PROCESS DESIGN CAPACITY

CE!! 2. UNIT OFFICIAL 2. UNIT OFFICIAL(frjjgf 3. AMOUNT USE W(°Ii 1. AMOUNT

ONLYJZ- cod.) cods)

. LI”— I U..’i” j

X-1S02 600 ‘ G 5—

X-T03 20 .2’.--

1 S04 130,650 G 7-—

2 8

i:::,:::;zz’EP.l Form 3510-3 (640) PAGE 1 OF 5 CONTINUE ON rtr.’

Continued from the front.0 0

C. SPACE FOR AOOITIONA PROCESS CODES OR FOR DESCRISING OTHER PROCESSES (code “T04”J. ron EACH PROCESS ENTERED HEREINCLUDE DESIGN CAPACITY.

Note: lll.C. Line 1

650 cubic yards x 201 gal /yd3 = 130,650 gallons

A. EPA HALHUQUS WASTE NUMbER — enter ne tour—aigIt numoer Trom 441 ç&H, Subpart I) for each listed hazardous wast, you will handle. if youhandle hazardous wastes which ar, not listed in 40 CFR, Subpart D, enter the four—.digit number(s) from 40 CFR, Subpart C that describes the charscteristica and/or the toxic contaminante of those hazardous wastes.

B. ESTIMATED ANNUAL QUANTITY — For each listed waste entered In column A estimate the quantity of that west, that will be handled on an annualbasis. For .di characteristic or toxic contaminant entered in column A estimate the total annual quantity of all the non—listed waste(s) that will be handledwhich poises. that characteristic or contaminant.

C. UNIT OF MEASURE — For each quantity entered in column S entr th. unit of measure code. Unite of measure which must be used end the appropriatecodei are:

FNitLlSH UNIT OF MEASURE- - - - CODE METRIC UNITOF MEASuRE CCIflE

POUNDS P KILOGRAMS K•

.-: — -. METRICTONS... ..., .

If facility records use any other unit of measure for quantity, th. units of measure must be converted into one of the required units of measure taking intoaccount th, appropriate density or specific gravity of the waste.

0. PROCESSES1. PROCESS CODES:

For listed hazardoue west.; For each listed hazardous waste entered In column A select the coda(s) from the list of process codes contained in Item illto indicate how the waste will be stored, treated, andlor disposed of-el the --

For non—fisted hazardous weetes: For each characteristic or toxic contaminant entered in column A, select the code(s) from the list of process codescontained in Item III to indicate all th. processes that will be used to store, treat, and/or dispose of all the non—listed hazardous wastes that possessthat characteristic or toxic contaminant.Not.: Four space, are provided for entering process codas. If more are needed: (1) Enter the first three as described above; (2) Enter “COO” in theextreme right box of Item IV.O(1); and (3) Enter in the apace provided on page 4, thi line number and the additional coda(s).

2. PROCESS DESCRIPTION: If a code snot listed for a process th.twilI be used, describe the process In the spec. provided on the form.

NOTE: HAZARDOUS WASTES DESCRIBED BY MORE ThAN ONE EPA HAZARDOUS WASTE NUMBER — Hazardous wastes that can be describea bymore than on. EPA Hazardous Waste Number shall be d.ecribed on the form as follows:

1. Select on. of the EPA Hazardous Wasp. Numbers end enter It in column A. On the sam. lin, complete columns B.C. and 0 by estimating the total annualquantity of the waste and describing all the procelees te be used to treat, store, and/or dispose of the waste.

2. In column A of th. next line enter th. other EPA Hazardous Waste Number that can be used to describe the waste. In column 0(2) on that line enter“included with above” and make no other entries on that line.

3. Repeat step 2 for each other EPA Hazardous Waste Number that can be used to describe the hazardous waste.

EXAMPLE FOR COMPLETING ITEM IV (those,, In I/n. numbers X 1, X.2. X.3 andX-4 below) — A facility will treat end dispose of an estimated 900 poundsper year of chrome shavinge from lth.r tanning and finishing operation. In addition, the facility will treat and dispose of three non—iisted wastes. Two wastesare corrosive only and there will be an eetlmeted,200 pouncis per yser of each waste. The etherraseta is corrosiwend ignitable and there will bean estimated100 pounds per year of that t.. Treatment will biln en Incinerator and dlspoeats.Iflbe in a landfTIf:---” .. -

A. EPA C. UNIT 0. PROCESSESId HAZARD. B. ESTIMATED ANNUAL MEAZ0 trASTENO QUANTITY OWASTE 5. PROCESS COOLS 2. PROCESS DESCRIPTION

Z (enter code) (enter) (if a coda e not entered in D(1))I F II I I I I

X-1K054 900 P T03D80II II II I I

X-2D002 400 P T03D80—. = -_.s—-•I-_. 5-’ T’F-. —

X-3D001 100 P T03D80- -

I l I I I I IFX4 D 0 0 2 included with above

EPA Form 3510.3 (b.8o) PAGE 2 OF 5 CONTINUE ON PACE 3

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\YSTONEEN1IONMENTAL RESOURCES, INC.

0

Mr. David J. BockelmannHydrologistHazardous Waste DivisionMississippi Department of Natural

ResourcesBureau of Pollution ControlBox 103852380 Highway 80 WestJackson, Mississippi 392014


I have enclosed a copy of the revised page 1 of 5 of the Part AApplication for Koppers Grenada, Mississippi facility.

The change brings the volume of work in the impoundment into linewith the amount reported on Pages 1-2 and 1—3 of the November1986 Closure Plan for the surface impoundment/sprayfield.

If you need any additional information before Friday, March 25,please call my phone number and ask for Chuck Vita.

Thanks for your help.

RA/bjEnc losure

Very truly yours,

Robert AndersonStaff Program Manager

Phone: 412/227-2694 436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219 Fax:

March 23, 1988

LJ 1._I I! I. I,I

U.S. ENVIRONMENTAL PROTECTION AGENCYHAZARDOUS WASTE PERMIT APPLICATION

Consolidated Permit Program(This information ii required under Section 3005 of RCRA.)

COMMENTS

Storage:CONTAINER (ban’ei, drum, etc.)TANKWASTE PILE

SURFACE IMPOUNDMENT

Disposal:INJECTION WELLLANDFILL

LAND APPLICATIONOCEAN DISPOSAL

SURFACE IMPOUNDMENT

501 GALLONS OR LITERS502 GALLONS OR LITERS503 CUBIC YARDS OR

CUBIC METERS504 GALLONS OR LITERS

079 GALLONS OR LITERS080 ACRE-FEET (the volume that

would cover one acre to adepth of one foot) ORHECTARE-METER

081 ACRES OR HECTARES082 GALLONS PER DAY OR


OTHER (Use for physical, chemical,thermal or biological treatmentprocesses not occurring In tanks,surface impoundments or incinerators. Describe the processes inthe space provided; Item 111-C.)

TOl GALLONS PER DAY ORLITERS PER DAY


T03 TONS PER HOUR ORMETRIC TONS PER HOUR;GALLONS PER HOUR ORLITERS PER HOUR


Please int or type n the unshaded areas onl(fill—in areas are spaced for elite type, i.e., 12 , ersfinch).

FORM

3RCRA

FOR OFFICIAL USE ONLYAPPLICATION I DATE RECEIVED

APPROVED I (yr.. mo.. & day)

Form Approved 0MB No. 758-S80004

I. EPA I.D. NUMBER’

FMISjDIOIo71o1f14I]1h_

II. FIRST OR REVISED APPLICATIONPlace an “X” in the appropriate box in A or B below (mark one box only) to indicate whether this is the first application you are submitting for your facility or arevised application. If this is your first application and you already know your facility’s EPA ID. Number, or if this is a revised application, enter your facility’sEPA ID. Number in Item I above.A. FIRST APPLICATION (place an “X” below and provide the appropriate date)

t. EXISTING FACILITY (See instructions for definition of “existing” facility. fl2.NEW FACILITY (Complete item below.)7, Complete item below.)-

FOR NEW FACILITIES,.

PROVIDE THE DATEi r v. J I ue. I ov 1 FOR EXISTING FACILITIES. PROVIDE THE DATE (yr.. mo., & day). Mj 1 V (yr., mo., & day) OPERA1 Ip Ip Ii Ip Ii I (use the boxes to the left)

EXPECTED TO BEGIN

I ii OPERATION BEGAN OR THE DATE CONSTRUCTION COMMENCED

I I I TION BEGAN OR IS1.__.I_n id 173 7.1 [77 71172 74 74 I I,,B. REVISED APPLICATION (place an “X” below and complete Itemlaboue)

1. FACILITY HAS INTERIM STATUS Da. FACILITY HAS A RCRA PERMIT7272

III. PROCESSES — CODES AND DESIGN CAPACITIES —

A, PROCESS CODE — Enter the code from the list of process codes below that best describes each process to be used at the facility. Ten lines are provided forentering codes. If more lines are needed, enter the code(s) in the space provided. If a process will be used that is not included in the list of codes,below, thendescribe the process (including its design capacity) In the space provided on the form (Item lllC).

B. PROCESS DESIGN CAPACITY — For each code entered in column A enter the capacity of the process.1. AMOUNT — Enter the amount.2. UNIT OF MEASURE — For each amount entered in column 8(1), enter the code from the list of unit measure codes below that describes the unit ofmeasure used. Only the units of measure that are listed below should be used.

. PRO- APPROPRIATE UNITS OF PRO. APPROPRIATE UNITS OFCESS MEASURE FOR PROCESS CES MEASURE FOR PROCESS(flCl riqintJ (‘PA(N1’Y PRflCFC rrinn flEI(.Pd rAPr’ITV

Treatment:TANK

SURFACE IMPOUNDMENT

INCINERATOR

UNITOF UNITOF UNITOFMEASURE MEASURE MEASUREUNIT OF MEASURE CODE UNIT OF MEASURE CODE UNIT OF MEASURE CODEGALLONS G LITERS PER DAY V ACRE-FEET.. ALITERS L TONS PER HOUR 0 HECTARE-METER FCUBIC YARDS V METRIC TONS PER HOUR W ACRES BCUBIC METERS C GALLONS PER HOUR E HECTARES 0GALLONS PER DAY U LITERS PER HOUR HEXAMPLE FOR COMPLETING ITEM III (shown in line numbers X-l and X’2 below): A facility has two storage tanks, one tank can hold 200 gallons and theother can hold 400 gallons. The facility also has an incinerator that can burn up to 20 gallons per hour.

DUP

A. PROB. PROCESS DESIGN CAPACITY

‘ W A. PROB. PROCESS DESIGN CAPACITYU CESS

... FOR U “E FORCODE

-.

-. 2. UNIT OFFICIAL 2. UNIT OFFIClAL(from list : ,

:.

OFM:A

OtY (from list 1. AMOUNT 0FM:A

.JZ- code) a

code)•1. 27 .‘.L tf.Ll .

X-1S02 600 G 5

X-:T03 2o.f.. E 6

I S04 52,360 C 7

2 8

3 9

4I•.__ !l I, 27

- — — —

10IC - II II

CONTINUE ON fllSFEPA Form 3510-3 (6-80) - PAGE 1 OF 5

C\ KEYSTONE

ENVIRONMENTAL RESOURCES, INC. R E C El V ED

436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219 MAR 18 1988Dept. of Natural flesourceslureau of Pollution ConErol

March 16, 1988

Mr. David J. Bockelmann, HydrologistHazardous Waste DivisionMississippi Department of Natural ResourcesBureau of Pollution ControlBox 103852380 Highway 80 WestJackson, MS 39204

Re: Koppers Company, Inc.Grenada, Mississippi FacilityEPA ID No. 007 027 543


Three copies of the groundwater sampling and analysis plan for the ash disposalarea at Koppers’ Grenada, Mississippi facility are attached. Samples werecollected In February 1988 for the first found. A report summarizing the samplingresults will be prepared at the end of July 1988.

Please call if you have any questions or comments.

Sincerely,

obert J. AndersonStaff Program ManagerKoppers Treated Wood Products

RJA/ crAttachments

DIRECT DIAL #412—22 7—2683

cc: J. Scarbrough EPA IVJ. D. ClaytonJ. R. BatchelderJ. Blundon (w/o attachment)M. Schlesinger (w/o attachment)

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KEYSTONEtNvIRuNMErcTAL RESOURCES, ç:,-J

436 ScenLh Avenue Suite 1940, Pittsburgh, PA 15219

TO: David i Bockelmann

COMPANY NAME: Mississippi Department of Natural Resources

COMPANY TELECOP IER NUMBER: 601- 961- 5190

FROM: Robert J. Anderson, Keystone Environmental Res., Inc.

NUMBER OF PAGES TO FOLLOW:

___________________________________

xr YOU DO NOT RECEIVE ALL MATERIAL TRANSMITTED, PLEASE CALL U ON:

(412) 227—2694,

OUR COPIER NUMBER IS (412) 227-2436, IT IS A PANAFAX UF-600AT.

SENT BY: JoanWililams.. TIME: 11:00 DATE: 3/jjqp

a

V03/24/1996 11:02 N KE’?STDNE •—<1222?2436 P.02

KEYSTONEFNVIRONMLNTAI. RESOURCES, (NC.

Phone: 412/227.2694 436 Seventh Avenue, Suite 1940, P1t(sburgh. Pt 15219 Faxz 412/227-2436

March 24, 1988 via FAX601—961—5190

Mr. David S. BockelmannHydrologistHazardous Waste DivisionMississippi Department of




with this FAX transmission are copies of revised pages 3. of S and2 of 5 of the Part A Application for Koppers Grenada, Mississippifacility.


Sincerely,

WcSs*tj 4’k9’%J(Robert J. AndersonStaff Program Manager

RJA1CJV’/j sw

Enclosures

L

aoEPA

FOR OFFICIAL USE ONLYAnLtcAtTSii. OA4zflCCtVIO

irtntcJII, FIRST OR REVISED APPLICATIONPine an “X” In the aporocriet, box in A or B below fmer* one box onlyl to indicate whether this it the first application you are jubmiiting for your facility or srevised applIcatIon. If this I; your first epplicatlon end you already know your facilky’s EPA 1.0. Number, or ii this lea reviled application, enter your facility’sEPA 1.0. Number In Item I show.a. wlnSrAPn.ICATION (plan an X” below and piuEda tk4propflafriate)

IXJSTINO FACILITY (Sn In, tnACttOM fØt 4,fln/haa of “extal/n” fecWty, *.nsw FACILITY (Complete It.’n below.)vi Complete Item helow,)

P05 NiW FACILITIES.PROVIDE THE DAT(l’a

____ ____ ____

1 QflNATJOM SEDAN81 IjJ j I i i’un t. baste to iii. ieTtTTHE OATS CONSTRUGPION COMMeNCED I ri ‘noN eKOAN OR II

Li ton EXISTING FACIUTCES. PSOVIOS tics OATS (yr.. Mo,. dewi VR

I I. j pfl i’vri, ma, * day) OPERA

wk3i4_1_1 ikL. !.!.ri-7:.!..i 7, ‘II ‘ jSXPECttOTOe,GIN..—,., srrhs.,sTlJn çpienon roewIemsea.......r...,,........1. rAtliITY HAS INTERIM STATUI

flROCESSSS — COPES AND DESIGN APi

LAND P.PPI.ICATIONOCEAN DISPOSAL

SUISFACE IMPOUNDMENT

TANK

SURFACE P4POUNPMSNT

N’•

- 03/24/1966 1103 ‘\\ KEN’STONE.ren sri acetic’ foe w//is pjj,j AcrsnAncM,

Pun’saSCRA

U.S. ENVIHDNMflTAL PROTECTION AGENCYHAZARDOUS WASTE PERMIT APPLICATION

Covesolldnd Penn/u ProgrfT/ste lnformattan knouind under Ste//an 3004 of ACM.)

22272436 P.03

‘,/ Porn, Approred DMa No, tSflUQQCd

I, EPA LD.NUMSERFr r i

PMIInIn Oil ft i c KLEi

COMM SN TI

a,

L PACJIJTY HAS A RCRA PCIIMIT

A. PROCESS CODE — Enter the code from the list of process codes below that beet describes nab process to be used at the facility. Ten inca are provided forentsnin codes. If more lines are needed, enter the code(s) In the specs provided, If a process will be used that Is not included In the list of codei,below, thendescribe the process Uxiudinglu dnlgw, in the apace provided ore the form (Sr I/bC).

B, PROCESS DESIGN CAPACITY — F seth code entered In column A enter the cepeclty of the process.1, AMOUNT — Enter the amount,2, UNIT OF MEASURE — For each amount entered h column Sill, enter the code from the list of unit mewsre coda below that describes the unit ofminute used. Qnly the units of enneure that a’s listed below should be used.

PRO. APPROPRIATE UNITS OF PRO. APPROPRIATE UNITS OPCESS MEASURE F OR PROCESS CESS MEASURE FOR PROCESSPflfM5

r. !!!

OSSItIN C$PACIT’L .... —, ,. Mt$CFS .

.!

COTht OSION.CAPACkfl

CONrAINIR (barrel, dnsss, eta)‘A N PtWASTE PILE

SURFACE IMPOUNDMENT

INJECTION Well.LANDFILl,

set GAIJ,DN*OR LITERSa* GALLONS OR Llflfl5*1 CUBIC Ype ON

CUIIC METERS504 flALLOMS Ofl LITERS

705

Tel

HOUR Cit

g::

To)

I.l.ONS OR

!ff 1S!?i

jE’”t4InelnetTI N

lIbC.)LITSfl

UNITOF VNITOF VN1TOPMEASURE MEASURE . . MEASURE.UNIT OP MEASURE ‘ CODt i ‘tlN1TOP MEASURE . ‘ COQE. UNIT OF MtASUE. __QOE

OALLONI ,,..,.,,.,.G LJflRSPSRPAV,,, Wv ACRE-FEETT,,t .7ONSPSRI4OUR ,,....,,,,,..D H4C’VARE-MStSR,, FCUSICYAROI, ,,,..,,,Y . METNICTONSPE$HOUL,,,...,W .,405a..__.J,.fl.,,CU iiC METcR% — raC,t -‘ *A$.Ofl PS*StOijN’ r* .-n I HffANEI a s—,, 0OAI.L.ONSPKROAY LltERSPtwNotaw,..,,; a

EXAMPLE FOR COMPLETING ITEM III (theses hsthsqnunsbsaX-V andX-2 below!; A facility has two storage tanks, one tank can hold 200 gellons and theother an hold 400 gellons, The fesility also bee en incinerstos’ thee can burn up to 20 gallons per hour,: .1A. PRO

B. PROCESS DfliaN CAPAClTVA PRO r

I, PROCESS DESIGN

J ‘VI W:! II !... rUNT

01:X-1802 ‘ 500 ‘ ‘ -‘ C S

-‘“ , ..“-

x—: ‘ Q 20 £ 5” •!••“! I

I $04 130,650 Q 7

2 8

‘ . 9

4 10EPA Fonn 351o.a 16401 PAGE 1 011’ 5 CONTINUE ON rr “!

S 03/24/1968 11:04 KEYSTONE

Li‘ continve item the Iran:,

iüRocESSESiconrjnt

WbEsciwTiN OF HAZARDOUS WASTES

_________ __________ ____

CPKRAzARDOUS WASTE NbMalr— Eñbr tkiö cur—c1gitiiiid*lTthi 4RSi5j$WDTor ieàWfiii’hattrdoiä weeta wuwtll hindu. if youhan&e tazsrdout weates which are not listed in 413 CPA, Subpan D, enter the four—digit number/si from 40 CPA. Subpart C that describes the cherecteris.:lt, md/or the toxic oontaminans of thoee hawdoua weØes.

9. ESTIMATED ANNUAL QUANTiTY — For each fisted waste entered in column A estimete the quantIty of that waste that will be handled on an ennuslbasis, For tech chansterietle or taxis eonmir*nt entered In column A estimate the total annual quantity of all the non—fisted waste(s) that will be handledwhich Øoeseee that characterIstIc or contaminant.

C. UNIT OF MEAfliRS — For each quantity entered in column 3 enter the unIt of ,neeaure coda, Unita of measure which must be used and the appropriatecodes era: ‘r’ .

kNGLlSHi1NlTflFMAffiifl -._ MET9ICiJNPrnFMcflj.( —POUNDS P K1I.OOPAM$TONI, . .g. •..&4 ‘A.tPi.t.!.5J.tt€’.’ ‘c’Z; M!TflICt0Nt.r ., •*.st . •.

if facility rscor* u any other unit of measure for quantity, the unite of measure miat be conterlad into one of the required units of measure taking intoaccount the epprcprlate density or epecific gravity of tite watt.

0. PRoCESSES1. PROCESS CODES:

For listed hazerdota were: For each listed hazardous waste entered in column A select the cove(s) horn the list of process codes cont&ted in lten’to Indicate how the waste will be stored, treated, end/ordiepcee& of-es the feclllty.—?fnrn’4’Foe nan—listed hazardoua welts: For each therectarirtic or toxic contarnirtant entered In column A, asian the code(s) from the list oi *cen cooescontained in Item lii to indlw, all the prose that will be used to store, teat, end/or dispoee of all the non—lined hezardoum wesuu met ponessthat charecterlstlc or toxic contaminant.Nn: Pour spaces are provided for entering pros codes, it more era needed: (1) Enter the first three es described above: (7) Enter “000” in theextreme right box of Item IV’O(l); and (3) Enter In the apera provided on page 4, the tine number end the additional code/a).

2. PROCESS DESCRIPTION: lie code is not listed fore process thatwill be used, descrIbe the proosa In the space provided an the font.NOTE: HAZARDOUS WASTES DESCRiBED IV MOM THAN ONE EPA HAZARDOUS WASTE NUMBER — Hazardous wastes that can be described bymore than one EPA Hazardous Waste Number shill be described on tha form a folIowst1. Select one of the EPA Hszerdoua W. Numbers arid enter it in column A. On the earn. line compin columns ES, end D by estimating the total annualquantity of the at, end desribing all the fromsee. to ha uead to ow,, store, endlor dispose of the weste.2. In column A of the next line enw the other EPA l4azardoua Waste Number that art be used to describe the waste, In column Dl?) on that line enter“included with above” and make no other enirlee on that line.

. /3, Repeat step 2 for each other EPA Hazardous Were Number that can be used to describe the hazardous were.

EXAMPLE FOR COMPLflNQ 17CM IV (Maim In /kv, numbers X’S,, X2, X4 end X4 below) — A facility will net end dispose of an estimated 900 pcundtper year of chrome shavinge front leather taming and finishing operation. In eltion, the facility wlIl net and dispose of three non—listed wastes. Two wastesera corrosive only and there will be an estimated 9O poumb per year of each teat,, The other.e is onalve end rtable end there will been anImatedtoo pounde pp yew of that waste Th...t,..at wiii’b. in an Incinerator and dlsposel will be in a landflif ‘- ‘f” -

A C.UlqIt- r

D.PROCESfl3o ‘;t:’;h41’ ::Ro.r?o;.

—1-

z (entsrtodflrode

-.

— — — . - — —

— fr - rr ri —r rX1K034 900 P T03D80--.—--t - -

i-r- r-r r— ri— —‘- .--X-2D002 400 P TQ3DSO-— — — — ---—

-. ;- : . l!9r .Lk.-... ‘tt:4.30001 ioo P 703080—---—fl. ---

--- ------i— ri-m-r- VrX4 2) 0 0 2 —. rnctudedwlthoboi’e - .. --a — a a — -- -L - — —

,‘-‘-22272436 P.04

Uc. sPACE POfl ASDIT1ONAL pnocset Coors Usa roWo.acqisirsa orn rsàcxsacs a. ‘704”). PO (AH PNQCCSS EMILPIEC H5PI(

•NCL.UOK fltSiqpi CAMCIfl.

Note; (II,C. Line 1

650 cubic yards x 201 gal /yd3 130r650 gallons

en nr

4’

EPA Form 35104 tO-SQlPAGE a oF 5 CONTINUE ON PAGE 3

03/24/1965 11:02 KEYST:NE

KEYSTONEFNVIRONMENTAL RESOURCES INC.

rt22272436 P.02

U

Phone: 412/227.2694 436 Seventh Avenue, Sidle 1940, Piftsburgh, PA 15219 Fax: 412/227-2436

March 24, 1988 Via FAX601—961—5190

Mr. David J. BockelinannHydrologistHazardous Waste DivisionMississippi Department of



With this FAX transmission are copies of revised pages 1 of 5 and2 of 5 of the Part A Application for Koppers Grenada, Mississippifacility.

If you need additionalme at (412) 227—2683.

information, please feel free to contact

Sincerely,

Wc4sttjRobert J. AndersonStaff Program Manager

RJA/CJV/j sw

Enclosures

AS GE fE/tEd


ESVM C’lCS O G

__

3EPAFOR OFFICIAL USE ONLY.APLtiiR DATiNIGCIViUzrrH, FIRST OR REVISED APPUCATIONPuce an “X” In rue appropriate bo* In A or a below fma,* one bo# only) to indIcate whether this is the firat apllcaulon you are submiutinp for your facility or arivited applIcatIon. I? thu is your tint epplication and you alnedy know your facilIty’, EPA 1.0. Nwnber, or if tbi ii ryiild application, enter your facility’.EPA (.0. Number In tam I .bo%q.

A. PROCESS CODE — Enter the code from the liii of proc,g codas below that be describes each process to be used et the facility. Ten (in.. are provIOe for•nterin codes. It more lInes are ncoded, enter the code(s) in the ,p.ce provided. If. process will be uaad that is not inch.id,d In the lust of od be’ow, thendnctibe the procase tlncIud1n1te dse1 ciry) In the apses provided on the form (fli” tll.G1.B. PROCESS DESIGN CAPACITY — Fw sedu code entered in column A enter the capacity of the precise.1, AMOUNT — Enter 5h amount.

2. UNIT OF MEASURE — For each imoum entered Iii column S(1I enter the code from the lIst of unit in.muce codes below that deicribes the unit ofmecowi used. Only the units of mesiure that w lIsted below should be used.PRO. APPROPRIATE UNFFS OF PRO. APPROPRIATE UNITS OFCESS MEASURE FOR PROCESS 0538 MEASURE FOR PROCESSrflS pSal2N C$PtTY

- CS DS*lNAPACl’Y --

lAN K

SURFACE (MPOUNGMCNTIIIGINCRAroR

07 OAOP4iO7l?3Risisal onqep ((he for ph sIc.? .he,nlcal,would corer a’,. acre to. thenus? o, bIcIesIoJtrva&,,entdepth of one fool) OR proca.a.. not occurrffii l.s tank,H(CTA’MSTeR .I?fkc, fmposandm,’,ja orfr,elnep.DCI AORC* OR 1410?ARCI atom. Pswrib. Usppsoe.aci InDii OALL.ONI PSR DAY OR thi spale prcild.d; item ll1.CJLIlIRI PiN DAYDII GALLONS 0$ LITERS

iJNITOF UNITOFMEASURE MEASUREUNIT OF MEASURE 000€ .i VNITOF MEASURE “ ‘ COOE, UNIT OF MEASURE., , , .. .0 1ris PEN DAY.,, ,, . V AC$1Fk;7 ,. A, ,L 70141 PIN NOUN , 0 45CrARIMCTCR F

CUPIC YARDS . .7 • METRIC ‘TONS PEN NOUN. .. , . .., W,• .. , •Aaa* V$.-fPI.....t’•t-.GALLONS PIN DAY . .., .;T•t LRTSRSpgRlOtg$. ...,..... ,M -EXAMPLE FOR COMPLETING ITEM III (thsem Ia/k,. msntMrT X.7 and X.2 1,/owl; A facility hes t storee tanks, on. tank can )uoIU 200 callon. end the

othir can held 400 pellana, Tb, facility also hi. en lrsc)niresc, thet can but up to 20 g&Ions per hour.

L -, : ,\\\\\\.\\\\S\\A. PRO. I. P$QCKU DESIGN CAPACITY ‘

AS. PROCESS DESIGN CAPACITYCEll

s.s,rnIT OFP?CIAI.‘u CR55 t UNIT OFiCIA

:i LL

ciX-]S02 600 ‘ •. a 5x-ros

- -

I so 4 130,650 G 7 — -

28— — —

— — — - - — — -—3

9

03/24/1986 11:03 (. KEYSTONEffllfr’in areas sac waced for ./itw eyp, ,.] )uvicr.reAneis),

PUNM

3

P.03

‘---fiiNvlRoNMcN1Ai.pno,cctIoNHAZARDOUS WASTE PERMIT APPLICATIONConwi dated Permits Pro,ram(This l’,(qr’,.ttsisr,saIrrd undi’r .ect$on 3005 of ACM,)

Ponn Anaroved 3M8 No, 158’s830c4

COMM EN TI

fr1M I 1017)012111314)1M1

A. FIRST APPLICAtION (pa c”X” be wandprvUTe she ipproprfat.jata)I, I*1ITINO FACILITY Set I’,,lnCtIeM for definitIon of ‘utith*g” facUlty. LNKW FACILITY (Complete 11am bitow.)Complete Starn below,)FOR NEW FACtLITICa.PROVIDI THE DAVEOPI$A?ION CIGAR

. it.. .. .1541 OATS CONITRUCVTON COMMeNCED

YiON CEGAN OR 1

va ae a v FOR EXISTING FACII.ITICI. PROVIDE 7.41 nATE (yr., ..,..

1ii. L’ ‘

(yr, 4 day) OpinA.

-. 1alI j(plac, an ‘X” b.S..v endiimpJaea lImes! mM-’ - -- ‘.

EXPECTED TO aEGIN

FACILITY HAl NilNise ITATUIz. pACIi.ITY HAS A RCRA PERMITHI PROCESSES — CODES AND DESICN CAPACITIES

COISFAINIR (knit, dmm, w.)YANKWASTI P11.1

SURFACE IMPOUSI Oks aver01.•NIcrION WEll.LANDFILL

LAND APPLICATIONOCeAN DISPOSAL

SURFACE IMPOUNDMENT

lot GALLONS ON LITERSSiR GALLONS ON LITERS$51 CUSIC YANDI ONCUIIC hSITCRI

5*4 GALLONS ON LITERS

701 GALLONS PER DAY ORLITERS PER DAY

705 GALLONS PER DAY ORLIII NC PER DAVOl ‘TONi PER HOUR ORMETRIC TONI PER HOUR,GALLONS PER HOUR ORLITERS PER HOUR

704 0*1.1.0141 PER DAY ORLITERS PIN CAY

UNITOFMSASLIR E.

CODE

4H___. II

CONTINUE ON rr. ‘(1EPA Form 35104 16401

PAGE 1 OF 5

0/24/1966 11:4 3. kE’STCNE

C’22224

P

Cotlnuid from the front,-

—.Ill. PROCESSES fconrüwed/i,Aea POR Aorrtop4AL. pxocx,s Cooi o ro DeiCttsKO orN FOGiIIO (coda “TO4”. ro c*ci. .i,ocees a HaRK

•C.UOL ØKCIGN C*PAGI?V.

Note: I1l.C. Line 1

650 cubic yards x 201 gal /yd3 130,650 gallons

WDiiUPTON OF ZARDOUS WASTESAVA KADOUB ?IASTI1ElIMB!W— Enter the fàur—di number from 4CFR, bØartO for echilatid hazardoiiö waste c51 fiandlEi1 youhindu hawdovs wIitai whioh are not listed lit 40 CFR, Subpart 0, enter It. four—digit nurnbevf,.I from 40 CFM. Subpart C that describes the cherectarls.ties and/cr the toxic contanilnente of those hazardous wanes.

P. ESTIMATED ANNUAL GUANT1I’Y — For wdt lbWd waste entered in column A astimete she quantity of that waste that will be handled on an annualbasis, For each cIta.aaterlit.ia ortane’onemWaa* entered In column A estimate the total irnniai quantity of all the nan—listed wiIte(I/ that will be hendiedwhich possess that charic*.rl,tIe Or contaminant.

C. UNIT OP MEAJR5 — For seMi quentley entered In column S enter th. unit of musw cod.. Unite of mewe which must be used end the pproprfatecodesirt:

NflLI4 UNIT P MF45)JR— QOj MfTlUi’4t’rF I4çASURE CODj. , . . . P SItLOORAMI . . N

Tarel. .

-! M!TR1C7ON._..,., . . . •. , M.if facility ricorde uai arty other unit f measure for quantity, tit. unit) of msesro muat be conwrted into on. of site reqUired Units of measure tilting into.ccoi.int the appropriate density or specif Ic grevity of the waste.

0. PROCESSESI. PROCESSCOQES:

For fisted hazardoue waste; For each Ibted hazardous weiss tered in column A select she cod,(, from the list of process codas contained in item illto IndiceS. how the were will be stored, trw.d, end/or diipaiedOfit the facUlty,— -‘‘‘

—

For non—4bt.d hazardous ww For esdi dtar,czsrlIlIc or toxic conwnlnmnt entered in column A, sliact the ood.fsJ from *ie (Its of precast codatcontslnd In Item lii so indians all the procasan that will be ued so store, treat, md/or dispose of all the non—lIsted hazardous wastes sits’ posteisthiS characterIstIc or toxic contaminant.Nose: Four space. are provIded for entering pro code.. if moe are nasded: 113 Enter the firit three is described above; (2) Ent.r “000” in hiextreme right box of item IV.Ol13; and (33 Enter in the sp.ea provided on page 4, the line number and she eddltionsi code/si.2. PROCESS OESCRlrriONs Ill codi I. not lined tort process duat will be used, decribe the process In the apace provided an she fanmNOTE: HAZARDOUS WASTES DESCRIBED IV hM ThAN ONE EPA HAZARDOUS WASTE NUMBER - Hazardous wissee thiS can be described by

more titan on EPA Hazardous Waite Number shift be dseuibed on the form as follows:1. Select one of the EPA Hicerdosse Wwe Numbers and enter It In column A. On the eem. lists complete columns B.C. and 0 by sitimatinc the total annuilquantity of the wse and deanibing Mt due proasasas to be used to treat, store, end/ar dispose of the wwte.

2. in column A of the nici line etiew the other EPA $azetdoua Weds Number that out be used to døcribe SIt, were, In column O2l en that Una enter“included with above” and make no other snuhe on that lists.3, Repeat step 2 for ants other EPA Hazardous War, Number shot con be ‘e.d to acecribe he hazardous welts,£XAMPLS FOR COMPLETiNG ITEM IV (Mien,, In Ihve ntm7harr XI X2, X4 and X.’d be/owl - A facility will ist end dupes, of en estimated 900 pounds

Pif VIM Of dhlOiSts ShOvIstli flaiW liathit neining and Ilrdthin operation. In acelition, the facility will trees end dispose of three non—listed were.. Two wastesSr. corrosive only and there will be an .stlmes 90 peumb yew of a.di wane. The esIsere is antoiNe and ignitable and there will be an estimated100 ocunde oar veer of that e. Tieeun.fl tiiWb,ln an tncln..,ici and d#ssleslllbe In • tandflW-’ ‘ .“ -AEPA C.IJNIT

-d fiAi a5 5F$A —

PROCK.scoucIiZ (etarcOd.?— — — — — —..— — — I 1 1 I I— i-X1K054 900 P T03D80— — — — —

-— —— I FT I 1 — I t

—.

X-2D002 400 P T03.D80—

-.X3001 100 P ro3D8o— — — — — -—— .— — —

- r—- —i—--i - r --—

X.4 1 0 0 2includedwlthabcii’e

— — — —--

— — — —SPA Foam 351O.31g,

PAGE a OF 5 CONTINUC 0t PALE 3

03/23/1998 11:25 KEYSTONE \222?2436 P.01

\YSTONEENVIRONMDTAL RISOURCES, INC.

— 436 Scvcnth Avenue, Sute 1940,, PhtSbUVhfr PA 15219 - ——

TO: W/ C

__ __ ____

COMPANY NAME: /l/s.jssi ‘r&/_4c

COMPANY TELECOPIER NUMBER: 6/ —7L/ 70 —

FROM;.

Eçf4zjvSCc&/‘t/

Ntfl2ER OF PAGES TO FOLLOW: - -.

IF YOU DO NOT RECEIVE ALL MATERIAL TRANSMITTED, PLEASE CALL US ON:

(412) 227—2694.

OUR COPIER NUMBER IS (412) 227-2436. IT IS A PANAFAX UF-600AT.

SENT BY:

____________________

TIME: _.. DATE:

________

03/23/1966 11:26 KEYSTONE 22272436 P.024

KEYSTONERESOURCES, INC.

Phone: 412/227..2694 436 Seventh Avenue, SuIte 1940, Pittsburgh, PA 15219 Fax:412/227-2436

March 23, 1988

Mr. David 3. BockelmannHydrologistHazardous Waste DivisionMississippi Department of Natural

ResourcesBureau of Pollution Controlaox 103852380 Highway 80 WestJackson, Mississippi 39204



I have enclosed a copy of the revised page 1 of 5 of the Part AApplication for Koppers Grenada, Mississippi facility.

The change brings the volume of work in the impoundment into linewith the amount reported on Pages 1—2 and 1—3 of the November1986 Closure Plan for the surface impoundment/sprayfield.

If you need any additional information before Friday, March 25,please call my phone number and ask for Chuck Vita,

Thanks for your help.

Very truly yours,

Robert AndersonStaff Program Manager

RA/bjEnc losure

03/23/1996 11:26 KEYSTONEPlease print or type In the uneheded areas only \ ,i(EWI—Inerep.ssn *pecd to, elite type. i.e.. 12 ch&*rsn6nchJ.

FOR dFñCIAL USE ONLYlitToN OaflREdriiiEP

D7rn

f22272436 P.03

‘Perot Aooroved DM8 Plo. 158.380004

CoNtcts (banrei, dnjm, etc.)TANKWAflt na

SURFACE IMPOUNDMENT

INJECTION WELl,Ar4DrsL.L.

ANo Arn.ICATIONOCEAN DISPOSALSURFAcE IMPOUNDMENT

S. FACILITY HAS A RCRA PERMIT1*

F-’”- -ae

FORM

aOnna

a0

APPLI,.,

U.S. ENVIRONMENTAL PROtECTION AGENCYHAZARDOUS WASTE PERMIT APPLICATION

Consolidated PennlW Prcg,vn(This Information (a required under rct1on 3005 of flORA.)

COMMENTS

It FIRST OR REVISED APPLICATION1Piece an “X” in the eooroprieta box in A or B below (srtrk one box only) to indicate whether this Is the first application you etc submitting for your facility or arevised application. If thia Ii your first eppllcetlon ene U already know your facility’s EPA 1.0. Number, or if this lie revised eppilcation, enter your fecllity’sEPA i.D. Number in Item I above,r*inst APPLICATIöW(ptace “X” baa tprbj,7e the aflj’QPNQIJ dote) -

..-.—-

..-- - --i. EXISTING FACILItY (See tn,fruct(on. definIdon of “flUting” faeiifly, a.rsEW FACILtTY (Complete item below,)me Complete Item

FOR NEW FACILiTIES,PROVIDE THE DATE‘va

_____ ____

FOR EXISTING FACILITIES, PROVIDE THE Dan (yr, so, &day) r;.r(jMo: nAY frt,,mo,,iday)OPERA.

J

[I--i OPERATION BEGAN OR THE Data CONSTRUCTION COMMENCED

_____

ffJj TION PECAN OR ISf jj (Lime the boxes to the left)

______ ______

.,. gPEC-rao TO BEGINS%sfl. ‘. flt ill.

--.,. -.- .r ,AL.. ——n. - AFPI.IcATIVN (place an A below wi* complete item i noon)

I. FACILITY HAS INTERIM STATUS

!I!! PROCESSES — CODES AND DESIGN CAPACITIES —

A, PROCESS CODE — enter the code from the let Of process codes below that best describes each process to ba used et the facility Ten lines erO provided forentering codes. if more lines era needed, enter the code(s) In the spece provided. if a process will be used that Is not included in thö list of codas1below, thendescribe the procaee iincludlnp (a design cepeclty) in the specs provided on the form (irn lI1.C).B. PROCESS DESIGN CAPACItY — For each code entered In column A enter the cspaclty of the process.11. AMOUNT — Enter the emount.

2. UNIT OF MEASURE — Far eech amount entered In cOlumn 9(11, enter the code from the hat of unit measure codes below that describes the unit of• rseessrn used. Only the units of measure that ire listed below should be used.PRO’ APPROPRIATE UN1TS OF PRO. APPROPRIATE UNITS OFCESS MEASURE FOR PROCESS CESS MEASURE FOR PROCESSPROCES5

•. COOP flEN CAPACITY. PROCESS eOot OPSICiNS.APAdTY

-—

Eel GAL.LDNS On s.lTfleSea GALLONE OR L.ITERS502 CUSIC YARDS OR

CURIO METERS$04 GA,LONS OR I.ITERS

070 GALLONS OR LITERSDee - ACRE-FEET (the uohnne that

would eqvar one acre foedepth oHmic root) ORHECTARE+IETEIS

psi ACRES Off NictangeDel GALI,ONS PER DAY OR

L.ITERS PER DAYDEC DALLONS OR LITERS

IJNITOFMEASURE

COflE_.. - UNIT OF MEASUREUN ltOFMEASURE

Treetment:TANK Tot GALLONSPERDAYOR

LITERS PER PAYSURFACE IMflI4MOMKNT TOE GALLONS PER DAY ORLITERS PER DAYINCINERATOR TOS TONS PR HOUR ORMETRIC TONS PER HOURJGALLONS PEn HOUR ORLITERS PER HOUR

OTHER (time for phyafeal ch*mfcai, T04 I$ALLONS PER DAY ORthermal or biological trealrnent LITERS PER DAYproçnmea not ocewrrtng In tanks,eurrecejmpoundmenha or Inclner’alor,. DeignS, the procetllea fnthe wace provIded; item 111.04

UNIT OFMEASURE

CODEGALLOnS C s.,IttRSpEqoAy _,,V ACRE•FE$t ALITERS ,,L -‘lQNSPEAHOUR .,,,.,,,,,,..D HECTARMETER,,,,,,,,,....FCUSICYARDS V METRICTQNSPERHflI.zff W ACRES SCUSICM(TtRS C . OALLONSPCRNOUR E HECTARES 0GALLONSPERPAY U * 5,ITERSPERHOU* NEXAMPI.t FOR COMPLETING ITEM IN (thawn hi line numberw X- I and X’R below): A feclilty has two storage tenks, one tank can hold 200 Gallons end theother cen hold 400 gallons. The facIlIty aleo his an Incinerator that can burn up to 2Ogellons per hour.

UNITOFMEASURE

UNIT OF MEASURE CODE

. Z- •--1JLiN\\X\\\\\\\\\\\\\\\\\\\ZB, PROCESS DESIGN CAPACITY 0. PROCESS DESIGN CAPACITYCESS-

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x-:ro 20 ‘ . E 61 S04 52,360 C 7

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CONTINUE ON ht”tbSEPA Form 36104 (6-80) PAGE 1 OF 5

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-y

\ KEYSTONE\ENVlONMENTALRESOURCES.INC. ‘ir o is8s

436 Seventh Avenue, Suite 1940, Pittsburgh, PA

March 9, 1988 FEDERAL EXPRESS

Mr. David J. Bockelmann, HydrologistHazardous Waste DivisionMississippi Department of NaturalResourcesBureau of Pollution ControlBox 10385Jackson, MS 39209

Re: Koppers Company, Inc.,Grenada, Mississippi FacilityReport of FindingsSprayfield CharacterizationEPA ID No. MSD 007027543

Dear Mr. Bockelniann:

This letter is in response to your January 25, 1988 letter to Mr.J. D. Clayton of Koppers Company regarding comments on the“Report of Findings——Sprayfield Characterization” (April 1987),which was prepared by Keystone Environmental Resources, Inc.

This study was conducted to satisfy item 2 of the MississippiCommission on Natural Resources Order Number 1208-87. Althoughthis study was performed to demonstrate that KOOl sludge has notbeen applied to the sprayfield, Koppers asserts that sprayfieldsare not RCRA——regulated hazardous waste management units.

Koppers is challenging EPA’s assertion (adopted by MDNR) thatsprayfields are RCRA—regulated hazardous waste units on the basisthat proper notice and comment rulemaking procedures were notfollowed by the Agency prior to making this determination.Enclosed for your information is a copy of the notice letterwhich has been sent to the Agency advising of our intent to filesuit if EPA does not agree to alter its position. Accordingly,we have no alternative except to decline to perform theadditional sampling or respond to other comments requested inyour January 25, 1988 letter until this issue has been resolved.

Mr.--’David J. Bockelmann, Hydrbgist

Mississippi Department of Natural ResourcesMarch 9, 1988

If you need additional information or have any questions, pleasecall me.

Sincerely,

‘T• ,‘4cRobert J. AndersonStaff Program Manager


RJA / c rEnclosure

cc: J. H. Scarbrough, EPA IVJ. R. BatchelderJ. D. ClaytonJ. M. BlundonR. M. Morosky

\YSTONEEN’IONMENTAL RESOURCES. INC.

0 0WElL, G0TsHAL & MANGEs

A PARTNERSHIP INCLUDING PROFESSIONAl. CORPORATIONS

1615 L STREET. N.W.767 FIFTH AVENUE 1600 REPUBUcSANK CENTER

NEW YORk. N.Y. IoIS3 WASHINGTON. D.C. 20036700 LOUISIANA

(2121 310.8000 - (202) 682-7000 HOUSTON. TEXAS 77002TELECOPIER (212) 310-8007 TELECOPIER (2021 857-0939 (713) 546-5000

CABLE: WEGOMA 2021 8s7-os4o TELECOPIER(7I31 224-9511TELEX: ITT 424281 TELEX: ITT 440045 TELCX: ITT 4620144

ITT 423144wRITER5 DIRECT LINE

701 BRICKELL AVENUE1100 ONE MAIN PLACE

MIAMI. FLORIDA 33131DALLAS. TEXAS 75202 (202) 682—7210 1305) 577-3100

(214) 746-7700TELECOPIER: (305) 374-7(59TELECOPIER: (2141 746-7777 February 26, 1988

VIA MESSENGER

Honorable Lee M. ThomasAdministratorUnited States Environmental Protection Agency401 M Street, S.W.Room W—1200Washington, D.C. 10540

Re: Notice of Citizen’s Suit-

Dear Mr. Thomas: -

Pursuant to Section 7002 of the ResourceConservation and Recovery Act (“RCRA”), 42 U.S.C. § 6972 and40 C.F.R. Part 254, the American Wood Preservers Institute(“AWPI”) and Koppers Company, Inc. (“Koppers”) notify you oftheir intention to bring suit for failure to perform anondiscretionary duty under 42 U.S.C. §6921(b). Brieflystated, EPA is enforcing, by means of an agency memorandum,a new rule which subjects previously unregulated sprayirrigation fields managing nonhazardous wastewater to thefull panoply of RCRA regulatory requirements for operationor closure of hazardous waste facilities. In so doing, EPAhas violated the explicit directives of both RCRA and theAdministrative Procedure Act (“APA”) by failing to complywith the requirements for designating wastes as hazardous.To subject an entire industry to the staggering costs ofRCRA compliance and in some instances enforcementproceedings by dispensing with the procedural safeguards andreasoned inquiry required for such decisions isindefensible.

Accordingly, AWPI and Koppers urge the Agency tohalt processing RCRA Part B permits for operation or closureof spray irrigation fields managing nonhazardous wastewaterand to dismiss enforcement proceedings seeking to impose

WElL, G0T5HAL & MANGES

Honorable LeeM. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page 2

-

RCRA requirements on operation or closure of such sprayfields until completion of a rulemaking proceedingdesignating wastewater as a hazardous waste. Absent relieffrom the Agency, we will have no choice but to pursue ourclaim in the district court.

Background

A. EPA Rulemaking

EPA honored the requirements of RCRA and the APAin May 1980, when it first determined through rulemakingthat bottom sediment sludgá from wood preserving processesthat use creosote or pentachiorophenol (hazardous waste No.KOOl) should be regulated as a hazardous waste, but that theprocess wastewater from treatment systems of such operationsshould not. See 45 Fed. Reg. 74,884, 74,889 (1980). Basedon this determination, many wood preserving plants lawfullyconcluded that no RCRA permit was required for the use ofspray irrigation fields as the last step in the managementof the nonha.zardous wastewater.

B. EPA Memoranda

In total disregard of its 1980 rulemaking, EPA hasattempted, through a series of internal memoranda, toabrogate its previous rulemaking on wastewater and insteadunilaterally impose RCRA regulation on facilities handling anonhazardous waste. For example, in November 1984, theAgency issued a memorandum stating that any facilitymanaging wastewater from wood preserving operations,including spray irrigation units, potentially could besubjet to the permitting requirement of section 3001 ofRCRA. Without any substantiation, EPA baldly asserted thatbiological action on land similar to that operating insurface impoundments could generate a “biomass material” atthese facilities which it presumed to be KOOl bottomsediment sludge. In such circumstances, owners of thesefacilities would be managing a listed hazardous waste andtherefore would require a RCRA permit for operation orclosure.

1. EPA memorandum from John H. Skinner, Director, Office ofSolid Waste to James H. Scarbrough, Chief, ResidualsManagement Branch, Region IV (November 23, 1984).

WElL, GoTsi-IAL & MANGES

Honorable Lee M. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page3

Moreover, EPA effectively denied companies theopportunity to demonstrate the absence of KOOl bottomsediment sludge in a spray irrigation field. Although theNovember 1984 memorandum ostensibly allowed owners offacilities to demonstrate that no KOOl sludge was formed inits spray field, the Agency did not set out an approvedmethodology by which facilities could do so. Thus, afacility owner could only rebut EPA’s regulatory presumptionat the whim of the Agency.

Similarly, in July 1985, the Agency issued anothermemorandum that simply concluded that spray irrigationfields managing astewater automatically were subject toRCRA regulation. As with the earlier November 1984memorandum, EPA merely restated its speculative conclusionsconcerning the presence of biomass/sludge at.these fieldswithout any supporting data.

C. EPA Enforcement

EPA has filed enforcement proceedings againstseveral wood preserving companies operating spray irrigationfields based solely on the purported authority of its ownmemoranda and the unsubstantiated theory articulatedtherein. Because the memoranda have never been published inthe Federal Register, individual wood preserving companieshad no prior notice of EPA’s reversal and no meaningfulopportunity to object or voluntarily comply with thememoranda. Instead, these companies faced protractedlitigation and the threat of penalties in order to challengeEPA’s illegal rule.

Further compounding this injury, the Agency isprocessing permit applications for operation or closure ofspray irrigation fields, thereby imposing the burden of RCRAcompliance costs on these facilities. The process of

2. EPA memorandum from John H.. Skinner, Director, Office ofSolid Waste to James H. Scarbrough, Chief, ResidualsManagement Branch, Region IV (July 17, 1985).

3. While objecting to EPA’S assertion of jurisdiction overspray. irrigation fields, many wood preserving companies havefiled permit applications protectively, to avoidjeopardizing their operations. See section 213(a) (2) of the

WElL, G0TSHAL & MANGES

Honorable Lee M. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page4

obtaining a RCRA hazardous waste permit alone can consumeseveral years and hundreds of thousands of dollars perfacility. In addition, facilities could be subject toextensive design and performance requirements for operationand closure, in some instances fo a period of at least 30years beyond their active life. These crushing coststhreaten the economic viability of many wood preservingcompanies. Moreover, failure to comply could result in EPAordering the facility to shut down.

D. Industry Response

In accordance with RCRA regulations and inresponse to the uncertainty generated by EPA’S memoranda,AWPI filed a petition with EPA on January 10, 1985, seekingreconsideration of the decision to classify spray irrigationfields managing nonhazardous materials as hazardous wastemanagement facilities. The EPA has failed to act on thispetition. In 1986, AWPI further requested a meeting withsenior officials in the Office of Solid Waste to discuss theregulatory status of. spray irrigation fields in the contextof EPA’S forthcoming rulemaking on the regulation ofadditional wastes from wood preserving operations. TheAgency rejected any such meeting.

AWPI also challenged EPA’s enforcement of itsillegal memoranda in an administrative proceeding. See, InRe Brown Wood Preserving Company, Inc., RCRA 84-l6--R. Inthat case, Athuinistrative Law Judge Thomas B. Yost found theAgency’s attempted regulation of spray irrigation fieldsillegal and prohibited further enforcement proceedings. Inreaching these conclusions, Judge Yost found that (1) theinternal agency memoranda, under which EPA assertedjurisdiction over spray irrigation fields managingnonhazardous wastewater, were invalid because the Agencyfailed to comply with the requirements of RCRA and the APA;and (2) the EPA could not rely on the “undocumented theory”articulated in these memoranda in enforcement proceedings.The EPA’s appeal of that decision is pending. Judge Yost,

Hazardous and Solid Waste Amendments of 1984, 42 U.S.C.6925(e)(2). That provision required owners of hazardouswaste facilities to submit Part B permit applications byNovember 8, 1985. Failure to do so could result in theAgency’s closing down the facility.

WiL, G0TsHAL & MANGEs

Honorable Lee 14. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page5

however, has resisted treating his opinion as determinativein cases involving similarly—situated facilities.Furthermore, in light of the Agency’s position that ownersand operators of spray irrigation fields managingnonhazardous wastewater have an independent obligation tocomply with the RCRA permitting process, administrativerelief clearly is inadequate.

E. Conclusion

- Although the only opinion reviewing EPA’Senforcement of the memoranda at issue here has declared theAgency’s conduct illegal, EPA persists in relying on thesememoranda to impose RCRA regulation for operation or closureon spray irrigation fields managing norihazardous wastewaterto the detriment of the wood preserving industry.Accordingly, we urge the Agency to withdraw these illegalmemoranda immediately until completion of a rulemakingconcerning the regulation of wastewater as a RCRA hazardouswaste.

Very truly yours,

44David R. BerzStanley 14. Spracker

Counsel for AWPI andKoppers Co., Inc.

\YSTONE\Et1ONMENTAL RESOURCES, INC.

436 Seventh Avenue, Suite 1948, Pittsburgh, PA

March 9, 1988 FEDERAL EXPRESS

- Mr. David J. Bockelmann, HydrologistHazardous Waste DivisionMississippi Department of Natural

-

Resources3-JO Bureau of Pollution Control

Box 10385Jackson, MS 39209

Re: Koppers Company, Inc.,Grenada, Mississippi FacilityReport of FindingsSprayfield CharacterizationEPA ID No. MSD 007027543

Dear Mr. Bockelmanri:

This letter is in response to your January 25, 1988 letter to Mr.J. D. Clayton of Koppers Company regarding comments on the“Report of Findings——Sprayfield Characterization” (April 1987),which was prepared by Keystone Environmental Resources, Inc.

This study was conducted to satisfy item 2 of the MississippiCommission on Natural Resources Order Number 1208-87. Althoughthis study was performed to demonstrate that KOOl sludge has notbeen applied to the sprayfield, Koppers asserts that sprayfieldsare not RCRA——regulated hazardous waste management units.

Koppers is challenging EPA’s assertion (adopted by MDNR) thatsprayfields are RCRA—regulated hazardous waste units on the basisthat proper notice and comment rulemaking procedures were notfollowed by the Agency prior to making this determination.Enclosed for your information is a copy of the notice letterwhich has been sent to the Agency advising of our intent to filesuit if EPA does not agree to alter its position. Accordingly,we have no alternative except to decline to perform theadditional sampling or respond to other comments requested inyour January 25, 1988 letter until this issue has been resolved.

0RE C E ! Efl

10 1988

(fl Page 2&) David J. Bockelmann, HydI’ogist

Mississippi Department of Natural ResourcesMarch 9, 1988

If you need additional information or have any questions, pleasecall me.

Sincerely,

A ‘- -i ‘—



RJA /crEnclosure

cc: J. H. Scarbrough, EPA IVJ. R. BatchelderJ. D. ClaytonJ. M. BlundonR. M. Morosky

\YSTONE\ENIO’MENTAL RESOURCES. INC.

0 0WEw, G0TsHAL & MANGES

A PARTNCPSM)P INCI.UOP4G PSOTCSSIONAL CORPORATIONS

1615 L STREET. N.W.767 FIFTH AvENUE 1600 REPUBLICSANK CENTERNEW YORK. N.Y. WAS)-)INGTON. D.C. 20038

700 LOUISIANA12)2) 3io- (202) 682-7000 - HOUSTON, TEXAS 77002IELECOPIER: (2)2) 310-8007 TCLECOPIER (202) 857-0939 1713 546-5000CABLE: WEGOMA (202) 857-0940 TELECOPIER: (7)31 224-9511TELEX: ITT 42428)

TELEX: ITT 440045 TELEX: ITT 4620144ITT 4IWRITERS DIRECT LINE

701 BRICKELL AVENUE1100 ONE MAIN PLACEMIAMI. FLORIDA 33131DAU.As.-rEXAS 7saoa (202) 682—7210 (305) 377-3)001214) 746-7700

TELECOPIER)3051 314-7)59TELECOPIERI2I4) 746-7777 February 26, 1988

VIA MESSENGER

Honorable Lee N. ThomasAdministratorUnited States Environmental Protection Agency401 M Street, S.W.Room W—1200Washington, D.C. 10540

Re: Notice of Citizen’s Suit

Dear Mr. Thomas:

Pursuant to Section 7002 of the ResourceConservation and Recovery Act (“RCRA’9, 42 U.S.C. § 6972 and40 C.F.R. Part 254, the American Wood Preservers Institute(“AWPI”) and Koppers Company, Inc. (“Koppers”) notify you oftheir intention to bring suit for failure to perform anondiscretionary duty under 42 U.S.C. §6921(b). Brieflystated, EPA is enforcing, by means of an agency memorandum,a new rule which subjects previously unregulated sprayirrigation fields managing nonhazardous wastewater to thefull panoply of RCRA regulatory requirements for operationor closure of hazardous waste facilities. In so doing, EPAhas violated the explicit directives of both RCRA and theAdministrative Procedure Act (“APA”) by failing to complywith the requirements for designating wastes as hazardous.To subject an entire industry to the staggering costs ofRCRA compliance and in some instances enforcementproceedings by dispensing with the procedural safeguards andreasoned inquiry required for such decisions isindefensible.

Accordingly, AWPI and Koppers urge the Agency tohalt processing RCRA Part B permits for operation or closureof spray irrigation fields managing nonhazardous wastewaterand to dismiss enforcement proceedings seeking to impose

WElL, G0TSHAt. & MANGEs

Honorable Lee N. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page 2

- -

RCRA requirements on operation or closure of such sprayfields until completion of a rulemaking proceedingdesignating wastewater as a hazardous waste. Absent relieffrom the Agency, we will have no choice but to pursue ourclaim in the district court.

Background

A. EPA Rulemaking

EPA honored the requirements of RCRA and the APAin May 1980, when it first determined through rulemakingthat bottom sediment sludge from wood preserving processesthat use creosote or pentachlorophenol (hazardous waste No.KOOl) should be regulated as a hazardous waste, but that theprocess wastewater from treatment systems of such operationsshould not. See 45 Fed. Reg. 74,884, 74,889 (1980). Basedon this determination, many wood preserving plants lawfullyconcluded that no RCRA permit was required for the use ofspray irrigation fields as the last step in the managementof the nonhazardous wastewater.

B. EPA Memoranda

In total disregard of its 1980 rulemaking, EPA hasattempted, through a series of internal memoranda, toabrogate its previous rulemaking on wastewater and insteadunilaterally impose RCRA regulation on facilities handling anorihazardous waste. For example, in November 1984, theAgency issued a memorandum stating that any facilitymanaging wastewater from wood preserving operations,including spray irrigation units, potentially could besubjet to the permitting requirement of section 3001 ofRCRA. Without any substantiation, EPA baldly asserted thatbiological action on land similar to that operating insurface impoundments could generate a “biomass material” atthese facilities which it presumed to be KOOl bottomsediment sludge. In such circumstances, owners of thesefacilities would be managing a listed hazardous waste andtherefore would require a RCRA permit for operation orclosure.

1. EPA memorandum from John H. Skinner, Director, Office ofSolid Waste to James H. Scarbrough, Chief, ResidualsManagement Branch, Region IV (November 23, 1984).

WL,GoTsHAL & MANGES 0Honorable Lee M. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page3

Moreover, EPA effectively denied companies theopportunity to demonstrate the absence of KOOl bottomsediment sludge in a spray irrigation field. Although theNovember 1984 memorandum ostensibly allowed owners offacilities to demonstrate that no KOOl sludge was formed inits spray field, the Agency did not set out an approvedmethodology by which facilities could do so. Thus, afacility owner could only rebut EPA’s regulatory presumptionat the whim of the Agency.

Similarly, in July 1985, the Agency issued anothermemorandum that simply concluded that spray irrigationfields managing ‘astewater automatically were subject toRCRA regulation. As with the earlier November 1984memorandum, EPA merely restated its speculative conclusionsconcerning the presence of biomass/sludge at these fieldswithout any supporting data.

C. EPA Enforcement

EPA has filed enforcement proceedings againstseveral wood preserving companies operating spray irrigationfields based solely on the purported authority of its ownmemoranda and the unsubstantiated theory articulatedtherein. Because the memoranda have never been published inthe Federal Register, individual wood preserving companieshad no prior notice of EPA’s reversal and no meaningfulopportunity to object or voluntarily comply with thememoranda. Instead, these companies faced protractedlitigation and the threat of penalties in order to challengeEPA’s illegal rule.

Further compounding this injury, the Agency isprocessing permit applications for operation or closure ofspray irrigation fields, thereby impoing the burden of RCRAcompliance costs on these facilities. The process of

2. EPA memorandum from John H. Skinner, Director, Office ofSolid Waste to James H. Scarbrough, Chief, ResidualsManagement Branch, Region IV (July 17, 1985).

3. While objecting to EPA’S assertion of jurisdiction overspray irrigation fields, many wood preserving companies havefiled permit applications protectively, to avoidjeopardizing their operations. See section 213(a) (2) of the

WEL, G0TSHAL & MANGEs flHonorable Lee M. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page4

obtaining a RCRA hazardous waste permit alone can consumeseveral years and hundreds of thousands of dollars perfacility. In addition, facilities could be subject toextensive design and performance requirements for operationand closure, in some instances for a period of at least 30years beyond their active life. These crushing coststhreaten the economic viability of many wood preservingcompanies. Moreover, failure to comply could result in EPAordering the facility to shut down.

D. Industry Response

In accordance with RCRA regulations and inresponse to the uncertainty generated by EPA’S memoranda,AWPI filed a petition with EPA on January 10, 1985, seekingreconsideration of the decision to classify spray irrigationfields managing northazardous materials as hazardous wastemanagement facilities. The EPA has failed to act on thispetition. In 1986, AWPI further requested a meeting withsenior officials in the Office of Solid Waste to discuss theregulatory status of. spray irrigation fields in the contextof EPA’S forthcoming rulemaking on the regulation ofadditional wastes from wood preserving operations. TheAgency rejected any such meeting.

AWPI also challenged EPA’s enforcement of itsillegal memoranda in an administrative proceeding. See, InRe Brown Wood Preserving Company, Inc., RCRA 84-16-R. Inthat case, Administrative Law Judge Thomas B. Yost found theAgency’s attempted regulation of spray irrigation fieldsillegal and prohibited further enforcement proceedings. Inreaching these conclusions, Judge Yost found that (1) theinternal agency memoranda, under which EPA assertedjurisdiction over spray irrigation fields managingnonhazardous wastewater, were invalid because the Agencyfailed to comply with the requirements of RCRA and the APA;and (2) the EPA could not rely on the “undocumented theory”articulated in these memoranda in enforcement proceedings.The EPA’s appeal of that decision is pending. Judge Yost,

Hazardous and Solid Waste Amendments of 1984, 42 U.S.C.6925(e)(2). That provision required owners of hazardouswaste facilities to submit Part B permit applications byNovember 8, 1985. Failure to do so could result in theAgency’s closing down the facility.

WaiL, G0TSHAL & MANGEs

Honorable Lee 11. ThomasAdministratorUnited States Environmental Protection AgencyFebruary 26, 1988Page5

however, has resisted treating his opinion as determinativein cases involving similarly—situated facilities.Furthermore, in light of the Agency’s position that ownersand operators of spray irrigation fields managingnonhazardous wastewater have an independent obligation tocomply with the RCRA permitting process, administrativerelief clearly is inadequate.

E. Conclusion

Although the only opinion reviewing EPA’Senforcement of the memoranda at issue here has declared theAgency’s conduct illegal, EPA persists in relying on thesememoranda to impose RCRR regulation for operation or closureon spray irrigation fields managing nonhazardous wastewaterto the detriment of the wood preserving industry.Accordingly, we urge the Agency to withdraw these illegalmemoranda immediately until completion of a rulemakingconcerning the regulation of wastewater as a RCRA hazardouswaste.

Very truly yours,

J

r4pjj

David R. BerzStanley N. Spracker

Counsel for AWPI andKoppers Co., Inc.

C) 0MISSISSIPPI DEPARTMENT OF NATURAL RESOURCES “I

Bureau of Pollution Control 4&HAj

Jackson Mssippi 39209(601) 961 5171

March 4, 1988

Mr. James H. Scarbrough, P. E., ChiefResiduals Managent BranchEnvironmental Protection Agency345 Courtland Street, N. E.Atlanta, Georgia 30365

Dear Mr. Scarbrough:

Re: Transmittal of DocumentsReceived fromKoppers Company, Inc.Grenada, MississippiMSD007027543

Enclosed is the following document for your review:

1.) 1987 Annual RCRA Groundwater Monitoring Summaryand accompanying letter addressed to Mr. JamesHardage from Mr. Robert J. Anderson, datedFebruary 26, 1988.

If you should have any questions or require anyadditional information, please contact me at (601)961—5171.

Sincerely,

David J. BockelmannHazardous Waste Division

DJB : mes

Enclosure

February 26, 1988

Mr. Jim HardageMississippi Department of Natural ResourcesBureau of Pollution ControlP.O. Box 10385Jackson, MS 39209

Dear Mr. Hardage:

FEB29 1998Dept. of NaturjBure. of PoI!uj, Corru,

On February 11, 1988, I called you concerning the status of the1987 Biennial Hazardous Waste Report since our Koppers’ Grenada,Mississippi facility had not received these report forms. At thattime you informed me that U. S. EPA was late in sending the Biennialforms to the State and the Mississippi DNR was going to extend thereporting deadline to April 1, 1988. Since the Grenada facility hadnot received the forms as of today, I assume the April 1st filing dateis still appropriate. If not please call me at (501) 945-4581.

Sincerely,

David L. KingRegional EnvironmentalCoordinator

cc. Rob AndersonJ. D. ClaytonChuck Vita

cthL I&L-- /‘ -

t± :. :Ji::4 dA I I--1 1L 4c’ T) //

‘212/

REGIONAL OFFICEP.O. Box 15490

North Little Rock, AR 72231

0 0\YSTONE

\ENIONMENTAL RESOURCES, INC.

436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219

February 26, 1988

Mr. Jim HardageMississippi Department of Natural ResourcesBureau of Pollution ControlP.O. Box 10385Jackson, MS 39209

Dear Mr. Hardage:

RECEIVFfl

FE629 1968Dept. of Natura,8ure of Polgu,0Contr

On February 11, 1988, I called you concerning the status of the1987 Biennial Hazardous Waste Report since our Koppera’ Grenada,Mississippi facility had not received these report forms. At thattime you informed me that U. S. EPA was late in sending the Biennialforms to the State and the Mississippi DNR was going to extend thereporting deadline to April 1, 1988. Since the Grenada facility hadnot received the forms as of today, I assume the April 1st filing dateis still appropriate. If not please call me at (501) 945-4581.

cc. Rob AndersonJ. D. ClaytonChuck Vita

David L. KingRegional EnvironmentalCoordinator

( [j’(’rJ? 7r

0\XYSTONE

\IONMENTAL RESOURCES, INC.

436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219

Dv:s:c\ CF SCL; WAS

REV”/t: BV

r)h E

Sincerely,

F J -‘L-j_

REGIONAL OFFICEP.O. Box 15490

North Little Rock, AR 72231

ovYs0

TONE\NVIONMENTAL RESOURCES, INC.

436 Seventh Avenue, Suite 1940, Pittsburgh, PA 15219 j 2 9 1988

February 26, 1988

Mr. James HardageMississippi Department of Natural

ResourcesBureau of Pollution ControlBox 10385Jackson, MS 39209

Re: Koppers Company, Inc.Grenada, MS FacilityAnnual Groundwater ReportEPA ID No. MSD 007 027 543

Dear Mr. Hardage:

The Annual RCRA Groundwater Monitoring Summary for 1987 isattached for the Koppers Company, Inc. Grenada, Mississippifacility. As you discussed in a February 2, 1988 phoneconversation with Mr. Dave King of Keystone EnvironmentalResources, Inc., the date for filing the Annual Generator andFacility Reports has been extended to April 1, 1988. This isbeing done because the appropriate forms have not yet beenreceived by the facility.

If you have any questions or would like additional information,please call me.

Sincerely,



RJA / crAttachment

cc: J. D. ClaytonJ. R. BatchelderJ. A. Quagliotti (w/o attachment)

.c:t)

C C

/\

Y

0 0MISSISSIPPI DEPARTMENT OF NATURAL RESOURCES

Bureau of Pollution ControlP.O. Box 10385 !/I

Jackson Mississippi 39209

February 11, j98

Mr. Robert J. AndersonKeystone Environmental Resources, Inc.436 Seventh Avenue, Suite 1970Pittsburgh, Pennsylvania 15219

Dear Mr. Anderson:

Re: Submittal of a Groundwater Samplingand Analysis PlanBoiler Ash Disposal AreaKoppers Company, Inc.Grenada, Mississippi

I have recently reviewed the document entitled “Closure Plan for the Ash WastePile as a Landfill Disposal Site” which we received on December 1, 1987. It isindicated in this document that a Groundwater Sampling and Analysis Plan willbe submitted prior to closure of the site and that the schedule for closurewill be based upon EPA’s ruling on Kopper’s petition to delist the boiler ashas a hazardous waste. Until such time as EPA rules on Koppers delistingpetition, the Bureau must consider the boiler ash disposal area to be in adetection monitoring status. It is therefore required that a GroundwaterSampling and Analysis Plan be submitted within 30 days of the receipt of thisletter. This plan should include an accelerated schedule of sampling with onesampling event per month for a four month period. These sampling events shouldbe scheduled to begin immediately after the submittal of the GroundwaterSampling and Analysis Plan. This data is required in order to establishbackground groundwater quality in the vicinity of the ash disposal area and toperform statistical analysis to determine if there has been an impact on thegroundwater from contamination.

If you should have any questions or require any additional information, pleasecontact me at (601) 961—6171.

Sincerely,

David J. Bockeliuann, HydrologistHazardous Waste Division

DB:cm O SCL.Dcc: Mr. J. D. “Rook” Clayton, Plant Manager

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FILE Cop’1,

January 25, 1988

J f) Vpakfl Clmtn, Plant NanacserKoçcrs Ctpariy, Inc.Oox 160Tin Pi.att, flissInsiri 38960

flcr Mr. Clayton:

Re Reprt of FlrtlingsSpray ?irZñ £laracteriaticmKoppera Cayan”, Inc.Grenada, Miissbaiji

I have recently ie1 the above referenced &x,wmnt for iqersCrçr, Inc. whict we receivnd on 7’prii 27, 1987. It is theci”-n :i, of the Bureau that this dcctnnt does not satisfy jt-in1:nd..d 2Y.li-jnse of t:33nr::t IYR -J’z-t the spray field at rnp>rr’Grenada pLtnt is not a tC v2-’c hazardous waste Th

l4JL”q i list Of cXflrEnt$ 1. :3: to this decisict:

1. Trçci.inctrw±nt putr intake. The rc!txtt :.‘ that t1w nrcintake is :t s >rointo1y 1.5 tc 2 itaet b J’.; the!s-cuflrnt uter lcd 2 the u2xv’ layer is at 1isrt 5Leet below the water level and .tt the nw Cr: : 3’ at an

te of 120 N:3 >r rdnute for 3 minuteperiock. ‘1t fact tha. the pivxp intake does not nrwe i:ditct r¼nt,ctt with 1t.. iuckw layer iS not concideraM tn be&!equate nrcnf that ‘ane of the aludqe raterfa! will not bt

drawn into the intake and €qi.ied to the £,tirs’ Lield.

2 • ljtewater tnfluent to tha zpnw fi. ‘Ic • The sarplos of theto the •‘::‘: i: id wore ajarently

i3tr at ons of the noz1es located ilonqthe iniCe of the inpounc)nent Lcnkr. It is annxi thatthe Tca:Cn’-nt ovapontion :rz1ez-: are part of the rcatwsysten as th” :les at the *pray fleldy hczs.a’!vcr, this isnot 2’ttec1 or dectinented in the report.

3. Pprzvt :c]d oi1 cz1et. The’ report nt.atrs that ..,soilrrq)e tnx the surfec to a døpth of 6 tncheD were

• .. Ttro;tu rcnreT4entanv ii haaqe wa onsite. when the spray ! told roil arple: were nnllcted andIsixs etatec3 t2Mt tIw top 1 to 2 inch ohl/orgaT%Ic layer wai

s. .7. D. WpcckW Cla’.’tonPage -2—

not i.’xhxIed in the soil sample coileetton. If the: top to

2 inch onil/crganic layer it-i conüden4d to be aeperite ircz

the underlvincr soil layer, then it chou?c! be sietp1xI as a

aopesatQ arzl discrete lav:r.

4. Analytical data — £‘oil, sludge end wastewater ualytis(Table 3-2 .and Appnii; B). Usinç the dat.!t pretente8 inpendr B, the cacentration of Bn.nzn(n)pyrnne for theavtrticj& soil Eat!3ln licted in Table 3—2 rhould be 238 • Suqftcg ant! not 25.0 uq/l:cj,

ift the conclusion of the report it is stated that 01W1 dataindicate that concentraticais in the soil an in fact lc%’r

than concentrations in the wastewater. Other data indicatethat where soil ccrzcentratiorn are greater, the dff±r;’ax::’

is only ver slight*. An e.acdwtinn of Tnhln 3—2 rtnn’that 3 ont of 17 of the nolynuclear arcantic hydnrar&ts(PN1’s) en] 7 out of 12 of the pherolic cctçounds analyzed

for had higher ocwsentration levels in the averaged soilsals’ than in the want..47ater rarqie. This reprerentcslightly over 3fl of the constituents i:’z’ for wttth

higher concentration levelt in the soil sañe than

in ti+ tr3stc’%iater sa’tçln (the malority - base ?x i: : o 2ardors of magnitude higher). This tuld SeCt to -

that scre acxtzrn.ilation is taking place within thi? spre.’-’

vojle.

5. Visual thnen’aticn of the spray tield. The :epntt states

that “...feld rtnesvation &rinq :cfpli;;r; JaIUtnd theabw?ncvi of any sludge layer or ether visual contaninationwithin Ur limits of the spray fIeld’t On Decat?r 15,1987, ttrmau repzesentativc-s Kim Ehret and I visited theKoppera’ Grenada facility. C vinsing the spray field, enoted that the vegetation around the spray field non lee wise

visibly stained a derker color than the surrc*u4ingV’cj(tüt±t in the area. A visual exaninatlon of the topsoil/orqanic layer s1x*ex! it to be a vr’r dark, sliqhtly

silty organic soil (the ioursWift tlwkye hi descrIbed a

consisting of “. . .&.rk soft slit and clay sediments withsatz* enjanic debris. . .9. Th staIned wqctat ion and the

aimi]aritv in the denerlpUona of the spray field eoi ant!the in>zirôrcnt aiwige nit! seeS to indicate that the

rx>nEtibiit’t for sludge çplicaticwi and/cr r;ludge generation

at the spray field does exist.

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Koppers Inc - Mississippi Department of Environmental Quality

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Transcript of Koppers Inc - Mississippi Department of Environmental Quality